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EPA Region 5 Records Ctr.\ laconi Inc.Bloomington ProjectOne City Centre. Suite 108Bloomington. IN 47404 257160(8)2)334-0030(812)334-7855(Fax)
VIACOMJune 1,2001
BP-01-0044
To: DISTRIBUTION LISTUSEPA Region 5Indiana Department of Environmental ManagementMonroe County Health DepartmentCity of Bloomington Utilities Services BoardTetraTech EM, Inc.Earth Tech
Re: Post-Excavation Groundwater Monitoring Results for March 21,2001;Neal's Landfill, Monroe County, Indiana
This letter summarizes the results of the March 21, 2001 sampling event performed byViacom, Inc. at the Neal's Landfill site. In accordance with interim monitoringrequirements outlined in the Neal's Landfill Statement of Work (SOW) dated March 5,1999, groundwater sampling was performed at the following five locations: South Spring,North Spring, Pig Pen Spring, Taylor Spring Branch and Branam Spring. The generallocations of these natural springs are shown on Figure 1 (attached).
The sampling method involved the collection of grab samples in accordance withapproved procedures outlined in the SOW. The only exception was the sample from PigPen Spring, which was collected from a 4" PVC slotted pipe that intersects a sub-colluvial channel. For this sample an ISCO Model 2900 sampler with a peristaltic pumpwas used.
Routine sampling parameters including temperature and conductivity were measured andrecorded. All samples were labeled and logged onto a chain-of-custody form. Thesamples were stored and transported on ice in insulated coolers. Custody of the watersamples was maintained by Viacom until shipment to the analytical laboratory.
Samples were analyzed by Heritage Lab of Indianapolis, Indiana. The samples wereanalyzed to a detection limit of 0.1 parts per billion (ppb) for all PCB parameters (exceptAroclor 1221; detection limit 0.5 ppb) by EPA Method 608/SW-846 Method 8082.Samples were also analyzed for total suspended solids (TSS) by EPA Method 160.2.
Field measurements, PCB analytical results, and QA/QC results for this monitoring eventare presented in Table 1 (attached). Historical PCB results for individual sampling pointsare presented in Tables 2 through 6.
Distribution ListJune 1,2001Page 2
Copies of the field log, chain-of-custody, laboratory analytical reports and validationstatements for the March samples are also attached.
If you have questions regarding this sampling event or the results reported herein, pleasecall Mike McCann at (812) 334-0030.
Sincerely,
Dorothy M.AlkeTSProject Director
Attachments
DISTRIBUTIONTom Alcamo, USEPA Region 5Jessica Huxhold, IDEMDennis Williamson, Monroe County Health Department
cc:John Langley, CBUV. Rajaram, Tetra Tech EM, Inc.John Bassett, Earth TechMike McCann, ViacomRuss Cepko, ViacomBP FilesProject File 30400.19 GWM
ATTACHMENTS
Post-Excavation Ground Water Monitoring ResultsMarch 21,2001Neal's Landfill
Figure 1 Sample Location MapTables of Spring Sampling ResultsField LogChain-of-CustodyLaboratory Analytical Reports and Data Validation
Meal's LandfillGroundwater Monitoring Locations
South SpringNorth SpringPigpen SpringTaylor Spring BranchBranam Spring
TABLE 1
RESULTS OF SAMPLINGMEAL'S LANDFILL POST-EXCAVATION INTERIM GROUNDWATER MONITORING
March 21,2001
LocationSouth Sp.South Sp.Field BlankNorth Sp.Pig Pen Sp.Taylor Sp. BranchBranam Sp.
Date3/21/013/21/013/21/013/21/013/21/013/21/013/21/01
Sample IDNL1519NL1520NL1521NL1522NL1523NL1524NL1525
PCB(ppb)0.930.92BDL0.31BDLBDLBDL
TSS(mg/L)
106
BDLBDL
3918
Conductivity(uS/cm)
526526
435459546736
Temperature(deg C)
12.312.3
10.810.517.27.8
Comments
DuplicateField Blank
BDL - Below Detection Limit
Table 2
Summary of PCB Samplingat South Spring
Date24-Feb-995-Mar-9912-Mar-9919-Mar-9926-Mar-994-May-9922-Jun-9916-Aug-991-Nov-991-Nov-99
18-Dec-9922-Feb-OO14-Apr-OO14-Apr-OO13-Jun-OO13-Jun-OO15-Aug-OO15-Aug-OO19-Oct-OO19-Oct-OO21-Dec-OO21-Dec-OO27-Feb-0127-Feb-0121-Mar-0121-Mar-01
PCBppb2.01.31.01.61.91.33
2.81.01.12.41.8
0.810.731.62.22.32.41.11.0
0.840.910.830.780.930.92
Comments
Duplicate
Duplicate
Duplicate
Duplicate
Duplicate
Duplicate
Duplicate
Table 3
Summary of PCB Samplingat North Spring
Date24-Feb-995-Mar-9912-Mar-9919-Mar-9926-Mar-994-May-9922-Jun-9911-Aug-99l-Nov-99
18-Dec-9922-Feb-OO14-Apr-OO13-Jun-OO15-Aug-OO19-Oct-OO21-Dec-OO27-Feb-0121-Mar-01
PCBppb0.700.560.250.660.950.631.51.91.22.10.680.291.61.5
0.360.330.230.31
Comments
QA/QC flagged J, estimate
Table 4
Summary of PCB Samplingat Pig Pen Spring
Date24-Feb-995-Mar-9912-Mar-9919-Mar-9926-Mar-994-May-9922-Jun-9911-Aug-991-Nov-99
18-Dec-9922-Feb-OO22-Feb-OO14-Apr-OO13-Jun-OO1 5-Aug-OO19-Oct-OO21-Dec-OO27-Feb-0121-Mar-01
PCBppbBDLBDLBDLBDL ^BDLBDL^BDLBDLBDLBDLBDLBDLBDLBDLBDLBDL
BDLBDL
Comments
Duplicate
Frozen - not sampled
Table 5
Summary of PCB Samplingat Taylor Spring Branch
Date24-Feb-995-Mar-9912-Mar-9919-Mar-9926-Mar-994-May-9922-Jun-9911-Aug-991-Nov-99
18-Dec-9922-Feb-OO14-Apr-OO13-Jun-OO15-Aug-OO19-Oct-OO21-Dec-OO27-Feb-0121-Mar-01
PCBppbBDLBDLBDLBDLBDLBDL
BDLBDL0.11BDL0.18BDLBDLBDLBDLBDL
Comments
DRYDRY
QA/QC flag R, unusable due to contamination
Table 6
Summary of PCB Samplingat Branam Spring
Date24-Feb-995-Mar-9912-Mar-9919-Mar-9926-Mar-994-May-9922-Jun-9911-Aug-991-Nov-9918-Dec-9922-Feb-OO26-Apr-OO13-Jun-OO15-Aug-OO19-Oct-OO21-Dec-OO27-Feb-0121-Mar-01
PCBppbBDLBDLBDLBDLBDLBDLBDL
BDLBDLBDLBDL0.17BDLBDLBDLBDLBDL
Comments
DRY
QA/QC flag R, unusable due to contamination
oun/ircere
HERITAGE ENVII . vN MENTAL SERVICESCOMMERCIAL LABORATORY OPERATIONS
7901 West Morris StreetIndianapolis, Indiana 46231 (317) 243-0811 Fax (317) 466-5095
I - 86680csu
K<5(S
ENVIRONMENTAL PROGRAM:
CWA NPDES IWP-
RCRA MW SW
SDWA.
.SLUDGE.
OTHFR
Sampled by:
ClienlID: Dale: Time: Sample Description
Mat
rix):
. S
oil.
Oil, S
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Analyses Requested(Note special detection limits or methods)
Report To:
Co:Add: frfy
f7</o#
Attn:Phone:
Accelerated Turnaround Requested _(Subject to Additional Change)
Result Request by:Mo Day Vr
[Data must be Accepted and Approved by Lab]
Remarks:UB
Sample No.
XAMPWAMPMAMFM zAMPMAMPM
DuWTlrn* fcewlwdby: (EHr*™™)
RahqulBlwd by; (Sgnibui*) Dula/Thi*
thH/nra
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Dfalribudon: White original and YsUow copy to accompany sample toPink copy (o ba ralalred by dient.
Property Preserved -
Broken Bottles C€»fi
Row ess
Validation Results for the March 2001 Neal's Landfill Spring Water Samples
1. Validation of the following samples has been completed:
o NL 1519-NL 1525
Validation was performed per the requirements for level 4 data in the project QAPjP. This includes acheck for: Holding Time, Calibration, Blank Contamination, Precision, Accuracy, and Accuracy ofNominal Reporting Limits against method requirements. Based on this review, no data qualificationflags are recommended
The QAPjP requires an assessment of the overall data quality with respect to Precision, Accuracy,Representativeness, Completeness and Comparability (PARCC).
o Precision and accuracy: Precision and accuracy were assessed by reviewing the labperformance on lab spiked samples, lab spike duplicates and field duplicates. Allrequirements were met.
o Representativeness: The representativeness requirement involves an assessment of thefield sampling and lab analytical techniques. The field sampling locations andtechniques as well as lab procedures were in accordance with the approved samplingplan and QAPjP. There were no deviations and the representativeness requirement wasmet.
o Completeness: The completeness goal for the project was for all project data to be 90%accepted. Completeness is calculated by dividing the total number of acceptableanalyses by the total performed. An acceptable analysis is defined as one thatconformed to QC protocols and is not rejected. All these sample results were accepted.
o Comparability: All the samples taken, analyzed and validated by Viacom were taken byViacom or its contractors sampling crews using the same procedures as previous samplesat this location. Care should be observed when attempting to trend these results with thehistorical data from a different lab. These samples were analyzed by Heritage labs.Some previous samples from this site were analyzed by Antech Labs.
Overall, the main objective of the sampling event was to determine if PCBs are present at a concentrationof .1 ppb or more. This data is of sufficient quality to satisfy this goal.
C E R T I F I C A T E O F A N A L Y S I S
Service Location
HERITAGE ENVIRONMENTAL SERVICES, LLCCOMMERCIAL LABORATORY OPERATIONS7901 W. MORRIS ST.INDIANAPOLIS, IN 46231(317)243-8304
Received
21-MAR-01Complete
29-MAR-01Printed
29-MAR-01
Project
4602Lab ID
A547959PO Number
BL0177 ***Sampled
21-MAR-01 13:45
Report To
JIM PATRICKCBS CORPORATIONONE CITY CENTRE - SUITE 210P.O. BOX 997BLOOMINGTON, IN 47404-0997
Bill To
ACCOUNTS PAYABLEVIACOM, INC.ONE CITY CENTRE - SUITEBLOOMINGTON, IN 47404
108
CLIENT ID: NL1519MATRIX TYPE: NON-SPECIFIC WATERMATRIX: WSSITE: NEALS LANDFILLSubmitter Code :2226
Sample Description
PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510CAnalyst: R. DOBVNE : Analysis Date: 23-MAR*01 Instrument: PREP Test: P230. 1.0
Parameter
INITIAL WEIGHT OR VOLUMEFINAL VOLUME
Result
940,.:"5:.: ",. '
Det. Limit Units
mLmL
PCB AROCLORS BY GAS CHROMAT06RAPHY/ECD SW846-8082 NELAC:YAnalyst: T. PINCKERT Analysis Date: 24-MAR-01 Instrument: GC/ECD Test: 0301.7.0
Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510CP230. 1.0
Parameter
PCB AROCLOR 1016PCB AROCLOR 1221PCB AROCLOR 1232PCB AROCLOR 1242PCB AROCLOR 1248PCB AROCLOR 1254PCB AROCLOR 1260PCB AROCLOR 1262
SURROGATE RECOVERY
DECACHLOROBIPHENYL (DCB)
Result
BDLBDLBDLBDL0.93BDLBDLBDL
90.0
Det. Limit
0.100.500.100.100.100.100.100.10
Units
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
% RecAroclor 1248 is degraded.
TOTAL PCB CALCULATION HLI3Analyst: T. PINCKERT Analysis Date: 24-MAR-01 Instrument: GC/ECD Test: 0301.3.0
Page 1 (continued on next page)
HERITAGE ENVIRONMENTAL SERVICES, LLC Sample ID: A547959 NL1519
TOTALTOTAL
PCBSPCB
Parameter
DETECTION LIMIT DOES NOT0.
INCLUDE AROCLOR
Result93
Det. Limit
0.10Units
uq/L1221
TOTAL SUSPENDEDAna lyst MCi CRAWFORD
SUSPENDED SOLIDS
SOLIDS EPA 160.Analysis
Parameter
2 NELAC: YDate: 22-MAR-01 19:00 : Test: G403.7.0
Result
10
Det. Limit
1
Unitsmq/L
Sample Comments
Sample was received within 6 hours of sampling.
BDL Below Detection Limit
Sample was received on ice at temperature 7.1 C.All aqueous samples are reported on a wet weight basis unless otherwise noted.Sample chain of custody number 86680.
This Certificate shall not be reproduced, except in full,without the written approval of the lab.The sample results relate only to the analytes of interest testedor to the sample as received by the lab.Heritage Environmental Services, LLC certifies that the test resultsindicated as NELAC (National Environmental Laboratory AccreditationConference) accredited (Yes for NELAC) meet all requirements of NELAC andIllinois EPA Part 186 unless otherwise explained or justified as to thethe exact nature of the deviations.Heritage Environmental Services, LLC is accredited under Illinois NELACaccreditation number 100401.
Additional copies of this report sent to:RUSS CEPKO, CBS CORPORATION11 STANWIX STREET, PITTSBURG, PA 15222-1384
Approved : ^ Vt,..,-.( tfi^A Page 2 (last page)
C E R T I F I C A T E O F A N A L Y S I S
Service Location
HERITAGE ENVIRONMENTAL SERVICES, LLCCOMMERCIAL LABORATORY OPERATIONS7901 W. MORRIS ST.INDIANAPOLIS, IN 46231(317)243-8304
Received
21-MAR-01Complete
29-MAR-01Printed
29-MAR-01
Project
4602Lab ID
A547960PO Number
BL0177 ***Sampled
21-MAR-01 13:45
Report To
JIM PATRICKCBS CORPORATIONONE CITY CENTRE - SUITE 210P.O. BOX 997BLOOMINGTON, IN 47404-0997
Bill To
ACCOUNTS PAYABLEVIACOM, INC.ONE CITY CENTRE - SUITE 108BLOOMINGTON, IN 47404
CLIENT ID: NL1520MATRIX TYPE: NON-SPECIFIC WATERMATRIX: WSSITE: NEALS LANDFILLSubmitter Code :2226
Sample Description
PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTIONAnalyst: RiDCiBYNE Analysis Date: 23-MAR-01
Parameter
INITIAL WEIGHT OR VOLUMEFINAL VOLUME
SW846-3510CInstrument: PREP: ;:;;;;: ;.
Result
950; • ; . . & • • • . • • • • : .
Test: P230.1UC
Det. Limit
'•• '- :-' : - :" " :
Units
mL::mL
PCB ARQCLORS BY GAS CHROMATOGRAPHY/ECD SW846-8082 NELACIYAnalyst: T '.': PfNCKERT Analysis Date: 24-MAR-01 Instrument: GC/ECD Test: 0301.7.0
Prep: RGB :SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION :SWS46-3510C:P230.:1.0
Parameter
PCB AROCLOR 1016PCB AROCLOR 1221PCB AROCLOR 1232PCB AROCLOR 1242PCB AROCLOR 1248PCB AROCLOR 1254PCB AROCLOR 1260PCB AROCLOR 1262
SURROGATE RECOVERY
DECACHLOROBIPHENYL (DCB)
Result
BDLBDLBDLBDL0.92BDLBDLBDL
88.0
Det. Limit
0.100,500.100.100.100.100.100.10
Units
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
% RecAroclor 1248 is degraded.
TOTAL PCB CALCULATION HLI3Analyst: T.PtNCKERT Analysis Date: 24-MAR-01 Instrument: GC/ECD Test: 0301.3.0
Page 1 (continued on next page)
HERITAGE ENVIRONMENTAL SERVICES, LLC Sample ID: A547960 NL1520
TOTALTOTAL
ParameterPCBSPCB DETECTION LIMIT DOES
Result0.92
Det. Limit0.10
Unitsuq/L
NOT INCLUDE AROCLOR 1221
TOTAL SUSPENDEDAnalyst: K,; CRAWFORD
SUSPENDED SOLIDS
SOLIDS EPA 160.Analysis
Parameter
2 NELAC: YDate: 22-MAR^01 19:00 Test: ;G4Q3. 7.0
Result
6Det. Limit
1
Units
mq/L
Sample CommentsSample was received within 6 hours of sampling.
BDL Below Detection Limit
Sample was received on ice at temperature 7.1 C.All aqueous samples are reported on a wet weight basis unless otherwise noted.Sample chain of custody number 86680.
This Certificate shall not be reproduced, except in full,without the written approval of the lab.The sample results relate only to the analytes of interest testedor to the sample as received by the lab.Heritage Environmental Services, LLC certifies that the test resultsindicated as NELAC (National Environmental Laboratory AccreditationConference) accredited (Yes for NELAC) meet all requirements of NELAC andIllinois EPA Part 186 unless otherwise explained or justified as to thethe exact nature of the deviations.Heritage Environmental Services, LLC is accredited under Illinois NELACaccreditation number 100401.
Additional copies of this report sent to:RUSS CEPKO, CBS CORPORATION11 STANWIX STREET, PITTSBURG, PA 15222-1384
Approved : OIL w -.t fty\v\ Page 2 (last page)
C E R T I F I C A T E O F A N A L Y S I S
Service Location
HERITAGE ENVIRONMENTAL SERVICES, LLCCOMMERCIAL LABORATORY OPERATIONS7901 W. MORRIS ST.INDIANAPOLIS, IN 46231(317)243-8304
Received
21-MAR-01Complete
29-MAR-01Printed
29-MAR-01
Project
4602Lab ID
A547961PO Number
BL0177 ***Sampled
21-MAR-01 13:55
Report To
JIM PATRICKCBS CORPORATIONONE CITY CENTRE - SUITE 210P.O. BOX 997BLOOMINGTON, IN 47404-0997
Bill To
ACCOUNTS PAYABLEVIACOM, INC.ONE CITY CENTRE - SUITE 108BLOOMINGTON, IN 47404
CLIENT ID: NL1521MATRIX TYPE: NON-SPECIFIC WATERMATRIX: WSSITE: NEALS LANDFILLSubmitter Code :2226
Sample Description
PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846i3510CAnalyst: R.: DOB YNE Analysis Date: 23-HAR-01 Instrument: PREP Test: P230.1.6
Parameter
INITIAL WEIGHT OR VOLUMEFINAL VOLUME
Result
1000,:>.&' ': ,
Det. Limit Units
mLmL
PCB AROGLORS BY GAS CHROMAT06RAPHY/ECD SW846-8082 NELAC:YAnalyst: T. PtNCJCER'T-' Analysis Date: 24-MAR-01 Instrument: GC/ECD : Test: 0301.7,10
Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510C P230; 1.0
Parameter
PCB AROCLOR 1016PCB AROCLOR 1221PCB AROCLOR 1232PCB AROCLOR 1242PCB AROCLOR 1248PCB AROCLOR 1254PCB AROCLOR 1260PCB AROCLOR 1262
SURROGATE RECOVERY
DECACHLOROBIPHENYL (DCB)
Result
BDLBDLBDLBDLBDLBDLBDLBOL
62.0
Det. Limit
0.100.500.100.100.100.100.100.10
Units
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
% Rec
TOTAL PCB CALCULATION HLI3Analyst: T. P1NCKERT Analysis Date: 24-MAR-01
Parameter
TOTAL PCBS
Instrument: GC/ECD Test:
Result Det. L
BDL
0301.3.0 •••;,, ',,
imit Units
0.10 uq/LTOTAL PCB DETECTION LIMIT DOES NOT INCLUDE AROCLOR 1221
Page 1 (continued on next page)
HERITAGE ENVIRONMENTAL SERVICES, LLC Sample ID; A547961 NL1521TOTAL SUSPENDEDAnalyst: *. CRAWFORD
SUSPENDED SOLIDS
SOLIDS EPA 160.Analysis
Parameter
2 NELAC :YDate: 22-MAR-01 19:00 Test: G403;7.0
Result
BDLDet. Limit
1
Units
mq/L
Sample CommentsSample was received within 6 hours of sampling.
BDL Below Detection Limit
Sample was received on ice at temperature 7.1 C.All aqueous samples are reported on a wet weight basis unless otherwise noted.Sample chain of custody number 86680.
This Certificate shall not be reproduced, except in full,without the written approval of the lab.The sample results relate only to the analytes of interest testedor to the sample as received by the lab.Heritage Environmental Services, LLC certifies that the test resultsindicated as NELAC (National Environmental Laboratory AccreditationConference) accredited (Yes for NELAC) meet all requirements of NELAC andIllinois EPA Part 186 unless otherwise explained or justified as to thethe exact nature of the deviations.Heritage Environmental Services, LLC is accredited under Illinois NELACaccreditation number 100401.
Additional copies of this report sent to:RUSS CEPKO, CBS CORPORATION11 STANUIX STREET, PITTSBURG, PA 15222-1384
Approved : JLLC-l. Page 2 (last page)
C E R T I F I C A T E O F A N A L Y S I S
Service Location
HERITAGE ENVIRONMENTAL SERVICES, LLCCOMMERCIAL LABORATORY OPERATIONS7901 W. MORRIS ST.INDIANAPOLIS, IN 46231(317)243-8304
Received
21-MAR-01Complete
29-MAR-01Printed
29-MAR-01
Project
4602Lab ID
A547962PO Nuntier
BL0177 ***Sampled
21-MAR-01 14:10
Report To
JIM PATRICKCBS CORPORATIONONE CITY CENTRE - SUITE 210P.O. BOX 997BLOOMINGTON, IN 47404-0997
B i l l To
ACCOUNTS PAYABLEVIACOM, INC.ONE CITY CENTRE - SUITE 108BLOOMINGTON, IN 47404
CLIENT ID: NL1522MATRIX TYPE: NON-SPECIFIC WATERMATRIX: WSSITE: NEALS LANDFILLSubmitter Code :2226
Sample Description
PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTIONAnalyst: R. DOBYNE Analysis: bate:;:^3-HAR-'01 %
Parameter
INITIAL WEIGHT OR VOLUMEFINAL VOLUME
SW846-3510CInstrument: PREP
Result
920. ...5- •- ' -
Test: P230.1.C
Det. Limit
> • ' .
Units
mLmL
PCB AROCLORS BY GAS CHROMATOGRAPHY/ECD SW846 -8082 NELAC:YAnalyst: H, WRIGHT .. Analysis Date:;^4-MAR-01 Instrument: GC/ECD Test: 0301.7.0
Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846 -35 IOC P230.1.0
Parameter
PCB AROCLOR 1016PCB AROCLOR 1221PCB AROCLOR 1232PCB AROCLOR 1242PCB AROCLOR 1248PCB AROC LOR 1254PCB AROCLOR 1260PCB AROCLOR 1262
SURROGATE RECOVERY
DECACHLOROBIPHENYL (DCB)
Result
BDLBDLBDLBDL0.31BDLBDLBDL
88.0
Det. Limit
0.100.500.100.100.100 . 100.100.10
Units
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
% RecAroclor 1248 is degraded.
TOTAL PCB CALCULATION HLI3Analyst: M;- WRIGHT Analysis Date: 24-MAR-01 Instrument: GC/ECD Test: 0301.3.0
Page 1 (continued on next page)
HERITAGE ENVIRONMENTAL SERVICES, LLC Sample ID: A547962 NL1522
TOTALTOTAL
PCBSParameter
PCB DETECTION LIMIT DOES NOT0.
INCLUDE AROCLOR
Result
31Det. Limit
0.10Units
uq/L1221
TOTAL SUSPENDEDAnalyst: Kit CRAWFORD
SUSPENDED SOLIDS
SOLIDS EPA 160.Analysis
Parameter
2 NELAC:YDate: 22-MAR-01 19:00 Test: G403.7.0
Result
BDLDet. Limit
1
Units
mq/L
Sample CommentsSample was received within 6 hours of sampling.
BDL Below Detection Limit
Sample was received on ice at temperature 7.1 C.All aqueous samples are reported on a wet weight basis unless otherwise noted.Sample chain of custody number 86680.
This Certificate shall not be reproduced, except in full,without the written approval of the lab.The sample results relate only to the analytes of interest testedor to the sample as received by the lab.Heritage Environmental Services, LLC certifies that the test resultsindicated as NELAC (National Environmental Laboratory AccreditationConference) accredited (Yes for NELAC) meet all requirements of NELAC andIllinois EPA Part 186 unless otherwise explained or justified as to thethe exact nature of the deviations.Heritage Environmental Services, LLC is accredited under Illinois NELACaccreditation number 100401.
Additional copies of this report sent to:RUSS CEPKO, CBS CORPORATION11 STANUIX STREET, PITTSBURG, PA 15222-1384
Approved : L>..C.< Page 2 (last page)
C E R T I F I C A T E O F A N A L Y S I S
Service Location
HERITAGE ENVIRONMENTAL SERVICES, LLCCOMMERCIAL LABORATORY OPERATIONS7901 W. MORRIS ST.INDIANAPOLIS, IN 46231(317)243-8304
Received
21-MAR-01Complete
29-MAR-01Printed
29-MAR-01
Project
4602Lab ID
A547963PO Number
BL0177 ***Sampled
21-MAR-01 14:20
Report To
JIM PATRICKCBS CORPORATIONONE CITY CENTRE - SUITE 210P.O. BOX 997BLOOMINGTON, IN 47404-0997
Bill To
ACCOUNTS PAYABLEVIACOM, INC.ONE CITY CENTRE - SUITE 108BLOOMINGTON, IN 47404
CLIENT ID: NL1523MATRIX TYPE: NON-SPECIFIC WATERMATRIX: WSSITE: NEALS LANDFILLSubmitter Code :2226
Sample Description
PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTIONAnalyst: R. DOBYNE : Analysis Date: 23*MAR-01 ;
Parameter
INITIAL WEIGHT OR VOLUMEFTNfli ' VnillMP "• ••:: ' : ' "' • - '•' • . • '•••" ::::': y'y '::. ::': . +: - :•,•••': .T. . ••• • ' • • ' •
SW846-3510C^instrument: PREP
Result
920•.*:: :.••::-•"• • • ' • . .
Test: P230.i.<
Det. Limit
J
Units
mLml
RGB AROCLORS BY GAS CHROMATOGRAPHY/ECD SW846^8082 NELACrYAnalyst: T. PINCKERT Analysis Date: :. 24*|WR-Ot<:-\;:0-lnstruniBnt: 'GC/ECD Test: 0301.7:0
Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510CP230. 1.0
Parameter
PCB AROCLOR 1016PCB AROCLOR 1221PCB AROCLOR 1232PCB AROCLOR 1242PCB AROCLOR 1248PCB AROCLOR 1254PCB AROCLOR 1260PCB AROCLOR 1262
SURROGATE RECOVERY
DECACHLOROBIPHENYL (DCB)
Result
BDLBDLBDLBDLBDLBDLBDLBDL
90.0
Det. Limit
0.100.500.100.100.100.100.100.10
Units
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
% Rec
TOTAL PCB CALCULATION HL I 3Analyst S.'T. PINCKERT Analysis Date: 24-MAR-01
Parameter
TOTAL PCBS
Instrument: GC/ECD Test:
Result Det. L
BDL
0301 .tiO
imit Units
0.10 uq/LTOTAL PCB DETECTION LIMIT DOES NOT INCLUDE AROCLOR 1221
Page 1 (continued on next page)
HERITAGE ENVIRONMENTAL SERVICES. LLC Sample ID; A547963 NL1523TOTAL SUSPENDED
Analyst: 1C. CRAWFORD
SUSPENDED SOLIDS
SOLIDS EPA 160.; Analysis
Parameter
2 NELAG:YDate: 22-MAR-01 19:00 test: G403.7.0:
Result3
Det. Limit
1Units
mq/L
Sample CommentsSample was received within 6 hours of sampling.
BDL Below Detection Limit
Sample was received on ice at temperature 7.1 C.All aqueous samples are reported on a wet weight basis unless otherwise noted.Sample chain of custody number 86680.
This Certificate shall not be reproduced, except in full,without the written approval of the lab.The sample results relate only to the analytes of interest testedor to the sample as received by the lab.Heritage Environmental Services, LLC certifies that the test resultsindicated as NELAC (National Environmental Laboratory AccreditationConference) accredited (Yes for NELAC) meet all requirements of NELAC andIllinois EPA Part 186 unless otherwise explained or justified as to thethe exact nature of the deviations.Heritage Environmental Services, LLC is accredited under Illinois NELACaccreditation number 100401.
Additional copies of this report sent to:RUSS CEPKO, CBS CORPORATION11 STANUIX STREET, PITTSBURG, PA 15222-1384
Approved : SflTA Page 2 (last page)
C E R T I F I C A T E O F A N A L Y S I S
Service Location
HERITAGE ENVIRONMENTAL SERVICES, LLCCOMMERCIAL LABORATORY OPERATIONS7901 W. MORRIS ST.INDIANAPOLIS, IN 46231(317)243-8304
Received
21-MAR-01Complete
29-MAR-01Printed
29-MAR-01
Project
4602Lab ID
A547964PO Number
BL0177 ***Sampled
21-MAR-01 14:50
Report To
JIM PATRICKCBS CORPORATIONONE CITY CENTRE - SUITE 210P.O. BOX 997BLOOMINGTON, IN 47404-0997
Bill To
ACCOUNTS PAYABLEVIACOM, INC.ONE CITY CENTRE - SUITEBLOOMINGTON, IN 47404
108
CLIENT ID: NL1524MATRIX TYPE: NON-SPECIFIC WATERMATRIX: WSSITE: NEALS LANDFILLSubmitter Code :2226
Sample Description
PCB SEPARATOR* FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510CAnalyst: R. D08YNE Analyst's Date: .i'ZS-HARHJr:: Instrument: PREP Test: P230Vl.O
Parameter
INITIAL WEIGHT OR VOLUMEFINAL VOLUME '.: -. ' , •" '•• , -. •' • --• •,•-••-.•;: •::,-:• ,:;:;•: "S :>:>'
Result
950••-s;. • • ' • • • • •
Det. Limit Units
mLmL
PCB AKOULUK5 bT tiA5 UHKUnAIUtiKAPHY/tbU 5Wb40rbAnalyst: M. WRIGHT Analysis Date: 24rMAR-01 :
Prep: PCB -SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510C
Parameter
PCB AROCLOR 1016PCB AROCLOR 1221PCB AROCLOR 1232PCB AROCLOR 1242PCB AROCLOR 1248PCB AROCLOR 1254PCB AROCLOR 1260PCB AROCLOR 1262
SURROGATE RECOVERY
DECACHLOROBIPHENYL (DCB)
UbZInstrument: GC/ECD
P230.1.0
Result
BDLBDLBDLBDLBDLBDLBDLBDL
86.0
Test: 0301.7.
Det. Limit
0.100.500.100.100.100.100.100.10
Nt LAI. : Y3
Units
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
% Rec
TOTAL PCB CALCULATION HLI3Analyst: M< WRIGHT Analysis Date: 24-MAR-01
Parameter
TOTAL PCBS
Instrument: GC/ECD V Test:
Result Det. L
BDL
0301.3,0
imit Units
0.10 uq/LTOTAL PCB DETECTION LIMIT DOES NOT INCLUDE AROCLOR 1221
Page 1 (continued on next page)
HERITAGE ENVIRONMENTAL SERVICES. LLC Sample ID; A547964 NL1524TOTAL SUSPENDEDAnalyst: <. CRAWFORD
SUSPENDED SOLIDS
SOLIDS EPA 160.Analysis
Parameter
2 ' '. • ::U.'' :"••:.;, ".:.:... • • • • . . • - • . • . • ? . . . ' " • NELAC i YDate: 22 -MAR- 01 19:00 :•• . Test: G4021. 7.0
Result
9Det. Limit
1
Units
mq/L
Sample CommentsSample was received within 6 hours of sampling.
BDL Below Detection Limit
Sample was received on ice at temperature 7.1 C.All aqueous samples are reported on a wet weight basis unless otherwise noted.Sample chain of custody number 86680.
This Certificate shall not be reproduced, except in full,without the written approval of the lab.The sample results relate only to the analytes of interest testedor to the sample as received by the lab.Heritage Environmental Services, LLC certifies that the test resultsindicated as NELAC (National Environmental Laboratory AccreditationConference) accredited (Yes for NELAC) meet all requirements of NELAC andIllinois EPA Part 186 unless otherwise explained or justified as to thethe exact nature of the deviations.Heritage Environmental Services, LLC is accredited under Illinois NELACaccreditation number 100401.
Additional copies of this report sent to:RUSS CEPKO, CBS CORPORATION11 STANWIX STREET, PITTSBURG, PA 15222-1384
Approved : Page 2 (last page)
C E R T I F I C A T E O F A N A L Y S I S
Service Location
HERITAGE ENVIRONMENTAL SERVICES, LLCCOMMERCIAL LABORATORY OPERATIONS7901 W. MORRIS ST.INDIANAPOLIS, IN 46231(317)243-8304
Received
21-MAR-01Complete
29-MAR-01Printed
29-MAR-01
Project
4602Lab ID
A547965PO Number
BL0177 ***Sampled
21-MAR-01 14:55
Report To
JIM PATRICKCBS CORPORATIONONE CITY CENTRE - SUITE 210P.O. BOX 997BLOOMIN6TON, IN 47404-0997
Bill To
ACCOUNTS PAYABLEVIACOM, INC.ONE CITY CENTRE - SUITEBLOOMINGTON, IN 47404
108
CLIENT ID: NL1525MATRIX TYPE: NON-SPECIFIC WATERMATRIX: WSSITE: NEALS LANDFILLSubmitter Code :2226
Sample Description
PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTIONAnalyst: L. JONES Analysis Date: 23-MAR-01
Parameter
INITIAL WEIGHT OR VOLUMEFINAL VOLUME '' "' ' . '•< : • • . - m ^ •>• y^ f . :. ,,,- ;>>:^
SW846-3510CInstrument: PREP
Result
940& •- :
Test: P230.1.C
Det. Limit
)
Units
mLmL
PCB AROCLORS BY GAS CHROMATOGRAPHY/ECD SW846-8082Analyst: "'Hi : WRIGHT Analysis Date: jVHAR-OIS: jhstrument: GC/ECD
Prep; PCB: SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510C P330. 1.0
Parameter
PCB AROCLOR 1016PCB AROCLOR 1221PCB AROCLOR 1232PCB AROCLOR 1242PCB AROCLOR 1248PCB AROCLOR 1254PCB AROCLOR 1260PCB AROCLOR 1262
SURROGATE RECOVERY
DECACHLOROBIPHENYL (DCB)
Result
BDLBDLBDLBDLBDLBDLBDLBDL
94.0
oNELAC:YTest: 0301.7.0
Det. Limit
0.100.500.100.100.100.100.100.10
Units
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
% Rec
TOTAL PCB CALCULATION HLI3Analyst: Hi:; WRIGHT Analysis Date: 24-MAR-01
Parameter
TOTAL PCBS
Instrument: GC/ECD Test:
Result Det. L
BDL
0301.3.0
imit Units
0.10 uq/LTOTAL PCB DETECTION LIMIT DOES NOT INCLUDE AROCLOR 1221
Page 1 (continued on next page)
Vt
HERITAGE ENVIRONMENTAL SERVICES. LLC Sample ID; A547965 NL1525TOTAL SUSPENDED; Aha tyst : Ki fcRAWFORD
SUSPENDED SOLIDS
SOLIDS EPA 160.: Analysis
Parameter
2 " ' " • : , , : • . • •• : . . . . • ' : " " • ' m\3&\\Date: 22-MAR-01 19:00 Test: G4Q3;7,0
Result18
Det. Limit1
Unitsmq/L
Sample CommentsSample was received within 6 hours of sampling.
BDL Below Detection Limit
Sample was received on ice at temperature 7.1 C.ATI aqueous samples are reported on a wet weight basis unless otherwise noted.Sample chain of custody number 86680.
This Certificate shall not be reproduced, except in full,without the written approval of the lab.The sample results relate only to the analytes of interest testedor to the sample as received by the lab.Heritage Environmental Services, LLC certifies that the test resultsindicated as NELAC (National Environmental Laboratory AccreditationConference) accredited (Yes for NELAC) meet all requirements of NELAC andIllinois EPA Part 186 unless otherwise explained or justified as to thethe exact nature of the deviations.Heritage Environmental Services, LLC is accredited under Illinois NELACaccreditation number 100401.
Additional copies of this report sent to:RUSS CEPKO, CBS CORPORATION11 STANUIX STREET, PITTSBURG, PA 15222-1384
Approved : JL' ./ c Q\fyA Page 2 (last page)