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This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
01/16/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha Labs200mg froggies
N/AMatrix : Edible
Certificateof Analysis
SAMPLE:DA00109009-002Harvest/Lot ID: cono1913
Seed to Sale #n/aBatch Date :N/A
Batch#: cono1913Sample Size Received: 56 gram
Ordered : 01/08/20Sampled : 01/08/20
Completed: 01/16/20 Expires: 01/16/21Sampling Method: SOP Client Method
Jan 16, 2020 | Green Roads5150 SW 48TH WAY DAVIEFL, USA 33314
PASSEDPage 1 of 5
PRODUCT IMAGE SAFETY RESULTS MISC.
PesticidesPASSED
Heavy MetalsPASSED
MicrobialsPASSED
MycotoxinsPASSED
ResidualsSolventsPASSED
FilthNOT TESTED
Water ActivityNOT TESTED
MoistureNOT TESTED
TerpenesTESTED
CANNABINOID RESULTS
Total THC
0.000%THC/Container :0.00 mg
Total CBD
0.334%CBD/Container :187.04mg
Total Cannabinoids
0.334%
CBC CBGA CBG THCV D8-THC CBDV CBN CBDA CBD THCA D9-THC
ND ND ND ND ND ND ND ND 0.334 % ND ND
ND ND ND ND ND ND ND ND3.340mg/g ND ND
0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.0001 0.001 0.0001
Cannabinoid Profile TestAnalyzed by Weight Extraction date : Extracted By :1224 3.0883g NA NA
Analysis Method -SOP.T.40.020, SOP.T.30.050Analytical Batch -DA009266POT Instrument Used : DA-LC-003 Batch Date : 01/09/20
Reagent Dilution Consums. ID
123019.R09 40 76124-662070219.R15 SFN-BX-1025010920.R05 849C4-849AK010920.R04 840C6-840HFull spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method:SOP.T.30.050 for sample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1mg/L).
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
01/16/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha Labs200mg froggies
N/AMatrix : Edible
Certificate of Analysis PASSED
Green Roads
5150 SW 48TH WAY DAVIEFL, USA 33314Telephone: (844) 747-3367Email: [email protected]
Sample : DA00109009-002Harvest/LOT ID: cono1913
Batch# : cono1913Sampled : 01/08/20Ordered : 01/08/20
Sample Size received : 56 gramCompleted : 01/16/20 Expires : 01/16/21Sample Method : SOP Client Method
Page 2 of 5
Terpenes TESTED
Terpenes LOD TEST RESULT (%)
ALPHA-CEDRENE 0.007 NDALPHA-HUMULENE 0.007 NDALPHA-PINENE 0.007 NDALPHA-TERPINENE 0.007 NDBETA-MYRCENE 0.007 NDBETA-PINENE 0.007 NDBORNEOL 0.013 NDCAMPHENE 0.007 NDCAMPHOR 0.013 NDCARYOPHYLLENE OXIDE 0.007 NDCEDROL 0.007 NDALPHA-BISABOLOL 0.007 NDISOPULEGOL 0.007 NDCIS-NEROLIDOL 0.007 ND3-CARENE 0.007 NDFENCHYL ALCOHOL 0.007 NDHEXAHYDROTHYMOL 0.007 NDEUCALYPTOL 0.007 NDISOBORNEOL 0.007 NDFARNESENE 0.007 NDFENCHONE 0.007 NDGAMMA-TERPINENE 0.007 NDGERANIOL 0.007 NDGERANYL ACETATE 0.007 NDGUAIOL 0.007 NDLIMONENE 0.007 NDLINALOOL 0.007 NDNEROL 0.007 NDOCIMENE 0.007 NDALPHA-PHELLANDRENE 0.007 NDPULEGONE 0.007 NDSABINENE 0.007 NDSABINENE HYDRATE 0.007 ND
Terpenes LOD TEST RESULT(%)
TERPINEOL 0.007 ND
TERPINOLENE 0.007 ND
BETA-CARYOPHYLLENE 0.007 ND
TRANS-NEROLIDOL 0.007 ND
VALENCENE 0.007 ND
Terpenes TESTED
Analyzed by Weight Extraction date Extracted By1118 0.9710g 01/09/20 1118
Analysis Method -SOP.T.40.090Analytical Batch -DA009267TERInstrument Used : Liquid Injection GCMS QP2020 (E-SHI-128)Batch Date : 01/09/20
Reagent Dilution Consums. ID
052119.04 10 76124-662280630187
Terpenoid profile screening is performed using GC-MS with Liquid Injection(Gas Chromatography – Mass Spectrometer) which can screen 38 terpenesusing Method SOP.T.40.091 Terpenoid Analysis Via GC/MS.
Total 0
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
01/16/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha Labs200mg froggies
N/AMatrix : Edible
Certificate of Analysis PASSED
Green Roads
5150 SW 48TH WAY DAVIEFL, USA 33314Telephone: (844) 747-3367Email: [email protected]
Sample : DA00109009-002Harvest/LOT ID: cono1913
Batch# : cono1913Sampled : 01/08/20Ordered : 01/08/20
Sample Size received : 56 gramCompleted : 01/16/20 Expires : 01/16/21Sample Method : SOP Client Method
Page 3 of 5
Pesticides PASSED
Pesticides LOD Action Level Units ResultCHLORDANE 0.005 0.1 ppm NDCAPTAN 0.05 3 ppm NDBOSCALID 0.01 3 PPM NDDIMETHOATE 0.01 0.1 ppm NDAZOXYSTROBIN 0.01 3 ppm NDABAMECTIN B1A 0.02 0.3 ppm NDCIS-PERMETHRIN 0.05 1 ppm NDSPINETORAM 0.01 3 PPM NDACEPHATE 0.001 3 ppm NDFENOXYCARB 0.01 0.1 ppm NDDIMETHOMORPH 0.005 3 ppm NDBIFENAZATE 0.01 3 ppm NDETHOPROPHOS 0.01 0.1 ppm NDACEQUINOCYL 0.01 2 ppm NDACETAMIPRID 0.01 3 ppm NDETOFENPROX 0.01 0.1 ppm NDBIFENTHRIN 0.01 0.5 ppm NDALDICARB 0.02 0.1 ppm NDETOXAZOLE 0.01 1.5 ppm NDFENPYROXIMATE 0.01 2 ppm NDFIPRONIL 0.02 0.1 ppm NDFENHEXAMID 0.01 3 ppm NDCARBARYL 0.01 0.5 ppm NDCARBOFURAN 0.01 0.1 ppm NDFLONICAMID 0.01 2 ppm NDFLUDIOXONIL 0.01 3 ppm NDCHLORFENAPYR 0.01 0.1 ppm NDCHLORANTRANILIPROLE 0.01 3 ppm NDHEXYTHIAZOX 0.01 2 ppm NDCHLORPYRIFOS 0.01 0.1 ppm NDIMAZALIL 0.01 0.1 ppm NDMALATHION 0.01 2 ppm NDCLOFENTEZINE 0.01 0.5 ppm NDDAMINOZIDE 0.02 0.1 ppm NDIMIDACLOPRID 0.01 3 ppm NDMETALAXYL 0.01 3 ppm NDDICHLORVOS 0.05 0.1 ppm NDMETHIOCARB 0.01 0.1 ppm NDCOUMAPHOS 0.005 0.1 ppm ND
Pesticides LOD Action Level Units ResultMETHOMYL 0.01 0.1 ppm NDKRESOXIM-METHYL 0.01 1 ppm NDDIAZANON 0.01 0.2 ppm NDCYPERMETHRIN 0.01 1 ppm NDMEVINPHOS 0.01 0.1 ppm NDMYCLOBUTANIL 0.01 3 ppm NDNALED 0.01 0.5 ppm NDOXAMYL 0.01 0.5 ppm NDPACLOBUTRAZOL 0.01 0.1 ppm NDTRANS-PERMETHRIN 0.05 1 ppm NDPHOSMET 0.01 0.2 ppm NDPIPERONYL BUTOXIDE 0.01 3 ppm NDPRALLETHRIN 0.05 0.4 ppm NDPROPICONAZOLE 0.01 1 ppm NDPROPOXUR 0.01 0.1 ppm NDPYRETHRIN I 0.01 1 ppm NDPYRIDABEN 0.01 3 ppm NDSPINOSAD (SPINOSYN A) 0.01 3 ppm NDSPINOSAD (SPINOSYN D) 0.01 3 ppm NDSPIROMESIFEN 0.01 3 ppm NDSPIROTETRAMAT 0.02 3 ppm NDSPIROXAMINE 0.01 0.1 ppm NDTEBUCONAZOLE 0.01 1 ppm NDTHIACLOPRID 0.01 0.1 ppm NDTHIAMETHOXAM 0.01 1 ppm NDTRIFLOXYSTROBIN 0.01 3 ppm ND
Pesticides PASSED
Analyzed by Weight Extraction date Extracted By585 0.9803g NA NA
Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch - DA009277PESInstrument Used : LCMS E-SHI-039Batch Date : 01/09/20
Reagent Dilution Consums. ID101519.04 180711010220.R05010220.R06
SOP.T.30.065, SOP.T.40.065
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
01/16/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha Labs200mg froggies
N/AMatrix : Edible
Certificate of Analysis PASSED
Green Roads
5150 SW 48TH WAY DAVIEFL, USA 33314Telephone: (844) 747-3367Email: [email protected]
Sample : DA00109009-002Harvest/LOT ID: cono1913
Batch# : cono1913Sampled : 01/08/20Ordered : 01/08/20
Sample Size received : 56 gramCompleted : 01/16/20 Expires : 01/16/21Sample Method : SOP Client Method
Page 4 of 5
Residual Solvents PASSED
SOLVENT LOD ACTIONLEVEL(PPM)
PASS/FAIL RESULT
PROPANE 120 2100 PASS ND
BUTANES (N-BUTANE) 96 2000 PASS ND
ETHYLENE OXIDE 0.6 5 PASS ND
METHANOL 22.5 250 PASS ND
ETHANOL 90 5000 PASS ND
PENTANES (N-PENTANE) 67.5 750 PASS ND
ETHYL ETHER 45 500 PASS ND
ACETONE 67.5 750 PASS ND
2-PROPANOL 45 500 PASS ND
ACETONITRILE 5.4 60 PASS ND
DICHLOROMETHANE 11.25 125 PASS ND
N-HEXANE 4.5 250 PASS ND
ETHYL ACETATE 36 400 PASS ND
BENZENE 0.09 1 PASS ND
HEPTANE 45 500 PASS ND
TOLUENE 13.5 150 PASS ND
CHLOROFORM 0.18 2 PASS ND
1,2-DICHLOROETHANE 0.18 2 PASS ND
TRICHLOROETHYLENE 2.25 25 PASS ND
1,1-DICHLOROETHENE 1 8 PASS ND
TOTAL XYLENES 13.5 150 PASS ND
Residual Solvents PASSED
Analyzed by Weight Extraction date Extracted By850 0.0252g 01/09/20 850
Analysis Method -SOP.T.40.032Analytical Batch -DA009287SOLInstrument Used : Headspace GCMSBatch Date : 01/09/20
Reagent Dilution Consums. ID
1 00268767161040-124152436
Residual solvents screening is performed using GC-MS which can detect belowsingle digit ppm concentrations. Currently we analyze for 34 Residual solvents.(Method: SOP.T.30.042 Residual Solvents Analysis via GC-MS).
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
01/16/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha Labs200mg froggies
N/AMatrix : Edible
Certificate of Analysis PASSED
Green Roads
5150 SW 48TH WAY DAVIEFL, USA 33314Telephone: (844) 747-3367Email: [email protected]
Sample : DA00109009-002Harvest/LOT ID: cono1913
Batch# : cono1913Sampled : 01/08/20Ordered : 01/08/20
Sample Size received : 56 gramCompleted : 01/16/20 Expires : 01/16/21Sample Method : SOP Client Method
Page 5 of 5
Mycotoxins PASSED
Analyte LOD Result Action Level(PPM)
AFLATOXIN G2 0.002 NDAFLATOXIN G1 0.002 NDAFLATOXIN B2 0.002 NDAFLATOXIN B1 0.002 NDOCHRATOXIN A+ 0.002 ND 0.02TOTAL AFLATOXINS 0.02 ND 0.02
Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch -DA009278Instrument Used : LCMS E-SHI-039Batch Date : 01/09/20
Analyzed by Weight Extraction date Extracted By585 1g NA NA
Microbials PASSED
Analyte LOD ResultASPERGILLUS_FLAVUS 10000 not present in 1 gram.ASPERGILLUS_FUMIGATUS 10000 not present in 1 gram.ASPERGILLUS_NIGER 10000 not present in 1 gram.ASPERGILLUS_TERREUS 10000 not present in 1 gram.ESCHERICHIA_COLI_SHIGELLA_SPP 10000 not present in 1 gram.SALMONELLA_SPECIFIC_GENE 10000 not present in 1 gram.TOTAL_YEAST_AND_MOLD 100 not present in 1 gram.
Analysis Method -SOP.T.40.043Analytical Batch -DA009268MICInstrument Used : PathogenDX PCR_Array ScannerBatch Date : 01/09/20
Analyzed by Weight Extraction date Extracted By513 1g NA NA
Heavy Metals PASSED
Reagent Dilution Consums. ID
010220.R09 50010820.R01010620.R02121319.R05010320.R03010220.R04111319.01
Metal LOD Result Action Level(PPM)
ARSENIC 0.01 ND 1.5CADMIUM 0.01 ND 0.5LEAD 0.01 ND 0.5MERCURY 0.01 ND 3
Analyzed by Weight Extraction date Extracted By53 0.2595g 01/09/20 457
Analysis Method -SOP.T.40.050, SOP.T.30.052Analytical Batch -DA009259HEAInstrument Used : ICPMS-2030Batch Date : 01/09/20
Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma – MassSpectrometer) which can screen down to below single digit ppb concentrations for regulated heavymetals using Method SOP.T.30.052 Sample Preparation for Heavy Metals Analysis via ICP-MS andSOP.T.40.050 Heavy Metals Analysis via ICP-MS.