MARTIN COUNTY - documents.martin.fl.us · MARTIN COUNTY BOARD OF COUNTY COMMISSIONERS UTILITIES & SOLID WASTE DEPARTMENT PO Box 9000 Stuart, FL 34995-9000 John E. Polley Director

usd2017L394.docx

May 1, 2017

Department of Environmental ProtectionDomestic Wastewater ProgramDEP DW Shared [email protected]

Re: Martin County Utilities Tropical Farms WWTF, Facility # FL0043214Somatic coliphage monitoring report

Dear DEP:

Attached please see the report and supplemental documents on somatic coliphage monitoring of the Neutralizer biosolids treatment process prepared by BCR Environmental. Submittal of this report is a condition of permit revision FL0043214-016-DW1P-RM, Section VI, Schedules, #3.

Coliphage monitoring was performed by BCR for one year subsequent to placing the new Neutralizer process into operation at the facility.

If you have any questions, please contact William Thiel, Laboratory Manager, at (772) 223-7926 or by email [email protected].

Sincerely,

Todd Leyland Treatment Plant Operations Administrator

TL/wt/cbEnclosures

C: Curtis D. Robinson, P.E., Senior Engineer, Holtz Consulting Engineers, Inc., [email protected] Christian, Environmental Specialist, DEP, [email protected] Thiel, Laboratory Manager, [email protected] Plummer, Treatment Plant Operations Manager, [email protected] Rodriguez, Chief Plant Operator, [email protected]

DOUG SMITHCommissioner, District 1

ED FIELDINGCommissioner, District 2

HAROLD E. JENKINS IICommissioner, District 3

SARAH HEARDCommissioner, District 4

EDWARD V. CIAMPICommissioner, District 5

TARYN KRYZDA, CPM County Administrator

SARAH W. WOODSActing County Attorney

TELEPHONE772-288-5400

WEB ADDRESShttp://www.martin.fl.us

MARTIN COUNTYBOARD OF COUNTY COMMISSIONERS

UTILITIES & SOLID WASTE DEPARTMENTPO Box 9000 Stuart, FL 34995-9000

John E. PolleyDirectorPhone (772) 221-1442Fax (772) 221-1447

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mailto:[email protected]







4/27/2017 Laura Boczek EPA 26 West Martin Luther King Drive Cincinnati OH 45268 Dear Laura, On November 11th 2010, BCR Environmental submitted an equivalent PFRP process proposal and was approved by the PEC as a process that was equivalent to a PFRP process in accordance with 40 CFR 503.32(a)(8). In order for the Neutralizer to be operating as an equivalent PFRP process, the following conditions must be met:

The Neutralizer process is to be used to treat waste activated sludge with a total solids

concentration less than or equal to 4%

Process Operations must be at a temperature greater than or equal to 15°C (59°F)

Following addition of stage 1 Oxidant (chlorine dioxide) ORP is required to be maintained

at a value greater than or equal to +100 mV ORP with a contact time at +100 mV ORP ≥ 1

hour

Stage 1 treatment is followed by Stage 2 treatment which is defined as Nitrite dose = 1500

mg/L sodium nitrite (NaNO2) with pH during NaNO2 contact time ≤ to 2.3s.u.

ORP during stage 2 must be > +100 mV and nitrite contact time at specified pH and ORP is

at least 6 hours

A limitation on the evaluation of the process was claimed by the EPA because the three facilities that conducted Neutralizer testing were done within the same county (Clay). Therefore, new installations of a Neutralizer process must demonstrate pathogen reduction by verifying somatic coliphage reduction when operating as above. Sampling and analysis of somatic phage must be conducted for a period of at least one year in accordance to the sampling method described at 40 CFR 503.16 (a). This approval letter is attached for your reference. BCR performed this testing over a period of 12 months at North Jenson WWTP (3100 NW Hillman Drive, Jensen Beach, FL 34957) and all analyses resulted in ‘non-detect’ or greater than a 3-log reduction (greater than 99.9% reduction) for somatic phage using ASTM 4994, the test results are summarized below:

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North Jensen

Sample Date Raw Treated

10/21/2015 8440 0.9

2/9/2016 5710 ≤2

4/6/2016 3870 ≤3.7

7/12/2016 893 ≤10.1

10/11/2016 846 ≤4.6

BCR also performed five (5) somatic phage tests at Tropical Farms WWTP (8595 SW Kansas Avenue, Stuart, FL 34997) over a period of 12 months in 2015-2016. The table below summarizes these results:

Tropical Farms

Sample Date

Raw (PFU/dry gram)

Treated (PFU/dry gram)

10/21/2015 1580 ≤0.9

1/5/2016 17200 ≤1.2

4/6/2016 5420 ≤3.4

7/12/2016 1380 ≤9.4

10/11/2016 2250 ≤3.7

All samples were taken in accordance with sampling procedures detailed in the Neutralizer Process QAPP, which was previously approved by the PEC. All lab reports are also attached for your review. As BCR Environmental has met the requirements of this monitoring condition as specified in the National Equivalency approval letter dated Nov 16, 2010, we are requesting removal of the somatic phage sampling and analysis provision for the Neutralizer® process at these facilities. Sincerely,

Fred P Mussari

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October 26, 2015

Dr. Fred P. Mussari

BCR Environmental

3740 St. Johns Bluff Rd. S. Ste 21

Jacksonville FL 32224

[email protected]

904-819-9170

Client ID: TF-Raw, TF-Treated, NJ-Raw, NJ-Treated

Dear Dr. Fred P. Mussari,

BCS ID: 1510295, 1510296, 1510297, 1510298

We have completed the analysis of the submitted samples as outlined below.

Following, you will find our report on the results of the analysis coducted on the referenced samples. Should you have any questions, please do not hesitate to contact me.

Sincerely,

George Lukasik, Ph.D. Laboratory Director

Biological Consulting Services

of North Florida, Inc.

Project Name: MCUA Tropical Farms

Analysis Method

Fecal Coliforms MPN EPA 1681; SM 9221E; BCS SOP B-4

Coliphage BCS SOP V-11

Page 1 of 6

Final Report BCS ID 1510295, 1510296, 1510297, 1510298

4609 NW 6th Street, Ste. A, Gainesville, Florida 32609

BCS Laboratories, Inc. – Gainesville

www.microbioservices.com

Tel. (352) 377-9272, Fax. (352) 377-5630

FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 68-03950, EPA# FL01147

This report shall not be reproduced, except in full, without the written consent of BCS Laboratories

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Client: BCR Environmental


Analysis Start: October 23, 2015 11:35

PFU/mL sample analyzed

Secondary Value: 1,580

Analysis: Coliphage

Primary Value: 3,632

Amount Sampled: 50

Qualifier:

Analysis Stop Date: October 24, 2015 15:00

g

PFU /dry gram

Analysis Notes: None

Client Sample ID: TF-Raw BCS Sample ID: 1510295

Sampling Date: October 21, 2015 9:16

Analyst: David Sekora

Percent Solids: 4.6

Date Received: October 23, 2015 9:37 deg C7.9

Biosolids liquid

Ice: NoReceipt Temperature:

Sample Description:




Fecal Coliforms MPN/mL sample analyzed

Secondary Value: ≤0.4

Analysis: Fecal Coliforms MPN

Primary Value: ≤0.02

Amount Sampled: 198

Qualifier: U


mL

Fecal coliforms/dry gram

Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units

Client Sample ID: TF-Treated BCS Sample ID: 1510296


Analyst: Monique Bessette

Percent Solids: 4.3


Biosolids liquid


Sample Description:

Page 2 of 6





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Analysis: Coliphage


Amount Sampled: 50

Qualifier: U


g

PFU /dry gram

Analysis Notes: None; Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units




Percent Solids: 4.3


Biosolids liquid


Sample Description:


Project Name: MCUA North Jensen




Analysis: Coliphage


Amount Sampled: 50

Qualifier:


g

PFU /dry gram


Client Sample ID: NJ-Raw BCS Sample ID: 1510297



Percent Solids: 3.5


Biosolids liquid


Sample Description:

Page 3 of 6





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Amount Sampled: 183

Qualifier: U


mL



Client Sample ID: NJ-Treated BCS Sample ID: 1510298



Percent Solids: 4.6


Biosolids liquid


Sample Description:






Analysis: Coliphage


Amount Sampled: 50

Qualifier: U


g

PFU /dry gram


Client Sample ID: NJ-Treated BCS Sample ID: 1510298



Percent Solids: 4.6


Biosolids liquid


Sample Description:

Page 4 of 6





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I certify that I have personally examined and am familiar with the information submitted herein. Based on my inquiry of those individuals immediately responsible for obtaining the information, I believe the submitted information is true, accurate, and complete. The above results relate only the collected and referenced sample(s) and to their condition at the time of process. The analysis results are not indicative or representative of a process. Sampling and field data information was submitted by the client. The analysis and presented results in this report meet the requirements of The NELAC Institute (TNI), ISO 17025, and The State of Florida Department of Public Health’s Laboratory Certification Program, as applicable unless otherwise noted.


Project: MCUA Tropical Farms

Signature of Laboratory Director/Authorized Rep. _________________________ Date: ___________________October 26, 2015

Method Detection Limit: 1 microorganism/ unit weight or volume analyzed

Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed

Report Notes: None to report

Page 5 of 6





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SYMBOL MEANING

B Results based on counts outside the acceptable range.

D Measurement was made in the field.

I

The reported value is between the laboratory method detection limit and the laboratory practical

quantitation limit.

J1 The sample matrix interfered with the ability to make any accurate determination.

J2 No Quality Control criteria exist for the component.

J3 The data are questionable because of improper laboratory or field protocols.

L Off scale high. Actual value is known to be greater than value given.

N

Presumptive evidence for the presence of material. There is an indication that the analyte is present,

but the confirmation requirement was not met.

O Sampled, but analysis not performed.

Q Sample held beyond the accepted holding time.

U

Indicates that the compound was analyzed for but not detected. The specified component was not

detected. The reported value is the method detection limit.

V Analyte was detected in both sample and associated method blank. Data may not be accurate.

Y The laboratory analysis was from an improperly preserved sample. The data may not be accurate.

Z

Too many colonies present (TNTC); the numeric value given represents the upper end of the value that

can be determined based on the volume.

?

Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.

Presence or absence of analyte could not be confirmed.

** Not reported due to interference.

! Data deviate from historically established concentration range.

# BCS Lab specific qualifier. See laboratory analysis notes.

DATA QUALIFIER CODES

Page 6 of 6





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January 13, 2016

Dr. Fred P. Mussari

BCR Environmental

3740 St. Johns Bluff Rd. S. Ste 21


[email protected]

904-819-9170

Client ID: TF-Raw, TF-Treated

Dear Dr. Fred P. Mussari,

BCS ID: 1601008, 1601009


Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me.

Sincerely,





Analysis Method

Fecal Coliforms MPN EPA 1681; SM 9221E; BCS SOP B-4

Coliphage BCS SOP V-11

Page 1 of 5

Final Report BCS ID 1601008, 1601009




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Analysis Start: January 07, 2016 10:25



Analysis: Coliphage


Amount Sampled: 10.08

Qualifier:

Analysis Stop Date: January 08, 2016 10:08

g

PFU /dry gram



Sampling Date: January 05, 2016 15:00


Percent Solids: 3.5

Date Received: January 07, 2016 9:38 deg C2.9

Biosolids

Ice: YesReceipt Temperature:

Sample Description:








Amount Sampled: 84

Qualifier: U


mL






Percent Solids: 4.2


Biosolids


Sample Description:

Page 2 of 5





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Analysis: Coliphage


Amount Sampled: 50

Qualifier: U


mL

PFU /dry gram





Percent Solids: 4.2


Biosolids


Sample Description:

Page 3 of 5





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I certify that I have personally examined and am familiar with the information submitted herein. The results presented pertain only to the samples analyzed associated identifier number(s). Based on my inquiry of the individuals immediately responsible for obtaining the information, I believe the submitted data are true, accurate, and complete. Sampling field data information was obtained from the submitted sampling documents. The analysis was authorized commissioned by the client. The data provided is strictly representative of the analysis conducted on the material/samples/articles provided by the client (or client’s representative) it’s (their) condition at the time of test. The sample(s) were analyzed in accordance with the method described for each analyte, however due to the inherent limitation(s) of method(s), microorganisms may avoid detection. Thus, BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Positive, negative, and blank controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis results presented in this report meet the requirements of The NELAC Institute (TNI), ISO 17025, The State of Florida Department of Public Health’s Laboratory Certification Program, as applicable unless otherwise noted.


Project: MCUA Tropical Farms

Signature of Laboratory Director/Authorized Rep. _________________________ Date: ___________________January 13, 2016




Page 4 of 5





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SYMBOL MEANING



IThe reported value is between the laboratory method detection limit and the laboratory practical

quantitation limit.





N Presumptive evidence for the presence of material. There is an indication that the analyte is

present, but the confirmation requirement was not met.



UIndicates that the compound was analyzed for but not detected. The specified component was

not detected. The reported value is the method detection limit.


Y The laboratory analysis was from an improperly preserved sample. The data may not be

ZToo many colonies present (TNTC); the numeric value given represents the upper end of the

value that can be determined based on the volume.

?Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.






Page 5 of 5





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April 11, 2016

Casey Cochran

Nuterra Management

3740 St. Johns Bluff Rd South Suite 21


[email protected]

904-819-9170

Client ID: TF-Raw, TF-Treated

Dear Casey Cochran,

BCS ID: 1604064, 1604065



Sincerely,




Project Name: Tropical Farms

Analysis Method

Fecal Coliforms MPN EPA 1681; SM 9221E; BCS SOP B-4 (ISO17025 and TNI Accredited)

Coliphage BCS SOP V-11 (ISO17025 and TNI Accredited)

Page 1 of 5





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Client: Nuterra Management


Analysis Start: April 08, 2016 11:00



Analysis: Coliphage



Qualifier:

Analysis Stop Date: April 09, 2016 9:45

g

PFU /dry gram



Sampling Date: April 06, 2016 12:00

Analyst: David Sekora, M.S.

Percent Solids: 4.2

Date Received: April 08, 2016 10:25 deg C5.2

Biosolids


Sample Description:





Secondary Value: 12.0


Primary Value: 0.49


Qualifier:


mL





Analyst: Jennifer Price

Percent Solids: 4.1


Biosolids


Sample Description:

Page 2 of 5





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Analysis: Coliphage



Qualifier: U


g

PFU /dry gram





Percent Solids: 4.1


Biosolids


Sample Description:

Page 3 of 5





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I certify that I have personally examined and am familiar with the information submitted herein. The results presented pertain only to the samples analyzed associated identifier number(s). Based on my inquiry of the individuals immediately responsible for obtaining the information, I believe the submitted data are true, accurate, and complete. Sampling field data information was obtained from the submitted sampling documents. The analysis was authorized commissioned by the client. The data provided is strictly representative of the analysis conducted on the material/samples/articles provided by the client (or client’s representative) it’s (their) condition at the time of test. The sample(s) were analyzed in accordance with the method described for each analyte, however due to the inherent limitation(s) of method(s), microorganisms may avoid detection. Thus, BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Positive, negative, and blank controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis results presented in this report meet the requirements of The NELAC Institute (TNI), ISO 17025, The State of Florida Department of Public Health’s Laboratory Certification Program, as applicable unless otherwise noted.


Project: Tropical Farms

Signature of Laboratory Director/Authorized Rep. _________________________ Date: ___________________April 11, 2016




Page 4 of 5





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SYMBOL MEANING



I

The reported value is between the laboratory method detection limit and the laboratory

practical quantitation limit.





N

Presumptive evidence for the presence of material. There is an indication that the analyte is

present, but the confirmation requirement was not met.



U

Indicates that the compound was analyzed for but not detected. The specified component was

not detected. The reported value is the method detection limit.


Y The laboratory analysis was from an improperly preserved sample. Data may not be accurate.

Z

Too many colonies present (TNTC); the numeric value given represents the upper end of the

value that can be determined based on the volume.

?

Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.





^ BCS is not currently accredited for this analyte.


Page 5 of 5





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July 15, 2016

Casey Cochran

Nuterra Management



[email protected]; [email protected]; [email protected]; [email protected]

904-819-9170

Client ID: Tropical Farm/Raw, Tropical Farm/Treated

Dear Casey Cochran,

BCS ID: 1607091, 1607092



Sincerely,

Bonnie Mull, MPH Laboratory Operations Manager




Analysis Method


Coliphage (male specific & somatic) Total Coliphage BCS SOP V-11 (ISO17025 and TNI Accredited)

Page 1 of 6Final Report BCS ID 1607091, 1607092




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Analysis Start: July 14, 2016 12:11



Analysis: Coliphage (male specific & somatic)


Volume Analyzed: 49.93

Qualifier: None

Analysis Stop Date: July 15, 2016 10:30

g

PFU /dry gram


Client Sample ID: Tropical Farm/Raw

BCS Sample ID: 1607091

Sample Date/Time: July 12, 2016 12:00


Percent Solids: 4.5Date Received: July 14, 2016 9:50

deg C2.2

Biosolids


Sample Description:









Qualifier: U


mL



Client Sample ID: Tropical Farm/Treated



Analyst: Monique Bessette, MPH


deg C2.2

Biosolids


Sample Description:





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Qualifier: U


g

PFU /dry gram


Client Sample ID: Tropical Farm/Treated





deg C2.2

Biosolids


Sample Description:





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Report Notes:

Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes.





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I certify that I have examined I am familiar with the information submitted herein. The results pertain only to analyzed sample(s) associated identifier #(s). Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, complete. Sampling field data was obtained from submitted documents. The analysis was authorized commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client’s representative) it’s/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis results presented in this report meet the requirements of The NELAC Institute (TNI), ISO 17025, and The FL Public Health’s Laboratory Certification Program, as applicable unless otherwise noted.

Signature of Laboratory Director/Authorized Rep. _________________________ Date: ___________________July 15, 2016





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SYMBOL MEANING




quantitation limit.





N Presumptive evidence for the presence of material. There is an indication that the analyte is present,




UIndicates that the compound was analyzed for but not detected. The specified component was not




ZToo many colonies present (TNTC); the numeric value given represents the upper end of the value

that can be determined based on the volume.











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October 17, 2016

Casey Cochran

Nuterra Management



[email protected]; [email protected]; [email protected]; [email protected]

904-819-9170

Client ID: TF Raw, TF Treated

Dear Casey Cochran,

BCS ID: 1610178, 1610179



Sincerely,

Bonnie Mull, MPH Laboratory Operations Manager




Analysis Method


Coliphage (male specific & somatic) Total Coliphage BCS SOP V-11 (ISO17025 and TNI Accredited)





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Primary Value: 716

Amount Analyzed: 25.06

Qualifier: None


g

PFU /dry gram


Client Sample ID: TF Raw


Sample Date/Time: October 11, 2016 9:00


% Solids: 1.3Date Received: October 13, 2016 9:40

deg C7.6

Biosolids

Preserved: YesReceipt Temperature:

Sample Description:

Amount Submitted:125 ml









Qualifier: U


mL



Client Sample ID: TF Treated



Analyst: Melanie O'Rourke, B.S.


deg C7.6

Biosolids


Sample Description:






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Qualifier: U


g

PFU /dry gram


Client Sample ID: TF Treated





deg C7.6

Biosolids


Sample Description:






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Report Notes:

Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes.





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I certify that I have examined I am familiar with the information submitted herein. The results pertain only to analyzed sample(s) associated identifier #(s). Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, complete. Sampling field data was obtained from submitted documents. The analysis was authorized commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client’s representative) it’s/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis results presented in this report meet the requirements of The NELAC Institute (TNI), ISO 17025, and The FL Public Health’s Laboratory Certification Program, as applicable unless otherwise noted.

Signature of Laboratory Director/Authorized Rep. _________________________ Date: ___________________October 17, 2016





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SYMBOL MEANING




quantitation limit.





N Presumptive evidence for the presence of material. There is an indication that the analyte is present,




UIndicates that the compound was analyzed for but not detected. The specified component was not




ZToo many colonies present (TNTC); the numeric value given represents the upper end of the value

that can be determined based on the volume.











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Documents

MARTIN COUNTY - documents.martin.fl.us · MARTIN COUNTY BOARD OF COUNTY COMMISSIONERS UTILITIES & SOLID WASTE DEPARTMENT PO Box 9000 Stuart, FL 34995-9000 John E. Polley Director