Letter submitting Removal Assessment Report with Report Attached · 2020-05-03 · cc Debra Dorsey, START Project Officer (cover letter only) X9025.15.0086.000 415 Oak Street, Kansas

['"ft:) TETRA TECH

April 20, 2016

Mr. Todd Campbell On-Scene Coordinator U.S. Environmental Protection Agency 11201 Renner Boulevard Lenexa, Kansas 66219

Subject: Removal Assessment Report Osage and Walnut Site, Coffeyville, Kansas U.S. EPA Region 7 START 4, Contract No. EP-S7-13-06, Task Order No. 0086 Task Monitor: Todd Campbell, On-Scene Coordinator

Dear Mr. Campbell:

Tetra Tech, Inc. is submitting the attached Removal Assessment Report regarding activities conducted at the Osage and Walnut site in Coffeyville, Kansas. If you have any questions or comments, please contact the Project Manager at (816) 412-1777.

Sincerely,

nny O' Connor ST ART Project Manager

/-;:z?/ Ted Faile, PG, CHMM ST ART Program Manager

Enclosures

cc Debra Dorsey, START Project Officer (cover letter only)

X9025.15.0086.000 415 Oak Street, Kansas City, MO 64106 Tel 816.412.1741 Fax 816.410.1748 www.tetratech.com

REMOVAL ASSESSMENT REPORT

OSAGE AND WALNUT SITE

COFFEYVILLE, MONTGOMERY COUNTY, KANSAS

Superfund Technical Assessment and Response Team (START) 4

Contract No. EP-S7-13-06, Task Order No. 0086

Prepared For:

U.S. Environmental Protection Agency

Region 7

11201 Renner Boulevard

Lenexa, Kansas 66219

April 20, 2016

Prepared By:

Tetra Tech, Inc.

415 Oak Street

Kansas City, Missouri 64106

(816) 412-1741

X9025.15.0086.000 i

CONTENTS

Section Page

1.0 INTRODUCTION ........................................................................................................................... 1

2.0 BACKGROUND INFORMATION ................................................................................................. 3

2.1 THE OSAGE AND WALNUT SITE .................................................................................. 3

2.2 THE COFFEYVILLE RE-CON SITE ................................................................................ 3

2.3 PREVIOUS INVESTIGATIONS ....................................................................................... 4

2.3.1 UST Trust Fund Activities ..................................................................................... 4

2.3.2 Site Reconnaissance and Evaluation ...................................................................... 4

2.3.3 KDHE RCRA Inspection ....................................................................................... 5

2.3.4 Consent Order ........................................................................................................ 5

2.3.5 Comprehensive Investigation ................................................................................. 6

2.3.6 Comprehensive Investigation Addendum .............................................................. 6

2.3.7 Integrated Assessment ............................................................................................ 7

3.0 REMOVAL ASSESSMENT ACTIVITIES ..................................................................................... 8

3.1 CONTAINER INVENTORYING, SAMPLING, AND FIELD SCREENING ................... 8

3.2 DIRECT-PUSH TECHNOLOGY SOIL SAMPLING ........................................................ 9

3.3 SURFACE SOIL SAMPLING .......................................................................................... 13

3.4 RADIOLOGICAL SURVEY ............................................................................................ 14

3.5 QUALITY CONTROL SAMPLING ................................................................................ 15

4.0 ANALYTICAL DATA SUMMARY ............................................................................................ 16

4.1 CONTAINER SAMPLE RESULTS ................................................................................. 16

4.2 DIRECT-PUSH TECHNOLOGY SAMPLE RESULTS .................................................. 16

4.2.1 Borings within the Suspected TCE Source Area .................................................. 17

4.2.2 Borings within the Suspected Petroleum Source Area ......................................... 17

4.2.3 Boring within Suspected Source Area East of Main Re-Con Building ................ 17

4.2.4 Boring within Suspected Source Area Northwest of Main Re-Con Building ...... 17

4.2.5 Boring within Suspected Source Area along West Property Boundary ................ 18

4.3 SURFACE SOIL SAMPLE RESULTS ............................................................................ 18

4.4 QUALITY CONTROL SAMPLE RESULTS ................................................................... 18

5.0 SUMMARY ................................................................................................................................... 20

5.1 REMOVAL CONSIDERATIONS .................................................................................... 20

5.2 PRE-REMEDIAL CONSIDERATIONS .......................................................................... 20

6.0 REFERENCES .............................................................................................................................. 22

X9025.15.0086.000 ii

CONTENTS (Continued)

APPENDICES

Appendix

A FIGURES

B LOG BOOK

C PHOTOGRAPHIC DOCUMENTATION

D CONTAINER SUMMARY TABLE

E BORING LOGS

F CHAIN-OF-CUSTODY FORMS, FIELD SHEETS, AND ANALYTICAL DATA

G ANALYTICAL DATA TABLES

TABLES

Table Page

1 SUMMARY OF DPT SOIL SAMPLES ........................................................................................ 11

2 SUMMARY OF SURFACE SOIL SAMPLES ............................................................................. 13

3 SUMMARY OF RADIOLOGICAL BACKGROUND SURVEY ................................................ 14

4 SUMMARY OF SURFACE SOIL FIELD DUPLICATE DATA

COMPARISON ............................................................................................................................. 19

X9025.15.0086.000 1

1.0 INTRODUCTION

The Tetra Tech, Inc. (Tetra Tech) Superfund Technical Assessment and Response Team (START) was

tasked by the U.S. Environmental Protection Agency (EPA) Region 7 Superfund Division to conduct a

removal assessment at the Osage and Walnut site in Pittsburg, Kansas. The Osage and Walnut site was

identified during quarterly groundwater monitoring of the Miller Brothers Oil Company property (later

referred to as the Osage and Walnut site) supported by the Kansas Petroleum Storage Tank Release Trust

Fund in 2000. During groundwater sample analysis, trichloroethene (TCE) was discovered to be

interfering with analytical detection limits. Subsequent investigations concluded that a release of TCE and

other chlorinated solvents had occurred upgradient of the Miller Brothers Oil Company property, likely

originating from the Coffeyville Re-Con, Inc. facility (Kansas Department of Health and Environment

[KDHE] 2007a). Subsequent investigations identified soil and groundwater contamination on and

downgradient of the Coffeyville Re-Con property (Coffeyville Re-Con site). In addition, numerous

containers of unknown contents were documented on the Coffeyville Re-Con site.

The primary purpose of the removal assessment was to investigate previously documented containers

staged at the Coffeyville Re-Con site to determine hazardous characteristics of their contents. In addition,

the removal assessment was to further investigate two potential source areas of contamination at the

Coffeyville Re-Con site. Removal assessment tasks included, but were not limited to:

Inventorying containers (drums, totes, and other containers) staged at the Coffeyville Re-Con site

to document any label information, estimate quantity of contents, and container condition

Collecting samples from inventoried containers for field screening purposes to document

hazardous characteristics

Collecting subsurface soil samples within suspected source areas by use of a Geoprobe® direct-

push technology (DPT) rig equipped with a Macro-Core sampler

Collecting composite surface soil (0 to 6 inches below ground surface [bgs]) samples at various

locations of suspected contamination at the Osage and Walnut site

Conducting an initial radiation assessment of remaining oil well equipment and surrounding soils

to determine if past operations at the Osage and Walnut site had radiologically impacted site

surfaces.

X9025.15.0086.000 2

The removal assessment proceeded under authority of the Comprehensive Environmental Response,

Compensation, and Liability Act of 1980 (CERCLA) and the Superfund Amendments and Reauthorization

Act of 1986 (SARA).

Danny O’Connor was the START Project Manager for the removal assessment. The EPA On-Scene

Coordinator (OSC) for the project was Todd Campbell.

X9025.15.0086.000 3

2.0 BACKGROUND INFORMATION

Multiple site investigations have determined that the Coffeyville Re-Con facility is the source of

chlorinated solvent contamination first observed in groundwater at the Osage and Walnut site. The

following sections summarize previous activities at both the Osage and Walnut site and Coffeyville

Re-Con site. Removal assessment activities described in this report focused on the Coffeyville Re-Con

site. This section presents information regarding locations and descriptions, operational histories, and

relevant investigation histories of the two sites.

2.1 THE OSAGE AND WALNUT SITE

The Osage and Walnut site is at the intersection of Osage Street and Walnut Street in Coffeyville, Kansas.

Geographic coordinates of the Osage and Walnut site are 37.013167 degrees north and 95.616110 degrees

west. Residential homes border the Osage and Walnut site north and west, and commercial businesses

border the Osage and Walnut site east and south, with the Coffeyville wastewater treatment plant beyond.

The Osage and Walnut site previously hosted Miller Brothers Oil Company, with presence of several on-

site underground storage tanks (UST) and aboveground storage tanks (AST). USTs were discovered

leaking in 1999. As of 2007, on-site structures included an old building, USTs, concrete pads, and a fuel

pump island. Eight monitoring wells were installed at the Osage and Walnut site (five on site and three on

adjacent properties) during site investigative work supported by the Kansas Petroleum Storage Tank

Release Trust Fund.

2.2 THE COFFEYVILLE RE-CON SITE

The Coffeyville Re-Con site is at 2410 Brown Avenue in Coffeyville, Kansas (see Appendix A, Figure 1).

Geographic coordinates of the site are 37.016317 degrees north and 95.618357 degrees west. The

Coffeyville Re-Con site is bounded north and south by open fields, east by residential properties, and west

by an active rail line. Three buildings are on site: the north former Coffeyville Re-Con building, the

central PrimeTime Industrial Painting, LLC (PrimeTime) building, and an eastern office building (KDHE

2013). The Coffeyville Re-Con site is approximately 0.25 mile northwest of the Osage and Walnut site.

The Kansas Oil Refining Company operated at the Coffeyville Re-Con site from the early 1900s until the

1930s. During 1943, ordnance material and rocket motors were manufactured on site by Multiscope

Company, Inc. In addition, the Coffeyville Re-Con site was used as a scrap yard, trucking facility, and for

other manufacturing and storage purposes. Drum refurbishing activities began in the 1950s, and the

Coffeyville Re-Con building was constructed in 1958. Coffeyville Re-Con began drum refurbishing

X9025.15.0086.000 4

operations at the Coffeyville Re-Con site during 1977. Operations ceased in December 2007 with closure

of the facility. PrimeTime operated at the Coffeyville Re-Con site from 2005 to 2007 (KDHE 2013).

2.3 PREVIOUS INVESTIGATIONS

This section summarizes relevant investigations at the Osage and Walnut site and the Coffeyville Re-Con

site.

2.3.1 UST Trust Fund Activities

In March 1999, USTs at the Miller Brothers Oil Company property (Osage and Walnut site) were

discovered leaking. In October 2000, JB Environmental Drilling was contracted to conduct a Limited Site

Assessment (LSA) supported by the Kansas Petroleum Storage Tank Release Trust Fund. The LSA report

recommended regular groundwater monitoring for benzene, toluene, ethylbenzene, and xylenes (BTEX);

1,2-dichloroethane (DCA); naphthalene; methyl tertiary butyl ether (MTBE); and tertiary butyl alcohol

(TBA) (KDHE 2007a). Eight monitoring wells were installed within the general site vicinity to monitor

groundwater contaminants. During groundwater sampling, TCE was discovered interfering with analytical

detections; therefore, subsequent groundwater sampling included TCE and cis-1,2-dichloroethene (DCE)

as analytes. Groundwater sample analytical data indicated TCE and cis-1,2-DCE at concentrations

exceeding their respective EPA Maximum Contaminant Levels (MCL) in multiple monitoring wells.

2.3.2 Site Reconnaissance and Evaluation

During January and April 2007, KDHE conducted a Pre-Comprehensive Environmental Response,

Compensation and Liability Information System (Pre-CERCLIS) Site Reconnaissance and Evaluation

(SRE) at the Osage and Walnut site to determine if a release of TCE had occurred. The SRE was

conducted in two phases—January and April 2007.

During the January sampling event, KDHE collected groundwater samples from eight site monitoring

wells at the Osage and Walnut site. Analytical data indicated that concentrations of TCE; cis-1,2-DCE;

1,1,2-trichloroethane; and 1,2-DCA exceeded their respective EPA MCLs in groundwater samples

collected from multiple site monitoring wells. TCE, the primary contaminant of concern, was detected in

three site monitoring wells at concentrations ranging from 13.1 to 2,400 micrograms per liter (µg/L).

KDHE returned to the site in April 2007 to continue groundwater assessment by focusing on areas

surrounding the Coffeyville Re-Con property, the suspected source. Groundwater samples were collected

X9025.15.0086.000 5

from six Geoprobe® DPT temporary monitoring wells—five installed downgradient and one upgradient of

the Coffeyville Re-Con property. Groundwater samples were collected for analysis via the KDHE Mobile

Laboratory Shimadzu Gas Chromatograph (Mobile Laboratory) and by the Kansas Division of Health and

Environmental Laboratories (DHEL). Mobile laboratory data indicated TCE in three of five samples

collected from downgradient wells at concentrations exceeding the MCL. No detectable TCE was reported

in the sample collected from the upgradient well. DHEL reported similar results, confirming elevated TCE

concentrations downgradient of the Coffeyville Re-Con site.

The SRE identified elevated TCE and cis-1,2-DCE concentrations in groundwater downgradient of the

Coffeyville Re-Con facility. No detectable VOCs were reported in groundwater samples collected

upgradient of the Coffeyville Re-Con facility. KDHE concluded that a release of TCE and other

chlorinated solvents to groundwater had occurred upgradient of the Osage and Walnut site, likely

originating from the Coffeyville Re-Con facility (KDHE 2007a).

2.3.3 KDHE RCRA Inspection

On August 7 and 8, 2007, the KDHE Bureau of Environmental Field Services conducted a Resource

Conservation and Recovery Act (RCRA) Compliance Evaluation Inspection of the Coffeyville Re-Con

facility. The purpose of the inspection was to identify types of wastes generated, points of waste

generation, methods of waste management, and review of relevant documents. The inspection documented

14 violations, and a Notice of Non-Compliance was issued to Coffeyville Re-Con (KDHE 2007b).

2.3.4 Consent Order

In 2008, KDHE and Coffeyville Re-Con entered into a Consent Order (CO) (Case No. 08-E-020). The

CO documented Coffeyville Re-Con’s agreement to prepare and implement a Comprehensive

Investigation/Corrective Action Study (CI/CAS) at its facility. The CO also outlined a work schedule and

required documents.

On October 9, 2008, WSP Environment & Energy (WSP) submitted a CI/CAS work plan on behalf of

Coffeyville Re-Con. The stated purpose of the CI/CAS was to evaluate possible source areas of

KDHE-identified contaminants of concern (COC) at the facility, and potential migration onto the property

from upgradient sources (WSP 2008).

WSP conducted sampling activities at the Coffeyville Re-Con site during January and February 2009.

TCE, cis-1,2-DCE, trans-1,2-DCE, vinyl chloride, total petroleum hydrocarbons (TPH)-gasoline range

X9025.15.0086.000 6

organics (GRO), TPH-diesel range organics (DRO), arsenic, cadmium, chromium, and lead were detected

during the investigation. WSP concluded that the source of contamination was on the Coffeyville Re-Con

site, but likely associated with historical operations prior to Coffeyville Re-Con’s presence on the site

(WSP 2008).

KDHE disagreed with the conclusion and asked Coffeyville Re-Con to conduct further investigation.

Coffeyville Re-Con refused additional assessment and instead reached a settlement with KDHE in

March 2012 (KDHE 2013).

2.3.5 Comprehensive Investigation

Following termination of the CO and subsequent settlement with Coffeyville Re-Con, KDHE conducted a

Comprehensive Investigation (CI) in 2012 at the Coffeyville Re-Con site. CI sampling activities occurred

between October 30 and December 20, 2012. Soil and groundwater samples were collected at and

downgradient of the site to better characterize contaminant distribution.

Analytical data from the 2012 CI indicated presence of TCE and its degradation products at concentrations

exceeding their respective EPA MCLs in groundwater immediately east-southeast of the Coffeyville

Re-Con building. Analytical results indicated migration of chlorinated VOC-contaminated groundwater

through a residential neighborhood downgradient of Coffeyville Re-Con. In addition, TPH results

indicated migration of petroleum-impacted groundwater off site. Elevated lead and arsenic concentrations

in soil were identified near the Coffeyville Re-Con paint booth. KDHE concluded that the Coffeyville Re-

Con facility was the source of VOC, metal, and TPH contamination (KDHE 2013).

2.3.6 Comprehensive Investigation Addendum

Several data gaps were identified in the 2012 CI; therefore, KDHE conducted a Comprehensive

Investigation Addendum (2013 CI) to address data gaps through further sampling at the site. The purposes

of the 2013 CI were to (1) identify and characterize on-site source areas, (2) install groundwater

monitoring wells, and (3) gain additional data to assist in evaluating remedial alternatives (KDHE 2014a).

CI sampling activities from February 28 to November 7, 2013, included collection of soil, groundwater,

and air samples on and downgradient of the Coffeyville Re-Con site. In addition, three groundwater

monitoring wells were installed to monitor contaminant concentrations and plume migration.

Results of the 2013 CI enabled KDHE to conclusively identify the Coffeyville Re-Con site as the source of

VOC contamination. Approximately 5,000 cubic yards of impacted soil was identified near the east

X9025.15.0086.000 7

central portion of the Coffeyville Re-Con site. TCE soil contamination corresponded to nearby elevated

TCE concentrations in groundwater, indicating a TCE source. KDHE recommended long-term

groundwater monitoring to continue assessment of contaminant distribution and degradation.

2.3.7 Integrated Assessment

During September 2014, KDHE conducted an Integrated Assessment (IA) of the Coffeyville Re-Con site

to assess potential releases of hazardous substances. The IA included review of historical information, a

summary of previous analytical data, an evaluation of the site according to Hazard Ranking System (HRS)

guidance, and a compilation of a comprehensive target survey.

KDHE recommended a removal action to remove drums and contaminated soil that had released or may

pose a threat of release of hazardous substances, pollutants, and contaminants to soil, air, surface water,

and adjacent residences. Following completion of a removal action, KDHE recommended completion of a

Site Inspection to fully evaluate potential pathways (KDHE 2014b).

X9025.15.0086.000 8

3.0 REMOVAL ASSESSMENT ACTIVITIES

START Members (SM) Joann Jeplawy, Adam Watkins, Cosmo Canacari, and Tommy Rebecchi

conducted removal assessment field activities January 25 to 27, 2016. Activities included (1) a

determination of hazardous characteristics of contents of on-site containers (drums, totes, and other

containers), (2) an assessment of subsurface soil to determine presence of contaminant source areas, (3) an

assessment of metal concentrations in surface soil and surface wastes at the site, (4) and a radiological

survey of former oil-well equipment and surrounding soils. Removal assessment activities accorded with

the approved Quality Assurance Project Plan (QAPP) dated January 20, 2016. Field activities were

documented in a logbook (see Appendix B). Site conditions were documented in a photographic log

included as Appendix C. A site layout map is provided as Figure 2 in Appendix A. The following

sections detail field activities.

3.1 CONTAINER INVENTORYING, SAMPLING, AND FIELD SCREENING

On January 12, 2016, EPA and Tetra Tech START conducted an initial site reconnaissance to determine

locations and quantities of containers (drums, totes, and other containers) at the Re-Con site. Containers

were documented at the following locations: the main Re-Con building, near the west property boundary,

north of the main Re-Con building, and near the PrimeTime building and office.

Crews returned on January 25, 2016, to complete a container inventory and collect field screening samples.

During the inventory, each container received a unique identification number, and the container location

was documented (see Appendix A, Figure 3). The following container information was documented

during container inventorying: size, composition, color, estimated volume of contents, and any label

information (see Appendix D). A total of 150 containers were inventoried during the removal assessment.

After completion of inventorying, START personnel opened each container and documented measurable

volatile organics in container headspace by use of a hand-held photoionization detector (PID). Field

personnel then attempted to collect a representative sample (field screening sample) from containers using

disposable thieving rods (liquids/sludges), disposable coliwasas (liquids/sludges), or hand trowels (solids).

Thieving rods and coliwasas were disposed of after sampling each container to avoid cross-contamination.

Hand trowels were decontaminated after investigation of each container via brush and washing with non-

phosphate detergent solution, followed by a rinsing with deionized water. Field screening samples were

collected directly into 40-milliliter (mL) vials (liquids) or 8-ounce glass jars (solids and sludges). When

multiple containers with similar contents were encountered, a subset of the similar containers was sampled

to represent the entire group’s contents. The majority of similar containers observed during the removal

X9025.15.0086.000 9

assessment were filled with “overspray material,” an assumed byproduct of drum refurbishing practices. A

total of 86 field screening samples were collected from the 150 inventoried containers.

Field screening samples were tested following HazCat® Chemical Identification System procedures to

determine if container contents were explosive, water reactive, water soluble, corrosive, an oxidizer, a

sulfide, flammable, a halide, or a cyanide. Results from testing field screening samples were as follows:

24 samples identified as flammable, 18 samples identified as combustible, and 1 sample identified as

corrosive. The remaining 43 samples did not exhibit any hazardous characteristics. Results are

summarized in Appendix D.

Because a significant number of identified containers were filled with “overspray material,” a composite

sample was collected from remnants of field screening samples and submitted to the EPA Region 7

laboratory under Analytical Service Request (ASR) #7077 for analyses for total Resource Conservation

and Recovery Act (RCRA) metals via Standard Operating Procedure (SOP) 3122.03, and for toxicity

characteristic leaching procedure (TCLP) RCRA metals via SOP 3171.01. The samples were delivered on

February 17, 2016. Section 4.1 discusses results of these analyses.

3.2 DIRECT-PUSH TECHNOLOGY SOIL SAMPLING

To further evaluate multiple potential contaminant source areas at the Coffeyville Re-Con site, subsurface

soil samples were collected by use of a Geoprobe® DPT rig. Subsurface soil sampling focused on two

primary potential source areas—a suspected TCE source area north of the site office building and a

suspected petroleum source area near the formerly operating oil well. Additional borings were advanced in

areas of surface staining near the main Re-Con building (see Appendix A, Figure 4).

At the first boring location (GP-1), a continuous boring was advanced to 24 feet bgs to characterize soils

all the way into the saturated zone. All remaining borings were advanced to 8 feet bgs, approximately the

top of the water table. Continuous borings were advanced by use of a Geoprobe® DPT rig equipped with a

Macro-Core sampler. Upon retrieving borings, Tetra Tech screened soils for measurable VOCs by use of a

hand-held PID. Tetra Tech documented PID readings, any observed staining, and soil lithology in boring

logs (see Appendix E). The two 1-foot boring intervals with the highest observed PID readings or most

noticeable visual anomalies were selected for sampling. If no visual anomalies or elevated PID readings

were observed, field team members sampled at default depths: one sample collected within the 7- to 8-foot

bgs interval, and an additional sample collected within the uppermost 4 feet of the boring.

X9025.15.0086.000 10

Within each sampling interval, soil samples for analysis for VOCs were collected first according to EPA

Method 5035 guidelines. The remaining soil (see Table 1 for list of analyses) was then transferred to

appropriate sample containers. Pertinent information, including analysis to be performed and exact sample

locations, was recorded on field sheets for each sample (see Appendix F). All soil samples were stored in

coolers maintained at or below 4 degrees Celsius (C) pending submittal to the EPA Region 7 laboratory in

Kansas City, Kansas under ASR #7041. DPT soil sample analysis varied depending on the location of the

boring. Table 1 summarizes DPT soil samples and corresponding laboratory analyses.

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TABLE 1

SUMMARY OF DPT SOIL SAMPLES

OSAGE AND WALNUT SITE, COFFEYVILLE, KANSAS

Sample Name Sample

Description

Latitude

(°N)

Longitude

(°W)

Collection

Date

Collection

Time

Laboratory

Sample ID

Laboratory Analysis

VOCs via

SOP 3230.16

Cyanide via

SOP 3135.02

TPH-GRO via

SOP 3230.19

TPH-DRO/ORO

via SOP 3270.01

GP-1 (1-2)

Within

suspected

TCE source

area

37.01626 95.61806 1/25/2016 1505 7041-101 X X

GP-1 (3-4) 1/25/2016 1505 7041-102 X X

GP-2 (1-2) 37.01625 95.61800

1/25/2016 1615 7041-103 X X

GP-2 (7-8) 1/25/2016 1625 7041-104 X X

GP-3 (1-2) 37.01623 95.61790

1/26/2016 0815 7041-105 X X

GP-3 (7-8) 1/26/2016 0820 7041-106 X X

GP-4 (1-2) 37.01614 95.61806

1/26/2016 0851 7041-107 X X

GP-4 (7-8) 1/26/2016 0900 7041-108 X X

GP-5 (1-2)

37.01613 95.61798

1/26/2016 0937 7041-109 X X

GP-5 (7-8) 1/26/2016 0950 7041-110 X X

GP-5 (7-8) FD 1/26/2016 0950 7041-110 FD X X

GP-6 (2-3) 37.01616 95.61788

1/26/2016 1028 7041-111 X X

GP-6 (7-8) 1/26/2016 1037 7041-112 X X

GP-7 (3-4) 37.01607 95.61806

1/26/2016 1102 7041-113 X X

GP-7 (7-8) 1/26/2016 1110 7041-114 X X

GP-8 (3-4) 37.01606 95.61794

1/26/2016 1130 7041-115 X X

GP-8 (7-8) 1/26/2016 1138 7041-116 X X

GP-9 (3-4) 37.01607 95.61784

1/26/2016 1159 7041-117 X X

GP-9 (7-8) 1/26/2016 1207 7041-118 X X

GP-10 (3-4) Within

suspected

TPH source

area

37.01468 95.61868 1/26/2016 1340 7041-119 X X

GP-10 (3-4) 1/26/2016 1340 7041-201 X X

GP-11 (3-4) 37.01469 95.61848

1/26/2016 1420 7041-120 X X

GP-11 (3-4) 1/26/2016 1420 7041-202 X X

GP-12 (3-4) East of

main

Re-Con

building

37.01707 95.61816

1/26/2016 1454 7041-121 X X

GP-12 (3-4) 1/26/2016 1454 7041-203 X X

GP-12 (7-8) 1/26/2016 1458 7041-122 X X

TABLE 1 (Continued)

SUMMARY OF DPT SOIL SAMPLES


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Sample Name Sample

Description

Latitude

(°N)

Longitude

(°W)

Collection

Date

Collection

Time

Laboratory

Sample ID

Laboratory Analysis

VOCs via

SOP 3230.16

Cyanide via

SOP 3135.02

TPH-GRO via

SOP 3230.19

TPH-DRO/ORO

via SOP 3270.01

GP-13 (2-3) Northwest

of main

Re-Con

building

37.01715 95.61892

1/26/2016 1540 7041-123 X X

GP-13 (7-8) 1/26/2016 1547 7041-124 X X

GP-14 (3-4) Along west

property

boundary

37.01758 95.61891 1/26/2016 1600 7041-125 X X

GP-14 (7-8) 1/26/2016 1605 7041-126 X X

Notes:

°N Degrees North

°W Degrees West

DRO/ORO Diesel-range organics/oil-range organics

FD Field duplicate

GRO Gasoline-range organics

ID Identification

SOP Standard Operating Procedure

TCE Trichloroethene

TPH Total petroleum hydrocarbons

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3.3 SURFACE SOIL SAMPLING

Composite surface soil samples were collected at various locations at the Re-Con site to determine impact

from historical site operations. Sampling locations are depicted on Figure 4 (see Appendix A) and

summarized in Table 2. Composite sampling proceeded first by defining a sampling area, known as a

decision unit (DU). Then within each DU, nine aliquots of approximate equal volume were collected by

use of a hand trowel. Field team members identified locations within each DU for collection of aliquots

according to a simple random sampling pattern. The composite samples were collected into labeled 8-

ounce glass jars for analysis of RCRA metals. The hand trowel was decontaminated after sampling within

each DU. Pertinent information, including analyses to be performed and sample locations, were recorded

on field sheets for each sample (see Appendix F). All soil samples were stored in coolers maintained at or

below 4 C pending submittal to the EPA Region 7 laboratory in Kansas City, Kansas, under ASR #7041

for analysis for RCRA metals via SOP 3122.03.

TABLE 2

SUMMARY OF SURFACE SOIL SAMPLES


Sample

Name Sample Description

Sample Location* Laboratory

Sample ID Latitude °N Longitude °W

DU-1 Soil staining east of main Re-Con building 37.016884 95.618081 7041-1

DU-2 North exterior of main Re-Con building, near

paint booth 37.017336 95.618499

7041-2

7041-2FD

DU-3 West of main Re-Con building 37.017049 95.018820 7041-3

DU-4 Waste material covering floor of main Re-Con

building 37.017006 95.618749 7041-4

DU-5 West of PrimeTime shop 37.016048 95.618863 7041-5

DU-6 South of PrimeTime shop 37.015749 95.618417 7041-6

DU-7 Near oil well 37.014789 95.618481 7041-7

Notes:

* Represents a central point within each decision unit

°N Degrees North

°W Degrees West

FD Field Duplicate

ID Identification

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3.4 RADIOLOGICAL SURVEY

On January 26, 2016, Tetra Tech START conducted an initial radiation assessment at the Coffeyville Re-

Con site to determine if past site operations had radiologically impacted site surfaces. The initial

assessment included a survey of remaining oil-well equipment and surrounding soils by use of a Ludlum

Model 2221 ratemeter with a Ludlum Model 44-20 sodium iodide (NaI) scintillation detector (detector).

To ensure proper functioning of the ratemeter and detector, a source check occurred prior to the survey by

use of a cesium-137 check source. The source check confirmed that the instruments were functioning

properly. To establish background radiation levels in the site area for comparative purposes, SMs selected

three areas (background location) with no suspected previous radiological impact. At each background

location, the ratemeter was set to scaler mode, and a 1-minute count time was initiated. The resulting

reading was in units of counts per minute (cpm). Background survey results are summarized in Table 3.

TABLE 3

SUMMARY OF RADIOLOGICAL BACKGROUND SURVEY


Location Description Latitude

(°N)

Longitude

(°W)

Reading

(cpm)

Grace Park 37.01969 95.61742 26,000

Alley east of the site 37.01720 95.61759 24,000

Near Osage Street 37.01309 95.61871 24,000

Notes:

°N Degrees North

°W Degrees West

cpm Counts per minute

The survey at the Coffeyville Re-Con site focused on remaining oil-well equipment and surrounding soils.

During the initial soil survey, the surveyor walked in a forward direction at 1 to 2 feet per second while

swinging the detector back and forth approximately 6 inches above the ground—generally covering a

serpentine pattern over the ground surface. Surfaces of remaining oil-well equipment were scanned by

moving the detector in a serpentine pattern 1 to 2 inches above each surface. Survey readings from soil

and oil-well equipment ranged from 18,000 to 31,000 cpm, comparable to readings at the three

background locations. No abnormal readings, such as concentrated areas of elevated readings, were

documented during the radiological survey.

X9025.15.0086.000 15

3.5 QUALITY CONTROL SAMPLING

Quality control (QC) samples for the removal assessment included two field duplicates—one collected

during DPT soil sampling and the other collected during surface soil sampling. Field duplicates were

collected to assess precision of analytical and sampling methods.

X9025.15.0086.000 16

4.0 ANALYTICAL DATA SUMMARY

This section summarizes analytical data from the removal assessment in January 2016. Soil samples were

delivered in two batches to the EPA Region 7—the first on January 27 (ASR #7041) and the second on

February 17, 2016 (ASR #7077). Sample field sheets, chain-of-custody records, and laboratory data are in

Appendix F. Analytical data are summarized in tabular form in Appendix G.

4.1 CONTAINER SAMPLE RESULTS

One composite sample from containers of “overspray material” was submitted to the EPA Region 7

laboratory under ASR #7077 for analyses for total RCRA metals via SOP 3122.03 and TCLP RCRA

metals via SOP 3171.01. Analytical data from RCRA metals analysis were compared to EPA Regional

Screening Levels (RSL) for industrial soil and to KDHE Tier 2 risk-based soil pathway benchmarks for

non-residential scenarios. Analytical data from TCLP analysis were compared to regulatory levels

specified in 40 Code of Federal Regulations Section 261.24. Review of analytical data indicated the

following:

The RCRA metals mercury, barium, cadmium, chromium, lead, selenium, and silver were detected

in the sample. No analyte concentration exceeded a comparative benchmark. Arsenic was not

detected in the sample; however, the reported detection limit of 5.10 milligrams per kilogram

(mg/kg) exceeded the EPA RSL for industrial soil of 3.00 mg/kg.

TCLP results indicated detections of the metals barium and selenium. Reported concentrations of

these analytes did not exceed their regulatory limits. TCLP results indicated that the overspray

material did not exhibit characteristics of toxicity specified in 40 CFR Section 261.24.

Analytical data from the overspray material are summarized in Appendix G, Table G-1.

4.2 DIRECT-PUSH TECHNOLOGY SAMPLE RESULTS

A total of 30 subsurface soil samples (including one field duplicate) were collected from 14 DPT borings

within five areas of suspected contamination during the removal assessment (see Appendix A, Figure 4).

Subsurface soil analytical data were compared to EPA RSLs for industrial soil and to KDHE Tier 2 risk-

based soil pathway benchmarks for non-residential scenarios. Subsurface soil sample analytical data are

summarized in Appendix G, Table G-2. The following subsections summarize analytical data from each

of the five suspected source areas.

X9025.15.0086.000 17

4.2.1 Borings within the Suspected TCE Source Area

Nineteen soil samples (including one field duplicate) were collected from nine borings (samples GP-1

through GP-9) advanced near the suspected TCE source at the Coffeyville Re-Con site. Samples were

analyzed for VOCs via SOP 3230.16 and cyanide via SOP 3135.02. Analytical data indicated presence in

one or more samples at concentrations above the reporting limit of the VOCs 1,1-DCA, acetone, benzene,

cis-1,2-DCE, cyclohexane, ethylbenzene, isopropylbenzene, xylene (m- and/or p-), MTBE,

methylcyclohexane, o-xylene, toluene, and vinyl chloride. No reported analyte concentration exceeded a

comparative benchmark. TCE and cyanide were not detected in any of the samples.

4.2.2 Borings within the Suspected Petroleum Source Area

Four soil samples were collected from two borings (GP-10 and GP-11) advanced near the suspected

petroleum source at the Coffeyville Re-Con site. Sample analyses included VOCs via SOP 3230.16,

cyanide via SOP 3135.02, TPH-GRO via SOP 3230.19, and TPH-DRO/ORO via SOP 3270.01. No

analytes were detected in the four samples.

4.2.3 Boring within Suspected Source Area East of Main Re-Con Building

Three soil samples were collected from one boring (GP-12) advanced within an area of soil staining east of

the main Re-Con building. Sample analyses included VOCs via SOP 3230.16, cyanide via SOP 3135.02,

TPH-GRO via SOP 3230.19, and TPH-DRO/ORO via SOP 3270.01. Analytical data indicated presence

above detection limits of the VOCs 1,1-DCA, acetone, chloroethane, and cis-1,2-DCE. TPH-DRO and

TPH-ORO also were reported above detection limits. No reported analyte concentration exceeded a

benchmark value. Cyanide was not detected in any of the samples.

4.2.4 Boring within Suspected Source Area Northwest of Main Re-Con Building

Two soil samples were collected from one boring (GP-13) advanced within an area of soil staining

northwest of the main Re-Con building. Soil samples were analyzed for VOCs via SOP 3230.16 and

cyanide via SOP 3135.02. Analytical data indicated presence of the VOC acetone above detection limits

but below comparative benchmarks.

X9025.15.0086.000 18

4.2.5 Boring within Suspected Source Area along West Property Boundary

Two soil samples were collected from one boring (GP-14) advanced within an area of soil staining near the

west property boundary. Soil samples were analyzed for VOCs via SOP 3230.16 and cyanide via SOP

3135.02. No analytes were detected in the two samples.

4.3 SURFACE SOIL SAMPLE RESULTS

A total of eight surface soil samples (including one field duplicate) were collected at various areas across

the Re-Con site. Surface soil samples were analyzed for total RCRA metals via SOP 3122.3. Surface soil

analytical data were compared to EPA RSLs for industrial soil and KDHE Tier 2 risk-based soil pathway

benchmarks for non-residential scenarios. In addition, detections were compared to U.S. Geological

Survey (USGS)-reported background concentrations in Montgomery County (USGS 2016). Surface soil

sample data are summarized in Appendix G, Table G-3.

Review of analytical data indicated detections of the metals mercury, arsenic, barium, cadmium,

chromium, and lead in one or more surface soil samples. Detected concentrations of mercury, barium,

cadmium, and lead did not exceed comparative benchmarks. Arsenic and chromium exceeded

comparative benchmarks as described below:

Arsenic was detected in all eight samples at concentrations ranging from 1.5 to 256 mg/kg,

exceeding the EPA RSL for industrial soil (3.0 mg/kg) in four samples and the KDHE Tier 2

benchmark (63.2 mg/kg) in one sample. Seven of the eight reported arsenic detections were

similar to the USGS reported average background concentration in Montgomery County of

7.94 mg/kg. The composite sample collected at DU-4, waste covering the floor of the main Re-

Con building, contained arsenic at 256 mg/kg, exceeding the EPA RSL for industrial soil and the

KDHE Tier 2 benchmark for non-residential scenarios.

Total chromium was detected in all eight samples at concentrations ranging from 7.1 to 197

mg/kg. The composite sample collected at DU-4, waste covering the floor of the main Re-Con

building, contained total chromium at 197 mg/kg, exceeding the KDHE Tier 2 benchmark for

non-residential scenarios. Further examination of KDHE’s Tier 2 Risk-Based Standards for

Kansas (RSK) values for chromium revealed that Tier 2 RSK values listed in the KDHE RSK

Manual for total chromium are based on toxicity data relevant to hexavalent chromium (the more

toxic form of chromium) (KDHE 2010). Further analysis of this DU may be warranted to assess

presence and quantity of hexavalent chromium.

4.4 QUALITY CONTROL SAMPLE RESULTS

QC sampling for this removal assessment included collection of two field duplicates. One field duplicate

was collected within the 7- to 8-foot bgs interval at DPT boring GP-5. The sample was analyzed for VOCs

X9025.15.0086.000 19

and cyanide. Analytical data indicated no analyte detections in either the field duplicate sample or the

original sample. The second field duplicate was collected at DU-2 and analyzed for RCRA metals. The

metals arsenic, barium, cadmium, chromium, and lead were detected in both the field duplicate sample and

the original sample. Table 4 summarizes surface soil field duplicate data.

TABLE 4

SUMMARY OF SURFACE SOIL FIELD DUPLICATE DATA COMPARISON

OSAGE AND WALNUT, COFFEYVILLE, KANSAS

Sample

Name

Laboratory

Sample ID

Analyte and Result

Arsenic Barium Cadmium Chromium Lead

DU-2 7041-2 1.50 30.3 0.690 14.2 141

7041-2FD 2.60 63.0 0.95 12.0 77.1

Average 2.05 46.7 0.82 13.1 109

RPD 53.7% 70.1% 31.7% 16.8% 58.6%

Notes:

All results reported as milligrams per kilogram

% Percent

DU Decision unit

FD Field duplicate

ID Identification

RPD Relative percent difference

Large variations reported in sample results for arsenic, barium, and lead likely indicate high heterogeneity

in DU-2. Reported concentrations do not exceed applicable benchmarks; therefore, reported contaminant

concentration variance does not impact project decision making.

X9025.15.0086.000 20

5.0 SUMMARY

Tetra Tech START was tasked by EPA Region 7 to conduct a removal assessment at the Osage and

Walnut site in Coffeyville, Kansas. The site previously hosted Miller Brothers Oil Company, with

presence of several on-site USTs and ASTs. Site groundwater was found contaminated with TCE during

tank closure sampling activities. Subsequent investigations determined the source of groundwater

contamination was the Coffeyville Re-Con site located northwest of the Osage and Walnut site.

Investigations documented presence of containers of unknown contents and several areas of suspected soil

contamination.

The primary purposes of this removal assessment were to (1) investigate containers staged at the site to

determine hazardous characteristics of their contents, (2) further investigate potential contaminant source

areas, and (3) investigate oil well equipment and surrounding soils to determine if they had been

radiologically impacted from historical site operations. Removal assessment activities focused on the

Coffeyville Re-Con site. The following sections discuss removal and pre-remedial considerations.

5.1 REMOVAL CONSIDERATIONS

Based on information obtained during the removal assessment, a removal action may be warranted to

address (1) containers identified as holding hazardous contents, and (2) waste covering the main Re-Con

building floor found to contain elevated concentrations of arsenic and total chromium.

Of the 150 containers inventoried during the removal assessment, 24 were identified as having flammable

contents, 18 were identified as having combustible contents, and 1 was identified as having corrosive

contents. Analytical data from DU-4, representing waste covering the floor of the main Re-Con building,

indicated presence of arsenic at 256 mg/kg and chromium at 197 mg/kg. These concentrations exceeded

comparative benchmarks.

5.2 PRE-REMEDIAL CONSIDERATIONS

Previous investigations by KDHE had identified groundwater contamination in the form of chlorinated

solvents at the site. The plume begins near the PrimeTime office building and continues southeast

(downgradient) through a residential neighborhood. The distal end of the plume is southeast of the Osage

and Walnut site near agricultural land. Previous vapor intrusion investigations in the residential

neighborhood had found no impact on indoor air quality. Drinking water for the area surrounding the

Osage and Walnut site is provided by the City of Coffeyville. Coffeyville obtains drinking water from the

X9025.15.0086.000 21

Verdigris River near Pfister Park, more than 3 miles upstream from the Osage and Walnut site. Based on

this information, no further pre-remedial considerations appear warranted at this time.

X9025.15.0086.000 22

6.0 REFERENCES

Kansas Department of Health and Environment (KDHE).

2007a. Site Reconnaissance and Evaluation. Osage and Walnut Site. May.

2007b. RCRA Compliance Evaluation Inspection Summary. August.

2010. Risk-Based Standards for Kansas, RSK Manual – 5th Version. October.

2013. Comprehensive Investigation. Coffeyville Re-Con Site. February 25.

2014a. Comprehensive Investigation Addendum. Coffeyville Re-Con Site. March 3.

2014b. Integrated Assessment. Coffeyville Re-Con Site. September 16.

WSP Environment & Energy (WSP). 2008. Comprehensive Investigation/Corrective Action Study

(CI/CAS) Work Plan. Coffeyville Re-Con, Inc. October 9.

U.S. Geological Survey (USGS). 2016. Average Concentrations of Elements in Montgomery County,

Kansas.

APPENDIX A

FIGURES

_̂

Source: USGS Coffeyville East, KS 7.5 Minute Topo Quads, 2016 USGS Coffeyville West, KS 7.5 Minute Topo Quad, 2016 USGS Elliot, OK 7.5 Minute Topo Quad, 2013 USGS South Coffeyville, OK 7.5 Minute Topo Quad, 2013X:\

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Osage & Walnut SiteCoffeyville, Kansas

Date: 1/19/2016 Drawn By: Gustavo Orozco Project No: X9025.15.0086.000

Figure 1Site Location Map

Approximate Site Location

±0 2,000 4,000

Feet

Montgomery County

PrimeTime Office

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Coffeyville Re-Con Site Boundaries

Main Re-Con Building

Osage and Walnut Site Boundaries

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Date: 4/11/2016 Drawn By: Clayton Hayes Project No: X9025.15.0086.000

Figure 2Site Layout Map±0 150 300

Feet

Legend!O Former oil well

Approximate site boundarySuspected petroleum source areaSuspected TCE source area

TCE Trichloroethene

Containers #131-134Container #135

Container #148Container #149

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Figure 3Container Inventory Summary Map±0 125 250

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LegendApproximate site boundaryContainer location

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Figure 4Sample Summary Map±0 150 300

Feet

Legend"J" Background radiation survey location!( DPT soil boring location

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APPENDIX C

PHOTOGRAPHIC DOCUMENTATION

Osage and Walnut Site

Coffeyville, Kansas

1

TETRA TECH

PROJECT NO.

103X9025150086

DESCRIPTION

This photograph shows the main Re-Con building at the

Coffeyville Re-Con, Inc. facility (Coffeyville Re-Con site).

The building, not currently in use, was previously utilized for

drum refurbishing.

1

CLIENT U.S. Environmental Protection Agency Region 7 Date

Direction: South PHOTOGRAPHER Joann Jeplawy 1/12/2016

TETRA TECH

PROJECT NO.

103X9025150086

DESCRIPTIONThis photograph shows the interior of the main Re-Con

building. 2


Direction: East PHOTOGRAPHER Joann Jeplawy 1/12/2016


Coffeyville, Kansas

2

TETRA TECH

PROJECT NO.

103X9025150086

DESCRIPTIONThis photograph shows the PrimeTime Industrial Painting,

LLC (PrimeTime) shop located centrally on the property. 3


Direction: Northwest PHOTOGRAPHER Joann Jeplawy 1/12/2016

TETRA TECH

PROJECT NO.

103X9025150086

DESCRIPTION This photograph shows the PrimeTime office building. 4


Direction: East PHOTOGRAPHER Joann Jeplawy 1/12/2016


Coffeyville, Kansas

3

TETRA TECH

PROJECT NO.

103X9025150086

DESCRIPTIONThis photograph shows the former oil well and related

equipment at the Coffeyville Re-Con site. 5


Direction: North PHOTOGRAPHER Joann Jeplawy 1/12/2016

TETRA TECH

PROJECT NO.

103X9025150086

DESCRIPTIONThis photograph shows the qualitative radiological survey of

soils surrounding the former oil well and related equipment.6


Direction: West PHOTOGRAPHER Cosmo Canacari 1/26/2016


Coffeyville, Kansas

4

TETRA TECH

PROJECT NO.

103X9025150086

DESCRIPTION

This photograph shows stained soil near the west property

boundary. Subsurface soil sampling was conducted in this

area to determine presence of contaminants.

7


Direction: NA PHOTOGRAPHER Joann Jeplawy 1/12/2016

TETRA TECH

PROJECT NO.

103X9025150086

DESCRIPTION

This photograph shows a truck-mounted direct-push

technology (DPT) rig conducting subsurface soil sampling in

the vicinity of the main Re-Con building.

8


Direction: North PHOTOGRAPHER Joann Jeplawy 1/26/2016


Coffeyville, Kansas

5

TETRA TECH

PROJECT NO.

103X9025150086

DESCRIPTION

This photograph shows three oil-water separators northeast of

the main Re-Con building. Samples were collected from each

of the containers and field tested to determine hazardous

characteristics.

9


Direction: North PHOTOGRAPHER Tommy Rebecchi 1/25/2016

TETRA TECH

PROJECT NO.

103X9025150086

DESCRIPTION

This photograph shows drums staged west of the main Re-

Con building. During the removal assessment, containers

were inventoried and subsequently sampled to determine if

contents were hazardous.

10


Direction: West PHOTOGRAPHER Joann Jeplawy 1/12/2016

APPENDIX D

CONTAINER SUMMARY TABLE


Container

ID #

Size

(gallons)Container Type Color

Estimated

Content

Amount

Material

State

PID Reading

(ppm)

Sample

Collected

(Y/N)

Explosive

(Y/N)

Water

Reactive

(Y/N)

Water

Soluble

(Dissolves,

Floats, Sinks)

pHOxidizer

(Y/N)

Sulfide

(Y/N)

Flammable

(Y/N)

Halide

(Y/N)

Cyanide

(Y/N)Comments

1 5 Paint Can/Bucket White 25% Sludge 880 Yes No No Dissolves NT NT NT Yes NT NT Industrial Finishes, satin black paint

2 5 Paint Can/Bucket Gray 100% Sludge 0 Yes No No Floats 5 No No Yes NT No Sherwin Williams Industrial Enamel

3 5 Paint Can/Bucket Rust 100% Sludge 49 Yes No No Floats 5 No No Yes NT No

4 5 Paint Can/Bucket Black 100% Sludge 849 Yes No No Floats 5 No No Yes NT No Industrial Finishes, 1346 Buff Primer

5 5 Paint Can/Bucket Black 100% Sludge 111 Yes No No Floats 5 No No Yes NT No

6 5 Paint Can/Bucket Rust 100% Sludge 36 Yes No No Floats 5 No No Yes NT No

7 5 Paint Can/Bucket White 100% Sludge 192 Yes No No Dissolves 5 No No Yes NT No Primer

8 5 Paint Can/Bucket White 100% Sludge 298 Yes No No Dissolves 5 No No Yes NT No Valspar, Black Urethane Primer

9 5 Paint Can/Bucket Gray 25% Sludge 182 Yes No No Floats 5 No No Yes NT No

10 5 Paint Can/Bucket Gray 75% Sludge 243 Yes No No Floats NT NT NT Yes NT NT

11 5 Paint Can/Bucket White 75% Sludge 656 Yes No No Floats NT NT NT Yes NT NT Industrial Finishes, DTM Enamel

12 5 Paint Can/Bucket Rust 75% Solid 225 No - - - - - - - - -Sherwin Williams Lacquer Thinner. Product was hardened and no sample was

collected

13 55 Drum Black 25% Solid 46.6 No - - - - - - - - - Crown Paint, Red Oxide Primer. Unable to collect sample

14 55 Drum Rust 50% Solid 25.5 Yes No No Dissolves 5 No No No NT No Overspray Material

15 5 Bucket Grey 25% Sludge 0 Yes No No Floats 3 No No Yes NT No

16 55 Drum Red 50% Solid 28.4 Yes No No Dissolves 5 No No No NT No Overspray Material

17 55 Drum Black 25% Sludge 171 Yes No No Dissolves 4 No No Yes NT No Primer

18 5 Bucket Black 100% Sludge 1460 Yes No No Floats NT NT NT Yes NT NT Carbit, White Booth Coating

19 5 Bucket Grey 100% Liquid 97 Yes No No Floats 5 No No Yes NT No Rich Paint Manufacturing, Ford Light Gray

20 5 Bucket Grey 25% Sludge 21 Yes No No Dissolves 8 No No No NT No Sherwin Williams, A-100 Exterior Satin Latex

21 5 Bucket Black 100% Liquid 0 Yes No No Floats 6 No No Combustible NT No Conoco, Hydraulic AW 46

22 1 Paint Can Grey 100% Liquid 43.9 Yes No No Floats 5 No No Yes NT No Unmarked paint can

23 1 Paint Can Grey 100% Liquid 254 Yes No No Floats 5 No No Yes NT No Unmarked paint can

24 1 Paint Can Rust 75% Liquid 5.5 Yes No No Floats 5 No No Yes NT No Unmarked paint can

25 5 Bucket Rust 25% Solid 275 Yes No No Floats 5 No No Yes NT No COOP, Masonry Paint

26 5 Bucket Rust 75% Sludge 448 Yes No No Sinks 5 No No Yes No No COOP, Masonry Paint

27 5 Bucket Rust 50% Sludge 15 Yes No No Sinks 5 No No No NT No COOP, Latex Masonry Paint

28 55 Drum Rust 25% Liquid 0 Yes No No Dissolves 9 No No No NT No Unmarked drum

29 5 Bucket Black 25% Liquid 0 Yes No No Floats 5 No No Combustible NT No Industrial Oil 70

30 1 Paint Can Rust 100% Liquid 146 Yes No No Floats 5 No No Yes NT No Unmarked paint can

31 5 Bucket Grey 100% Liquid 212 Yes No No Floats 5 No No Yes NT No PMI, non-lift Red Oxide Primer

32 5 Bucket Grey 100% Sludge 94.9 Yes No No Sinks 5 No No Yes No No PMI, 1329 Light Grey

33 55 Drum Black 75% Solid 7.4 Yes No No Floats 5 No No No NT No Overspray Material

34 55 Drum Black 75% Solid 0 Yes No No Floats 5 No No No NT No Overspray Material

35 55 Drum Black 75% Liquid 6 Yes No No Dissolves 5 No No No NT No Rainwater/Overspray Material

36 55 Drum Grey - - 3.4 - - - - - - - - - - Overspray Material. Same as container 33.

37 55 Drum Black - - 0 - - - - - - - - - - Overspray Material. Same as container 33.

38 5 Bucket Black 50% Liquid 0 Yes No No Floats 5 No No No NT No Conoco, Hydraulic AW 46

39 5 Bucket Black 25% Solid 0 Yes No No Floats NT NT NT Combustible NT NT Unmarked

40 55 Drum Black - - 24.3 - - - - - - - - - - Overspray Material. Same as container 33.

41 55 Drum Black 75% Solid 4.1 Yes No No Floats 5 No No No NT No Overspray Material

42 55 Drum Black - - 3.3 - - - - - - - - - - Overspray Material. Same as container 33.

43 5 Bucket Yellow 50% Liquid 0 Yes No No Floats 5 No No No NT No Orscheln, Premium 303 Tractor Hydraulic and Transmission Fluid

44 55 Drum Rust - - 0 - - - - - - - - - - Overspray Material. Same as container 33.


46 55 Drum Rust - - 0.4 - - - - - - - - - - Overspray Material. Same as container 33.

47 55 Drum Rust - - - - - - - - - - - - Overspray Material. Same as container 33.



50 55 Drum Rust 75% Solid 11.1 Yes No No Floats 5 No No No NT No Overspray Material



53 55 Drum Rust - - - - - - - - - - - - - Overspray Material. Same as container 33.






Page 1 of 3


Container

ID #

Size


Estimated

Content

Amount

Material

State

PID Reading

(ppm)

Sample

Collected

(Y/N)

Explosive

(Y/N)

Water

Reactive

(Y/N)

Water

Soluble

(Dissolves,

Floats, Sinks)

pHOxidizer

(Y/N)

Sulfide

(Y/N)

Flammable

(Y/N)

Halide

(Y/N)

Cyanide

(Y/N)Comments






64 55 Drum Rust 100% Solid 0 Yes No No Floats 6 No No No NT No Overspray Material and Rain Water

















81 55 Drum Rust 75% Solid 0 Yes No No Floats 5 No No No NT No Overspray Material

































Page 2 of 3


Container

ID #

Size


Estimated

Content

Amount

Material

State

PID Reading

(ppm)

Sample

Collected

(Y/N)

Explosive

(Y/N)

Water

Reactive

(Y/N)

Water

Soluble

(Dissolves,

Floats, Sinks)

pHOxidizer

(Y/N)

Sulfide

(Y/N)

Flammable

(Y/N)

Halide

(Y/N)

Cyanide

(Y/N)Comments






119 55 Drum Rust 100% Solid - Yes No No Floats 5 No No No NT No Overspray Material






125 55 Drum Rust 50% Solid 0 Yes No No Floats 5 No No No NT No Overspray Material

126 5 Bucket Black 75% Liquid 0 Yes No No Dissolves 5 No No No NT No Industrial Oil

127 5 Bucket Black 50% Liquid 0 Yes No No Floats 5 No No Combustible NT No Industrial Oil 70

128 5 Bucket Black 100% Liquid 0 Yes No No Dissolves 5 No No No NT No Industrial Oil

129 55 Drum Black 25% Solid 0 Yes No No Sinks 5 No No No NT No Overspray Material

130 55 Drum Black - - 0 - - - - - - - - - - Overspray Material. Same as container 33.

131 5 Bucket Grey 75% Sludge 401 Yes No No Floats NT NT NT Yes NT NT Partial flammable sticker on outside of container

132 40 Drum Blue 75% Sludge 0 Yes No No Floats 6 No No Combustible NT No Unisol Liquid Green 2B

133 40 Drum Blue 50% Sludge 73.9 Yes No No Floats 6 No No Combustible NT No Unisol Liquid Blue A

134 55 Drum Rust 75% Liquid - Yes No No Sinks 5 No No No No No Unisol Liquid Blue A

135 5 Bucket Rust 50% Sludge - Yes No No Sinks 6 No No No NT No No markings on outside of drum

136 5 Bucket Rust 50% Liquid - Yes No No Floats 5 No No Combustible NT No No markings on outside of drum

137 55 Drum Rust 25% Liquid - Yes No No Floats 5 No No Combustible NT No No markings on outside of drum

138 55 Drum Rust 50% Liquid - Yes No No Floats 5 No No Combustible NT No No markings on outside of drum

139 1 Sprayer Rust 75% Liquid - Yes No No Floats 5 No No Combustible NT No No markings on outside of drum

140 5 Bucket Rust 50% Solid - Yes No No Floats NT NT NT Combustible NT No Plastic Roof Cement

141 5 Bucket Rust 100% Liquid - Yes No No Sinks 5 No No Combustible No No WT-2010 Polymer Blend

142 5 Bucket Rust 25% Liquid - Yes No No Dissolves 10 No No Combustible No No Brainerd, Cyclohexylamine

143 5 Bucket Rust 50% Liquid - Yes No No Dissolves 14 No No No NT No Betco, Stripper

144 5 Bucket Rust 25% Sludge - Yes No No Sinks 6 No No Combustible No No No markings on outside of drum

145 55 Drum Rust 50% Sludge - Yes No No Floats NT NT NT Combustible NT NT No markings on outside of drum

146 55 Drum Rust 50% Sludge - Yes No No Floats NT NT NT Combustible NT NT No markings on outside of drum

147 55 Drum Rust 50% Solid - Yes No No Floats 5 No No Combustible NT No No markings on outside of drum

148 ~2,000 Oil/Water Separator Black 10% Liquid - Yes No No Dissolves 5 No No No NT No

149 ~2,000 Oil/Water Separator Black 10% Liquid - Yes No No Floats 5 No No No NT No

150 ~2,000 Oil/Water Separator Black 10% Liquid - Yes No No Floats 5 No No Combustible NT No

Notes:

% Percent

# Number

NT Not tested

PID Photoionization detector

ppm Parts per million

Page 3 of 3

APPENDIX E

BORING LOGS

Boring Loa Form

Site Name: OsaQe and Walnut Boring Number: 1:;;-f( - \ Date Drilled (Start/Finish): \I~ cf11- IL.I C.u - l f,, f) .;-

Drilling Method: DPT Drilling Company: Sea au II Elevation: Total Depth: 1-D' Coordinates: 1 J. C \'D'J..io Iv ti:i !~f'OCf.2 IN Depth to Water: Geologist:

Project Number: 103X9025150086.000 Weather: ~"F '"-... "' •,,, r .. .e:-l- . -~r.rl_~ I

' C» \J

> c: ., - iii :s - " - "' " .c:~ ,.. :C: en c. > > .,

"' E - 1i) Color C» E ~ ~ a: ., c. c. ., 0 c. 0 Description and Remarks .,

a: c. Ql LL 0 f! ..J "' - - (Munsell (/) .E .E ·s c~ c~

<.!l .c: (/) c:: or Rock) -:i

1,.. "}, - ')Vf}."t\

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- ,\1)\) ·.':/ - ·1? ... ~Jc - '°""""<? 2.tl l -...,. --~··- - '.?"°If'

25

----

30

Boring Log Form

Site Name: Osaqe and Walnut Boring Number: G-P - 2 Date Drilled (Start/Finish): l I 2.4 lt;i \\ii \O-\i,,'7 .<; Drilling Method: DPT Drilling Company: Seaaull Elevation: Total Depth: q, \ Coordinates: Depth to Water: Geologist: Project Number: 103X9025150086.000 Weather: i..-jf)',::;. 'f\Vl\,-t.v.i- 1. lV\d\.J

' C) J

Ill - > c: () - "' iii () :s - .c: ~ "' :.c C') c. > > Ill

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E lii ~ cc Ill c. c. Ill 0 c. 0 Description and Remarks Ill cc c. Ill Ll. 0 f! .J "' - - '(5 c- (Munsell en .E .E c- .c: (!j en a: or Rock) -::i \, D - lvt-,vt..I

(1 \ \ v\'1.'.«k~ iet I -~-4 U· \J ~ - cu{, 11vi;.uV\ Git/ --

\ ~.t

5 ' l -

\.\A \).U - \ ''l """ vv~v.M Lit! ---___!Q

-

---15 r------20 ,..____

----y

----30

Boring Log Form

Site Name: Osage and Walnut Boring Number: r..-v - z, Date Drilled (Start/Finish): ,j11,,i1to r1<! \C .- ~,tr> "7 r-..

Drilling Method: DPT Drilling Company: Seaoull Elevation: Total Depth: ~~' Coordinates: Depth to Water: Geologist:

Project Number: 103X9025150086.000 Weather: 7-.vc i::- C:.. \,)y'\V'\A A

• Cl J

Q) -,; c

.S:! - "' iii 0 :.a - .c ~ >-c. > > Q) "' E c. 1i) Color Cl .c Cl

E ~ ~ cc Q) c. 0 c. 0 Description and Remarks Q) Q) Q)

"' - - 'Ci cc c. o~ (Munsell 0 !!! -'

(/) .E .E o~ .c (.!) (/) a: or Rock) -:::;

0 () - io •' vr,1it.~

-A1<1\.t vvvWV\ tL~J

))-\ e·~ - ' •\;

- -•:\ , .. 5 ~·V -

q.'-1, - \'J\~\}J"' t\ll ,r \i<'\} ---

-10 ,____

-"""" --

15 --

---

20 ----

-25 -

-

---

30

Boring Log Form

Site Name: Osage and Walnut Boring Number: l...-i7-Li Date Drilled (Start/Finish): \I ?Ao Ii r~ h4 (.j <:'.: - G"l () i'l Drilling Method: DPT •

Drilling Company: Seaaull Elevation: Total Depth: Q ' Coordinates: Depth to Water: Geologist:

Project Number: 103X9025150086.000 Weather: .z, Cj ~ \)VWv-.A

C)

Ql - > c (.) - "' ~ (.) :s - .c ~ >- :c C> c. > Ql "' E a ru Color C)

E - - a: Ql c. 0 c. 0 Description and Remarks Ql Ql a: c. Ql Ql ~ ...J "' - - ·a c1=- (Munsell 0 (J) .5 .5 c- .c c.!l

(J) a: or Rock) -:J

\) u ,_ \f o-1(, \ y·iicvt\ ! t,ctvv{

v, - {U.\ ~ \/Vli,(l ~/

i) ~ ,_ 19vi;..v"' l, •'1 ,v

c\i;tvll \?Vii.NII GVJ -,_

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~}b - \')vuJvh L(J fl c ,_ U'

\11 v """" ( lt<-j 4. ';)r-1.vx:l ---

10

---

-15

--

--

20 ----

-~

-

-

--

30

Boring log Form

Site Name: Osaqe and Walnut Boring Number: LP- CJ" Date Drilled (Start/Finish): ,;,,,,,,,,,, 1)C/ 2 .. r-, Drilling Method: DPT ' Drilling Company: Seaaull Elevation: Total Depth:

Coordinates: Depth to Water: Geologist:

Project Number: 103X9025150086.000 Weather: '2, c.. "'>""' V'-.~ •

m } :> c:

Q) - o; :s - " - "' " .c:~ ,.. :.c Cl c. > > Q) "' E - Qi Color m

E lii ~ 0: Q) c. c. Q) 0 c. 0 Description and Remarks "' - $ 0: c. Ql LL

(Munsell 0 f! ...J (/) .E .E ·a c- c- .c: (!)

(/) a: or Rock) -:::; ~.~

•Jfi14S - (tlt

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~.\l -

- i-

I-

10

i-

I-

i-

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----

20

-

-

--

25

----

30

Boring log Form

Site Name: Osaqe and Walnut Boring Number: l-P.-/ ,, Date Drilled (Start/Finish): \ j,., I" 111" lo ? ('.: Drilling Method: DPT Drilling Company: Seagull Elevation: Total Depth: 4. \


Project Number: 1 03X9025150086. 000 Weather: :,c:, L'\.JnlAA~

' Cl ,I

Ql - :> c () - "' ~ () :s - .c: ~ > :c C> Q. > Ql "' E c. (i) Color Cl E iii - a: Ql Q. 0 Q. 0 Description and Remarks Ql Ql Ql

"' -- 'i5 a: Q. c !::. (Munsell 0 f: ...J

en .5 .5 c~ .c: Cl en c:: or Rock) -::J - y tl\.lC,

- <Jt!"-&11 'JVV-Vv\

{)-"' - JJt Vl'N"i"'- \:,,~ --5 - \fl I! l, '.\i'(\ . '" .

' t.\,q, - i -

- I- \\vjl'1..\' ~ cvv; -

10 -I-

I-

-I-

15 --I-

I-

-20

----

25

----

30

Boring Log Form

Site Name: Osaae and Walnut Boring Number: 4-17-\ Date Drilled (Start/Finish): \)li.\\Ji 1(-'.l!:;n i o'7 C,

Drilling Method: DPT Drilling Company: Seai:iull Elevation: Total Depth: {/_ ; , Coordinates: Depth to Water: Geologist: Project Number: 103X9025150086.000 Weather: 1,?) ". Vi\V\-' {,. J\\I\ ,,jAA

• Cl / ~

Q) - > c: 0 - "' o; 0 :c - J: ~ >- :c tJ) c. > > Q)

"' E Q.. (i) Color Cl E ~ ~ cc Q) c. 0 c. 0 Description and Remarks Q) Q) Q)

"' - - ·5 cc c. c !:!::. (Munsell 0 !!! ..J (/) .5 .5 c~ J: (!)

(/) a: or Rock) ."!::: -'

I- ( tl""

i))\ I- \tll tlN"j

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10 -----

15 ----

-~ I-

-I-

I-

25 r--

I-

I-

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30

Boring Log Form

Site Name: Osage and Walnut Boring Number: i-rO-' 'f.. Date Drilled (Start/Finish): \/,He 11 Iv ~ \ [ '2,c:.- I I 7,'*-.

Drilling Method: DPT Drilling Company: Sea~ull

Elevation: Total Depth: Cf..'


Project Number: 103X9025150086.000 Weather: U D' i:: <;ul'll'\M Ww·l..t

Cl

"' - :> c: .S:? - "' c;; 0 :a - .s::~ ,.,

c. > > "' "' E c. (i) Color Cl .s:: Cl E ~ ~ a: "' c. 0 c. 0 Description and Remarks

"' "' Q) "' - - ·c; a: c. c !!::. (Munsell 0 E-' (/) .E .E c~ .s:: (.!) (/) c: or Rock) -:J

i).il - {u:A.4 ~\\ \\"'1,\tV-q_t

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-10

----

15

----

20

----

25

----

30

Boring log Form

Site Name: Osage and Walnut Boring Number: 1-rP ·- q Date Drilled (Start/Finish): \f'11.li(/l \1C::>-v Drilling Method: DPT I

Drilling Company: Seaqull Elevation: Total Depth: "O \ Coordinates: Depth to Water: Geologist:

Project Number: 1 03X9025150086. 000 Weather: Wu "c '>Vl'lVVVi

Cl J :> c: Q>- a; " :s- .c: ~ » " Q. ~ > "' E - 'al Color Cl :c Ol E iii ~ a: c. c. 0 c. 0 Description and Remarks a: c. u. 0 ~ ...J "' - - '(5 o~ (Munsell (/) .5 .5 o~ .c: <.!l

(/) ii: or Rock) -:::; .Y\ \\ [tJr-~~~

~t .... l>J 2,,\- C '""} ~ \:JVIV.n J

vv\ ....

~ \, - ()At· \?11\)\.>JY\ cL°'1 \J•

--5 . ,___

\X ~~ \~~ vwv-J \-\A --

·- --~

10

----

15

----

20 ---

--

25 --

--

-30

Boring log Form

Site Name: Osaqe and Walnut Boring Number: /!2!Ji irP-ID Date Drilled (StarUFinish): I/ Z,l!J I I lo 1;-z,t:; - 1;'--10 Drilling Method: DPT Drilling Company: Seaaull Elevation: Total Depth: u' Coordinates: Depth to Water: Geologist:

Project Number: 103X9025150086.000 Weather: u O'' r:; c -·-·-Cl

_, <ll - > <::

.!::! - "' iii " :s - .s::~ >-c. > > <ll "' E - 1ii Color Cl .s:: Cl E lii ~ cc <ll c. c. <ll 0 c. 0 Description and Remarks <ll cc c. <ll LL 0 E-' "' - - (Munsell (/) .E .E ·c; c~

c~ .s:: (!)

(/) 0:: or Rock) :!::: ...J

\~ '{ o().l

I- ,e\\\ ~ . ).eV. -b "''~

~,'\ - VIAl\t Wt'-"\'\ c ltx; '( V: \c~ 1,,\'l1~" ~.I:> -

¥"ft"'" rJ~ - -5

-I-

--

10

----

15 ---

-I-

20 I---

----~ I-

--I-

30

Boring Log Form

Site Name: Osage and Walnut Boring Number: L~9--\\ Date Drilled (Start/Finish): d ·1 lo 111., \'-(\e;- -Drilling Method: DPT Drilling Company: SeaQull Elevation: Total Depth: L.i \ Coordinates: Depth to Water: Geologist:

Project Number: 103X9025150086.000 Weather: LtO" ~ c..' <V"\l!'V..__A

' Cl J ., - :> c

.S:? - "' Oi 0 :a - .c:~ "' c. > > ., "' E Q. Q) Color Cl .c: Cl

E ~ ~ 0: ., c. 0 c. 0 Description and Remarks ., ., ., "' - - ·c; 0: c. Q !:!:. (Munsell 0 E-' en .E .E Q~ .c: (!) en a: or Rock) -:::;

~~ - .811 \lfU-SS Y~0~v c{'~

0'\-\ >- (~~) (,\lb \:JtDWV\

~~ --- \'.)VbvJI\. ~ 5

-

-

--

10

----

15 ---

--

20 -

-

-->--

25 t---

->---- 30

Boring Log Form

Site Name: Osaae and Walnut Boring Number: (.,.\/- \ ")

Date Drilled (Start/Finish): \/'7i- \In 11..f '70 - it>bD Drilling Method: DPT I

Drilling Company: SeaQull Elevation: Total Depth: <;('I

Coordinates: Depth to Water: Geologist: Project Number: 103X9025150086.000 Weather: LID" C...\)f\V\M

~

01 \J :> c <1>-~ (.) ~- .J: ~ >-

(.) - "' :C en Cl. > "' E - a; Color 01 E Oi - a: Cl. Cl. 0 Cl. 0 Description and Remarks a: Cl. LI.. 0 f: ...I "' - - (Munsell ({) .E .E "C5 Cl~

o~ C) .J:

({) 0:: or Rock) -::J - voc\L

\~ - ~ \\ ~.\0\f\C\,\

J: I-

c\cvi ~rt>)\~ fs1c>.1 'N.cl) o.y<f' e,1" !r ~eiYo\9.u , ,,~ -,_ OcUv

~" ~ ' v/tJ -

\1vvt '>tAl"Wj Clvv--/

--I-

'()ytWJ\ (;~ I-

10 r---

I-

I-

-I-

15

-I-

I-

-20

----

25

----

30

Boring log Form

Site Name: Osage and Walnut Boring Number: (.., V- \2.. Date Drilled (Start/Finish): \I 11 n II in I '7 :z, i.:.,

Drilling Method: DPT '

Drilling Company: Seaaull Elevation: Total Depth: q,' Coordinates: Depth to Water: Geologist: Project Number: 103X9025150086.000 Weather: L\l) . C.; vW\• '

Cl ) Cl> - :> " .!:? - "' <ti " =s - .c: ~ ,., c. > > Cl> "' E - -a; Color Cl .c: Cl E lii ~ a: C1> c. c. Cl> 0 c. 0 Description and Remarks Cl> a: c. Cl> u. 0 E _. "' - - ·o o~ (Munsell en .E .E o~ .c: (!) en 0:: or Rock) -:::;

\1\t\(,\t 'i V1.Ji.i.u, ';~1>"1f'ol \_I" 'Ii," ) -H(Ys(~\\

~_,'\ --

\')Vbwn C\fM..j ;l' -Ir

5 I ,• ...---~ -

"\;1, - \I;

·11c1h.\: iovc,..V\ Cl~ - .... ....

10 ,.._

----15

----

20

----

25

----

30

Boring log Form

Site Name: OsaQe and Walnut Boring Number: forF'-IY Date Drilled (Start/Finish): \l'7,L·,l\1., I c:. c:., c... - I/,; (Jc;-

Drilling Method: DPT ' . Drilling Company: Seaoull Elevation: Total Depth: ~I, I


Project Number: 103X9025150086. 000 Weather:

Cl <1>- :> c

" - tll iii " =a - .c ~ >- :E en Cl. > > Cl> m E c..m Color Cl E Q; - a: Cl> Cl. 0 Cl. 0 Description and Remarks Cl> Cl> Cl> tll - - 'i5

a: Cl. c '==- (Munsell 0 e _, (fJ ..5 ..5 c~ .c G

(fJ c:: or Rock) -::; \" \11titlt ";iwko..tt '7ttilV\•l"J - \rQ[,\,_ I h\I -

V"'-\ - \1l'Olr!V1 e,livj ,f -... 1 ~ 5 -

'\''-Ii - \ ll)Y,-1- W C"'"' cl~ -~ ~

-10 -

-

---_:!2

--

--20 --------25 -------30

APPENDIX F

CHAIN-OF-CUSTODY FORMS, FIELD SHEETS, AND ANALYTICAL DATA

J

ACTIVITY LEADER(Print) --fvdd c. <?<1 pbetl

CONTENTS OF SHIPMENT

SAMPLE

CHAIN OF CUSTODY RECORD ENVIRONMENTAL PROTECTION AGENCY REGION VII

I NAME OF SURVEY OR ACTIVITY Osa'!c:. tv'cl Wo.l "Vl- ~ 1 Ir..

~

TYPE OF CONTAINERS SAMPLED MEDIA

IDATE OF COLLECTION I SHtt I ~ J....,_ ~I ltl DAY MONTH YEAR I 0

)._

RECEIVING LABORATORY ro ;e c,i..~i1 ... v~._,,1 ... \.-z. ~OA SET c olher AEMARKS10THEA INFORMATION NUMBER eUeii'AiNER" iOi'fIT BOT'TiT BOTTLE VIALS EA) ~

~ lcond11ton of samples upon rece<pl , '\)•Q"' ... g '5 ~ olher sample numbers. elc I NUMBERS OF CONTAINERS PER SAMPLE NUMBER ~ " ~ 'O

7041 - IOI I I )C.

- loz. I I

- 10~ I I - IOI./ ' ' -10s I '2..

-101.. I I

-101 I I

- 108 ' I - l DC\ I I

-110 I I

-\lo F1> t l - It\ I I

' I • - 111-

-113 I I

-114 I I

-11;" I I - II lo ' ' -111 I ' - I\ 8 I I

- 11 '\ \ I -1'2.o I l

- l'-1 I 2. -IZ't. I I I - I 'Z. 3 I ' hV

DESCRIPTION OF SHIPMENT MODE OF SHIPMENT

PIECE(S) CONSISTING OF BOX(ES) --COMMERCIAL CARRIER:

s --COURIER ICE CHEST(S): OTHER ---X--SAMPLER CONVEYED -(SHIPPING DOCUMENT NUMBER)

PERSONNEL CUSTODY RECORD

nEU~:tr ~MPLER) DATE TIME RECEI V ED B Y REASON FOR CHANGE OF CUS T ODY

1/i-1/1/tJ /2- c:, 0 TuiJ~ Ze~· J o:f::,, fl.e-6 11 SEAi:: D UNSEALED Ii:_ h SEALED UNSEALED N R ELIN Q UI SHED BY DATE TI M E RECEI V ED B Y REASON FOR CHAN GE O F CUST O D Y

nsEALED UNSEALEDr hsEALED UNSEALED r RELIN QUISHED BY DATE TIME RECEIVED B Y REASON FOR CHANGE OF CU STODY

I SEALED UNSEALEDr ! SE A LED UNSEALEDr

7-EPA-9262 (Rev1sed 5/ 85)

CHAIN OF CUSTODY RECORD ENVIRONMENTAL PROTECTION AGENCY REGION Vil

ACTIVITY LEADER(Print) I NAME OF SURVEY OR ACTIVITY lDATE OF C~LECTION <.. I SHtt1

f' odd f' owl Jo< I/ ()544~ 6¥'.J ""*"'"'"'+ Sile. ~ <V\ U>I I I 'I DAY Mt'1NTH ~ ..2 O ..:2

CONTENTS OF SHIPMENT TYPE OF CONTAINERS SAMPLED MEOIA RECEIVING LABORATORY

SAMPLE 8·..,.. l11. [ ., ~ (. 'J~ <lb.\ t.~vOA SET c other REMARKS.OTHER INFORMATION NUMBER Ctl81TAIN£1r BcffiIT BOTILE BOTILE VIALS EA)

~ e (cond1l1on ol samples upon 1ece1p1

~ ~ "' other sample numbers etc I NUMBERS OF CONTAINERS PER SAMPLE NUMBER o.o. 3' " 'O

-o~\-1?.c.f I I y.

-.'ZS l t -I lb ' I -zol I I

-2oZ.. I I

-20'3 I I lw

/ ~

/ r7

.,v \ \ v

/ \ t

~\ [/ \ \U A - /

/ \ l, / \~ /

h, \. \ / / ",) IV

/ \l "' \ -\A~' v:,\< r 0 . '/ VJ' v

r I\

/ / ~o Y1 \ / '" /"'\:~ I~

/ ~1\u Y/

v ...

/ / '


PIECE(S) CONSISTING OF BOX( ES) --COMMERCIAL CARRIER

3 --COURIER

ICE CHEST(S): OTHER -X....SAMPLER CONVEYED (SHIPPING DOCUMENT NUMBER)

PERSONNEL CUSTODY RECORD Ft~~JISHED,,SY (SAMPLER) OATE TIME RECEIVED BY REASON FOR CHANGE OF CUSTODY

- ~ 1/1r ''- /Z~lJ ~~~ f2ev'J af:- rbJ..b M SEALED UNSEALED rt: h SEALED UNSEALEO L RELINQUISHED BY DATE TIME RECEIVED BY REASON FOR CHANGE OF CUSTODY

llsEALED UNSEALEDr hsEALED UNSEALED r RELINQUISHED BY DATE TIME RECEIVED BY REASON FOR CHANGE OF CUSTODY

lSEALED UNSEALEDr 11 SEALED UNSEALEDr

7-EPA-9262(Rev1sed 5/85 J ·u.s. GPO: 2002-756-917140053

... CHAIN OF CUSTODY RECORD

ENVIRONMENlAL PROTECTION AGENCY REGION VII ACTIVITY LEADER(Print) I NAME OF SURVEY OR ACTIVITY 1D~TE OF COLLECTION I SHEEl

·d '/ """'DAY MONTH -vdir- I I I ofl ' , 14 t "'

CONTENTS OF SHIPMENT -TYPE OF CONT AINEAS SAMPLED MEDIA RECEIVING LABORATORY

SAMPLE .JI' l VOA SET c oiner REMARKS OTHER INFO RMATION

NUMBER CUBITAtNER 8cITTIT BOTILE BoffIT (2 VIALS EA) ~ e (cond111on ot samples upon 1ece1p1

; ~ ~ ~ othe1 sample numbe1s etc l

NUMBERS OF CONTAINERS PEA SAMPLE NUMBER " " "lol./l-1 y.

_., .. ' -2FD I

- 3 I

- t.f I -s I -(., I -7 I , ... ,,, \{I

·- ... -I- --'--- -- -- _,,,

~ _,,/

,,.,,. i..-

I/ ,,. ..,

1\ '""' / /

~

) / . ,, .

I -1' r /1 v

/ /IC. ' .J

/. ~ I

'

/""' ~f v 1/V

v I ~-

,, _,., y

- - --· - --- .__. - -- - - ,_ a-. - - -DESCRIPTION OF SHIPMENT MODE OF SHIPMENT

PIECE(S) CONSISTING OF BOX(ES) --COMMERCIAL CARRIER --COURIER

' ICE CHEST(S). OTHER ~SAMPLER CONVEYED (SHIPPING DOCUMENT NUMBER)

PERSONNEL CUSTODY RECORD FIELINQUISHEO BY (SAMPLER) DATE TIME REJ;;EIVEO BY •• REASON FOR CHANGE OF CUSTODY

:i' 'I I 1- ~, ,i; 12, ... 1~~--- t.~,_ ·)(IA .,_{)

!").SEALED UNSEALED r,- h SEALED ''-'' UNSEALED r REL INQUI SHED BY DATE TIME RECEIVED BY REASON FOR CHANGE OF CUSTODY

ll SEAL ED U NSEALEDr hsEALED UNSEALED r RELINQUISHED BY DATE TIME RECEIVED BY REASON FOR CHANGE OF CUSTODY

n SEALED UNSEALED! hsEALED UNSEALEDr

7-EPA-9262<Rev1sed 5/85) ·u.s. GPO: 2002-755-917/~0053

CHAIN OF CUSTODY RECORD ENVIRONMENlAL PROTECTION AGENCY REGION VII

f\CTIVITY LEADER(Print) I NAME OF SURVEY OR ACTIVITY IDATE OF COLLECTION I SHtt I

; "J.J l <- ·\Pb• II .,~ 't- w-u:I t.)e../ •1 vf _:z_ '· - ~I 1°11 DAY MONTH YEAR I

CONTENTS OF SHIPMENT TYPE. OF CONTAINERS SAMPLED MEDIA RECEIVING LABORATORY

SAMPLE rr '", ~"-"'< //..alt-C!J~' -- VOA SET c otner REMARKS.OTHER INFORMATION NUMBER CVlll Al NEil' '8lffitf eom E 8oTlli (2 VIALS EA) u e (cond1t1on ol samples upon receipt

i ~ ~ ~ otner sample numbers elc )

NUMBERS OF CONTAINERS PER SAMPLE NUMBER :0

"' /Oi , - I J I x - - - ~ - I-

J

,/

/ ,,

....... "" /

/ f1 I/ /

\ ~

/ l' '7

" ... / "

1/ J

'-',, ~I\

(" I

7~/ J \ \ \l·" r- \\

,.., ,,.

, \ Iv \ \c \ v~v

I . \ \ .. . f' . /\f; /'

' ~

' / ~ ,

/

/ /

I I I - -

DESCRIPTION OF SHIPM ENT MODE OF SHIPMENT

--PIECE(S) CONSISTING OF BOX(ES) --COMMERCIAL CARRIER --COURIER

ICE CHEST(S). OTHER _.:__ SAMPLER CONVEYED (SHIPPING DOCUMENT NUMBER)

PERSONNEL CUSTODY RECO RD FtELINQUISHED BY (S A M PL E R) DATE TIM E REC~1f BY / •

REASO N F O R CH A N G E OF CUSTODY

- .-2 I '1/1 1 I A.J

Z<:'olcit ~ ' ...,. tfi;-r' h SEAL~O ~f-rl SEALED U N S EAL E D i7

R E LINQU ISH E D B Y DATE T IME R E CE IVED B Y REA SON F O R CHANGE OF CUSTODY

hsEALED UNSEALEDr hsEAL E D U NSEALED l RELINQUISHED BY DATE TIME REC E IVED B Y REASON F O R CH A NG E O F CUSTODY

n SEALE D UNS EALED! hsEALE D UNSEAL ED r

7-EPA-92621Rev1sed 5185) ·u.s. GPO: 200?-755-917/(0053

Sample Collection Field Sheet US EPA Region 7 Kansas City, KS

ASR Number: 7041 Sample Number: 101 QC Code: _ Matrix: Solid Tag ID: 7041-101-_

Project ID: TCB794 Project Manager: Todd Campbell -Project Desc: Osage and Walnut site - Removal Assessment sampling

City: Coffeyville State: Kansas Program: Superfund

Site Name: Osage and Walnut site - Site ID: B794 Site OU: 00

Location Desc: Soil VOA & CN samples

Expected Cone: (or Circle One:

Latitude:

Longitude:

Laboratory Analyses: Container

4 - 40mL VOA vials (soil VOA 5035) 1 - 8 oz glass

Sample Comments:

(N/A)

Preservative

4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Deg C

Sample Collected By: TT

External Sample Number:

Low Medium High)

Sample Collection: Start:

End:

Holding Time Analysis

Date Time(24 hr) I .,--o-S-

@t::~ •/""')'"

14 Days 1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap

28 Days 1 Cyanide, Total in Soil

1 of 1



Project ID: TCB794 Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling





Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative




Low Medium High)


End:


Date

LJ2£/11P _}_)_

Time(24 hr)



1 of 1








Latitude:

Longitude:


4 - 40ml VOA vials (soil VOA 5035) 1 - 8 oz glass

Sample Comments:

(N/A)

Preservative




Low Medium High) Date Time(24 hr)


End:


14 Days 1 VOC's in Soi! at Low Levels by GC/MS Closed-System Purge-and-Trap


1 of 1





Site Name: Osage and Walnut site - Site ID: 8794 Site OU: 00



Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative

4 Deg C1 H20 + sodium bisulfate (in 2 vials) 4 Deg C



Low Medium High)


End:


,;.p- 2 0 -'?>) Date

J_j']f)J]Q

_/_/_

Time(24 hr)



1 of 1

Sample Collection field Sheet US EPA Region 7 Kansas City, KS







Latitude:

Longitude:



Sample Comments:

(N/A) \t-l';v \"' .

Preservative




Low Medium High)


End:


Date Time(24 hr)



1 of 1








Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative




Low Medium High)


End:


Date Time(24 hr)

L:i_::b_C

14 Days ,

1 VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap


1 of 1








Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative

4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Oeg C



Low Medium High)


End:


Date

L!1kllli _/_/_

Time(24 hr)



1 of 1








Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative




Low Medium High)


End:


Date Time(24 hr)

0°1 :CC



1 of 1








Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative






End:




1 of 1








Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative




Low Medium High.)


End:


Date

lJ11cl Tu> _J_j_

Time(24 hr)



1 of 1


i\0 "!\D·-1=0 ASR Number: 7041 Sample Number: .J.R QC Code: :e,? Matrix: Solid Tag ID: 7041-;t,.;q-~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~-*'~µ.~ll~

Project ID: TCB794 ,\,_,v\\ Project Manager: Todd Campbell Project Desc: Osage and Walnut site - Removal Assessment sampling


Site Name: Osage and Walnut site -



Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative

4 Deg C, H20 + sodium bisu!fate (in 2 vials) 4 Deg C


Site ID: B794 Site OU: 00



()C}_: So Sample Collection: Start:

Holding Time

14 Days

28 Days

1 of 1

End:

Analysis


1 Cyanide, Total in Soil

Sample Collection Field Sheet us EPA Region 7 Kansas City, KS

ASR Number: 7041 Sample Number: 111 QC Code:_ Matrix: Solid Tag ID: 7041-111-_






Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative




Low Medium High)


End:


Date

j_jJMJ_lo _}_}_

Time(24 hr)

-·-



1 of 1





Site Name: Osage and Walnut site - Site ID: B794 Site OU: DO



Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative

4 Deg C, H20 + sodium bisulfate (in 2 vials) 4 Oeg C



Low Medium High)


End:


Date

lJ21&11o _/_/_

Time(24 hr)



1 of 1








Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative




Low Medium High)


End:


Date Time(24 hr)

\_\ :1:>'2..



1 of 1








Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative




Low Medium High)


End:


Date Time(24 hr)

\j_: \0



1 of 1

Sample Collection Field Sheet: US EPA Region 7 Kansas City, KS







Latitude:

Longitude:


4 - 40mL VOA vials (soi! VOA 5035) 1 - 8 oz glass

Sample Comments:

(N/A)

Preservative




Low Medium High)


End:


Date Time(24 hr)

l_I :~ o


28 Days 1 Cyanide, Tota! in Soil

1 of 1








Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start:

Longitude: End:

Laboratory Analyses: Container Preservative Holding Time Analysis

4 - 40mL VOA vials (soil VOA 5035)

4 Deg C, H20 + sodium 14 Days bisulfate (in 2 vials)


1 - 8 oz glass

Sample Comments:

(N/A)

4 Deg C 28 Days


1 of 1









Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative




Low Medium High)


End:


Date

lJfu!l_fv _/_/_

Time(24 hr)


28 Days 1 Cyanide, Total in Soll

1 of 1








Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative




Low Medium High)


End:


Date

_l__j 2Jd __Llo

_)_)_

Time(24 hr)

\k_:v·:i



1 of 1








Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative




Low Medium High)


End:


Date

VZiolU.o _J_J_

Time(24 hr)



1 of 1








Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative




Low Medium High)


End:


Date Time(24 hr)

i.':L: io


28 Days 1 Cyanide, Tota! in Soil

1 of 1








Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative






End:




1 of 1


ASR Number: 7041 Sample Number: \1-'2- QC Code:_ Matrix: Solid Tag ID: 7041-\7.2--_







Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative

4 Deg C, H20 + sodium bisulfate {in 2 vials) 4 Deg C


Sample Colle~tion: Start: LlWllP _J_J_

l:i.:_2'b

Holding Time

14 Days

28 Days

1of1

End: -·-

Analysis




ASR Number: 7041 Sample Number: \I-3 QC Code:_ Matrix: Solid Tag ID: 7041-\7.. 3-_






Latitude:

Longitude:



Sample Comments:

(N/A}

Preservative

4 Deg C, H20 + sodium bisulfate {in 2 vials) 4 Deg C



Low Medium High)


End:


Date Time(24 hr)

l.i:.:!_O

-·-

14 Days 1 VDC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap


1of1


ASR Number: 7041 Sample Number: \Z- '-\ QC Code: _ Matrix: Solid Tag ID: 7041-\L.'-\-_



Site Name: Osage and Walnut site - Site ID: B794 Site OU: OD



Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative

4 Deg C, H20 + sodium bisulfate (in 2 vials} 4 Deg C



Low Medium High)

Sample Colle.ction: Start:

End:


Date

L'.lk'lli _J_J_

<

Time(24 hr)

6-: L\\

-·-



1of1


ASR Number: 7041 Sample Number: \1-t5 QC Code: _ Matrix: Solid Tag ID: 7041- \V7-_






Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative




Low Medium High)

Sample Colle.ction: Start:

End:


Date

L!lW.llo _j_J_

Time(24 hr)

ik_:oD

-·-



1of1


ASR Number: 7041 Sample Number: \1..l.ll QC Code:_ Matrix: Solid Tag ID: 7041-\'Zio-_






Latitude:

Longitude:



Sample Comments:

(N/A)

Preservative

4 Deg C, H20 + sodium blsulfate (in 2 vials) 4 Deg C



Low Medium High)

Sample Collei:;tion: Start:

End:


Date Time(24 hr)

-·-



1 of 1






Location Desc: Soil TPH VOA (GRO) & SVOA (DRO/ORO) samples


Latitude:

Longitude:


2 - 40ml VOA vial

1 ~ 8 oz glass

Sample Comments:

(N/A)

Preservative

4 Deg C

4 Deg C




Sample Collection: Start: \~:40

End:


14 Days 1 Volatile TPH in Soil by GC/MS

14 Days 1 Semi-Volatile TPH (DRO & ORO) in Soil by GC/FID

1 of 1








Latitude:

Longitude:


2 - 40mL VOA vial

1 - 8 oz glass

Sample Comments:

(N/A)

Preservative

4 Deg C

4 Deg C



Low Medium High) Date


End:



Time(24 hr)

L1:L:Lo

14 Days 1 Semi-Volatile TPH (ORO & ORO) in Soil by GC/FID

1 of 1








Latitude:

Longitude:


2 - 40ml VOA vial

1 - 8 oz glass

Sample Comments:

(N/A)

Preservative

4 Deg C

4 Deg C



Low Medium High)


End:


Date

l_f&l(i?

__/__/_


Time(24 hr)

IL\ :_2'-1

-·-

14 Days 1 Semi-Volatile TPH (DRO & ORO) in Soil by GC/FID

1 of 1

ACTIVITY LEAOER(Print) lt>c/,,., (,.-pl t'.I/

CONTENTS OF SHIPMENT

SAMPLE ' ~11"!n· ir,.·

CHAIN OF CUSTODY RECORD ENVIRONMENtAL PROTECTION AGENCY REGION VII I NAME OF SURVEY OR ACTIVITY

( r r ,;;;.•. i-J If., i-1 ..,

TYPE OF CONTAINERS SAMPLED MEDIA

IOATE OF COLLECTION I SHttl

-2...L ~ ~ .2a!L. I I I of I I DAY -ONTH YEAR

RECEIVING LABORATORY VOA SET c Olher REMARKS.OTHER IN FORMATION

NUMBER CUBITAtNER BOTILE Bomf BciffiE (2 VIALS EA) ~ e (cond1t1on of samples upon receipt

NUMBERS OF CONTAINERS PER SAMPLE NUMBER i ~ ~ ~ other sample numbers etc l 'C

I 'I I J I y. _.,

I ... -lFD I

- 3 I -~ I -s j

-1.. I

-7 I 1- / '1t' -- -- ~~

~ ~ ,,....

~,.,,

/ .....

> "'\ ./

t\vtv ~ v""

J,. ,) iv ./

_ ,., e /i v

//Jt. f / ~

/. ~~ I ) ,

/ r1 ')F ,.vt.ll( v l 1" J I/'-_, ""4"""

/ !.-l/

/ / '\ ------· - ·- --


PIECE(S) CONSISTING OF BOX(ES) --COMMERCIAL CARRIER --COURIER

J ICE CHEST(S). OTHER ___'L_sAMPLER CONVEYED (SHIPPING DOCUMENT NUMBER)

PERSONNEL CUSTODY RECORD .. DATE TIME Rrt-iVEO BY • •• REASON FOR CHANGE O F CUSTODY FlELINGIUISH-ED. &Y (SAMPLER) , c·') ;z. .1,; ,1, ... C'11 c; -avJ~>---· 2~4 1) ~146 t~SEALED ...__ UNSEALED [."'" ilSEALED ~ UNSEALED f" RELINQUISHED BY DATE TIME RECEIVED BY REASON FOR CHANGE OF CUSTODY

n SEALED UNSEA LEDr nsEALED UNSEALED j RELINQUISHED BY DATE TI ME RECEIVED BY REASON F OR CHANGE OF CUSTODY

l SEALED UNSEALED! l SEALED UNSEALEDr

7-EPA-9262(Re111sed 5185) 'U.S . GPO: 2002-755-917/~0053






Location Desc: RCRA metals & Hg samples

External Sample Number: _u_tJ_-~i __________ _


!l_:OS Latitude: iE:,_011p&&"I'

Longitude: -M· '-•&Oii ·


1 - 8 oz glass

1 - 8 oz glass

Sample Comments:

(N/A)

Preservative

4 Deg C

4 Deg C


Sample Collection: Start: _LJ~ ~

End: _J_J_


28 Days 1 Mercury in Soil or Sediment

180 Days 1 Total Metals Analysis of TCLP Metals in Soil by ICP-AES

1 of 1







External Sample Number: [)() - 2.

Expected Cone: (or Circle One: Low Medium High) Date

Latitude: J-=t-. ot=l-'!1"'.14"

Longitude: -"I§·~ ~'I\·


1 - 8 oz glass

Preservative

4 Deg C

Sample Collection: Start: l_fl..~llo>

End: _J_J_



Time(24 hr)

1 - 8 oz glass 4 Deg C 180 Days 1 Total Metals Analysis of TCLP Metals in Soil by ICP-AES

Sample Comments:

(N/A)


1 of 1


z.- f."D

ASR Number: 7041 Sample Number: 8 QC Code:_ ..

Matrix: Solid Tag ID: 7041-;#_







Latitude: 3~·0\'l!:.~.'~!. •

Longitude: -"t'll'.~"l"l"l•


1 - 8 oz glass

Preservative

4 Deg C

Sample Collection: Start: _j_/£!}!.J,_

End: __J__J_



Time(24 hr)


Sample Comments:

(N/A)


1 of 1









Latitude: :!>':!-. 01=!-0"t~'

Longitude: -"16'.~&20'


1 - 8 oz glass

Preservative

4 Deg C

Sample Collection: Start: _l__P.~1111>

End: _/_/_



Time(24 hr)


Sample Comments:

(N/A)


1of1







External Sample Number: Du- l/


Latitude: n,_o 11t-oo to·

Longitude: -~.~~ •


1 - 8 oz glass

Preservative

Sample Collection: Start: _l_fl.~\lo

End: _)_)_


28 Days 1 Mercury in Soi! or Sediment

Time(24 hr)

~:"Z-"1

1 - 8 oz glass

4 Deg C

4 Deg C 180 Days 1 Total Metals Analysis of TCLP Metals in Soil by ICP-AES

Sample Comments:

(N/A)


1 of 1









Latitude: 1'11-. 01 i. o"ifL_ Sample Collection: Start: J_fo__'!/llo

Longitude: •"1'!L!o1t&tU.'S' End: _)_)_

Laboratory Analyses: Container Preservative Holding Time Analysis

' /- 8 oz glass 4 Deg C 28 Days 1 Mercury in Soil or Sediment

Time(24 hr)

!l__ :'?!>I

~ )I'- 8 oz glass 4 Deg C 180 Days 1 Total Metals Analysis of TCLP Metals in Soil by ICP-AES

Sample Comments:

(N/A)


1 of 1









Latitude: ~':1-.0~'ll-~'

Longitude: •':\!i .1.1$ "I l'=I-'


1 - 8 oz glass

Preservative

4 Deg C

Sample Collection: Start: _L;2.__!; ~

End: _)_)_



Time(24 hr)

l.\_:~


Sample Comments:

(N/A)


1 of 1









Latitude: ~'*· 0\'4 ~6'"1 •

Longitude: ~'l'J.~~·


1 - 8 oz glass

Preservative

4 Deg C

Sample Collection: Start: _l__fo__:!!:/ Ile

End: _/_/_



Time(24 hr)


Sample Comments:

(N/A)


1 of 1

1 of 1

7077ASR Number: 1Sample Number: __QC Code: SolidMatrix:

_____________________________________________________________Location Desc:

__/__/__Start:

__/__/__End:

__________________________External Sample Number:

TTSample Collected By:

(N/A)

Sample Comments:

TCB794Project ID: Todd CampbellProject Manager:Osage and Walnut site - Removal Assessment samplingProject Desc:CoffeyvilleCity: KansasState:SuperfundProgram:

B794Site ID: 00Site OU:Osage and Walnut site - Site Name:

Sample Collection:

Tag ID: 7077-1-__

Date Time(24 hr)Expected Conc: (or Circle One: Low Medium High)

Latitude:

Longitude:

___ ___ ___

___ ___ ___

__:__

__:__

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

1 - 8 oz glass

1 - 8 oz glass

1 - 8 oz glass

1 - 8 oz glass

0 -

Container

4 Deg C

4 Deg C

4 Deg C

None

4 Deg C

Preservative

28

180

180

28

0

Holding Time

Mercury in Soil or Sediment

Total Metals Analysis of TCLP Metals in Soil by ICP-AES

TCLP Metals in Soil

TCLP Mercury in Soil

Percent Solid

Analysis Laboratory Analyses:

Days

Days

Days

Days

Days

1

1

1

1

1

Page 1 of 23

02/29/2016Date:

7041

TCB794

Osage and Walnut site - Removal Assessment sampling

Todd CampbellSUPR/ERNB

Transmittal of Sample Analysis Results for ASR #:

Project ID:

Project Description:

Margaret E.W. St. Germain, ChiefLaboratory Technology & Analysis Branch, Environmental Sciences & Technology Division

To:

Enclosed are the analytical data for the above-referenced Analytical Services Request (ASR) andProject. The Regional Laboratory has reviewed and verified the results in accordance with proceduresdescribed in our Quality Manual (QM). In addition to all of the analytical results, this transmittalcontains pertinent information that may have influenced the reported results and documents anydeviations from the established requirements of the QM.

Please contact us within 14 days of receipt of this package if you determine there is a need for anychanges. Please complete the enclosed Customer Satisfaction Survey and Data Disposition/SampleRelease memo for this ASR as soon as possible. The process of disposing of the samples for this ASRwill be initiated 30 days from the date of this transmittal unless an alternate release date is specifiedon the Data Disposition/Sample Release memo.

If you have any questions or concerns relating to this data package, contact our customer service lineat 913-551-5295.

Enclosures

cc: Analytical Data File.

United States Environmental Protection AgencyRegion 7

300 Minnesota AvenueKansas City, KS 66101

Subject:

From:

Page 2 of 23

7041ASR Number: 02/29/2016

Todd Campbell SUPR/ERNB 913-551-7115

TCB794


Coffeyville Kansas Superfund

Osage and Walnut site - B794Site ID: 00

Site Cleanup Support

Removal assessment sampling at the Osage and Walnut site. Field activities includesurface & subsurface soil sampling.

Project Manager: Org: Phone:

Project ID:

Project Desc:

Location: State: Program:

Site Name: Site OU:

Purpose:

__ = Field SampleFD = Field Duplicate

QC Codes identify the type of sample for quality control purpose.

Milligrams per KilogramMicrograms per Kilogram

Specific units in which results arereported.

The analyte was not detected at or above the reporting limit. The reportinglimit is an estimate.The presence or absence of the analyte can not be determined from the datadue to severe quality control problems. The data are rejected andconsidered unusable.The identification of the analyte is acceptable; the reported value is anestimate.The analyte was not detected at or above the reporting limit.

Specific codes used in conjunction with data values to provide additional information on the quality of reported results, or used to explain the absence of a specific value.

Summary of Project Information

Explanation of Codes, Units and Qualifiers used on this report

Sample QC Codes: Units:

UJ

R

J

U

=

=

=

=

Data Qualifiers:

= Values have been reviewed and found acceptable for use. (Blank)

mg/kgug/kg

==

TO BE SUBMITTEDQAPP Number:

303DC6GPRA PRC:

Page 3 of 23

1

2

2

3

4

5

6

7

101

102

103

104

105

106

107

108

109

110

110

111

112

113

114

115

116

117

118

119

120

121

122

123

124

125

126

201

202

203

SampleNo

__

__

FD

__

__

__

__

__

__

__

__

__

__

__

__

__

__

__

FD

__

__

__

__

__

__

__

__

__

__

__

__

__

__

__

__

__

__

__

QCCode

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Solid

Matrix

DU-1

DU-2

DU-2

DU-3

DU-4

DU-5

DU-6

DU-7

GP-1 (1-2)

GP-1 (3-4)

GP-2 (1-2)

GP-2 (7-8)

GP-3 (1-2)

GP-3 (7-8)

GP-4 (1-2)

GP-4 (7-8)

GP-5 (1-2)

GP-5 (7-8)

GP-5 (7-8)

GP-6 (2-3)

GP-6 (7-8)

GP-7 (3-4)

GP-7 (7-8)

GP-8 (3-4)

GP-8 (7-8)

GP-9 (3-4)

GP-9 (7-8)

GP-10 (3-4)

GP-11 (3-4)

GP-12 (3-4)

GP-12 (7-8)

GP-13 (2-3)

GP-13 (7-8)

GP-14 (3-4)

GP-14 (7-8)

GP-10 (3-4)

GP-11 (3-4)

GP-12 (3-4)

Location DescriptionExternal

Sample No

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/25/2016

01/25/2016

01/25/2016

01/25/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

01/26/2016

Start Date

11:05

11:10

11:10

11:18

11:24

11:31

11:38

11:49

15:05

15:05

16:15

16:25

08:15

08:20

08:51

09:00

09:37

09:50

09:50

10:28

10:37

11:02

11:10

11:30

11:38

11:59

12:07

13:40

14:20

14:54

14:58

15:40

15:47

16:00

16:05

13:40

14:20

14:54

Start Time

End Date

End Time

02/01/2016

02/01/2016

02/01/2016

02/01/2016

02/01/2016

02/01/2016

02/01/2016

02/01/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

01/27/2016

ReceiptDate

7041 02/29/2016

TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc:

ASR Number: Sample Information Summary

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

Page 4 of 23

1

1

1

1

Cyanide, Total in Soil


Semi-Volatile TPH (DRO & ORO) in Soil by GC/FID


Contract Lab Program (Out-Source)


RASP Contract Lab (Out-Source)


Lab:

Lab:

Lab:

Lab:

CLP Statement of Work


Similar to Modified version of SW846 Method 8015 (see comments)


Method:

Method:

Method:

Method:

(N/A)

(N/A)

Silver in samples -1 through -7 was UJ-coded. This analyte was not found in the samplesat or above the reporting limits, however, the reporting limits are an estimate (UJ-coded)due to negative recovery of this analyte in the interference check samples (ICS) which was

Comments:

Comments:

Comments:

Comments:

101-__ 102-__ 103-__ 104-__ 105-__ 106-__ 107-__108-__ 109-__ 110-__ 110-FD 111-__ 112-__ 113-__114-__ 115-__ 116-__ 117-__ 118-__ 119-__ 120-__121-__ 122-__ 123-__ 124-__ 125-__ 126-__

1-__ 2-__ 2-FD 3-__ 4-__ 5-__ 6-__7-__

201-__ 202-__ 203-__

1-__ 2-__ 2-FD 3-__ 4-__ 5-__ 6-__7-__

Samples:

Samples:

Samples:

Samples:

7041ASR Number: 02/29/2016

TCB794Project ID: Osage and Walnut site - Removal Assessment samplingProject Desc

RLAB Approved Analysis Comments

Analysis Comments About Results For This Analysis

Dry

Dry

Dry

Dry

Basis:

Basis:

Basis:

Basis:

Page 5 of 23

1

1

VOC's in Soil at Low Levels by GC/MS Closed-System Purge-and-Trap

Volatile TPH in Soil by GC/MS


RASP Contract Lab (Out-Source)

Lab:

Lab:

CLP Statement of WorkMethod:

not present in the ICS solution but whose absolute values were greater than the methoddetection limits (MDL), therefore, a possibility of false negatives exists. The actualreporting limits may be higher than the reported values.

1,2-dibromoethane had unacceptable response in one initial calibration curve (RRF: 0.195vs 0.20). It was therefore not possible to obtain valid results for this analyte. Results of'N/A' were reported for 1,2-dibromoethane with R-codes for samples -102 through -106, -108, and -110.

Bromoform, 1,2-dichlorobenzene, 1,3-dichlorobenzene, 1,4-dichlorobenzene, 1,2-dibromo-3-chloropropane, 1,2,4-trichlorobenzene, and 1,2,3-trichlorobenzene were UJ-coded insample -103. These analytes were not found in the sample at or above the reportinglimits, however, the reporting limits are an estimate (UJ-coded) due to low internalstandard response. The actual reporting limits for these analytes may be lower than thereported values.

Acetone, cyclohexane, and methylcyclohexane were J-coded in sample -101. Although theanalyte in question has been positively identified in the sample, the quantitation is anestimate (J-coded) due to high recoveries of surrogate analytes (2-butanone-d5: 137-161% vs 20-135% and 1,2-dichloropropane-d6: 123-136% vs 70-120%) in this sample.The actual concentrations for these analytes may be lower than the reported values.

Cis-1,2-dichloroethene was J-coded in samples -103 and -108. Although the analyte inquestion has been positively identified in the samples, the quantitations are an estimate (J-coded) due to low recoveries of a surrogate analyte (1,1-dichloroethene-d2: 36-44% vs 45-110%) in these samples. The actual concentrations for this analyte may be higher than thereported values.

Cis-1,2-dichloroethene in samples -104, -105, -106, and -110 and trans-1,2-dichloroethene and 1,1-dichloroethene in samples -103 through -106, -108, and -110 wereUJ-coded. These analytes were not found in the samples at or above the reporting limits,however, the reporting limits are an estimate (UJ-coded) due to low recoveries of thesurrogate analyte (1,1-dichloroethene-d2: 36-44% vs 45-110%). The actual reportinglimits for these analytes may be higher than the reported values.

Comments:

101-__ 102-__ 103-__ 104-__ 105-__ 106-__ 107-__108-__ 109-__ 110-__ 110-FD 111-__ 112-__ 113-__114-__ 115-__ 116-__ 117-__ 118-__ 119-__ 120-__121-__ 122-__ 123-__ 124-__ 125-__ 126-__

Samples:

7041ASR Number: 02/29/2016




DryBasis:

Page 6 of 23

Similar to Volatile TPH by GC/MS (see comments)Method:

(N/A)Comments:

201-__ 202-__ 203-__ Samples:

7041ASR Number: 02/29/2016




DryBasis:

Page 7 of 23

1

1



Analysis/ Analyte

Mercury

Arsenic

Barium

Cadmium

Chromium

Lead

Selenium

Silver

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

Units 1-__ 2-__ 2-FD 3-__

0.11 U 0.11 U 0.11 U 0.12 U

1.7 1.5 2.6 8.5

52.9 30.3 63.0 103

1.2 0.69 0.95 1.4

7.1 14.2 12.0 32.9

36.6 141 77.1 140

3.1 U 3.0 U 3.0 U 3.2 U

0.89 UJ 0.86 UJ 0.84 UJ 0.90 UJ

7041ASR Number: 02/29/2016


RLAB Approved Sample Analysis Results

Page 8 of 23

1

1



Analysis/ Analyte

Mercury

Arsenic

Barium

Cadmium

Chromium

Lead

Selenium

Silver

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

Units 4-__ 5-__ 6-__ 7-__

0.73 0.11 U 0.12 U 0.29

256 1.9 3.2 3.8

597 94.7 125 66.5

22.1 1.3 2.6 4.7

197 11.7 18.0 69.4

256 82.7 151 31.9

3.2 U 3.3 U 3.3 U 3.4 U

9.0 UJ 0.94 UJ 0.93 UJ 0.97 UJ

7041ASR Number: 02/29/2016



Page 9 of 23

1

1



Analysis/ Analyte

Cyanide

Acetone

Benzene

Bromochloromethane

Bromodichloromethane

Bromoform

Bromomethane

2-Butanone

Carbon Disulfide

Carbon Tetrachloride

Chlorobenzene

Chloroethane

Chloroform

Chloromethane

Cyclohexane

1,2-Dibromo-3-Chloropropane

Dibromochloromethane

1,2-Dibromoethane

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

Dichlorodifluoromethane

1,1-Dichloroethane

1,2-Dichloroethane

1,1-Dichloroethene

cis-1,2-Dichloroethene

trans-1,2-Dichloroethene

1,2-Dichloropropane

cis-1,3-Dichloropropene

trans-1,3-Dichloropropene

Ethyl Benzene

2-Hexanone

Isopropylbenzene

Methyl Acetate

Methyl tert-butyl ether

Methylcyclohexane

Methylene Chloride

4-Methyl-2-Pentanone

Styrene

1,1,2,2-Tetrachloroethane

Tetrachloroethene

Toluene

1,2,3-Trichlorobenzene


mg/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

Units 101-__ 102-__ 103-__ 104-__

0.60 U 0.62 U 0.62 U 0.62 U

120 J 11 27 11 U

5.3 U 5.5 U 10 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

5.3 U 5.5 U 5.0 UJ 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

11 U 11 U 10 U 11 U

5.3 U 5.5 U 5.0 U 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

15 J 5.5 U 1300 5.3 U

5.3 U 5.5 U 5.0 UJ 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

5.3 U N/A R N/A R N/A R

5.3 U 5.5 U 5.0 UJ 5.3 U

5.3 U 5.5 U 5.0 UJ 5.3 U

5.3 U 5.5 U 5.0 UJ 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

21 12 16 20

5.3 U 5.5 U 5.0 U 5.3 U

5.3 U 5.5 U 5.0 UJ 5.3 UJ

7.9 5.5 U 5.2 J 5.3 UJ

5.3 U 5.5 U 5.0 UJ 5.3 UJ

5.3 U 5.5 U 5.0 U 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

8.3 5.5 U 54 5.3 U

5.3 U 11 U 10 U 11 U

5.3 U 5.5 U 9.2 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

5.3 U 5.5 U 5.0 U 14

6.7 J 5.5 U 23 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

11 U 11 U 10 U 11 U

5.3 U 5.5 U 5.0 U 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

16 5.5 U 130 5.3 U

5.3 U 5.5 U 5.0 UJ 5.3 U

5.3 U 5.5 U 5.0 UJ 5.3 U

7041ASR Number: 02/29/2016



Page 10 of 23

Analysis/ Analyte

1,1,1-Trichloroethane


Trichloroethene

Trichlorofluoromethane

1,1,2-Trichlorotrifluoroethane

Vinyl Chloride

m and/or p-Xylene

o-Xylene

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

Units 101-__ 102-__ 103-__ 104-__

5.3 U 5.5 U 5.0 U 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

5.3 U 5.5 U 5.0 U 5.3 U

5.3 7.1 5.0 U 6.2

39 5.5 U 1300 5.3 U

27 5.5 U 850 5.3 U

7041ASR Number: 02/29/2016



Page 11 of 23

1

1



Analysis/ Analyte

Cyanide

Acetone

Benzene

Bromochloromethane


Bromoform

Bromomethane

2-Butanone

Carbon Disulfide


Chlorobenzene

Chloroethane

Chloroform

Chloromethane

Cyclohexane



1,2-Dibromoethane

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


1,1-Dichloroethane

1,2-Dichloroethane

1,1-Dichloroethene



1,2-Dichloropropane



Ethyl Benzene

2-Hexanone

Isopropylbenzene

Methyl Acetate


Methylcyclohexane

Methylene Chloride


Styrene


Tetrachloroethene

Toluene



mg/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

Units 105-__ 106-__ 107-__ 108-__

0.59 U 0.62 U 0.61 U 0.59 U

10 U 11 U 21 10 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

10 U 11 U 13 U 10 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

N/A R N/A R 6.3 U N/A R

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 6.8

5.2 U 5.6 U 6.3 U 5.0 U

5.2 UJ 5.6 UJ 6.3 U 5.0 UJ

5.2 UJ 5.6 UJ 6.3 U 24 J

5.2 UJ 5.6 UJ 6.3 U 5.0 UJ

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 23 5.0 U

10 U 11 U 13 U 10 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 33 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

10 U 11 U 13 U 10 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

7041ASR Number: 02/29/2016



Page 12 of 23

Analysis/ Analyte



Trichloroethene



Vinyl Chloride

m and/or p-Xylene

o-Xylene

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

Units 105-__ 106-__ 107-__ 108-__

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

5.2 U 5.6 U 42 5.0 U

5.2 U 5.6 U 6.3 U 5.0 U

7041ASR Number: 02/29/2016



Page 13 of 23

1

1



Analysis/ Analyte

Cyanide

Acetone

Benzene

Bromochloromethane


Bromoform

Bromomethane

2-Butanone

Carbon Disulfide


Chlorobenzene

Chloroethane

Chloroform

Chloromethane

Cyclohexane



1,2-Dibromoethane

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


1,1-Dichloroethane

1,2-Dichloroethane

1,1-Dichloroethene



1,2-Dichloropropane



Ethyl Benzene

2-Hexanone

Isopropylbenzene

Methyl Acetate


Methylcyclohexane

Methylene Chloride


Styrene


Tetrachloroethene

Toluene



mg/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

Units 109-__ 110-__ 110-FD 111-__

0.60 U 0.61 U 0.61 U 0.66 U

19 10 U 9.9 U 12 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

10 U 10 U 9.9 U 12 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U N/A R 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 UJ 5.0 U 6.2 U

5.2 U 5.1 UJ 5.0 U 6.2 U

5.2 U 5.1 UJ 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

10 U 10 U 9.9 U 12 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

10 U 10 U 9.9 U 12 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

7041ASR Number: 02/29/2016



Page 14 of 23

Analysis/ Analyte



Trichloroethene



Vinyl Chloride

m and/or p-Xylene

o-Xylene

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

Units 109-__ 110-__ 110-FD 111-__

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

5.2 U 5.1 U 5.0 U 6.2 U

7041ASR Number: 02/29/2016



Page 15 of 23

1

1



Analysis/ Analyte

Cyanide

Acetone

Benzene

Bromochloromethane


Bromoform

Bromomethane

2-Butanone

Carbon Disulfide


Chlorobenzene

Chloroethane

Chloroform

Chloromethane

Cyclohexane



1,2-Dibromoethane

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


1,1-Dichloroethane

1,2-Dichloroethane

1,1-Dichloroethene



1,2-Dichloropropane



Ethyl Benzene

2-Hexanone

Isopropylbenzene

Methyl Acetate


Methylcyclohexane

Methylene Chloride


Styrene


Tetrachloroethene

Toluene



mg/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

Units 112-__ 113-__ 114-__ 115-__

0.62 U 0.64 U 0.59 U 0.66 U

11 U 11 9.4 U 11 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

11 U 11 U 9.4 U 11 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

11 U 11 U 9.4 U 11 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

11 U 11 U 9.4 U 11 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

7041ASR Number: 02/29/2016



Page 16 of 23

Analysis/ Analyte



Trichloroethene



Vinyl Chloride

m and/or p-Xylene

o-Xylene

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

Units 112-__ 113-__ 114-__ 115-__

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

5.4 U 5.5 U 4.7 U 5.5 U

7041ASR Number: 02/29/2016



Page 17 of 23

1

1



Analysis/ Analyte

Cyanide

Acetone

Benzene

Bromochloromethane


Bromoform

Bromomethane

2-Butanone

Carbon Disulfide


Chlorobenzene

Chloroethane

Chloroform

Chloromethane

Cyclohexane



1,2-Dibromoethane

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


1,1-Dichloroethane

1,2-Dichloroethane

1,1-Dichloroethene



1,2-Dichloropropane



Ethyl Benzene

2-Hexanone

Isopropylbenzene

Methyl Acetate


Methylcyclohexane

Methylene Chloride


Styrene


Tetrachloroethene

Toluene



mg/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

Units 116-__ 117-__ 118-__ 119-__

0.61 U 0.57 U 0.59 U 0.56 U

11 U 9.6 U 9.3 U 9.2 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

11 U 9.6 U 9.3 U 9.2 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

11 U 9.6 U 9.3 U 9.2 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

11 U 9.6 U 9.3 U 9.2 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

7041ASR Number: 02/29/2016



Page 18 of 23

Analysis/ Analyte



Trichloroethene



Vinyl Chloride

m and/or p-Xylene

o-Xylene

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

Units 116-__ 117-__ 118-__ 119-__

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

5.3 U 4.8 U 4.7 U 4.6 U

7041ASR Number: 02/29/2016



Page 19 of 23

1

1



Analysis/ Analyte

Cyanide

Acetone

Benzene

Bromochloromethane


Bromoform

Bromomethane

2-Butanone

Carbon Disulfide


Chlorobenzene

Chloroethane

Chloroform

Chloromethane

Cyclohexane



1,2-Dibromoethane

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


1,1-Dichloroethane

1,2-Dichloroethane

1,1-Dichloroethene



1,2-Dichloropropane



Ethyl Benzene

2-Hexanone

Isopropylbenzene

Methyl Acetate


Methylcyclohexane

Methylene Chloride


Styrene


Tetrachloroethene

Toluene



mg/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

Units 120-__ 121-__ 122-__ 123-__

0.63 U 0.57 U 0.61 U 0.62 U

10 U 11 9.3 U 13

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

10 U 9.1 U 9.3 U 9.8 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 17 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 9.9 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 42 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

10 U 9.1 U 9.3 U 9.8 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

10 U 9.1 U 9.3 U 9.8 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

7041ASR Number: 02/29/2016



Page 20 of 23

Analysis/ Analyte



Trichloroethene



Vinyl Chloride

m and/or p-Xylene

o-Xylene

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

Units 120-__ 121-__ 122-__ 123-__

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

5.2 U 4.5 U 4.6 U 4.9 U

7041ASR Number: 02/29/2016



Page 21 of 23

1

1

1




Analysis/ Analyte

Cyanide

TPH DRO

TPH ORO

Acetone

Benzene

Bromochloromethane


Bromoform

Bromomethane

2-Butanone

Carbon Disulfide


Chlorobenzene

Chloroethane

Chloroform

Chloromethane

Cyclohexane



1,2-Dibromoethane

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


1,1-Dichloroethane

1,2-Dichloroethane

1,1-Dichloroethene



1,2-Dichloropropane



Ethyl Benzene

2-Hexanone

Isopropylbenzene

Methyl Acetate


Methylcyclohexane

Methylene Chloride


Styrene


Tetrachloroethene

mg/kg

mg/kg

mg/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

Units 124-__ 125-__ 126-__ 201-__

0.59 U 0.60 U 0.58 U

10.8 U

86.7 U

10 U 9.5 U 9.8 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

10 U 9.5 U 9.8 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

10 U 9.5 U 9.8 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

10 U 9.5 U 9.8 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

7041ASR Number: 02/29/2016



Page 22 of 23

1 Volatile TPH in Soil by GC/MS

Analysis/ Analyte

Toluene





Trichloroethene



Vinyl Chloride

m and/or p-Xylene

o-Xylene

TPH GRO

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

mg/kg

Units 124-__ 125-__ 126-__ 201-__

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

5.2 U 4.8 U 4.9 U

2.24 U

7041ASR Number: 02/29/2016



Page 23 of 23

1

1


Volatile TPH in Soil by GC/MS

Analysis/ Analyte

TPH DRO

TPH ORO

TPH GRO

mg/kg

mg/kg

mg/kg

Units 202-__ 203-__

10.3 U 21.5

82.8 U 201

2.09 U 2.21 U

7041ASR Number: 02/29/2016



7041

TCB794Project ID:



United States Environmental Protection AgencyRegion VII


__/__/____

Data Disposition/Sample Disposition for ASR #


Subject:

Alisha ClaycampENST/LTAB/LABS

I have received and reviewed the Transmittal of Sample Analysis Results for the above-referencedAnalytical Services Request(ASR) and have indicated my findings below by checking one of theboxes for Data Disposition and Sample Disposition.

I understand all samples will be disposed of unless samples are requested to be held. If I do notreturn this form within 30 days of the transmittal all samples will have a waste determinationmade and scheduled for disposal.

"RELEASED" - Read-only to all Region 7 employees and contractors that have R7LIMS"Customer" account. All Samples may be disposed of upon receipt of this form if not requested to

"Project Manager Accessible" - Available on the LAN in R7LIMS for my use only. All Samples maybe disposed of upon receipt of this form if not requested to be held.

"Archived" - THIS DATA IS OF A SENSITIVE NATURE. Any future reports must be requestedthrough the laboratory. All samples may be disposed of upon receipt of the form if not requestedto be held.

Transmittal Date:

From:

To:

No longer need samples for site characterization

Hold Samples - I have determined that the samples need to be held until ______________, afterwhich time they will be disposed of in accordance with applicable regulations. The reason for the hold is:

Samples are associated with a legal proceeding.

Question/Concern with data - possible reanalysis requested.

Other:________________________________________________________________

Data Disposition

Sample Disposition

Page 1 of 6

03/17/2016Date:

7077

TCB794



Transmittal of Sample Analysis Results for ASR #:

Project ID:


Margaret E.W. St. Germain, ChiefLaboratory Technology & Analysis Branch, Environmental Sciences & Technology Division

To:

Enclosed are the analytical data for the above-referenced Analytical Services Request (ASR) andProject. The Regional Laboratory has reviewed and verified the results in accordance with proceduresdescribed in our Quality Manual (QM). In addition to all of the analytical results, this transmittalcontains pertinent information that may have influenced the reported results and documents anydeviations from the established requirements of the QM.

Please contact us within 14 days of receipt of this package if you determine there is a need for anychanges. Please complete the enclosed Customer Satisfaction Survey and Data Disposition/SampleRelease memo for this ASR as soon as possible. The process of disposing of the samples for this ASRwill be initiated 30 days from the date of this transmittal unless an alternate release date is specifiedon the Data Disposition/Sample Release memo.

If you have any questions or concerns relating to this data package, contact our customer service lineat 913-551-5295.

Enclosures

cc: Analytical Data File.

United States Environmental Protection AgencyRegion 7


Subject:

From:

Page 2 of 6

7077ASR Number: 03/17/2016

Todd Campbell SUPR/ERNB 913-551-7115

TCB794


Coffeyville Kansas Superfund

Osage and Walnut site - B794Site ID: 00

Site Cleanup Support

Removal Assessment.Sample collected from 55-gallon drum containing overspray material. This samplewas a sample of opportunity collected w/ASR #7041.

Project Manager: Org: Phone:

Project ID:

Project Desc:

Location: State: Program:

Site Name: Site OU:

Purpose:

__ = Field Sample

QC Codes identify the type of sample for quality control purpose.

Milligrams per KilogramPercentMilligrams per Liter

Specific units in which results arereported.

The analyte was not detected at or above the reporting limit. The reportinglimit is an estimate.The identification of the analyte is acceptable; the reported value is anestimate.The analyte was not detected at or above the reporting limit.

Specific codes used in conjunction with data values to provide additional information on the quality of reported results, or used to explain the absence of a specific value.

Summary of Project Information

Explanation of Codes, Units and Qualifiers used on this report

Sample QC Codes: Units:

UJ

J

U

=

=

=

Data Qualifiers:

= Values have been reviewed and found acceptable for use. (Blank)

mg/kg%

mg/L

===

303DC6GPRA PRC:

Page 3 of 6

1

SampleNo

__

QCCode

Solid

Matrix

Overspray material

Location DescriptionExternal

Sample No

01/27/2016

Start Date

12:00

Start Time

End Date

End Time

02/17/2016

ReceiptDate

7077 03/17/2016


ASR Number: Sample Information Summary

-

Page 4 of 6

1

1

1

1

1


Percent Solid


TCLP Metals in Soil


Region 7 ESAT Contract Lab (In-House)





Lab:

Lab:

Lab:

Lab:

Lab:

EPA Region 7 RLAB Method 3121.23D

EPA Region 7 RLAB Method 3142.9G

EPA Region 7 RLAB Method 3121.23D applied to TCLP extracts

EPA Region 7 RLAB Method 3122.3F TCLP

EPA Region 7 RLAB Method 3122.3F

Method:

Method:

Method:

Method:

Method:

(N/A)

(N/A)

Sample 1 was analyzed 6 day(s) past their 28 day holding time. The results foranalytes that were not found at or above the reporting limit were UJ-coded to indicate thatthe reporting limit is an estimated value. The actual reporting limit may be higher than thereported value.

Comments:

Comments:

Comments:

Comments:

1-__

1-__

1-__

1-__

Samples:

Samples:

Samples:

Samples:

7077ASR Number: 03/17/2016




Dry

N/A

N/A

N/A

Basis:

Basis:

Basis:

Basis:

Page 5 of 6

Arsenic (56,44,75-115) was UJ-coded in sample 1. This analyte was not found in thesample at or above the reporting limit, however, the reporting limit is an estimate (UJ-coded) due to low recovery of this analyte in the laboratory matrix spike. The actualreporting limit for this analyte may be higher than the reported value.

Selenium (41,32,75-108) was J-coded in sample 1. Although the analyte in question hasbeen positively identified in the sample, the quantitation is an estimate (J-coded) due tolow recovery of this analyte in the laboratory matrix spike. The actual concentration forthis analyte may be higher than the reported value.

Arsenic (23,7.6) was UJ-coded in sample 1. This analyte was not found in the sample at orabove the reporting limit, however, the reporting limit is an estimate (UJ-coded) due topoor precision obtained for this analyte in the laboratory matrix spike and matrix spikeduplicate. The actual reporting limit for this analyte may be higher than the reportedvalue.

Comments:

1-__ Samples:

7077ASR Number: 03/17/2016




DryBasis:

Page 6 of 6

1

1

1

1

1


Percent Solid


TCLP Metals in Soil


Analysis/ Analyte

Mercury

Solids, percent

Mercury

Arsenic

Barium

Cadmium

Chromium

Lead

Selenium

Silver

Arsenic

Barium

Cadmium

Chromium

Lead

Selenium

Silver

mg/kg

%

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

Units 1-__

0.00857

98.7

0.000250 UJ

0.050 U

0.162

0.005 U

0.015 U

0.050 U

0.542

0.025 U

5.1 UJ

36.1

1.9

20.8

8.1

96.3 J

3.6

7077ASR Number: 03/17/2016



7077

TCB794Project ID:



United States Environmental Protection AgencyRegion VII


__/__/____

Data Disposition/Sample Disposition for ASR #


Subject:

Alisha ClaycampENST/LTAB/LABS

I have received and reviewed the Transmittal of Sample Analysis Results for the above-referencedAnalytical Services Request(ASR) and have indicated my findings below by checking one of theboxes for Data Disposition and Sample Disposition.

I understand all samples will be disposed of unless samples are requested to be held. If I do notreturn this form within 30 days of the transmittal all samples will have a waste determinationmade and scheduled for disposal.

"RELEASED" - Read-only to all Region 7 employees and contractors that have R7LIMS"Customer" account. All Samples may be disposed of upon receipt of this form if not requested to

"Project Manager Accessible" - Available on the LAN in R7LIMS for my use only. All Samples maybe disposed of upon receipt of this form if not requested to be held.

"Archived" - THIS DATA IS OF A SENSITIVE NATURE. Any future reports must be requestedthrough the laboratory. All samples may be disposed of upon receipt of the form if not requestedto be held.

Transmittal Date:

From:

To:

No longer need samples for site characterization

Hold Samples - I have determined that the samples need to be held until ______________, afterwhich time they will be disposed of in accordance with applicable regulations. The reason for the hold is:

Samples are associated with a legal proceeding.

Question/Concern with data - possible reanalysis requested.

Other:________________________________________________________________

Data Disposition

Sample Disposition

APPENDIX G

ANALYTICAL DATA TABLES

Mercury Arsenic Barium Cadmium Chromium Lead Selenium Silver

Overspray Material 7077-1 0.00857 5.10 UJ 36.1 1.90 20.8 8.10 96.3 J 3.60

46 3.00 2.25E+05 980 NE* 800 5.80E+03 5.80E+03

20 63.2 2.77E+05 965 111** 1.00E+03 1.02E+04 1.02E+04

Overspray Material 7077-1 2.50E-04 U 0.050 U 0.162 0.005 U 0.015 U 0.050 U 0.542 0.025 U

0.200 5.00 100 1.00 5.00 5.00 1.00 5.00

Notes:

Italicized value indicates the reporting limit exceeds a benchmark.

* No benchmark exists for total chromium

** This value is for total chromium

EPA U.S. Environmental Protection Agency

ID Identification

J The identification of the analyte is acceptable. The reported value is an estimate.

KDHE Kansas Department of Health and Environment

mg/kg milligrams per kilogram

mg/L milligrams per liter

RCRA Resource Conservation and Recovery Act

RSL Regional Screening Level

TCLP Toxicity characteristic leaching procedure

U The analyte was not detected at or above the reporting limit

UJ The analyte was not detected at or above the reporting limit. The reporting limit is an estimate.

TCLP Regulatory Limits

Sample Name Laboratory Sample IDAnalyte and Result

Total RCRA Metals Results (mg/kg)

TABLE G-1

SUMMARY OF OVERSPRAY MATERIAL ANALYTICAL DATA


TCLP RCRA Metals Results (mg/L)

EPA RSL for Industrial Soil

KDHE Tier 2 Benchmark for Non-Residential Scenario

1,1

-DC

A

Aceto

ne

Ben

zen

e

Ch

loroeth

an

e

cis

-1,2

-DC

E

Cyclo

hexan

e

Eth

yl

Ben

zen

e

Isop

rop

ylb

en

zen

e

m a

nd

/or p

-Xyle

ne

Meth

yl

tert-

bu

tyl

eth

er

Meth

ylc

yclo

hexan

e

o-X

yle

ne

Tetr

ach

loroeth

en

e

Tolu

en

e

Tric

hlo

roeth

en

e

Vin

yl

Ch

lorid

e

TP

H-D

RO

TP

H-O

RO

TP

H-G

RO

GP-1 (1-2) 1/25/2016 1505 7041-101 21 120 J 5.3 U 5.3 U 7.9 15 J 8.3 5.3 U 39 5.3 U 6.7 J 27 5.3 U 16 5.3 U 5.3 - - -

GP-1 (3-4) 1/25/2016 1505 7041-102 12 11 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 5.5 U 7.1 - - -

GP-2 (1-2) 1/25/2016 1615 7041-103 16 27 10 5.0 U 5.2 J 1.30E+03 54 9.2 1.30E+03 5.0 U 23 850 5.0 U 130 5.0 U 5.0 U - - -

GP-2 (7-8) 1/25/2016 1625 7041-104 20 11 U 5.3 U 5.3 U 5.3 UJ 5.3 U 5.3 U 5.3 U 5.3 U 14 5.3 U 5.3 U 5.3 U 5.3 U 5.3 U 6.2 - - -

GP-3 (1-2) 1/26/2016 0815 7041-105 5.2 U 10 U 5.2 U 5.2 U 5.2 UJ 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U - - -

GP-3 (7-8) 1/26/2016 0820 7041-106 5.6 U 11 U 5.6 U 5.6 U 5.6 UJ 5.6 U 5.6 U 5.6 U 5.6 U 5.6 U 5.6 U 5.6 U 5.6 U 5.6 U 5.6 U 5.6 U - - -

GP-4 (1-2) 1/26/2016 0851 7041-107 6.3 U 21 6.3 U 6.3 U 6.3 U 6.3 U 23 6.3 U 42 6.3 U 33 6.3 U 6.3 U 6.3 U 6.3 U 6.3 U - - -

GP-4 (7-8) 1/26/2016 0900 7041-108 6.8 10 U 5.0 U 5.0 U 24 J 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U - - -

GP-5 (1-2) 1/26/2016 0937 7041-109 5.2 U 19 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U 5.2 U - - -

GP-5 (7-8) 1/26/2016 0950 7041-110 5.1 U 9.9 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U - - -

GP-5 (7-8) FD 1/26/2016 0950 7041-110 FD 5.0 U 10 U 5.1 U 5.1 U 5.1 UJ 5.1 U 5.1 U 5.1 U 5.1 U 5.1 U 5.1 U 5.1 U 5.1 U 5.1 U 5.1 U 5.1 U - - -

GP-6 (2-3) 1/26/2016 1028 7041-111 6.2 U 12 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U 6.2 U - - -









GP-10 (3-4) 1/26/2016 1340 7041-201 - - - - - - - - - - - - - - - - 1.08E+04 U 8.67E+04 U 2.24E+03 U


GP-11 (3-4) 1/26/2016 1420 7041-202 - - - - - - - - - - - - - - - - 1.03E+04 U 8.28E+04 U 2.09E+03 U

GP-12 (3-4) 1/26/2016 1454 7041-121 4.5 U 11 4.5 U 17 4.5 U 4.5 U 4.5 U 4.5 U 4.5 U 4.5 U 4.5 U 4.5 U 4.5 U 4.5 U 4.5 U 4.5 U - - -

GP-12 (3-4) 1/26/2016 1454 7041-203 - - - - - - - - - - - - - - - - 2.15E+04 2.01E+05 2.21E+03 U

GP-12 (7-8) 1/26/2016 1458 7041-122 9.9 9.3 U 4.6 U 4.6 U 42 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U 4.6 U - - -





2.00E+03 6.70E+08 5.10E+03 2.30E+07 2.30E+06 3.10E+06 2.50E+04 NE 2.50E+06 2.10E+05 NE 2.80E+06 1.20E+05 4.70E+07 6.00E+03 1.70E+03 6.00E+05 4.20E+05 3.30E+07

7.99E+04 4.06E+08 2.82E+04 2.81E+07 3.87E+04 1.33E+07 1.45E+05 NE 1.41E+06 1.05E+06 NE 1.41E+06 2.10E+05 2.98E+04 9.91E+03 9.21E+03 3.50E+05 9.50E+05 2.75E+07

Notes

°N Degrees north

°W Degrees west

µg/kg Micrograms per kilogram

1,1-DCA 1,1-Dichloroethane

cis-1,2-DCE cis-1,2-Dichloroethene

DPT Direct-push technology

DU Decision Unit


ID Identification

J The identification of the analyte is acceptable; the reported value is an estimate


NE Not established


TCE Trichloroethene

TPH-DRO Total petroleum hydrocarbons-diesel range organics

TPH-GRO Total petroleum hydrocarbons-gasoline range organics

TPH-ORO Total petroleum hydrocarbons-oil range organics


USGS United States Geological Survey

KDHE Tier 2 Risk Based Benchmark for Nonresidential Scenarios

TABLE G-2

SUMMARY OF DPT SOIL SAMPLE ANALYTICAL DATA


East of main Re-Con

building

Northwest of main

Re-Con building

Along west property

boundary

Latitude

(°N)

Longitude

(°W)


37.01468 95.61868

37.01707 95.61816

37.01469 95.61848

Within suspected

TCE source area

Within suspected

Petroleum source

area

95.6179037.01623

95.6180037.01625

95.6180637.01626

37.01613 95.61798

37.01614 95.61806

95.6178437.01607

37.01606 95.61794

37.01607 95.61806

37.01616 95.61788

37.01758 95.61891

37.01715 95.61892

Analyte and Result (µg/kg)

Sample Name Sample DescriptionCollection

Date

Collection

Time

Laboratory

Sample ID

Latitude °N Longitude °W Mercury Arsenic Barium Cadmium Chromium Lead Selenium Silver

DU-1 Soil staining east of main Re-Con building 37.016884 95.618081 7041-1 0.11 U 1.7 52.9 1.2 7.1 36.6 3.1 U 0.89 UJ

7041-2 0.11 U 1.5 30.3 0.69 14.2 141 3.0 U 0.84 UJ

7041-2FD 0.11 U 2.6 63 0.95 12.0 77.1 3.0 U 0.86 UJ

DU-3 West of main Re-Con building 37.017049 95.018820 7041-3 0.12 U 8.5 103 1.4 32.9 140 3.2 U 0.90 UJ

DU-4Waste material covering floor of main Re-Con

building37.017006 95.618749 7041-4 0.73 256 597 22.1 197 256 3.2 U 9.0 UJ

DU-5 West of PrimeTime shop 37.016048 95.618863 7041-5 0.11 U 1.9 94.7 1.3 11.7 82.7 3.3 U 0.94 UJ

DU-6 South of PrimeTime shop 37.015749 95.618417 7041-6 0.12 U 3.2 125 2.6 18.0 151 3.3 U 0.93 UJ

DU-7 Near oil well 37.014789 95.618481 7041-7 0.29 3.8 66.5 4.7 69.4 31.9 3.4 U 0.97 UJ

0.017 7.941 NE NE NE 23.226 0.365 NE

46 3.00 2.25E+05 980 NE* 800 5.80E+03 5.80E+03

20 63.2 2.77E+05 965 111** 1.00E+03 1.02E+04 1.02E+04

Notes

Bolded value indicates analyte exceeds one health-based benchmark

Bolded and shaded value indicates analyte exceeds both health-based benchmarks

* No benchmark exists for total chromium

** This value is for total chromium

°N Degrees north

°W Degrees west

DU Decision Unit


ID Identification


mg/kg Milligrams per kilogram

NE Not established



UJ

USGS United States Geological Survey

The analyte was not detected at or above the reporting limit. The reporting limit is an estimate

USGS Average Background Concentration for Montgomery County

KDHE Tier 2 Risk Based Benchmark for Non-Residential Scenario (soil pathway)


Laboratory

Sample ID

Analyte and Result (mg/kg)

37.017336

TABLE G-3

SUMMARY OF SURFACE SOIL SAMPLE ANALYTICAL DATA


Sample Location

North exterior of main Re-Con building, near

paint boothDU-2 95.618499

Sample

NameSample Description

Documents

Letter submitting Removal Assessment Report with Report Attached · 2020-05-03 · cc Debra Dorsey, START Project Officer (cover letter only) X9025.15.0086.000 415 Oak Street, Kansas