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D. W. Herrin, Ph.D., P.E. University of Kentucky Department of Mechanical Engineering Measurement of Bulk Materials

Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

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Page 1: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

D. W. Herrin, Ph.D., P.E. University of Kentucky

Department of Mechanical Engineering

Measurement of Bulk Materials

Page 2: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

2

Motivation

  Determining the bulk properties ü  Complex wave number and characteristic impedance ü  Complex speed of sound and density

  Bulk properties are used ü  For designing layered absorbers ü  In FEM and BEM models

Page 3: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

3

Overview of Approaches

Direct Measurement

Measure Sound Absorption

Measure Flow Resistance

Ø  Two load method ASTM E 1050 Ø  Two cavity method Utsuno, 1989 Ø  Three microphone method Iwase et al., 1998

Curve fit to find flow resistivity based on empirical equations Simon et al., 2006

Curve fit to find Biot parameters based on theory

Find bulk properties from fitted Biot parameters Allard, J. F., 1999

Find bulk properties from measured flow resistivity Wu, 1988; Mechel et al., 2002

Find bulk properties from measured flow resistivity Wu, 1988; Mechel et al., 2002

Page 4: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

4

Overview of Approaches

Direct Measurement

Measure Flow Resistance

Ø  Two load method ASTM E 1050 Ø  Two cavity method Utsuno, 1989 Ø  Three microphone method Iwase et al., 1998

Find bulk properties from measured flow resistivity Wu, 1988; Mechel et al., 2002

Page 5: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

5 5

Two-load Method

( )

1

,2,1

sin2

111

kseHeH

jAsljk

refjkl

ref+−− −

=

( )

1

,1.2

sin2

111

kseHeH

jBjkl

refsljk

ref −=

+

( )

2

,4,3

sin2

222

kseHeH

jCjkl

refsljk

ref −=

+

( )

2

,3,4

sin2

222

kseHeH

jDsljk

refjkl

ref+−− −

=

For each load:

ASTM E2611-09

1 2

s1 s2 l1 l2

d

A

B

C

D

3 4 x=0

Load a Load b

Page 6: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

6

( ) cBAuBAp

ρ/0

0

−=

+=( ) cDeCeu

DeCepjkdjkd

d

jkdjkdd

ρ/−=

+=−

Pressures and particle velocities at two ends of the sample:

Four-pole matrix

⎥⎥⎥⎥

⎢⎢⎢⎢

=

dadbdbda

adbbda

dadbdbda

dabdba

dadbdbda

dbadab

dadbdbda

dabdba

upupupup

upupuuuu

upuppppp

upupupup

T0000

0000

ASTM E2611-09

Transmission Loss Measurement

⎟⎟⎠

⎞⎜⎜⎝

⎛+++= 2221

121110 2

1log20 TcTcTTTL ρρ

Page 7: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

7

Load a and Load b

0

0.2

0.4

0.6

0.8

1

0 500 1000 1500 2000 2500 3000Frequency (Hz)

Abso

rptio

n C

oeffi

cien

t

Load A Load B

Load A: Open tube. Load B: Close the tube with 4” absorbing material.

Load B

Load A

ASTM E2611-09

Page 8: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

8

Two Load Method

Load 1

Load 2

Loudspeaker

Piston

Impedance tube

Microphones

Sample

1 2 3 4

1 2 3 4

Open

( ) ( )( ) ( ) ⎥⎦

⎤⎢⎣

⎡=⎥

⎤⎢⎣

dk/zdkjdkjzdk

DCBA

ccc

ccc

cossinsincos

djAzBk

B/Cz

cc

c

⎟⎟⎠

⎞⎜⎜⎝

⎛=

=

arctan

ASTM E2611-09

Page 9: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

9

Two Cavity Method

L d

L’ d

Cavity 1

Cavity 2

Loudspeaker Piston

Impedance tube

Microphones

( ) ( )( ) ( )''

''''

c zzzzzzzzzzzzz

1122

11222211

−−−

−−−±=

( )( )( )( )⎟

⎟⎠

⎞⎜⎜⎝

+−

−+⎟⎟⎠

⎞⎜⎜⎝

⎛=

cc

ccc zzzz

zzzzjd1k

21

21ln2

Utsuno,1989

z2 z1

z2 ’ z1

Page 10: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

10

Rigid End

L s

Microphones

Loudspeaker

Sample

d x

x = 0

1 2

3 A

B

Iwase et al., 1998

Three Microphone Method

Page 11: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

11

jkLjks

jks

eeHHe R 2

12

12−−

−=

Rigid end

L s

Microphones Sample

d x

x = 0

1 2

3

Speaker

Iwase et al., 1998

Three Microphone Method

Reflection coefficient:

Page 12: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

12

The complex wave number of the sample is:

231 1cos1 H

ReeR

dk jkLjkLc −

+

+=

The characteristic impedance of the sample is:

zc = jz01+ R1− R

tan kcd( )

Iwase et al., 1998

Three Microphone Method

Page 13: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

13

1 inch Melamine Foam

Melamine Characteristic Impedance

-4

-2

0

2

4

6

0 1000 2000 3000 4000 5000

Cha

ract

eris

tic Im

peda

mce

Frequency (Hz)

Three Microphone (Re) Three Microphone (Im) Two Cavity (Re) Two Cavity (Im) Two Load (Re) Two Load (Im)

Page 14: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

14

Melamine Complex Wave Number

1 inch Melamine Foam

-40

0

40

80

120

0 1000 2000 3000 4000 5000

Com

plex

Wav

e N

umbe

r (1/

m)

Frequency (Hz)

Three Microphone (Re) Three Microphone (Im) Two Cavity (Re) Two Cavity (Im) Two Load (Re) Two Load (Im)

Page 15: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

15

Melamine Sound Absorption Coefficient

1 inch Melamine Foam

0

0.2

0.4

0.6

0.8

1

0 1000 2000 3000 4000 5000

Abs

orpt

ion

Coe

ffici

ent

Frequency (Hz)

Two Load

Two Cavity

Three Microphone

Page 16: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

16

1 inch Melamine Foam

0

2

4

6

8

10

0 1000 2000 3000 4000 5000

Tran

smis

sion

Los

s (d

B)

Frequency (Hz)

Two Load

Two Cavity

Three Microphone

Melamine Transmission Loss

Page 17: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

17

1 inch Glass Fiber

Fiber Characteristic Impedance

-4

-2

0

2

4

0 1000 2000 3000 4000 5000

Cha

ract

eris

tic Im

peda

nce

Frequency (Hz)

Two Load (Re) Two Load (Im) Two Cavity (Re) Two Cavity (Im) Three Microphone (Re) Three Microphone (Im)

Page 18: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

18

1 inch Glass Fiber

Fiber Complex Wave Number

-40

0

40

80

120

0 1000 2000 3000 4000 5000

Com

plex

Wav

e N

umbe

r (1/

m)

Frequency (Hz)

Two Load (Re) Two Load (Im) Two Cavity (Re) Two Cavity (Im) Three Microphone (Re) Three Microphone (Im)

Page 19: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

19

Fiber Sound Absorption Coefficient

1 inch Glass Fiber

0

0.2

0.4

0.6

0.8

1

0 1000 2000 3000 4000 5000

Abs

orpt

ion

Coe

ffici

ent

Frequency (Hz)

Two Cavity

Two Load

Three Microphone

Page 20: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

20

Fiber Transmission Loss

1 inch Glass Fiber

0

2

4

6

8

10

0 1000 2000 3000 4000 5000

Tran

smis

sion

Los

s (d

B)

Frequency (Hz)

Two Cavity

Two Load

Three Microphone

Page 21: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

21

Comparison

Two Load Two Cavity Three Microphone

No. of Loads 2 2 1

No. of Calibrations 3 1 2

Smoothness of Curve Good Good Excellent

Page 22: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

22

Overview of Approaches

Direct Measurement

Measure Flow Resistance

Ø  Two load method ASTM E 1050 Ø  Two cavity method Utsuno, 1989 Ø  Three microphone method Iwase et.al., 1998

Find bulk properties from measured flow resistivity Wu, 1988; Mechel et al., 2002

Page 23: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

23

Measure Flow Resistance

Plug into Empirical Models Wu (1988) or Mechel et al. (2002)

Measure Flow Resistivity Using

ASTM C522

Vacuum source

u

ΔP Sample (thickness t )

Flow resistance:

uΔPrs =

Flow resistivity:

trσ s=

Wu, 1988; Mechel et al., 2002

Page 24: Measurement of Bulk Materialsweb.engr.uky.edu/~dherrin/Bandung/11_Bulk_Properties.pdf · Measurement of Bulk Properties Noise and Vibration Short Course Dept. of Mech. Engineering

Measurement of Bulk Properties

Noise and Vibration Short Course

Dept. of Mech. Engineering University of Kentucky

24

Summary

  Compared the various methods for determining the bulk properties of sound absorbers.

  Curve fitting approaches are adequate for common sound absorbing materials.