Nhóm 22 - Maltodextrin Từ Khoai Lang

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    Nhom 22 1 Lp: Hc11Tp

    Trng i hc Bch Khoa Tp.HCM

    Khoa Kthut Ho hc

    Bmn: Cng nghThc phm

    Bo co mn Cng nghchbin thc phm

    ti:

    CNG NGHSN XUT

    MALTODEXTRIN TKHOAI LANG

    CBGD: PGS.TS L VN VIT MN

    SVTH: Trn Ngc Huy_61101387

    Hong ThYn Phng_61102647

    HThQuyn_61102808

    Nguyn Ngc HuTin_61103569

    Nguyn ThKim Tin_61103601

    Nm hc: 20132014

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    i

    Mu

    Maltodextrin, l mt polysaccharide gm cc gc D glucose lin kt vi nhau bng

    lin kt 14 glycoside, cng thc phn t(C6H10O5)n.2H2O, l sn phm tsthuphn tinh

    bt khng hon ton vi chsDE nm trong khong t420.

    Maltodextrin tan hon ton trong nc, c chuyn ho trong c thtng tnh tinh bt,

    do maltodextrin thch hp cho bnh nhn mc bnh tiu ng. Ngoi ra maltodextrin l cht

    c rt t v thm ch khng c vngt, khng c mi tinh bt v khng nh hng n mi vcc

    cht khc (Morris, 1984).

    V nhng c im c bit ni bt nh trn, nn hin nay maltodextrin c nghin cu v

    ng dng nhiu trong ngnh cng nghthc phm.

    Bng vic so snh hai qui trnh cng nghcng sn xut Maltodextrin, chn ra qui trnh

    thch hp, m bo cht lng sn phm cng nh ti u vkinh t(chi ph sn xut, gi thnh

    sn phm)

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    ii

    MC LC

    I. NGUYN LIU................................................................................................................. 11. Khoai lang.................................................................................................................... 11.1. Carbohydrate .............................................................................................................. 11.2. Tinh bt ...................................................................................................................... 11.3. ng ......................................................................................................................... 51.4. Cht x....................................................................................................................... 61.5. Protein ........................................................................................................................ 61.6. Vitamin ....................................................................................................................... 71.7. Khong ....................................................................................................................... 72. Enzyme......................................................................................................................... 83. Cc nguyn liu ph.................................................................................................. 103.1. Nc ......................................................................................................................... 103.2. CaCl2, NaOH, HCl, than hot tnh ........................................................................... 11

    II. QUI TRNH CNG NGH........................................................................................ 131. Qui trnh cng ngh1............................................................................................... 131.1 S ......................................................................................................................... 131.2 Thuyt minh qui trnh................................................................................................ 15

    2.

    Qui trnh cng ngh2............................................................................................... 31

    2.1 S khi ................................................................................................................. 312.2 M tqui trnh ........................................................................................................... 323. So snh hai qui trnh cng ngh............................................................................... 38

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    iii

    III. SN PHM................................................................................................................. 391. Tnh cht vt l ca Maltodextrin........................................................................... 392. Cc chtiu cht lng sn phm............................................................................ 40

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    iv

    Danh mc hnhHnh 1.Cu to tinh bt..................................................................................................................... 2Hnh 2.Cu trc phn tAmylose...................................................................................................... 2Hnh 3.Cu trc Amylopectin............................................................................................................ 3Hnh 4.Phn ng thy phn tinh bt.................................................................................................. 3Hnh 5.Thit bloi btp cht...................................................................................................... 15Hnh 6.Thit bra.......................................................................................................................... 16Hnh 7.Thit bct........................................................................................................................... 17Hnh 8.Thit bnghin rng............................................................................................................. 18Hnh 9.Thit bhha Jet-cooker................................................................................................... 21Hnh 10.Thng dch ha.................................................................................................................. 22Hnh 11.S hha-dch ha....................................................................................................... 23Hnh 12.Thit bty mu bng than hot tnh................................................................................. 25Hnh 13.M hnh lc khung bn...................................................................................................... 27Hnh 14.Hnh nh thc tca thit blc khung bn...................................................................... 27Hnh 15.S thit bc c ng tun hon................................................................................... 28Hnh 16.S thit bsy................................................................................................................ 30Hnh 17.C chtrao i ion............................................................................................................ 35Hnh 18.Thit btrao i ion........................................................................................................... 35Hnh 19.M hnh c c bng membrane....................................................................................... 37Hnh 20.Hthng thm thu thc ttrong cng nghip............................................................... 37

    http://c/Users/Tran/Desktop/new/Nh%C3%B3m%2022%20-%20Maltodextrin%20t%E1%BB%AB%20khoai%20lang.docx%23_Toc388163723http://c/Users/Tran/Desktop/new/Nh%C3%B3m%2022%20-%20Maltodextrin%20t%E1%BB%AB%20khoai%20lang.docx%23_Toc388163723http://c/Users/Tran/Desktop/new/Nh%C3%B3m%2022%20-%20Maltodextrin%20t%E1%BB%AB%20khoai%20lang.docx%23_Toc388163723http://c/Users/Tran/Desktop/new/Nh%C3%B3m%2022%20-%20Maltodextrin%20t%E1%BB%AB%20khoai%20lang.docx%23_Toc388163723http://c/Users/Tran/Desktop/new/Nh%C3%B3m%2022%20-%20Maltodextrin%20t%E1%BB%AB%20khoai%20lang.docx%23_Toc388163723http://c/Users/Tran/Desktop/new/Nh%C3%B3m%2022%20-%20Maltodextrin%20t%E1%BB%AB%20khoai%20lang.docx%23_Toc388163723http://c/Users/Tran/Desktop/new/Nh%C3%B3m%2022%20-%20Maltodextrin%20t%E1%BB%AB%20khoai%20lang.docx%23_Toc388163723http://c/Users/Tran/Desktop/new/Nh%C3%B3m%2022%20-%20Maltodextrin%20t%E1%BB%AB%20khoai%20lang.docx%23_Toc388163723http://c/Users/Tran/Desktop/new/Nh%C3%B3m%2022%20-%20Maltodextrin%20t%E1%BB%AB%20khoai%20lang.docx%23_Toc388163723http://c/Users/Tran/Desktop/new/Nh%C3%B3m%2022%20-%20Maltodextrin%20t%E1%BB%AB%20khoai%20lang.docx%23_Toc388163723http://c/Users/Tran/Desktop/new/Nh%C3%B3m%2022%20-%20Maltodextrin%20t%E1%BB%AB%20khoai%20lang.docx%23_Toc388163723http://c/Users/Tran/Desktop/new/Nh%C3%B3m%2022%20-%20Maltodextrin%20t%E1%BB%AB%20khoai%20lang.docx%23_Toc388163723http://c/Users/Tran/Desktop/new/Nh%C3%B3m%2022%20-%20Maltodextrin%20t%E1%BB%AB%20khoai%20lang.docx%23_Toc388163723http://c/Users/Tran/Desktop/new/Nh%C3%B3m%2022%20-%20Maltodextrin%20t%E1%BB%AB%20khoai%20lang.docx%23_Toc388163723http://c/Users/Tran/Desktop/new/Nh%C3%B3m%2022%20-%20Maltodextrin%20t%E1%BB%AB%20khoai%20lang.docx%23_Toc388163723http://c/Users/Tran/Desktop/new/Nh%C3%B3m%2022%20-%20Maltodextrin%20t%E1%BB%AB%20khoai%20lang.docx%23_Toc388163723http://c/Users/Tran/Desktop/new/Nh%C3%B3m%2022%20-%20Maltodextrin%20t%E1%BB%AB%20khoai%20lang.docx%23_Toc388163723http://c/Users/Tran/Desktop/new/Nh%C3%B3m%2022%20-%20Maltodextrin%20t%E1%BB%AB%20khoai%20lang.docx%23_Toc388163723http://c/Users/Tran/Desktop/new/Nh%C3%B3m%2022%20-%20Maltodextrin%20t%E1%BB%AB%20khoai%20lang.docx%23_Toc388163723
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    v

    Danh mc bngBng 1.Thnh phn ha hc ca khoai lang..................................................................................... 1Bng 2.Thnh phn Glucid ca khoai lang....................................................................................... 5Bng 3.Thnh phn acid amin khng thay thca khoai lang.......................................................... 6Bng 4.Thnh phn vitamin trong khoai lang................................................................................... 7Bng 5.Thnh phn khong trong khoai lang................................................................................... 7Bng 6.Chtiu cht lng ca chphm enzyme Termamyl........................................................... 9Bng 7.Sthay i DE theo nng enzyme sdng...................................................................... 9Bng 8.Chtiu cht lng nc..................................................................................................... 10Bng 9.Chtiu cht lng NaOH................................................................................................... 11Bng 10.Chtiu cht lng CaCl2................................................................................................. 12Bng 11.Chtiu cht lng HCl.................................................................................................... 12Bng 12.Chtiu cht lng than hot tnh..................................................................................... 13Bng 13.Chtiu cht lng bt trlc Diatomit.......................................................................... 13Bng 14.n nh ca Termamyl................................................................................................. 33Bng 15.So snh hai quy trnh cng ngh....................................................................................... 38Bng 16.So snh chung vhai quy trnh.......................................................................................... 39Bng 17.Tnh cht vt l ca Matodextrin....................................................................................... 39

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    CNCB Maltodextrin t khoai lang GVHD: PGS.TS Le Van Viet Man

    Nhom 22 1 Lp: Hc11Tp

    I. NGUYN LIU1. Khoai langThnh phn ha hc ca khoai lang

    Bng 1.Thnh phn ha hc ca khoai lang

    Thnh phn Hm lng (%)

    Nc 68,0

    Protein 0,8

    Lipid 0,2

    Carbohydrate 28,5

    Cellulose 1,3

    Tro 1,2

    1.1. CarbohydrateCarbohydrat l thnh phn chyu ca cht khv chim 24-27% trng lng ti.Thnh

    phn ca glucid ch yu l ng v tinh bt, ngoi ra cn c cc cht khc nh pectin,

    cellulose, hemicellulose, chim slng t.

    1.2. Tinh btTrung bnh chim khong 60-70% carbohydrate.

    Tinh bt gm hai polysaccharide khc nhau: amylose v amylopectin trong amylose

    chim khong 17-20%. Do , tinh bt khoai lang dho tan trong nc (m, nng) hn cc

    loi tinh bt giu amylose khc, do c cu to cng knh nn tinh bt khoai lang khng c xu

    hng kt tinh trli v do c khnng ginc ln.

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    CNCB Maltodextrin t khoai lang GVHD: PGS.TS Le Van Viet Man

    Nhom 22 2 Lp: Hc11Tp

    Hnh 1.Cu to tinh bt

    Amylose:Cu trc phn tc dng mch thng, chui di t500-2000 n vglucose,

    lin kt nhau bng lin kt glucoside. Phn tamylose gm nhiu chui xp song song

    vi nhau, trong cc chui cun li thnh hnh xon c.Trong cu to ca phn tamylose c

    1 u khv 1 u khng kh.

    Hnh 2.Cu trc phn tAmylose

    Amylopectin:Cu trc phn tc dng mch nhnh gom 600-6000 phan t glucose lin

    kt vi nhau bng 2 loi lin kt -1,4 glucoside v -1,6 glucoside. Phn tamylopectin ch

    c 1 u khduy nht.Mi lin kt nhnh ny lm cho phn tcng knh hn, chiu di ca

    chuimch nhnh ny khong 25 30 n v glucose. Phn t amylopectin c th cha ti

    100000 n vglucose.

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    CNCB Maltodextrin t khoai lang GVHD: PGS.TS Le Van Viet Man

    Nhom 22 3 Lp: Hc11Tp

    Hnh 3.Cu trc Amylopectin

    Tnh cht ca tinh bt nh hng n qui trnh sn xut maltodextrin.

    Tnh cht ho hc:

    Phn ng thy phn:l qu trnh thy phn lin kt gia cc n vglucose bng acid

    hoc bng enzyme. Acid v enzyme ging nhau l u thy phn cc phn t tinh bt bng

    cch thy phn lin kt - D - 1,4 glucoside. c trng ca phn ng ny l nht ca dung

    dch gim nhanh chng v sinh ra ng.

    Hnh 4.Phn ng thy phn tinh bt

    Phn ng to phc: Khi tng tc vi iode, amylase s cho phc mu xanh,

    amylopectinto phc vi iode cho mu tm c trng. V vy, iode c thcoi l thuc th c

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    CNCB Maltodextrin t khoai lang GVHD: PGS.TS Le Van Viet Man

    Nhom 22 4 Lp: Hc11Tp

    trng xc nh hm lng amylose trong tinh bt bng phng php trc quang. phn

    ng c th cc phn tamylase phi c dng xon c hnh thnh ng xon c n ca

    amylose bao quanh phn tiode. Cc dextrin c t hn 6 gc glucose khng cho phn ng vi

    iode v khng to c mt vng xon c hon chnh.Ngoi khnng to phc vi iode, amylose cn c khnng to phc vi nhiu cht hu

    c c cc cng nh khng cc nh: cc ru no, cc ru thm, phenol, cc ceton phn t

    lng thp.

    Tnh hp thca tinh bt:Ht tinh bt c cu to lxp nn khi tng tc vi cc cht

    bhp thth bmt trong v ngoi ca tinh bt u tham d. V vy trong qu trnh bo qun,

    sy v chbin cn phi ht sc quan tm tnh cht ny. Cc ion lin kt vi tinh bt thng

    nh hng n kh nng hp th ca tinh bt. Kh nng hp th ca cc loi tinh bt ph

    thuc cu trc bn trong ca ht v khnng trng nca chng.

    Khnng hp thnc v khnng ha tan ca tinh bt: Xc nh khnng hp th

    nc v khnng ha tan ca tinh bt cho php iu chnh c t ldung dch tinh bt v

    nhit cn thit trong qu trnh cng nghip, cn c ngha trong qu trnh bo qun, sy v

    chbin thy nhit. Rt nhiu tnh cht chc nng ca tinh bt phthuc vo tng tc ca

    tinh bt v nc (tnh cht thy nhit, shha, to gel, to mng).

    Tnh cht vt l

    tan ca tinh bt:Amylose mi tch ttinh bt c tan cao hn song khng bn

    nn nhanh chng b thoi ha trnn khng ha tan trong nc. Amylopectin kh tan trong

    nc nhit thng m chtan trong nc nng. Tinh bt bkt ta trong cn,v vy cn l

    mt tc nhn tt tng hiu quthu hi tinh bt.

    Strng n:Khi ngm tinh bt vo nc th thtch ht tng do shp thnc, lm

    cho ht tinh bt trng phng ln. Hin tng ny gi l hin tng trng nca ht tinh bt.

    tng kch thc khi ngm vo nc ca tinh bt l 28,4%.

    Tnh cht hha ca tinh bt:Nhit ph vht chuyn tinh bt ttrng thi uthnh dung dch keo gi l nhit hha. Phn ln tinh bt bhha khi nu v trng thi

    trng nc sdng nhiu hn trng thi tnhin. Cc bin i ha l khi hha nh

    sau: ht tinh bt trng ln, tng trong sut v nht, cc phn tmch thng v nhth

    ha tan v sau t lin hp vi nhau to thnh gel. Nhit hha khng phi l mt

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    CNCB Maltodextrin t khoai lang GVHD: PGS.TS Le Van Viet Man

    Nhom 22 5 Lp: Hc11Tp

    im m l mt khong nhit nht nh.Ty iu kin hha nh nhit , ngun gc tinh

    bt, kch thc ht v pH m nhit ph vv trng nca tinh bt bin i mt cch rng

    ln.

    Nhit hho ca tinh bt khoai lang: 52 64o

    C, so vi nhng loi tinh bt khc thnhit ny tng i thp, iu m nhiu nh sn xut lun mun c c.

    nht ca htinh bt: Phn ttinh bt c nhiu nhm hydroxyl c khnng lin kt

    c vi nhau lm cho phn ttinh bt tp hp li, ginhiu nc hn khin cho dung dch c

    c, dnh, do v nht cao hn. Yu tchnh nh hng n nht ca dung dch

    tinh bt l ng knh biu kin ca cc phn thoc ca cc ht phn tn, c tnh bn trong

    ca tinh bt nh kch thc, thtch, cu trc, v sbt i xng ca phn t. Nng tinh

    bt, pH, nhit , tc nhn oxi ha, cc thuc thph hy lin kt hydro u lm cho tng tc

    ca cc phn ttinh bt thay i do lm thay i nht ca dung dch tinh bt.

    Khnng to gel v sthoi ha gel: Tinh bt sau khi hha v ngui, cc phn t

    stng tc nhau v sp xp li mt cch c trt tto thnh gel tinh bt vi cu trc mng

    3 chiu. to c gel th dung dch tinh bt phi c nng m c va phi, phi c

    hha chuyn tinh bt thnh trng thi ha tan v sau c ngui trng thi yn

    tnh. Trong gel tinh bt ch c cc lin kt hydro tham gia, c th ni trc tip cc mch

    polyglucoside hoc gin tip qua phn tnc.

    Khi gel tinh bt ngui mt thi gian di sco li v lng dch thsthot ra, gi l

    sthoi ha.Qu trnh ny scng tng mnh nu gel lnh ng ri sau cho tan bng.

    1.3. ngSbin ng vhm lng ng tng t5-10 % trng lng khoai lang.

    Yu tquan trng nh hng n hm lng ng trong ckhoai lang l ging, ngoi ra

    cn c cc yu tkhc nh thi gian thu hoch, bo qun

    Thnh phn ca ng gm saccharose, glucose, fructose, v mt t maltose.

    Bng 2.Thnh phn Glucid ca khoai lang

    Thnh phn Hm lng (%)

    Saccharosse 5,16 10,95

    Glucose 2,11 4,61

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    CNCB Maltodextrin t khoai lang GVHD: PGS.TS Le Van Viet Man

    Nhom 22 6 Lp: Hc11Tp

    Maltose 1,59 6,85

    Fructose 1,16 3,561.4. Cht x

    X ngvai tr quan trng trong vic phng chng mt sbnh nh ung th, tiu ng,tim mch...

    X nc bao gm cc hp cht pectin, cellulose v hemicellulose. Hm lng cht x

    n c trong cc ging khoai lang ca o Tonga l 4%, ca Ml 3,6%. Ngoi ra cn cha

    0,4% lignin.

    1.5. ProteinHm lng protein trong cc ging khoai lang l khng cao, trung bnh khong 5% cht

    kh. Hm lng protein thng khng cao nhng do khoai lang c nng sut c cao, nn

    protein thu c trn mt n vtrng trt l ng k, khng thua km cc loi ng cc. Ngoi

    ra thnh phn cc acid amin trong protein ca khoai lang kh cn i, nht l cc acid amin

    khng thay th.

    Thnh phn acid amin khng thay thca ckhoai lang (tnh theo % trng lng khong

    ca protein th)

    Bng 3.Thnh phn acid amin khng thay thca khoai lang

    Acid amin Hm lng (%)

    Arginin 2,9

    Histidine 1,4

    Lysine 4,3

    Tryptophane 1,8

    Phenylalanine 4,3

    Methionine 1,7

    Threonine 3,8

    Leucine 4,8

    Isoleucine 3,6

    Valine 5,6

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    CNCB Maltodextrin t khoai lang GVHD: PGS.TS Le Van Viet Man

    Nhom 22 7 Lp: Hc11Tp

    1.6. VitaminKhoai lang ccha nhiu loi vitamin nh C, A, B1, B2, PP, acid pentotenic. Ty vo

    ging m hm lng vitamin trong khoai lang l khc nhau. V d: khoai lang nghcn cha

    nhiu -caroten n 44,6 %, trong khi cng ging khoai lang trng chcha 0,5% -caroten.Bng 4.Thnh phn vitamin trong khoai lang

    Thnh phn Hm lng (%)

    Vitamin A 7,4

    Vitamin B1 0,88

    Vitamin B2 10,88

    Vitamin PP 13,4

    Acid pentotenic 11,1

    Cc vitamin tp trung nhiu vng ngoi ca rut c.Vv phn trung tm ccha t

    vitamin hn.

    1.7. KhongThnh phn khong trong khoai lang bin ng tng i ln tuthuc vo loi t trng

    v phn bn sdng.

    Thnh phn khong chyu trong khoai lang (% so vi trng lng tro)

    Bng 5.Thnh phn khong trong khoai lang

    Thnh phn Hm lng (%)

    Cl 2,5

    K2O 58,1

    Na2O 8,1

    CaO 5,6

    MgO 4,1

    Fe2O3 0,54

    Mn2O3 Vt

    P2O5 16,1

    SO3 2,9

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    CNCB Maltodextrin t khoai lang GVHD: PGS.TS Le Van Viet Man

    Nhom 22 8 Lp: Hc11Tp

    Tiu chun chn khoai lang

    Cu to ckhoai lang gm 3 phn:

    Vbao chim 1% khi lng c Vci chim 5-12% khi lng c Tht cLng tinh bt trong khoai lang thng dao ng t15-31%, kch thc ht tinh bt t

    15-80 m.

    Khng mc mm, hm lng tinh bt khng di 14%, tp cht t di 15%, dp nt

    di 2%.

    Nguyn liu tbi cha c xe xc a vo phu phn phi.2. Enzyme

    Cng ngh thu phn tinh bt bng acid c gii thiu t th k 19 (Naegeli, 1874;

    Lintner, 1886) v pht trin trong mt thi gian di. Tuy nhin cng nghny c mt snhc

    im: yu cu dng cthit bphi lm bng cc vt liu chng n mn, tn nng lng cho

    qu trnh gia nhit, kh khn trong vic kim sot, nh hng n mu sc sn phm, stn ti

    ca cc hp cht mui sau khi trung ho v c bit l nh hng n mi trng. V nhng

    nhc im ni trn nn hin nay acid khng cn c khuyn khch sdng thu phn

    tinh bt, m thay vo l enzyme.

    Enzyme c sdng thuphn tinh bt to sn phm c chsDE khc nhau.Trong

    qui trnh sn xut, enzyme c sdng cng on dch ho (sau khi tinh bt c hho

    thuphn tinh bt thnh mch ngn) v ng ho (thuphn sn phm dch ho to thnh sn

    phm cho chsDE nh mong mun).

    Enzyme c s dng thu phn tinh bt l enzyme amylase v hu ht cc loi

    enzyme ny u c hiu vi lin kt -1,4-glucoside nhng khng c khnng ct c lin

    kt -1,6-glucoside. y l mt iu kh khn trong vic sdng enzyme thuphn honton amylopectin thnh glucose.

    Enzyme amylase (1,4Dglucan glucanohydrolases) l mt enzyme thuphn

    c hiu vi lin kt 1,4--D-glucoside v ct mch tinh bt tvtr gia mch.

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    CNCB Maltodextrin t khoai lang GVHD: PGS.TS Le Van Viet Man

    Nhom 22 9 Lp: Hc11Tp

    Cc loi enzyme thng mi c s dng thu phn tinh bt trong sn xut cng

    nghip c sn xut ch yu t 2 chng vi khun Bacillus amyloliquefaciens v Bacillus

    licheniformis(sn xut enzyme c tn thng mi l Termamyl hay novozyme). Enzyme c

    sn xut t2 chng ny c skhc bit vkhnng chu nhit, nhit 1100

    C hot tnh caTermamyl bmt t hnB. amyloliquefaciens-amylase. (Martin F. Chaplin, 1990).

    ti ny s dng enzyme Termamyl 120L c sn xut t Bacillus

    licheniformis.Enzyme hot ng tt iu kin nng Ca2+50 70ppm, chng xc tc thu

    phn tinh bt nhit rt cao 95100oC, di y l bng chtiu cht lng enzyme.

    Bng 6.Chtiu cht lng ca chphm enzyme Termamyl

    Tn chtiu Thng sk thut

    Trng thi, mu sc Dung dch dng lng, mu nuTtrng, g/ml 1,201,25

    Hot tnh, KNU/g 120

    KNU (Kilo Novo alpha amylase Unit): s lng enzyme ph hu5,26 g tinh bt/gi

    (theo phng php Novozyme xc nh alphaamylase).

    Dng nhit v hot enzyme sau dch ho m bo DE cho sn phm.

    La chn nng enzyme

    Bng 7.Sthay i DE theo nng enzyme sdng

    STTNng enzyme

    so vi tinh bt (%)Bx DE nht

    1 0,04 20 7,67 5,48

    2 0,06 20 9,20 4,98

    3 0,07 20 10,46 3,76

    4 0,08 20 11,86 3,12

    5 0,1 20 12,30 2,58

    6 0,12 20 14,91 2,47

    7 0,14 20 17,21 2,26

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    Nhom 22 10 Lp: Hc11Tp

    8 0,16 20 18,56 2,15

    Nng enzyme tng th tt phn ng tng ln. Nng enzyme Termamyl 120L t

    0,081,0% th DE thay i t11,8612,30. Trong khong ny nng enzyme 0,08% tuy nht c cao hn so vi nht nng 0,1% nhng ti 0,08% cho hiu qukinh tcao hn.

    V thta chn nng enzyme Termamyl 120L 0,08%.

    3. Cc nguyn liu ph3.1. Nc

    Nc sdng trong sn xut phi p ng c cc yu cu v cht lng theo QCVN

    01:2009/BYT quy chun kthut quc gia vcht lng nc n ung, cth: khng c mi, v

    l, pH Trong khong 6,5-8,5, slng Coliform tng s/100ml nc l 0, slng E.coli hoc

    Coliform chu nhit/100ml l 0, di y l bng mt schtiu ca nc n ung.

    Bng 8.Chtiu cht lng nc

    Mu sc(*) TCU 15

    Mi v(*) - Khng c mi, vl

    c(*) NTU 2

    cng, tnh theo CaCO3(*) mg/l 300

    Tng cht rn ho tan (TDS)(*) mg/l 1000

    Hm lng Nhm(*) mg/l 0,2

    Hm lng Amoni(*) mg/l 3

    Hm lng Antimon mg/l 0,005

    Hm lng Asen tng s mg/l 0,01

    Hm lng Bari mg/l 0,7

    Hm lng Bo tnh chung cho c Borat vAxit boric

    mg/l 0,3

    Hm lng Cadimi mg/l 0,003

    Hm lng Clorua(*) mg/l 250

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    CNCB Maltodextrin t khoai lang GVHD: PGS.TS Le Van Viet Man

    Nhom 22 11 Lp: Hc11Tp

    300(**)

    Hm lng Crom tng s mg/l 0,05

    Hm lng ng tng s(*) mg/l 1

    Hm lng Xianua mg/l 0,07

    Hm lng Florua mg/l 1,5

    Hm lng Hydro sunfur(*) mg/l 0,05

    Hm lng St tng s(Fe2++ Fe3+)(*) mg/l 0,3

    Hm lng Ch mg/l 0,01

    Hm lng Mangan tng s mg/l 0,3

    Hm lng Thungn tng s mg/l 0,001

    Hm lng Niken mg/l 0,02

    Hm lng Nitrat mg/l 50

    Hm lng Nitrit mg/l 3

    Hm lng Selen mg/l 0,01

    Hm lng Natri mg/l 200

    Hm lng Sunpht(*) mg/l 250

    Hm lng Km(*) mg/l 3

    (*): l chtiu cm quan

    3.2. CaCl2, NaOH, HCl, than hot tnhChtiu cht lng NaOH (TCVN: 3793-83)

    Bng 9.Chtiu cht lng NaOH

    Tnchtiu Thng sk thut

    Dng bn ngoi v mu scDung dch trong sut hoc c mu tm

    xanh nht

    Hm lng natri hidroxit (NaOH), % 40

    Hm lng natri cacbonatt (Na2CO3), % 0,6

    Hm lng natri clorua (NaCl), % 0,05

    Hm lng st chuyn ra st III oxit (Fe2O3), % 0,015

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    CNCB Maltodextrin t khoai lang GVHD: PGS.TS Le Van Viet Man

    Nhom 22 12 Lp: Hc11Tp

    Hm lng natri clorat (NaClO3), % 0,01

    Hm lng sunfat (SO42+), % 0,03

    Hm lng canxi (Ca); magi (Mg), % 0,006

    Hm lng kim loi nng thuc nhm hydrosunfua (H2S) chuyn ra ch, %

    0,003

    Hm lng axit silixic (H2SiO3), % 0,01

    Hm lng nhm chuyn ra nhm oxit (Al2O3), % 0,01

    Hm lng thungn (Hg), % 0,00125

    Bng 10.Chtiu cht lng CaCl2

    Tn chtiu Thng sk thutHm lng CaCl2, % 95%

    Hnh dng, mu sc Cht bt tinh thmu trng

    Ttrng 250C, g/ml 2,15

    Tnh tan Tan hon ton trong nc

    pH ca dung dch nng 100g/lt 10

    Bng 11.Chtiu cht lng HCl

    Tn chtiu Thng skthut

    Trng thi, mu sc Dung dch khng mu hoc vng nht

    HCl, % 31,5

    Clo tdo, % 0,004

    Fe, % 0,001

    Ttrng, g/ml 1,151,16

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    Nhom 22 13 Lp: Hc11Tp

    Bng 12.Chtiu cht lng than hot tnh

    Tn chtiu Thng sk thut

    Hnh dng Dng ht khng nh hnh

    Mu sc Mu en c trng ca than

    Ttrng 250C, g/ml 0,440,6

    Tnh tan trong nc v dung mi khc Khng

    m, % 10

    Tro, % 3

    cng, % 95

    pH 911

    im chy,0

    C 450mn qua sng 0,076 mm tnh bng, % 80

    Bng 13.Chtiu cht lng bt trlc Diatomit

    Thng sha l Diatomit ( kch thc 1300 m)

    Thnh phn 86% SiO2, 5% Na, 3% Mg, 2% Fe

    Ngun gc Tto bin

    Cht lng tnhin Bcanxi ha nhTtrng kh (g/l) 320 - 480

    Ttrng nc (g/l) 290 - 4000

    xp 84 - 90

    II. QUI TRNH CNG NGH1. Qui trnh cng ngh11.1 S

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    Nhom 22 14 Lp: Hc11Tp

    Nghin

    Thy phn

    Ty mu

    Termamyl120L

    Phi trn

    CaCl2

    Cht chnh pH

    Nc thi

    Nc

    C c chn khn

    Sy phun

    Bao gi

    Maltodextrin

    Lc

    Than hot tnh

    Tp cht

    Tp cht

    V hot enzyme

    Lm sch s b

    Khoai lang

    Ra

    Ct khc

    Lm ngui

    Nc

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    Nhom 22 15 Lp: Hc11Tp

    1.2 Thuyt minh qui trnh1.2.1 Lm sch s b

    Mc ch cng ngh: chun bcho qu trnh nghin.Cc bin i:

    Vt l: khi lng ca cgim ty thuc vo mc tp cht.

    Ha sinh: c thbsm mu cc vt tn thng c hc.

    Thit bvthng scng ngh

    Cu to ca thit bgm nhng thanh st song song vi nhau thnh trtrn rng c cc

    khe hbi t, tp cht ri ra ngoi. Khi ng c quay thit bquay theo do nh

    lc ma st gia cvi c, gia cvi thn my t ri ra ngoi, cn khoai tip tc i

    qua thit bra. C nghing nht nh t1520o.

    Hnh 5.Thit bloi btp cht

    1.2.2 RaMc ch cng ngh:chun bcho qu trnh nghin.

    Cc bin i

    Vt l: sau khi ra stch c 95-97% tp cht ra khi c, khi lng chung gim cn

    93-94,5% so vi ban u.

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    Nhom 22 16 Lp: Hc11Tp

    Ho hc: din ra khng ng k.

    Ho sinh: shot ng ca enzyme oxi ho lm en cc vt try xc trn bmt vt

    liu.

    Thit bvthng scng ngh:

    Hnh 6.Thit bra

    Sdng nc phun ttrn xung vi p lc cao ln bmt c. Dng cnh khuy dng trc vis vi tc dng va o trn mnh va y cvpha trc.

    ng thi to ma st gia cvi c, v cvi thit btng khnng lm sch.

    Dng mt bm, bm nc theo chiu ngc chiu vi trc vis nhm m bo nc bnskhng nhim li vo c sch.

    Chiu di ca thng ra c tnh ton sao cho khi cc y ra n ca thot liuchng c ra sch lp vt ct .Tp cht nng sc lng xung v tho qua l

    y thng.

    1.2.3 Ct khcMc ch

    Chun b: Ct nhnguyn liu qu trnh nghin tip theo t hiu sut cao hn.

    Cc bin i ca nguyn liu

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    Nhom 22 17 Lp: Hc11Tp

    Bin i vt l: Gim kch thc, ban u tckhoai ban u (15-20 cm) xung cn nh

    hn 3cm.

    Bin i ho sinh: Shot ng ca cc enzyme oxi ho lm bin i mu khoai nhng

    chbct, nhng khng ng k.Thit bvthng scng ngh

    Thit bdng hnh hp chnht thng y. Cho nguyn liu i vou trn, di tc

    dng ca hthng cc dao ct c gn trn mt trc, trc quay nhng c ngoi thit b, s

    ct nhnguyn liu v ri xung bng ti.

    Hnh 7.Thit bct

    1.2.4 NghinMc ch cng ngh: chun bcho qu trnh thy phn.

    Cc bin i ca nguyn liu :

    Vt l: kch thc ca nguyn liu sgim i, din tch bmt ring stng ln lm tng

    tc phn ng oxi ho do tip xc vi oxi nhiu hn.

    Trong qu trnh nghin, di tc dng ca cc lc, nhit ca vt liu stng ln lm

    xut hin mt sbin i vcu trc.

    Ho sinh: mt vi sinh vt trn vt liu stng ln v cc phn ng c xc tc bi

    enzyme s d dng hn, enzyme oxi ho kh nh polyphenol oxidase s lm sm mu sn

    phm.

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    Nhom 22 18 Lp: Hc11Tp

    Thit b:

    Hnh 8.Thit bnghin rng

    1. Vmy 2. Trc quay 3.Tang quay

    4. Rng 5. y t l 6.Cn iu chnh

    Nguyn tc hot ng:

    Nguyn liu c np vo ca pha trn do schuyn ng ca tang quay 3, nguyn

    liu c ko vo khe hgia vmy v tang quay, nhma st ca cc dao 4 gn trn tang

    quay v sma st ca nguyn liu vi vmy m tbo tinh bt ca ckhoai bph v, pha

    di c y c l5, y ny cho cc sn phm nghin mn lt qua, cn phn cha mn li tiptc nghin cho n khi c nghin mn, cn iu chnh 6 dng iu chnh khong cch

    gia tang quay v vmy ( iu chnh khi nghin). Rng c chiu cao tnh tbmt tang quay

    l 12 mm. Trong qu trnh nghin cn thm nc nc a bt nghin ra ngoi thng qua

    lli.

    Thng skthut:

    Cng sut ng c: 5,5 kWh Tng quay c ng knh 50cm. Trn c rnh theo chiu dc gn li dao hay

    li ca. Ty theo yu cu m c t1012 rngca, khong cch gia cc li dao

    l 5mm.

    Vn tc quay: 1000 v/p Nng sut lm vic: 10 tn c/ ngy.

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    Nhom 22 19 Lp: Hc11Tp

    Kch thc sau nghin: 535 m.1.2.5 Phi trn

    Mc ch cng ngh

    Chun bnhm tng phn tn ca dch huyn ph, chun bcho qu trnh thy phntip theo.

    Cc bin i :

    Vt l Sphn tn ca tinh bt trong nc tng dn n ng nht ca nguyn liu

    tng.

    Hsdn nhit tng.

    Thtch ht tinh bt tng do shp thnc lm ht tinh bt trng ln. Ho l:

    Ht tinh bt hp thu mt lng nhnc (25-50 % nc) nhng cha trng n. Trng thi ca nguyn liu sau khuy trn dng huyn ph. Tng khnng tip xc gia ht tinh bt v nc.

    Cm quan ng nht ca nguyn liu.

    Cc yu tnh hng:

    Thnh phn ho hc ca nguyn liu. Tlphi trn ca nguyn liu nh hng n thi gian khuy trn. Tc phi trn ca thit b.

    Thit bvthng scng ngh

    Thit b c dng hnh trng, c cnh khuy c kt ni vi 1 motor, xungquanh bn trong thit bc cc tm chn, tng hiu sut khuy trn. C van x

    y ni vi h thng bm ly tm bm dch vo thit bhho, cnh khuy

    c m vi tc 400 vng/pht. Nn khi ng cnh khuy trc khi bm

    dch tinh bt vo.

    Phi trn nhit thng Phi trn nguyn liu vi nc t hm lng cht kh khong 20 - 25%.

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    Nhom 22 20 Lp: Hc11Tp

    Chnh pH ca hn hp v 7 l pH ti thch ca -amylase s dng trong quytrnh.

    B sung CaCl2 nng Ca2+t 70 ppm duy tr hot ng ca amylasetrong qu trnh thuphn.

    Bsung enzyme amylase (Termamyl) vi liu lng 0,08% so vi hm lngtinh bt.

    1.2.6 Thy phnMc ch cng ngh

    Thy phn gm 2 qu trnh l hha v dch ha. Mc ch cng nghl chbin.

    Cc bin i ca nguyn liu Vt l: Trong qu trnh hha, huyn ph tinh bt sc gia nhit lm nhit khi huyn ph tng, ht nc chuyn ng xm nhp vo ht tinh bt, ht tinh bt

    trng n, thtch dung dch tng do tinh bt trng n, thtch tng ht tng dn n

    tng thtch dung dch. Sau ht tinh bt bph vcu trc to ra cc si amylose v

    amylopectin, nht tng cc i giai on hha.

    Ho l: Khi tng nhit trong giai on hha, mc hp phnc ca tinh bttng theo. Huyn ph tinh bt schuyn sang dng khi paste khi kt thc qu trnh h

    ha. Nu tng nhit cao hn thc hin tip giai on dch ha, khi cho sha

    lng.

    Ha sinh: Chphm enzyme ct mch tinh bt vtr - 1- 4 glucoside vtr giamch to ra sn phm chnh l dextrin, ngoi ra cn c oligosaccharide.

    Ha hc: Phn ng Maillard xy ra do cc axit amin c trong nguyn liu v ngsinh ra trong qu trnh thy phn tinh bt, tuy nhin phn ng khng ng k v hm

    lng axit amin c trong nguyn liu rt thp, thi gian lu ca qu trnh hha l kh

    thp.

    Sinh hc: Enzyme, vi sinh vt c trong tinh bt gim do btiu dit bi nhit cao.Thit bvthng scng ngh

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    Nhom 22 21 Lp: Hc11Tp

    Hho

    Hnh 9.Thit bhha Jet-cooker

    Cu to: thit bgm mt ng huyn ph tinh bt v mt ng hi giao nhau qua mt khe

    hnh cn, hi c phun trc tip vo huyn ph tinh bt, lng hi c iu chnh bi van

    qua hthng kh nn.

    Nguyn tc hot ng: huyn ph tinh bt c phun cng bc vo thit bv tip xc

    trc tip vi hinc, hi nc khi tip xc vi tinh bt c nhit thp hn sngng tmt

    phn nhng hu ht hi nc vn cn p sut cao nn vn cung cp nhit lng nng nhit

    nhm hho tinh bt.Thi gian lu trong thit bJetcooker rt ngn.

    Lng tinh bt c hho mt phn sbng qua mt dy cc ct lu cao p duy tr

    nhit 95 100oC. Thi gian lu: 5 10 pht. Tnh ton bo n, tn tht nhit khi i qua

    cc ct lu sao cho khi i ti thit bdch ha, nhit ca khi cho hcn 90 95oC ph

    hp vi nhit xc tc ti uca enzyme.

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    Nhom 22 22 Lp: Hc11Tp

    Dch ho

    Hnh 10.Thng dch ha

    Cu to: thit bl thng kn ni 2 v, c vo iu nhit, trong thng chia lm nhiu

    ngn, mi ngn c cnh khuy ni chung vi mt trc c dn bi ng c.

    Nguyn tc hot ng: dung dch i ttrn xung qua mi ngn theo ng trung tm. Do

    vy dung dch sc lu mt thi gian cnh trong thng, o iu nhit pha ngoi nhm

    ginhit dch ho m bo 95oC.

    Tc cnh khuy: 150 - 200 vng/pht.

    Thi gian lu ca khi tinh bt trong thit bt10 20 pht. Sau tng khong thi gian

    nht nh, ta ly mu ra kim tra chsDE.

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    Nhom 22 23 Lp: Hc11Tp

    Hnh 11.S hha-dch ha

    1.2.7 V hot enzymeDng tc nhn nhit.

    Mc ch cng ngh

    Mc ch y l hon thin. Nhit kim hm hot ng enzyme l lm cho gi tr

    DE ca maltodextrin n nh, khng b thay i trong qu trnh sn xut, n nh cht lng

    u ra ca sn phm.

    Cc bin i xy ra

    Ho sinh: khi nng nhit ln cao, qu trnh trao i cht ca enzyme bnh ch, bt hot

    enzyme, ngng qu trnh thuphn tinh bt.

    Ha hc: cc phn ng nh maillard hoc caramen c th din ra, nhng do thi gian

    nhanh v nng cc cht tham gia thp, nn khng ng k.

    Thng svthit bcng ngh

    Xl nhit bng hi bo ha nhit t120 - 125oC.Thi gian v hot t: 5-10 pht.

    Thit b: thc hin bng thit btruyn nhit dng bn mng.

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    Nhom 22 24 Lp: Hc11Tp

    1.2.8 Lm nguiMc ch cng ngh: chun bcho qu trnh ty mu.

    Thit bvthng scng ngh:

    Thit b: thit btrao i nhit dng bn mng.Sau khi v hot enzyme, hn hp dch phi lm ngui dch bng nc lnh (5 - 10oC),

    bng mt thit btrao i nhit dng bn mng, nhit sau khi lm ngui l 65 - 700C. Sau

    c bm vo thit b ty mu. Mc ch ca vic ny l lm tng khnng hp phca

    than hot tnh, nhit cng thp, khnng hp phca than cng cao.

    1.2.9 Ty muMc ch cng ngh

    Hon thin: dung dch sau thy phn dxy ra phn ng maillard do trong dung dch vn

    cn st mt lng nhcc axit amin sphn ng vi ng khlm dung dch bsm mu,

    ngoi ra ty mu cn loi mt stp cht khc sinh ra trong qu trnh phn ng (cc cu t

    protein bin tnh, cc cht keo t).

    Cc bin i ca nguyn liu

    Ho l: Cht mu v mt stp cht trong dch thy phn shp phtrong mao dn ca

    ht than hot tnh.

    Cc bin i khc khng ng k.

    Thit bvthng scng ngh

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    Nhom 22 25 Lp: Hc11Tp

    Hnh 12.Thit bty mu bng than hot tnh

    Thit bc hnh trdng ng, y cu, bn trong thit bc cnh khuy, bn ngoi phn

    y c vo iu nhit.

    Sn phm sau khi ty mu c tho ra qua ca y.

    Hm lng than hot tnh sdng khong xp x0,75% lng cht kh trong dch thy

    phn.Ngi ta schun bhuyn ph than hot tnh vi nng 15%, sau a vo thit b

    qua ca nh, trong khong thi gian ny o trn lin tc.

    Nhit xl: 65 - 70oC.

    Thi gian xl khong: 25-30 pht.

    Tc cnh khuy: 200 vng/pht.

    1.2.10 LcMc ch cng ngh

    Hon thin: qu trnh lc gip ci thin mt schtiu cht lng ca sn phm (trong

    ca dch maltodextrin).

    Khai thc: phn ring huyn ph, gili cu tcn thit, thu hi maltodextrin, loi bcc

    tp cht (protein, cellulose, tinh bt cha thy phn) v than hot tnh.

    Cc bin i

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    Nhom 22 26 Lp: Hc11Tp

    Vt l: do xy ra sphn ring hai pha, pha phn tn bao gm cc tp cht, cn bn bln

    trong dung dch thuphn, pha lin tc l dch maltodextrin c tinh sch nn mt sch

    tiu vt l ca dch lc s thay i so vi huyn ph ban u nh khi lng gim, t trng

    gim, trong tngHa l: C sphn ring hai pha: pha phn tn bao gm cc ht than hp phcc cht

    mu v mt stp cht bln trong dung dch thy phn, pha lin tc l dch maltodextrin.

    Sinh hc: qu trnh lc khng gy ra nhng bin i sinh hc. Tuy nhin nu thi gian

    lc qu di th hvi sinh vt c sn trong huyn ph hoc cc vi sinh vt tmi trng bn

    ngoi c thbnhim vo huyn ph spht trin.

    Ho sinh: qu trnh lc khng gy ra nhng bin i ho sinh.

    Ho hc: qu trnh lc khng gy ra nhng bin i ho hc ng k.

    Cm quan: trong ca dung dch tng.

    Thit bvthng scng ngh

    Thit b: lc khung bng vi mng lc vi c phmt lp bt trlc diatomite.

    Thit blm vic bn lin tc. Vic np v tho dch lc ra khi thit bc ththc hin

    lin tc trong mt khong thi gian, tuy nhin vic tho b lc phi c thc hin gin on.

    Thit bgm hai bphn chnh vi tit din hnh vung. Khung c chc nng cha b lc v l

    ni bm huyn ph vo. Cn bn lc c chc nng to nn bmt lc vi cc rnh dn dch

    lc.

    Nguyn l:mt my lc khung bng bao gm cc khung v bng gn vi nhau bng cc

    tm giy lc ph c 2 pha ca bng. Sau khi cc khung v bng c p st nhau, khong

    khng gia cc khung sl ni cha huyn ph bt trlc v dung dch cn lc. Lp o bt tr

    lc sc phln bmt vi lc, dung dch c lc si qua cc tm bng ra ngoi.

    Nguyn tc ca qu trnh lc l khi va bt u lc ln thnht cn bsung nc nng

    hoc hi nng hm nng my lc trong khong thi gian 10 pht trnh trng hp nhit

    chnh lch t ngt c thlm bin dng khung bng, lm tc cc bb v dch lc. Sau mi iu chnh tng dn dn tc cp dch lc vo my lc.

    Trong qu trnh lc, nu thy bt k dch lc ca khung bng no mang theo b , dch thu

    c bc chng tvi lc ca khung y b rch hoc lp khng ng, cn kim tra li h

    thng.

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    CNCB Maltodextrin t khoai lang GVHD: PGS.TS Le Van Viet Man

    Nhom 22 27 Lp: Hc11Tp

    n mt thi gian nht nh trong khung lc c y b, lm tng trlc v tc lc

    sthay i rt nhanh, nu tip tc lc slm tng thi gian lc. Do cn phi tho my p lc

    thu hi b lc.

    Hnh 13.M hnh lc khung bng

    Hnh 14.Hnh nh thc tca thit blc khung bng

    My lc khung bng c bmt lc t20 - 400 m2, hiu sut ca my c tht 200 -

    400L/m2.h .

    Thng scng ngh:p sut lc: 25 bar.

    Nhit : 60 - 650C.

    Kch thc li lc: 0,010,05 mm.

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    Nhom 22 28 Lp: Hc11Tp

    1.2.11 C cMc ch cng ngh

    Chun b: cho qu trnh sy gip qu trnh sy din ra ddng v tit kim chi ph nng

    lng trong ton bquy trnh sn xut.Khai thc: lm bay hi nc, tng nng cht kh trong dung dch.

    Cc bin i ca nguyn liu

    Vt l: Nhit dung dch tng, nng cht kh tng, nht tng, ttrng tng, nhit

    ca dung dch tng theo thi gian c c.

    Ho l: C schuyn pha ca nc.

    Ho hc: nu cc acid amin hoc peptide cha c loi bhon ton trong qu trnh tinh

    sch trc th chng scng vi mt t ng khtham gia phn ng Maillard lm cho dch

    thnh phm sm mu nhng khng ng k.

    Thit bvthng scng ngh

    Hnh 15.S thit bc c ng tun hon

    Nguyn l hot ng

    Thit bc c ng tun hon, pha trn gn vi thit bto chn khng nhm gim nhit

    si ca dung dch gip cho dch maltodextrin khng bsm mu.

    Nguyn l lm vic ca ni c c: phn di ca thit bl bung hi gm c cc ng

    truyn nhit. Dung dch c mt hthng phn vo cc ng theo c chchy mng trong ng,

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    Nhom 22 29 Lp: Hc11Tp

    hi t si trong khong khng gian pha ngoi ng. Khi lm vic, dung dch trong ng trao

    i nhit vi hi pha ngoi ng, hi nc trong dung dch sbc hi v dn ra ngoi. Dch c

    c srt xung v c bm tun hon li cho n khi t Bx theo yu cu.

    Kt qul trong thit bc chuyn ng tun hon tnhin ttrn xung trong ng tunhon. Sn phm c xra pha ca y.

    Thng sthit b:

    Nng cht kh sau khi c c: 45-50 0Bx. Nhit c c: 700C p sut hi t: 1,25 atm chn khng ca bung bc: 0,30,4 at.

    1.2.12Sy phun

    Mc ch cng ngh

    Khai thc: qu trnh sy tch bt nc ra khi nguyn liu, do hm lng cc cht kh

    c trong 1 n vkhi lng sn phm stng ln.

    Bo qun: qu trnh sy lm gim gi trhot nc trong nguyn liu nn c chhvi

    sinh vt gip ko di thi gian bo qun sn phm. Trong qu trnh sy, nhit ca nguyn

    liu kh cao lm mt svi sinh vt trong nguyn liu bv hot.

    Hon thin: sn phm thu c dng bt dho tan.

    Cc bin i ca nguyn liu

    Vt l: xut hin gradient nhit trong nguyn liu, ttrng ca sn phm gim, m

    nguyn liu gim.

    Ho l: c schuyn pha ca nc tlng thnh hi.

    Thit bvthng scng ngh

    H thng thit bsy phun dng u phun kh ng: gm cc bphn chnh: caloriphe

    gia nhit tc nhn sy, c cu phun sng, bung sy v hthng thu hi sn phm.

    Nguyn tc sy gm 3 giai on:Giai on 1: chuyn dch maltodextrin thnh dng sng m nhc cu phun sng kh

    ng. Kch thc cc ht sng 10-200 m.

    Giai on 2: ha trn sng m vi dng tc nhn sy trong bung sy.

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    Nhom 22 30 Lp: Hc11Tp

    Giai on 3: Tch sn phm ra khi dng tc nhn sy bng cch s dng h thng

    cyclone thu hi sn phm theo c chlng xoy tm.

    Hnh 16.S thit bsy

    Thng scng ngh

    Nhit tc nhn sy vo: 350oC p sut bm cao p: 15 - 20 bar.

    m sn phm: khng qu 5-6% Thi gian sy: 5-7s.

    1.2.13 Bao giMc ch cng ngh

    Bo qun: trnh tip xc vi mi trng khng kh. i vi maltodextrin dng bt, m

    5-6% rt dht m trli, gim chtiu vho l cm quan... Do cn bao gi sau sy.

    Hon thin: to thun tin cho ngi tiu dng.

    Bin i nguyn liu: hu nh khng c bin i no ng k

    Vt l iu cu to: ti nha polyetilen dy t5060 m.

    Thit bv thng scng ngh:

    - Bao gi v ht chn khng.

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    Nhom 22 31 Lp: Hc11Tp

    2. Qui trnh cng ngh22.1 S khi

    Khoai lang

    Lm sch s b

    Ra

    Nghin

    Phi trn

    Thy phn

    Lc

    Trao i ion

    C c membrane

    Sy phun

    Tp cht

    H2O

    Tp cht

    Maltodextrin

    Ct ltNc thi

    V hot enzymeHCl

    EnzymeTermamyl 120L CaCl2

    Cht chnh pH

    Nc

    Nc

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    Nhom 22 32 Lp: Hc11Tp

    2.2 M tqui trnh2.2.1 Lm sch s b2.2.2 Ct khc2.2.3 Nghin2.2.4 Phi trn2.2.5 Thy phn2.2.6 V hot enzyme

    Sdng tc nhn nhit kt hp vi HCl

    Mc ch cng ngh

    Hon thin: di tc dng HCl, enzyme bv hot, lm cho gi trDE ca maltodextrin

    n nh, khng bthay i trong qu trnh sn xut, n nh cht lng u ra ca sn phm.

    Cc bin i

    Ha hc: xy ra cc phn ng thy phn nhng khng ng k.

    Ha sinh: cc enzyme bv hot.

    Thit bvthng scng ngh

    Thc hin trong cng thit bdch ha.

    Nng HCl 0,1N.

    pH v hot l 4,25,7.

    Nhit : 95oC

    Thi gian: 510 pht.

    Tc cnh khuy: 200 vng/ pht.

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    Nhom 22 33 Lp: Hc11Tp

    Bng 14.n nh ca Termamyl

    2.2.7 Lc- Sdng thit bging quy trnh 1- Thng sthit b: Nhit lc: 85900C. Kch thc li lc: 0,05 mm. p sut: 25 bar.

    2.2.8 Trao i ionMc ch cng ngh:hon thinHon thin cht lng sn phm, loi b cc cht khng tt cho sn phm. Dch

    maltodextrin trong hn.

    Cc cht c mu, c mi, protein, cc tp cht tch in sbgili trn cc cationit v

    anionit, 95% cht khong, 70% cc hp cht c cha nitv 80% cc cht mu sb tch ra

    trong qu trnh ny. Cht lng cm quan ca sn phm tt hn.

    Cc bin i

    Bin i ho hc: ti cc ct xy ra cc phn ng trao i ion

    Ti ct cationit c cc ht nha polystyrene - divinylbenzen c gn mt s iondng, nh H+, -SO3H, -COOH, c tc dng chuyn cc mui trong dung dch

    thnh cc acid tng ng:

    RSO3H + NaClRSO3Na +HCl

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    CNCB Maltodextrin t khoai lang GVHD: PGS.TS Le Van Viet Man

    Nhom 22 34 Lp: Hc11Tp

    RSO3H +CaSO4(RSO3)2Ca + H2SO4

    Ti ct anionit c cc ht nha trn nhng gn vo 1 nhm bazo yuNR3, c tcdng hp thcc acid mnh, cc cht hu c, cht mu

    NR3+ HClNR3HClNR3+H2SO4(NR3)2H2SO4

    Ngoi tnh cht trao i ion dng v m (tp cht) trong dung dch, cc cht traoi ion dng trong cng nghip ny cn c tnh hp ph, hp ph tt cc

    aminoacid, furrurol, cc hp cht hu c khc, khnng tch mu tng ln.

    Bin i vt l: Sau khi i qua ct cationit, pH dung dch sgim xung rt thp (pH =2).

    Tuy nhin sau khi c a qua ct anionit, pH ca n s tng ln cao hn (pH=5 hoc cao

    hn).

    Bin i cm quan: 80% cht mu cng cc tp cht c tch bnn dch maltodextrin

    strng v trong hn.

    Bin i ho l: khng gy ra sbin i vpha.

    Bin i sinh hc v ho sinh: khng gy ra nhng bin i vsinh hc v ho sinh.

    Thit bvthng scng ngh:

    Bn cht ca phng php l stng tc gia dch maltodextrin v pha rn c cha sn

    cc ion, c thi chvi cc ion c trong ngun dch cn xl (Ca2+, Na+, Cl-, Mg2+, SO42-,

    mt scht hu c)

    Thit b: thit btrao i ion.

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    Nhom 22 35 Lp: Hc11Tp

    Hnh 17.C chtrao i ion

    Hnh 18.Thit btrao i ion

    y l thit bdng hnh tr, c y a, chu c p lc. Chiu cao tng nha t1-

    1,5m.

    Gm 2 ct hnh tr, mi ct c cha mt loi nha trao i ion. Ct thnht gm cationit loi acid mnh, c nhm chc -SO3H. Ct thhai gm anionit loi kim yu, c nhmNR3.

    Nguyn tc: dung dch c bm vo ct 1 loi cation sau a qua ct 2 tip tc

    loi anion v iu chnh pH cho dung dch. Hng chuyn ng ca dung dch ttrn xung,

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    CNCB Maltodextrin t khoai lang GVHD: PGS.TS Le Van Viet Man

    Nhom 22 36 Lp: Hc11Tp

    nha nh l mt tm m, cch n gin nht tng nha l y ct vo y ca thng.

    ng thi lp ct ny c chc nng hn chschy tri ca cc ht nha trao i ion theo

    dng ra ca dch maltodextrin quaxl. Sau khi lp nha ny ht tc dng c thti sinh

    trli. a cationit v dng ban u, cho dung dch HCl 2- 4% chy qua ct 1. V a

    anionit vdng ban u bng cch cho dung dch NaOH 2- 4% qua ct 2.

    Nhit tin hnh: 70 - 750C.

    2.2.9 C c bng membraneMc ch cng ngh: chun bv khai thc

    Chun b: qu trnh c c bng membrane nhm chun bcho qu trnh sy, gip lm

    gim mt lng nc kh ln trc khi a vo sy, gim nng lng v thi gian cho qu

    trnh sy.

    Khai thc: qu trnh phn ring bng membrane gip tch bt nc ra khi dch

    maltodextrin, lm tng nng cht kh ln.

    Cc bin i

    Bin i vt l: nht dung dch, khi lng ring, t trng v nng cht kh ca sau c c tng.

    Bin i ho hc:- Cc vitamin trong nc b tht thot. Bin i sinh hc:- c ch v tiu dit cc vi sinh vt do nng cht kh cao.Thit bvthng scng ngh

    Thit b: sdng thit bc c membrane.

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    Nhom 22 37 Lp: Hc11Tp

    Hnh 19.M hnh c c bng membrane

    Nguyn l hot ng:

    Mng lc NF (Nano Filltration) hot ng trn c chchuyn ng ca cc phn tnc

    nhp lc nn ca my bm cao p to ra mt dng chy mnh y cc phn tnc chuyn

    ng mnh v chui qua lmng, khi ta thu c dng dch maltodextrin c. Tin hnh

    hon lu nu nng dch ra cha t yu cu k thut.

    Thng scng ngh:

    Bdy: 150m Kch thc l: 5 nm.

    Hnh 20.Hthng thm thu thc ttrong cng nghip

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    Nhom 22 38 Lp: Hc11Tp

    M hnh: dng nhiu ng ng. p sut qu trnh: 40 bar. Nhit : 550C. Nng cht kh: 30 - 35 %.

    2.2.10 Sy phun- Thit bging quy trnh 1.Thng scng ngh

    Nhit tc nhn sy vo: 350oC p sut bm cao p: 10 - 15 bar. m sn phm: khng qu 5-6% Thi gian sy: 10 - 15s.

    2.2.11 Bao gi3. So snh hai qui trnh cng ngh

    Bng 15.So snh hai quy trnh cng ngh

    Cc chtiu Quy trnh 1 Quy trnh 2

    Qu trnh ty

    mu

    Than hot tnh l cht dkim,

    rtin.

    Nha c gn cht trao i ion vi

    dch maltodextrin t tin hn.

    Qu trnh lcSau khi ty mu bng than hot

    tnh phi c qu trnh lc tch

    than v tp cht.

    Khng cn c qu trnh lc sautrao i ion nhng cn lc trc

    khi vo ct trnh tc nghn.

    Qu trnh v hot

    enzyme

    Sdng nhit cao. Cn thm

    thit btrao i nhit bn mng

    nng nhit c chhot ng

    ca enzyme.

    Tn chi ph nng lng.

    Sdng cht ho hc acid HCl.

    V hot enzyme trong chnh thit

    bdch ho.

    Khng tn thm nng lng cho

    v hot enzyme nhng cn thit btrao i ion loi bHCl d.

    Thit bn mn.

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    CNCB Maltodextrin t khoai lang GVHD: PGS.TS Le Van Viet Man

    Nhom 22 39 Lp: Hc11Tp

    Bng 16.So snh chung vhai quy trnh

    c im Quy trnh 1 Quy trnh 2

    Thit b Thit bn gin hn Thit bphc tp hn

    Din tch nh xng t chim hn Nhiu hn

    Vsinh thit bDhn Kh hn

    Nng lng Tiu tn hn t hn

    III. SN PHM1. Tnh cht vt l ca Maltodextrin

    Bng 17.Tnh cht vt l ca Matodextrin

    Maltodextrin(C6H10O5)n.H2O

    KLR (g/cc) DE pH Tnh cht

    0,3-0,5 4-20 4,0-7,0

    Bt mu trng, d sy kh, tht mKhng ngt hoc t ngt, tan tttrong cho dung dch khng mu.

    Maltodextrin l sn phm thy phn tinh bt khng hon ton bi enzyme hoc acid, l

    hn hp cc polyme c n vl D glucose c ng lng dextrose DE di 20.

    Tu theo DE l bao nhiu m sn phm bt Maltodextrin c sdng cho nhng mcch cng nghkhc nhau. qui trnh ny sn xut Maltodextrin c DE = 9-12.

    Maltodextrin c DE = 9-12 ng dng trong:

    Cng nghip sn xut ung, c bit l ung cho trem.

    Qu trnh c c

    Dng tc nhn nhit, sn phm

    dbnh hng cht lng cm

    quan (mu sm). Nng cht

    kh cao hn.

    Thit bc c membrane n

    gin, dvn hnh, nng sut ln,

    tit kim chi ph nng lng. Tuy

    nhin, nng cht kh thp vchim din tch nh xng cao

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    CNCB Maltodextrin t khoai lang GVHD: PGS.TS Le Van Viet Man

    Nhom 22 40 Lp: Hc11Tp

    ung v thc n king cho cc ng vin ththao: dtiu ho, dho tan, tnggi trdinh dng cho sn phm.

    Lm cht trsy, cht gihng, yu tto hnh.2. Cc chtiu cht lng sn phm

    Sn phm t ngt, t ht m, hm lng glucose 0.8%, maltose 2.9% cht kh.

    Chtiu cm quan: bt mn, mu trng.

    Chtiu ho lho hc:

    m: 5% pH: 6,5 - 7 tan: 98%

    mn: 99.6% (qua lry 150 mm) DE: 912 Tro: 0.3% Hm lng kim loi nng: khng c.

    Chtiu vi sinh

    Tng svi khun hiu kh: < 3000 Cfu/g Coliform: < 30 Cfu/100g E.coli: 0 Samolnella: 0

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    Nhom 22 41 Lp: Hc11Tp

    TI LIU THAM KHO

    1. L Vn Vit Mn v cng s(2004). Cng nghchbin sa v cc sn phm tsa.Tp.HCh Minh,NXB i Hc Quc Gia Tp. HCh Minh.

    2. L Vn Vit Mn v cng s(2011). Cng nghchbin thc phm, ti bn ln 2.Tp. HCh Minh,NXB i Hc Quc Gia Tp. HCh Minh.

    3. L Ngc T & cng s. (2002).Ho sinh cng nghip.H Ni, Khoa hc v kthut.4. JohnM.deMan. (1999). Principle of food chemistry, third edition. United States ofAmerica, Aspen Publishers.

    5. Martin F. Chaplin, C. B. (1990). Enzyme Technology. New York: The press syndicate ofthe University of Cambridge.

    6. Wang, Y.; Wang, L.; Starch. 2000, 52, 8.7. Storz, E.; Steffens, K.; Starch. 2004, 56, 1.8. Williams, P. C.; Kuzina, D. F.; Hlinka, I.; Cereal Chem. 1970, 47, 1979. Mazurs, E. G.; Schoch, T. J.; Kite, F. E.; Cereal Chem. 1957, 34, 3.10. Leach, H. W.; McCowen, L. D.; Schoch, T. J.; Cereal Chem. 1963, 36, 6.11. Whistler, R. L; Paschall, E. F.; Starch: Chemistry and Technology, 2th ed., Academic Press:N.Y., 1984, p. 1-718

    12. Franco, L. M. C.; Ciacco, F. C.; Starch. 1988, 40, 113. J. Scott Smith; Y.H Hui; Food ProcessingPrinciples and Applications.14. UNIFEM.1988. Cereal Processing. 3stfood cycle technology source book. New york, NY10017 USA, 1988, printed by photosystem, S.r.l in Rome, Italy.