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MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLES RIK JONCKHEERE, BART BAUDEMPREZ, TOBIAS WAEHLER A , DIETER VAN DEN HEUVEL, HEIKO SCHMALFUß A , OLIVER BRUX A , PETER DREß A , CHRISTOPH KAPPEL B , LEANDER ZICKLER B A SÜSS MICROTEC PHOTOMASK EQUIPMENT GMBH & CO.KG B NANOMETRICS

MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

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Page 1: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

MINIMIZING PARTICLE CONTAMINATION

OF NXE3100 RETICLES

RIK JONCKHEERE, BART BAUDEMPREZ, TOBIAS WAEHLER A,

DIETER VAN DEN HEUVEL, HEIKO SCHMALFUß A, OLIVER BRUX A,

PETER DREß A, CHRISTOPH KAPPEL B, LEANDER ZICKLER B

A SÜSS MICROTEC PHOTOMASK EQUIPMENT GMBH & CO.KG

B NANOMETRICS

Page 2: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

OUTLINE

Introduction: ADT learning

Installed infrastructure

Monitoring NXE3100 reticles

▸ Back-side

▸ Front-side

EUV pod related

Conclusions

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS 2

Page 3: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS 3

Page 4: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

BACK-SIDE PARTICLES

CAUSE OVERLAY ISSUES

Recovering required manual clean of reticle clamp.

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS 4

Particle on clamp Reference data After clamp cleaning

Originally it was the main reason why imec installed

a mask cleaner (HamaTech* MaskTrack Pro): AVOIDANCE

ADT

* Now Suss MicroTec

Page 5: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS 5

Page 6: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

LEARNING CURVE

FOR EUV RETICLE HANDLING

Manual

loading

Shipping

box ADT

Mask

shop

- Mask not cleaned

- Shipping

- Manual handling

- SB not cleanable SB

Mask

cleaned

Manual

loading

Shipping

box ADT

Mask

shop

MT-Pro

- Shipping

- Manual

handling

- SB not

cleanable SB SB

NXE Mask

shop MT-Pro

- (Almost) free of

manual reticle handling

- Cleanable

EUV pod

EUVpod

NXE Mask

shop MT-Pro

EUVpod EUVpod - Free of manual

reticle handling

- Cleanable

EUV pod

RSP200

6 R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS

(Type A)

GOAL: reduction of particle adders caused by ...

ADT situation before MT-Pro

ADT situation with MT-Pro

Present situation for NXE3100 environment

Target situation for NXE3100 environment

1) 2)

one universal EUV pod

(“Type B” ?) (Type A ?)

Note: Type A vs. B see SEMI E152

Page 7: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

UNIQUE INFRASTRUCTURE REALIZED INTEGRATING CLEANING, BACK-SIDE INSPECTION

AND AUTOMATED HANDLING OF NXE3100 RETICLES

7

NXE3100

Facility IN

Dry Flip

Soft RTP

172 nm UV

Exposure Wet

Transfer

Final Clean Pre Clean

Aligner Buffer Buffer

Dual Pod

Load Port

EIP

Library

Backside Particle

Inspection

Exchange

Port

Reticle Transfer

Handling

EIP

Transfer

Handling

Transfer Handling

MaskTrack Pro Cleaner MT Pro InSync

Aligner

Mask shop

EU

V P

OD

Typ

e A

Was for ADT)

SPARK

SMIF

Load Port

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS

Page 8: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

RETICLE BACK-SIDE INSPECTION

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS 8

Darkfield full substrate imaging technology

Typical Performance

Reticle

SPARK-RIM

Assignment of a size to a detection is based on the intensity of the scattered light!

DISCLAIMER: Calibration done for PSL. Mind that the sizing accuracy

for an arbitrary “defect” with a given shape and morphology may be limited.

Particle detection size 150nm (via PSL)

Routine use (back-side) >95% capture rate >250nm

Defect size repeatability >90%

Measurement time < 5min

Defect detection on front-side Empty areas, needs dedicated calibration

integrated

in InSync

Page 9: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

OUR TARGET SCENARIO FOR MASK HANDLING

New NXE3100 reticles ▸ Receive the reticle in EUV pod.

▸ Inspect reticle back-side on SPARK.

▸ Evaluate inspection results against practical target “OK for NXE3100” - If OK: Reticle in Type A EUV Pod can be moved to Scanner

- If not OK: Clean reticle to reach OK status ( + follow-up if not possible)

▸ Reticle mates with fixed EUV pod.

Routine check of NXE3100 reticles in use

(particle monitoring) ▸ Same way, automated, via its EUV pod Type A in use on the NXE3100

All via fully automated handling within MT Pro + InSync

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS 9

Page 10: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

OUR PRESENT SCENARIO FOR MASK HANDLING

New NXE3100 reticles ▸ The reticle is received from the mask shop in ...

- ... shipping box: manual load into RSP200, auto transfer into EUV pod on InSync

- ... RSP200: auto transfer into EUV pod on InSync

- ... EUV pod: so far it was not yet fully considered shippable

▸ Reticle back-side is inspected on SPARK.

▸ Evaluate inspection results against practical target “OK for NXE3100”

Still operator decision (inspired by # detections)

▸ Reticle mates with fixed EUV pod.

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS 10

Page 11: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

OUTLINE

Introduction: ADT learning

Installed infrastructure

Monitoring NXE3100 reticles

▸ Back-side

▸ Front-side

EUV pod related

Conclusions

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS 11

Page 12: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

Size bin (µm)

BACK-SIDE INSPECTION BY SPARK EXAMPLE 1: OUR NXE3100 MONITOR RETICLE

▸ Monitor reticle used 2-3x/week

▸ It has several detections >1um

▸ Many cleanable,

yet some cleaning-resistant (clamping artifacts ?).

▸ Yet, the reticle gives persistent good overlay.

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS 12

Dec 2011 July 2012

Only detections > 1µm shown

Reminder: size of DETECTION

(real size unknown)

reticle clean

0

100

200

300

1 - 2 2 - 5 5 -10 10-20 20-50

# D

ete

ctio

ns

Detection binning

Page 13: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

SUDDEN OVERLAY EXCURSION

Printed overlay suffered

from increased residuals

in distortion map

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS 13

Dec 2011

23/07/2012

26/07/2012 27/07/2012

03/08/2012

reticle clean

Page 14: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

Printed overlay correlates to SPARK measurements (residual).

Origin of this overlay killing particle unknown.

Could not yet AVOID particle on clamp by monitoring.

Recovered from bad overlay via clamp clean by “stamping”.

SUDDEN OVERLAY EXCURSION

FOUND DUE TO PARTICLE ON RETICLE CLAMP

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS 14

Printed overlay

3 Detections:

1, 6 and 26 µm.

But all reduced

to sub-critical

by reticle clean.

Mask backside (Before cleaning)

Page 15: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

BACKSIDE MONITORING NXE3100 MONITOR RETICLE

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS

OK

“Not OK” ? (= Large number

of large detections)

# D

ete

ctio

ns

15

Number of large detections not really feasible as criterion.

Size binning has no info on height:

How interpret if overlay sensitive ?

Define threshold

of acceptable number ?

Cle

anin

g done

Page 16: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

BACK-SIDE INSPECTION, EXAMPLE 2: RETICLE WITH LOADING HISTORY

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS 16

20x c

lam

pin

g

on

reti

cle

sta

ge

# D

ete

ctio

ns

Only detections > 1µm shown

Need way to differentiate between chuck artifacts and

(potentially) overlay-critical particles.

Page 17: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

BACK-SIDE INSPECTION, EXAMPLE 3: RETICLE WITHOUT LOADING HISTORY

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS 17

Fre

sh, n

o p

rior

use

Use

d for

exposu

res

Use

d for

expo

sure

s

Use

d for

exposu

res

...

# D

ete

ctio

ns

Adder examples

Added by first use Adder examples

Lost by

first use ?

Target of monitoring is to flag

potentially overlay-critical particle adders.

Page 18: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

OUTLINE

Introduction: ADT learning

Installed infrastructure

Monitoring NXE3100 reticles

▸ Back-side

▸ Front-side

EUV pod related

Conclusions

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS 18

Page 19: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

MONITORING FOR FRONT-SIDE ADDERS

▸ Evaluation by wafer printing + wafer inspection + repeater analysis - Estimated capability for particles/defects >~60 nm

- Note: at 32nm l/s: ~30nm would be printable (= causing >10% CD change)

▸ Procedure: - Keep reference wafer, exposed when reticle was new(er)

- After additional use of the reticle, expose a new wafer with multiple dies

- Via wafer inspection check for repeating defects across multiple dies

- Upon finding new repeaters check on reference exposure whether it was

already there (but possibly missed by wafer inspection)

- Absence on the reference wafer confirms it is new adder on the reticle

Has been very valuable in the past to identify adders by handling

(manual transfer, shipping, ...)

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS 19

reference new repeaters

Not present on ...

added particle

exposed die

Page 20: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

FRONT-SIDE ADDERS DURING EXPOSURE

After minimizing adders related to handling

in the fab, the technique reveals also

other adder contributors: inside the scanner

(reminder: pellicle-less is EUV specific)

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS 20

Note: imec’s NXE3100 does not include all ASML’s latest mitigation techniques

1 2 3 4

5 6 7 8

...

...

1 2 3 4

5 6 7 8

...

...

1

2

3

4

5

6

7

8

Page 21: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

EUV POD RELATED...

EUV pod status ▸ So far only Entregris pods Type A in use at imec.

▸ Imec ordered modified Type B of Entegris (InSync requiring “pockets”).

▸ The latter is now less relevant because of shipping data for Type A ?

▸ Gudeng pods: More recently qualified for NXE3100 by ASML. Modification

to InSync EIP gripper scheduled. Hence not used at imec so far.

EUV pod cleanliness testing (Entegris Type A)

▸ 1st test via 20x open/close cycling on InSync + SPARK measurement of blank:

no adder for new pod, nor for one after ~10 months of use

Shipping results in EUV pods (Entegris Type A)

▸ 2 blanks, prequalified on SPARK, sent back and forth to US, one site each

- Front-side : both plates have zero adders >250nm

- Back-side : 1st plate has 2 adders >1µm, 2nd plate has 6 such adders

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS 21

Need to establish shipping by/from mask shop in EUV pod !!

(= removable hard pellicle, assuring FS cleanliness)

Page 22: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

CONCLUSIONS

▸ Infrastructure in place for integrated cleaning, automated

handling and back-side inspection of NXE reticles

(interfaced to scanner via EUV pods).

▸ Particle adders by on-site handling are minimized.

▸ Very valuable for learning about particle contamination of NXE reticles,

and avoiding it.

▸ Back-side monitoring helps a lot to trace overlay critical particles,

but still misses capability to differentiate between those

and other (large) detections.

▸ Infrastructure and procedures (partially) in place ...

allow to reveal possible particle adders due to the scanner

(further mitigation by ASML ongoing).

▸ The next step according to us is ...

To start using EUV pods for reticle shipping from the mask shop.

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS 22

Page 23: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,

ACKNOWLEDGEMENTS

▸ Colleagues at imec:

Jan Hermans, Christiane Jehoul, Rudi De Ruyter, Jan Hermans,

Eric Hendrickx, Kurt Ronse, Geert Vandenberghe

▸ ASML: local team at imec, Carmen Zoldesi, Michael O’Connor,

Mircea Dusa, Noreen Harned, John Zimmerman

▸ Suss: Wilma Koolen-Hermkens*, Uwe Dietze, Manfred Zimmermann

▸ Nanometrics: Lars Markwort, Greg Savage, Andreas Reichel

▸ Partners in Advanced Litho Program for encouragement

▸ Suss + imec acknowledge EC for project FP7 SEAL (SP2)

R. JONCKHEERE @ EUVL SYMPOSIUM 2012, BRUSSELS 23

* Now at TNO

Page 24: MINIMIZING PARTICLE CONTAMINATION OF NXE3100 RETICLESeuvlsymposium.lbl.gov/pdf/2012/pres/R. Jonckheere.pdf · minimizing particle contamination of nxe3100 reticles rik jonckheere,