March 25, 2010: UNC report of chemical odor in septic tank · for offsite disposal. Once these activities are completed, UNC plans to resume normal pump and haul activities. Please

The University of North Carolina at Chapel HillUNC Department of Environment Health amp Safety EJVRf)Nv1ENI I 120 Estes Drive Ext CB 1650 HFlTH amp S1fETY Cl~ Hill North Carolina7599-1650

March 25 2010

Matthew Fleahman DENR Division ofWater Quality Raleigh Regional Office 1628 Mail Service Center Raleigh NC 27699-1628

Subject Unusual Odor in Septic Tank The University of North Carolina at Chapel Hill (UNC) Bingham Facility (former Research Resource Facility)

Dear Mr Fleahman

I am writing in follow-up to your telephone conversation with Larry Daw on March 17 2010 regarding an unusual odor in the septic tank at the subject facility

On March 1 20 I 0 operators at the Bingham Facility detected an unusual odor emanating from the septic tank of the permitted wastewater treatment system EHS personnel were notified the next day (March 2 2010) and began investigating with the operators to determine the source of the odor The odor was strong in both the septic tank and the nearest wet well and the odor registered at levels up to 30 parts per million on a photoionization detector (PID) On-site methods used to determine the chemical composition of the odor were inconclusive

That same day EHS personnel and the wastewater treatment system operators investigated sewer cleanouts from both Bingham I ( older building) and Bingham 2 and they detected no odor or elevated PID readings Additionally EHS personnel and the facility operators visually inspected Bingham I and 2 and interviewed employees at the facility in an attempt to discover the source of the odor however nothing conclusive was identified

EHS personnel and facility operators also inspected Bingham 3 which is under construction as well as two manholes outside of Bingham 3 EHS personnel and facility operators determined that the manholes and visible piping were dry The construction activities at Bingham 3 have involved installation ofpropylene glycol into the cooling system installation of epoxy flooring and finishing activities

The Bingham Facility is currently operating under a DENR Division of Water Quality (DWQ) Pump and Haul Permit (Permit No WQ0034607) Under the Pump and Haul Permit wastewater from the Bingham Facility is collected within the animal wastewater treatment plant and transported to the Orange Water and Sewer Authority (OWASA) Wastewater Treatment Plant located in Chapel Hill North Carolina Upon becoming aware of the odor from the septic system EHS personnel ceased all pump and haul operations as of March 2 2010 There is adequate storage capacity on-site to collect and retain the wastewater

The University of North Carolina at Chapel HillUNC Department of Environment Health amp Safety lNv IR( )N rvllmiddot0middot1 1120 Estes Drive Ext CB 1650 l-11lTlmiddotI laquo 1f Y 9lgtJel Hill North Carolina_~]599l5c0_____

On March 2 2010 UNCs consultant McKim amp Creed (MampC) collected a water sample from the domestic wastewater system at the septic tank effulent pump station (referred to in the chain-of-custody documents as the post septic tank) EHS personnel requested expedited processing of these results (Attachment 1) which EHS received on the afternoon of March 4 2010 These results showed the presence of toluene and ethylene glycol

Following receipt of these results UNC and MampC determined that additional sampling would be conducted at the equalization basin of the animal wastewater system (referred to in the chain-of-custody documents as the Capetown system) in order to gain additional information regarding the constituents of concern (CoC) and to provide OW ASA with further data about the wastewater to be sent to OWASA This additional sampling was conducted on March 5 2010 UNC also requested expedited processing of these results (Attachment 2) and received them late on Tuesday March 9 2010 The delay in receipt of these results was due to analytical equipment problems at the laboratory

Upon review of the March 5 2010 sampling results UNC and MampC determined that further resampling was necessary because acetone was present in the samples and because UNC and MampC believed that the presence of acetone was a laboratory artifact To confirm that the acetone was a laboratory artifact UNC sent a part of the March 5 2010 sample to SGS North America Inc for analysis (Attachment 3)

On March 11 2010 MampC collected two samples from the equalization basin of the animal wastewater system and a composite sample of the septic tank Each sample was split and one part was sent to EnviroChem for analysis while the second part was sent to SGS for analysis in order to ensure the accuracy of the results UNC requested expedited processing of these results which UNC received on March 15 2010 (Attachment 4)

The main CoC identified in all of the samples included toluene ethylene glycol and propylene glycol which are components of the materials being utilized in the construction site of Building 3 Additionally these chemicals are not commonly used at the Bingham Facility Consequently UNC believes that the construction materials were the likely source of the CoCs The main construction activities have been completed and the floor drains have been covered to reduce the likelihood of a recurrence

On March 16 2010 UNC contacted Damon Forney the Operations Manager at OWASA to supply him with analytical data from the samples collected to date (including an analysis of samples (Attachment 5) taken on February 18-19 2010 which were collected to initiate UNCs evaluation of the wastewater treatment system) and to inquire whether OWASA could continue to accept the wastewater The following day OWASA stated that it could not receive the wastewater because of the concentration of toluene present in the wastewater

UNC has contracted with Clean Harbors to dispose of the wastewater and to determine how to clean out the wastewater system The current plan is to flushclean the wastewater piping from Building 3 remove contaminated water store it on-site in frac tanks and clean the septic tank

The University of North Carolina at Chapel Hill Department of Environment Health amp Safety

l1-VlltONvLNl 1120 Estes Drive Ext CB 1650 lmiddotllbullilll-1 ltmiddot lmiddotFTY

Chapel Hill North Carolina 27_~22bulllc650-----------

and basins in the wastewater system Clean Harbors initiated this process on Monday March 22 2010

Following containerization of the contaminated wastewater the material will be characterized for offsite disposal Once these activities are completed UNC plans to resume normal pump and haul activities

Please contact me if you have any questions or comments

Sincerely

~~~~ Mary Beth Koza Director - Environment Health amp Safety

Attachment 1

6602 Windmill Way Wifmington NC 28405ENVIRONMENTAL CHEMISTS INC OFFCE 910-392-0223 FAX 910-392-4t24

NCDENR DWQ CERTIFICATION 94 NCDHHS DLS CERTIFICATION 37729 Analytical amp Consulting Chemists

COLLECTION AND CHAIN OF CUSTODY

CLIENT vle-k-bull~ f Cr_J ___f- ( PROJECTNAME Uk__ -J1- REPORTNO o -tt~~

ADDRESS_______________CONTACTNAME K_~ f-tv- f E bull PONO _____________

__________________REPORTTO______________ PHONEIFAX___________

COPYTO______________~E-MAIL

Sampled By fYgt~_ pound~r bull t- SAMPLE TYPE I= Influent E Effluent W =Well ST= Stream SO = Soil SL = Sludge Other - 1 Collection

Sample Identification

Date Time Temp

i)0 LS t_ (J -t_ ~ llflt bull (--t-

CI~bull f(I- )

H ~ +1-

I te~ ~

Ii ~ amp ~ t E 0

C G

C

G C

G C

G

C

G C

G C G C

G C

G C

G

~ ~ 1 ~50 EJS ClS ~ E

- p

G p

G p

G p

G p

G p

G p

G p

G p

G p

G

0 a_w lt( _ il

PRESERVATION

~ Ia IgI8 I5 I2 zCNzocc

i r z I-

_

I-

ffi ANALYSIS REQUESTED

5

Jl-l or to -lo--~~

94=1 )01 s-)

NOTl~E - DECHLORINATION Sam~es for Ammonia ~N Cyanide Phe~I and Bacteria must be dechlorinated (02 ppm or less) In the field at the time of collectlon_ See revese for l~ns

OatefTimeTransfer I Relinquished By I DateTime I Received By

1 _2

Temperature when Received gtmiddotLPlt--- Accepted tL Rejected0 Resample Requested ________

Delivered By ~ Received By -frac14 amp-- Date 312-zlaquon Time l t su Comments z 9 t 0 -s -fr vlt--1 71

3eigt C4 TURNAROUND s ( ~ o rcent I ~A

Environmental Chemists Inc 6602 Windmill Way bull Wilmington NC 28405

(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)

710 Bowsertown Road bull Manteo NC 27954 (252) 473-5702

ANALYTICAL ampCONSULTING CHEMISTS NCDENR DWQ CERTIFICATE 94 DLS CERTIFICATE 37729

Customer

McKIM amp CREED - RALEIGH Date of Report March 3 2010 1730 Varsity Drive Suite 500 Raleigh NC 27606 Purchase Order Attn Kevin Eberle PE

Report Number 10-1978

REPORT OF ANALYSIS

Date Sampled 030210 Project UNC - Bingham

Sampled By Jay Baker ( Envirochern)

WASTEWATERmiddot Paget of4 SW 846 METHOD 8260B Domestic Waste (Post Septic)

Analyte microgL 4655 Benzene lt2 Bromobenzene lt2 Bromochloromethane lt2 Bromodichloromethane lt2 Bromoform lt2 Bromomethane lt2 n-Butylbenzene lt2 Sec-Butvlbenzene lt2 Tert-Butylbenzene lt2 Carbon Tetrachloride lt2 Chlorobenzene lt2 Chloroethane lt2 2-Chloroethyl vinyl ether lt2 Chloroform lt2 Chloromethane lt2 2-Chlorotoluene lt2 4-Chlorotoluene lt2 Dibromochloromethane lt2 12-Dibromo-3-chloronropane lt2 Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)


ANALYTICAL amp CONSULTING CHEMISTS NCDENR DWQ CERTIFICATE 94 DlS CERTIFICATE 37729

Customer McKim amp Creed Report l 0-l 97 8 Page 2 of 4

WASTEWATERmiddot SW 846 METHOD 8260B Domestic Waste (Post Septic)

Analyte microgL 4655

Dibromomethane lt2 I 2-Dibromoethane (EDB) lt2

12-Dichlorobenzene lt2

13-Dicblorobenzene lt2


11-Dichloroetbane lt2

11-Dichloroethene lt2

l 2-Dichloroethane lt2

cis-12-Dichloroethene lt2

T rans-12-Dichloroethene lt2

12-Dichloropropane lt2

l 3-Dichloropropane lt2


11-Dichloropropene lt2

cis-13-Dichloropropene lt2

trans-13-Dichloropropene lt2

lt2Dichlorodifiuoromethane

Ethylbenzene lt2

lt2Hexachlorobutadiene

lsopropylbenzene lt2

P-Isopropyltoluene lt2

Methylene Chloride lt2

123-Trichlorobenzene lt2


Trichloroethene lt2

Naphthalene lt2

n-Propylbenzene lt2

Styrene lt2

II I 2-Tetrachloroethane lt2

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)


ANALYTICAL amp CONSULTING CHEMISTS NCDENR DWQ CERTIFICATE 94 DLS CERTIFICATE 37729

Customer McKim amp Creed Report to-t 978 Page 3 of 4

WASTEWATERmiddot METHOD8260 domestic Waste (Post Septic)

4655Analyte microwJ Il 22-Tetrachloroethane lt2

Tetrachloroethene lt2

Toluene 328

l t 1-Trichloroethane lt2

11 2-Trichloroethane lt2

Trichlorofluoromethane lt2

123-Trichloropropane lt2

124-Trimethylbenzene lt2


Vinyl Chloride lt2

M+PXylene lt4

O-Xylene lt2

IPE lt2

MTBE lt2

Acetone lt 10

MEK ltlO

ltJO

2-Hexanone

MIBK

lt2

Ethanol lt2

Vinyl Acetate lt2

Date Analyzed 030310

SW 846 METHOD 8015 Domestic Wate (Post Septic) 4655Analyte mgL

Ethylene Glycol 270

Date Analyred 030310

Comments

Environmental Chemists Inc 6602 Windmill Way bull Wilmh1gton NC 28405

(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)

710 Bowsert6wn Road bull Manteo NC 27954 (252) 473-5702


Customer McKim amp Creed Report 10-1978 Page 4 of 4

Domestic Waste (Post Septic) 4655 Results ofLibrary Search Compouflds for 625

Match Result Number Compound CAS

Probability microgL

1 Propanaf 123-38-6 7882 8050

2 Acetic Aldehyde 75-07-0 7455 752

3 1-propanol 71-23-8 9391 1152

4

5

6

7

8

9

11

12

Comment

Tentatively Identified Compound (Tlq refers to substances which are not present in the list of target compounds Therefore not all TCs are identified and quantitated using individual standards TIC listings are prepared utilizing a computerized library search ofelectron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist

Quantitation is accomplished by relative peak height of the compound compared to that of the nearest internal standard from the total ion chromatograph TICs are identified and qnantitated only if the peak height is equal or greater than 10 of that of the nearest internal standard Quantitation provided is an estimate

Reviewed by

Attachment 2

Analytical amp Consulting Chemists

6602 Windmlll Way Wilmington NC 28405 ENVIRONMENTAL CHEMISTS INC OFFICE 910-392-0223 FAX 910-392-4424

NCDENR DWQ CERTIFICATION 94 NCDHHS DLS CERTIFICATION 3n29


CLIENT MJltin i- CreeJ PROJECT NAME U(L - (h1Vivuri foe 11i ry REPORT NO 0 - d I10 ADDRESS_____________CONTACTNAME__________f__ PO NO ___________

________________REPORTTO_____________PHONEIFAX__________

COPY TO~----- -middot ___E-MAILmiddot

Sampled By a(V J~etl SAMPLE TYPE I = Influent E = Effluent W = Well ST= Stream SO= Soll SL = Sludge Other

Collection


Date I Time Temp

~ bull () 1 I3-os-o IDso c1Za-ttJt1_Da~ lo)middot ~

ot 7 amp8 ~

lt n JAJr~~q~h on _0_$~

~-6Sio Ior-lt

T

0001 eqt I

tltJ vJ L bull Ba~ ~ 3-cG-ID I Joio

itE~Jl

11 ~ _ bull PRESERVATION deg c 5ltgt 5-J Qwamp~ 55 aa m w ~ a 8 r 0 E (J Sa C E 5=gt ~ 0 ti) z ~ Xg u- u z z r x c ~

C p

~ ~ 4956

C p

G G C p

G G

C p

G G 49pound1

C p

~ $-C p

G G

C p

~ G frac1295J I)( C p

G G X C p

G G II C p

G G

I ANALYSIS REQUESTED

GJ4 [pJsI

-eslh~ Jl)wl oj~hi

ampJ4 4d5-7

e~ 57ul ~ ~iJ gthi~

ib)_ 1sS 1J5 )lt

CoO To1o 111 1ura J flrltCr ltdeg-

NOTICE__DECHLORINATION SamJ)les for Ammonlt_TKN Cyanide Phenol and Bacteria must be dechlorinated (02 ppm or less) in the field at the time of collection See reverse for Instructions

Transfer I Relinquished By I DateTime I Received By OatefTime

1 2 7(ltt~+fTemperature when1Recelved ~-2 deg Accepted __- Resample Requested DellveredBy4C-- OWJY Received~ ~J(XA J2---ltgt Date3-dS-1O Time ZJ3aComments___________________________________TURNAROUND _________


(910) 392-0223 (Lab) bull (90) 392-4424 (Fax)


ANALYTICAL amp CONSULTING CHEMISTS NCDENR DWQ CERTlFICAfE 94 DLS CEfUIFICATE 37729

Customer



REPORT OF ANALYSIS

Date Sampled 030510 Project UNC-Bingham Facility

Sampled By Zach Owen ( Envirochem)

EOUALIZATION BASIN Pae 1 of6

Equalization Basin Equalization Basin EPA Method 624 (Duplicate)

4950 4951

Benzene

Analyte microgL lt40lt40 lt40lt40Bromodichloromethane

Bromoform lt40lt40 Bromometbane lt40 lt40 Carbon Tetrachloride lt40lt40

Chlorobenzene lt40 lt40 Chloroetbane lt40 lt40 2-Chloroethylvinyl ether lt40lt40 Chloroform lt40lt40 Chloromethane lt40lt40 Dibromocblorometbane lt40lt40 12-Dicblorobenzene lt40 lt40 13-Dicblorobenzene lt40 lt40 14-Dicblorobenzene lt40lt40 11-Dicbloroethane lt40lt40 12-Dichloroetbane lt40 lt40 1lcDicbloroethenc lt40 lt40 Trans-12-Dicbloroetbene lt40 lt40 12-Dichlorooropane lt40 lt40 Cis-13-Dicbloroprooene lt40 lt40 Trans-13-Dicbloroorooenc lt40lt40

Comments Quantitation limit elevated due to sample matrix interference


(910) 392-0223 (Lab bull (910) 392-4424 (Fax


ANALYTICAL amp CONSULTING CHEMISTS NCDENR DWQ CERTIFICATE 1lt4 DLS CERTIFICATE 37729

Customer McKim amp Creed Report 10-2110 Page 2 of6

EQUALIZATION BASINmiddot Equalization Basin

Equalization Basin EPA Method 624 (Duplicate)4950

4951

lt40

Analyte microgL

lt40

Methylene Chloride

Ethyl benzene lt40

1122-Tetracbloroethane

lt40

lt40 lt40

lt40lt40Tetrachloroethene 158

111-Trlchloroetbane

148Toluene lt40

112-Trichloroethane

lt40

lt40 lt40

Trlchloroethene lt40

Trichlorot1uoromethane

lt40

lt40

Vinyl Chloride

lt40

lt40 lt40

M+PXylene lt80 lt80

0-Xylene lt40 lt40

MTBE lt40 lt40

Acetone 656 532

030610Date Analyzed

Comments

Quantitation limit elevated due to sample matrix interference


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)


ANALYTICAL amp CONSULTING

CHEMISTS NCDENR DWQCERTJFICATE 94 DLS CER11FICATE 37729 -=c_middot------------middotmiddotmiddot-middotmiddot--middot-------middot--=--==-=--middot=-middot==---=middot--middot==middot=====middotmiddotmiddotmiddotmiddot=middotmiddotmiddotc


EOUALIZATION BASIN

EPA Method 625 Analyte microgL

Equalization Basin 4950

Equalization Basin (Duplicate)

4951

Acenaphthvlene lt50 lt50 Anthracene lt50 lt50 Benzo(a)anthracene lt50 lt50 Benzo(a)pyrene lt50 lt50 Benzo(b)fluoranthene lt50 lt50 Benzo(ghi)perylene lt50 lt50 Benzo(k)fluoranthene lt50 lt50 Bis(2-Chloroethoxy)methane lt50 lt50 Bis(2-Chloroethyl)ether lt50 lt50 Bis(2-Chloroisopropyl)ether lt50 lt50 Bis(2-ethylhexyl)phthalate lt50 lt50 4-bromophenyl phenyl ether lt50 lt50 Butylbenzylpbthalate lt50 lt50 2-Chloronaphthalene lt50 lt50 4-Cbloronhenyl phenyl ether lt50 lt50 Chrysene lt50 lt50 Di-n-Butylphthalate 291 515 Di-n-octylphthalate lt50 lt50 Dibenzo(ah)anthracene lt50 lt50 12-Dichlorobenzene lt50 lt50 13-Dichlorobenzene lt50 lt50 14-Dichlorobenzene lt50 lt50 33-Dichlorobenzidine lt50 lt50 Diethylphthalate lt50 lt50 Dimethylphthalate lt 50 lt 50 24-Dinitrotoluene lt50 lt50 26-Dinitrotoluene lt50 lt50 Fluoranthene lt50 lt50 Fluorene lt50 lt50 Hexacblorobenzene lt50 lt 50 Hexachlorobutadiene lt50 lt50 Hexachlorocyclopentadiene lt50 lt50

Comments

ANALYTICAL amp CONSULTING CHEMISTS


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)


NCDENR DWQ CERTIFICATE 94 DlS CERTIFICATE 37729

Customer McKim amp Creed

EQUALIZATION BASINmiddot

Report 10-2110 Page 4 of6




4951

Hexachloroethane lt50 lt50 Indeno(l23-cd)pyrene lt50 lt50

lsophorone lt50 lt50 Naphthalene lt50 lt50

Nitrobenzene lt50 lt50 N-Nitrosodi-n-propylamine lt50 lt50 Phenanthrene lt50 lt50 Pyrene

lt50 lt50 124-Trichlorobenzene lt50 lt50

Ackl Extractable middot middot middot _ middotmiddot bull middotmiddot _-c bull

4-Chloro-3-methylphenol lt50 lt50 2-Chlorophenol lt50 lt50 24-Dichlorophenol lt50 lt50 24-Dimethylphenol lt50 lt50 24-Dinitrophenol lt50 lt50 2-Methyl-46-dinitrophenol lt 50 lt 50 2-Nitrophenol lt50 lt50 4-Nitrophenol lt50 lt50 Pentachlorophenol lt50 lt50 Phenol lt50 lt50 246-Trichlorophenol lt50 lt50 4-Methylphenol 353 818

Date Extracted middot 030510 Date Analyzed 030810

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer McKim amp Creed Report 10-2110

4950 Results ofLibrary Search Compounds for 625 Match

Number Compound CAS Probability

l Cholesterol 57-88-5 889

2 Dicyclohexyl Phthalate 84-61-7 913

3 N-Hexadecanoic Acid 57-10-3 845

4 N-Nonylphenol 25154-52-3 815

5 NN-Dimcthyl-lDodccaneaminc 112-18-5 842

6 56-Dihydro-246-Triethyl-4H-13S-Dithiazine

54717-17-8 906

7 Cis-35-Diethyl-124-Trithiolane 38348-26-4 833

8 Trans-35-Diethyl-124-Trithiolane 38348-26-4 839

9 lndolc 120-72-9 944

10 P-Cresol 106-44-5 875

11

12

Comment

Tentatively Identified Compound (TIC) refers to substances which are uot preseut in the list of target compounds Therefore not all TI Cs are identified and quantitated using individual standards TIC listings are prepared utilizing a computerized library search of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist

Quantitation is accomplished by relative peak height of the compound compared to that of the nearest internal standard from the total ion chromatograph TICs are identified and quantitated only if the peak height is equal or greater than 10 of that of the nearest internal standard Quantitation provided is an estimate

Page 5 of6

Result microgL

100

174

61

94

101

99

112

127

57

354


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)


ANALYTICAL amp CONSULTING CHEMISTS NCDENR DWQ CERTIFICATE 94 DIS CERTIFICATE 37729


4951 Results ofLibrary Search Compoundsfor625

Number Compound

I Cholesterol

2 Dicyclohexyl Phthalate

3 N-Hexadecanoic Acid

4 N-Nonylphenol

5 NN-Dimethyl-lDodecaneamine

6 56-Dihydro-246-Triethyl-4H-l35-Dithiazine

7 35-Diethyl-124-Trithiolane

8 lndolzin

9 P-Cresol

11

12

Comment

CAS Match

Probability Result microgL

57-88-5 907 121

84-61-7 887 201

57-10-3 821 72

25154-52-3 845 ll3

ll2-18-5 844 91

54717-17-8 855 272

54644-28-9 846 231

274-40-8 884 67

106-44-5 899 820

Tentatively Identified Compound (TIC) refers to substances which are not present in the list of target compounds Therefore not all TICs are identified and qnantitated using individual standards TIC listings are prepared utilizing a computerized library search of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist

Quantitation is accomplished by relative peak height of the compound compared to that of the nearest internal standard from the total ion chromatograph TICs are identified and quantitated only if the peak height is equal or greater than 10 of that of the nearest internal standard Qnantitation provided is an estimate

~~~

Reviewed by-~==bull_---itt-~==__------

Field Sample Collection and Analysis

Client 1ck(V 1-- reed Report ) - )1tgt

Collected Analyzed By 2th 0NIZA Date 3 middotOS-10

Sample Type Influent (I) Effluent (E) Well (W) Stream (s) Other _______

1 2 3 4 Sample Type Sample Location t 11-0 1 ~ Time Collected Time Analyzed lO~oo oH units 7(1 oH units (duolicate) 7(3 Duplicate pH readings must be withinplusmn 01 units pH and Chlorine must be analyzed within 15 min of collection DO analyzed immediately

DO meL Chlorine (residual) ueL Temperature degC

DO Calibration Time Calibrated

H Calibration

CgtJbull Make Model

Air Calibration Adjusted Comment Calibration

Time Calibrated

0 D

pH 4 Buffer Calibration

pH 10 Buffer pH 7 Buffer Calibration Check

)

Comment

Return Trip Check

1)efilW Model J1ta1

Chlorine Calibration Makemiddot Modelmiddot Time Calibrated

Standard I ( ) mgL

Standard 2 ( ) mgL

Standard 3 ( ) mgL

Mid- Range Standard True Value Reading mgL rngL

Recovery

Annual Standard Curve for Ran on by DI Water Blank

-

Thermometer Make UOf ~ ~YJJQ _ Serial No ___3-s_-t~----

Attachment 3

SGS North America Inc

SGS Mr Ray Porter EnviroChem 6602 Windmill Way Wilmington NC 28405

Report Number G 171-349

Client Project E6414

Dear Mr Porter

Enclosed are the results of the analytical services performed under the referenced project The samples are certified to meet the requirements of the National Environmental Laboratory Accreditation Conference Standards Copies of this report and supporting data will be retained in our files for a period of five years in the event they are required for future reference Any samples submitted to our laboratory will will be retained for a maximum of thirty (30) days from the date of this report unless other arrangements are requested

Ifthere are any questions about the report or the services performed during this project please call SGS at (910) 350-1903 We will be happy to answer any questions or concerns which you may have

Thank you for using SGS Environmental Services for your analytical services We look forward to working with you again on any additional analytical needs which you may have

Sincerely SGS Environmental Services Inc

Environmental Division 5500 Business Dr Wilmington NC 28405 t 910) 350-1903 f (910) 350-l557 wwwussgscom

Member ol lhamp SGS Group Page1of8


Case Narrative Revision EnviroChem

SGS Project G 171-349 Project Name E6414


March 121 2010

bull Two waste water samples were accepted into the laboratory on March I 011 20 IO at 1415

for analyses as indicated on the chain of custody The samples were received in good condition with a temperature of20C

bull All extractions and analyses were completed within holding time limits with the following quality control exceptions

624 Analyses

bull Acetone was requested to be reported per client communication Acetone is not part of the 624 continuing calibration report but is evaluated under the 8260 QC check

bull Although both sample chromatograms display a peak eluting at the calibrated retention time for Acetone it is the opinion of the laboratory that this detection cannot accurately be reported as Acetone Due to a co-eluting non-target compound containing an abundance of ion 58 which is the secondary ion for Acetone this factor creates ion ratios that are inconsistent with the mass-spectral pattern of this compound

Page 2 of 8


List of Reporting Abbreviations And Data Qualifiers

B =Compound also detected in batch blank

BQL = Below Quantification Limit (RL or MDL)

DF =Dilution Factor

Dup =Duplicate

D =Detected but RPD is gt 40 between results in dual column method

E = Estimated concemiddotntration exceeds calibration range

J = Estimated concentration below calibration range and above MDL

LCS(D) = Laboratory Control Spike (Duplicate)

MDL= Method Detection Limit

MS(D) = Matrix Spike (Duplicate)

PQL = Practical Quantitation Limit

RLCL =Reporting Limit Control Limit

RPD = Relative Percent Difference

UJ =Target analytes with recoveries that are I0 lt R lt LCL of MEs are allowable and compounds are not detected in the sample

mgkg = milligram per kilogram ppm parts per million

ugkg = micrograms per kilogram ppb parts per billion

mgL = milligram per liter ppm parts per million

ugL = micrograms per liter ppb parts per billion

Rec = Percent Recovery

soilds = Percent Solids

Special Notes I) Metals and mercury samples are digested with a hot block see the standard

operating procedure document for details 2) Uncertainty for all reported data is less than or equal to 30 percent

M13402 I 8084

Page 3 of 8

Client Sample ID 4950 Client Project ID E6414

Lab Sample ID G171-349-1A Lab Project ID G171-349

Compound Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane Dibromochloromethane 12-Dichlorobenzene 13-Dlchlorobenzene 14-Dichlorobenzene 11-Dlchloroethane 11-Dichloroethene 12-Dichloroethane trans-12-dichloroethene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Acetone Ethylbenzene Methylene chloride Methyl-tert-butyl ether (MTBE) 1122-Tetrachloroethane Tetrachloroethene Toluene Trichloroethane 111-Trichloroethane 112-Trichloroethane Trichlorofluoromethane Vinyl chloride m-p-Xylene o-Xylene

12-Dichloroethane-d4 Toluene-de 4-Bromofluorobenzene

Comments

Flags BQL = Below owintitalion Limits

Analyst l


Results for Volatiles

Result UGL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL

113 BQL BQL BQL BQL BQL BQL BQL

byGCMS624

Quantitation Limit UGL

400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400

Spike Spike Added Result

10 102 10 994 10 999

Paga 1 of2

Analyzed By CLP Date Collected 352010 950 Date Received 310201 O

Matrix Water Sample Amount 5 ml

Dilution Date Factor Analyzed

4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100

Reviewed By cmiddot~

GCMSxlamp

Page 4 of 8


Results of Library Search for Volatile Compounds byGCMS

Client Sample ID 4950 Analyzed By CLP Client Project ID E6414 Date Collected 03-05-2010

Lab Sample ID g171-349-1a Date Received 03-10-2010 Lab Project ID G171-349 Matrix Water

Sample Vol 5 ml Dilution 1 Date Analyzed 03-11-2010

No Comoound Retention

Time CAS Match

Probabllltv Result uaL

0 0 0 4 5 6 7 8 9 10

Dimethyl sulfide Acetaldehyde Propane 1-(methylthio)-Disulfide dimethyl

298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment

Tentatively Identified Compound (TIC) refers to substances which are not present in the list of target compounds Therefore not all TICs are identified and quanlilated using individual standards TIC listings are prepared utilizing a computerized library search of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist

Quantitation is accomplished by relative peak area of the compound compared to that of the nearest Internal standard from the totalIon chromatogram TICs are Identified and quantitated only if the peak area is equal to or greater than 10 of that of the nearest internal standard Quantitatlon provided is an estimate

Reviewed by middot fltmiddot

Page 1 Of 1 VOA_TICS_UMSxls

Page 5 of 8



Compound Benzene Bromodlchloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene 11-Dichloroethane 11-Dlchloroethene 12-Dichloroethane trans-12-dlchloroethene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Acetone Ethylbenzene Methylene chloride Methyl-tert-butyl ether MTBE) 1122-Tetrachloroethane Tetrachloroethene Toluene Trichloroethane 1 1 1-Trichloroethane 112-Trichloroethane Trichlorofluoromethane Vinyl chloride m-p-Xylene o-Xylene

12-Dichloroethane-d4 Toluene-dB 4-Bromofluorobenzene

Comments

Flags BQL = Below titation Limits


Results for Volatiles byGCMS624

Result Quantltatlon UGL Limit UGL BQL 400 BQL 400 BQL 400 BQL 400 BQL 400 BQL 400 BQL 400 BQL 500 BQL 400 BQL 400 BQL 400 BQL 400 BQL 400 BQL 400 BQL 400 BQL 400 BQL 400 BQL 400 BQL 400 BQL 400 BQL 400 BQL 100 BQL 400 BQL 200 BQL 400 BQL 400 BQL 400

108 400 BQL 400 BQL 400 BQL 400 BQL 400 BQL 400 BQL 800 BQL 400


10 101 10 99 10 102

Page 1 of 2

Analyzed By CLP Date Collected 352010 955 Date Received 3102010



4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624




Lab Sample ID g171-349-2a Lab Project ID G171-349

Sample Vol 5 ml Dilution 1

Analyzed By CLP Date Collected 03-05-2010 Date Received 03-10-2010

Matrix Water

Date Analyzed 03-11-2010

Retention Match Result No Compound Time CAS Probabllltv ugL 0 Dimethyl sulfide 297 000075-18-3 91 142 0 Acetaldehyde 181 000075-07-0 90 0 0 Propane 1-(methylthio)- 591 003877-15-4 97 0 4 5 6

7

8 9

10

Comment

Tentatively Identified Compound (TIC) refers to substances which are not present in the list of target compounds Therefore not all TICs are identified and quantitated using individual standards TIC listings are prepared utilizing a computerized library search of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist

Quantitation is accomplished by relative peak area of the compound compared to that of the nearest internal standard from the total ion chromatogram TICs are identified and quantitated only if the peak area is equal to or greater than 10 of that of the nearest internal standard Quantitation provided is an estimate

Reviewed by 1j

Page 1 of1 VOA_TICS_UMSxs

Page 7 of 8

-----------

G1ft~3Cfr- -ENVIRONMENTAL CHEMISTS INC

6602 Windmill Way Wilmington NC 28405 Phone (910) 392-0223 Fax (910) 392-4424

REQUEST EOR SUBCONTRACTED SEEYICES

Subcontracted To Sc 5 Contact___L______ Purchase Order ( - -

Phone __________ Fax ____________

Lab ID I Sampled I Date Time

Sample Description Analysis Requested Preservation

I L~SD $ lsiiv ltj S-0

1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc

7 - h ISpecial Instructions iVJ _ L__ ~ )_--- bull bgtAmf4-S ~

en G) en z 0s sect (D

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Send Reports To ______________ echemwiiagt1com or Fax 910-392-4424

Please Mail Original to Environmental Chemists Inc

g J Prepared by ___________For Shipment By __________ Tracking No ________

g_ Relinquished by ~-_ fh Date 3 rclt q Time I-iilt ~ p Q 7L

Received by 1tti~ Date ]jJ6 0 I Time ( lf5 z oc

Attachment 4

__________________

6602 Windmill Way Wilmington NC 28405ENVIRONMENTAL CHEMISTS INC OF=ICE 910-392-0223 FAX 910-3924424

NCDENR DWQ CERTIFICATION 94 NCDHHS DLS CERTIFICATION 37729 Anatytical amp Consulting Chemists


CLIENT cC-- f c-_-JZ~~1 ADDRESS_______________

Sampled By -~ (-_r- ZL o1 bull r- __ z_


) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

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pl- Ct

Collection

Date Time Temo fltos 0

C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c

PROJECTNAME u-c- -_(___

CONTACTNAME ficmiddotv r6crk -pound REPORTTO______________

COPY TO ____ -~__ _ _ _ _

REPORTNO o middot ZJ Pj

PONO _____________

PHONEFAX___________

E-MAILmiddot

SAMPLE TYPE 1- lnfluen~ E = Effluent W = Well ST= Stream SO= Soil SL - Sludge Other

bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

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PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

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0

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C p

G G

C p

G G (C)

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( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~

nsvss ~ lr-1~-I Lz ltfx -amp acc_1c) ftbull Pltlt ( bull 9~ gt eftltJlt z f)~Jvk~_ ~~ =

(fl~-(lt_ - ~ -J(~ ) -

NOTICE - OECHLORINA TlON Samp~ for Ammonia TKN Cyanide Phenol and Bacteria must be dechlorinated (02 ppm or less) in the- field at the time of collection s~ reverse for instructions

Transfer Relinquished By DateTime Received By

1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0

Resample Rred Date gt ~

r

Daternme

Time z ltrgt gt T

4

~

4

Environmental Chemists Inc 6602 Windmill Wfly bull Wilmington NC 28405

(910) 392-0223 (Lab) bull (910) 392-4424 (hix)

710 l3owsPrlmvn Ro)d bull Mlt1nleo NC 27954 (252) 473-5702

ANALYTICAL amp CONSULTING CHEMISTS NCDENR DWQ CERTIFCAH 94 DLS CERTJFlCAfE 1137729

Customer

McKIM amp CREED - RALEIGH Date of Original Report March 15 2010 1730 Varsity Drive Suite 500 Raleigh NC 27606 Purchase Order Attn Kevin Eberle PE

Report Number I 0-2303

REPORT OF ANALYSIS


Sampled By Jay Baker ( Envirochem)

WASTEWATER page l 0 f4 EPA 624

Analytc microgL Capetown

5446 Septic 5447

--middot--Benzene lt20 lt20 Bromodichloromethane lt20 lt 20 Bromoform lt20 lt20 Bromomethane lt20 lt20 Carbon Tetrachloride lt20 lt20 Chlorobenzcne lt20 lt20 Chloroethane lt20 lt20 2-Chloroethylvinyl ether lt20 lt20 Chloroform lt20 lt20 Chloromethane lt20 lt20 Dibromochloromethane lt20 lt20 12-Dichlorobenzene lt20 lt 20

--middotmiddot-middotmiddot-middot _____ _

13-Dichlorobenwne lt 20 lt20 middot-middotmiddotmiddotmiddotmiddotmiddotmiddotmiddot

14-Dichlorobenwne lt20 lt20 11-Dichloroethane lt20 lt20 l2-Dichloroetha11e lt20 lt20 I 1-Dichloroethene lt20 lt20 Trans-l 2-Dichloroethene lt20 lt20



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)


ANALYTICAL amp CONSULTING CHEMISTS NCDEN[lc OWQ CERTFfCArE 94 DLS CERTlrfCATE 37729

-==============middotcmiddotmiddotmiddotmiddotmiddot=middotmiddotmiddotmiddot=middotmiddotmiddotmiddot-=middotmiddotmiddotmiddot-==

Customer McKim amp Creed Report I0-2303 Page 2 of 4

WASTEWATERmiddot EPA 624

Capetown SepticAnalyte microgL 5446 5447

-middot -12-Dichloropropane lt20 lt20 Cis-13-Dichloropropene lt20 lt20 Trans-13-Dichloropropene lt20 lt20 Ethyl benzene lt2036 Methylene Chloride lt20 lt20 l 122-Tetrachloroethane lt20 lt20 Tetrachloroethene lt20 lt20 Toluene 136 529 11 I-Trichloroethane lt20 lt20 112-Trichloroethane lt20 lt20 Trichloroethene lt20 lt20 Trichlorofluoromethane lt20 lt20

Vinyl Chloride lt20 lt20 M_+P Xylene lt4094 O-Xylene lt2016

MTBE lt20 lt20 Acetone lt1037

Date Analyzed 031210 031210

SW 846 METHOD 8015 Capetown Septic Date

-_ 1nallte lllIL middotmiddot--middotmiddotmiddot-middotmiddotmiddot-middot- 5446 5447 Analywd

Ethylene Glycol 164 194 0312JO

Propylene Glycol lt25 252 0312JO

-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer McKim amp Creed Report 10-2303 Page3 of 4

Domestic Waste (Post Septic) 5446 Results ofLibrary Search Compounds for 624

Match ResultNumber Compound CAS Probability 04 microgL

Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105

5 1-(methylthio )propane 3877-15-4 9411 320

6

7

8

9

10

JI

12

Comment bull Compound is reported as unknown if match probability is less than 70


Quantitation is accomplished by relative peak height of the compound compared to that of the nearest internal standard from the total ion chromatograph TlCs are identified and quantitated only if the peak height is equal or greater than IOfrac14 of that of the nearest internal standard Quantitation provided is an estimate

Environmental Chemists Inc 6602 Windmill Wlt1y bull Wilmington NC 28405

(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)


ANALYTICAL amp CONSULTING CHEMISTS NCDENR DWQ CERTIFICATE lll4 DIS CERTIFICAfE ff7729


Domestic Waste (Post Septic) 5447 Results ofLibrary Search Compountlsfor 624

Match ResuliNumber Compound CAS Probability microgL

Unknown 320

2 1-Propanol 71-23-8 9377 232

3 1-(methylthio)propane 3877-15-4 9348 160

4

5

6

7

8

9

10

11

12



Quantitation is accomplished by relative peak height of the compound compared to that of the nearest internal standard from the total ion chromatograph TICs are identified and quantitated only if the peak height is equal or greater than IO of that of the nearest internal standard Qnantitation provided is an estimate

___ _ _ _ _ _


6602 Windmill Way WIimington NC 28405ENVIRONMENTAL CHEMISTS INC OF1CE 910-392-0223 FAX 910-392-4424

NCDENR DWQ CERTIFICATION 94 NCDHHS DLS CERTIFICATION 3TT29


CLIENT lcC-_ ~ ea_tf-Zlaquo~lct PROJECTNAME laquo-lt - 4-__ REPORTNO o - L-J PJ ADDRESS_______________CONTACTNAME lZ ~6ltrk pound PONO _____________

__________________REPORTTO______________PHONEFAX___________

COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~


) c flt- -I-_ fJJ I ff 91 L

z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

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Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-

SAMPLE TYPE I= Influent E = Effluent W = Well ST= Stream SO= Soil SL= Sludge 0th-i8 g e 0 e 0 u

(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

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sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

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~

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z ~ ~ ~

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0 ~

ANALYSlS REQUESTED

ampo~lt-l) -laquo- 1 ~~ r gt 755 JS$ ~ 1r1~-4 LZ ltex -4pound aeee) fw 9v t bull fgtOf S-e-U_cJ~ z j)OJvk~ cl~

N

(JI--(_ - J - )

NOTICE bull DECHLORINATION Samples for Ammonia TKN Cyanide Phenol and Bacteria must be dechlorinated (02 ppm or less) Jn the field at the time of collection See rnve-rse for insbuciions

Transfer Relinquished By DateTime Received By Daterrime

1

2 when Received

~ ~ -r

p ~

tJ L Accepted --Received By

]-fgt - rtlt-- --rbullvc f C

Rejected

~-0 ~ v [_ ~O

Resample Rzzted Date gt bull a

~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)

710 Bowertown Road bull Manteo NC 27954 (252) 473-5702


Customer

McKIM amp CREED- RALEIGH Date of Original Report March 15 2010 1730 Varsity Drive Suite 500 Raleigh NC 27606 Purchase Order Attn Kevin Eberle PE


REPORT OF ANALYSIS



WASTEWATER pale l 0 f4 EPA 624

Analyte microgL Capetown

5446 Septic 5447

Benzene lt20 lt20 Bromodichloromethane lt20 lt20 Bromoform lt20 lt20 Bro mom ethane lt20 lt20 Carbon Tetrachloride lt20 lt20 Chlorobenzene lt20 lt20 Chloroethane lt20 lt20 2-Chloroethylvinyl ether lt20 lt20 Chloroform lt 20 lt20 Chloromethane lt20 lt20 Dibromochloromethane lt20 lt20 l2-Dichlorobenzene lt20 lt20 I 3-Dichlorobenzene lt20 lt20 14-Dichlorobenzene lt20 lt20 l1-Dichloroethane lt20 lt20 12-Dichloroethane lt20 lt20 11-Dichloroetbene lt20 lt20 Trans-12-Dichloroethene lt20 lt20



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)


ANALYTICAL amp CONSULTING CHEMISTS NC DEN R DWQ CERTlflCATE 94 DLS CERT FlCATE 37729

middot==================middotmiddotmiddotmiddotmiddot-middotmiddotmiddotmiddot-bullmiddotmiddotmiddot


WASTEWATER EPA 624

Capetown 5446

Septic 5447 Analyte microgL

12-Dichloropropane lt20 lt20

Cis-13-Dichloropropene lt20 lt20

Trans-13-Dichloropropene lt20 lt20

Ethyl benzene 36 lt20 Methylene Chloride lt20 lt20

1122-Tetrachloroethane lt20 lt20

Tetrachloroethene lt20 lt20

Toluene 136 529

111-Trichloroethane lt20 lt20


Trichloroethene lt20 lt20

Tricblorofluoromethane lt20 lt20

Vinyl Chloride lt20 lt20

M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO


SW 846 METHOD 8015 Capetown 5446

Septic 5447

Date AnalyzedAnalvte meL

Ethylene Glycol 164 194 031210

Propylene Glycol lt 25 252 031210



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer McKim amp Creed Report 10-2303 Page3 of4


Match Result Number Compound CAS Probability microgL

Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105

5 1-(methylthio)propane 3877-15-4 94l I 320

6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





Number Compound CAS Match


1

2

3

4

Unknown

1-Propanol

1-(methylthio)propane

71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12

Comment Compound is reported as unknown if match probability is less than 70

Tentatively Identified Compound (TIC) refers to substances which are not present in the list of target compounds Therefore not all TlCs are identified and quantitated using individual standards TIC listings are prepared utilizing a computerized library search of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist


Reviewed by pound~ ~ __~-=-J--91)lv-f_______=-~~- LEJ



Report Number GI 71-350

Client Project Split Samples

Dear Mr Porter


If there are any questions about the report or the services performed during this project please call SGS at (910) 350-1903 We will be happy to answer any questions or concerns which you may have



9

middotroJt Lori Loe

Environmental Division 5500 Business Or Wilmington NC 28405 t (910) 350middot 1903 f 910) 350-1557 wwwussgscom

Member of the SGS Group Page 1 of 12



SGS Project Gl71-350 Project Name I0-2303


March IS 2010

bull Two waste water samples were accepted into the laboratory on March 11 h 20 IO at 1706 for analyses as indicated on the chain of custody The samples were received in good condition with a temperature of 20C


624 Analyses

bull Acetone was requested to be repotted per client communication Acetone is not part of the 624 continuing calibration report but is evaluated under the 8260 QC check

bull Although sample chromatograms for sample Cape Town display a peak eluting at the calibrated retention time for Acetone it is the opinion of the laboratory that this detection cannot accurately be reported as Acetone Due to a co-eluting non-target compound containing an abundance of ion 58 which is the secondary ion for Acetone this factor creates ion ratios that are inconsistent with the mass-spectral pattern of this compound

Page 2 of 12



B = Compound also detected in batch blank


DF = Dilution Factor

Dup = Duplicate

D = Detected but RPD isgt 40 between results in dual column method

E = Estimated concentration exceeds calibration range



MDL = Method Detection Limit



RLCL = Reporting Limit I Control Limit


UJ = Target analytes with recoveries that are I 0 lt R lt LCL of MEs are allowable and compounds are not detected in the sample

mgkg= milligram per kilogram ppm parts per million





soi Ids= Percent Solids



Ml3402 I 8084

Page 3 of 12


Client Sample ID Capetown

Client Project ID Split Samples

Lab Sample ID G171-350-1B

Lab Project ID G171-350

Analyte

Ethylene Glycol Propylene Glycol

Comments All values corrected for dilution BQL = Below quantitation limit

Results for Glycols by GC 8015 Modified

Analyzed By BWS

Date Collected 3112010 940

Date Received 31112010

Matrix Water

Result RL Dilution Date mgL mgL Factor Analyzed

BQL 200 3122010 BQL 200 31122010

Reviewed By lltJ Page4 of 12



Client Sample ID Septic Analyzed By BWS

Client Project ID Split Samples Date Collected 3112010 1040

Lab Sample ID G171-350-2B Date Received 3112010

Lab Project ID G171-350 Matrix Water

Analyte Result RL Dilution Date mgll mgll Factor Analyzed

Ethylene Glycol 124 100 5 3122010 Propylene Glycol BQL 100 5 3122010


Reviewed By JJ2_ Page 5 of 12

Client Sample ID Capetown Client Project ID Split Samples

Lab Sample ID G171-350-1A Lab Project ID 8171-350

Compound Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 1 4-Dichlorobenzene 11-Dichloroethane 11-Dichloroethene 12-Dichloroethane trans-12-dichloroethene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Acetone Ethyl benzene Methylene chloride Methyl-tert-buty ether (MTBE) 1122-Tetrachloroethane Tetrachloroethene Toluene Trichloroethane 1 1 1-Trlchloroethane 112-Trichloroethane Trichlorofluoromethane Vinyl chloride m-p-Xylene o-Xylene


Comments

Flags


Results for Volatiles byGCMS 624


140 400 BQL 400 BQL 400 BQL 400 BQL 400 BQL 400

111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2

Analyzed By DVO Date Collected 311201 O940 Date Received 3112010



4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624


Lab Sample ID G171bull350-1A Lab Project ID G171-350

Compound BQL = Below Quantitation Limits

I middot 0Ana yst ___e_____



Result Quantitation UGL Limit UGL

Analyzed By DVO Date Collected 3112010 940 Date Received 31112010



Reviewed By _a_middot___

Page 2 of 2 GCMS

Page 7 of 12 624



Client Sample ID Capetown Analyzed By DVO Client Project ID Split Samples Date Collected 03-11-2010

Lab Sample ID G171-350-1A Date Received 03-11-2010 Lab Project ID G171-350 Matrix Water


No Compound Retention

Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide

Propane 1-(methylthio)-

1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~

Page 1 Of 1 VOA_TCS_LIMSxls

Page 8 of 12

Client Sample ID Septic Client Project ID Split Samples


Compound Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene 11-Dichloroethane 11-Dichloroethene 12-Dichloroethane trans-12-dichloroethene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Acetone Ethylbenzene Methylene chloride Methyl-tert-butyl ether (MTBE) 1122-Tetrachloroethane Tetrachloroethene Toluene Trichloroethene 1 1 1-Trlchloroethane 1 12-Trichloroethane Trichlorofluoromethane Vinyl chloride m-p-Xylene o-Xylene


Comments

Flags






10 842 10 998 10 972

Page 1 of 2



DIiution Date Factor Analyzed

25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624




Analyst _ ___D-v--J---



Result Quantltation UGL Limit UGL

Analyzed By DVO Date Collected 3112010 1040 Date Received 311 201 O



Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624



Client Sample ID Septic Analyzed By DVO Client Project ID Split Samples Date Collected 03-11-2010




Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment


Quantitation is accomplished by relative peak area of the compound compared to that of the nearest internal standard from the total ion chromatogram TICs are identified and quantitated only if the peak area is equal to or greater than 10 of that of the nearest internal standard Quantltation provided is an estimate

Reviewed by _tli-__

Page 1 Of 1 VOA_TlCS_UMSxls

Page11of12

(__ 17- JY-0 ENVIRONMENT AL CHEMISTS INC 6602Wlndmi11Way Wilmington NC 28405 41(iJi OFFlCE 910-392-0223 FAX 910-392-4424

NCDENR DWQ CERTIFlCA TION 94 NCDHHS DLS CERTIFICATION 3n29Anafytlcal amp Consulting Chemists


CLIENT poundreck- --t 5G-5 PROJECTNAME ff f- 5_lfe_s j REPORTNO 0-27ltgt3 ADDRESS_____________CONTACT NAME 7J PO NO ___________

________________REPORT TO hy J-1-_- PHONEFAX__________

COPYTO_____________~E-MAIL

Sa_mp_ed_Bymiddot s--ampZv SAMPLE TYPE I= Influent E = Effluent W = Well ST= Stream SO= Soil SL= Sludge Other

J

JiI

O 1 Q

Delivered By c -- Received By ~ Date 5I I OI Time 7 Cb CommentsJ TURNAROUND --------

Collection - bull Q 0 PRESERVATIONbull -bull E E _Q 8 8 ~ ~

_w Sample Identification ll - - 1l ml w ii ~ X ANALYSIS REQUESTED ~ ~ 0 - C 0 ie _

~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~

Date Time Temo ltJ - z X X z 0

) J oV C p t Z-lf Yyct~ ft1 -AE acc+-11 Cjlt+o I ~ G G ~-N-l- X l( micro~k-- 1r_c-bull __

C p vc f lfl - lot)

~ G G -Jo 0 f-gt C p

2-) lt _c_

lo~O G G

iv i-Xyk(- -rS~ ee~T~~ s ~-fltfJ- f- k I bull Z p-o -4_ of-_

C p u _ SoJJltf( -_)01) lG G C p

s_ -7-I- 5f- J G G C p 9--ffc rgt- 5~J) G G

C p Cc -f7 wl

G G C p I

G G C p _ooc G G

C p no Cv-$frJr lteq G G

NOTICE bull OECHLORfNATION Samples for Ammonia TKN Cyanide Phenol and Bacterta must be dechlorinated (02 ppm or less) in the- field at the time ofcollection See teverBe for lmrtructlons

Transfer Relinauished By DateTime Received Bv DateTime

1

2 Temperature w~e~ ~ Accepted _ Rej~ed Resample Requested _

Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer

McKIM amp CREED - RALEIGH Date of Report March 12 20 I0 1730 Varsity Drive Suite 500 Raleigh NC 27606 Purchase Order Attu Kevin Eberle PE

Report Number l0-1636

REPORT OF ANALYSIS

Date Sampled 021910 Project UNC-Bingham Faclility

Sampled By Eric McHomey ( Envirochem)

SURFACE WATER pael of 3

Influent Effluent Method Date Parameters 3893 3894 Code Analyzed

Biochemical Oxygen Demand BOD as 0 2 mIL

533 5 SM5210B 021910

Carbonaceous Biochemical Oxygen Demand CBOD5 as 0 2 miL

444 3 SM5210B 021910

Chemical Oxygen Demand COD as 0 2 mgL 1080 80 SM5220D 022310

Total Organic Carbon TOC mgL 304 246 SM5310B 022410

Settleable Solids SS mlL lt01 lt01 SM 2540F 021910

Total Suspended Solids TSS mgL 342 5 SM2540D 022310

Turbidity NTU 815 61 SM21308 021910

Total Kjeldahl Nitrogen TKN mgL 196 Pending EPA 3512 030810

Ammonia Nitrogen NH3-N mgL 967 Pending EPA350t 022610

Nitrate + Nitrite Nitrogen NO3+ NO-N mgL 036 970 EPA3532 030110

Total Phosphorus as P mgL 415 282 SM4500P-F 030810

Alkalinity as CaCO3 mgL 895 62 SM 2320B 022510

Color units 200 100 SM2120B 030110

Total Phenol mgL 0313 lt0004 SM 420l 022410 -

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter

Temperature degC Eric McHoruey Certificate 94 -

pH units

-

lntluent Effiuent Method Date 3893 3894 Code Analyzed

lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510

middotmiddot---Influent Effiuent Method Date 3893 3894 Code Analyzed

68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments

Environmental Chemists Inc 6602 WindmiII Way bull Wilmington NC 28405

(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)

710 Bowsertown Road bull Mante0 NC 27954

(252) 473-5702 ANALYTICAL amp CONSULTING

CHEMISTS NCDENR DWQ CERTIFICATE 94 DLS CERTIFICATE 37729



Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobeozene Chloroethane 2-Chloroethylvinyl ether Chloroform Cbloromethane Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene 11-Dichloroethane 12-Dichloroetbane 1 1-Dichloroetbene Trans-12-Dichloroethene 12-Dichloropropane Cis-13-Dichloropropene Trans-13-Dlchloronropene Ethyl benzene Methylene Chloride 1122-Tetrachloroethane Tetrachloroethene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethene Trichlorofluoromethane Vinyl Chloride M+PXylene O-Xvlene MTBE Acetone Date Analysis Started Date Analysis Completed

Influent Effluent 3893 3894

lt20 lt05 lt20 lt05 lt20 lt05 lt20 lt05 lt20 lt05 lt20 lt05 lt20 lt 05 lt20 lt05 lt20 lt05 lt20 lt05 lt20 lt05 lt20 lt05 lt20 lt05 lt20 lt05 lt20 lt05 lt20 lt05 lt20 lt05 lt20 lt05 lt20 lt 05 lt20 lt05 lt20 lt05 lt20 lt05 lt 20 lt05 lt20 lt05 lt 20 lt05

186 lt05 lt 20 lt05 lt20 lt05 lt20 lt05 lt20 lt05 lt20 lt05 lt40 lt 10 lt20 lt05 lt20 lt05

199 030310 030910middot--middot--

258

Comments Reviewed by


6602 WJndmll Way Wilmington NC 28405ENVIRONMENTAL CHEMISTS INC OFltCE 910-392-0223 FAX 910-392-4424

NCDENR DWQ CERTIFICATION II 94 NCDHHS DLS CERTIFICATION 37729

COLLECTION AtID CHAIN OF CUSTODY

CLIENT 1dlti ~ Cormicrod- kt(ei~k PROJECTNAME liVC--jL REPORT NO I) - I(J ( ADDRESS____________CONTACTNAME et-~ the_ P PO NO ___________

_______________REPORT TO 4 _ltgt- f 1cf k $b-e-e PHONEFAX_________

COPY TO E-MAIL

middot SAMPLE TYPE I =Influent E =Effluent W =Well ST =Stream SO =Soil SL= Slu~_e Other Sample_ci_Bymiddot

-A~---~~ IL J I

Collection j ~ bull eei PRESERVATION

~ 6bullaamp 5 Sample Identification 1~ ls l i~ it

w g ~

ANALYSIS REQUESTEDi 5~ ii 0 0 8~ z q sDrte Time Temp ltgt z z bull bull

ft)Clfto middot~G11 C p -~8-1s $ e D c wJ CB41)

1 ~ t

I

I h~l---lt- -t I amp amp L G G SS 7S- 1lt N Nt-1r C p ~ a~

1 -rtP 1 I ti

pf-f zf_ fc G G (c ~~-middot ( tb_1t - nlt-1pound C p

lr vmiddotampcL~~) ~~ it--c-i-- I

G G ()-

rfiCgtj 11- -la C p 1 -1r- bull

-i [v iti ff( 1_L-_t

__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p

G G NOTICE bull OECHLORINATION Samples for Ammonffl TKN Cyanide Phenol and Bacteria must be- dechlorinated (02 ppm or tess) In thamp fretd at the time ofcolfectfon See tElvene for in5tructlons

Transfer Relinauished By DateTime Received By Dat~Time

1 2

- - -

Dellvered By tf- JA-ti+~ -- ~ Received~ltmiddotJj4)l--u2 C-c -e--= Date iJ4frac12 Time~~ f-_ Comments__________T ________________________TURNAROUND _________

The University of North Carolina at Chapel HillUNC Department of Environment Health amp Safety lNv IR( )N rvllmiddot0middot1 1120 Estes Drive Ext CB 1650 l-11lTlmiddotI laquo 1f Y 9lgtJel Hill North Carolina_~]599l5c0_____

On March 2 2010 UNCs consultant McKim amp Creed (MampC) collected a water sample from the domestic wastewater system at the septic tank effulent pump station (referred to in the chain-of-custody documents as the post septic tank) EHS personnel requested expedited processing of these results (Attachment 1) which EHS received on the afternoon of March 4 2010 These results showed the presence of toluene and ethylene glycol

Following receipt of these results UNC and MampC determined that additional sampling would be conducted at the equalization basin of the animal wastewater system (referred to in the chain-of-custody documents as the Capetown system) in order to gain additional information regarding the constituents of concern (CoC) and to provide OW ASA with further data about the wastewater to be sent to OWASA This additional sampling was conducted on March 5 2010 UNC also requested expedited processing of these results (Attachment 2) and received them late on Tuesday March 9 2010 The delay in receipt of these results was due to analytical equipment problems at the laboratory

Upon review of the March 5 2010 sampling results UNC and MampC determined that further resampling was necessary because acetone was present in the samples and because UNC and MampC believed that the presence of acetone was a laboratory artifact To confirm that the acetone was a laboratory artifact UNC sent a part of the March 5 2010 sample to SGS North America Inc for analysis (Attachment 3)

On March 11 2010 MampC collected two samples from the equalization basin of the animal wastewater system and a composite sample of the septic tank Each sample was split and one part was sent to EnviroChem for analysis while the second part was sent to SGS for analysis in order to ensure the accuracy of the results UNC requested expedited processing of these results which UNC received on March 15 2010 (Attachment 4)

The main CoC identified in all of the samples included toluene ethylene glycol and propylene glycol which are components of the materials being utilized in the construction site of Building 3 Additionally these chemicals are not commonly used at the Bingham Facility Consequently UNC believes that the construction materials were the likely source of the CoCs The main construction activities have been completed and the floor drains have been covered to reduce the likelihood of a recurrence

On March 16 2010 UNC contacted Damon Forney the Operations Manager at OWASA to supply him with analytical data from the samples collected to date (including an analysis of samples (Attachment 5) taken on February 18-19 2010 which were collected to initiate UNCs evaluation of the wastewater treatment system) and to inquire whether OWASA could continue to accept the wastewater The following day OWASA stated that it could not receive the wastewater because of the concentration of toluene present in the wastewater

UNC has contracted with Clean Harbors to dispose of the wastewater and to determine how to clean out the wastewater system The current plan is to flushclean the wastewater piping from Building 3 remove contaminated water store it on-site in frac tanks and clean the septic tank







Sincerely


Attachment 1










Date Time Temp


CI~bull f(I- )

H ~ +1-

I te~ ~

Ii ~ amp ~ t E 0

C G

C

G C

G C

G

C

G C

G C G C

G C

G C

G

~ ~ 1 ~50 EJS ClS ~ E

- p

G p

G p

G p

G p

G p

G p

G p

G p

G p

G

0 a_w lt( _ il

PRESERVATION


i r z I-

_

I-


5

Jl-l or to -lo--~~

94=1 )01 s-)



1 _2





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






















Ethylbenzene lt2







Trichloroethene lt2

Naphthalene lt2

n-Propylbenzene lt2

Styrene lt2


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







Toluene 328







Vinyl Chloride lt2

M+PXylene lt4

O-Xylene lt2

IPE lt2

MTBE lt2

Acetone lt 10

MEK ltlO

ltJO

2-Hexanone

MIBK

lt2

Ethanol lt2

Vinyl Acetate lt2



Ethylene Glycol 270


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Probability microgL

1 Propanaf 123-38-6 7882 8050


3 1-propanol 71-23-8 9391 1152

4

5

6

7

8

9

11

12

Comment



Reviewed by

Attachment 2









Collection


Date I Time Temp


ot 7 amp8 ~


~-6Sio Ior-lt

T

0001 eqt I


itE~Jl


C p

~ ~ 4956

C p

G G C p

G G

C p

G G 49pound1

C p

~ $-C p

G G

C p


G G X C p

G G II C p

G G


GJ4 [pJsI

-eslh~ Jl)wl oj~hi

ampJ4 4d5-7

e~ 57ul ~ ~iJ gthi~

ib)_ 1sS 1J5 )lt






(910) 392-0223 (Lab) bull (90) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





4950 4951

Benzene






(910) 392-0223 (Lab bull (910) 392-4424 (Fax






4951

lt40

Analyte microgL

lt40

Methylene Chloride

Ethyl benzene lt40


lt40

lt40 lt40


111-Trlchloroetbane

148Toluene lt40

112-Trichloroethane

lt40

lt40 lt40



lt40

lt40

Vinyl Chloride

lt40

lt40 lt40

M+PXylene lt80 lt80

0-Xylene lt40 lt40

MTBE lt40 lt40

Acetone 656 532

030610Date Analyzed

Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





EOUALIZATION BASIN




4951


Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)









4951








Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)












54717-17-8 906



9 lndolc 120-72-9 944

10 P-Cresol 106-44-5 875

11

12

Comment



Page 5 of6

Result microgL

100

174

61

94

101

99

112

127

57

354


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





Number Compound

I Cholesterol



4 N-Nonylphenol




8 lndolzin

9 P-Cresol

11

12

Comment

CAS Match


57-88-5 907 121

84-61-7 887 201

57-10-3 821 72

25154-52-3 845 ll3

ll2-18-5 844 91

54717-17-8 855 272

54644-28-9 846 231

274-40-8 884 67

106-44-5 899 820



~~~









H Calibration

CgtJbull Make Model


Time Calibrated

0 D



)

Comment

Return Trip Check

1)efilW Model J1ta1


Standard I ( ) mgL

Standard 2 ( ) mgL

Standard 3 ( ) mgL


Recovery


-


Attachment 3





Dear Mr Porter











March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -








Sincerely


Attachment 1










Date Time Temp


CI~bull f(I- )

H ~ +1-

I te~ ~

Ii ~ amp ~ t E 0

C G

C

G C

G C

G

C

G C

G C G C

G C

G C

G

~ ~ 1 ~50 EJS ClS ~ E

- p

G p

G p

G p

G p

G p

G p

G p

G p

G p

G

0 a_w lt( _ il

PRESERVATION


i r z I-

_

I-


5

Jl-l or to -lo--~~

94=1 )01 s-)



1 _2





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






















Ethylbenzene lt2







Trichloroethene lt2

Naphthalene lt2

n-Propylbenzene lt2

Styrene lt2


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







Toluene 328







Vinyl Chloride lt2

M+PXylene lt4

O-Xylene lt2

IPE lt2

MTBE lt2

Acetone lt 10

MEK ltlO

ltJO

2-Hexanone

MIBK

lt2

Ethanol lt2

Vinyl Acetate lt2



Ethylene Glycol 270


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Probability microgL

1 Propanaf 123-38-6 7882 8050


3 1-propanol 71-23-8 9391 1152

4

5

6

7

8

9

11

12

Comment



Reviewed by

Attachment 2









Collection


Date I Time Temp


ot 7 amp8 ~


~-6Sio Ior-lt

T

0001 eqt I


itE~Jl


C p

~ ~ 4956

C p

G G C p

G G

C p

G G 49pound1

C p

~ $-C p

G G

C p


G G X C p

G G II C p

G G


GJ4 [pJsI

-eslh~ Jl)wl oj~hi

ampJ4 4d5-7

e~ 57ul ~ ~iJ gthi~

ib)_ 1sS 1J5 )lt






(910) 392-0223 (Lab) bull (90) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





4950 4951

Benzene






(910) 392-0223 (Lab bull (910) 392-4424 (Fax






4951

lt40

Analyte microgL

lt40

Methylene Chloride

Ethyl benzene lt40


lt40

lt40 lt40


111-Trlchloroetbane

148Toluene lt40

112-Trichloroethane

lt40

lt40 lt40



lt40

lt40

Vinyl Chloride

lt40

lt40 lt40

M+PXylene lt80 lt80

0-Xylene lt40 lt40

MTBE lt40 lt40

Acetone 656 532

030610Date Analyzed

Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





EOUALIZATION BASIN




4951


Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)









4951








Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)












54717-17-8 906



9 lndolc 120-72-9 944

10 P-Cresol 106-44-5 875

11

12

Comment



Page 5 of6

Result microgL

100

174

61

94

101

99

112

127

57

354


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





Number Compound

I Cholesterol



4 N-Nonylphenol




8 lndolzin

9 P-Cresol

11

12

Comment

CAS Match


57-88-5 907 121

84-61-7 887 201

57-10-3 821 72

25154-52-3 845 ll3

ll2-18-5 844 91

54717-17-8 855 272

54644-28-9 846 231

274-40-8 884 67

106-44-5 899 820



~~~









H Calibration

CgtJbull Make Model


Time Calibrated

0 D



)

Comment

Return Trip Check

1)efilW Model J1ta1


Standard I ( ) mgL

Standard 2 ( ) mgL

Standard 3 ( ) mgL


Recovery


-


Attachment 3





Dear Mr Porter











March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -


Attachment 1










Date Time Temp


CI~bull f(I- )

H ~ +1-

I te~ ~

Ii ~ amp ~ t E 0

C G

C

G C

G C

G

C

G C

G C G C

G C

G C

G

~ ~ 1 ~50 EJS ClS ~ E

- p

G p

G p

G p

G p

G p

G p

G p

G p

G p

G

0 a_w lt( _ il

PRESERVATION


i r z I-

_

I-


5

Jl-l or to -lo--~~

94=1 )01 s-)



1 _2





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






















Ethylbenzene lt2







Trichloroethene lt2

Naphthalene lt2

n-Propylbenzene lt2

Styrene lt2


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







Toluene 328







Vinyl Chloride lt2

M+PXylene lt4

O-Xylene lt2

IPE lt2

MTBE lt2

Acetone lt 10

MEK ltlO

ltJO

2-Hexanone

MIBK

lt2

Ethanol lt2

Vinyl Acetate lt2



Ethylene Glycol 270


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Probability microgL

1 Propanaf 123-38-6 7882 8050


3 1-propanol 71-23-8 9391 1152

4

5

6

7

8

9

11

12

Comment



Reviewed by

Attachment 2









Collection


Date I Time Temp


ot 7 amp8 ~


~-6Sio Ior-lt

T

0001 eqt I


itE~Jl


C p

~ ~ 4956

C p

G G C p

G G

C p

G G 49pound1

C p

~ $-C p

G G

C p


G G X C p

G G II C p

G G


GJ4 [pJsI

-eslh~ Jl)wl oj~hi

ampJ4 4d5-7

e~ 57ul ~ ~iJ gthi~

ib)_ 1sS 1J5 )lt






(910) 392-0223 (Lab) bull (90) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





4950 4951

Benzene






(910) 392-0223 (Lab bull (910) 392-4424 (Fax






4951

lt40

Analyte microgL

lt40

Methylene Chloride

Ethyl benzene lt40


lt40

lt40 lt40


111-Trlchloroetbane

148Toluene lt40

112-Trichloroethane

lt40

lt40 lt40



lt40

lt40

Vinyl Chloride

lt40

lt40 lt40

M+PXylene lt80 lt80

0-Xylene lt40 lt40

MTBE lt40 lt40

Acetone 656 532

030610Date Analyzed

Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





EOUALIZATION BASIN




4951


Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)









4951








Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)












54717-17-8 906



9 lndolc 120-72-9 944

10 P-Cresol 106-44-5 875

11

12

Comment



Page 5 of6

Result microgL

100

174

61

94

101

99

112

127

57

354


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





Number Compound

I Cholesterol



4 N-Nonylphenol




8 lndolzin

9 P-Cresol

11

12

Comment

CAS Match


57-88-5 907 121

84-61-7 887 201

57-10-3 821 72

25154-52-3 845 ll3

ll2-18-5 844 91

54717-17-8 855 272

54644-28-9 846 231

274-40-8 884 67

106-44-5 899 820



~~~









H Calibration

CgtJbull Make Model


Time Calibrated

0 D



)

Comment

Return Trip Check

1)efilW Model J1ta1


Standard I ( ) mgL

Standard 2 ( ) mgL

Standard 3 ( ) mgL


Recovery


-


Attachment 3





Dear Mr Porter











March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -











Date Time Temp


CI~bull f(I- )

H ~ +1-

I te~ ~

Ii ~ amp ~ t E 0

C G

C

G C

G C

G

C

G C

G C G C

G C

G C

G

~ ~ 1 ~50 EJS ClS ~ E

- p

G p

G p

G p

G p

G p

G p

G p

G p

G p

G

0 a_w lt( _ il

PRESERVATION


i r z I-

_

I-


5

Jl-l or to -lo--~~

94=1 )01 s-)



1 _2





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






















Ethylbenzene lt2







Trichloroethene lt2

Naphthalene lt2

n-Propylbenzene lt2

Styrene lt2


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







Toluene 328







Vinyl Chloride lt2

M+PXylene lt4

O-Xylene lt2

IPE lt2

MTBE lt2

Acetone lt 10

MEK ltlO

ltJO

2-Hexanone

MIBK

lt2

Ethanol lt2

Vinyl Acetate lt2



Ethylene Glycol 270


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Probability microgL

1 Propanaf 123-38-6 7882 8050


3 1-propanol 71-23-8 9391 1152

4

5

6

7

8

9

11

12

Comment



Reviewed by

Attachment 2









Collection


Date I Time Temp


ot 7 amp8 ~


~-6Sio Ior-lt

T

0001 eqt I


itE~Jl


C p

~ ~ 4956

C p

G G C p

G G

C p

G G 49pound1

C p

~ $-C p

G G

C p


G G X C p

G G II C p

G G


GJ4 [pJsI

-eslh~ Jl)wl oj~hi

ampJ4 4d5-7

e~ 57ul ~ ~iJ gthi~

ib)_ 1sS 1J5 )lt






(910) 392-0223 (Lab) bull (90) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





4950 4951

Benzene






(910) 392-0223 (Lab bull (910) 392-4424 (Fax






4951

lt40

Analyte microgL

lt40

Methylene Chloride

Ethyl benzene lt40


lt40

lt40 lt40


111-Trlchloroetbane

148Toluene lt40

112-Trichloroethane

lt40

lt40 lt40



lt40

lt40

Vinyl Chloride

lt40

lt40 lt40

M+PXylene lt80 lt80

0-Xylene lt40 lt40

MTBE lt40 lt40

Acetone 656 532

030610Date Analyzed

Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





EOUALIZATION BASIN




4951


Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)









4951








Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)












54717-17-8 906



9 lndolc 120-72-9 944

10 P-Cresol 106-44-5 875

11

12

Comment



Page 5 of6

Result microgL

100

174

61

94

101

99

112

127

57

354


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





Number Compound

I Cholesterol



4 N-Nonylphenol




8 lndolzin

9 P-Cresol

11

12

Comment

CAS Match


57-88-5 907 121

84-61-7 887 201

57-10-3 821 72

25154-52-3 845 ll3

ll2-18-5 844 91

54717-17-8 855 272

54644-28-9 846 231

274-40-8 884 67

106-44-5 899 820



~~~









H Calibration

CgtJbull Make Model


Time Calibrated

0 D



)

Comment

Return Trip Check

1)efilW Model J1ta1


Standard I ( ) mgL

Standard 2 ( ) mgL

Standard 3 ( ) mgL


Recovery


-


Attachment 3





Dear Mr Porter











March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






















Ethylbenzene lt2







Trichloroethene lt2

Naphthalene lt2

n-Propylbenzene lt2

Styrene lt2


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







Toluene 328







Vinyl Chloride lt2

M+PXylene lt4

O-Xylene lt2

IPE lt2

MTBE lt2

Acetone lt 10

MEK ltlO

ltJO

2-Hexanone

MIBK

lt2

Ethanol lt2

Vinyl Acetate lt2



Ethylene Glycol 270


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Probability microgL

1 Propanaf 123-38-6 7882 8050


3 1-propanol 71-23-8 9391 1152

4

5

6

7

8

9

11

12

Comment



Reviewed by

Attachment 2









Collection


Date I Time Temp


ot 7 amp8 ~


~-6Sio Ior-lt

T

0001 eqt I


itE~Jl


C p

~ ~ 4956

C p

G G C p

G G

C p

G G 49pound1

C p

~ $-C p

G G

C p


G G X C p

G G II C p

G G


GJ4 [pJsI

-eslh~ Jl)wl oj~hi

ampJ4 4d5-7

e~ 57ul ~ ~iJ gthi~

ib)_ 1sS 1J5 )lt






(910) 392-0223 (Lab) bull (90) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





4950 4951

Benzene






(910) 392-0223 (Lab bull (910) 392-4424 (Fax






4951

lt40

Analyte microgL

lt40

Methylene Chloride

Ethyl benzene lt40


lt40

lt40 lt40


111-Trlchloroetbane

148Toluene lt40

112-Trichloroethane

lt40

lt40 lt40



lt40

lt40

Vinyl Chloride

lt40

lt40 lt40

M+PXylene lt80 lt80

0-Xylene lt40 lt40

MTBE lt40 lt40

Acetone 656 532

030610Date Analyzed

Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





EOUALIZATION BASIN




4951


Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)









4951








Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)












54717-17-8 906



9 lndolc 120-72-9 944

10 P-Cresol 106-44-5 875

11

12

Comment



Page 5 of6

Result microgL

100

174

61

94

101

99

112

127

57

354


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





Number Compound

I Cholesterol



4 N-Nonylphenol




8 lndolzin

9 P-Cresol

11

12

Comment

CAS Match


57-88-5 907 121

84-61-7 887 201

57-10-3 821 72

25154-52-3 845 ll3

ll2-18-5 844 91

54717-17-8 855 272

54644-28-9 846 231

274-40-8 884 67

106-44-5 899 820



~~~









H Calibration

CgtJbull Make Model


Time Calibrated

0 D



)

Comment

Return Trip Check

1)efilW Model J1ta1


Standard I ( ) mgL

Standard 2 ( ) mgL

Standard 3 ( ) mgL


Recovery


-


Attachment 3





Dear Mr Porter











March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






















Ethylbenzene lt2







Trichloroethene lt2

Naphthalene lt2

n-Propylbenzene lt2

Styrene lt2


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







Toluene 328







Vinyl Chloride lt2

M+PXylene lt4

O-Xylene lt2

IPE lt2

MTBE lt2

Acetone lt 10

MEK ltlO

ltJO

2-Hexanone

MIBK

lt2

Ethanol lt2

Vinyl Acetate lt2



Ethylene Glycol 270


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Probability microgL

1 Propanaf 123-38-6 7882 8050


3 1-propanol 71-23-8 9391 1152

4

5

6

7

8

9

11

12

Comment



Reviewed by

Attachment 2









Collection


Date I Time Temp


ot 7 amp8 ~


~-6Sio Ior-lt

T

0001 eqt I


itE~Jl


C p

~ ~ 4956

C p

G G C p

G G

C p

G G 49pound1

C p

~ $-C p

G G

C p


G G X C p

G G II C p

G G


GJ4 [pJsI

-eslh~ Jl)wl oj~hi

ampJ4 4d5-7

e~ 57ul ~ ~iJ gthi~

ib)_ 1sS 1J5 )lt






(910) 392-0223 (Lab) bull (90) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





4950 4951

Benzene






(910) 392-0223 (Lab bull (910) 392-4424 (Fax






4951

lt40

Analyte microgL

lt40

Methylene Chloride

Ethyl benzene lt40


lt40

lt40 lt40


111-Trlchloroetbane

148Toluene lt40

112-Trichloroethane

lt40

lt40 lt40



lt40

lt40

Vinyl Chloride

lt40

lt40 lt40

M+PXylene lt80 lt80

0-Xylene lt40 lt40

MTBE lt40 lt40

Acetone 656 532

030610Date Analyzed

Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





EOUALIZATION BASIN




4951


Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)









4951








Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)












54717-17-8 906



9 lndolc 120-72-9 944

10 P-Cresol 106-44-5 875

11

12

Comment



Page 5 of6

Result microgL

100

174

61

94

101

99

112

127

57

354


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





Number Compound

I Cholesterol



4 N-Nonylphenol




8 lndolzin

9 P-Cresol

11

12

Comment

CAS Match


57-88-5 907 121

84-61-7 887 201

57-10-3 821 72

25154-52-3 845 ll3

ll2-18-5 844 91

54717-17-8 855 272

54644-28-9 846 231

274-40-8 884 67

106-44-5 899 820



~~~









H Calibration

CgtJbull Make Model


Time Calibrated

0 D



)

Comment

Return Trip Check

1)efilW Model J1ta1


Standard I ( ) mgL

Standard 2 ( ) mgL

Standard 3 ( ) mgL


Recovery


-


Attachment 3





Dear Mr Porter











March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







Toluene 328







Vinyl Chloride lt2

M+PXylene lt4

O-Xylene lt2

IPE lt2

MTBE lt2

Acetone lt 10

MEK ltlO

ltJO

2-Hexanone

MIBK

lt2

Ethanol lt2

Vinyl Acetate lt2



Ethylene Glycol 270


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Probability microgL

1 Propanaf 123-38-6 7882 8050


3 1-propanol 71-23-8 9391 1152

4

5

6

7

8

9

11

12

Comment



Reviewed by

Attachment 2









Collection


Date I Time Temp


ot 7 amp8 ~


~-6Sio Ior-lt

T

0001 eqt I


itE~Jl


C p

~ ~ 4956

C p

G G C p

G G

C p

G G 49pound1

C p

~ $-C p

G G

C p


G G X C p

G G II C p

G G


GJ4 [pJsI

-eslh~ Jl)wl oj~hi

ampJ4 4d5-7

e~ 57ul ~ ~iJ gthi~

ib)_ 1sS 1J5 )lt






(910) 392-0223 (Lab) bull (90) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





4950 4951

Benzene






(910) 392-0223 (Lab bull (910) 392-4424 (Fax






4951

lt40

Analyte microgL

lt40

Methylene Chloride

Ethyl benzene lt40


lt40

lt40 lt40


111-Trlchloroetbane

148Toluene lt40

112-Trichloroethane

lt40

lt40 lt40



lt40

lt40

Vinyl Chloride

lt40

lt40 lt40

M+PXylene lt80 lt80

0-Xylene lt40 lt40

MTBE lt40 lt40

Acetone 656 532

030610Date Analyzed

Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





EOUALIZATION BASIN




4951


Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)









4951








Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)












54717-17-8 906



9 lndolc 120-72-9 944

10 P-Cresol 106-44-5 875

11

12

Comment



Page 5 of6

Result microgL

100

174

61

94

101

99

112

127

57

354


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





Number Compound

I Cholesterol



4 N-Nonylphenol




8 lndolzin

9 P-Cresol

11

12

Comment

CAS Match


57-88-5 907 121

84-61-7 887 201

57-10-3 821 72

25154-52-3 845 ll3

ll2-18-5 844 91

54717-17-8 855 272

54644-28-9 846 231

274-40-8 884 67

106-44-5 899 820



~~~









H Calibration

CgtJbull Make Model


Time Calibrated

0 D



)

Comment

Return Trip Check

1)efilW Model J1ta1


Standard I ( ) mgL

Standard 2 ( ) mgL

Standard 3 ( ) mgL


Recovery


-


Attachment 3





Dear Mr Porter











March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Probability microgL

1 Propanaf 123-38-6 7882 8050


3 1-propanol 71-23-8 9391 1152

4

5

6

7

8

9

11

12

Comment



Reviewed by

Attachment 2









Collection


Date I Time Temp


ot 7 amp8 ~


~-6Sio Ior-lt

T

0001 eqt I


itE~Jl


C p

~ ~ 4956

C p

G G C p

G G

C p

G G 49pound1

C p

~ $-C p

G G

C p


G G X C p

G G II C p

G G


GJ4 [pJsI

-eslh~ Jl)wl oj~hi

ampJ4 4d5-7

e~ 57ul ~ ~iJ gthi~

ib)_ 1sS 1J5 )lt






(910) 392-0223 (Lab) bull (90) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





4950 4951

Benzene






(910) 392-0223 (Lab bull (910) 392-4424 (Fax






4951

lt40

Analyte microgL

lt40

Methylene Chloride

Ethyl benzene lt40


lt40

lt40 lt40


111-Trlchloroetbane

148Toluene lt40

112-Trichloroethane

lt40

lt40 lt40



lt40

lt40

Vinyl Chloride

lt40

lt40 lt40

M+PXylene lt80 lt80

0-Xylene lt40 lt40

MTBE lt40 lt40

Acetone 656 532

030610Date Analyzed

Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





EOUALIZATION BASIN




4951


Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)









4951








Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)












54717-17-8 906



9 lndolc 120-72-9 944

10 P-Cresol 106-44-5 875

11

12

Comment



Page 5 of6

Result microgL

100

174

61

94

101

99

112

127

57

354


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





Number Compound

I Cholesterol



4 N-Nonylphenol




8 lndolzin

9 P-Cresol

11

12

Comment

CAS Match


57-88-5 907 121

84-61-7 887 201

57-10-3 821 72

25154-52-3 845 ll3

ll2-18-5 844 91

54717-17-8 855 272

54644-28-9 846 231

274-40-8 884 67

106-44-5 899 820



~~~









H Calibration

CgtJbull Make Model


Time Calibrated

0 D



)

Comment

Return Trip Check

1)efilW Model J1ta1


Standard I ( ) mgL

Standard 2 ( ) mgL

Standard 3 ( ) mgL


Recovery


-


Attachment 3





Dear Mr Porter











March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -


Attachment 2









Collection


Date I Time Temp


ot 7 amp8 ~


~-6Sio Ior-lt

T

0001 eqt I


itE~Jl


C p

~ ~ 4956

C p

G G C p

G G

C p

G G 49pound1

C p

~ $-C p

G G

C p


G G X C p

G G II C p

G G


GJ4 [pJsI

-eslh~ Jl)wl oj~hi

ampJ4 4d5-7

e~ 57ul ~ ~iJ gthi~

ib)_ 1sS 1J5 )lt






(910) 392-0223 (Lab) bull (90) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





4950 4951

Benzene






(910) 392-0223 (Lab bull (910) 392-4424 (Fax






4951

lt40

Analyte microgL

lt40

Methylene Chloride

Ethyl benzene lt40


lt40

lt40 lt40


111-Trlchloroetbane

148Toluene lt40

112-Trichloroethane

lt40

lt40 lt40



lt40

lt40

Vinyl Chloride

lt40

lt40 lt40

M+PXylene lt80 lt80

0-Xylene lt40 lt40

MTBE lt40 lt40

Acetone 656 532

030610Date Analyzed

Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





EOUALIZATION BASIN




4951


Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)









4951








Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)












54717-17-8 906



9 lndolc 120-72-9 944

10 P-Cresol 106-44-5 875

11

12

Comment



Page 5 of6

Result microgL

100

174

61

94

101

99

112

127

57

354


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





Number Compound

I Cholesterol



4 N-Nonylphenol




8 lndolzin

9 P-Cresol

11

12

Comment

CAS Match


57-88-5 907 121

84-61-7 887 201

57-10-3 821 72

25154-52-3 845 ll3

ll2-18-5 844 91

54717-17-8 855 272

54644-28-9 846 231

274-40-8 884 67

106-44-5 899 820



~~~









H Calibration

CgtJbull Make Model


Time Calibrated

0 D



)

Comment

Return Trip Check

1)efilW Model J1ta1


Standard I ( ) mgL

Standard 2 ( ) mgL

Standard 3 ( ) mgL


Recovery


-


Attachment 3





Dear Mr Porter











March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -










Collection


Date I Time Temp


ot 7 amp8 ~


~-6Sio Ior-lt

T

0001 eqt I


itE~Jl


C p

~ ~ 4956

C p

G G C p

G G

C p

G G 49pound1

C p

~ $-C p

G G

C p


G G X C p

G G II C p

G G


GJ4 [pJsI

-eslh~ Jl)wl oj~hi

ampJ4 4d5-7

e~ 57ul ~ ~iJ gthi~

ib)_ 1sS 1J5 )lt






(910) 392-0223 (Lab) bull (90) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





4950 4951

Benzene






(910) 392-0223 (Lab bull (910) 392-4424 (Fax






4951

lt40

Analyte microgL

lt40

Methylene Chloride

Ethyl benzene lt40


lt40

lt40 lt40


111-Trlchloroetbane

148Toluene lt40

112-Trichloroethane

lt40

lt40 lt40



lt40

lt40

Vinyl Chloride

lt40

lt40 lt40

M+PXylene lt80 lt80

0-Xylene lt40 lt40

MTBE lt40 lt40

Acetone 656 532

030610Date Analyzed

Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





EOUALIZATION BASIN




4951


Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)









4951








Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)












54717-17-8 906



9 lndolc 120-72-9 944

10 P-Cresol 106-44-5 875

11

12

Comment



Page 5 of6

Result microgL

100

174

61

94

101

99

112

127

57

354


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





Number Compound

I Cholesterol



4 N-Nonylphenol




8 lndolzin

9 P-Cresol

11

12

Comment

CAS Match


57-88-5 907 121

84-61-7 887 201

57-10-3 821 72

25154-52-3 845 ll3

ll2-18-5 844 91

54717-17-8 855 272

54644-28-9 846 231

274-40-8 884 67

106-44-5 899 820



~~~









H Calibration

CgtJbull Make Model


Time Calibrated

0 D



)

Comment

Return Trip Check

1)efilW Model J1ta1


Standard I ( ) mgL

Standard 2 ( ) mgL

Standard 3 ( ) mgL


Recovery


-


Attachment 3





Dear Mr Porter











March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab) bull (90) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





4950 4951

Benzene






(910) 392-0223 (Lab bull (910) 392-4424 (Fax






4951

lt40

Analyte microgL

lt40

Methylene Chloride

Ethyl benzene lt40


lt40

lt40 lt40


111-Trlchloroetbane

148Toluene lt40

112-Trichloroethane

lt40

lt40 lt40



lt40

lt40

Vinyl Chloride

lt40

lt40 lt40

M+PXylene lt80 lt80

0-Xylene lt40 lt40

MTBE lt40 lt40

Acetone 656 532

030610Date Analyzed

Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





EOUALIZATION BASIN




4951


Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)









4951








Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)












54717-17-8 906



9 lndolc 120-72-9 944

10 P-Cresol 106-44-5 875

11

12

Comment



Page 5 of6

Result microgL

100

174

61

94

101

99

112

127

57

354


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





Number Compound

I Cholesterol



4 N-Nonylphenol




8 lndolzin

9 P-Cresol

11

12

Comment

CAS Match


57-88-5 907 121

84-61-7 887 201

57-10-3 821 72

25154-52-3 845 ll3

ll2-18-5 844 91

54717-17-8 855 272

54644-28-9 846 231

274-40-8 884 67

106-44-5 899 820



~~~









H Calibration

CgtJbull Make Model


Time Calibrated

0 D



)

Comment

Return Trip Check

1)efilW Model J1ta1


Standard I ( ) mgL

Standard 2 ( ) mgL

Standard 3 ( ) mgL


Recovery


-


Attachment 3





Dear Mr Porter











March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab bull (910) 392-4424 (Fax






4951

lt40

Analyte microgL

lt40

Methylene Chloride

Ethyl benzene lt40


lt40

lt40 lt40


111-Trlchloroetbane

148Toluene lt40

112-Trichloroethane

lt40

lt40 lt40



lt40

lt40

Vinyl Chloride

lt40

lt40 lt40

M+PXylene lt80 lt80

0-Xylene lt40 lt40

MTBE lt40 lt40

Acetone 656 532

030610Date Analyzed

Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





EOUALIZATION BASIN




4951


Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)









4951








Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)












54717-17-8 906



9 lndolc 120-72-9 944

10 P-Cresol 106-44-5 875

11

12

Comment



Page 5 of6

Result microgL

100

174

61

94

101

99

112

127

57

354


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





Number Compound

I Cholesterol



4 N-Nonylphenol




8 lndolzin

9 P-Cresol

11

12

Comment

CAS Match


57-88-5 907 121

84-61-7 887 201

57-10-3 821 72

25154-52-3 845 ll3

ll2-18-5 844 91

54717-17-8 855 272

54644-28-9 846 231

274-40-8 884 67

106-44-5 899 820



~~~









H Calibration

CgtJbull Make Model


Time Calibrated

0 D



)

Comment

Return Trip Check

1)efilW Model J1ta1


Standard I ( ) mgL

Standard 2 ( ) mgL

Standard 3 ( ) mgL


Recovery


-


Attachment 3





Dear Mr Porter











March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





EOUALIZATION BASIN




4951


Comments



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)









4951








Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)












54717-17-8 906



9 lndolc 120-72-9 944

10 P-Cresol 106-44-5 875

11

12

Comment



Page 5 of6

Result microgL

100

174

61

94

101

99

112

127

57

354


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





Number Compound

I Cholesterol



4 N-Nonylphenol




8 lndolzin

9 P-Cresol

11

12

Comment

CAS Match


57-88-5 907 121

84-61-7 887 201

57-10-3 821 72

25154-52-3 845 ll3

ll2-18-5 844 91

54717-17-8 855 272

54644-28-9 846 231

274-40-8 884 67

106-44-5 899 820



~~~









H Calibration

CgtJbull Make Model


Time Calibrated

0 D



)

Comment

Return Trip Check

1)efilW Model J1ta1


Standard I ( ) mgL

Standard 2 ( ) mgL

Standard 3 ( ) mgL


Recovery


-


Attachment 3





Dear Mr Porter











March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)









4951








Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)












54717-17-8 906



9 lndolc 120-72-9 944

10 P-Cresol 106-44-5 875

11

12

Comment



Page 5 of6

Result microgL

100

174

61

94

101

99

112

127

57

354


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





Number Compound

I Cholesterol



4 N-Nonylphenol




8 lndolzin

9 P-Cresol

11

12

Comment

CAS Match


57-88-5 907 121

84-61-7 887 201

57-10-3 821 72

25154-52-3 845 ll3

ll2-18-5 844 91

54717-17-8 855 272

54644-28-9 846 231

274-40-8 884 67

106-44-5 899 820



~~~









H Calibration

CgtJbull Make Model


Time Calibrated

0 D



)

Comment

Return Trip Check

1)efilW Model J1ta1


Standard I ( ) mgL

Standard 2 ( ) mgL

Standard 3 ( ) mgL


Recovery


-


Attachment 3





Dear Mr Porter











March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)












54717-17-8 906



9 lndolc 120-72-9 944

10 P-Cresol 106-44-5 875

11

12

Comment



Page 5 of6

Result microgL

100

174

61

94

101

99

112

127

57

354


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





Number Compound

I Cholesterol



4 N-Nonylphenol




8 lndolzin

9 P-Cresol

11

12

Comment

CAS Match


57-88-5 907 121

84-61-7 887 201

57-10-3 821 72

25154-52-3 845 ll3

ll2-18-5 844 91

54717-17-8 855 272

54644-28-9 846 231

274-40-8 884 67

106-44-5 899 820



~~~









H Calibration

CgtJbull Make Model


Time Calibrated

0 D



)

Comment

Return Trip Check

1)efilW Model J1ta1


Standard I ( ) mgL

Standard 2 ( ) mgL

Standard 3 ( ) mgL


Recovery


-


Attachment 3





Dear Mr Porter











March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





Number Compound

I Cholesterol



4 N-Nonylphenol




8 lndolzin

9 P-Cresol

11

12

Comment

CAS Match


57-88-5 907 121

84-61-7 887 201

57-10-3 821 72

25154-52-3 845 ll3

ll2-18-5 844 91

54717-17-8 855 272

54644-28-9 846 231

274-40-8 884 67

106-44-5 899 820



~~~









H Calibration

CgtJbull Make Model


Time Calibrated

0 D



)

Comment

Return Trip Check

1)efilW Model J1ta1


Standard I ( ) mgL

Standard 2 ( ) mgL

Standard 3 ( ) mgL


Recovery


-


Attachment 3





Dear Mr Porter











March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -









H Calibration

CgtJbull Make Model


Time Calibrated

0 D



)

Comment

Return Trip Check

1)efilW Model J1ta1


Standard I ( ) mgL

Standard 2 ( ) mgL

Standard 3 ( ) mgL


Recovery


-


Attachment 3





Dear Mr Porter











March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -


Attachment 3





Dear Mr Porter











March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -






Dear Mr Porter











March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -






March 121 2010




624 Analyses



Page 2 of 8





DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -






DF =Dilution Factor

Dup =Duplicate



















M13402 I 8084

Page 3 of 8





Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -






Comments


Analyst l





byGCMS624


400 400 400 400 400 400 400 500 400 400 400 400 400 400 400 400 400 400 400 400 400 100 400 200 400 400 400 400 400 400 400 400 400 800 400


10 102 10 994 10 999

Paga 1 of2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

102 99 100


GCMSxlamp

Page 4 of 8







Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -








Time CAS Match


0 0 0 4 5 6 7 8 9 10


298 182 590 654

000075-18-3 000075-07-0 003877-15-4 000624-92-0

91 90 97 95

137 101 922 716

Comment





Page 5 of 8





Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -






Comments







10 101 10 99 10 102

Page 1 of 2




4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010 4 3112010

Percent Recovered

101 99 102

Reviewed ByTpound

GCMSxa

Page 6 of 8

624







Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -








Matrix Water



7

8 9

10

Comment



Reviewed by 1j


Page 7 of 8

-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -


-----------





Phone __________ Fax ____________




1(q SI S5k10 1))

Wftvfrac14 ~L j

Co 2~_ -+ I(_ I - se -kJlt--L (-1-- T

1 bull cl ~ i-lc



~ 5 rgt






Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -


Attachment 4

__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -


__________________







) Claquo~I-~ tJ

p ff 91 L

2) frc ( C _ ) -

plf Jo

) S~nlc frgt

__f~ I

pl- Ct

Collection


C7gt0

I

J1_ ~lt0 Y 5 lt

UgtO

I 0--I ff

0

c



COPY TO ____ -~__ _ _ _ _


PONO _____________

PHONEFAX___________

E-MAILmiddot


bull0 8E ~

1bullo~~ 0 E e 0 ()

bull-CC

bull- 0C 0

ll -

bull-- Ogt ~E ()

C ll m~ lt( i1

w z 0 z

PRESERVATION

~ X8 u 0 8 0 Q

X N z lt X X X z

ll w X

0

(C) G

(P (G

tlt ( )lt ( )lt

C p

G G

C p

G G (C)

G

(Ip

( G) svV -

C p

G G

C p

G G degfi

C (Pl (G) G

C p

G G

C p

G G

C p

G G

ANALYSIS REQUESTED

60~c) -1 ltI_ 1 ~lt r ~


(fl~-(lt_ - ~ -J(~ ) -



1

2 when Received

~ ~ i

LI- L

J fgt

p _ __

- Accepted

Received By

- ~(-$ -f V C I C

Rejected

=-) _d ~ -t- gt-0


r

Daternme

Time z ltrgt gt T

4

~

4


(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab) bull (910) 392-4424 (hix)



Customer



REPORT OF ANALYSIS





5446 Septic 5447







(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)















-



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknownbull 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

10

JI

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 320

2 1-Propanol 71-23-8 9377 232


4

5

6

7

8

9

10

11

12




___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -


___ _ _ _ _ _







COPYTO E-MAIL

Sampled BX_ -1- lt----- Z~~ -~~



z) gter-1c(e_) -

pl t Jo

) S~dc 0 -f-f-~k

gt t-1- (Ct

Date 30

)t I

I bull

Collection

Time ltlto

7gt0

f-fO

(0gt0

10

- z__

bull0E obull Temp

0

L I C

( pound -

ff f 0

lt-


(C) G C

G C

G IC)

G C

G

C

G

C fG)

C

G

C

G

C

G

-sosC 0 0 0 u-

(P)

(G) p

G p

G (Pl ( G)

p

G p

G ( PJ

G p

G p

G p

G

sbull ~t u

9 ffi 10 10

I sectiz

rN(

ifI 1

sltli r

w z 0 z

Y-

PRESERVATION

0 X

(

ii 0 N X

~

8 z X

X 0

z ~ ~ ~

~ w X

0 ~

ANALYSlS REQUESTED


N

(JI--(_ - J - )



1

2 when Received

~ ~ -r

p ~



Rejected

~-0 ~ v [_ ~O


~

Time 7- ltFfp7-


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS





5446 Septic 5447




(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)





WASTEWATER EPA 624

Capetown 5446








Toluene 136 529






M+PXylene 94 lt40

O-Xylene 16 lt20

MTBE lt20 lt20

Acetone 37 lt JO



Septic 5447






(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)






Unknown 143

2 Unknownbull 128

3 Unknown 345

4 1-Propanol 71-23-8 9447 105


6

7

8

9

JO

11

12





(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)







1

2

3

4

Unknown

1-Propanol


71-23-8

3877-15-4

9377

9348

320

232

160

5

6

7

8

9

II

12









Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -






Dear Mr Porter





9

middotroJt Lori Loe







March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -






March IS 2010



624 Analyses



Page 2 of 12






Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -







Dup = Duplicate



















Ml3402 I 8084

Page 3 of 12






Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -







Analyte




Analyzed By BWS



Matrix Water


BQL 200 3122010 BQL 200 31122010
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -
















Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -






Comments

Flags





111 800 BQL 400


10 841 10 992 10 10

Page 1 of 2




4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010 4 3152010

Percent Recovered

84 99 100

GCMS

Page 6 of 12 624












Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -













Page 2 of 2 GCMS

Page 7 of 12 624







Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -








Time CAS Match


2

3

4

5 6

7

8

9

10

Dimethyl sulfide


1-Propanethiol

299

592

429

000075-18-3

003877-15-4

000107-03-9

91

94

96

418

163

683

Comment



Reviewed by L~


Page 8 of 12





Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -






Comments

Flags






10 842 10 998 10 972

Page 1 of 2




25 3152010 25 31152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31512010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 31152010 25 31152010 25 31152010 25 3152010 25 31512010 25 3152010 25 31512010 25 31512010 25 31152010 25 31152010 25 31152010 25 31152010 25 31152010 25 3152010 25 3152010 25 3152010 25 3152010 25 3152010 25 31512010 25 3152010 25 31152010 25 31152010

Percent Recovered

84 100 97

GCMS

Page 9 of 12

624











Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -












Reviewed By -~----

GCMSPage 2 of2

Page 10 of 12 624







Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -








Time CAS Match

Probability

78

Result uaL 1423

4

5

6

7

8 9

10

1-Propanol 404 000071-23-8

Comment



Reviewed by _tli-__


Page11of12








J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -









J

JiI

O 1 Q




~ w E lt z

0 0 X 0 0 11

ltJ _ z 0 X ~ z ~ ~



C p vc f lfl - lot)


2-) lt _c_

lo~O G G




C p Cc -f7 wl

G G C p I

G G C p _ooc G G




1


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -


Attachment 5


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)



Customer



REPORT OF ANALYSIS






533 5 SM5210B 021910


444 3 SM5210B 021910











Color units 200 100 SM2120B 030110


Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)




Parameters

Antimony Sb mgL

ArsenicAs mgL

Barium Ba mgL

Beryllium Be mgL

Cadmium Cd mgL

Chromium Cr mgL

Cobalt Co mgL

Copper Cu mgL

Lead Pb mgL

Nickel Ni mgL

Selenium Se mgL

Silver Ag mgL

Thallium TI mgL

Vanadium V mgL

Zinc Zn mgL

Parameter


pH units

-


lt 0010 lt 0010 EPA 2007 022410

lt 0010 lt 0010 EPA 2007 022310

0154 lt 0010 EPA2007 022410

lt0010 lt 0010 EPA2007 022410

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 0010 EPA 2007 022310

lt 0010 lt 00IO EPA 2007 022410

0077 0021 EPA 2007 022310

0039 lt 0010 EPA2007 022310

0016 0014 EPA2007 022310

lt 0010 lt0010 EPA 2007 022310

lt 0010 lt 0010 EPA2007 022310

lt0010 lt 0010 EPA 2007 022510

lt 0010 lt 0010 EPA 2007 022510

0625 0845 EPA2007 022510


68 64 SM2550B 021910

880 673 SM 4500 ff+

021910B

Comments


(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -



(910) 392-0223 (Lab) bull (910) 392-4424 (Fax)










199 030310 030910middot--middot--

258








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -








COPY TO E-MAIL


-A~---~~ IL J I



w g ~



1 ~ t

I


1 -rtP 1 I ti



G G ()-



__ 1 l Q

Gf c ltv1t G G G

C p

oil-- amp ~ ~7-

G G

C p

G G C p

G G C p

G G C p

G G C p



1 2

- - -


Documents

March 25, 2010: UNC report of chemical odor in septic tank · for offsite disposal. Once these activities are completed, UNC plans to resume normal pump and haul activities. Please