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www.amengtest.com
CONSULTANTS
ENVIRONMENTAL
GEOTECHNICAL
MATERIALS
FORENSICS
Lead in Drinking Water Testing Report Jefferson Jr. High School 1200 W. 26th St. Minneapolis, MN 55405
AET Project No. 03-06427
Date:
January 27, 2017
Prepared for:
Minneapolis Public Schools Capital Planning and Project Development (CPPD) 1250 West Broadway 4th Floor North Building Minneapolis, MN 55411
550 Cleveland Avenue North St. Paul, MN 55114Phone 651-659-9001 Toll Free 800-972-6364 Fax 651-659-1379 www.amengtest.com AA/EEO
This document shall not be reproduced, except in full, without written approval from American Engineering Testing, Inc.
CONSULTANTS
ENVIRONMENTAL
GEOTECHNICAL
MATERIALS
FORENSICS
January 27, 2017
Minneapolis Public Schools Capital Planning and Project Development (CPPD) 1250 West Broadway 4th Floor North Building Minneapolis, MN 55411
Attn: Ms. Amy Ennen [email protected]
RE: Lead in Drinking Water Assessment Report Jefferson Jr. High School 1200 W. 26th St. Minneapolis, MN 55405 AET Project No. 03-06427
Dear Ms. Ennen:
American Engineering Testing, Inc. (AET) has completed the Lead in Drinking Water Testing at the Jefferson Jr. High School and the results are presented in the attached report. Our services were conducted on December 22, 2016 and performed according to AET’s Proposal No. 03-06427.
We appreciate your business and the opportunity to have been of service to you. If you have any questions regarding the information in this report or if we can be of additional service, please do not hesitate to contact me.
Sincerely,
Bruce A. Boehm Carlson Senior Environmental Project Manager
Direct: (651) 999-1387 Email: [email protected]
Lead in Drinking Water Testing Jefferson Jr. High – Minneapolis, MN January 27, 2017 AET Project No. 03-06427
AMERICAN ENGINEERING TESTING, INC.
TABLE OF CONTENTS
Page
TABLE OF CONTENTS ................................................................................................................. i EXECUTIVE SUMMARY ........................................................................................................... iii 1.0 INTRODUCTION .................................................................................................................... 1
1.1 BACKGROUND................................................................................................................. 1 1.2 SITE DESCRIPTION ......................................................................................................... 2 1.3 SCOPE OF SERVICES ....................................................................................................... 2 1.4 SAMPLING AND ANALYTICAL METHODOLOGIES ................................................. 2 1.5 REGULATORY REQUIREMENTS .................................................................................. 2
2.0 ANALYTICAL RESULTS ...................................................................................................... 3 2.1 LEAD DRINKING WATER SAMPLE RESULTS ............................................................ 3
3.0 CONCLUSIONS....................................................................................................................... 4 4.0 RECOMMENDATIONS .......................................................................................................... 5 5.0 STANDARD OF CARE ........................................................................................................... 6 APPENDICES A. Diagrams for Samples of Concern B. Analytical Results Summary C. Analytical Laboratory Reports and Chain of Custody D. Laboratory Accreditation, Personnel Certifications E. Sampling Methodologies and Analysis F. Supporting Documents
Page i
Lead in Drinking Water Testing Jefferson Jr. High – Minneapolis, MN January 27, 2017 AET Project No. 03-06427
AMERICAN ENGINEERING TESTING, INC.
EXECUTIVE SUMMARY
American Engineering Testing (AET) was authorized by Ms. Amy Ennen, Planning Design Manager for Minneapolis Public Schools (Client), to conduct lead in drinking water testing at the Jefferson Jr. High School located at 1200 W. 26th Street in Minneapolis, Minnesota (the Site). Services were performed according to AET’s Proposal No. 03-06427, dated October 24, 2016. Todd Lewis, Lead Risk Assessor, and Jake Langstaff, Environmental Technician, conducted the lead inspection and testing on December 22, 2016. The purpose for the lead in drinking water testing was to determine lead concentrations in the drinking water throughout the school, determine a potential source(s) for any lead identified in the system, and recommend methods for reducing the lead exposure. This assessment was limited to the faucets and fountains within the school building. AET collected a total of 204 samples, which were broken down between 122 first-draw and 82 second-draw potable drinking water samples. Laboratory analytical results are provided in Appendix C. Based on the analytical results, a concern for lead exposure exists in some faucets/fountains due to first-draw concentrations above the regulated limit of 20 parts per billion (ppb), or 20 micrograms per liter (µg/L). One faucet/fountain is a concern for lead exposure due to a second-draw concentration above the regulated limit of 20 ppb. AET recommends the following corrective actions to be taken to reduce the potential exposure to lead:
• Continue to follow the twice daily Flush Program.
• Remove/replace the faucets/fountains/fixtures for the following locations:
o Sample 9, Cafeteria Kitchen sink faucet with a concentration of 20.1 ppb.
o Sample 15, Community Partners classroom, left sink faucet with a concentration of 52.7 ppb.
o Sample 17, Community Partners classroom, right sink faucet with a concentration of 22.9 ppb.
o Sample 23, Music Room Office bathroom sink with a concentration of 18.1 ppb.
o Sample 25, Music Room Classroom utility sink faucet with a concentration of 84.9 ppb.
o Sample 33, Classroom 116 bathroom sink faucet with a concentration of 20.1 ppb.
o Sample 34, Classroom 116 bathroom pipes leading to the sink (second draw/flush sample) with a concentration of 38.4 ppb.
Page ii
Lead in Drinking Water Testing Jefferson Jr. High – Minneapolis, MN January 27, 2017 AET Project No. 03-06427
AMERICAN ENGINEERING TESTING, INC.
o Sample 53, Room 102 (Main Office) right bathroom sink faucet with a concentration of 19.1 ppb.
o Sample 66, Classroom 138 sink faucet with a concentration of 63.9 ppb.
o Sample 78, Classroom 128 sink faucet with a concentration of 29.6 ppb.
o Sample 80, Classroom 127 Restroom sink faucet with a concentration of 23.6 ppb.
o Sample 116, Room 204, Media Room sink faucet with a concentration of 66.7 ppb.
o Sample 120, Classroom 208 sink faucet with a concentration of 21 ppb.
o Sample 122, Classroom 210 sink faucet with a concentration of 25 ppb.
o Sample 124, Classroom 212 sink faucet with a concentration of 586 ppb.
o Sample 142, Room 329, Girl’s Restroom handwashing sink faucet with a concentration of 21.1 ppb.
o Sample 144, Classroom 334 middle faucet for the south sink with a concentration of 28 ppb.
o Sample 145, Classroom 334 right faucet for the south sink with a concentration of 25.5 ppb.
• Consider removing/replacing the faucet/fountain/fixture for the following location:
o Sample 54, Hallway Utility Closet Outside Room 102, utility sink faucet with a concentration of 15.5 ppb.
• Consider replacing all faucets/fountains/fixtures throughout the building and the pipes
leading to the bathroom in Classroom 116 to further reduce potential lead in drinking water exposures.
• If any of the above mentioned fixtures are replaced, conduct additional testing following replacement to document and confirm lead in drinking water concentration reduction.
Page iii
Lead in Drinking Water Testing Jefferson Jr. High – Minneapolis, MN January 27, 2017 AET Project No. 03-06427
AMERICAN ENGINEERING TESTING, INC.
1.0 INTRODUCTION
American Engineering Testing (AET) was authorized by Ms. Amy Ennen, Planning Design Manager for Minneapolis Public Schools (Client), to conduct lead in drinking water testing at the Jefferson Jr. High School located at 1200 W. 26th Street in Minneapolis, Minnesota (the Site). Services were performed according to AET’s Proposal No. 03-06427, dated October 24, 2016. Todd Lewis, Lead Risk Assessor, and Jake Langstaff, Environmental Technician, conducted the lead inspection and testing on December 22, 2016. The purpose for the lead in drinking water testing was to determine lead concentrations in the drinking water throughout the school, determine a potential source(s) for any lead identified in the system, and recommend methods for reducing the lead exposure. This assessment was limited to the faucets and fountains within the school building. This report includes analytical results, conclusions, and recommendations. Refer to the Appendices for an introduction to lead, methodologies for lead sampling and analysis, diagrams, laboratory reports, and other supporting documents.
1.1 BACKGROUND
Background information was obtained from an interview and information provided by the Client. Information provided by other parties is assumed accurate unless determined otherwise. The Client provided the last lead in drinking water test results, which were collected by the Minneapolis Environmental Health and Safety and Plumbing Departments on September 26, 1998. They collected samples from 17 locations, following the first-draw protocol, throughout the school and found that 13 of the 17 samples contained lead above the Environmental Protection Agency (EPA) Action Level of 20 parts per billion (ppb). Based on the results they determined that the School needed to remain in the “Flushing Program”, which is an internally developed program, following EPA guidelines, for flushing the drinking water system at the school twice daily in an attempt to reduce lead in drinking water exposures. This program must remain in place until further testing shows a reduction in the first draw lead in drinking water concentrations. At the time of our testing, the Client indicated that they were still following the twice daily flushing program. The Client also indicated that the drinking water system had not been used since the night before, which resulted in the drinking water system being left for a minimum of six hour stagnation, as required by the EPA lead in drinking water sampling guidelines.
Page 1 of 6
Lead in Drinking Water Testing Jefferson Jr. High – Minneapolis, MN January 27, 2017 AET Project No. 03-06427
AMERICAN ENGINEERING TESTING, INC.
1.2 SITE DESCRIPTION
The Jefferson Jr. High School building is a four-story building. AET identified approximately 128 fountains, faucets, and fixtures, which would require sampling and testing as part of this project. 1.3 SCOPE OF SERVICES
AET’s project scope of work includes the following items:
• Collect two water samples at each location; a first draw sample and a flush sample.
• Collect two samples from a faucet, sink or exterior spigot near where the water enters the building to evaluate the lead concentration in the pipe leading from the street to the building.
• Submit the water samples to an accredited laboratory for analyses utilizing appropriate analytical methods.
• Prepare a sample/site diagram.
• Prepare a written report describing our sampling process, outlining the sampling locations, discussing the locations with elevated lead concentrations and identify the source of the contamination based on the analytical results.
1.4 SAMPLING AND ANALYTICAL METHODOLOGIES
Information on sampling methodologies and laboratory analyses are provided in Appendix E. 1.5 REGULATORY REQUIREMENTS
A summary of relevant EPA regulatory requirements are provided in each section. Additional information on lead is available in Appendix F. 1.5.1 Lead in Drinking Water
EPA regulates lead in drinking water in residential buildings and schools. The Occupational Safety and Health Administration (OSHA) or the EPA regulates lead in drinking water in commercial buildings. However, lead in residential potable water sources is used as a guideline in determining if lead in drinking water is acceptable and the basis for recommending corrective actions to reduce lead levels in the drinking water source. EPA recommends lead in residential drinking water be less than 15 ppb or 15 µg/L. In schools, the EPA recommends lead in drinking water to be less than 20 ppb or 20 µg/L. The maximum contaminant level goal (MCLG) is zero. These are the levels determined to be safe by toxicological and biomedical considerations, independent of feasibility.
Page 2 of 6
Lead in Drinking Water Testing Jefferson Jr. High – Minneapolis, MN January 27, 2017 AET Project No. 03-06427
AMERICAN ENGINEERING TESTING, INC.
2.0 ANALYTICAL RESULTS
Analytical results are summarized in this section and in Appendix B. Laboratory reports, analytical results, and chain of custodies are provided in Appendix C. Laboratory accreditation and MN Lead Inspector/Risk Assessor licenses are provided in Appendix D. 2.1 LEAD DRINKING WATER SAMPLE RESULTS
The samples of concern are discussed below. Appendix A contains figures showing the locations of the samples of concern, which are discussed below. The EPA regulates lead levels in school buildings with an Action Level of 20 ppb. Results that exceed 20 ppb require corrective action and results below 20 ppb can be inferred to acceptable based on the EPA regulated limits. However, attention should be paid to samples with results that are approaching 20 ppb as well as to those that exceed 20 ppb. The following first draw samples were found to exceed the EPA Action Level of 20 ppb:
• Sample 9, Cafeteria Kitchen sink faucet with a concentration of 20.1 ppb.
• Sample 15, Community Partners classroom, left sink faucet with a concentration of 52.7 ppb.
• Sample 17, Community Partners classroom, right sink faucet with a concentration of 22.9 ppb.
• Sample 25, Music Room Classroom utility sink faucet with a concentration of 84.9 ppb.
• Sample 33, Classroom 116 bathroom sink faucet with a concentration of 20.1 ppb.
• Sample 66, Classroom 138 sink faucet with a concentration of 63.9 ppb.
• Sample 78, Classroom 128 sink faucet with a concentration of 29.6 ppb.
• Sample 80, Classroom 127 Restroom sink faucet with a concentration of 23.6 ppb.
• Sample 116, Room 204, Media Room sink faucet with a concentration of 66.7 ppb.
• Sample 120, Classroom 208 sink faucet with a concentration of 21 ppb.
• Sample 122, Classroom 210 sink faucet with a concentration of 25 ppb.
• Sample 124, Classroom 212 sink faucet with a concentration of 586 ppb.
• Sample 142, Room 329, Girl’s Restroom handwashing sink faucet with a concentration of 21.1 ppb.
• Sample 144, Classroom 334 middle faucet for the south sink with a concentration of 28 ppb.
Page 3 of 6
Lead in Drinking Water Testing Jefferson Jr. High – Minneapolis, MN January 27, 2017 AET Project No. 03-06427
AMERICAN ENGINEERING TESTING, INC.
• Sample 145, Classroom 334 right faucet for the south sink with a concentration of 25.5 ppb.
The following second draw sample was found to exceed the EPA Action Level of 20 ppb:
• Sample 34, Classroom 116 bathroom pipes leading to the sink (second draw/flush sample) with a concentration of 38.4 ppb.
The following first draw samples were just below the EPA Action Level of 20 ppb and should likely be included as faucets/fixtures that exceed 20 ppb:
• Sample 23, Music Room Office bathroom sink with a concentration of 18.1 ppb.
• Sample 53, Room 102 (Main Office) right bathroom sink faucet with a concentration of 19.1 ppb.
The following sample exceeded the EPA regulated level for residential drinking water, which is 15 ppb. This is a faucet/fixtures that should be evaluated periodically as it is approaching the EPA Action Level of 20 ppb.
• Sample 54, Hallway Utility Closet Outside Room 102, utility sink faucet with a concentration of 15.5 ppb.
Results for samples collected from other sample locations were below the EPA threshold limit of 15.0 ppb. 3.0 CONCLUSIONS
The conclusions in this report are based on information obtained from the Client and the interpretation of the sample results. AET reached the following conclusions:
• The source of the lead, which is causing the elevated lead in drinking water concentrations, appears to be in the fixtures as the samples with results exceeding the EPA Action Level of 20 ppb were all first-draw samples.
• One location, Classroom 166 Bathroom, revealed a source of lead, which is causing the elevated lead in drinking water concentrations, to be in the pipes leading to the bathroom fixture as sample 34, which exceeded the EPA Action Level of 20 ppb, was a second draw/flush sample.
• The samples which exceed 20 ppb appear to be scattered throughout the building.
• All other potable water sources tested below the 15 ppb EPA regulatory level for residential buildings.
Page 4 of 6
Lead in Drinking Water Testing Jefferson Jr. High – Minneapolis, MN January 27, 2017 AET Project No. 03-06427
AMERICAN ENGINEERING TESTING, INC.
4.0 RECOMMENDATIONS
The recommendations provided in this report are limited to available information and the interpretation of the sample results. AET recommends the following:
• Continue to follow the twice daily Flush Program.
• Remove/replace the faucets/fountains/fixtures for the following locations:
o Sample 9, Cafeteria Kitchen sink faucet with a concentration of 20.1 ppb.
o Sample 15, Community Partners classroom, left sink faucet with a concentration of 52.7 ppb.
o Sample 17, Community Partners classroom, right sink faucet with a concentration of 22.9 ppb.
o Sample 23, Music Room Office bathroom sink with a concentration of 18.1 ppb.
o Sample 25, Music Room Classroom utility sink faucet with a concentration of 84.9 ppb.
o Sample 33, Classroom 116 bathroom sink faucet with a concentration of 20.1 ppb.
o Sample 34, Classroom 116 bathroom pipes leading to the sink (second draw/flush sample) with a concentration of 38.4 ppb.
o Sample 53, Room 102 (Main Office) right bathroom sink faucet with a concentration of 19.1 ppb.
o Sample 66, Classroom 138 sink faucet with a concentration of 63.9 ppb.
o Sample 78, Classroom 128 sink faucet with a concentration of 29.6 ppb.
o Sample 80, Classroom 127 Restroom sink faucet with a concentration of 23.6 ppb.
o Sample 116, Room 204, Media Room sink faucet with a concentration of 66.7 ppb.
o Sample 120, Classroom 208 sink faucet with a concentration of 21 ppb.
o Sample 122, Classroom 210 sink faucet with a concentration of 25 ppb.
o Sample 124, Classroom 212 sink faucet with a concentration of 586 ppb.
o Sample 142, Room 329, Girl’s Restroom handwashing sink faucet with a concentration of 21.1 ppb.
o Sample 144, Classroom 334 middle faucet for the south sink with a concentration of 28 ppb.
Page 5 of 6
Lead in Drinking Water Testing Jefferson Jr. High – Minneapolis, MN January 27, 2017 AET Project No. 03-06427
AMERICAN ENGINEERING TESTING, INC.
o Sample 145, Classroom 334 right faucet for the south sink with a concentration of25.5 ppb.
• Consider removing/replacing the faucet/fountain/fixture for the following location:
o Sample 54, Hallway Utility Closet Outside Room 102, utility sink faucet with aconcentration of 15.5 ppb.
• Consider replacing all faucets/fountains/fixtures throughout the building and the pipesleading to the bathroom in Classroom 116 to further reduce potential lead in drinkingwater exposures.
• If any of the above mentioned fixtures are replaced, conduct additional testing followingreplacement to document and confirm lead in drinking water concentration reduction.
5.0 STANDARD OF CARE
The Standard of Care for all professional services performed or furnished by AET are at the level and care used ordinarily exercised by members of the profession practicing under similar conditions at the same time, locality, and cost constraints. The results, findings, conclusions, and recommendations expressed in this report are based on conditions observed during the building survey. The information contained in this report is relevant to the date on which this service was performed. AET provides no warranty, expressed or implied, in connection with the services.
If you have questions about this report or would like to discuss the assessment in more detail, please do not hesitate to contact me at 651-999-1387 or at [email protected].
Sincerely, American Engineering Testing, Inc. American Engineering Testing, Inc.
Bruce A. Boehm Carlson Tyler Boley, GIT Senior Environmental Project Manager Geologist
Page 6 of 6
Figure 1Ground Floor – Sample of Concern Location Diagram
Lead in Drinking Water Testing
Date: 1/23/17 AET Project No.: 03-06427
Jefferson Jr. High School
1200 W. 26th
St.
Minneapolis, MN
Scale: Not to Scale
Legend
### – Sample of Concern
9
15
17
2325
Figure 2First Floor – Sample of Concern Location Diagram
Lead in Drinking Water Testing
Date: 1/23/17 AET Project No.: 03-06427
Jefferson Jr. High School
1200 W. 26th
St.
Minneapolis, MN
Scale: Not to Scale
Legend
### – Sample of Concern
33,
34
53
54
66
78
80
Figure 3Second Floor – Sample of Concern Location Diagram
Lead in Drinking Water Testing
Date: 1/23/17 AET Project No.: 03-06427
Jefferson Jr. High School
1200 W. 26th
St.
Minneapolis, MN
Scale: Not to Scale
Legend
### – Sample of Concern
116120122
124
Figure 4Third Floor – Sample of Concern Location Diagram
Lead in Drinking Water Testing
Date: 1/23/17 AET Project No.: 03-06427
Jefferson Jr. High School
1200 W. 26th
St.
Minneapolis, MN
Scale: Not to Scale
Legend
### – Sample of Concern
142
144,
145
ResultsLab
NumberLocation/Room Draw Fixture
Location Description Room Type Draw Type of Fixture
Plumbing Concern
ug/L (ppb) Limit is 20 ppb
1 M FD S Mechanical Rm. Bathroom first draw sink Fixture 0.21
2 M SD S Mechanical Rm. Mechanical Rm.second draw sink
Street to Building Pipe 0.19
3 B FD S Boiler Rm. Main first draw faucet Fixture 0.86
4 B SD S Boiler Rm. Mainsecond draw faucet
Pipes to Fixture 0.5
5 BW FD F Boiler Rm. Main first draw wash station Fixture 1.5
6 BW SD F Boiler Rm. Mainsecond draw wash station
Pipes to Fixture 0.86
7 M FD UF Mechanical Rm. Utility Rm. first draw utility faucet Fixture 0.85
8 M SD UF Mechanical Rm. Utility Rm.second draw utility faucet
Pipes to Fixture 0.86
9 C FD S Cafeteria Main first draw sink Fixture 20.1
10 C SD S Cafeteria Mainsecond draw sink
Pipes to Fixture 4.6
11 C FD DF Cafeteria Main first drawdrinking fountain Fixture 1.2
12 C SD DF Cafeteria Mainsecond draw
drinking fountain
Pipes to Fixture 1.3
13 C FD 2S Cafeteria Main first draw second sink Fixture 3.1
14 C SD 2S Cafeteria Mainsecond draw second sink
Pipes to Fixture 3.2
15 CP FD FLCommunity Partners classroom first draw left faucet Fixture 52.7
16 CP FD FMCommunity Partners classroom first draw middle faucet Fixture 5.4
17 CP FD FRCommunity Partners classroom first draw right faucet Fixture 22.9
Sample Descripton Sample NumberJefferson Jr. High Lead Assessment Data
AET Project No. 03-06427 Page B1 of 16
ResultsLab
NumberLocation/Room Draw Fixture
Location Description Room Type Draw Type of Fixture
Plumbing Concern
ug/L (ppb) Limit is 20 ppb
Sample Descripton Sample Number
18 CP SD FRCommunity Partners classroom
second draw right faucet
Pipes to Fixture 1.5
19 CP FD SACommunity Partners bathroom first draw faucet for sink Fixture 2.1
20 MU FD S Music Rm. classroom first draw faucet for sink Fixture 6.121 MU FD SF Music Rm. classroom first draw sink fountain Fixture 2.2
22 MU SD SF Music Rm. classroomsecond draw sink fountain
Pipes to Fixture 4.3
23 MUO FD SA Music Rm. Office bathroom first draw faucet for sink Fixture 18.1
24 MUO SD SA Music Rm. Office bathroomsecond draw faucet for sink
Pipes to Fixture 5.3
25 MU FD US Music Rm. classroom first draw utility sink Fixture 84.9
26 MU SD US Music Rm. classroomsecond draw utility sink
Pipes to Fixture 5.3
27 122 FD SA 122 bathroom first draw faucet for sink Fixture 14.8
28 122 SD SA 122 bathroomsecond draw faucet for sink
Pipes to Fixture 0.26
29 120 FD S 120 classroom first draw faucet for sink Fixture 4.5
30 120 SD S 120 classroomsecond draw faucet for sink
Pipes to Fixture 0.27
31 116 FD S 116 classroom first draw faucet for sink Fixture 11.9
32 116 SD S 116 classroomsecond draw faucet for sink
Pipes to Fixture 2.2
33 116 FD SA 116 bathroom first draw faucet for sink Fixture 20.1
AET Project No. 03-06427 Page B2 of 16
ResultsLab
NumberLocation/Room Draw Fixture
Location Description Room Type Draw Type of Fixture
Plumbing Concern
ug/L (ppb) Limit is 20 ppb
Sample Descripton Sample Number
34 116 SD SA 116 bathroomsecond draw faucet for sink
Pipes to Fixture 38.4
35 112 FD S 112 classroom first draw faucet for sink Fixture 12.8
36 112 SD S 112 classroomsecond draw faucet for sink
Pipes to Fixture 2
37 112 FD SA 112 bathroom first draw faucet for sink Fixture 3.6
38 112 SD SA 112 bathroomsecond draw faucet for sink
Pipes to Fixture 0.78
39 110 FD S 110 classroom first draw faucet for sink Fixture 3.4
40 110 SD S 110 classroomsecond draw faucet for sink
Pipes to Fixture 1.5
41 110 FD SA 110 bathroom first draw faucet for sink Fixture 0.82
42 110 SD SA 110 bathroomsecond draw faucet for sink
Pipes to Fixture 0.75
43 108 FD S 108 classroom first draw faucet for sink Fixture 15
44 108 SD S 108 classroomsecond draw faucet for sink
Pipes to Fixture 1
45 107 FD S 107 classroom first draw faucet for sink Fixture 1.5
46 107 SD S 107 classroomsecond draw faucet for sink
Pipes to Fixture 0.22
47 H106 FD DF Outside 106 hallway first drawdrinking fountain Fixture 0.14
48 H106 SD DF Outside 106 hallwaysecond draw
drinking fountain
Pipes to Fixture
None Detect (ND)
AET Project No. 03-06427 Page B3 of 16
ResultsLab
NumberLocation/Room Draw Fixture
Location Description Room Type Draw Type of Fixture
Plumbing Concern
ug/L (ppb) Limit is 20 ppb
Sample Descripton Sample Number
49 106 FD S 106 classroom first draw faucet for sink Fixture 0.56
50 106 SD S 106 classroomsecond draw faucet for sink
Pipes to Fixture 0.2
51 102 FD SA 102 (Main Off.) left bathroom first draw faucet for sink Fixture 9.6
52 102 SD SA 102 (Main Off.) left bathroomsecond draw faucet for sink
Pipes to Fixture 2.1
53 102 FD SB 102 (Main Off.) right bathroom first draw faucet for sink Fixture 19.154 H102 FD US Outside 102 hallway first draw utility sink Fixture 15.5
55 H102 SD US Outside 102 hallwaysecond draw utility sink
Pipes to Fixture 0.65
56 H102 FD DF Outside 102 hallway first drawdrinking fountain Fixture 0.33
57 H102 SD DF Outside 102 hallwaysecond draw
drinking fountain
Pipes to Fixture 0.11
58 102C FD S 102C classroom first draw faucet for sink Fixture 5.4
59 102C SD S 102C classroomsecond draw faucet for sink
Pipes to Fixture 1.3
60 TRH106 FD S Teachers RR bathroom first draw faucet for sink Fixture 0.54
61 TRH106 SD S Teachers RR bathroomsecond draw faucet for sink
Pipes to Fixture 0.34
62 101 FD S 101 (Health Off.) main first draw faucet for sink Fixture 6.6
63 101 SD S 101 (Health Off.) Mainsecond draw faucet for sink
Pipes to Fixture 1.2
64 101 FD SA 101 (Health Off.) bathroom first draw faucet for sink Fixture 7.2
AET Project No. 03-06427 Page B4 of 16
ResultsLab
NumberLocation/Room Draw Fixture
Location Description Room Type Draw Type of Fixture
Plumbing Concern
ug/L (ppb) Limit is 20 ppb
Sample Descripton Sample Number
65 101 SD SA 101 (Health Off.) bathroomsecond draw faucet for sink
Pipes to Fixture 2.1
66 138 FD S 138 classroom first draw faucet for sink Fixture 63.9
67 138 SD S 138 classroomsecond draw faucet for sink
Pipes to Fixture 1.1
68 134 FD S 134 classroom first draw faucet for sink Fixture 14.2
69 134 SD S 134 classroomsecond draw faucet for sink
Pipes to Fixture 2
70 132 FD S 132 classroom first draw faucet for sink Fixture 8.4
71 132 SD S 132 classroomsecond draw faucet for sink
Pipes to Fixture 0.96
72 130 FD DF 130 classroom first drawdrinking fountain Fixture 9.7
73 130 SD DF 130 classroomsecond draw
drinking fountain
Pipes to Fixture 1.5
74 H129 FD DFHallway Outside
129 hallway first drawdrinking fountain Fixture 2.1
75 H129 SD DFHallway Outside
129 hallwaysecond draw
drinking fountain
Pipes to Fixture 0.74
76 129 FD HWA 129 girls restroom first drawhand washing
station Fixture 0.98
77 129 SD HWA 129 girls restroomsecond draw
hand washing station
Pipes to Fixture 0.69
78 128 FD S 128 classroom first draw faucet for sink Fixture 29.6
AET Project No. 03-06427 Page B5 of 16
ResultsLab
NumberLocation/Room Draw Fixture
Location Description Room Type Draw Type of Fixture
Plumbing Concern
ug/L (ppb) Limit is 20 ppb
Sample Descripton Sample Number
79 128 SD S 128 classroomsecond draw faucet for sink
Pipes to Fixture 4.4
80 127 FD SA 127 classroom w/ rr first draw faucet for sink Fixture 23.6
81 127 SD SA 127 classroom w/ rrsecond draw faucet for sink
Pipes to Fixture 1.8
82 H127 FD US H127 janitors closet first draw utility sink Fixture 0.55
83 H127 SD US H127 janitors closetsecond draw utility sink
Pipes to Fixture ND
84 123 FD SA 123 classroom w/ rr first draw faucet for sink Fixture 0.41
85 123 SD SA 123 classroom w/ rrsecond draw faucet for sink
Pipes to Fixture 0.16
86 121 FD HWA 121 boys restroom first drawhand washing
station Fixture 2.6
87 121 SD HWA 121 boys restroomsecond draw
hand washing station
Pipes to Fixture 1.5
88 H121 FD DF1Hallway Outside
121 hallway
first draw (sample 87 is second draw as these are back to
back)
lower drinking fountain Fixture 0.15
89 H121 FD DF2Hallway Outside
121 hallway
first draw (sample 87 is second draw as these are back to
back)
upper drinking fountain Fixture ND
90 H221 FD DF1Hallway Outide
221 hallway first drawlower drinking
fountain Fixture 0.47
AET Project No. 03-06427 Page B6 of 16
ResultsLab
NumberLocation/Room Draw Fixture
Location Description Room Type Draw Type of Fixture
Plumbing Concern
ug/L (ppb) Limit is 20 ppb
Sample Descripton Sample Number
91 H221 FD DF2Hallway Outide
221 hallway first drawupper drinking
fountain Fixture 0.54
92 H221 SD DF1Hallway Outide
221 hallwaysecond draw
lower drinking fountain
Pipes to Fixture 0.12
93 221 FD HWA 221 room 128
first draw (sample 92 is second draw as these are back to
back)
hand washing station Fixture 1.8
94 223 FD SA 223 workroom rr first draw faucet for sink Fixture 1.4
95 223 SD SA 223 workroom rrsecond draw faucet for sink
Pipes to Fixture 0.64
96A H225 FD USHallway Outside
225 hallway first draw utility sink Fixture 1.5
96B H225 SD USHallway Outside
225 hallwaysecond draw utility sink
Pipes to Fixture ND
97 H229 FD DF1Hallway Outside
229 hallway first drawlower drinking
fountain Fixture 1.3
98 H229 FD DF2Hallway Outside
229 hallway first drawupper drinking
fountain Fixture 0.91
99 H229 SD DF2Hallway Outside
229 hallwaysecond draw
upper drinking fountain
Pipes to Fixture 0.54
100 229 FD HWA 229 girls restroom
first draw (sample 99 is second draw as these are back to
back)
hand washing station Fixture 1.1
AET Project No. 03-06427 Page B7 of 16
ResultsLab
NumberLocation/Room Draw Fixture
Location Description Room Type Draw Type of Fixture
Plumbing Concern
ug/L (ppb) Limit is 20 ppb
Sample Descripton Sample Number
101 228 FD S 228 staff room first draw faucet for sink Fixture 3
102 228 SD S 228 staff roomsecond draw faucet for sink
Pipes to Fixture 1.3
103 228 FD HWA 228 staff room first drawhand washing
station Fixture 2.5
104 228 SD HWA 228 staff roomsecond draw
hand washing station
Pipes to Fixture 2.2
105 234 FD S 234 classroom first draw faucet for sink Fixture 0.61106 234 FD SF 234 classroom first draw sink fountain Fixture 0.12
107 234 SD S 234 classroomsecond draw faucet for sink
Pipes to Fixture 0.18
108 236 FD S 236 classroom first draw faucet for sink Fixture 0.42109 236 FD SF 236 classroom first draw sink fountain Fixture 0.78
110 236 SD S 236 classroomsecond draw faucet for sink
Pipes to Fixture 0.31
111 238 FD S 238 classroom first draw faucet for sink Fixture 0.48112 238 FD SF 238 classroom first draw sink fountain Fixture 0.65
113 238 SD S 238 classroomsecond draw faucet for sink
Pipes to Fixture 0.35
114 H202 FD DFHallway Outside
202 hallway first drawdrinking fountain Fixture 0.41
115 H202 SD DFHallway Outside
202 hallwaysecond draw
drinking fountain
Pipes to Fixture 0.16
116 204 FD S 204 media room first draw faucet for sink Fixture 66.7
AET Project No. 03-06427 Page B8 of 16
ResultsLab
NumberLocation/Room Draw Fixture
Location Description Room Type Draw Type of Fixture
Plumbing Concern
ug/L (ppb) Limit is 20 ppb
Sample Descripton Sample Number
117 204 SD S 204 media roomsecond draw faucet for sink
Pipes to Fixture 10.8
118 H207 FD DFHallway Across
From 207 hallway first drawdrinking fountain Fixture 0.56
119 H207 SD DFHallway Across
From 207 hallwaysecond draw
drinking fountain
Pipes to Fixture 0.19
120 208 FD S 208 classroom first draw faucet for sink Fixture 21
121 208 SD S 208 classroomsecond draw faucet for sink
Pipes to Fixture 2.4
122 210 FD S 210 classroom first draw faucet for sink Fixture 25
123 210 SD S 210 classroomsecond draw faucet for sink
Pipes to Fixture 5.2
124 212 FD S 212 classroom first draw faucet for sink Fixture 586
125 212 SD S 212 classroomsecond draw faucet for sink
Pipes to Fixture 11.1
126 216 FD S 216 classroom first draw faucet for sink Fixture 8.5
127 216 SD S 216 classroomsecond draw faucet for sink
Pipes to Fixture 0.8
128 220 FD S 220 classroom first draw faucet for sink Fixture 9
129 220 SD S 220 classroomsecond draw faucet for sink
Pipes to Fixture 0.65
130 H321 FD DF1Hallway Outside
321 hallway first drawlower drinking
fountain Fixture 0.48
AET Project No. 03-06427 Page B9 of 16
ResultsLab
NumberLocation/Room Draw Fixture
Location Description Room Type Draw Type of Fixture
Plumbing Concern
ug/L (ppb) Limit is 20 ppb
Sample Descripton Sample Number
131 H321 FD DF2Hallway Outside
321 hallway first drawupper drinking
fountain Fixture 0.37
132 H321 SD DF2Hallway Outside
321 hallwaysecond draw
upper drinking fountain
Pipes to Fixture 0.13
133 321 FD HWA 321 classroom
first draw (sample 132 is second draw as these are back to
back)
hand washing station Fixture 2.1
134 TRH321 FD S TRH321 teachers rr first draw faucet for sink Fixture 0.57
135 TRH321 SD S TRH321 teachers rrsecond draw faucet for sink
Pipes to Fixture 0.2
136 322 FD S 322 classroom first draw faucet for sink Fixture 2.1
137 322 SD S 322 classroomsecond draw faucet for sink
Pipes to Fixture 2.2
138 327 FD S 327 classroom first draw faucet for sink Fixture 8.1
139 327 SD S 327 classroomsecond draw faucet for sink
Pipes to Fixture 1.1
140 H329 FD DFHallway Outside
329 hallway first drawdrinking fountain
Pipes to Fixture 5.3
141 H329 SD DFHallway Outside
329 hallwaysecond draw
drinking fountain Fixture 4.1
142 329 FD HWA 329 girls restroom
first draw (sample 141 is second draw as these are back to
back) faucet for sink Fixture 21.1
AET Project No. 03-06427 Page B10 of 16
ResultsLab
NumberLocation/Room Draw Fixture
Location Description Room Type Draw Type of Fixture
Plumbing Concern
ug/L (ppb) Limit is 20 ppb
Sample Descripton Sample Number
143 334 FD SSL 334 classroom first drawleft faucet for south sink
Pipes to Fixture 6.9
144 334 FD SSM 334 classroom first drawmiddle faucet for south sink Fixture 28
145 334 FD SSR 334 classroom first drawright faucet for south sink Fixture 25.5
146 334 FD SNL 334 classroom first drawleft faucet for north sink Fixture 8.4
147 334 FD SNM 334 classroom first drawmiddle faucet for north sink Fixture 9.9
148 334 FD SNR 334 classroom first drawright faucet for north sink Fixture 6.9
149 334 SD SNR 334 classroomsecond draw
right faucet for north sink
Pipes to Fixture 5.8
150 336 FD SSL 336 classroom first drawleft faucet for south sink
Pipes to Fixture 3.7
151 336 FD SSM 336 classroom first drawmiddle faucet for south sink Fixture 2.8
152 336 FD SSR 336 classroom first drawright faucet for south sink Fixture 3.2
153 336 FD SNL 336 classroom first drawleft faucet for north sink Fixture 1.3
154 336 FD SNM 336 classroom first drawmiddle faucet for north sink Fixture 0.9
155 336 FD SNR 336 classroom first drawright faucet for north sink Fixture 1.3
AET Project No. 03-06427 Page B11 of 16
ResultsLab
NumberLocation/Room Draw Fixture
Location Description Room Type Draw Type of Fixture
Plumbing Concern
ug/L (ppb) Limit is 20 ppb
Sample Descripton Sample Number
156 336 SD SNR 336 classroomsecond draw
right faucet for north sink
Pipes to Fixture 0.36
157 302 FD SSWW 302 classroom first drawwest faucet for southwest sink Fixture 0.86
158 302 FD SSWE 302 classroom first draweast faucet for southwest sink Fixture 2
159 302 SD SSWE 302 classroomsecond draw
east faucet for southwest sink
Pipes to Fixture 0.27
160 302 FD SWW 302 classroom first drawwest faucet for
west sink Fixture 1.9
161 302 FD SWE 302 classroom first draweast faucet for
west sink Fixture 4.6
162 302 SD SWW 302 classroomsecond draw
west faucet for west sink
Pipes to Fixture 0.4
163 302 FD SNWW 302 classroom first drawwest faucet for northwest sink Fixture 0.98
164 302 FD SNWE 302 classroom first draweast faucet for northwest sink Fixture 2.9
AET Project No. 03-06427 Page B12 of 16
ResultsLab
NumberLocation/Room Draw Fixture
Location Description Room Type Draw Type of Fixture
Plumbing Concern
ug/L (ppb) Limit is 20 ppb
Sample Descripton Sample Number
165 302 SD SNWE 302 classroomsecond draw
east faucet for northwest sink
Pipes to Fixture 0.46
166 302 FD SSEW 302 classroom first drawwest faucet for southeast sink Fixture 1.1
167 302 FD SSEE 302 classroom first draweast faucet for southeast sink Fixture 1.4
168 302 SD SSEE 302 classroomsecond draw
east faucet for southeast sink
Pipes to Fixture 0.41
169 302 FD SEW 302 classroom first drawwest faucet for south sink Fixture 1.4
170 302 FD SEE 302 classroom first draweast faucet for south sink Fixture 1.9
171 302 SD SEE 302 classroomsecond draw
east faucet for south sink
Pipes to Fixture 0.3
172 302 FD SNEW 302 classroom first drawwest faucet for northeast sink Fixture 5.1
173 302 FD SNEE 302 classroom first draweast faucet for northeast sink Fixture 4.1
174 302 SD SNEE 302 classroomsecond draw
east faucet for northeast sink
Pipes to Fixture 0.73
175 302 FD SE 302 classroom first drawfaucet for east
sink Fixture 0.2
AET Project No. 03-06427 Page B13 of 16
ResultsLab
NumberLocation/Room Draw Fixture
Location Description Room Type Draw Type of Fixture
Plumbing Concern
ug/L (ppb) Limit is 20 ppb
Sample Descripton Sample Number
176 302 SD SE 302 classroomsecond draw
faucet for east sink
Pipes to Fixture ND
177 302 FD SN 302 classroom first drawfaucet for north sink Fixture 1
178 302 SD SN 302 classroomsecond draw
faucet for north sink
Pipes to Fixture 0.26
179 302 FD SNN 302 classroom first drawnorth faucet for north sink Fixture 2.6
180 302 FD SNS 302 classroom first drawsouth faucet for north sink Fixture 11.9
181 302 SD SNS 302 classroomsecond draw
south faucet for north sink
Pipes to Fixture 0.22
182 302PREP FD S 302PREP prep room first draw sink Fixture 4.1
183 302PREP SD S 302PREP prep roomsecond draw sink
Pipes to Fixture 1
184 304 FD SNWW 304 classroom first drawwest faucet for northwest sink Fixture 1.6
185 304 FD SNWE 304 classroom first draweast faucet for northwest sink Fixture 1.1
186 304 SD SNWE 304 classroomsecond draw
east faucet for northwest sink
Pipes to Fixture 0.37
187 304 FD SWW 304 classroom first drawwest faucet for
west sink Fixture 0.5
188 304 FD SWE 304 classroom first draweast faucet for
west sink Fixture 1.1
AET Project No. 03-06427 Page B14 of 16
ResultsLab
NumberLocation/Room Draw Fixture
Location Description Room Type Draw Type of Fixture
Plumbing Concern
ug/L (ppb) Limit is 20 ppb
Sample Descripton Sample Number
189 304 SD SWE 304 classroomsecond draw
east faucet for west sink
Pipes to Fixture 0.46
190 304 FD SSWW 304 classroom first drawwest faucet for southwest sink Fixture 1.5
191 304 FD SSWE 304 classroom first draweast faucet for southwest sink Fixture 2.3
192 304 SD SSWE 304 classroomsecond draw
east faucet for southwest sink
Pipes to Fixture 0.64
193 304 FD SEW 304 classroom first drawwest faucet for
east sink Fixture 1.1
194 304 FD SEE 304 classroom first draweast faucet for
east sink Fixture 0.8
195 304 SD SEE 304 classroomsecond draw
east faucet for southeast sink
Pipes to Fixture 0.27
196 304 FD SSN 304 classroom first drawnorth faucet for south sink Fixture 2.5
197 304 FD SSS 304 classroom first drawsouth faucet for south sink Fixture 1.4
198 304 SD SSS 304 classroomsecond draw
south faucet for south sink
Pipes to Fixture 0.38
199 304 FD SS 304 classroom first drawfaucet for south sink Fixture 0.36
200 304 SD SS 304 classroomsecond draw
faucet for south sink
Pipes to Fixture 0.12
AET Project No. 03-06427 Page B15 of 16
ResultsLab
NumberLocation/Room Draw Fixture
Location Description Room Type Draw Type of Fixture
Plumbing Concern
ug/L (ppb) Limit is 20 ppb
Sample Descripton Sample Number
201 304 FD SE 304 classroom first drawfaucet for east
sink Fixture 0.97
202 304 SD SE 304 classroomsecond draw
faucet for east sink
Pipes to Fixture 0.31
203 H306 FD DFHallway Outside
306 hallway first drawdrinking fountain Fixture 0.28
204 H306 SD DFHalway Outside
306 hallwaysecond draw
drinking fountain
Pipes to Fixture 0.18
A ‐ Bathroom 1HW ‐ Handwashing
B ‐ Bathroom 2
LEGENDFD ‐ First DrawSD ‐ Second Draw/Flush Sample
FM ‐ Faucet MiddleFL ‐ Faucet LeftUS ‐ Utility SinkUF ‐ Utility Faucet (no sink)SA‐ Bathroom Sink
F‐ FountainDF ‐ Drinking FountainM ‐ Mechanical RoomB ‐ Boiler RoomC ‐ CafeteriaCP ‐ Community Partners
FR ‐ Faucet RightS ‐ Sink Faucet
AET Project No. 03-06427 Page B16 of 16
#=CL#
December 30, 2016
LIMS USE: FR - BRUCE CARLSON
LIMS OBJECT ID: 10374222
10374222
Project:
Pace Project No.:
RE:
Bruce Boehm CarlsonAmerican Engineer Testing550 Cleveland Avenue NorthSaint Paul, MN 55114
03-06427 Jefferson Pb Water
Dear Bruce Carlson:
Enclosed are the analytical results for sample(s) received by the laboratory on December 23, 2016.The results relate only to the samples included in this report. Results reported herein conform to themost current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kabor Xiong
Project Manager
Enclosures
cc: Todd Lewis, American Engineering Testing
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 1 of 245
AET Project No.03-06427 Page C1 of 245
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Minnesota Certification IDs
1700 Elm Street SE Suite 200, Minneapolis, MN 55414
Alaska Certification UST-107
525 N 8th Street, Salina, KS 67401
A2LA Certification #: 2926.01
Alaska Certification #: UST-078
Alaska Certification #MN00064
Alabama Certification #40770
Arizona Certification #: AZ-0014
Arkansas Certification #: 88-0680
California Certification #: 01155CA
Colorado Certification #Pace
Connecticut Certification #: PH-0256
EPA Region 8 Certification #: 8TMS-L
Florida/NELAP Certification #: E87605
Guam Certification #:14-008r
Georgia Certification #: 959
Georgia EPD #: Pace
Idaho Certification #: MN00064
Hawaii Certification #MN00064
Illinois Certification #: 200011
Indiana Certification#C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky Dept of Envi. Protection - DW #90062
Kentucky Dept of Envi. Protection - WW #:90062
Louisiana DEQ Certification #: 3086
Louisiana DHH #: LA140001
Maine Certification #: 2013011
Maryland Certification #: 322
Michigan DEPH Certification #: 9909
Minnesota Certification #: 027-053-137
Mississippi Certification #: Pace
Montana Certification #: MT0092
Nevada Certification #: MN_00064
Nebraska Certification #: Pace
New Jersey Certification #: MN-002
New York Certification #: 11647
North Carolina Certification #: 530
North Carolina State Public Health #: 27700
North Dakota Certification #: R-036
Ohio EPA #: 4150
Ohio VAP Certification #: CL101
Oklahoma Certification #: 9507
Oregon Certification #: MN200001
Oregon Certification #: MN300001
Pennsylvania Certification #: 68-00563
Puerto Rico Certification
Saipan (CNMI) #:MP0003
South Carolina #:74003001
Texas Certification #: T104704192
Tennessee Certification #: 02818
Utah Certification #: MN000642013-4
Virginia DGS Certification #: 251
Virginia/VELAP Certification #: Pace
Washington Certification #: C486
West Virginia Certification #: 382
West Virginia DHHR #:9952C
Wisconsin Certification #: 999407970
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 2 of 245
AET Project No.03-06427 Page C2 of 245
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Lab ID Sample ID Matrix Date Collected Date Received
10374222001 1 Water 12/22/16 00:00 12/23/16 12:15
10374222002 2 Water 12/22/16 00:00 12/23/16 12:15
10374222003 3 Water 12/22/16 00:00 12/23/16 12:15
10374222004 4 Water 12/22/16 00:00 12/23/16 12:15
10374222005 5 Water 12/22/16 00:00 12/23/16 12:15
10374222006 6 Water 12/22/16 00:00 12/23/16 12:15
10374222007 7 Water 12/22/16 00:00 12/23/16 12:15
10374222008 8 Water 12/22/16 00:00 12/23/16 12:15
10374222009 9 Water 12/22/16 00:00 12/23/16 12:15
10374222010 10 Water 12/22/16 00:00 12/23/16 12:15
10374222011 11 Water 12/22/16 00:00 12/23/16 12:15
10374222012 12 Water 12/22/16 00:00 12/23/16 12:15
10374222013 13 Water 12/22/16 00:00 12/23/16 12:15
10374222014 14 Water 12/22/16 00:00 12/23/16 12:15
10374222015 15 Water 12/22/16 00:00 12/23/16 12:15
10374222016 16 Water 12/22/16 00:00 12/23/16 12:15
10374222017 17 Water 12/22/16 00:00 12/23/16 12:15
10374222018 18 Water 12/22/16 00:00 12/23/16 12:15
10374222019 19 Water 12/22/16 00:00 12/23/16 12:15
10374222020 20 Water 12/22/16 00:00 12/23/16 12:15
10374222021 21 Water 12/22/16 00:00 12/23/16 12:15
10374222022 22 Water 12/22/16 00:00 12/23/16 12:15
10374222023 23 Water 12/22/16 00:00 12/23/16 12:15
10374222024 24 Water 12/22/16 00:00 12/23/16 12:15
10374222025 25 Water 12/22/16 00:00 12/23/16 12:15
10374222026 26 Water 12/22/16 00:00 12/23/16 12:15
10374222027 27 Water 12/22/16 00:00 12/23/16 12:15
10374222028 28 Water 12/22/16 00:00 12/23/16 12:15
10374222029 29 Water 12/22/16 00:00 12/23/16 12:15
10374222030 30 Water 12/22/16 00:00 12/23/16 12:15
10374222031 31 Water 12/22/16 00:00 12/23/16 12:15
10374222032 32 Water 12/22/16 00:00 12/23/16 12:15
10374222033 33 Water 12/22/16 00:00 12/23/16 12:15
10374222034 34 Water 12/22/16 00:00 12/23/16 12:15
10374222035 35 Water 12/22/16 00:00 12/23/16 12:15
10374222036 36 Water 12/22/16 00:00 12/23/16 12:15
10374222037 37 Water 12/22/16 00:00 12/23/16 12:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 3 of 245
AET Project No.03-06427 Page C3 of 245
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Lab ID Sample ID Matrix Date Collected Date Received
10374222038 38 Water 12/22/16 00:00 12/23/16 12:15
10374222039 39 Water 12/22/16 00:00 12/23/16 12:15
10374222040 40 Water 12/22/16 00:00 12/23/16 12:15
10374222041 41 Water 12/22/16 00:00 12/23/16 12:15
10374222042 42 Water 12/22/16 00:00 12/23/16 12:15
10374222043 43 Water 12/22/16 00:00 12/23/16 12:15
10374222044 44 Water 12/22/16 00:00 12/23/16 12:15
10374222045 45 Water 12/22/16 00:00 12/23/16 12:15
10374222046 46 Water 12/22/16 00:00 12/23/16 12:15
10374222047 47 Water 12/22/16 00:00 12/23/16 12:15
10374222048 48 Water 12/22/16 00:00 12/23/16 12:15
10374222049 49 Water 12/22/16 00:00 12/23/16 12:15
10374222050 50 Water 12/22/16 00:00 12/23/16 12:15
10374222051 51 Water 12/22/16 00:00 12/23/16 12:15
10374222052 52 Water 12/22/16 00:00 12/23/16 12:15
10374222053 53 Water 12/22/16 00:00 12/23/16 12:15
10374222054 54 Water 12/22/16 00:00 12/23/16 12:15
10374222055 55 Water 12/22/16 00:00 12/23/16 12:15
10374222056 56 Water 12/22/16 00:00 12/23/16 12:15
10374222057 57 Water 12/22/16 00:00 12/23/16 12:15
10374222058 58 Water 12/22/16 00:00 12/23/16 12:15
10374222059 59 Water 12/22/16 00:00 12/23/16 12:15
10374222060 60 Water 12/22/16 00:00 12/23/16 12:15
10374222061 61 Water 12/22/16 00:00 12/23/16 12:15
10374222062 62 Water 12/22/16 00:00 12/23/16 12:15
10374222063 63 Water 12/22/16 00:00 12/23/16 12:15
10374222064 64 Water 12/22/16 00:00 12/23/16 12:15
10374222065 65 Water 12/22/16 00:00 12/23/16 12:15
10374222066 66 Water 12/22/16 00:00 12/23/16 12:15
10374222067 67 Water 12/22/16 00:00 12/23/16 12:15
10374222068 68 Water 12/22/16 00:00 12/23/16 12:15
10374222069 69 Water 12/22/16 00:00 12/23/16 12:15
10374222070 70 Water 12/22/16 00:00 12/23/16 12:15
10374222071 71 Water 12/22/16 00:00 12/23/16 12:15
10374222072 72 Water 12/22/16 00:00 12/23/16 12:15
10374222073 73 Water 12/22/16 00:00 12/23/16 12:15
10374222074 74 Water 12/22/16 00:00 12/23/16 12:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 4 of 245
AET Project No.03-06427 Page C4 of 245
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Lab ID Sample ID Matrix Date Collected Date Received
10374222075 75 Water 12/22/16 00:00 12/23/16 12:15
10374222076 76 Water 12/22/16 00:00 12/23/16 12:15
10374222077 77 Water 12/22/16 00:00 12/23/16 12:15
10374222078 78 Water 12/22/16 00:00 12/23/16 12:15
10374222079 79 Water 12/22/16 00:00 12/23/16 12:15
10374222080 80 Water 12/22/16 00:00 12/23/16 12:15
10374222081 81 Water 12/22/16 00:00 12/23/16 12:15
10374222082 82 Water 12/22/16 00:00 12/23/16 12:15
10374222083 83 Water 12/22/16 00:00 12/23/16 12:15
10374222084 84 Water 12/22/16 00:00 12/23/16 12:15
10374222085 85 Water 12/22/16 00:00 12/23/16 12:15
10374222086 86 Water 12/22/16 00:00 12/23/16 12:15
10374222087 87 Water 12/22/16 00:00 12/23/16 12:15
10374222088 88 Water 12/22/16 00:00 12/23/16 12:15
10374222089 89 Water 12/22/16 00:00 12/23/16 12:15
10374222090 90 Water 12/22/16 00:00 12/23/16 12:15
10374222091 91 Water 12/22/16 00:00 12/23/16 12:15
10374222092 92 Water 12/22/16 00:00 12/23/16 12:15
10374222093 93 Water 12/22/16 00:00 12/23/16 12:15
10374222094 94 Water 12/22/16 00:00 12/23/16 12:15
10374222095 95 Water 12/22/16 00:00 12/23/16 12:15
10374222096 96 (A) Water 12/22/16 00:00 12/23/16 12:15
10374222097 97 Water 12/22/16 00:00 12/23/16 12:15
10374222098 98 Water 12/22/16 00:00 12/23/16 12:15
10374222099 99 Water 12/22/16 00:00 12/23/16 12:15
10374222100 100 Water 12/22/16 00:00 12/23/16 12:15
10374222101 101 Water 12/22/16 00:00 12/23/16 12:15
10374222102 102 Water 12/22/16 00:00 12/23/16 12:15
10374222103 103 Water 12/22/16 00:00 12/23/16 12:15
10374222104 104 Water 12/22/16 00:00 12/23/16 12:15
10374222105 105 Water 12/22/16 00:00 12/23/16 12:15
10374222106 106 Water 12/22/16 00:00 12/23/16 12:15
10374222107 107 Water 12/22/16 00:00 12/23/16 12:15
10374222108 108 Water 12/22/16 00:00 12/23/16 12:15
10374222109 109 Water 12/22/16 00:00 12/23/16 12:15
10374222110 110 Water 12/22/16 00:00 12/23/16 12:15
10374222111 111 Water 12/22/16 00:00 12/23/16 12:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 5 of 245
AET Project No.03-06427 Page C5 of 245
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Lab ID Sample ID Matrix Date Collected Date Received
10374222112 112 Water 12/22/16 00:00 12/23/16 12:15
10374222113 113 Water 12/22/16 00:00 12/23/16 12:15
10374222114 114 Water 12/22/16 00:00 12/23/16 12:15
10374222115 115 Water 12/22/16 00:00 12/23/16 12:15
10374222116 116 Water 12/22/16 00:00 12/23/16 12:15
10374222117 117 Water 12/22/16 00:00 12/23/16 12:15
10374222118 118 Water 12/22/16 00:00 12/23/16 12:15
10374222119 119 Water 12/22/16 00:00 12/23/16 12:15
10374222120 120 Water 12/22/16 00:00 12/23/16 12:15
10374222121 121 Water 12/22/16 00:00 12/23/16 12:15
10374222122 122 Water 12/22/16 00:00 12/23/16 12:15
10374222123 123 Water 12/22/16 00:00 12/23/16 12:15
10374222124 124 Water 12/22/16 00:00 12/23/16 12:15
10374222125 125 Water 12/22/16 00:00 12/23/16 12:15
10374222126 126 Water 12/22/16 00:00 12/23/16 12:15
10374222127 127 Water 12/22/16 00:00 12/23/16 12:15
10374222128 128 Water 12/22/16 00:00 12/23/16 12:15
10374222129 129 Water 12/22/16 00:00 12/23/16 12:15
10374222130 130 Water 12/22/16 00:00 12/23/16 12:15
10374222131 131 Water 12/22/16 00:00 12/23/16 12:15
10374222132 132 Water 12/22/16 00:00 12/23/16 12:15
10374222133 133 Water 12/22/16 00:00 12/23/16 12:15
10374222134 134 Water 12/22/16 00:00 12/23/16 12:15
10374222135 135 Water 12/22/16 00:00 12/23/16 12:15
10374222136 136 Water 12/22/16 00:00 12/23/16 12:15
10374222137 137 Water 12/22/16 00:00 12/23/16 12:15
10374222138 138 Water 12/22/16 00:00 12/23/16 12:15
10374222139 139 Water 12/22/16 00:00 12/23/16 12:15
10374222140 140 Water 12/22/16 00:00 12/23/16 12:15
10374222141 141 Water 12/22/16 00:00 12/23/16 12:15
10374222142 142 Water 12/22/16 00:00 12/23/16 12:15
10374222143 143 Water 12/22/16 00:00 12/23/16 12:15
10374222144 144 Water 12/22/16 00:00 12/23/16 12:15
10374222145 145 Water 12/22/16 00:00 12/23/16 12:15
10374222146 146 Water 12/22/16 00:00 12/23/16 12:15
10374222147 147 Water 12/22/16 00:00 12/23/16 12:15
10374222148 148 Water 12/22/16 00:00 12/23/16 12:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 6 of 245
AET Project No.03-06427 Page C6 of 245
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Lab ID Sample ID Matrix Date Collected Date Received
10374222149 149 Water 12/22/16 00:00 12/23/16 12:15
10374222150 150 Water 12/22/16 00:00 12/23/16 12:15
10374222151 151 Water 12/22/16 00:00 12/23/16 12:15
10374222152 152 Water 12/22/16 00:00 12/23/16 12:15
10374222153 153 Water 12/22/16 00:00 12/23/16 12:15
10374222154 154 Water 12/22/16 00:00 12/23/16 12:15
10374222155 155 Water 12/22/16 00:00 12/23/16 12:15
10374222156 156 Water 12/22/16 00:00 12/23/16 12:15
10374222157 157 Water 12/22/16 00:00 12/23/16 12:15
10374222158 158 Water 12/22/16 00:00 12/23/16 12:15
10374222159 159 Water 12/22/16 00:00 12/23/16 12:15
10374222160 160 Water 12/22/16 00:00 12/23/16 12:15
10374222161 161 Water 12/22/16 00:00 12/23/16 12:15
10374222162 162 Water 12/22/16 00:00 12/23/16 12:15
10374222163 163 Water 12/22/16 00:00 12/23/16 12:15
10374222164 164 Water 12/22/16 00:00 12/23/16 12:15
10374222165 165 Water 12/22/16 00:00 12/23/16 12:15
10374222166 166 Water 12/22/16 00:00 12/23/16 12:15
10374222167 167 Water 12/22/16 00:00 12/23/16 12:15
10374222168 168 Water 12/22/16 00:00 12/23/16 12:15
10374222169 169 Water 12/22/16 00:00 12/23/16 12:15
10374222170 170 Water 12/22/16 00:00 12/23/16 12:15
10374222171 171 Water 12/22/16 00:00 12/23/16 12:15
10374222172 172 Water 12/22/16 00:00 12/23/16 12:15
10374222173 173 Water 12/22/16 00:00 12/23/16 12:15
10374222174 174 Water 12/22/16 00:00 12/23/16 12:15
10374222175 175 Water 12/22/16 00:00 12/23/16 12:15
10374222176 176 Water 12/22/16 00:00 12/23/16 12:15
10374222177 177 Water 12/22/16 00:00 12/23/16 12:15
10374222178 178 Water 12/22/16 00:00 12/23/16 12:15
10374222179 179 Water 12/22/16 00:00 12/23/16 12:15
10374222180 180 Water 12/22/16 00:00 12/23/16 12:15
10374222181 181 Water 12/22/16 00:00 12/23/16 12:15
10374222182 182 Water 12/22/16 00:00 12/23/16 12:15
10374222183 183 Water 12/22/16 00:00 12/23/16 12:15
10374222184 184 Water 12/22/16 00:00 12/23/16 12:15
10374222185 185 Water 12/22/16 00:00 12/23/16 12:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 7 of 245
AET Project No.03-06427 Page C7 of 245
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Lab ID Sample ID Matrix Date Collected Date Received
10374222186 186 Water 12/22/16 00:00 12/23/16 12:15
10374222187 187 Water 12/22/16 00:00 12/23/16 12:15
10374222188 188 Water 12/22/16 00:00 12/23/16 12:15
10374222189 189 Water 12/22/16 00:00 12/23/16 12:15
10374222190 190 Water 12/22/16 00:00 12/23/16 12:15
10374222191 191 Water 12/22/16 00:00 12/23/16 12:15
10374222192 192 Water 12/22/16 00:00 12/23/16 12:15
10374222193 193 Water 12/22/16 00:00 12/23/16 12:15
10374222194 194 Water 12/22/16 00:00 12/23/16 12:15
10374222195 195 Water 12/22/16 00:00 12/23/16 12:15
10374222196 196 Water 12/22/16 00:00 12/23/16 12:15
10374222197 197 Water 12/22/16 00:00 12/23/16 12:15
10374222198 198 Water 12/22/16 00:00 12/23/16 12:15
10374222199 199 Water 12/22/16 00:00 12/23/16 12:15
10374222200 200 Water 12/22/16 00:00 12/23/16 12:15
10374222201 201 Water 12/22/16 00:00 12/23/16 12:15
10374222202 202 Water 12/22/16 00:00 12/23/16 12:15
10374222203 203 Water 12/22/16 00:00 12/23/16 12:15
10374222204 204 Water 12/22/16 00:00 12/23/16 12:15
10374222205 96(B) Water 12/22/16 00:00 12/23/16 12:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 8 of 245
AET Project No.03-06427 Page C8 of 245
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
10374222001 1 EPA 200.8 1 PASI-MTT3
10374222002 2 EPA 200.8 1 PASI-MTT3
10374222003 3 EPA 200.8 1 PASI-MTT3
10374222004 4 EPA 200.8 1 PASI-MTT3
10374222005 5 EPA 200.8 1 PASI-MTT3
10374222006 6 EPA 200.8 1 PASI-MTT3
10374222007 7 EPA 200.8 1 PASI-MTT3
10374222008 8 EPA 200.8 1 PASI-MTT3
10374222009 9 EPA 200.8 1 PASI-MTT3
10374222010 10 EPA 200.8 1 PASI-MTT3
10374222011 11 EPA 200.8 1 PASI-MTT3
10374222012 12 EPA 200.8 1 PASI-MTT3
10374222013 13 EPA 200.8 1 PASI-MTT3
10374222014 14 EPA 200.8 1 PASI-MTT3
10374222015 15 EPA 200.8 1 PASI-MTT3
10374222016 16 EPA 200.8 1 PASI-MTT3
10374222017 17 EPA 200.8 1 PASI-MTT3
10374222018 18 EPA 200.8 1 PASI-MTT3
10374222019 19 EPA 200.8 1 PASI-MTT3
10374222020 20 EPA 200.8 1 PASI-MTT3
10374222021 21 EPA 200.8 1 PASI-MTT3
10374222022 22 EPA 200.8 1 PASI-MTT3
10374222023 23 EPA 200.8 1 PASI-MTT3
10374222024 24 EPA 200.8 1 PASI-MTT3
10374222025 25 EPA 200.8 1 PASI-MTT3
10374222026 26 EPA 200.8 1 PASI-MTT3
10374222027 27 EPA 200.8 1 PASI-MRJS
10374222028 28 EPA 200.8 1 PASI-MTT3
10374222029 29 EPA 200.8 1 PASI-MTT3
10374222030 30 EPA 200.8 1 PASI-MTT3
10374222031 31 EPA 200.8 1 PASI-MTT3
10374222032 32 EPA 200.8 1 PASI-MTT3
10374222033 33 EPA 200.8 1 PASI-MTT3
10374222034 34 EPA 200.8 1 PASI-MTT3
10374222035 35 EPA 200.8 1 PASI-MTT3
10374222036 36 EPA 200.8 1 PASI-MTT3
10374222037 37 EPA 200.8 1 PASI-MTT3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 9 of 245
AET Project No.03-06427 Page C9 of 245
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
10374222038 38 EPA 200.8 1 PASI-MTT3
10374222039 39 EPA 200.8 1 PASI-MTT3
10374222040 40 EPA 200.8 1 PASI-MTT3
10374222041 41 EPA 200.8 1 PASI-MTT3
10374222042 42 EPA 200.8 1 PASI-MTT3
10374222043 43 EPA 200.8 1 PASI-MTT3
10374222044 44 EPA 200.8 1 PASI-MTT3
10374222045 45 EPA 200.8 1 PASI-MTT3
10374222046 46 EPA 200.8 1 PASI-MTT3
10374222047 47 EPA 200.8 1 PASI-MTT3
10374222048 48 EPA 200.8 1 PASI-MTT3
10374222049 49 EPA 200.8 1 PASI-MTT3
10374222050 50 EPA 200.8 1 PASI-MTT3
10374222051 51 EPA 200.8 1 PASI-MTT3
10374222052 52 EPA 200.8 1 PASI-MTT3
10374222053 53 EPA 200.8 1 PASI-MTT3
10374222054 54 EPA 200.8 1 PASI-MTT3
10374222055 55 EPA 200.8 1 PASI-MTT3
10374222056 56 EPA 200.8 1 PASI-MTT3
10374222057 57 EPA 200.8 1 PASI-MTT3
10374222058 58 EPA 200.8 1 PASI-MTT3
10374222059 59 EPA 200.8 1 PASI-MTT3
10374222060 60 EPA 200.8 1 PASI-MTT3
10374222061 61 EPA 200.8 1 PASI-MTT3
10374222062 62 EPA 200.8 1 PASI-MTT3
10374222063 63 EPA 200.8 1 PASI-MTT3
10374222064 64 EPA 200.8 1 PASI-MTT3
10374222065 65 EPA 200.8 1 PASI-MTT3
10374222066 66 EPA 200.8 1 PASI-MRJS
10374222067 67 EPA 200.8 1 PASI-MTT3
10374222068 68 EPA 200.8 1 PASI-MTT3
10374222069 69 EPA 200.8 1 PASI-MTT3
10374222070 70 EPA 200.8 1 PASI-MTT3
10374222071 71 EPA 200.8 1 PASI-MTT3
10374222072 72 EPA 200.8 1 PASI-MTT3
10374222073 73 EPA 200.8 1 PASI-MTT3
10374222074 74 EPA 200.8 1 PASI-MRJS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 10 of 245
AET Project No.03-06427 Page C10 of 245
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
10374222075 75 EPA 200.8 1 PASI-MTT3
10374222076 76 EPA 200.8 1 PASI-MTT3
10374222077 77 EPA 200.8 1 PASI-MTT3
10374222078 78 EPA 200.8 1 PASI-MTT3
10374222079 79 EPA 200.8 1 PASI-MTT3
10374222080 80 EPA 200.8 1 PASI-MTT3
10374222081 81 EPA 200.8 1 PASI-MTT3
10374222082 82 EPA 200.8 1 PASI-MTT3
10374222083 83 EPA 200.8 1 PASI-MTT3
10374222084 84 EPA 200.8 1 PASI-MTT3
10374222085 85 EPA 200.8 1 PASI-MTT3
10374222086 86 EPA 200.8 1 PASI-MTT3
10374222087 87 EPA 200.8 1 PASI-MTT3
10374222088 88 EPA 200.8 1 PASI-MTT3
10374222089 89 EPA 200.8 1 PASI-MTT3
10374222090 90 EPA 200.8 1 PASI-MTT3
10374222091 91 EPA 200.8 1 PASI-MTT3
10374222092 92 EPA 200.8 1 PASI-MTT3
10374222093 93 EPA 200.8 1 PASI-MTT3
10374222094 94 EPA 200.8 1 PASI-MTT3
10374222095 95 EPA 200.8 1 PASI-MTT3
10374222096 96 (A) EPA 200.8 1 PASI-MTT3
10374222097 97 EPA 200.8 1 PASI-MTT3
10374222098 98 EPA 200.8 1 PASI-MTT3
10374222099 99 EPA 200.8 1 PASI-MTT3
10374222100 100 EPA 200.8 1 PASI-MTT3
10374222101 101 EPA 200.8 1 PASI-MTT3
10374222102 102 EPA 200.8 1 PASI-MTT3
10374222103 103 EPA 200.8 1 PASI-MTT3
10374222104 104 EPA 200.8 1 PASI-MTT3
10374222105 105 EPA 200.8 1 PASI-MTT3
10374222106 106 EPA 200.8 1 PASI-MTT3
10374222107 107 EPA 200.8 1 PASI-MTT3
10374222108 108 EPA 200.8 1 PASI-MTT3
10374222109 109 EPA 200.8 1 PASI-MTT3
10374222110 110 EPA 200.8 1 PASI-MTT3
10374222111 111 EPA 200.8 1 PASI-MTT3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 11 of 245
AET Project No.03-06427 Page C11 of 245
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
10374222112 112 EPA 200.8 1 PASI-MTT3
10374222113 113 EPA 200.8 1 PASI-MTT3
10374222114 114 EPA 200.8 1 PASI-MTT3
10374222115 115 EPA 200.8 1 PASI-MTT3
10374222116 116 EPA 200.8 1 PASI-MTT3
10374222117 117 EPA 200.8 1 PASI-MTT3
10374222118 118 EPA 200.8 1 PASI-MTT3
10374222119 119 EPA 200.8 1 PASI-MTT3
10374222120 120 EPA 200.8 1 PASI-MTT3
10374222121 121 EPA 200.8 1 PASI-MRJS
10374222122 122 EPA 200.8 1 PASI-MRJS
10374222123 123 EPA 200.8 1 PASI-MRJS
10374222124 124 EPA 200.8 1 PASI-MRJS
10374222125 125 EPA 200.8 1 PASI-MRJS
10374222126 126 EPA 200.8 1 PASI-MRJS
10374222127 127 EPA 200.8 1 PASI-MRJS
10374222128 128 EPA 200.8 1 PASI-MRJS
10374222129 129 EPA 200.8 1 PASI-MRJS
10374222130 130 EPA 200.8 1 PASI-MRJS
10374222131 131 EPA 200.8 1 PASI-MRJS
10374222132 132 EPA 200.8 1 PASI-MRJS
10374222133 133 EPA 200.8 1 PASI-MRJS
10374222134 134 EPA 200.8 1 PASI-MRJS
10374222135 135 EPA 200.8 1 PASI-MRJS
10374222136 136 EPA 200.8 1 PASI-MRJS
10374222137 137 EPA 200.8 1 PASI-MRJS
10374222138 138 EPA 200.8 1 PASI-MRJS
10374222139 139 EPA 200.8 1 PASI-MRJS
10374222140 140 EPA 200.8 1 PASI-MRJS
10374222141 141 EPA 200.8 1 PASI-MRJS
10374222142 142 EPA 200.8 1 PASI-MRJS
10374222143 143 EPA 200.8 1 PASI-MRJS
10374222144 144 EPA 200.8 1 PASI-MRJS
10374222145 145 EPA 200.8 1 PASI-MRJS
10374222146 146 EPA 200.8 1 PASI-MRJS
10374222147 147 EPA 200.8 1 PASI-MRJS
10374222148 148 EPA 200.8 1 PASI-MRJS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 12 of 245
AET Project No.03-06427 Page C12 of 245
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
10374222149 149 EPA 200.8 1 PASI-MRJS
10374222150 150 EPA 200.8 1 PASI-MRJS
10374222151 151 EPA 200.8 1 PASI-MRJS
10374222152 152 EPA 200.8 1 PASI-MRJS
10374222153 153 EPA 200.8 1 PASI-MRJS
10374222154 154 EPA 200.8 1 PASI-MRJS
10374222155 155 EPA 200.8 1 PASI-MRJS
10374222156 156 EPA 200.8 1 PASI-MRJS
10374222157 157 EPA 200.8 1 PASI-MRJS
10374222158 158 EPA 200.8 1 PASI-MRJS
10374222159 159 EPA 200.8 1 PASI-MRJS
10374222160 160 EPA 200.8 1 PASI-MRJS
10374222161 161 EPA 200.8 1 PASI-MTT3
10374222162 162 EPA 200.8 1 PASI-MTT3
10374222163 163 EPA 200.8 1 PASI-MTT3
10374222164 164 EPA 200.8 1 PASI-MTT3
10374222165 165 EPA 200.8 1 PASI-MTT3
10374222166 166 EPA 200.8 1 PASI-MTT3
10374222167 167 EPA 200.8 1 PASI-MTT3
10374222168 168 EPA 200.8 1 PASI-MTT3
10374222169 169 EPA 200.8 1 PASI-MTT3
10374222170 170 EPA 200.8 1 PASI-MTT3
10374222171 171 EPA 200.8 1 PASI-MTT3
10374222172 172 EPA 200.8 1 PASI-MTT3
10374222173 173 EPA 200.8 1 PASI-MTT3
10374222174 174 EPA 200.8 1 PASI-MTT3
10374222175 175 EPA 200.8 1 PASI-MTT3
10374222176 176 EPA 200.8 1 PASI-MTT3
10374222177 177 EPA 200.8 1 PASI-MTT3
10374222178 178 EPA 200.8 1 PASI-MTT3
10374222179 179 EPA 200.8 1 PASI-MTT3
10374222180 180 EPA 200.8 1 PASI-MRJS
10374222181 181 EPA 200.8 1 PASI-MTT3
10374222182 182 EPA 200.8 1 PASI-MTT3
10374222183 183 EPA 200.8 1 PASI-MTT3
10374222184 184 EPA 200.8 1 PASI-MTT3
10374222185 185 EPA 200.8 1 PASI-MTT3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 13 of 245
AET Project No.03-06427 Page C13 of 245
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
10374222186 186 EPA 200.8 1 PASI-MTT3
10374222187 187 EPA 200.8 1 PASI-MTT3
10374222188 188 EPA 200.8 1 PASI-MTT3
10374222189 189 EPA 200.8 1 PASI-MTT3
10374222190 190 EPA 200.8 1 PASI-MTT3
10374222191 191 EPA 200.8 1 PASI-MTT3
10374222192 192 EPA 200.8 1 PASI-MTT3
10374222193 193 EPA 200.8 1 PASI-MTT3
10374222194 194 EPA 200.8 1 PASI-MTT3
10374222195 195 EPA 200.8 1 PASI-MTT3
10374222196 196 EPA 200.8 1 PASI-MTT3
10374222197 197 EPA 200.8 1 PASI-MTT3
10374222198 198 EPA 200.8 1 PASI-MTT3
10374222199 199 EPA 200.8 1 PASI-MTT3
10374222200 200 EPA 200.8 1 PASI-MTT3
10374222201 201 EPA 200.8 1 PASI-MTT3
10374222202 202 EPA 200.8 1 PASI-MTT3
10374222203 203 EPA 200.8 1 PASI-MTT3
10374222204 204 EPA 200.8 1 PASI-MTT3
10374222205 96(B) EPA 200.8 1 PASI-MTT3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 14 of 245
AET Project No.03-06427 Page C14 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 1 Lab ID: 10374222001 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.21 ug/L 12/27/16 14:01 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 15 of 245
AET Project No.03-06427 Page C15 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 2 Lab ID: 10374222002 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.19 ug/L 12/27/16 14:05 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 16 of 245
AET Project No.03-06427 Page C16 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 3 Lab ID: 10374222003 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.86 ug/L 12/27/16 14:06 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 17 of 245
AET Project No.03-06427 Page C17 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 4 Lab ID: 10374222004 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.50 ug/L 12/27/16 14:07 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 18 of 245
AET Project No.03-06427 Page C18 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 5 Lab ID: 10374222005 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.5 ug/L 12/27/16 14:08 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 19 of 245
AET Project No.03-06427 Page C19 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 6 Lab ID: 10374222006 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.86 ug/L 12/27/16 14:12 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 20 of 245
AET Project No.03-06427 Page C20 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 7 Lab ID: 10374222007 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.85 ug/L 12/27/16 14:13 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 21 of 245
AET Project No.03-06427 Page C21 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 8 Lab ID: 10374222008 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.86 ug/L 12/27/16 14:14 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 22 of 245
AET Project No.03-06427 Page C22 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 9 Lab ID: 10374222009 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 20.1 ug/L 12/27/16 14:15 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 23 of 245
AET Project No.03-06427 Page C23 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 10 Lab ID: 10374222010 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 4.6 ug/L 12/27/16 14:16 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 24 of 245
AET Project No.03-06427 Page C24 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 11 Lab ID: 10374222011 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.2 ug/L 12/27/16 14:17 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 25 of 245
AET Project No.03-06427 Page C25 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 12 Lab ID: 10374222012 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.3 ug/L 12/27/16 14:19 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 26 of 245
AET Project No.03-06427 Page C26 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 13 Lab ID: 10374222013 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 3.1 ug/L 12/27/16 14:20 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 27 of 245
AET Project No.03-06427 Page C27 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 14 Lab ID: 10374222014 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 3.2 ug/L 12/27/16 14:21 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 28 of 245
AET Project No.03-06427 Page C28 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 15 Lab ID: 10374222015 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 52.7 ug/L 12/27/16 14:27 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 29 of 245
AET Project No.03-06427 Page C29 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 16 Lab ID: 10374222016 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 5.4 ug/L 12/27/16 14:28 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 30 of 245
AET Project No.03-06427 Page C30 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 17 Lab ID: 10374222017 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 22.9 ug/L 12/27/16 14:29 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 31 of 245
AET Project No.03-06427 Page C31 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 18 Lab ID: 10374222018 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.5 ug/L 12/27/16 14:30 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 32 of 245
AET Project No.03-06427 Page C32 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 19 Lab ID: 10374222019 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.1 ug/L 12/27/16 14:32 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 33 of 245
AET Project No.03-06427 Page C33 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 20 Lab ID: 10374222020 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 6.1 ug/L 12/27/16 14:33 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 34 of 245
AET Project No.03-06427 Page C34 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 21 Lab ID: 10374222021 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.2 ug/L 12/27/16 14:34 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 35 of 245
AET Project No.03-06427 Page C35 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 22 Lab ID: 10374222022 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 4.3 ug/L 12/27/16 14:40 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 36 of 245
AET Project No.03-06427 Page C36 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 23 Lab ID: 10374222023 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 18.1 ug/L 12/27/16 14:41 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 37 of 245
AET Project No.03-06427 Page C37 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 24 Lab ID: 10374222024 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 5.3 ug/L 12/27/16 14:42 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 38 of 245
AET Project No.03-06427 Page C38 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 25 Lab ID: 10374222025 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 84.9 ug/L 12/27/16 14:43 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 39 of 245
AET Project No.03-06427 Page C39 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 26 Lab ID: 10374222026 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 5.3 ug/L 12/27/16 14:44 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 40 of 245
AET Project No.03-06427 Page C40 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 27 Lab ID: 10374222027 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8 Preparation Method: EPA 200.8200.8 MET ICPMS
Lead 14.8 ug/L 12/29/16 22:05 7439-92-112/29/16 09:360.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 41 of 245
AET Project No.03-06427 Page C41 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 28 Lab ID: 10374222028 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.26 ug/L 12/27/16 14:45 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 42 of 245
AET Project No.03-06427 Page C42 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 29 Lab ID: 10374222029 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 4.5 ug/L 12/27/16 14:47 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 43 of 245
AET Project No.03-06427 Page C43 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 30 Lab ID: 10374222030 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.27 ug/L 12/27/16 14:48 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 44 of 245
AET Project No.03-06427 Page C44 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 31 Lab ID: 10374222031 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 11.9 ug/L 12/27/16 14:51 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 45 of 245
AET Project No.03-06427 Page C45 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 32 Lab ID: 10374222032 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.2 ug/L 12/27/16 14:52 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 46 of 245
AET Project No.03-06427 Page C46 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 33 Lab ID: 10374222033 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 20.1 ug/L 12/27/16 14:54 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 47 of 245
AET Project No.03-06427 Page C47 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 34 Lab ID: 10374222034 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 38.4 ug/L 12/27/16 14:55 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 48 of 245
AET Project No.03-06427 Page C48 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 35 Lab ID: 10374222035 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 12.8 ug/L 12/27/16 14:56 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 49 of 245
AET Project No.03-06427 Page C49 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 36 Lab ID: 10374222036 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.0 ug/L 12/27/16 14:57 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 50 of 245
AET Project No.03-06427 Page C50 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 37 Lab ID: 10374222037 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 3.6 ug/L 12/27/16 14:59 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 51 of 245
AET Project No.03-06427 Page C51 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 38 Lab ID: 10374222038 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.78 ug/L 12/27/16 15:00 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 52 of 245
AET Project No.03-06427 Page C52 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 39 Lab ID: 10374222039 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 3.4 ug/L 12/27/16 15:01 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 53 of 245
AET Project No.03-06427 Page C53 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 40 Lab ID: 10374222040 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.5 ug/L 12/27/16 15:06 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 54 of 245
AET Project No.03-06427 Page C54 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 41 Lab ID: 10374222041 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.82 ug/L 12/27/16 15:07 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 55 of 245
AET Project No.03-06427 Page C55 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 42 Lab ID: 10374222042 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.75 ug/L 12/27/16 15:11 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 56 of 245
AET Project No.03-06427 Page C56 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 43 Lab ID: 10374222043 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 15.0 ug/L 12/27/16 15:12 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 57 of 245
AET Project No.03-06427 Page C57 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 44 Lab ID: 10374222044 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.0 ug/L 12/27/16 15:14 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 58 of 245
AET Project No.03-06427 Page C58 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 45 Lab ID: 10374222045 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.5 ug/L 12/27/16 15:18 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 59 of 245
AET Project No.03-06427 Page C59 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 46 Lab ID: 10374222046 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.22 ug/L 12/27/16 15:19 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 60 of 245
AET Project No.03-06427 Page C60 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 47 Lab ID: 10374222047 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.14 ug/L 12/27/16 15:20 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 61 of 245
AET Project No.03-06427 Page C61 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 48 Lab ID: 10374222048 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead ND ug/L 12/27/16 15:21 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 62 of 245
AET Project No.03-06427 Page C62 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 49 Lab ID: 10374222049 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.56 ug/L 12/27/16 15:22 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 63 of 245
AET Project No.03-06427 Page C63 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 50 Lab ID: 10374222050 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.20 ug/L 12/27/16 15:23 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 64 of 245
AET Project No.03-06427 Page C64 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 51 Lab ID: 10374222051 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 9.6 ug/L 12/27/16 15:24 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 65 of 245
AET Project No.03-06427 Page C65 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 52 Lab ID: 10374222052 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.1 ug/L 12/27/16 15:26 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 66 of 245
AET Project No.03-06427 Page C66 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 53 Lab ID: 10374222053 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 19.1 ug/L 12/27/16 15:27 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 67 of 245
AET Project No.03-06427 Page C67 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 54 Lab ID: 10374222054 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 15.5 ug/L 12/27/16 15:33 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 68 of 245
AET Project No.03-06427 Page C68 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 55 Lab ID: 10374222055 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.65 ug/L 12/27/16 15:34 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 69 of 245
AET Project No.03-06427 Page C69 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 56 Lab ID: 10374222056 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.33 ug/L 12/27/16 15:35 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 70 of 245
AET Project No.03-06427 Page C70 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 57 Lab ID: 10374222057 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.11 ug/L 12/27/16 15:36 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 71 of 245
AET Project No.03-06427 Page C71 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 58 Lab ID: 10374222058 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 5.4 ug/L 12/27/16 15:37 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 72 of 245
AET Project No.03-06427 Page C72 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 59 Lab ID: 10374222059 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.3 ug/L 12/27/16 15:38 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 73 of 245
AET Project No.03-06427 Page C73 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 60 Lab ID: 10374222060 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.54 ug/L 12/27/16 15:39 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 74 of 245
AET Project No.03-06427 Page C74 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 61 Lab ID: 10374222061 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.34 ug/L 12/27/16 15:40 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 75 of 245
AET Project No.03-06427 Page C75 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 62 Lab ID: 10374222062 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 6.6 ug/L 12/27/16 15:46 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 76 of 245
AET Project No.03-06427 Page C76 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 63 Lab ID: 10374222063 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.2 ug/L 12/27/16 15:47 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 77 of 245
AET Project No.03-06427 Page C77 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 64 Lab ID: 10374222064 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 7.2 ug/L 12/27/16 15:49 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 78 of 245
AET Project No.03-06427 Page C78 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 65 Lab ID: 10374222065 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.1 ug/L 12/27/16 15:50 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 79 of 245
AET Project No.03-06427 Page C79 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 66 Lab ID: 10374222066 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8 Preparation Method: EPA 200.8200.8 MET ICPMS
Lead 63.9 ug/L 12/29/16 22:17 7439-92-112/29/16 09:360.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 80 of 245
AET Project No.03-06427 Page C80 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 67 Lab ID: 10374222067 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.1 ug/L 12/27/16 15:51 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 81 of 245
AET Project No.03-06427 Page C81 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 68 Lab ID: 10374222068 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 14.2 ug/L 12/27/16 15:52 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 82 of 245
AET Project No.03-06427 Page C82 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 69 Lab ID: 10374222069 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.0 ug/L 12/27/16 15:53 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 83 of 245
AET Project No.03-06427 Page C83 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 70 Lab ID: 10374222070 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 8.4 ug/L 12/27/16 16:47 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 84 of 245
AET Project No.03-06427 Page C84 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 71 Lab ID: 10374222071 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.96 ug/L 12/27/16 16:48 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 85 of 245
AET Project No.03-06427 Page C85 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 72 Lab ID: 10374222072 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 9.7 ug/L 12/27/16 16:49 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 86 of 245
AET Project No.03-06427 Page C86 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 73 Lab ID: 10374222073 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.5 ug/L 12/27/16 16:51 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 87 of 245
AET Project No.03-06427 Page C87 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 74 Lab ID: 10374222074 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8 Preparation Method: EPA 200.8200.8 MET ICPMS
Lead 2.1 ug/L 12/29/16 22:20 7439-92-112/29/16 09:360.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 88 of 245
AET Project No.03-06427 Page C88 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 75 Lab ID: 10374222075 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.74 ug/L 12/27/16 16:52 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 89 of 245
AET Project No.03-06427 Page C89 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 76 Lab ID: 10374222076 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.98 ug/L 12/27/16 16:53 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 90 of 245
AET Project No.03-06427 Page C90 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 77 Lab ID: 10374222077 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.69 ug/L 12/27/16 16:54 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 91 of 245
AET Project No.03-06427 Page C91 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 78 Lab ID: 10374222078 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 29.6 ug/L 12/27/16 16:55 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 92 of 245
AET Project No.03-06427 Page C92 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 79 Lab ID: 10374222079 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 4.4 ug/L 12/27/16 16:56 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 93 of 245
AET Project No.03-06427 Page C93 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 80 Lab ID: 10374222080 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 23.6 ug/L 12/27/16 17:02 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 94 of 245
AET Project No.03-06427 Page C94 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 81 Lab ID: 10374222081 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.8 ug/L 12/27/16 17:03 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 95 of 245
AET Project No.03-06427 Page C95 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 82 Lab ID: 10374222082 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.55 ug/L 12/27/16 17:07 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 96 of 245
AET Project No.03-06427 Page C96 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 83 Lab ID: 10374222083 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead ND ug/L 12/27/16 17:08 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 97 of 245
AET Project No.03-06427 Page C97 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 84 Lab ID: 10374222084 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.41 ug/L 12/27/16 17:09 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 98 of 245
AET Project No.03-06427 Page C98 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 85 Lab ID: 10374222085 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.16 ug/L 12/27/16 17:13 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 99 of 245
AET Project No.03-06427 Page C99 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 86 Lab ID: 10374222086 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.6 ug/L 12/27/16 17:14 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 100 of 245
AET Project No.03-06427 Page C100 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 87 Lab ID: 10374222087 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.5 ug/L 12/27/16 17:15 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 101 of 245
AET Project No.03-06427 Page C101 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 88 Lab ID: 10374222088 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.15 ug/L 12/27/16 17:16 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 102 of 245
AET Project No.03-06427 Page C102 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 89 Lab ID: 10374222089 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead ND ug/L 12/27/16 17:17 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 103 of 245
AET Project No.03-06427 Page C103 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 90 Lab ID: 10374222090 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.47 ug/L 12/27/16 17:18 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 104 of 245
AET Project No.03-06427 Page C104 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 91 Lab ID: 10374222091 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.54 ug/L 12/27/16 17:19 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 105 of 245
AET Project No.03-06427 Page C105 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 92 Lab ID: 10374222092 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.12 ug/L 12/27/16 17:21 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 106 of 245
AET Project No.03-06427 Page C106 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 93 Lab ID: 10374222093 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.8 ug/L 12/27/16 17:22 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 107 of 245
AET Project No.03-06427 Page C107 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 94 Lab ID: 10374222094 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.4 ug/L 12/27/16 17:27 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 108 of 245
AET Project No.03-06427 Page C108 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 95 Lab ID: 10374222095 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.64 ug/L 12/27/16 17:29 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 109 of 245
AET Project No.03-06427 Page C109 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 96 (A) Lab ID: 10374222096 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.5 ug/L 12/27/16 17:30 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 110 of 245
AET Project No.03-06427 Page C110 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 97 Lab ID: 10374222097 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.3 ug/L 12/27/16 17:31 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 111 of 245
AET Project No.03-06427 Page C111 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 98 Lab ID: 10374222098 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.91 ug/L 12/27/16 17:32 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 112 of 245
AET Project No.03-06427 Page C112 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 99 Lab ID: 10374222099 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.54 ug/L 12/27/16 17:33 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 113 of 245
AET Project No.03-06427 Page C113 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 100 Lab ID: 10374222100 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.1 ug/L 12/27/16 17:34 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 114 of 245
AET Project No.03-06427 Page C114 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 101 Lab ID: 10374222101 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 3.0 ug/L 12/27/16 17:35 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 115 of 245
AET Project No.03-06427 Page C115 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 102 Lab ID: 10374222102 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.3 ug/L 12/27/16 17:41 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 116 of 245
AET Project No.03-06427 Page C116 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 103 Lab ID: 10374222103 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.5 ug/L 12/27/16 17:42 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 117 of 245
AET Project No.03-06427 Page C117 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 104 Lab ID: 10374222104 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.2 ug/L 12/27/16 17:43 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 118 of 245
AET Project No.03-06427 Page C118 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 105 Lab ID: 10374222105 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.61 ug/L 12/27/16 17:45 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 119 of 245
AET Project No.03-06427 Page C119 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 106 Lab ID: 10374222106 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.12 ug/L 12/27/16 17:46 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 120 of 245
AET Project No.03-06427 Page C120 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 107 Lab ID: 10374222107 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.18 ug/L 12/27/16 17:47 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 121 of 245
AET Project No.03-06427 Page C121 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 108 Lab ID: 10374222108 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.42 ug/L 12/27/16 17:48 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 122 of 245
AET Project No.03-06427 Page C122 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 109 Lab ID: 10374222109 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.78 ug/L 12/28/16 07:39 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 123 of 245
AET Project No.03-06427 Page C123 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 110 Lab ID: 10374222110 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.31 ug/L 12/28/16 07:41 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 124 of 245
AET Project No.03-06427 Page C124 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 111 Lab ID: 10374222111 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.48 ug/L 12/28/16 07:42 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 125 of 245
AET Project No.03-06427 Page C125 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 112 Lab ID: 10374222112 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.65 ug/L 12/28/16 07:45 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 126 of 245
AET Project No.03-06427 Page C126 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 113 Lab ID: 10374222113 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.35 ug/L 12/28/16 07:46 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 127 of 245
AET Project No.03-06427 Page C127 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 114 Lab ID: 10374222114 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.41 ug/L 12/28/16 07:47 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 128 of 245
AET Project No.03-06427 Page C128 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 115 Lab ID: 10374222115 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.16 ug/L 12/28/16 07:48 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 129 of 245
AET Project No.03-06427 Page C129 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 116 Lab ID: 10374222116 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 66.7 ug/L 12/28/16 07:49 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 130 of 245
AET Project No.03-06427 Page C130 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 117 Lab ID: 10374222117 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 10.8 ug/L 12/28/16 07:50 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 131 of 245
AET Project No.03-06427 Page C131 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 118 Lab ID: 10374222118 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.56 ug/L 12/27/16 16:35 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 132 of 245
AET Project No.03-06427 Page C132 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 119 Lab ID: 10374222119 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.19 ug/L 12/27/16 16:36 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 133 of 245
AET Project No.03-06427 Page C133 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 120 Lab ID: 10374222120 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 21.0 ug/L 12/27/16 16:37 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 134 of 245
AET Project No.03-06427 Page C134 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 121 Lab ID: 10374222121 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.4 ug/L 12/29/16 18:52 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 135 of 245
AET Project No.03-06427 Page C135 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 122 Lab ID: 10374222122 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 25.0 ug/L 12/29/16 19:04 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 136 of 245
AET Project No.03-06427 Page C136 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 123 Lab ID: 10374222123 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 5.2 ug/L 12/29/16 19:07 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 137 of 245
AET Project No.03-06427 Page C137 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 124 Lab ID: 10374222124 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 586 ug/L 12/29/16 19:10 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 138 of 245
AET Project No.03-06427 Page C138 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 125 Lab ID: 10374222125 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 11.1 ug/L 12/29/16 19:13 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 139 of 245
AET Project No.03-06427 Page C139 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 126 Lab ID: 10374222126 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 8.5 ug/L 12/29/16 19:22 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 140 of 245
AET Project No.03-06427 Page C140 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 127 Lab ID: 10374222127 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.80 ug/L 12/29/16 19:25 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 141 of 245
AET Project No.03-06427 Page C141 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 128 Lab ID: 10374222128 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 9.0 ug/L 12/29/16 19:28 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 142 of 245
AET Project No.03-06427 Page C142 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 129 Lab ID: 10374222129 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.65 ug/L 12/29/16 19:31 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 143 of 245
AET Project No.03-06427 Page C143 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 130 Lab ID: 10374222130 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.48 ug/L 12/29/16 19:34 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 144 of 245
AET Project No.03-06427 Page C144 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 131 Lab ID: 10374222131 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.37 ug/L 12/29/16 19:37 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 145 of 245
AET Project No.03-06427 Page C145 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 132 Lab ID: 10374222132 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.13 ug/L 12/29/16 19:40 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 146 of 245
AET Project No.03-06427 Page C146 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 133 Lab ID: 10374222133 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.1 ug/L 12/29/16 19:43 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 147 of 245
AET Project No.03-06427 Page C147 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 134 Lab ID: 10374222134 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.57 ug/L 12/29/16 19:46 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 148 of 245
AET Project No.03-06427 Page C148 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 135 Lab ID: 10374222135 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.20 ug/L 12/29/16 19:49 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 149 of 245
AET Project No.03-06427 Page C149 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 136 Lab ID: 10374222136 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.1 ug/L 12/29/16 20:04 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 150 of 245
AET Project No.03-06427 Page C150 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 137 Lab ID: 10374222137 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.2 ug/L 12/29/16 20:07 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 151 of 245
AET Project No.03-06427 Page C151 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 138 Lab ID: 10374222138 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 8.1 ug/L 12/29/16 20:10 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 152 of 245
AET Project No.03-06427 Page C152 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 139 Lab ID: 10374222139 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.1 ug/L 12/29/16 20:13 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 153 of 245
AET Project No.03-06427 Page C153 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 140 Lab ID: 10374222140 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 5.3 ug/L 12/29/16 20:16 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 154 of 245
AET Project No.03-06427 Page C154 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 141 Lab ID: 10374222141 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 4.1 ug/L 12/29/16 20:22 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 155 of 245
AET Project No.03-06427 Page C155 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 142 Lab ID: 10374222142 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 21.1 ug/L 12/29/16 20:41 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 156 of 245
AET Project No.03-06427 Page C156 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 143 Lab ID: 10374222143 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 6.9 ug/L 12/29/16 20:44 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 157 of 245
AET Project No.03-06427 Page C157 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 144 Lab ID: 10374222144 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 28.0 ug/L 12/29/16 20:47 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 158 of 245
AET Project No.03-06427 Page C158 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 145 Lab ID: 10374222145 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 25.5 ug/L 12/29/16 20:50 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 159 of 245
AET Project No.03-06427 Page C159 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 146 Lab ID: 10374222146 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 8.4 ug/L 12/29/16 20:53 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 160 of 245
AET Project No.03-06427 Page C160 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 147 Lab ID: 10374222147 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 9.9 ug/L 12/29/16 20:56 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 161 of 245
AET Project No.03-06427 Page C161 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 148 Lab ID: 10374222148 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 6.9 ug/L 12/29/16 20:59 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 162 of 245
AET Project No.03-06427 Page C162 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 149 Lab ID: 10374222149 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 5.8 ug/L 12/29/16 21:01 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 163 of 245
AET Project No.03-06427 Page C163 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 150 Lab ID: 10374222150 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 3.7 ug/L 12/29/16 21:11 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 164 of 245
AET Project No.03-06427 Page C164 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 151 Lab ID: 10374222151 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.8 ug/L 12/29/16 21:14 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 165 of 245
AET Project No.03-06427 Page C165 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 152 Lab ID: 10374222152 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 3.2 ug/L 12/29/16 21:16 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 166 of 245
AET Project No.03-06427 Page C166 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 153 Lab ID: 10374222153 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.3 ug/L 12/29/16 21:20 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 167 of 245
AET Project No.03-06427 Page C167 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 154 Lab ID: 10374222154 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.90 ug/L 12/29/16 21:23 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 168 of 245
AET Project No.03-06427 Page C168 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 155 Lab ID: 10374222155 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.3 ug/L 12/29/16 21:26 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 169 of 245
AET Project No.03-06427 Page C169 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 156 Lab ID: 10374222156 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.36 ug/L 12/29/16 21:29 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 170 of 245
AET Project No.03-06427 Page C170 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 157 Lab ID: 10374222157 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.86 ug/L 12/29/16 21:32 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 171 of 245
AET Project No.03-06427 Page C171 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 158 Lab ID: 10374222158 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.0 ug/L 12/29/16 21:35 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 172 of 245
AET Project No.03-06427 Page C172 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 159 Lab ID: 10374222159 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.27 ug/L 12/29/16 21:38 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 173 of 245
AET Project No.03-06427 Page C173 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 160 Lab ID: 10374222160 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.9 ug/L 12/29/16 21:47 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 174 of 245
AET Project No.03-06427 Page C174 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 161 Lab ID: 10374222161 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 4.6 ug/L 12/28/16 08:22 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 175 of 245
AET Project No.03-06427 Page C175 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 162 Lab ID: 10374222162 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.40 ug/L 12/28/16 08:27 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 176 of 245
AET Project No.03-06427 Page C176 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 163 Lab ID: 10374222163 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.98 ug/L 12/28/16 08:28 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 177 of 245
AET Project No.03-06427 Page C177 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 164 Lab ID: 10374222164 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.9 ug/L 12/28/16 08:29 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 178 of 245
AET Project No.03-06427 Page C178 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 165 Lab ID: 10374222165 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.46 ug/L 12/28/16 08:32 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 179 of 245
AET Project No.03-06427 Page C179 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 166 Lab ID: 10374222166 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.1 ug/L 12/28/16 08:33 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 180 of 245
AET Project No.03-06427 Page C180 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 167 Lab ID: 10374222167 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.4 ug/L 12/28/16 08:34 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 181 of 245
AET Project No.03-06427 Page C181 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 168 Lab ID: 10374222168 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.41 ug/L 12/28/16 08:35 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 182 of 245
AET Project No.03-06427 Page C182 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 169 Lab ID: 10374222169 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.4 ug/L 12/28/16 08:36 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 183 of 245
AET Project No.03-06427 Page C183 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 170 Lab ID: 10374222170 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.9 ug/L 12/28/16 08:37 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 184 of 245
AET Project No.03-06427 Page C184 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 171 Lab ID: 10374222171 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.30 ug/L 12/28/16 08:38 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 185 of 245
AET Project No.03-06427 Page C185 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 172 Lab ID: 10374222172 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 5.1 ug/L 12/28/16 08:40 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 186 of 245
AET Project No.03-06427 Page C186 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 173 Lab ID: 10374222173 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 4.1 ug/L 12/28/16 08:41 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 187 of 245
AET Project No.03-06427 Page C187 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 174 Lab ID: 10374222174 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.73 ug/L 12/28/16 08:47 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 188 of 245
AET Project No.03-06427 Page C188 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 175 Lab ID: 10374222175 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.20 ug/L 12/28/16 08:48 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 189 of 245
AET Project No.03-06427 Page C189 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 176 Lab ID: 10374222176 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead ND ug/L 12/28/16 08:49 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 190 of 245
AET Project No.03-06427 Page C190 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 177 Lab ID: 10374222177 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.0 ug/L 12/28/16 08:50 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 191 of 245
AET Project No.03-06427 Page C191 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 178 Lab ID: 10374222178 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.26 ug/L 12/28/16 08:51 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 192 of 245
AET Project No.03-06427 Page C192 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 179 Lab ID: 10374222179 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.6 ug/L 12/28/16 08:52 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 193 of 245
AET Project No.03-06427 Page C193 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 180 Lab ID: 10374222180 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8 Preparation Method: EPA 200.8200.8 MET ICPMS
Lead 11.9 ug/L 12/29/16 22:23 7439-92-112/29/16 09:360.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 194 of 245
AET Project No.03-06427 Page C194 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 181 Lab ID: 10374222181 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.22 ug/L 12/28/16 08:53 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 195 of 245
AET Project No.03-06427 Page C195 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 182 Lab ID: 10374222182 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 4.1 ug/L 12/28/16 09:00 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 196 of 245
AET Project No.03-06427 Page C196 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 183 Lab ID: 10374222183 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.0 ug/L 12/28/16 09:01 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 197 of 245
AET Project No.03-06427 Page C197 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 184 Lab ID: 10374222184 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.6 ug/L 12/28/16 09:02 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 198 of 245
AET Project No.03-06427 Page C198 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 185 Lab ID: 10374222185 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.1 ug/L 12/28/16 09:03 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 199 of 245
AET Project No.03-06427 Page C199 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 186 Lab ID: 10374222186 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.37 ug/L 12/28/16 09:04 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 200 of 245
AET Project No.03-06427 Page C200 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 187 Lab ID: 10374222187 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.50 ug/L 12/28/16 09:05 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 201 of 245
AET Project No.03-06427 Page C201 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 188 Lab ID: 10374222188 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.1 ug/L 12/28/16 09:06 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 202 of 245
AET Project No.03-06427 Page C202 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 189 Lab ID: 10374222189 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.46 ug/L 12/28/16 09:07 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 203 of 245
AET Project No.03-06427 Page C203 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 190 Lab ID: 10374222190 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.5 ug/L 12/28/16 09:10 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 204 of 245
AET Project No.03-06427 Page C204 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 191 Lab ID: 10374222191 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.3 ug/L 12/28/16 09:11 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 205 of 245
AET Project No.03-06427 Page C205 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 192 Lab ID: 10374222192 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.64 ug/L 12/28/16 09:14 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 206 of 245
AET Project No.03-06427 Page C206 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 193 Lab ID: 10374222193 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.1 ug/L 12/28/16 09:15 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 207 of 245
AET Project No.03-06427 Page C207 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 194 Lab ID: 10374222194 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.80 ug/L 12/28/16 09:16 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 208 of 245
AET Project No.03-06427 Page C208 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 195 Lab ID: 10374222195 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.27 ug/L 12/28/16 09:17 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 209 of 245
AET Project No.03-06427 Page C209 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 196 Lab ID: 10374222196 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.5 ug/L 12/28/16 09:18 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 210 of 245
AET Project No.03-06427 Page C210 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 197 Lab ID: 10374222197 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.4 ug/L 12/28/16 09:19 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 211 of 245
AET Project No.03-06427 Page C211 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 198 Lab ID: 10374222198 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.38 ug/L 12/28/16 09:20 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 212 of 245
AET Project No.03-06427 Page C212 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 199 Lab ID: 10374222199 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.36 ug/L 12/28/16 09:25 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 213 of 245
AET Project No.03-06427 Page C213 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 200 Lab ID: 10374222200 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.12 ug/L 12/28/16 09:26 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 214 of 245
AET Project No.03-06427 Page C214 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 201 Lab ID: 10374222201 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.97 ug/L 12/28/16 09:27 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 215 of 245
AET Project No.03-06427 Page C215 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 202 Lab ID: 10374222202 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.31 ug/L 12/28/16 09:31 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 216 of 245
AET Project No.03-06427 Page C216 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 203 Lab ID: 10374222203 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.28 ug/L 12/28/16 09:33 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 217 of 245
AET Project No.03-06427 Page C217 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 204 Lab ID: 10374222204 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.18 ug/L 12/28/16 09:36 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 218 of 245
AET Project No.03-06427 Page C218 of 245
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Sample: 96(B) Lab ID: 10374222205 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead ND ug/L 12/28/16 09:37 7439-92-10.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 219 of 245
AET Project No.03-06427 Page C219 of 245
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
453250
EPA 200.8
EPA 200.8
ICPMS Metals, Drinking Water
Associated Lab Samples: 10374222001, 10374222002, 10374222003, 10374222004, 10374222005, 10374222006, 10374222007,10374222008, 10374222009, 10374222010, 10374222011, 10374222012, 10374222013, 10374222014,10374222015, 10374222016, 10374222017, 10374222018, 10374222019, 10374222020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2481496
Associated Lab Samples: 10374222001, 10374222002, 10374222003, 10374222004, 10374222005, 10374222006, 10374222007,10374222008, 10374222009, 10374222010, 10374222011, 10374222012, 10374222013, 10374222014,10374222015, 10374222016, 10374222017, 10374222018, 10374222019, 10374222020
Matrix: Water
Analyzed
Lead ug/L ND 0.10 12/27/16 13:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2481497LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 101100 101 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2482275MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
10374222001
2482276
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 100 96 70-13096 0 201000.21 96.7 96.5
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2482277MATRIX SPIKE SAMPLE:
MSSpike
Result
10374222011
Lead ug/L 113100 112 70-1301.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 220 of 245
AET Project No.03-06427 Page C220 of 245
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
453251
EPA 200.8
EPA 200.8
ICPMS Metals, Drinking Water
Associated Lab Samples: 10374222021, 10374222022, 10374222023, 10374222024, 10374222025, 10374222026, 10374222028,10374222029, 10374222030, 10374222031, 10374222032, 10374222033, 10374222034, 10374222035,10374222036, 10374222037, 10374222038, 10374222039, 10374222040
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2481499
Associated Lab Samples: 10374222021, 10374222022, 10374222023, 10374222024, 10374222025, 10374222026, 10374222028,10374222029, 10374222030, 10374222031, 10374222032, 10374222033, 10374222034, 10374222035,10374222036, 10374222037, 10374222038, 10374222039, 10374222040
Matrix: Water
Analyzed
Lead ug/L ND 0.10 12/27/16 14:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2481500LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 99.2100 99 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2482310MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
10374222021
2482311
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 100 100 70-13098 2 201002.2 102 100
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2482312MATRIX SPIKE SAMPLE:
MSSpike
Result
10374222032
Lead ug/L 110100 108 70-1302.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 221 of 245
AET Project No.03-06427 Page C221 of 245
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
453252
EPA 200.8
EPA 200.8
ICPMS Metals, Drinking Water
Associated Lab Samples: 10374222041, 10374222042, 10374222043, 10374222044, 10374222045, 10374222046, 10374222047,10374222048, 10374222049, 10374222050, 10374222051, 10374222052, 10374222053, 10374222054,10374222055, 10374222056, 10374222057, 10374222058, 10374222059, 10374222060
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2481503
Associated Lab Samples: 10374222041, 10374222042, 10374222043, 10374222044, 10374222045, 10374222046, 10374222047,10374222048, 10374222049, 10374222050, 10374222051, 10374222052, 10374222053, 10374222054,10374222055, 10374222056, 10374222057, 10374222058, 10374222059, 10374222060
Matrix: Water
Analyzed
Lead ug/L ND 0.10 12/27/16 15:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2481504LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 102100 102 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2482326MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
10374222041
2482327
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 100 98 70-130101 2 201000.82 99.3 102
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2482328MATRIX SPIKE SAMPLE:
MSSpike
Result
10374222051
Lead ug/L 112100 103 70-1309.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 222 of 245
AET Project No.03-06427 Page C222 of 245
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
453253
EPA 200.8
EPA 200.8
ICPMS Metals, Drinking Water
Associated Lab Samples: 10374222061, 10374222062, 10374222063, 10374222064, 10374222065, 10374222067, 10374222068,10374222069, 10374222070, 10374222071, 10374222072, 10374222073, 10374222075, 10374222076,10374222077, 10374222078, 10374222079, 10374222080
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2481507
Associated Lab Samples: 10374222061, 10374222062, 10374222063, 10374222064, 10374222065, 10374222067, 10374222068,10374222069, 10374222070, 10374222071, 10374222072, 10374222073, 10374222075, 10374222076,10374222077, 10374222078, 10374222079, 10374222080
Matrix: Water
Analyzed
Lead ug/L ND 0.10 12/27/16 15:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2481508LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 104100 104 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2482355MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
10374222061
2482356
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 100 98 70-13096 1 201000.34 97.9 96.6
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2482357MATRIX SPIKE SAMPLE:
MSSpike
Result
10374222072
Lead ug/L 108100 98 70-1309.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 223 of 245
AET Project No.03-06427 Page C223 of 245
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
453254
EPA 200.8
EPA 200.8
ICPMS Metals, Drinking Water
Associated Lab Samples: 10374222081, 10374222082, 10374222083, 10374222084, 10374222085, 10374222086, 10374222087,10374222088, 10374222089, 10374222090, 10374222091, 10374222092, 10374222093, 10374222094,10374222095, 10374222096, 10374222097, 10374222098, 10374222099, 10374222100
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2481512
Associated Lab Samples: 10374222081, 10374222082, 10374222083, 10374222084, 10374222085, 10374222086, 10374222087,10374222088, 10374222089, 10374222090, 10374222091, 10374222092, 10374222093, 10374222094,10374222095, 10374222096, 10374222097, 10374222098, 10374222099, 10374222100
Matrix: Water
Analyzed
Lead ug/L ND 0.10 12/27/16 17:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2481513LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 101100 101 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2482370MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
10374222081
2482371
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 100 102 70-13099 2 201001.8 103 101
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2482372MATRIX SPIKE SAMPLE:
MSSpike
Result
10374222091
Lead ug/L 99.5100 99 70-1300.54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 224 of 245
AET Project No.03-06427 Page C224 of 245
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
453255
EPA 200.8
EPA 200.8
ICPMS Metals, Drinking Water
Associated Lab Samples: 10374222101, 10374222102, 10374222103, 10374222104, 10374222105, 10374222106, 10374222107,10374222108, 10374222109, 10374222110, 10374222111, 10374222112, 10374222113, 10374222114,10374222115, 10374222116, 10374222117, 10374222118, 10374222119, 10374222120
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2481517
Associated Lab Samples: 10374222101, 10374222102, 10374222103, 10374222104, 10374222105, 10374222106, 10374222107,10374222108, 10374222109, 10374222110, 10374222111, 10374222112, 10374222113, 10374222114,10374222115, 10374222116, 10374222117, 10374222118, 10374222119, 10374222120
Matrix: Water
Analyzed
Lead ug/L ND 0.10 12/27/16 17:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2481518LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 102100 102 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2482412MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
10374222101
2482413
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 100 98 70-130101 3 201003.0 101 104
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2482414MATRIX SPIKE SAMPLE:
MSSpike
Result
10374222111
Lead ug/L 96.7100 96 70-1300.48
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 225 of 245
AET Project No.03-06427 Page C225 of 245
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
453256
EPA 200.8
EPA 200.8
ICPMS Metals, Drinking Water
Associated Lab Samples: 10374222121, 10374222122, 10374222123, 10374222124, 10374222125, 10374222126, 10374222127,10374222128, 10374222129, 10374222130, 10374222131, 10374222132, 10374222133, 10374222134,10374222135, 10374222136, 10374222137, 10374222138, 10374222139, 10374222140
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2481521
Associated Lab Samples: 10374222121, 10374222122, 10374222123, 10374222124, 10374222125, 10374222126, 10374222127,10374222128, 10374222129, 10374222130, 10374222131, 10374222132, 10374222133, 10374222134,10374222135, 10374222136, 10374222137, 10374222138, 10374222139, 10374222140
Matrix: Water
Analyzed
Lead ug/L ND 0.10 12/29/16 18:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2481522LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 104100 104 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2482588MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
10374222121
2482589
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 100 100 70-13099 1 201002.4 103 101
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2482590MATRIX SPIKE SAMPLE:
MSSpike
Result
10374222140
Lead ug/L 103100 97 70-1305.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 226 of 245
AET Project No.03-06427 Page C226 of 245
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
453257
EPA 200.8
EPA 200.8
ICPMS Metals, Drinking Water
Associated Lab Samples: 10374222141, 10374222142, 10374222143, 10374222144, 10374222145, 10374222146, 10374222147,10374222148, 10374222149, 10374222150, 10374222151, 10374222152, 10374222153, 10374222154,10374222155, 10374222156, 10374222157, 10374222158, 10374222159, 10374222160
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2481524
Associated Lab Samples: 10374222141, 10374222142, 10374222143, 10374222144, 10374222145, 10374222146, 10374222147,10374222148, 10374222149, 10374222150, 10374222151, 10374222152, 10374222153, 10374222154,10374222155, 10374222156, 10374222157, 10374222158, 10374222159, 10374222160
Matrix: Water
Analyzed
Lead ug/L ND 0.10 12/29/16 19:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2481525LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 106100 106 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2483480MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
10374222141
2483481
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 100 99 70-13097 1 201004.1 103 101
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2483482MATRIX SPIKE SAMPLE:
MSSpike
Result
10374222160
Lead ug/L 103100 101 70-1301.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 227 of 245
AET Project No.03-06427 Page C227 of 245
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
453258
EPA 200.8
EPA 200.8
ICPMS Metals, Drinking Water
Associated Lab Samples: 10374222161, 10374222162, 10374222163, 10374222164, 10374222165, 10374222166, 10374222167,10374222168, 10374222169, 10374222170, 10374222171, 10374222172, 10374222173, 10374222174,10374222175, 10374222176, 10374222177, 10374222178, 10374222179
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2481529
Associated Lab Samples: 10374222161, 10374222162, 10374222163, 10374222164, 10374222165, 10374222166, 10374222167,10374222168, 10374222169, 10374222170, 10374222171, 10374222172, 10374222173, 10374222174,10374222175, 10374222176, 10374222177, 10374222178, 10374222179
Matrix: Water
Analyzed
Lead ug/L ND 0.10 12/28/16 08:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2481530LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 99.7100 100 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2482571MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
10374222161
2482572
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 100 99 70-13095 4 201004.6 103 99.2
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2482573MATRIX SPIKE SAMPLE:
MSSpike
Result
10374222171
Lead ug/L 95.9100 96 70-1300.30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 228 of 245
AET Project No.03-06427 Page C228 of 245
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
453259
EPA 200.8
EPA 200.8
ICPMS Metals, Drinking Water
Associated Lab Samples: 10374222181, 10374222182, 10374222183, 10374222184, 10374222185, 10374222186, 10374222187,10374222188, 10374222189, 10374222190, 10374222191, 10374222192, 10374222193, 10374222194,10374222195, 10374222196, 10374222197, 10374222198, 10374222199, 10374222200
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2481535
Associated Lab Samples: 10374222181, 10374222182, 10374222183, 10374222184, 10374222185, 10374222186, 10374222187,10374222188, 10374222189, 10374222190, 10374222191, 10374222192, 10374222193, 10374222194,10374222195, 10374222196, 10374222197, 10374222198, 10374222199, 10374222200
Matrix: Water
Analyzed
Lead ug/L ND 0.10 12/28/16 08:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2481536LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 96.2100 96 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2482576MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
10374222181
2482577
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 100 90 70-13095 5 201000.22 90.1 95.0
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2482578MATRIX SPIKE SAMPLE:
MSSpike
Result
10374222191
Lead ug/L 94.7100 92 70-1302.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 229 of 245
AET Project No.03-06427 Page C229 of 245
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
453260
EPA 200.8
EPA 200.8
ICPMS Metals, Drinking Water
Associated Lab Samples: 10374222201, 10374222202, 10374222203, 10374222204, 10374222205
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2481539
Associated Lab Samples: 10374222201, 10374222202, 10374222203, 10374222204, 10374222205
Matrix: Water
Analyzed
Lead ug/L ND 0.10 12/28/16 09:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2481540LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 97.5100 98 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2482585MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
10374222201
2482586
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 100 96 70-13096 1 201000.97 97.4 96.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 230 of 245
AET Project No.03-06427 Page C230 of 245
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
453517
EPA 200.8
EPA 200.8
200.8 MET
Associated Lab Samples: 10374222027, 10374222066, 10374222074, 10374222180
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2482629
Associated Lab Samples: 10374222027, 10374222066, 10374222074, 10374222180
Matrix: Water
Analyzed
Lead ug/L ND 0.10 12/29/16 21:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2482630LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 106100 106 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2482631MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
10374222027
2482632
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 100 105 70-130105 0 2010014.8 120 120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 231 of 245
AET Project No.03-06427 Page C231 of 245
#=QL#
QUALIFIERS
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - MinneapolisPASI-M
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 232 of 245
AET Project No.03-06427 Page C232 of 245
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
10374222001 4532501 EPA 200.8
10374222002 4532502 EPA 200.8
10374222003 4532503 EPA 200.8
10374222004 4532504 EPA 200.8
10374222005 4532505 EPA 200.8
10374222006 4532506 EPA 200.8
10374222007 4532507 EPA 200.8
10374222008 4532508 EPA 200.8
10374222009 4532509 EPA 200.8
10374222010 45325010 EPA 200.8
10374222011 45325011 EPA 200.8
10374222012 45325012 EPA 200.8
10374222013 45325013 EPA 200.8
10374222014 45325014 EPA 200.8
10374222015 45325015 EPA 200.8
10374222016 45325016 EPA 200.8
10374222017 45325017 EPA 200.8
10374222018 45325018 EPA 200.8
10374222019 45325019 EPA 200.8
10374222020 45325020 EPA 200.8
10374222021 45325121 EPA 200.8
10374222022 45325122 EPA 200.8
10374222023 45325123 EPA 200.8
10374222024 45325124 EPA 200.8
10374222025 45325125 EPA 200.8
10374222026 45325126 EPA 200.8
10374222028 45325128 EPA 200.8
10374222029 45325129 EPA 200.8
10374222030 45325130 EPA 200.8
10374222031 45325131 EPA 200.8
10374222032 45325132 EPA 200.8
10374222033 45325133 EPA 200.8
10374222034 45325134 EPA 200.8
10374222035 45325135 EPA 200.8
10374222036 45325136 EPA 200.8
10374222037 45325137 EPA 200.8
10374222038 45325138 EPA 200.8
10374222039 45325139 EPA 200.8
10374222040 45325140 EPA 200.8
10374222041 45325241 EPA 200.8
10374222042 45325242 EPA 200.8
10374222043 45325243 EPA 200.8
10374222044 45325244 EPA 200.8
10374222045 45325245 EPA 200.8
10374222046 45325246 EPA 200.8
10374222047 45325247 EPA 200.8
10374222048 45325248 EPA 200.8
10374222049 45325249 EPA 200.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 233 of 245
AET Project No.03-06427 Page C233 of 245
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
10374222050 45325250 EPA 200.8
10374222051 45325251 EPA 200.8
10374222052 45325252 EPA 200.8
10374222053 45325253 EPA 200.8
10374222054 45325254 EPA 200.8
10374222055 45325255 EPA 200.8
10374222056 45325256 EPA 200.8
10374222057 45325257 EPA 200.8
10374222058 45325258 EPA 200.8
10374222059 45325259 EPA 200.8
10374222060 45325260 EPA 200.8
10374222061 45325361 EPA 200.8
10374222062 45325362 EPA 200.8
10374222063 45325363 EPA 200.8
10374222064 45325364 EPA 200.8
10374222065 45325365 EPA 200.8
10374222067 45325367 EPA 200.8
10374222068 45325368 EPA 200.8
10374222069 45325369 EPA 200.8
10374222070 45325370 EPA 200.8
10374222071 45325371 EPA 200.8
10374222072 45325372 EPA 200.8
10374222073 45325373 EPA 200.8
10374222075 45325375 EPA 200.8
10374222076 45325376 EPA 200.8
10374222077 45325377 EPA 200.8
10374222078 45325378 EPA 200.8
10374222079 45325379 EPA 200.8
10374222080 45325380 EPA 200.8
10374222081 45325481 EPA 200.8
10374222082 45325482 EPA 200.8
10374222083 45325483 EPA 200.8
10374222084 45325484 EPA 200.8
10374222085 45325485 EPA 200.8
10374222086 45325486 EPA 200.8
10374222087 45325487 EPA 200.8
10374222088 45325488 EPA 200.8
10374222089 45325489 EPA 200.8
10374222090 45325490 EPA 200.8
10374222091 45325491 EPA 200.8
10374222092 45325492 EPA 200.8
10374222093 45325493 EPA 200.8
10374222094 45325494 EPA 200.8
10374222095 45325495 EPA 200.8
10374222096 45325496 (A) EPA 200.8
10374222097 45325497 EPA 200.8
10374222098 45325498 EPA 200.8
10374222099 45325499 EPA 200.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 234 of 245
AET Project No.03-06427 Page C234 of 245
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
10374222100 453254100 EPA 200.8
10374222101 453255101 EPA 200.8
10374222102 453255102 EPA 200.8
10374222103 453255103 EPA 200.8
10374222104 453255104 EPA 200.8
10374222105 453255105 EPA 200.8
10374222106 453255106 EPA 200.8
10374222107 453255107 EPA 200.8
10374222108 453255108 EPA 200.8
10374222109 453255109 EPA 200.8
10374222110 453255110 EPA 200.8
10374222111 453255111 EPA 200.8
10374222112 453255112 EPA 200.8
10374222113 453255113 EPA 200.8
10374222114 453255114 EPA 200.8
10374222115 453255115 EPA 200.8
10374222116 453255116 EPA 200.8
10374222117 453255117 EPA 200.8
10374222118 453255118 EPA 200.8
10374222119 453255119 EPA 200.8
10374222120 453255120 EPA 200.8
10374222121 453256121 EPA 200.8
10374222122 453256122 EPA 200.8
10374222123 453256123 EPA 200.8
10374222124 453256124 EPA 200.8
10374222125 453256125 EPA 200.8
10374222126 453256126 EPA 200.8
10374222127 453256127 EPA 200.8
10374222128 453256128 EPA 200.8
10374222129 453256129 EPA 200.8
10374222130 453256130 EPA 200.8
10374222131 453256131 EPA 200.8
10374222132 453256132 EPA 200.8
10374222133 453256133 EPA 200.8
10374222134 453256134 EPA 200.8
10374222135 453256135 EPA 200.8
10374222136 453256136 EPA 200.8
10374222137 453256137 EPA 200.8
10374222138 453256138 EPA 200.8
10374222139 453256139 EPA 200.8
10374222140 453256140 EPA 200.8
10374222141 453257141 EPA 200.8
10374222142 453257142 EPA 200.8
10374222143 453257143 EPA 200.8
10374222144 453257144 EPA 200.8
10374222145 453257145 EPA 200.8
10374222146 453257146 EPA 200.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 235 of 245
AET Project No.03-06427 Page C235 of 245
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
10374222147 453257147 EPA 200.8
10374222148 453257148 EPA 200.8
10374222149 453257149 EPA 200.8
10374222150 453257150 EPA 200.8
10374222151 453257151 EPA 200.8
10374222152 453257152 EPA 200.8
10374222153 453257153 EPA 200.8
10374222154 453257154 EPA 200.8
10374222155 453257155 EPA 200.8
10374222156 453257156 EPA 200.8
10374222157 453257157 EPA 200.8
10374222158 453257158 EPA 200.8
10374222159 453257159 EPA 200.8
10374222160 453257160 EPA 200.8
10374222161 453258161 EPA 200.8
10374222162 453258162 EPA 200.8
10374222163 453258163 EPA 200.8
10374222164 453258164 EPA 200.8
10374222165 453258165 EPA 200.8
10374222166 453258166 EPA 200.8
10374222167 453258167 EPA 200.8
10374222168 453258168 EPA 200.8
10374222169 453258169 EPA 200.8
10374222170 453258170 EPA 200.8
10374222171 453258171 EPA 200.8
10374222172 453258172 EPA 200.8
10374222173 453258173 EPA 200.8
10374222174 453258174 EPA 200.8
10374222175 453258175 EPA 200.8
10374222176 453258176 EPA 200.8
10374222177 453258177 EPA 200.8
10374222178 453258178 EPA 200.8
10374222179 453258179 EPA 200.8
10374222181 453259181 EPA 200.8
10374222182 453259182 EPA 200.8
10374222183 453259183 EPA 200.8
10374222184 453259184 EPA 200.8
10374222185 453259185 EPA 200.8
10374222186 453259186 EPA 200.8
10374222187 453259187 EPA 200.8
10374222188 453259188 EPA 200.8
10374222189 453259189 EPA 200.8
10374222190 453259190 EPA 200.8
10374222191 453259191 EPA 200.8
10374222192 453259192 EPA 200.8
10374222193 453259193 EPA 200.8
10374222194 453259194 EPA 200.8
10374222195 453259195 EPA 200.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 236 of 245
AET Project No.03-06427 Page C236 of 245
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
10374222
03-06427 Jefferson Pb Water
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
10374222196 453259196 EPA 200.8
10374222197 453259197 EPA 200.8
10374222198 453259198 EPA 200.8
10374222199 453259199 EPA 200.8
10374222200 453259200 EPA 200.8
10374222201 453260201 EPA 200.8
10374222202 453260202 EPA 200.8
10374222203 453260203 EPA 200.8
10374222204 453260204 EPA 200.8
10374222205 45326096(B) EPA 200.8
10374222027 453517 45379227 EPA 200.8 EPA 200.8
10374222066 453517 45379266 EPA 200.8 EPA 200.8
10374222074 453517 45379274 EPA 200.8 EPA 200.8
10374222180 453517 453792180 EPA 200.8 EPA 200.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607-1700
Page 237 of 245
AET Project No.03-06427 Page C237 of 245
for fields of accreditation listed on the laboratory's accompanying Scope of Certification
in accordance with the provisions in Minnesota Laws and Rules.
Continued accreditation is contingent upon successful on-going compliance with Minnesota Statutes 144.97 to 144.98, 2009 TNI
Standard and applicable Minnesota Rules 4740.2010 to 4740.2120. The laboratory's Scope of Certification cites the specific
programs, methods, analytes and matrices for which MDH issues this accreditation.
This certificate is valid proof of accreditation only when associated with its accompanying Scope of Certification.
The Scope of Certification and reports of on-site assessments are on file at the Minnesota Department of Health,
601 Robert Street North, Saint Paul, Minnesota. Customers may verify the laboratory's accreditation status in
Minnesota by contacting MNELAP at (651) 201-5324.
Minnesota Department of Health
Environmental Laboratory Accreditation Program
Issues accreditation to
State Laboratory ID: 027-053-137
EPA Lab Code: MN00064
Pace Analytical Services, LLC. - Minneapolis MN
1700 Elm Street SE, Suite 200
Minneapolis, MN 55414
Effective Date: 12/22/2016
Expires: 12/31/2017
Certificate Number: 1179284
Issued under the authoritydelegated by theCommissioner of Health,State of Minnesota
AET Project No. 03-06427 Page D3 of 90
Printed on 12/22/2016
THIS LISTING OF FIELDS OF ACCREDITATION MUST BE
ACCOMPANIED BY CERTIFICATE NUMBER: 1179284
Pace Analytical Services, LLC. - Minneapolis MN
1700 Elm Street SE, Suite 200
Minneapolis, MN 55414
EPA 3C Preparation Techniques: N/A
EPA Method 23 Preparation Techniques: N/A
Environmental Laboratory Accreditation Program
Scope of Certification
State Laboratory ID: 027-053-137 EPA Lab Code: MN00064 Issue Date: 12/22/2016
Expiration Date: 12/31/2017
Clean Air Act
Program Method Analyte Matrix Primary SOP
CAA EPA 3C Carbon dioxide AIR MN
CAA EPA 3C Carbon monoxide AIR MN
CAA EPA 3C Methane AIR MN
CAA EPA 3C Nitrogen AIR MN
CAA EPA 3C Oxygen AIR MN
Program Method Analyte Matrix Primary SOP
CAA EPA Method 23 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)
AIR MN
CAA EPA Method 23 1,2,3,4,6,7,8,9-Octachlorodibenzofuran(OCDF)
AIR MN
CAA EPA Method 23 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)
AIR MN
CAA EPA Method 23 1,2,3,4,6,7,8-Heptachlorodibenzofuran(1,2,3,4,6,7,8-hpcdf)
AIR MN
Page 1 of 87
AET Project No. 03-06427 Page D4 of 90
Printed on 12/22/2016
EPA RSK-175 (GC/FID) Preparation Techniques: N/A
EPA TO-13A Preparation Techniques: N/A
Program Method Analyte Matrix Primary SOP
CAA EPA Method 23 1,2,3,4,7,8,9-Heptachlorodibenzofuran(1,2,3,4,7,8,9-hpcdf)
AIR MN
CAA EPA Method 23 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,4,7,8-Hxcdd)
AIR MN
CAA EPA Method 23 1,2,3,4,7,8-Hexachlorodibenzofuran(1,2,3,4,7,8-Hxcdf)
AIR MN
CAA EPA Method 23 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,6,7,8-Hxcdd)
AIR MN
CAA EPA Method 23 1,2,3,6,7,8-Hexachlorodibenzofuran(1,2,3,6,7,8-Hxcdf)
AIR MN
CAA EPA Method 23 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin(1,2,3,7,8,9-Hxcdd)
AIR MN
CAA EPA Method 23 1,2,3,7,8,9-Hexachlorodibenzofuran(1,2,3,7,8,9-Hxcdf)
AIR MN
CAA EPA Method 23 1,2,3,7,8-Pentachlorodibenzo-p-dioxin(1,2,3,7,8-Pecdd)
AIR MN
CAA EPA Method 23 1,2,3,7,8-Pentachlorodibenzofuran(1,2,3,7,8-Pecdf)
AIR MN
CAA EPA Method 23 2,3,4,6,7,8-Hexachlorodibenzofuran AIR MN
CAA EPA Method 23 2,3,4,7,8-Pentachlorodibenzofuran AIR MN
CAA EPA Method 23 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)
AIR MN
CAA EPA Method 23 2,3,7,8-Tetrachlorodibenzofuran AIR MN
Program Method Analyte Matrix Primary SOP
CAA EPA RSK-175 (GC/FID) Ethane AIR MN
CAA EPA RSK-175 (GC/FID) Ethene AIR MN
CAA EPA RSK-175 (GC/FID) Methane AIR MN
CAA EPA RSK-175 (GC/FID) n-Propane AIR MN
Program Method Analyte Matrix Primary SOP
CAA EPA TO-13A 2-Methylnaphthalene AIR MN
CAA EPA TO-13A Acenaphthene AIR MN
CAA EPA TO-13A Acenaphthylene AIR MN
Page 2 of 87
AET Project No. 03-06427 Page D5 of 90
Printed on 12/22/2016
EPA TO-14A Preparation Techniques: N/A
Program Method Analyte Matrix Primary SOP
CAA EPA TO-13A Anthracene AIR MN
CAA EPA TO-13A Benzo(a)anthracene AIR MN
CAA EPA TO-13A Benzo(a)pyrene AIR MN
CAA EPA TO-13A Benzo(e)pyrene AIR MN
CAA EPA TO-13A Benzo(g,h,i)perylene AIR MN
CAA EPA TO-13A Benzo(k)fluoranthene AIR MN
CAA EPA TO-13A Benzo[b]fluoranthene AIR MN
CAA EPA TO-13A Chrysene AIR MN
CAA EPA TO-13A Dibenz(a,h) anthracene AIR MN
CAA EPA TO-13A Fluoranthene AIR MN
CAA EPA TO-13A Fluorene AIR MN
CAA EPA TO-13A Indeno(1,2,3-cd) pyrene AIR MN
CAA EPA TO-13A Naphthalene AIR MN
CAA EPA TO-13A Phenanthrene AIR MN
CAA EPA TO-13A Pyrene AIR MN
Program Method Analyte Matrix Primary SOP
CAA EPA TO-14A 1,1,1-Trichloroethane AIR MN
CAA EPA TO-14A 1,1,2,2-Tetrachloroethane AIR MN
CAA EPA TO-14A 1,1,2-Trichloro-1,2,2-trifluoroethane(Freon 113)
AIR MN
CAA EPA TO-14A 1,1,2-Trichloroethane AIR MN
CAA EPA TO-14A 1,1-Dichloroethane AIR MN
CAA EPA TO-14A 1,1-Dichloroethylene AIR MN
CAA EPA TO-14A 1,2,4-Trichlorobenzene AIR MN
CAA EPA TO-14A 1,2,4-Trimethylbenzene AIR MN
CAA EPA TO-14A 1,2-Dibromoethane (EDB, Ethylenedibromide)
AIR MN
CAA EPA TO-14A 1,2-Dichloro-1,1,2,2-tetrafluoroethane(Freon-114)
AIR MN
CAA EPA TO-14A 1,2-Dichlorobenzene AIR MN
CAA EPA TO-14A 1,2-Dichloroethane (Ethylene dichloride) AIR MN
CAA EPA TO-14A 1,2-Dichloroethene (total) AIR MN
CAA EPA TO-14A 1,2-Dichloropropane AIR MN
Page 3 of 87
AET Project No. 03-06427 Page D6 of 90
Printed on 12/22/2016
EPA TO-17
Program Method Analyte Matrix Primary SOP
CAA EPA TO-14A 1,3-Dichlorobenzene AIR MN
CAA EPA TO-14A 1,4-Dichlorobenzene AIR MN
CAA EPA TO-14A Benzene AIR MN
CAA EPA TO-14A Benzyl chloride AIR MN
CAA EPA TO-14A Bromoform AIR MN
CAA EPA TO-14A Bromomethane AIR MN
CAA EPA TO-14A Carbon tetrachloride AIR MN
CAA EPA TO-14A Chlorobenzene AIR MN
CAA EPA TO-14A Chloroethane (Ethyl chloride) AIR MN
CAA EPA TO-14A Chloroform AIR MN
CAA EPA TO-14A cis-1,2-Dichloroethylene AIR MN
CAA EPA TO-14A cis-1,3-Dichloropropene AIR MN
CAA EPA TO-14A Dichlorodifluoromethane (Freon-12) AIR MN
CAA EPA TO-14A Ethylbenzene AIR MN
CAA EPA TO-14A Hexachloro-1,3-butadiene AIR MN
CAA EPA TO-14A Hexachlorobutadiene AIR MN
CAA EPA TO-14A m+p-xylene AIR MN
CAA EPA TO-14A Methyl chloride (Chloromethane) AIR MN
CAA EPA TO-14A Methyl tert-butyl ether (MTBE) AIR MN
CAA EPA TO-14A Methylene chloride (Dichloromethane) AIR MN
CAA EPA TO-14A n-Hexane AIR MN
CAA EPA TO-14A o-Xylene AIR MN
CAA EPA TO-14A Styrene AIR MN
CAA EPA TO-14A Tetrachloroethene AIR MN
CAA EPA TO-14A THC as Gas AIR MN
CAA EPA TO-14A Toluene AIR MN
CAA EPA TO-14A trans-1,2-Dichloroethylene AIR MN
CAA EPA TO-14A trans-1,3-Dichloropropylene AIR MN
CAA EPA TO-14A Trichloroethene (Trichloroethylene) AIR MN
CAA EPA TO-14A Trichlorofluoromethane(Fluorotrichloromethane, Freon 11)
AIR MN
CAA EPA TO-14A Vinyl chloride AIR MN
CAA EPA TO-14A Xylene (total) AIR MN
Page 4 of 87
AET Project No. 03-06427 Page D7 of 90
Printed on 12/22/2016
Preparation Techniques: N/A
Program Method Analyte Matrix Primary SOP
CAA EPA TO-17 1,1,1-Trichloroethane AIR MN
CAA EPA TO-17 1,1,2,2-Tetrachloroethane AIR MN
CAA EPA TO-17 1,1,2-Trichloro-1,2,2-trifluoroethane(Freon 113)
AIR MN
CAA EPA TO-17 1,1,2-Trichloroethane AIR MN
CAA EPA TO-17 1,1-Dichloroethane AIR MN
CAA EPA TO-17 1,1-Dichloroethylene AIR MN
CAA EPA TO-17 1,2,4-Trichlorobenzene AIR MN
CAA EPA TO-17 1,2,4-Trimethylbenzene AIR MN
CAA EPA TO-17 1,2-Dibromoethane (EDB, Ethylenedibromide)
AIR MN
CAA EPA TO-17 1,2-Dichlorobenzene AIR MN
CAA EPA TO-17 1,2-Dichloroethane (Ethylene dichloride) AIR MN
CAA EPA TO-17 1,2-Dichloropropane AIR MN
CAA EPA TO-17 1,3,5-Trimethylbenzene AIR MN
CAA EPA TO-17 1,3-Butadiene AIR MN
CAA EPA TO-17 1,3-Dichlorobenzene AIR MN
CAA EPA TO-17 1,4-Dichlorobenzene AIR MN
CAA EPA TO-17 1,4-Dioxane (1,4- Diethyleneoxide) AIR MN
CAA EPA TO-17 2-Butanone (Methyl ethyl ketone, MEK) AIR MN
CAA EPA TO-17 2-Hexanone AIR MN
CAA EPA TO-17 4-Ethyltoluene AIR MN
CAA EPA TO-17 4-Methyl-2-pentanone (MIBK) AIR MN
CAA EPA TO-17 Acetone AIR MN
CAA EPA TO-17 Acrolein (Propenal) AIR MN
CAA EPA TO-17 Acrylonitrile AIR MN
CAA EPA TO-17 Benzene AIR MN
CAA EPA TO-17 Benzyl chloride AIR MN
CAA EPA TO-17 Bromodichloromethane AIR MN
CAA EPA TO-17 Bromoform AIR MN
CAA EPA TO-17 Bromomethane AIR MN
CAA EPA TO-17 Carbon disulfide AIR MN
CAA EPA TO-17 Carbon tetrachloride AIR MN
CAA EPA TO-17 Chlorobenzene AIR MN
CAA EPA TO-17 Chloroethane (Ethyl chloride) AIR MN
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Program Method Analyte Matrix Primary SOP
CAA EPA TO-17 Chloroform AIR MN
CAA EPA TO-17 cis-1,2-Dichloroethylene AIR MN
CAA EPA TO-17 cis-1,3-Dichloropropene AIR MN
CAA EPA TO-17 Cyclohexane AIR MN
CAA EPA TO-17 Dibromochloromethane AIR MN
CAA EPA TO-17 Dichlorodifluoromethane (Freon-12) AIR MN
CAA EPA TO-17 Dichlorotetrafluoroethane AIR MN
CAA EPA TO-17 Ethanol AIR MN
CAA EPA TO-17 Ethyl acetate AIR MN
CAA EPA TO-17 Ethylbenzene AIR MN
CAA EPA TO-17 Hexachloro-1,3-butadiene AIR MN
CAA EPA TO-17 Isopropyl alcohol (2-Propanol,Isopropanol)
AIR MN
CAA EPA TO-17 Isopropylbenzene AIR MN
CAA EPA TO-17 m+p-xylene AIR MN
CAA EPA TO-17 Methyl chloride (Chloromethane) AIR MN
CAA EPA TO-17 Methyl tert-butyl ether (MTBE) AIR MN
CAA EPA TO-17 Methylene chloride (Dichloromethane) AIR MN
CAA EPA TO-17 n-Butylbenzene AIR MN
CAA EPA TO-17 n-Heptane AIR MN
CAA EPA TO-17 n-Hexane AIR MN
CAA EPA TO-17 n-Propylbenzene AIR MN
CAA EPA TO-17 Naphthalene AIR MN
CAA EPA TO-17 o-Xylene AIR MN
CAA EPA TO-17 sec-Butylbenzene AIR MN
CAA EPA TO-17 Styrene AIR MN
CAA EPA TO-17 Tetrachloroethene AIR MN
CAA EPA TO-17 Tetrahydrofuran (THF) AIR MN
CAA EPA TO-17 Toluene AIR MN
CAA EPA TO-17 trans-1,2-Dichloroethylene AIR MN
CAA EPA TO-17 trans-1,3-Dichloropropylene AIR MN
CAA EPA TO-17 Trichloroethene (Trichloroethylene) AIR MN
CAA EPA TO-17 Trichlorofluoromethane(Fluorotrichloromethane, Freon 11)
AIR MN
CAA EPA TO-17 Vinyl acetate AIR MN
CAA EPA TO-17 Vinyl chloride AIR MN
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EPA TO-3 Preparation Techniques: N/A
EPA TO-9A Preparation Techniques: N/A
Program Method Analyte Matrix Primary SOP
CAA EPA TO-3 1,2,4-Trimethylbenzene AIR MN
CAA EPA TO-3 Benzene AIR MN
CAA EPA TO-3 Ethane AIR MN
CAA EPA TO-3 Ethene AIR MN
CAA EPA TO-3 Ethylbenzene AIR MN
CAA EPA TO-3 m+p-xylene AIR MN
CAA EPA TO-3 Methane AIR MN
CAA EPA TO-3 Methyl tert-butyl ether (MTBE) AIR MN
CAA EPA TO-3 n-Hexane AIR MN
CAA EPA TO-3 o-Xylene AIR MN
CAA EPA TO-3 THC as C1-C4 AIR MN
CAA EPA TO-3 THC as Gas AIR MN
CAA EPA TO-3 Toluene AIR MN
CAA EPA TO-3 Total BTEX AIR MN
CAA EPA TO-3 Xylene (total) AIR MN
Program Method Analyte Matrix Primary SOP
CAA EPA TO-9A 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)
AIR MN
CAA EPA TO-9A 1,2,3,4,6,7,8,9-Octachlorodibenzofuran(OCDF)
AIR MN
CAA EPA TO-9A 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)
AIR MN
CAA EPA TO-9A 1,2,3,4,6,7,8-Heptachlorodibenzofuran(1,2,3,4,6,7,8-hpcdf)
AIR MN
CAA EPA TO-9A 1,2,3,4,7,8,9-Heptachlorodibenzofuran(1,2,3,4,7,8,9-hpcdf)
AIR MN
CAA EPA TO-9A 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,4,7,8-Hxcdd)
AIR MN
CAA EPA TO-9A 1,2,3,4,7,8-Hexachlorodibenzofuran(1,2,3,4,7,8-Hxcdf)
AIR MN
CAA EPA TO-9A 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,6,7,8-Hxcdd)
AIR MN
CAA EPA TO-9A 1,2,3,6,7,8-Hexachlorodibenzofuran(1,2,3,6,7,8-Hxcdf)
AIR MN
Page 7 of 87
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ASTM D516-90 Preparation Techniques: N/A
EPA 120.1 Preparation Techniques: N/A
EPA 160.4 Preparation Techniques: N/A
EPA 1664A (HEM) Preparation Techniques: Extraction, separatory funnel liquid-liquid (LLE);
Program Method Analyte Matrix Primary SOP
CAA EPA TO-9A 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin(1,2,3,7,8,9-Hxcdd)
AIR MN
CAA EPA TO-9A 1,2,3,7,8,9-Hexachlorodibenzofuran(1,2,3,7,8,9-Hxcdf)
AIR MN
CAA EPA TO-9A 1,2,3,7,8-Pentachlorodibenzo-p-dioxin(1,2,3,7,8-Pecdd)
AIR MN
CAA EPA TO-9A 1,2,3,7,8-Pentachlorodibenzofuran(1,2,3,7,8-Pecdf)
AIR MN
CAA EPA TO-9A 2,3,4,6,7,8-Hexachlorodibenzofuran AIR MN
CAA EPA TO-9A 2,3,4,7,8-Pentachlorodibenzofuran AIR MN
CAA EPA TO-9A 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)
AIR MN
CAA EPA TO-9A 2,3,7,8-Tetrachlorodibenzofuran AIR MN
Clean Water Program
Program Method Analyte Matrix Primary SOP
CWP ASTM D516-90 Sulfate NPW MN
Program Method Analyte Matrix Primary SOP
CWP EPA 120.1 Conductivity NPW MN
Program Method Analyte Matrix Primary SOP
CWP EPA 160.4 Residue-volatile NPW MN
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EPA 1664A (SGT-HEM) Preparation Techniques: Extraction, solid phase (SPE);
EPA 180.1 Preparation Techniques: N/A
EPA 300.0 Preparation Techniques: N/A
EPA 300.0 Preparation Techniques: N/A
EPA 350.1
Program Method Analyte Matrix Primary SOP
CWP EPA 1664A (HEM) Oil & Grease NPW MN
Program Method Analyte Matrix Primary SOP
CWP EPA 1664A (SGT-HEM) Oil & Grease NPW MN
Program Method Analyte Matrix Primary SOP
CWP EPA 180.1 Turbidity NPW MN
Program Method Analyte Matrix Primary SOP
CWP EPA 300.0 Bromide NPW MN
CWP EPA 300.0 Chloride NPW MN
CWP EPA 300.0 Fluoride NPW MN
CWP EPA 300.0 Nitrate as N NPW MN
CWP EPA 300.0 Nitrite as N NPW MN
CWP EPA 300.0 Sulfate NPW MN
Program Method Analyte Matrix Primary SOP
CWP EPA 300.0 Bromide NPW MN
Page 9 of 87
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Preparation Techniques: Distillation, MIDI;
EPA 353.2 Preparation Techniques: N/A
EPA 353.2 (calc.) Preparation Techniques: N/A
EPA 410.4 Preparation Techniques: Digestion, hotplate or HotBlock;
EPA 420.4 Preparation Techniques: Distillation, MIDI;
Hach 10360 Preparation Techniques: N/A
Program Method Analyte Matrix Primary SOP
CWP EPA 350.1 Ammonia as N NPW MN
Program Method Analyte Matrix Primary SOP
CWP EPA 353.2 Nitrate-nitrite NPW MN
CWP EPA 353.2 Nitrite as N NPW MN
Program Method Analyte Matrix Primary SOP
CWP EPA 353.2 (calc.) Nitrate as N NPW MN
Program Method Analyte Matrix Primary SOP
CWP EPA 410.4 Chemical oxygen demand NPW MN
Program Method Analyte Matrix Primary SOP
CWP EPA 420.4 Total Phenolics NPW MN
Page 10 of 87
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SM 2320 B-97 Preparation Techniques: N/A
SM 2340 B-97 Preparation Techniques: N/A
SM 2510 B-97 Preparation Techniques: N/A
SM 2540 B-97 Preparation Techniques: N/A
SM 2540 C-97 Preparation Techniques: N/A
Program Method Analyte Matrix Primary SOP
CWP Hach 10360 Biochemical oxygen demand NPW MN
CWP Hach 10360 Carbonaceous BOD, CBOD NPW MN
CWP Hach 10360 Oxygen, dissolved NPW MN
Program Method Analyte Matrix Primary SOP
CWP SM 2320 B-97 Alkalinity as CaCO3 NPW MN
Program Method Analyte Matrix Primary SOP
CWP SM 2340 B-97 Total hardness as CaCO3 NPW MN
Program Method Analyte Matrix Primary SOP
CWP SM 2510 B-97 Conductivity NPW MN
Program Method Analyte Matrix Primary SOP
CWP SM 2540 B-97 Residue-total NPW MN
Program Method Analyte Matrix Primary SOP
CWP SM 2540 C-97 Residue-filterable (TDS) NPW MN
Page 11 of 87
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SM 2540 D-97 Preparation Techniques: N/A
SM 2540 F-97 Preparation Techniques: N/A
SM 4500-Cl G-93 Preparation Techniques: N/A
SM 4500-Cl¯ E-97 Preparation Techniques: N/A
SM 4500-CN¯ E-97 Preparation Techniques: Distillation, micro; Distillation, macro; Distillation, MIDI;
SM 4500-CN¯ G-97 Preparation Techniques: Distillation, micro; Distillation, macro; Distillation, MIDI;
Program Method Analyte Matrix Primary SOP
CWP SM 2540 D-97 Residue-nonfilterable (TSS) NPW MN
Program Method Analyte Matrix Primary SOP
CWP SM 2540 F-97 Residue-settleable NPW MN
Program Method Analyte Matrix Primary SOP
CWP SM 4500-Cl G-93 Total residual chlorine NPW MN
Program Method Analyte Matrix Primary SOP
CWP SM 4500-Cl¯ E-97 Chloride NPW MN
Program Method Analyte Matrix Primary SOP
CWP SM 4500-CN¯ E-97 Total Cyanide NPW MN
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SM 4500-F¯ C-97 Preparation Techniques: N/A;
SM 4500-H+ B-96 Preparation Techniques: N/A
SM 4500-NO2¯ B-93 Preparation Techniques: N/A
SM 4500-NO3¯ H-97 Preparation Techniques: N/A
SM 4500-P E-97 Preparation Techniques: N/A
Program Method Analyte Matrix Primary SOP
CWP SM 4500-CN¯ G-97 Free cyanide NPW MN
Program Method Analyte Matrix Primary SOP
CWP SM 4500-F¯ C-97 Fluoride NPW MN
Program Method Analyte Matrix Primary SOP
CWP SM 4500-H+ B-96 pH NPW MN
Program Method Analyte Matrix Primary SOP
CWP SM 4500-NO2¯ B-93 Nitrite as N NPW MN
Program Method Analyte Matrix Primary SOP
CWP SM 4500-NO3¯ H-97 Nitrate-nitrite NPW MN
Program Method Analyte Matrix Primary SOP
CWP SM 4500-P E-97 Orthophosphate as P NPW MN
CWP SM 4500-P E-97 Total Phosphorus NPW MN
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SM 4500-P G-1999 Preparation Techniques: N/A
SM 5220 D-97 Preparation Techniques: Digestion, hotplate or HotBlock;
EPA 200.7 Preparation Techniques: Digestion, hotplate or HotBlock;
Program Method Analyte Matrix Primary SOP
CWP SM 4500-P G-1999 Orthophosphate as P NPW MN
Program Method Analyte Matrix Primary SOP
CWP SM 5220 D-97 Chemical oxygen demand NPW MN
Program Method Analyte Matrix Primary SOP
CWP EPA 200.7 Aluminum NPW MN
CWP EPA 200.7 Antimony NPW MN
CWP EPA 200.7 Arsenic NPW MN
CWP EPA 200.7 Barium NPW MN
CWP EPA 200.7 Beryllium NPW MN
CWP EPA 200.7 Boron NPW MN
CWP EPA 200.7 Cadmium NPW MN
CWP EPA 200.7 Calcium NPW MN
CWP EPA 200.7 Cobalt NPW MN
CWP EPA 200.7 Copper NPW MN
CWP EPA 200.7 Iron NPW MN
CWP EPA 200.7 Lead NPW MN
CWP EPA 200.7 Magnesium NPW MN
CWP EPA 200.7 Manganese NPW MN
CWP EPA 200.7 Molybdenum NPW MN
CWP EPA 200.7 Nickel NPW MN
CWP EPA 200.7 Potassium NPW MN
CWP EPA 200.7 Selenium NPW MN
CWP EPA 200.7 Silver NPW MN
CWP EPA 200.7 Sodium NPW MN
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EPA 200.7 Preparation Techniques: Digestion, hotplate or HotBlock;
EPA 200.8 Preparation Techniques: Digestion, hotplate or HotBlock;
Program Method Analyte Matrix Primary SOP
CWP EPA 200.7 Thallium NPW MN
CWP EPA 200.7 Tin NPW MN
CWP EPA 200.7 Titanium NPW MN
CWP EPA 200.7 Total chromium NPW MN
CWP EPA 200.7 Vanadium NPW MN
CWP EPA 200.7 Zinc NPW MN
Program Method Analyte Matrix Primary SOP
CWP EPA 200.7 Total hardness as CaCO3 NPW MN
Program Method Analyte Matrix Primary SOP
CWP EPA 200.8 Aluminum NPW MN
CWP EPA 200.8 Antimony NPW MN
CWP EPA 200.8 Arsenic NPW MN
CWP EPA 200.8 Barium NPW MN
CWP EPA 200.8 Beryllium NPW MN
CWP EPA 200.8 Bismuth NPW MN
CWP EPA 200.8 Boron NPW MN
CWP EPA 200.8 Cadmium NPW MN
CWP EPA 200.8 Calcium NPW MN
CWP EPA 200.8 Chromium NPW MN
CWP EPA 200.8 Cobalt NPW MN
CWP EPA 200.8 Copper NPW MN
CWP EPA 200.8 Iron NPW MN
CWP EPA 200.8 Lead NPW MN
CWP EPA 200.8 Lithium NPW MN
CWP EPA 200.8 Magnesium NPW MN
CWP EPA 200.8 Manganese NPW MN
CWP EPA 200.8 Molybdenum NPW MN
Page 15 of 87
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EPA 245.1 Preparation Techniques: N/A
EPA 7471B Preparation Techniques: N/A
SM 3500-Cr B-97 Preparation Techniques: N/A
Program Method Analyte Matrix Primary SOP
CWP EPA 200.8 Nickel NPW MN
CWP EPA 200.8 Palladium NPW MN
CWP EPA 200.8 Platinum NPW MN
CWP EPA 200.8 Potassium NPW MN
CWP EPA 200.8 Selenium NPW MN
CWP EPA 200.8 Silicon NPW MN
CWP EPA 200.8 Silver NPW MN
CWP EPA 200.8 Sodium NPW MN
CWP EPA 200.8 Strontium NPW MN
CWP EPA 200.8 Thallium NPW MN
CWP EPA 200.8 Tin NPW MN
CWP EPA 200.8 Titanium NPW MN
CWP EPA 200.8 Total chromium NPW MN
CWP EPA 200.8 Uranium NPW MN
CWP EPA 200.8 Vanadium NPW MN
CWP EPA 200.8 Zinc NPW MN
Program Method Analyte Matrix Primary SOP
CWP EPA 245.1 Mercury NPW MN
Program Method Analyte Matrix Primary SOP
CWP EPA 7471B Mercury NPW MN User Defined S-MN-I-306 Rev. 00
Program Method Analyte Matrix Primary SOP
CWP SM 3500-Cr B-97 Chromium VI NPW MN
Page 16 of 87
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SM 3500-Fe B-2011 Preparation Techniques: N/A
SM 3500-Fe B-97 Preparation Techniques: N/A
SM 9222 B (M-Endo)-97 Preparation Techniques: N/A
SM 9222 D (m-FC)-97 Preparation Techniques: N/A
SM 9223 B (Colilert® Quanti-Tray®)-97 Preparation Techniques: N/A
EPA 1613B Preparation Techniques: Extraction, solid phase (SPE); Extraction, automated soxhlet; Extraction, separatory funnel liquid-liquid
(LLE);
Program Method Analyte Matrix Primary SOP
CWP SM 3500-Fe B-2011 Iron NPW MN
Program Method Analyte Matrix Primary SOP
CWP SM 3500-Fe B-97 Iron NPW MN
Program Method Analyte Matrix Primary SOP
CWP SM 9222 B (M-Endo)-97 Total coliforms NPW MN
Program Method Analyte Matrix Primary SOP
CWP SM 9222 D (m-FC)-97 Fecal coliforms NPW MN
Program Method Analyte Matrix Primary SOP
CWP SM 9223 B (Colilert®Quanti-Tray®)-97
Escherichia coli NPW MN
Page 17 of 87
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EPA 1668A Preparation Techniques: N/A
Program Method Analyte Matrix Primary SOP
CWP EPA 1613B 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)
NPW MN
CWP EPA 1613B 1,2,3,4,6,7,8,9-Octachlorodibenzofuran(OCDF)
NPW MN
CWP EPA 1613B 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)
NPW MN
CWP EPA 1613B 1,2,3,4,6,7,8-Heptachlorodibenzofuran(1,2,3,4,6,7,8-hpcdf)
NPW MN
CWP EPA 1613B 1,2,3,4,7,8,9-Heptachlorodibenzofuran(1,2,3,4,7,8,9-hpcdf)
NPW MN
CWP EPA 1613B 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,4,7,8-Hxcdd)
NPW MN
CWP EPA 1613B 1,2,3,4,7,8-Hexachlorodibenzofuran(1,2,3,4,7,8-Hxcdf)
NPW MN
CWP EPA 1613B 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,6,7,8-Hxcdd)
NPW MN
CWP EPA 1613B 1,2,3,6,7,8-Hexachlorodibenzofuran(1,2,3,6,7,8-Hxcdf)
NPW MN
CWP EPA 1613B 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin(1,2,3,7,8,9-Hxcdd)
NPW MN
CWP EPA 1613B 1,2,3,7,8,9-Hexachlorodibenzofuran(1,2,3,7,8,9-Hxcdf)
NPW MN
CWP EPA 1613B 1,2,3,7,8-Pentachlorodibenzo-p-dioxin(1,2,3,7,8-Pecdd)
NPW MN
CWP EPA 1613B 1,2,3,7,8-Pentachlorodibenzofuran(1,2,3,7,8-Pecdf)
NPW MN
CWP EPA 1613B 2,3,4,6,7,8-Hexachlorodibenzofuran NPW MN
CWP EPA 1613B 2,3,4,7,8-Pentachlorodibenzofuran NPW MN
CWP EPA 1613B 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)
NPW MN
CWP EPA 1613B 2,3,7,8-Tetrachlorodibenzofuran NPW MN
CWP EPA 1613B Total HpCDD NPW MN
CWP EPA 1613B Total HpCDF NPW MN
CWP EPA 1613B Total HxCDD NPW MN
CWP EPA 1613B Total HxCDF NPW MN
CWP EPA 1613B Total PeCDD NPW MN
CWP EPA 1613B Total PeCDF NPW MN
CWP EPA 1613B Total TCDD NPW MN
CWP EPA 1613B Total TCDF NPW MN
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Program Method Analyte Matrix Primary SOP
CWP EPA 1668A 2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl(BZ-206)
NPW MN
CWP EPA 1668A 2,2',3,3',4,4',5,5'-Octachlorobiphenyl(BZ-194)
NPW MN
CWP EPA 1668A 2,2',3,3',4,4',5,6'-Octachlorobiphenyl(BZ-196)
NPW MN
CWP EPA 1668A 2,2',3,3',4,4',5,6,6'-Nonachlorobiphenyl(BZ-207)
NPW MN
CWP EPA 1668A 2,2',3,3',4,4',5,6-Octachlorobiphenyl(BZ-195)
NPW MN
CWP EPA 1668A 2,2',3,3',4,4',5-Heptachlorobiphenyl (BZ-170)
NPW MN
CWP EPA 1668A 2,2',3,3',4,5',6'-Heptachlorobiphenyl(BZ-177)
NPW MN
CWP EPA 1668A 2,2',3,3',4,5',6,6'-Octachlorobiphenyl(BZ-201)
NPW MN
CWP EPA 1668A 2,2',3,3',4,5',6-Heptachlorobiphenyl (BZ-175)
NPW MN
CWP EPA 1668A 2,2',3,3',4,5'-Hexachlorobiphenyl (BZ-130)
NPW MN
CWP EPA 1668A 2,2',3,3',4,5,5',6,6'-Nonachlorobiphenyl(BZ-208)
NPW MN
CWP EPA 1668A 2,2',3,3',4,5,5'-Heptachlorobiphenyl (BZ-172)
NPW MN
CWP EPA 1668A 2,2',3,3',4,5,6'-Heptachlorobiphenyl (BZ-174)
NPW MN
CWP EPA 1668A 2,2',3,3',4,6'-Hexachlorobiphenyl (BZ-132)
NPW MN
CWP EPA 1668A 2,2',3,3',4,6,6'-Heptachlorobiphenyl (BZ-176)
NPW MN
CWP EPA 1668A 2,2',3,3',4,6-Hexachlorobiphenyl (BZ-131)
NPW MN
CWP EPA 1668A 2,2',3,3',4-Pentachlorobiphenyl (BZ-82) NPW MN
CWP EPA 1668A 2,2',3,3',5,5',6,6'-Octachlorobiphenyl(BZ-202)
NPW MN
CWP EPA 1668A 2,2',3,3',5,5',6-Heptachlorobiphenyl (BZ-178)
NPW MN
CWP EPA 1668A 2,2',3,3',5,5'-Hexachlorobiphenyl (BZ-133)
NPW MN
CWP EPA 1668A 2,2',3,3',5,6,6'-Heptachlorobiphenyl (BZ-179)
NPW MN
CWP EPA 1668A 2,2',3,3',5-Pentachlorobiphenyl (BZ-83) NPW MN
CWP EPA 1668A 2,2',3,3',6,6'-Hexachlorobiphenyl (BZ-136)
NPW MN
CWP EPA 1668A 2,2',3,3',6-Pentachlorobiphenyl (BZ-84) NPW MN
CWP EPA 1668A 2,2',3,4',5,5'-Hexachlorobiphenyl (BZ-146)
NPW MN
CWP EPA 1668A 2,2',3,4',5,6'-Hexachlorobiphenyl (BZ-148)
NPW MN
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Program Method Analyte Matrix Primary SOP
CWP EPA 1668A 2,2',3,4',5,6,6'-Heptachlorobiphenyl (BZ-188)
NPW MN
CWP EPA 1668A 2,2',3,4',6,6'-Hexachlorobiphenyl (BZ-150)
NPW MN
CWP EPA 1668A 2,2',3,4'-Tetrachlorobiphenyl (BZ-42) NPW MN
CWP EPA 1668A 2,2',3,4,4',5,5',6-Octachlorobiphenyl(BZ-203)
NPW MN
CWP EPA 1668A 2,2',3,4,4',5,6'-Heptachlorobiphenyl (BZ-182)
NPW MN
CWP EPA 1668A 2,2',3,4,4',5,6,6'-Octachlorobiphenyl(BZ-204)
NPW MN
CWP EPA 1668A 2,2',3,4,4',5,6-Heptachlorobiphenyl (BZ-181)
NPW MN
CWP EPA 1668A 2,2',3,4,4',5-Hexachlorobiphenyl (BZ-137)
NPW MN
CWP EPA 1668A 2,2',3,4,4',6,6'-Heptachlorobiphenyl (BZ-184)
NPW MN
CWP EPA 1668A 2,2',3,4,5',6-Hexachlorobiphenyl (BZ-144)
NPW MN
CWP EPA 1668A 2,2',3,4,5,5'-Hexachlorobiphenyl (BZ-141)
NPW MN
CWP EPA 1668A 2,2',3,4,5,6,6'-Heptachlorobiphenyl (BZ-186)
NPW MN
CWP EPA 1668A 2,2',3,4,5,6-Hexachlorobiphenyl (BZ-142)
NPW MN
CWP EPA 1668A 2,2',3,4,6'-Pentachlorobiphenyl (BZ-89) NPW MN
CWP EPA 1668A 2,2',3,4,6,6'-Hexachlorobiphenyl (BZ-145)
NPW MN
CWP EPA 1668A 2,2',3,5',6-Pentachlorobiphenyl (BZ-95) NPW MN
CWP EPA 1668A 2,2',3,5,5'-Pentachlorobiphenyl (BZ-92) NPW MN
CWP EPA 1668A 2,2',3,5,6'-Pentachlorobiphenyl (BZ-94) NPW MN
CWP EPA 1668A 2,2',3,5,6,6'-Hexachlorobiphenyl (BZ-152)
NPW MN
CWP EPA 1668A 2,2',3,6'-Tetrachlorobiphenyl (BZ-46) NPW MN
CWP EPA 1668A 2,2',3,6,6'-Pentachlorobiphenyl (BZ-96) NPW MN
CWP EPA 1668A 2,2',3-Trichlorobiphenyl (BZ-16) NPW MN
CWP EPA 1668A 2,2',4,4',5,6'-Hexachlorobiphenyl (BZ-154)
NPW MN
CWP EPA 1668A 2,2',4,4',5-Pentachlorobiphenyl (BZ-99) NPW MN
CWP EPA 1668A 2,2',4,4',6,6'-Hexachlorobiphenyl (BZ-155)
NPW MN
CWP EPA 1668A 2,2',4,5',6-Pentachlorobiphenyl (BZ-103) NPW MN
CWP EPA 1668A 2,2',4,5-Tetrachlorobiphenyl (BZ-48) NPW MN
CWP EPA 1668A 2,2',4,6,6'-Pentachlorobiphenyl (BZ-104) NPW MN
CWP EPA 1668A 2,2',4-Trichlorobiphenyl (BZ-17) NPW MN
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Program Method Analyte Matrix Primary SOP
CWP EPA 1668A 2,2',5,5'-Tetrachlorobiphenyl (BZ-52) NPW MN
CWP EPA 1668A 2,2',6,6'-Tetrachlorobiphenyl (BZ-54) NPW MN
CWP EPA 1668A 2,2',6-Trichlorobiphenyl (BZ-19) NPW MN
CWP EPA 1668A 2,2'-Dichlorobiphenyl (BZ-4) NPW MN
CWP EPA 1668A 2,3',4,4',5'-Pentachlorobiphenyl (BZ-123)
NPW MN
CWP EPA 1668A 2,3',4,4',5,5'-Hexachlorobiphenyl (BZ-167)
NPW MN
CWP EPA 1668A 2,3',4,4',5-Pentachlorobiphenyl (BZ-118) NPW MN
CWP EPA 1668A 2,3',4,4'-Tetrachlorobiphenyl (BZ-66) NPW MN
CWP EPA 1668A 2,3',4,5',6-Pentachlorobiphenyl (BZ-121) NPW MN
CWP EPA 1668A 2,3',4,5'-Tetrachlorobiphenyl (BZ-68) NPW MN
CWP EPA 1668A 2,3',4,5,5'-Pentachlorobiphenyl (BZ-120) NPW MN
CWP EPA 1668A 2,3',4,5-Tetrachlorobiphenyl (BZ-67) NPW MN
CWP EPA 1668A 2,3',4-Trichlorobiphenyl (BZ-25) NPW MN
CWP EPA 1668A 2,3',5'-Trichlorobiphenyl (BZ-34) NPW MN
CWP EPA 1668A 2,3',5,5'-Tetrachlorobiphenyl (BZ-72) NPW MN
CWP EPA 1668A 2,3',6-Trichlorobiphenyl (BZ-27) NPW MN
CWP EPA 1668A 2,3'-Dichlorobiphenyl (BZ-6) NPW MN
CWP EPA 1668A 2,3,3',4',5',6-Hexachlorobiphenyl (BZ-164)
NPW MN
CWP EPA 1668A 2,3,3',4',5'-Pentachlorobiphenyl (BZ-122)
NPW MN
CWP EPA 1668A 2,3,3',4',5,5'-Hexachlorobiphenyl (BZ-162)
NPW MN
CWP EPA 1668A 2,3,3',4'-Tetrachlorobiphenyl (BZ-56) NPW MN
CWP EPA 1668A 2,3,3',4,4',5',6-Heptachlorobiphenyl (BZ-191)
NPW MN
CWP EPA 1668A 2,3,3',4,4',5,5',6-Octachlorobiphenyl(BZ-205)
NPW MN
CWP EPA 1668A 2,3,3',4,4',5,5'-Heptachlorobiphenyl (BZ-189)
NPW MN
CWP EPA 1668A 2,3,3',4,4',5,6-Heptachlorobiphenyl (BZ-190)
NPW MN
CWP EPA 1668A 2,3,3',4,4',6-Hexachlorobiphenyl (BZ-158)
NPW MN
CWP EPA 1668A 2,3,3',4,4'-Pentachlorobiphenyl (BZ-105) NPW MN
CWP EPA 1668A 2,3,3',4,5',6-Hexachlorobiphenyl (BZ-161)
NPW MN
CWP EPA 1668A 2,3,3',4,5,5',6-Heptachlorobiphenyl (BZ-192)
NPW MN
CWP EPA 1668A 2,3,3',4,5,5'-Hexachlorobiphenyl (BZ-159)
NPW MN
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Program Method Analyte Matrix Primary SOP
CWP EPA 1668A 2,3,3',4,5,6-Hexachlorobiphenyl (BZ-160)
NPW MN
CWP EPA 1668A 2,3,3',4,5-Pentachlorobiphenyl (BZ-106) NPW MN
CWP EPA 1668A 2,3,3',4,6-Pentachlorobiphenyl (BZ-109) NPW MN
CWP EPA 1668A 2,3,3',4-Tetrachlorobiphenyl (BZ-55) NPW MN
CWP EPA 1668A 2,3,3',5'-Tetrachlorobiphenyl (BZ-58) NPW MN
CWP EPA 1668A 2,3,3',5,5',6-Hexachlorobiphenyl (BZ-165)
NPW MN
CWP EPA 1668A 2,3,3',5,5'-Pentachlorobiphenyl (BZ-111) NPW MN
CWP EPA 1668A 2,3,3',5,6-Pentachlorobiphenyl (BZ-112) NPW MN
CWP EPA 1668A 2,3,3',5-Tetrachlorobiphenyl (BZ-57) NPW MN
CWP EPA 1668A 2,3,4',5-Tetrachlorobiphenyl (BZ-63) NPW MN
CWP EPA 1668A 2,3,4',6-Tetrachlorobiphenyl (BZ-64) NPW MN
CWP EPA 1668A 2,3,4'-Trichlorobiphenyl (BZ-22) NPW MN
CWP EPA 1668A 2,3,4,4',5-Pentachlorobiphenyl (BZ-114) NPW MN
CWP EPA 1668A 2,3,4,4'-Tetrachlorobiphenyl (BZ-60) NPW MN
CWP EPA 1668A 2,3,5-Trichlorobiphenyl (BZ-23) NPW MN
CWP EPA 1668A 2,3,6-Trichlorobiphenyl (BZ-24) NPW MN
CWP EPA 1668A 2,3-Dichlorobiphenyl (BZ-5) NPW MN
CWP EPA 1668A 2,4',5-Trichlorobiphenyl (BZ-31) NPW MN
CWP EPA 1668A 2,4',6-Trichlorobiphenyl (BZ-32) NPW MN
CWP EPA 1668A 2,4'-Dichlorobiphenyl (BZ-8) NPW MN
CWP EPA 1668A 2,4-Dichlorobiphenyl (BZ-7) NPW MN
CWP EPA 1668A 2,5-Dichlorobiphenyl (BZ-9) NPW MN
CWP EPA 1668A 2,6-Dichlorobiphenyl (BZ-10) NPW MN
CWP EPA 1668A 2-Chlorobiphenyl (BZ-1) NPW MN
CWP EPA 1668A 3,3',4,4',5,5'-Hexachlorobiphenyl (BZ-169)
NPW MN
CWP EPA 1668A 3,3',4,4',5-Pentachlorobiphenyl (BZ-126) NPW MN
CWP EPA 1668A 3,3',4,4'-Tetrachlorobiphenyl (BZ-77) NPW MN
CWP EPA 1668A 3,3',4,5'-Tetrachlorobiphenyl (BZ-79) NPW MN
CWP EPA 1668A 3,3',4,5,5'-Pentachlorobiphenyl (BZ-127) NPW MN
CWP EPA 1668A 3,3',4,5-Tetrachlorobiphenyl (BZ-78) NPW MN
CWP EPA 1668A 3,3',4-Trichlorobiphenyl (BZ-35) NPW MN
CWP EPA 1668A 3,3',5,5'-Tetrachlorobiphenyl (BZ-80) NPW MN
CWP EPA 1668A 3,3',5-Trichlorobiphenyl (BZ-36) NPW MN
CWP EPA 1668A 3,3'-Dichlorobiphenyl (BZ-11) NPW MN
CWP EPA 1668A 3,4',5-Trichlorobiphenyl (BZ-39) NPW MN
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Program Method Analyte Matrix Primary SOP
CWP EPA 1668A 3,4,4',5-Tetrachlorobiphenyl (BZ-81) NPW MN
CWP EPA 1668A 3,4,4'-Trichlorobiphenyl (BZ-37) NPW MN
CWP EPA 1668A 3,4,5-Trichlorobiphenyl (BZ-38) NPW MN
CWP EPA 1668A 3,5-Dichlorobiphenyl (BZ-14) NPW MN
CWP EPA 1668A 3-Chlorobiphenyl (BZ-2) NPW MN
CWP EPA 1668A 4,4'-Dichlorobiphenyl (BZ-15) NPW MN
CWP EPA 1668A 4-Chlorobiphenyl (BZ-3) NPW MN
CWP EPA 1668A Decachlorobiphenyl (BZ-209) NPW MN
CWP EPA 1668A PCB-(100/93/102/98) NPW MN
CWP EPA 1668A PCB-(107/124) NPW MN
CWP EPA 1668A PCB-(108/119/86/97/125/87) NPW MN
CWP EPA 1668A PCB-(110/115) NPW MN
CWP EPA 1668A PCB-(113/90/101) NPW MN
CWP EPA 1668A PCB-(117/116/85) NPW MN
CWP EPA 1668A PCB-(128/166) NPW MN
CWP EPA 1668A PCB-(13/12) NPW MN
CWP EPA 1668A PCB-(134/143) NPW MN
CWP EPA 1668A PCB-(138/163/129) NPW MN
CWP EPA 1668A PCB-(139/140) NPW MN
CWP EPA 1668A PCB-(147/149) NPW MN
CWP EPA 1668A PCB-(151/135) NPW MN
CWP EPA 1668A PCB-(153/168) NPW MN
CWP EPA 1668A PCB-(156/157) NPW MN
CWP EPA 1668A PCB-(171/173) NPW MN
CWP EPA 1668A PCB-(180/193) NPW MN
CWP EPA 1668A PCB-(183/185) NPW MN
CWP EPA 1668A PCB-(197/200) NPW MN
CWP EPA 1668A PCB-(198/199) NPW MN
CWP EPA 1668A PCB-(21/33) NPW MN
CWP EPA 1668A PCB-(26/29) NPW MN
CWP EPA 1668A PCB-(28/20) NPW MN
CWP EPA 1668A PCB-(30/18) NPW MN
CWP EPA 1668A PCB-(41/40/71) NPW MN
CWP EPA 1668A PCB-(44/47/65) NPW MN
CWP EPA 1668A PCB-(45/51) NPW MN
CWP EPA 1668A PCB-(50/53) NPW MN
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EPA 625 Preparation Techniques: Extraction, continuous liquid-liquid (LLE); Extraction, separatory funnel liquid-liquid (LLE);
Program Method Analyte Matrix Primary SOP
CWP EPA 1668A PCB-(59/62/75) NPW MN
CWP EPA 1668A PCB-(61/70/74/76) NPW MN
CWP EPA 1668A PCB-(69/49) NPW MN
CWP EPA 1668A PCB-(73/43) NPW MN
CWP EPA 1668A PCB-(88/91) NPW MN
Program Method Analyte Matrix Primary SOP
CWP EPA 625 1,2,4-Trichlorobenzene NPW MN
CWP EPA 625 2,4,5-Trichlorophenol NPW MN
CWP EPA 625 2,4,6-Trichlorophenol NPW MN
CWP EPA 625 2,4-Dichlorophenol NPW MN
CWP EPA 625 2,4-Dimethylphenol NPW MN
CWP EPA 625 2,4-Dinitrophenol NPW MN
CWP EPA 625 2,4-Dinitrotoluene (2,4-DNT) NPW MN
CWP EPA 625 2,6-Dinitrotoluene (2,6-DNT) NPW MN
CWP EPA 625 2-Chloronaphthalene NPW MN
CWP EPA 625 2-Chlorophenol NPW MN
CWP EPA 625 2-Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol)
NPW MN
CWP EPA 625 2-Nitrophenol NPW MN
CWP EPA 625 3,3'-Dichlorobenzidine NPW MN
CWP EPA 625 4-Bromophenyl phenyl ether NPW MN
CWP EPA 625 4-Chloro-3-methylphenol NPW MN
CWP EPA 625 4-Chlorophenyl phenylether NPW MN
CWP EPA 625 4-Nitrophenol NPW MN
CWP EPA 625 Acenaphthene NPW MN
CWP EPA 625 Acenaphthylene NPW MN
CWP EPA 625 Anthracene NPW MN
CWP EPA 625 Benzidine NPW MN
CWP EPA 625 Benzo(a)anthracene NPW MN
CWP EPA 625 Benzo(a)pyrene NPW MN
CWP EPA 625 Benzo(g,h,i)perylene NPW MN
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EPA 624 Preparation Techniques: Purge and trap;
Program Method Analyte Matrix Primary SOP
CWP EPA 625 Benzo(k)fluoranthene NPW MN
CWP EPA 625 Benzo[b]fluoranthene NPW MN
CWP EPA 625 bis(2-Chloroethoxy)methane NPW MN
CWP EPA 625 bis(2-Chloroethyl) ether NPW MN
CWP EPA 625 bis(2-Chloroisopropyl) ether NPW MN
CWP EPA 625 Butyl benzyl phthalate NPW MN
CWP EPA 625 Chrysene NPW MN
CWP EPA 625 Di(2-ethylhexyl) phthalate (bis(2-Ethylhexyl)phthalate, DEHP)
NPW MN
CWP EPA 625 Di-n-butyl phthalate NPW MN
CWP EPA 625 Di-n-octyl phthalate NPW MN
CWP EPA 625 Dibenz(a,h) anthracene NPW MN
CWP EPA 625 Diethyl phthalate NPW MN
CWP EPA 625 Dimethyl phthalate NPW MN
CWP EPA 625 Fluoranthene NPW MN
CWP EPA 625 Fluorene NPW MN
CWP EPA 625 Hexachlorobenzene NPW MN
CWP EPA 625 Hexachlorobutadiene NPW MN
CWP EPA 625 Hexachlorocyclopentadiene NPW MN
CWP EPA 625 Hexachloroethane NPW MN
CWP EPA 625 Indeno(1,2,3-cd) pyrene NPW MN
CWP EPA 625 Isophorone NPW MN
CWP EPA 625 n-Nitrosodi-n-propylamine NPW MN
CWP EPA 625 n-Nitrosodimethylamine NPW MN
CWP EPA 625 n-Nitrosodiphenylamine NPW MN
CWP EPA 625 Naphthalene NPW MN
CWP EPA 625 Nitrobenzene NPW MN
CWP EPA 625 Pentachlorophenol NPW MN
CWP EPA 625 Phenanthrene NPW MN
CWP EPA 625 Phenol NPW MN
CWP EPA 625 Pyrene NPW MN
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Program Method Analyte Matrix Primary SOP
CWP EPA 624 1,1,1-Trichloroethane NPW MN
CWP EPA 624 1,1,2,2-Tetrachloroethane NPW MN
CWP EPA 624 1,1,2-Trichloroethane NPW MN
CWP EPA 624 1,1-Dichloroethane NPW MN
CWP EPA 624 1,1-Dichloroethylene NPW MN
CWP EPA 624 1,2,4-Trichlorobenzene NPW MN
CWP EPA 624 1,2-Dichlorobenzene NPW MN
CWP EPA 624 1,2-Dichloroethane (Ethylene dichloride) NPW MN
CWP EPA 624 1,2-Dichloropropane NPW MN
CWP EPA 624 1,3-Dichlorobenzene NPW MN
CWP EPA 624 1,4-Dichlorobenzene NPW MN
CWP EPA 624 2-Chloroethyl vinyl ether NPW MN
CWP EPA 624 Acrolein (Propenal) NPW MN
CWP EPA 624 Acrylonitrile NPW MN
CWP EPA 624 Benzene NPW MN
CWP EPA 624 Bromodichloromethane NPW MN
CWP EPA 624 Bromoform NPW MN
CWP EPA 624 Carbon tetrachloride NPW MN
CWP EPA 624 Chlorobenzene NPW MN
CWP EPA 624 Chlorodibromomethane NPW MN
CWP EPA 624 Chloroethane (Ethyl chloride) NPW MN
CWP EPA 624 Chloroform NPW MN
CWP EPA 624 cis-1,3-Dichloropropene NPW MN
CWP EPA 624 Ethylbenzene NPW MN
CWP EPA 624 Isopropylbenzene NPW MN
CWP EPA 624 Methyl bromide (Bromomethane) NPW MN
CWP EPA 624 Methyl chloride (Chloromethane) NPW MN
CWP EPA 624 Methylene chloride (Dichloromethane) NPW MN
CWP EPA 624 Tetrachloroethylene (Perchloroethylene) NPW MN
CWP EPA 624 Toluene NPW MN
CWP EPA 624 trans-1,2-Dichloroethylene NPW MN
CWP EPA 624 trans-1,3-Dichloropropylene NPW MN
CWP EPA 624 Trichloroethene (Trichloroethylene) NPW MN
CWP EPA 624 Trichlorofluoromethane(Fluorotrichloromethane, Freon 11)
NPW MN
CWP EPA 624 Vinyl chloride NPW MN
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MDA GD24 (Ag List 2) Preparation Techniques: Extraction, microwave; Extraction, separatory funnel liquid-liquid (LLE);
EPA 9045D Preparation Techniques: N/A
EPA 9056A Preparation Techniques: N/A
EPA 9071B
Resource Conservation Recovery Program
Program Method Analyte Matrix Primary SOP
RCRP MDA GD24 (Ag List 2) 2,4-DB NPW MN
RCRP MDA GD24 (Ag List 2) 2,4-DB SCM MN
RCRP MDA GD24 (Ag List 2) Bentazon NPW MN
RCRP MDA GD24 (Ag List 2) Bentazon SCM MN
RCRP MDA GD24 (Ag List 2) Garlon (Triclopyr) NPW MN
RCRP MDA GD24 (Ag List 2) Garlon (Triclopyr) SCM MN
RCRP MDA GD24 (Ag List 2) MCPA NPW MN
RCRP MDA GD24 (Ag List 2) MCPA SCM MN
RCRP MDA GD24 (Ag List 2) Picloram SCM MN
RCRP MDA GD24 (Ag List 2) Picloram NPW MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 9045D pH SCM MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 9056A Bromide NPW MN
RCRP EPA 9056A Chloride NPW MN
RCRP EPA 9056A Fluoride NPW MN
RCRP EPA 9056A Nitrate NPW MN
RCRP EPA 9056A Nitrite NPW MN
RCRP EPA 9056A Sulfate NPW MN
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Preparation Techniques: N/A
EPA 6010B Preparation Techniques: Digestion, hotplate or HotBlock; Extraction, EPA 1311 TCLP, non-volatiles; Extraction, EPA 1312 SPLP,
non-volatiles;
Program Method Analyte Matrix Primary SOP
RCRP EPA 9071B n-Hexane Extractable Material (O&G) SCM MN
RCRP EPA 9071B Oil & Grease SCM MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 6010B Aluminum NPW MN
RCRP EPA 6010B Aluminum SCM MN
RCRP EPA 6010B Antimony SCM MN
RCRP EPA 6010B Antimony NPW MN
RCRP EPA 6010B Arsenic NPW MN
RCRP EPA 6010B Arsenic SCM MN
RCRP EPA 6010B Barium SCM MN
RCRP EPA 6010B Barium NPW MN
RCRP EPA 6010B Beryllium SCM MN
RCRP EPA 6010B Beryllium NPW MN
RCRP EPA 6010B Boron SCM MN
RCRP EPA 6010B Boron NPW MN
RCRP EPA 6010B Cadmium SCM MN
RCRP EPA 6010B Cadmium NPW MN
RCRP EPA 6010B Calcium SCM MN
RCRP EPA 6010B Calcium NPW MN
RCRP EPA 6010B Chromium SCM MN
RCRP EPA 6010B Cobalt NPW MN
RCRP EPA 6010B Cobalt SCM MN
RCRP EPA 6010B Copper SCM MN
RCRP EPA 6010B Copper NPW MN
RCRP EPA 6010B Iron NPW MN
RCRP EPA 6010B Iron SCM MN
RCRP EPA 6010B Lead SCM MN
RCRP EPA 6010B Lead NPW MN
RCRP EPA 6010B Magnesium SCM MN
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EPA 6010C Preparation Techniques: Digestion, hotplate or HotBlock; Extraction, EPA 1311 TCLP, non-volatiles; Extraction, EPA 1312 SPLP,
non-volatiles;
Program Method Analyte Matrix Primary SOP
RCRP EPA 6010B Magnesium NPW MN
RCRP EPA 6010B Manganese NPW MN
RCRP EPA 6010B Manganese SCM MN
RCRP EPA 6010B Molybdenum NPW MN
RCRP EPA 6010B Molybdenum SCM MN
RCRP EPA 6010B Nickel SCM MN
RCRP EPA 6010B Nickel NPW MN
RCRP EPA 6010B Potassium SCM MN
RCRP EPA 6010B Potassium NPW MN
RCRP EPA 6010B Selenium SCM MN
RCRP EPA 6010B Selenium NPW MN
RCRP EPA 6010B Silver NPW MN
RCRP EPA 6010B Silver SCM MN
RCRP EPA 6010B Sodium NPW MN
RCRP EPA 6010B Sodium SCM MN
RCRP EPA 6010B Thallium SCM MN
RCRP EPA 6010B Thallium NPW MN
RCRP EPA 6010B Tin SCM MN
RCRP EPA 6010B Tin NPW MN
RCRP EPA 6010B Titanium NPW MN
RCRP EPA 6010B Titanium SCM MN
RCRP EPA 6010B Total chromium NPW MN
RCRP EPA 6010B Vanadium NPW MN
RCRP EPA 6010B Vanadium SCM MN
RCRP EPA 6010B Zinc NPW MN
RCRP EPA 6010B Zinc SCM MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 6010C Aluminum SCM MN
RCRP EPA 6010C Aluminum NPW MN
RCRP EPA 6010C Antimony NPW MN
RCRP EPA 6010C Antimony SCM MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 6010C Arsenic SCM MN
RCRP EPA 6010C Arsenic NPW MN
RCRP EPA 6010C Barium NPW MN
RCRP EPA 6010C Barium SCM MN
RCRP EPA 6010C Beryllium NPW MN
RCRP EPA 6010C Beryllium SCM MN
RCRP EPA 6010C Boron NPW MN
RCRP EPA 6010C Boron SCM MN
RCRP EPA 6010C Cadmium SCM MN
RCRP EPA 6010C Cadmium NPW MN
RCRP EPA 6010C Calcium SCM MN
RCRP EPA 6010C Calcium NPW MN
RCRP EPA 6010C Chromium NPW MN
RCRP EPA 6010C Chromium SCM MN
RCRP EPA 6010C Cobalt NPW MN
RCRP EPA 6010C Cobalt SCM MN
RCRP EPA 6010C Copper NPW MN
RCRP EPA 6010C Copper SCM MN
RCRP EPA 6010C Iron SCM MN
RCRP EPA 6010C Iron NPW MN
RCRP EPA 6010C Lead NPW MN
RCRP EPA 6010C Lead SCM MN
RCRP EPA 6010C Magnesium SCM MN
RCRP EPA 6010C Magnesium NPW MN
RCRP EPA 6010C Manganese NPW MN
RCRP EPA 6010C Manganese SCM MN
RCRP EPA 6010C Molybdenum NPW MN
RCRP EPA 6010C Molybdenum SCM MN
RCRP EPA 6010C Nickel NPW MN
RCRP EPA 6010C Nickel SCM MN
RCRP EPA 6010C Potassium NPW MN
RCRP EPA 6010C Potassium SCM MN
RCRP EPA 6010C Selenium SCM MN
RCRP EPA 6010C Selenium NPW MN
RCRP EPA 6010C Silver SCM MN
RCRP EPA 6010C Silver NPW MN
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EPA 6020 Preparation Techniques: Digestion, hotplate or HotBlock; Extraction, EPA 1311 TCLP, non-volatiles; Extraction, EPA 1312 SPLP,
non-volatiles;
Program Method Analyte Matrix Primary SOP
RCRP EPA 6010C Sodium SCM MN
RCRP EPA 6010C Sodium NPW MN
RCRP EPA 6010C Thallium SCM MN
RCRP EPA 6010C Thallium NPW MN
RCRP EPA 6010C Tin SCM MN
RCRP EPA 6010C Tin NPW MN
RCRP EPA 6010C Titanium SCM MN
RCRP EPA 6010C Titanium NPW MN
RCRP EPA 6010C Vanadium NPW MN
RCRP EPA 6010C Vanadium SCM MN
RCRP EPA 6010C Zinc NPW MN
RCRP EPA 6010C Zinc SCM MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 6020 Aluminum SCM MN
RCRP EPA 6020 Aluminum NPW MN
RCRP EPA 6020 Antimony SCM MN
RCRP EPA 6020 Antimony NPW MN
RCRP EPA 6020 Arsenic NPW MN
RCRP EPA 6020 Arsenic SCM MN
RCRP EPA 6020 Barium SCM MN
RCRP EPA 6020 Barium NPW MN
RCRP EPA 6020 Beryllium SCM MN
RCRP EPA 6020 Beryllium NPW MN
RCRP EPA 6020 Bismuth SCM MN
RCRP EPA 6020 Bismuth NPW MN
RCRP EPA 6020 Boron NPW MN
RCRP EPA 6020 Boron SCM MN
RCRP EPA 6020 Cadmium SCM MN
RCRP EPA 6020 Cadmium NPW MN
RCRP EPA 6020 Calcium SCM MN
RCRP EPA 6020 Calcium NPW MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 6020 Chromium SCM MN
RCRP EPA 6020 Chromium NPW MN
RCRP EPA 6020 Cobalt NPW MN
RCRP EPA 6020 Cobalt SCM MN
RCRP EPA 6020 Copper NPW MN
RCRP EPA 6020 Copper SCM MN
RCRP EPA 6020 Iron NPW MN
RCRP EPA 6020 Iron SCM MN
RCRP EPA 6020 Lead NPW MN
RCRP EPA 6020 Lead SCM MN
RCRP EPA 6020 Lithium SCM MN
RCRP EPA 6020 Lithium NPW MN
RCRP EPA 6020 Magnesium SCM MN
RCRP EPA 6020 Magnesium NPW MN
RCRP EPA 6020 Manganese NPW MN
RCRP EPA 6020 Manganese SCM MN
RCRP EPA 6020 Molybdenum SCM MN
RCRP EPA 6020 Molybdenum NPW MN
RCRP EPA 6020 Nickel SCM MN
RCRP EPA 6020 Nickel NPW MN
RCRP EPA 6020 Palladium NPW MN
RCRP EPA 6020 Platinum NPW MN
RCRP EPA 6020 Potassium SCM MN
RCRP EPA 6020 Potassium NPW MN
RCRP EPA 6020 Selenium SCM MN
RCRP EPA 6020 Selenium NPW MN
RCRP EPA 6020 Silicon NPW MN
RCRP EPA 6020 Silicon SCM MN
RCRP EPA 6020 Silver NPW MN
RCRP EPA 6020 Silver SCM MN
RCRP EPA 6020 Sodium NPW MN
RCRP EPA 6020 Sodium SCM MN
RCRP EPA 6020 Strontium SCM MN
RCRP EPA 6020 Strontium NPW MN
RCRP EPA 6020 Thallium NPW MN
RCRP EPA 6020 Thallium SCM MN
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EPA 6020A Preparation Techniques: Digestion, hotplate or HotBlock; Extraction, EPA 1311 TCLP, non-volatiles; Extraction, EPA 1312 SPLP,
non-volatiles;
Program Method Analyte Matrix Primary SOP
RCRP EPA 6020 Tin NPW MN
RCRP EPA 6020 Tin SCM MN
RCRP EPA 6020 Titanium NPW MN
RCRP EPA 6020 Titanium SCM MN
RCRP EPA 6020 Total chromium NPW MN
RCRP EPA 6020 Uranium NPW MN
RCRP EPA 6020 Uranium SCM MN
RCRP EPA 6020 Vanadium NPW MN
RCRP EPA 6020 Vanadium SCM MN
RCRP EPA 6020 Zinc SCM MN
RCRP EPA 6020 Zinc NPW MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 6020A Aluminum NPW MN
RCRP EPA 6020A Aluminum SCM MN
RCRP EPA 6020A Antimony SCM MN
RCRP EPA 6020A Antimony NPW MN
RCRP EPA 6020A Arsenic NPW MN
RCRP EPA 6020A Arsenic SCM MN
RCRP EPA 6020A Barium NPW MN
RCRP EPA 6020A Barium SCM MN
RCRP EPA 6020A Beryllium SCM MN
RCRP EPA 6020A Beryllium NPW MN
RCRP EPA 6020A Bismuth SCM MN
RCRP EPA 6020A Bismuth NPW MN
RCRP EPA 6020A Boron NPW MN
RCRP EPA 6020A Boron SCM MN
RCRP EPA 6020A Cadmium SCM MN
RCRP EPA 6020A Cadmium NPW MN
RCRP EPA 6020A Calcium SCM MN
RCRP EPA 6020A Calcium NPW MN
RCRP EPA 6020A Chromium NPW MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 6020A Chromium SCM MN
RCRP EPA 6020A Cobalt SCM MN
RCRP EPA 6020A Cobalt NPW MN
RCRP EPA 6020A Copper SCM MN
RCRP EPA 6020A Copper NPW MN
RCRP EPA 6020A Iron SCM MN
RCRP EPA 6020A Iron NPW MN
RCRP EPA 6020A Lead SCM MN
RCRP EPA 6020A Lead NPW MN
RCRP EPA 6020A Lithium NPW MN
RCRP EPA 6020A Lithium SCM MN
RCRP EPA 6020A Magnesium NPW MN
RCRP EPA 6020A Magnesium SCM MN
RCRP EPA 6020A Manganese NPW MN
RCRP EPA 6020A Manganese SCM MN
RCRP EPA 6020A Molybdenum NPW MN
RCRP EPA 6020A Molybdenum SCM MN
RCRP EPA 6020A Nickel SCM MN
RCRP EPA 6020A Nickel NPW MN
RCRP EPA 6020A Palladium NPW MN
RCRP EPA 6020A Platinum NPW MN
RCRP EPA 6020A Potassium NPW MN
RCRP EPA 6020A Potassium SCM MN
RCRP EPA 6020A Selenium NPW MN
RCRP EPA 6020A Selenium SCM MN
RCRP EPA 6020A Silicon SCM MN
RCRP EPA 6020A Silicon NPW MN
RCRP EPA 6020A Silver SCM MN
RCRP EPA 6020A Silver NPW MN
RCRP EPA 6020A Sodium NPW MN
RCRP EPA 6020A Sodium SCM MN
RCRP EPA 6020A Strontium SCM MN
RCRP EPA 6020A Strontium NPW MN
RCRP EPA 6020A Thallium NPW MN
RCRP EPA 6020A Thallium SCM MN
RCRP EPA 6020A Tin SCM MN
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EPA 7470A Preparation Techniques: N/A
EPA 7471A Preparation Techniques: N/A
EPA 7471B Preparation Techniques: N/A
EPA 1613B Preparation Techniques: Extraction, solid phase (SPE); Extraction, automated soxhlet; Extraction, separatory funnel liquid-liquid
(LLE);
Program Method Analyte Matrix Primary SOP
RCRP EPA 6020A Tin NPW MN
RCRP EPA 6020A Titanium SCM MN
RCRP EPA 6020A Titanium NPW MN
RCRP EPA 6020A Uranium SCM MN
RCRP EPA 6020A Uranium NPW MN
RCRP EPA 6020A Vanadium SCM MN
RCRP EPA 6020A Vanadium NPW MN
RCRP EPA 6020A Zinc NPW MN
RCRP EPA 6020A Zinc SCM MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 7470A Mercury NPW MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 7471A Mercury SCM MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 7471B Mercury SCM MN
RCRP EPA 7471B Mercury NPW MN User Defined S-MN-I-490 Rev. 00
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Program Method Analyte Matrix Primary SOP
RCRP EPA 1613B 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)
TISSUE MN
RCRP EPA 1613B 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)
SCM MN
RCRP EPA 1613B 1,2,3,4,6,7,8,9-Octachlorodibenzofuran(OCDF)
SCM MN
RCRP EPA 1613B 1,2,3,4,6,7,8,9-Octachlorodibenzofuran(OCDF)
TISSUE MN
RCRP EPA 1613B 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)
TISSUE MN
RCRP EPA 1613B 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)
SCM MN
RCRP EPA 1613B 1,2,3,4,6,7,8-Heptachlorodibenzofuran(1,2,3,4,6,7,8-hpcdf)
SCM MN
RCRP EPA 1613B 1,2,3,4,6,7,8-Heptachlorodibenzofuran(1,2,3,4,6,7,8-hpcdf)
TISSUE MN
RCRP EPA 1613B 1,2,3,4,7,8,9-Heptachlorodibenzofuran(1,2,3,4,7,8,9-hpcdf)
SCM MN
RCRP EPA 1613B 1,2,3,4,7,8,9-Heptachlorodibenzofuran(1,2,3,4,7,8,9-hpcdf)
TISSUE MN
RCRP EPA 1613B 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,4,7,8-Hxcdd)
SCM MN
RCRP EPA 1613B 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,4,7,8-Hxcdd)
TISSUE MN
RCRP EPA 1613B 1,2,3,4,7,8-Hexachlorodibenzofuran(1,2,3,4,7,8-Hxcdf)
SCM MN
RCRP EPA 1613B 1,2,3,4,7,8-Hexachlorodibenzofuran(1,2,3,4,7,8-Hxcdf)
TISSUE MN
RCRP EPA 1613B 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,6,7,8-Hxcdd)
SCM MN
RCRP EPA 1613B 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,6,7,8-Hxcdd)
TISSUE MN
RCRP EPA 1613B 1,2,3,6,7,8-Hexachlorodibenzofuran(1,2,3,6,7,8-Hxcdf)
TISSUE MN
RCRP EPA 1613B 1,2,3,6,7,8-Hexachlorodibenzofuran(1,2,3,6,7,8-Hxcdf)
SCM MN
RCRP EPA 1613B 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin(1,2,3,7,8,9-Hxcdd)
TISSUE MN
RCRP EPA 1613B 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin(1,2,3,7,8,9-Hxcdd)
SCM MN
RCRP EPA 1613B 1,2,3,7,8,9-Hexachlorodibenzofuran(1,2,3,7,8,9-Hxcdf)
SCM MN
RCRP EPA 1613B 1,2,3,7,8,9-Hexachlorodibenzofuran(1,2,3,7,8,9-Hxcdf)
TISSUE MN
RCRP EPA 1613B 1,2,3,7,8-Pentachlorodibenzo-p-dioxin(1,2,3,7,8-Pecdd)
TISSUE MN
RCRP EPA 1613B 1,2,3,7,8-Pentachlorodibenzo-p-dioxin(1,2,3,7,8-Pecdd)
SCM MN
RCRP EPA 1613B 1,2,3,7,8-Pentachlorodibenzofuran(1,2,3,7,8-Pecdf)
SCM MN
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EPA 1668A Preparation Techniques: N/A
Program Method Analyte Matrix Primary SOP
RCRP EPA 1613B 1,2,3,7,8-Pentachlorodibenzofuran(1,2,3,7,8-Pecdf)
TISSUE MN
RCRP EPA 1613B 2,3,4,6,7,8-Hexachlorodibenzofuran SCM MN
RCRP EPA 1613B 2,3,4,6,7,8-Hexachlorodibenzofuran TISSUE MN
RCRP EPA 1613B 2,3,4,7,8-Pentachlorodibenzofuran TISSUE MN
RCRP EPA 1613B 2,3,4,7,8-Pentachlorodibenzofuran SCM MN
RCRP EPA 1613B 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)
TISSUE MN
RCRP EPA 1613B 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)
SCM MN
RCRP EPA 1613B 2,3,7,8-Tetrachlorodibenzofuran SCM MN
RCRP EPA 1613B 2,3,7,8-Tetrachlorodibenzofuran TISSUE MN
RCRP EPA 1613B Total HpCDD TISSUE MN
RCRP EPA 1613B Total HpCDD SCM MN
RCRP EPA 1613B Total HpCDF TISSUE MN
RCRP EPA 1613B Total HpCDF SCM MN
RCRP EPA 1613B Total HxCDD SCM MN
RCRP EPA 1613B Total HxCDD TISSUE MN
RCRP EPA 1613B Total HxCDF TISSUE MN
RCRP EPA 1613B Total HxCDF SCM MN
RCRP EPA 1613B Total PeCDD SCM MN
RCRP EPA 1613B Total PeCDD TISSUE MN
RCRP EPA 1613B Total PeCDF TISSUE MN
RCRP EPA 1613B Total PeCDF SCM MN
RCRP EPA 1613B Total TCDD SCM MN
RCRP EPA 1613B Total TCDD TISSUE MN
RCRP EPA 1613B Total TCDF TISSUE MN
RCRP EPA 1613B Total TCDF SCM MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 1668A 2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl(BZ-206)
SCM MN
RCRP EPA 1668A 2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl(BZ-206)
TISSUE MN
RCRP EPA 1668A 2,2',3,3',4,4',5,5'-Octachlorobiphenyl(BZ-194)
TISSUE MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 1668A 2,2',3,3',4,4',5,5'-Octachlorobiphenyl(BZ-194)
SCM MN
RCRP EPA 1668A 2,2',3,3',4,4',5,6'-Octachlorobiphenyl(BZ-196)
TISSUE MN
RCRP EPA 1668A 2,2',3,3',4,4',5,6'-Octachlorobiphenyl(BZ-196)
SCM MN
RCRP EPA 1668A 2,2',3,3',4,4',5,6,6'-Nonachlorobiphenyl(BZ-207)
SCM MN
RCRP EPA 1668A 2,2',3,3',4,4',5,6,6'-Nonachlorobiphenyl(BZ-207)
TISSUE MN
RCRP EPA 1668A 2,2',3,3',4,4',5,6-Octachlorobiphenyl(BZ-195)
SCM MN
RCRP EPA 1668A 2,2',3,3',4,4',5,6-Octachlorobiphenyl(BZ-195)
TISSUE MN
RCRP EPA 1668A 2,2',3,3',4,4',5-Heptachlorobiphenyl (BZ-170)
SCM MN
RCRP EPA 1668A 2,2',3,3',4,4',5-Heptachlorobiphenyl (BZ-170)
TISSUE MN
RCRP EPA 1668A 2,2',3,3',4,5',6'-Heptachlorobiphenyl(BZ-177)
TISSUE MN
RCRP EPA 1668A 2,2',3,3',4,5',6'-Heptachlorobiphenyl(BZ-177)
SCM MN
RCRP EPA 1668A 2,2',3,3',4,5',6,6'-Octachlorobiphenyl(BZ-201)
TISSUE MN
RCRP EPA 1668A 2,2',3,3',4,5',6,6'-Octachlorobiphenyl(BZ-201)
SCM MN
RCRP EPA 1668A 2,2',3,3',4,5',6-Heptachlorobiphenyl (BZ-175)
SCM MN
RCRP EPA 1668A 2,2',3,3',4,5',6-Heptachlorobiphenyl (BZ-175)
TISSUE MN
RCRP EPA 1668A 2,2',3,3',4,5'-Hexachlorobiphenyl (BZ-130)
SCM MN
RCRP EPA 1668A 2,2',3,3',4,5'-Hexachlorobiphenyl (BZ-130)
TISSUE MN
RCRP EPA 1668A 2,2',3,3',4,5,5',6,6'-Nonachlorobiphenyl(BZ-208)
TISSUE MN
RCRP EPA 1668A 2,2',3,3',4,5,5',6,6'-Nonachlorobiphenyl(BZ-208)
SCM MN
RCRP EPA 1668A 2,2',3,3',4,5,5'-Heptachlorobiphenyl (BZ-172)
TISSUE MN
RCRP EPA 1668A 2,2',3,3',4,5,5'-Heptachlorobiphenyl (BZ-172)
SCM MN
RCRP EPA 1668A 2,2',3,3',4,5,6'-Heptachlorobiphenyl (BZ-174)
SCM MN
RCRP EPA 1668A 2,2',3,3',4,5,6'-Heptachlorobiphenyl (BZ-174)
TISSUE MN
RCRP EPA 1668A 2,2',3,3',4,6'-Hexachlorobiphenyl (BZ-132)
SCM MN
RCRP EPA 1668A 2,2',3,3',4,6'-Hexachlorobiphenyl (BZ-132)
TISSUE MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 1668A 2,2',3,3',4,6,6'-Heptachlorobiphenyl (BZ-176)
TISSUE MN
RCRP EPA 1668A 2,2',3,3',4,6,6'-Heptachlorobiphenyl (BZ-176)
SCM MN
RCRP EPA 1668A 2,2',3,3',4,6-Hexachlorobiphenyl (BZ-131)
SCM MN
RCRP EPA 1668A 2,2',3,3',4,6-Hexachlorobiphenyl (BZ-131)
TISSUE MN
RCRP EPA 1668A 2,2',3,3',4-Pentachlorobiphenyl (BZ-82) TISSUE MN
RCRP EPA 1668A 2,2',3,3',4-Pentachlorobiphenyl (BZ-82) SCM MN
RCRP EPA 1668A 2,2',3,3',5,5',6,6'-Octachlorobiphenyl(BZ-202)
SCM MN
RCRP EPA 1668A 2,2',3,3',5,5',6,6'-Octachlorobiphenyl(BZ-202)
TISSUE MN
RCRP EPA 1668A 2,2',3,3',5,5',6-Heptachlorobiphenyl (BZ-178)
SCM MN
RCRP EPA 1668A 2,2',3,3',5,5',6-Heptachlorobiphenyl (BZ-178)
TISSUE MN
RCRP EPA 1668A 2,2',3,3',5,5'-Hexachlorobiphenyl (BZ-133)
SCM MN
RCRP EPA 1668A 2,2',3,3',5,5'-Hexachlorobiphenyl (BZ-133)
TISSUE MN
RCRP EPA 1668A 2,2',3,3',5,6,6'-Heptachlorobiphenyl (BZ-179)
TISSUE MN
RCRP EPA 1668A 2,2',3,3',5,6,6'-Heptachlorobiphenyl (BZ-179)
SCM MN
RCRP EPA 1668A 2,2',3,3',5-Pentachlorobiphenyl (BZ-83) SCM MN
RCRP EPA 1668A 2,2',3,3',5-Pentachlorobiphenyl (BZ-83) TISSUE MN
RCRP EPA 1668A 2,2',3,3',6,6'-Hexachlorobiphenyl (BZ-136)
SCM MN
RCRP EPA 1668A 2,2',3,3',6,6'-Hexachlorobiphenyl (BZ-136)
TISSUE MN
RCRP EPA 1668A 2,2',3,3',6-Pentachlorobiphenyl (BZ-84) TISSUE MN
RCRP EPA 1668A 2,2',3,3',6-Pentachlorobiphenyl (BZ-84) SCM MN
RCRP EPA 1668A 2,2',3,4',5,5'-Hexachlorobiphenyl (BZ-146)
TISSUE MN
RCRP EPA 1668A 2,2',3,4',5,5'-Hexachlorobiphenyl (BZ-146)
SCM MN
RCRP EPA 1668A 2,2',3,4',5,6'-Hexachlorobiphenyl (BZ-148)
TISSUE MN
RCRP EPA 1668A 2,2',3,4',5,6'-Hexachlorobiphenyl (BZ-148)
SCM MN
RCRP EPA 1668A 2,2',3,4',5,6,6'-Heptachlorobiphenyl (BZ-188)
TISSUE MN
RCRP EPA 1668A 2,2',3,4',5,6,6'-Heptachlorobiphenyl (BZ-188)
SCM MN
RCRP EPA 1668A 2,2',3,4',6,6'-Hexachlorobiphenyl (BZ-150)
SCM MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 1668A 2,2',3,4',6,6'-Hexachlorobiphenyl (BZ-150)
TISSUE MN
RCRP EPA 1668A 2,2',3,4'-Tetrachlorobiphenyl (BZ-42) SCM MN
RCRP EPA 1668A 2,2',3,4'-Tetrachlorobiphenyl (BZ-42) TISSUE MN
RCRP EPA 1668A 2,2',3,4,4',5,5',6-Octachlorobiphenyl(BZ-203)
SCM MN
RCRP EPA 1668A 2,2',3,4,4',5,5',6-Octachlorobiphenyl(BZ-203)
TISSUE MN
RCRP EPA 1668A 2,2',3,4,4',5,6'-Heptachlorobiphenyl (BZ-182)
TISSUE MN
RCRP EPA 1668A 2,2',3,4,4',5,6'-Heptachlorobiphenyl (BZ-182)
SCM MN
RCRP EPA 1668A 2,2',3,4,4',5,6,6'-Octachlorobiphenyl(BZ-204)
TISSUE MN
RCRP EPA 1668A 2,2',3,4,4',5,6,6'-Octachlorobiphenyl(BZ-204)
SCM MN
RCRP EPA 1668A 2,2',3,4,4',5,6-Heptachlorobiphenyl (BZ-181)
SCM MN
RCRP EPA 1668A 2,2',3,4,4',5,6-Heptachlorobiphenyl (BZ-181)
TISSUE MN
RCRP EPA 1668A 2,2',3,4,4',5-Hexachlorobiphenyl (BZ-137)
TISSUE MN
RCRP EPA 1668A 2,2',3,4,4',5-Hexachlorobiphenyl (BZ-137)
SCM MN
RCRP EPA 1668A 2,2',3,4,4',6,6'-Heptachlorobiphenyl (BZ-184)
SCM MN
RCRP EPA 1668A 2,2',3,4,4',6,6'-Heptachlorobiphenyl (BZ-184)
TISSUE MN
RCRP EPA 1668A 2,2',3,4,5',6-Hexachlorobiphenyl (BZ-144)
SCM MN
RCRP EPA 1668A 2,2',3,4,5',6-Hexachlorobiphenyl (BZ-144)
TISSUE MN
RCRP EPA 1668A 2,2',3,4,5,5'-Hexachlorobiphenyl (BZ-141)
SCM MN
RCRP EPA 1668A 2,2',3,4,5,5'-Hexachlorobiphenyl (BZ-141)
TISSUE MN
RCRP EPA 1668A 2,2',3,4,5,6,6'-Heptachlorobiphenyl (BZ-186)
SCM MN
RCRP EPA 1668A 2,2',3,4,5,6,6'-Heptachlorobiphenyl (BZ-186)
TISSUE MN
RCRP EPA 1668A 2,2',3,4,5,6-Hexachlorobiphenyl (BZ-142)
TISSUE MN
RCRP EPA 1668A 2,2',3,4,5,6-Hexachlorobiphenyl (BZ-142)
SCM MN
RCRP EPA 1668A 2,2',3,4,6'-Pentachlorobiphenyl (BZ-89) TISSUE MN
RCRP EPA 1668A 2,2',3,4,6'-Pentachlorobiphenyl (BZ-89) SCM MN
RCRP EPA 1668A 2,2',3,4,6,6'-Hexachlorobiphenyl (BZ-145)
SCM MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 1668A 2,2',3,4,6,6'-Hexachlorobiphenyl (BZ-145)
TISSUE MN
RCRP EPA 1668A 2,2',3,5',6-Pentachlorobiphenyl (BZ-95) TISSUE MN
RCRP EPA 1668A 2,2',3,5',6-Pentachlorobiphenyl (BZ-95) SCM MN
RCRP EPA 1668A 2,2',3,5,5'-Pentachlorobiphenyl (BZ-92) SCM MN
RCRP EPA 1668A 2,2',3,5,5'-Pentachlorobiphenyl (BZ-92) TISSUE MN
RCRP EPA 1668A 2,2',3,5,6'-Pentachlorobiphenyl (BZ-94) TISSUE MN
RCRP EPA 1668A 2,2',3,5,6'-Pentachlorobiphenyl (BZ-94) SCM MN
RCRP EPA 1668A 2,2',3,5,6,6'-Hexachlorobiphenyl (BZ-152)
TISSUE MN
RCRP EPA 1668A 2,2',3,5,6,6'-Hexachlorobiphenyl (BZ-152)
SCM MN
RCRP EPA 1668A 2,2',3,6'-Tetrachlorobiphenyl (BZ-46) SCM MN
RCRP EPA 1668A 2,2',3,6'-Tetrachlorobiphenyl (BZ-46) TISSUE MN
RCRP EPA 1668A 2,2',3,6,6'-Pentachlorobiphenyl (BZ-96) TISSUE MN
RCRP EPA 1668A 2,2',3,6,6'-Pentachlorobiphenyl (BZ-96) SCM MN
RCRP EPA 1668A 2,2',3-Trichlorobiphenyl (BZ-16) TISSUE MN
RCRP EPA 1668A 2,2',3-Trichlorobiphenyl (BZ-16) SCM MN
RCRP EPA 1668A 2,2',4,4',5,6'-Hexachlorobiphenyl (BZ-154)
SCM MN
RCRP EPA 1668A 2,2',4,4',5,6'-Hexachlorobiphenyl (BZ-154)
TISSUE MN
RCRP EPA 1668A 2,2',4,4',5-Pentachlorobiphenyl (BZ-99) TISSUE MN
RCRP EPA 1668A 2,2',4,4',5-Pentachlorobiphenyl (BZ-99) SCM MN
RCRP EPA 1668A 2,2',4,4',6,6'-Hexachlorobiphenyl (BZ-155)
TISSUE MN
RCRP EPA 1668A 2,2',4,4',6,6'-Hexachlorobiphenyl (BZ-155)
SCM MN
RCRP EPA 1668A 2,2',4,5',6-Pentachlorobiphenyl (BZ-103) SCM MN
RCRP EPA 1668A 2,2',4,5',6-Pentachlorobiphenyl (BZ-103) TISSUE MN
RCRP EPA 1668A 2,2',4,5-Tetrachlorobiphenyl (BZ-48) TISSUE MN
RCRP EPA 1668A 2,2',4,5-Tetrachlorobiphenyl (BZ-48) SCM MN
RCRP EPA 1668A 2,2',4,6,6'-Pentachlorobiphenyl (BZ-104) TISSUE MN
RCRP EPA 1668A 2,2',4,6,6'-Pentachlorobiphenyl (BZ-104) SCM MN
RCRP EPA 1668A 2,2',4-Trichlorobiphenyl (BZ-17) SCM MN
RCRP EPA 1668A 2,2',4-Trichlorobiphenyl (BZ-17) TISSUE MN
RCRP EPA 1668A 2,2',5,5'-Tetrachlorobiphenyl (BZ-52) TISSUE MN
RCRP EPA 1668A 2,2',5,5'-Tetrachlorobiphenyl (BZ-52) SCM MN
RCRP EPA 1668A 2,2',6,6'-Tetrachlorobiphenyl (BZ-54) SCM MN
RCRP EPA 1668A 2,2',6,6'-Tetrachlorobiphenyl (BZ-54) TISSUE MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 1668A 2,2',6-Trichlorobiphenyl (BZ-19) TISSUE MN
RCRP EPA 1668A 2,2',6-Trichlorobiphenyl (BZ-19) SCM MN
RCRP EPA 1668A 2,2'-Dichlorobiphenyl (BZ-4) TISSUE MN
RCRP EPA 1668A 2,2'-Dichlorobiphenyl (BZ-4) SCM MN
RCRP EPA 1668A 2,3',4,4',5'-Pentachlorobiphenyl (BZ-123)
TISSUE MN
RCRP EPA 1668A 2,3',4,4',5'-Pentachlorobiphenyl (BZ-123)
NPW MN
RCRP EPA 1668A 2,3',4,4',5'-Pentachlorobiphenyl (BZ-123)
SCM MN
RCRP EPA 1668A 2,3',4,4',5,5'-Hexachlorobiphenyl (BZ-167)
SCM MN
RCRP EPA 1668A 2,3',4,4',5,5'-Hexachlorobiphenyl (BZ-167)
NPW MN
RCRP EPA 1668A 2,3',4,4',5,5'-Hexachlorobiphenyl (BZ-167)
TISSUE MN
RCRP EPA 1668A 2,3',4,4',5-Pentachlorobiphenyl (BZ-118) SCM MN
RCRP EPA 1668A 2,3',4,4',5-Pentachlorobiphenyl (BZ-118) NPW MN
RCRP EPA 1668A 2,3',4,4',5-Pentachlorobiphenyl (BZ-118) TISSUE MN
RCRP EPA 1668A 2,3',4,4'-Tetrachlorobiphenyl (BZ-66) SCM MN
RCRP EPA 1668A 2,3',4,4'-Tetrachlorobiphenyl (BZ-66) TISSUE MN
RCRP EPA 1668A 2,3',4,5',6-Pentachlorobiphenyl (BZ-121) SCM MN
RCRP EPA 1668A 2,3',4,5',6-Pentachlorobiphenyl (BZ-121) TISSUE MN
RCRP EPA 1668A 2,3',4,5'-Tetrachlorobiphenyl (BZ-68) SCM MN
RCRP EPA 1668A 2,3',4,5'-Tetrachlorobiphenyl (BZ-68) TISSUE MN
RCRP EPA 1668A 2,3',4,5,5'-Pentachlorobiphenyl (BZ-120) SCM MN
RCRP EPA 1668A 2,3',4,5,5'-Pentachlorobiphenyl (BZ-120) TISSUE MN
RCRP EPA 1668A 2,3',4,5-Tetrachlorobiphenyl (BZ-67) TISSUE MN
RCRP EPA 1668A 2,3',4,5-Tetrachlorobiphenyl (BZ-67) SCM MN
RCRP EPA 1668A 2,3',4-Trichlorobiphenyl (BZ-25) SCM MN
RCRP EPA 1668A 2,3',4-Trichlorobiphenyl (BZ-25) TISSUE MN
RCRP EPA 1668A 2,3',5'-Trichlorobiphenyl (BZ-34) SCM MN
RCRP EPA 1668A 2,3',5'-Trichlorobiphenyl (BZ-34) TISSUE MN
RCRP EPA 1668A 2,3',5,5'-Tetrachlorobiphenyl (BZ-72) SCM MN
RCRP EPA 1668A 2,3',5,5'-Tetrachlorobiphenyl (BZ-72) TISSUE MN
RCRP EPA 1668A 2,3',6-Trichlorobiphenyl (BZ-27) SCM MN
RCRP EPA 1668A 2,3',6-Trichlorobiphenyl (BZ-27) TISSUE MN
RCRP EPA 1668A 2,3'-Dichlorobiphenyl (BZ-6) SCM MN
RCRP EPA 1668A 2,3'-Dichlorobiphenyl (BZ-6) TISSUE MN
Page 42 of 87
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Program Method Analyte Matrix Primary SOP
RCRP EPA 1668A 2,3,3',4',5',6-Hexachlorobiphenyl (BZ-164)
SCM MN
RCRP EPA 1668A 2,3,3',4',5',6-Hexachlorobiphenyl (BZ-164)
TISSUE MN
RCRP EPA 1668A 2,3,3',4',5'-Pentachlorobiphenyl (BZ-122)
SCM MN
RCRP EPA 1668A 2,3,3',4',5'-Pentachlorobiphenyl (BZ-122)
TISSUE MN
RCRP EPA 1668A 2,3,3',4',5,5'-Hexachlorobiphenyl (BZ-162)
TISSUE MN
RCRP EPA 1668A 2,3,3',4',5,5'-Hexachlorobiphenyl (BZ-162)
SCM MN
RCRP EPA 1668A 2,3,3',4'-Tetrachlorobiphenyl (BZ-56) SCM MN
RCRP EPA 1668A 2,3,3',4'-Tetrachlorobiphenyl (BZ-56) TISSUE MN
RCRP EPA 1668A 2,3,3',4,4',5',6-Heptachlorobiphenyl (BZ-191)
SCM MN
RCRP EPA 1668A 2,3,3',4,4',5',6-Heptachlorobiphenyl (BZ-191)
TISSUE MN
RCRP EPA 1668A 2,3,3',4,4',5'-Hexachlorobiphenyl (BZ-157)
NPW MN
RCRP EPA 1668A 2,3,3',4,4',5'-Hexachlorobiphenyl (BZ-157)
SCM MN
RCRP EPA 1668A 2,3,3',4,4',5,5',6-Octachlorobiphenyl(BZ-205)
TISSUE MN
RCRP EPA 1668A 2,3,3',4,4',5,5',6-Octachlorobiphenyl(BZ-205)
SCM MN
RCRP EPA 1668A 2,3,3',4,4',5,5'-Heptachlorobiphenyl (BZ-189)
NPW MN
RCRP EPA 1668A 2,3,3',4,4',5,5'-Heptachlorobiphenyl (BZ-189)
TISSUE MN
RCRP EPA 1668A 2,3,3',4,4',5,5'-Heptachlorobiphenyl (BZ-189)
SCM MN
RCRP EPA 1668A 2,3,3',4,4',5,6-Heptachlorobiphenyl (BZ-190)
SCM MN
RCRP EPA 1668A 2,3,3',4,4',5,6-Heptachlorobiphenyl (BZ-190)
TISSUE MN
RCRP EPA 1668A 2,3,3',4,4',5-Hexachlorobiphenyl (BZ-156)
SCM MN
RCRP EPA 1668A 2,3,3',4,4',5-Hexachlorobiphenyl (BZ-156)
NPW MN
RCRP EPA 1668A 2,3,3',4,4',6-Hexachlorobiphenyl (BZ-158)
TISSUE MN
RCRP EPA 1668A 2,3,3',4,4',6-Hexachlorobiphenyl (BZ-158)
SCM MN
RCRP EPA 1668A 2,3,3',4,4'-Pentachlorobiphenyl (BZ-105) NPW MN
RCRP EPA 1668A 2,3,3',4,4'-Pentachlorobiphenyl (BZ-105) TISSUE MN
RCRP EPA 1668A 2,3,3',4,4'-Pentachlorobiphenyl (BZ-105) SCM MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 1668A 2,3,3',4,5',6-Hexachlorobiphenyl (BZ-161)
TISSUE MN
RCRP EPA 1668A 2,3,3',4,5',6-Hexachlorobiphenyl (BZ-161)
SCM MN
RCRP EPA 1668A 2,3,3',4,5,5',6-Heptachlorobiphenyl (BZ-192)
SCM MN
RCRP EPA 1668A 2,3,3',4,5,5',6-Heptachlorobiphenyl (BZ-192)
TISSUE MN
RCRP EPA 1668A 2,3,3',4,5,5'-Hexachlorobiphenyl (BZ-159)
SCM MN
RCRP EPA 1668A 2,3,3',4,5,5'-Hexachlorobiphenyl (BZ-159)
TISSUE MN
RCRP EPA 1668A 2,3,3',4,5,6-Hexachlorobiphenyl (BZ-160)
SCM MN
RCRP EPA 1668A 2,3,3',4,5,6-Hexachlorobiphenyl (BZ-160)
TISSUE MN
RCRP EPA 1668A 2,3,3',4,5-Pentachlorobiphenyl (BZ-106) SCM MN
RCRP EPA 1668A 2,3,3',4,5-Pentachlorobiphenyl (BZ-106) TISSUE MN
RCRP EPA 1668A 2,3,3',4,6-Pentachlorobiphenyl (BZ-109) SCM MN
RCRP EPA 1668A 2,3,3',4,6-Pentachlorobiphenyl (BZ-109) TISSUE MN
RCRP EPA 1668A 2,3,3',4-Tetrachlorobiphenyl (BZ-55) SCM MN
RCRP EPA 1668A 2,3,3',4-Tetrachlorobiphenyl (BZ-55) TISSUE MN
RCRP EPA 1668A 2,3,3',5'-Tetrachlorobiphenyl (BZ-58) TISSUE MN
RCRP EPA 1668A 2,3,3',5'-Tetrachlorobiphenyl (BZ-58) SCM MN
RCRP EPA 1668A 2,3,3',5,5',6-Hexachlorobiphenyl (BZ-165)
SCM MN
RCRP EPA 1668A 2,3,3',5,5',6-Hexachlorobiphenyl (BZ-165)
TISSUE MN
RCRP EPA 1668A 2,3,3',5,5'-Pentachlorobiphenyl (BZ-111) TISSUE MN
RCRP EPA 1668A 2,3,3',5,5'-Pentachlorobiphenyl (BZ-111) SCM MN
RCRP EPA 1668A 2,3,3',5,6-Pentachlorobiphenyl (BZ-112) SCM MN
RCRP EPA 1668A 2,3,3',5,6-Pentachlorobiphenyl (BZ-112) TISSUE MN
RCRP EPA 1668A 2,3,3',5-Tetrachlorobiphenyl (BZ-57) SCM MN
RCRP EPA 1668A 2,3,3',5-Tetrachlorobiphenyl (BZ-57) TISSUE MN
RCRP EPA 1668A 2,3,4',5-Tetrachlorobiphenyl (BZ-63) SCM MN
RCRP EPA 1668A 2,3,4',5-Tetrachlorobiphenyl (BZ-63) TISSUE MN
RCRP EPA 1668A 2,3,4',6-Tetrachlorobiphenyl (BZ-64) TISSUE MN
RCRP EPA 1668A 2,3,4',6-Tetrachlorobiphenyl (BZ-64) SCM MN
RCRP EPA 1668A 2,3,4'-Trichlorobiphenyl (BZ-22) SCM MN
RCRP EPA 1668A 2,3,4'-Trichlorobiphenyl (BZ-22) TISSUE MN
RCRP EPA 1668A 2,3,4,4',5-Pentachlorobiphenyl (BZ-114) SCM MN
RCRP EPA 1668A 2,3,4,4',5-Pentachlorobiphenyl (BZ-114) NPW MN
Page 44 of 87
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Program Method Analyte Matrix Primary SOP
RCRP EPA 1668A 2,3,4,4',5-Pentachlorobiphenyl (BZ-114) TISSUE MN
RCRP EPA 1668A 2,3,4,4'-Tetrachlorobiphenyl (BZ-60) SCM MN
RCRP EPA 1668A 2,3,4,4'-Tetrachlorobiphenyl (BZ-60) TISSUE MN
RCRP EPA 1668A 2,3,5-Trichlorobiphenyl (BZ-23) SCM MN
RCRP EPA 1668A 2,3,5-Trichlorobiphenyl (BZ-23) TISSUE MN
RCRP EPA 1668A 2,3,6-Trichlorobiphenyl (BZ-24) SCM MN
RCRP EPA 1668A 2,3,6-Trichlorobiphenyl (BZ-24) TISSUE MN
RCRP EPA 1668A 2,3-Dichlorobiphenyl (BZ-5) SCM MN
RCRP EPA 1668A 2,3-Dichlorobiphenyl (BZ-5) TISSUE MN
RCRP EPA 1668A 2,4',5-Trichlorobiphenyl (BZ-31) SCM MN
RCRP EPA 1668A 2,4',5-Trichlorobiphenyl (BZ-31) TISSUE MN
RCRP EPA 1668A 2,4',6-Trichlorobiphenyl (BZ-32) TISSUE MN
RCRP EPA 1668A 2,4',6-Trichlorobiphenyl (BZ-32) SCM MN
RCRP EPA 1668A 2,4'-Dichlorobiphenyl (BZ-8) TISSUE MN
RCRP EPA 1668A 2,4'-Dichlorobiphenyl (BZ-8) SCM MN
RCRP EPA 1668A 2,4-Dichlorobiphenyl (BZ-7) SCM MN
RCRP EPA 1668A 2,4-Dichlorobiphenyl (BZ-7) TISSUE MN
RCRP EPA 1668A 2,5-Dichlorobiphenyl (BZ-9) SCM MN
RCRP EPA 1668A 2,5-Dichlorobiphenyl (BZ-9) TISSUE MN
RCRP EPA 1668A 2,6-Dichlorobiphenyl (BZ-10) SCM MN
RCRP EPA 1668A 2,6-Dichlorobiphenyl (BZ-10) TISSUE MN
RCRP EPA 1668A 2-Chlorobiphenyl (BZ-1) SCM MN
RCRP EPA 1668A 2-Chlorobiphenyl (BZ-1) TISSUE MN
RCRP EPA 1668A 3,3',4,4',5,5'-Hexachlorobiphenyl (BZ-169)
TISSUE MN
RCRP EPA 1668A 3,3',4,4',5,5'-Hexachlorobiphenyl (BZ-169)
SCM MN
RCRP EPA 1668A 3,3',4,4',5,5'-Hexachlorobiphenyl (BZ-169)
NPW MN
RCRP EPA 1668A 3,3',4,4',5-Pentachlorobiphenyl (BZ-126) NPW MN
RCRP EPA 1668A 3,3',4,4',5-Pentachlorobiphenyl (BZ-126) TISSUE MN
RCRP EPA 1668A 3,3',4,4',5-Pentachlorobiphenyl (BZ-126) SCM MN
RCRP EPA 1668A 3,3',4,4'-Tetrachlorobiphenyl (BZ-77) NPW MN
RCRP EPA 1668A 3,3',4,4'-Tetrachlorobiphenyl (BZ-77) TISSUE MN
RCRP EPA 1668A 3,3',4,4'-Tetrachlorobiphenyl (BZ-77) SCM MN
RCRP EPA 1668A 3,3',4,5'-Tetrachlorobiphenyl (BZ-79) TISSUE MN
RCRP EPA 1668A 3,3',4,5'-Tetrachlorobiphenyl (BZ-79) SCM MN
RCRP EPA 1668A 3,3',4,5,5'-Pentachlorobiphenyl (BZ-127) TISSUE MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 1668A 3,3',4,5,5'-Pentachlorobiphenyl (BZ-127) SCM MN
RCRP EPA 1668A 3,3',4,5-Tetrachlorobiphenyl (BZ-78) SCM MN
RCRP EPA 1668A 3,3',4,5-Tetrachlorobiphenyl (BZ-78) TISSUE MN
RCRP EPA 1668A 3,3',4-Trichlorobiphenyl (BZ-35) SCM MN
RCRP EPA 1668A 3,3',4-Trichlorobiphenyl (BZ-35) TISSUE MN
RCRP EPA 1668A 3,3',5,5'-Tetrachlorobiphenyl (BZ-80) SCM MN
RCRP EPA 1668A 3,3',5,5'-Tetrachlorobiphenyl (BZ-80) TISSUE MN
RCRP EPA 1668A 3,3',5-Trichlorobiphenyl (BZ-36) TISSUE MN
RCRP EPA 1668A 3,3',5-Trichlorobiphenyl (BZ-36) SCM MN
RCRP EPA 1668A 3,3'-Dichlorobiphenyl (BZ-11) TISSUE MN
RCRP EPA 1668A 3,3'-Dichlorobiphenyl (BZ-11) SCM MN
RCRP EPA 1668A 3,4',5-Trichlorobiphenyl (BZ-39) SCM MN
RCRP EPA 1668A 3,4',5-Trichlorobiphenyl (BZ-39) TISSUE MN
RCRP EPA 1668A 3,4,4',5-Tetrachlorobiphenyl (BZ-81) SCM MN
RCRP EPA 1668A 3,4,4',5-Tetrachlorobiphenyl (BZ-81) NPW MN
RCRP EPA 1668A 3,4,4',5-Tetrachlorobiphenyl (BZ-81) TISSUE MN
RCRP EPA 1668A 3,4,4'-Trichlorobiphenyl (BZ-37) TISSUE MN
RCRP EPA 1668A 3,4,4'-Trichlorobiphenyl (BZ-37) SCM MN
RCRP EPA 1668A 3,4,5-Trichlorobiphenyl (BZ-38) TISSUE MN
RCRP EPA 1668A 3,4,5-Trichlorobiphenyl (BZ-38) SCM MN
RCRP EPA 1668A 3,5-Dichlorobiphenyl (BZ-14) SCM MN
RCRP EPA 1668A 3,5-Dichlorobiphenyl (BZ-14) TISSUE MN
RCRP EPA 1668A 3-Chlorobiphenyl (BZ-2) TISSUE MN
RCRP EPA 1668A 3-Chlorobiphenyl (BZ-2) SCM MN
RCRP EPA 1668A 4,4'-Dichlorobiphenyl (BZ-15) TISSUE MN
RCRP EPA 1668A 4,4'-Dichlorobiphenyl (BZ-15) SCM MN
RCRP EPA 1668A 4-Chlorobiphenyl (BZ-3) SCM MN
RCRP EPA 1668A 4-Chlorobiphenyl (BZ-3) TISSUE MN
RCRP EPA 1668A Decachlorobiphenyl (BZ-209) SCM MN
RCRP EPA 1668A Decachlorobiphenyl (BZ-209) TISSUE MN
RCRP EPA 1668A PCB-(100/93/102/98) SCM MN
RCRP EPA 1668A PCB-(100/93/102/98) TISSUE MN
RCRP EPA 1668A PCB-(107/124) SCM MN
RCRP EPA 1668A PCB-(107/124) TISSUE MN
RCRP EPA 1668A PCB-(108/119/86/97/125/87) TISSUE MN
RCRP EPA 1668A PCB-(108/119/86/97/125/87) SCM MN
Page 46 of 87
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Program Method Analyte Matrix Primary SOP
RCRP EPA 1668A PCB-(110/115) TISSUE MN
RCRP EPA 1668A PCB-(110/115) SCM MN
RCRP EPA 1668A PCB-(113/90/101) TISSUE MN
RCRP EPA 1668A PCB-(113/90/101) SCM MN
RCRP EPA 1668A PCB-(117/116/85) SCM MN
RCRP EPA 1668A PCB-(117/116/85) TISSUE MN
RCRP EPA 1668A PCB-(128/166) SCM MN
RCRP EPA 1668A PCB-(128/166) TISSUE MN
RCRP EPA 1668A PCB-(13/12) TISSUE MN
RCRP EPA 1668A PCB-(13/12) SCM MN
RCRP EPA 1668A PCB-(134/143) SCM MN
RCRP EPA 1668A PCB-(134/143) TISSUE MN
RCRP EPA 1668A PCB-(138/163/129) TISSUE MN
RCRP EPA 1668A PCB-(138/163/129) SCM MN
RCRP EPA 1668A PCB-(139/140) SCM MN
RCRP EPA 1668A PCB-(139/140) TISSUE MN
RCRP EPA 1668A PCB-(147/149) TISSUE MN
RCRP EPA 1668A PCB-(147/149) SCM MN
RCRP EPA 1668A PCB-(151/135) SCM MN
RCRP EPA 1668A PCB-(151/135) TISSUE MN
RCRP EPA 1668A PCB-(153/168) TISSUE MN
RCRP EPA 1668A PCB-(153/168) SCM MN
RCRP EPA 1668A PCB-(156/157) SCM MN
RCRP EPA 1668A PCB-(156/157) TISSUE MN
RCRP EPA 1668A PCB-(171/173) TISSUE MN
RCRP EPA 1668A PCB-(171/173) SCM MN
RCRP EPA 1668A PCB-(180/193) SCM MN
RCRP EPA 1668A PCB-(180/193) TISSUE MN
RCRP EPA 1668A PCB-(183/185) SCM MN
RCRP EPA 1668A PCB-(183/185) TISSUE MN
RCRP EPA 1668A PCB-(197/200) TISSUE MN
RCRP EPA 1668A PCB-(197/200) SCM MN
RCRP EPA 1668A PCB-(198/199) SCM MN
RCRP EPA 1668A PCB-(198/199) TISSUE MN
RCRP EPA 1668A PCB-(21/33) TISSUE MN
RCRP EPA 1668A PCB-(21/33) SCM MN
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EPA 1668C Preparation Techniques: N/A
Program Method Analyte Matrix Primary SOP
RCRP EPA 1668A PCB-(26/29) TISSUE MN
RCRP EPA 1668A PCB-(26/29) SCM MN
RCRP EPA 1668A PCB-(28/20) SCM MN
RCRP EPA 1668A PCB-(28/20) TISSUE MN
RCRP EPA 1668A PCB-(30/18) SCM MN
RCRP EPA 1668A PCB-(30/18) TISSUE MN
RCRP EPA 1668A PCB-(41/40/71) SCM MN
RCRP EPA 1668A PCB-(41/40/71) TISSUE MN
RCRP EPA 1668A PCB-(44/47/65) SCM MN
RCRP EPA 1668A PCB-(44/47/65) TISSUE MN
RCRP EPA 1668A PCB-(45/51) TISSUE MN
RCRP EPA 1668A PCB-(45/51) SCM MN
RCRP EPA 1668A PCB-(50/53) TISSUE MN
RCRP EPA 1668A PCB-(50/53) SCM MN
RCRP EPA 1668A PCB-(59/62/75) SCM MN
RCRP EPA 1668A PCB-(59/62/75) TISSUE MN
RCRP EPA 1668A PCB-(61/70/74/76) TISSUE MN
RCRP EPA 1668A PCB-(61/70/74/76) SCM MN
RCRP EPA 1668A PCB-(69/49) TISSUE MN
RCRP EPA 1668A PCB-(69/49) SCM MN
RCRP EPA 1668A PCB-(73/43) TISSUE MN
RCRP EPA 1668A PCB-(73/43) SCM MN
RCRP EPA 1668A PCB-(88/91) TISSUE MN
RCRP EPA 1668A PCB-(88/91) SCM MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 1668C 2,3',5',6-Tetrachlorobiphenyl (BZ-73) TISSUE MN
RCRP EPA 1668C 2,3',5',6-Tetrachlorobiphenyl (BZ-73) NPW MN
RCRP EPA 1668C 2,3',5',6-Tetrachlorobiphenyl (BZ-73) SCM MN
RCRP EPA 1668C PCB-(100/93/102/98) TISSUE MN
RCRP EPA 1668C PCB-(100/93/102/98) SCM MN
RCRP EPA 1668C PCB-(107/124) NPW MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 1668C PCB-(107/124) SCM MN
RCRP EPA 1668C PCB-(107/124) TISSUE MN
RCRP EPA 1668C PCB-(108/119/86/97/125/87) SCM MN
RCRP EPA 1668C PCB-(108/119/86/97/125/87) TISSUE MN
RCRP EPA 1668C PCB-(110/115) TISSUE MN
RCRP EPA 1668C PCB-(110/115) NPW MN
RCRP EPA 1668C PCB-(110/115) SCM MN
RCRP EPA 1668C PCB-(113/90/101) SCM MN
RCRP EPA 1668C PCB-(113/90/101) NPW MN
RCRP EPA 1668C PCB-(113/90/101) TISSUE MN
RCRP EPA 1668C PCB-(117/116/85) NPW MN
RCRP EPA 1668C PCB-(117/116/85) TISSUE MN
RCRP EPA 1668C PCB-(117/116/85) SCM MN
RCRP EPA 1668C PCB-(128/166) SCM MN
RCRP EPA 1668C PCB-(128/166) TISSUE MN
RCRP EPA 1668C PCB-(128/166) NPW MN
RCRP EPA 1668C PCB-(13/12) NPW MN
RCRP EPA 1668C PCB-(13/12) TISSUE MN
RCRP EPA 1668C PCB-(13/12) SCM MN
RCRP EPA 1668C PCB-(134/143) TISSUE MN
RCRP EPA 1668C PCB-(134/143) SCM MN
RCRP EPA 1668C PCB-(134/143) NPW MN
RCRP EPA 1668C PCB-(138/163/129) SCM MN
RCRP EPA 1668C PCB-(138/163/129) NPW MN
RCRP EPA 1668C PCB-(138/163/129) TISSUE MN
RCRP EPA 1668C PCB-(139/140) TISSUE MN
RCRP EPA 1668C PCB-(139/140) NPW MN
RCRP EPA 1668C PCB-(139/140) SCM MN
RCRP EPA 1668C PCB-(147/149) NPW MN
RCRP EPA 1668C PCB-(147/149) TISSUE MN
RCRP EPA 1668C PCB-(147/149) SCM MN
RCRP EPA 1668C PCB-(151/135) NPW MN
RCRP EPA 1668C PCB-(151/135) SCM MN
RCRP EPA 1668C PCB-(151/135) TISSUE MN
RCRP EPA 1668C PCB-(153/168) TISSUE MN
RCRP EPA 1668C PCB-(153/168) NPW MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 1668C PCB-(153/168) SCM MN
RCRP EPA 1668C PCB-(156/157) TISSUE MN
RCRP EPA 1668C PCB-(156/157) NPW MN
RCRP EPA 1668C PCB-(156/157) SCM MN
RCRP EPA 1668C PCB-(171/173) SCM MN
RCRP EPA 1668C PCB-(171/173) TISSUE MN
RCRP EPA 1668C PCB-(171/173) NPW MN
RCRP EPA 1668C PCB-(180/193) SCM MN
RCRP EPA 1668C PCB-(180/193) TISSUE MN
RCRP EPA 1668C PCB-(180/193) NPW MN
RCRP EPA 1668C PCB-(183/185) TISSUE MN
RCRP EPA 1668C PCB-(183/185) SCM MN
RCRP EPA 1668C PCB-(183/185) NPW MN
RCRP EPA 1668C PCB-(197/200) NPW MN
RCRP EPA 1668C PCB-(197/200) TISSUE MN
RCRP EPA 1668C PCB-(197/200) SCM MN
RCRP EPA 1668C PCB-(198/199) SCM MN
RCRP EPA 1668C PCB-(198/199) TISSUE MN
RCRP EPA 1668C PCB-(198/199) NPW MN
RCRP EPA 1668C PCB-(21/33) NPW MN
RCRP EPA 1668C PCB-(21/33) SCM MN
RCRP EPA 1668C PCB-(21/33) TISSUE MN
RCRP EPA 1668C PCB-(26/29) TISSUE MN
RCRP EPA 1668C PCB-(26/29) NPW MN
RCRP EPA 1668C PCB-(26/29) SCM MN
RCRP EPA 1668C PCB-(28/20) SCM MN
RCRP EPA 1668C PCB-(28/20) NPW MN
RCRP EPA 1668C PCB-(28/20) TISSUE MN
RCRP EPA 1668C PCB-(30/18) NPW MN
RCRP EPA 1668C PCB-(30/18) TISSUE MN
RCRP EPA 1668C PCB-(30/18) SCM MN
RCRP EPA 1668C PCB-(41/40/71) TISSUE MN
RCRP EPA 1668C PCB-(41/40/71) NPW MN
RCRP EPA 1668C PCB-(41/40/71) SCM MN
RCRP EPA 1668C PCB-(44/47/65) TISSUE MN
RCRP EPA 1668C PCB-(44/47/65) NPW MN
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EPA 8011 Preparation Techniques: Extraction, continuous liquid-liquid (LLE);
EPA 8081B Preparation Techniques: Extraction, ultrasonic; Extraction, separatory funnel liquid-liquid (LLE);
Program Method Analyte Matrix Primary SOP
RCRP EPA 1668C PCB-(44/47/65) SCM MN
RCRP EPA 1668C PCB-(45/51) SCM MN
RCRP EPA 1668C PCB-(45/51) TISSUE MN
RCRP EPA 1668C PCB-(45/51) NPW MN
RCRP EPA 1668C PCB-(50/53) NPW MN
RCRP EPA 1668C PCB-(50/53) TISSUE MN
RCRP EPA 1668C PCB-(50/53) SCM MN
RCRP EPA 1668C PCB-(59/62/75) TISSUE MN
RCRP EPA 1668C PCB-(59/62/75) NPW MN
RCRP EPA 1668C PCB-(59/62/75) SCM MN
RCRP EPA 1668C PCB-(61/70/74/76) SCM MN
RCRP EPA 1668C PCB-(61/70/74/76) NPW MN
RCRP EPA 1668C PCB-(61/70/74/76) TISSUE MN
RCRP EPA 1668C PCB-(69/49) NPW MN
RCRP EPA 1668C PCB-(69/49) TISSUE MN
RCRP EPA 1668C PCB-(69/49) SCM MN
RCRP EPA 1668C PCB-(88/91) SCM MN
RCRP EPA 1668C PCB-(88/91) TISSUE MN
RCRP EPA 1668C PCB-(88/91) NPW MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 8011 1,2-Dibromo-3-chloropropane (DBCP) NPW MN
RCRP EPA 8011 1,2-Dibromoethane (EDB, Ethylenedibromide)
NPW MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 8081B 4,4'-DDD SCM MN
RCRP EPA 8081B 4,4'-DDD NPW MN
RCRP EPA 8081B 4,4'-DDE SCM MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 8081B 4,4'-DDE NPW MN
RCRP EPA 8081B 4,4'-DDT NPW MN
RCRP EPA 8081B 4,4'-DDT SCM MN
RCRP EPA 8081B Aldrin NPW MN
RCRP EPA 8081B Aldrin SCM MN
RCRP EPA 8081B alpha-BHC (alpha-Hexachlorocyclohexane)
SCM MN
RCRP EPA 8081B alpha-BHC (alpha-Hexachlorocyclohexane)
NPW MN
RCRP EPA 8081B alpha-Chlordane NPW MN
RCRP EPA 8081B alpha-Chlordane SCM MN
RCRP EPA 8081B beta-BHC (beta-Hexachlorocyclohexane) NPW MN
RCRP EPA 8081B beta-BHC (beta-Hexachlorocyclohexane) SCM MN
RCRP EPA 8081B Chlordane (tech.) NPW MN
RCRP EPA 8081B Chlordane (tech.) SCM MN
RCRP EPA 8081B delta-BHC NPW MN
RCRP EPA 8081B delta-BHC SCM MN
RCRP EPA 8081B Dieldrin SCM MN
RCRP EPA 8081B Dieldrin NPW MN
RCRP EPA 8081B Endosulfan I SCM MN
RCRP EPA 8081B Endosulfan I NPW MN
RCRP EPA 8081B Endosulfan II NPW MN
RCRP EPA 8081B Endosulfan II SCM MN
RCRP EPA 8081B Endosulfan sulfate SCM MN
RCRP EPA 8081B Endosulfan sulfate NPW MN
RCRP EPA 8081B Endrin SCM MN
RCRP EPA 8081B Endrin NPW MN
RCRP EPA 8081B Endrin aldehyde SCM MN
RCRP EPA 8081B Endrin aldehyde NPW MN
RCRP EPA 8081B Endrin ketone SCM MN
RCRP EPA 8081B Endrin ketone NPW MN
RCRP EPA 8081B gamma-BHC (Lindane, gamma-HexachlorocyclohexanE)
SCM MN
RCRP EPA 8081B gamma-BHC (Lindane, gamma-HexachlorocyclohexanE)
NPW MN
RCRP EPA 8081B gamma-Chlordane NPW MN
RCRP EPA 8081B gamma-Chlordane SCM MN
RCRP EPA 8081B Heptachlor SCM MN
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EPA 8082 Preparation Techniques: Extraction, microwave; Extraction, ultrasonic; Extraction, soxhlet; Extraction, separatory funnel liquid-liquid
(LLE);
EPA 8082A Preparation Techniques: Extraction, microwave; Extraction, ultrasonic; Extraction, soxhlet; Extraction, separatory funnel liquid-liquid
(LLE);
Program Method Analyte Matrix Primary SOP
RCRP EPA 8081B Heptachlor NPW MN
RCRP EPA 8081B Heptachlor epoxide NPW MN
RCRP EPA 8081B Heptachlor epoxide SCM MN
RCRP EPA 8081B Isodrin NPW MN
RCRP EPA 8081B Isodrin SCM MN
RCRP EPA 8081B Methoxychlor SCM MN
RCRP EPA 8081B Methoxychlor NPW MN
RCRP EPA 8081B Toxaphene (Chlorinated camphene) SCM MN
RCRP EPA 8081B Toxaphene (Chlorinated camphene) NPW MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 8082 Aroclor-1016 (PCB-1016) NPW MN
RCRP EPA 8082 Aroclor-1016 (PCB-1016) SCM MN
RCRP EPA 8082 Aroclor-1221 (PCB-1221) SCM MN
RCRP EPA 8082 Aroclor-1221 (PCB-1221) NPW MN
RCRP EPA 8082 Aroclor-1232 (PCB-1232) SCM MN
RCRP EPA 8082 Aroclor-1232 (PCB-1232) NPW MN
RCRP EPA 8082 Aroclor-1242 (PCB-1242) NPW MN
RCRP EPA 8082 Aroclor-1242 (PCB-1242) SCM MN
RCRP EPA 8082 Aroclor-1248 (PCB-1248) NPW MN
RCRP EPA 8082 Aroclor-1248 (PCB-1248) SCM MN
RCRP EPA 8082 Aroclor-1254 (PCB-1254) SCM MN
RCRP EPA 8082 Aroclor-1254 (PCB-1254) NPW MN
RCRP EPA 8082 Aroclor-1260 (PCB-1260) SCM MN
RCRP EPA 8082 Aroclor-1260 (PCB-1260) NPW MN
RCRP EPA 8082 PCBs SCM MN
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EPA 8270C Preparation Techniques: Extraction, ultrasonic; Extraction, continuous liquid-liquid (LLE); Extraction, EPA 1311 TCLP, non-
volatiles; Extraction, soxhlet; Extraction, separatory funnel liquid-liquid (LLE); Extraction, EPA 1312 SPLP, non-volatiles;
Program Method Analyte Matrix Primary SOP
RCRP EPA 8082A Aroclor-1016 (PCB-1016) SCM MN
RCRP EPA 8082A Aroclor-1016 (PCB-1016) NPW MN
RCRP EPA 8082A Aroclor-1221 (PCB-1221) SCM MN
RCRP EPA 8082A Aroclor-1221 (PCB-1221) NPW MN
RCRP EPA 8082A Aroclor-1232 (PCB-1232) SCM MN
RCRP EPA 8082A Aroclor-1232 (PCB-1232) NPW MN
RCRP EPA 8082A Aroclor-1242 (PCB-1242) NPW MN
RCRP EPA 8082A Aroclor-1242 (PCB-1242) SCM MN
RCRP EPA 8082A Aroclor-1248 (PCB-1248) NPW MN
RCRP EPA 8082A Aroclor-1248 (PCB-1248) SCM MN
RCRP EPA 8082A Aroclor-1254 (PCB-1254) SCM MN
RCRP EPA 8082A Aroclor-1254 (PCB-1254) NPW MN
RCRP EPA 8082A Aroclor-1260 (PCB-1260) NPW MN
RCRP EPA 8082A Aroclor-1260 (PCB-1260) SCM MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 8270C 1,2,4-Trichlorobenzene SCM MN
RCRP EPA 8270C 1,2,4-Trichlorobenzene NPW MN
RCRP EPA 8270C 1,2-Dichlorobenzene NPW MN
RCRP EPA 8270C 1,2-Dichlorobenzene SCM MN
RCRP EPA 8270C 1,2-Diphenylhydrazine NPW MN
RCRP EPA 8270C 1,2-Diphenylhydrazine SCM MN
RCRP EPA 8270C 1,3-Dichlorobenzene SCM MN
RCRP EPA 8270C 1,3-Dichlorobenzene NPW MN
RCRP EPA 8270C 1,4-Dichlorobenzene NPW MN
RCRP EPA 8270C 1,4-Dichlorobenzene SCM MN
RCRP EPA 8270C 2,4,5-Trichlorophenol NPW MN
RCRP EPA 8270C 2,4,5-Trichlorophenol SCM MN
RCRP EPA 8270C 2,4,6-Trichlorophenol SCM MN
RCRP EPA 8270C 2,4,6-Trichlorophenol NPW MN
RCRP EPA 8270C 2,4-Dichlorophenol SCM MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 8270C 2,4-Dichlorophenol NPW MN
RCRP EPA 8270C 2,4-Dimethylphenol SCM MN
RCRP EPA 8270C 2,4-Dimethylphenol NPW MN
RCRP EPA 8270C 2,4-Dinitrophenol SCM MN
RCRP EPA 8270C 2,4-Dinitrophenol NPW MN
RCRP EPA 8270C 2,4-Dinitrotoluene (2,4-DNT) NPW MN
RCRP EPA 8270C 2,4-Dinitrotoluene (2,4-DNT) SCM MN
RCRP EPA 8270C 2,6-Dinitrotoluene (2,6-DNT) NPW MN
RCRP EPA 8270C 2,6-Dinitrotoluene (2,6-DNT) SCM MN
RCRP EPA 8270C 2-Chloronaphthalene NPW MN
RCRP EPA 8270C 2-Chloronaphthalene SCM MN
RCRP EPA 8270C 2-Chlorophenol SCM MN
RCRP EPA 8270C 2-Chlorophenol NPW MN
RCRP EPA 8270C 2-Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol)
SCM MN
RCRP EPA 8270C 2-Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol)
NPW MN
RCRP EPA 8270C 2-Methylnaphthalene NPW MN
RCRP EPA 8270C 2-Methylnaphthalene SCM MN
RCRP EPA 8270C 2-Methylphenol (o-Cresol) SCM MN
RCRP EPA 8270C 2-Methylphenol (o-Cresol) NPW MN
RCRP EPA 8270C 2-Nitroaniline SCM MN
RCRP EPA 8270C 2-Nitroaniline NPW MN
RCRP EPA 8270C 2-Nitrophenol SCM MN
RCRP EPA 8270C 2-Nitrophenol NPW MN
RCRP EPA 8270C 3,3'-Dichlorobenzidine NPW MN
RCRP EPA 8270C 3,3'-Dichlorobenzidine SCM MN
RCRP EPA 8270C 3-Methylphenol (m-Cresol) NPW MN
RCRP EPA 8270C 3-Methylphenol (m-Cresol) SCM MN
RCRP EPA 8270C 3-Nitroaniline SCM MN
RCRP EPA 8270C 3-Nitroaniline NPW MN
RCRP EPA 8270C 4-Bromophenyl phenyl ether NPW MN
RCRP EPA 8270C 4-Bromophenyl phenyl ether SCM MN
RCRP EPA 8270C 4-Chloro-3-methylphenol NPW MN
RCRP EPA 8270C 4-Chloro-3-methylphenol SCM MN
RCRP EPA 8270C 4-Chloroaniline NPW MN
RCRP EPA 8270C 4-Chloroaniline SCM MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 8270C 4-Chlorophenyl phenylether SCM MN
RCRP EPA 8270C 4-Chlorophenyl phenylether NPW MN
RCRP EPA 8270C 4-Methylphenol (p-Cresol) NPW MN
RCRP EPA 8270C 4-Methylphenol (p-Cresol) SCM MN
RCRP EPA 8270C 4-Nitroaniline SCM MN
RCRP EPA 8270C 4-Nitroaniline NPW MN
RCRP EPA 8270C 4-Nitrophenol NPW MN
RCRP EPA 8270C 4-Nitrophenol SCM MN
RCRP EPA 8270C Acenaphthene SCM MN
RCRP EPA 8270C Acenaphthene NPW MN
RCRP EPA 8270C Acenaphthylene SCM MN
RCRP EPA 8270C Acenaphthylene NPW MN
RCRP EPA 8270C Anthracene SCM MN
RCRP EPA 8270C Anthracene NPW MN
RCRP EPA 8270C Benzidine NPW MN
RCRP EPA 8270C Benzidine SCM MN
RCRP EPA 8270C Benzo(a)anthracene NPW MN
RCRP EPA 8270C Benzo(a)anthracene SCM MN
RCRP EPA 8270C Benzo(a)pyrene NPW MN
RCRP EPA 8270C Benzo(a)pyrene SCM MN
RCRP EPA 8270C Benzo(g,h,i)perylene SCM MN
RCRP EPA 8270C Benzo(g,h,i)perylene NPW MN
RCRP EPA 8270C Benzo(k)fluoranthene SCM MN
RCRP EPA 8270C Benzo(k)fluoranthene NPW MN
RCRP EPA 8270C Benzo[b]fluoranthene SCM MN
RCRP EPA 8270C Benzo[b]fluoranthene NPW MN
RCRP EPA 8270C Benzoic acid NPW MN
RCRP EPA 8270C Benzoic acid SCM MN
RCRP EPA 8270C Benzyl alcohol NPW MN
RCRP EPA 8270C Benzyl alcohol SCM MN
RCRP EPA 8270C bis(2-Chloroethoxy)methane SCM MN
RCRP EPA 8270C bis(2-Chloroethoxy)methane NPW MN
RCRP EPA 8270C bis(2-Chloroethyl) ether NPW MN
RCRP EPA 8270C bis(2-Chloroethyl) ether SCM MN
RCRP EPA 8270C bis(2-Chloroisopropyl) ether NPW MN
RCRP EPA 8270C bis(2-Chloroisopropyl) ether SCM MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 8270C Butyl benzyl phthalate SCM MN
RCRP EPA 8270C Butyl benzyl phthalate NPW MN
RCRP EPA 8270C Chrysene SCM MN
RCRP EPA 8270C Chrysene NPW MN
RCRP EPA 8270C Di(2-ethylhexyl) phthalate (bis(2-Ethylhexyl)phthalate, DEHP)
NPW MN
RCRP EPA 8270C Di(2-ethylhexyl) phthalate (bis(2-Ethylhexyl)phthalate, DEHP)
SCM MN
RCRP EPA 8270C Di-n-butyl phthalate NPW MN
RCRP EPA 8270C Di-n-butyl phthalate SCM MN
RCRP EPA 8270C Di-n-octyl phthalate SCM MN
RCRP EPA 8270C Di-n-octyl phthalate NPW MN
RCRP EPA 8270C Dibenz(a,h) anthracene SCM MN
RCRP EPA 8270C Dibenz(a,h) anthracene NPW MN
RCRP EPA 8270C Dibenzofuran NPW MN
RCRP EPA 8270C Dibenzofuran SCM MN
RCRP EPA 8270C Diethyl phthalate SCM MN
RCRP EPA 8270C Diethyl phthalate NPW MN
RCRP EPA 8270C Dimethyl phthalate SCM MN
RCRP EPA 8270C Dimethyl phthalate NPW MN
RCRP EPA 8270C Fluoranthene NPW MN
RCRP EPA 8270C Fluoranthene SCM MN
RCRP EPA 8270C Fluorene NPW MN
RCRP EPA 8270C Fluorene SCM MN
RCRP EPA 8270C Hexachlorobenzene NPW MN
RCRP EPA 8270C Hexachlorobenzene SCM MN
RCRP EPA 8270C Hexachlorobutadiene NPW MN
RCRP EPA 8270C Hexachlorobutadiene SCM MN
RCRP EPA 8270C Hexachlorocyclopentadiene SCM MN
RCRP EPA 8270C Hexachlorocyclopentadiene NPW MN
RCRP EPA 8270C Hexachloroethane NPW MN
RCRP EPA 8270C Hexachloroethane SCM MN
RCRP EPA 8270C Indeno(1,2,3-cd) pyrene NPW MN
RCRP EPA 8270C Indeno(1,2,3-cd) pyrene SCM MN
RCRP EPA 8270C Isophorone NPW MN
RCRP EPA 8270C Isophorone SCM MN
RCRP EPA 8270C n-Nitrosodi-n-propylamine SCM MN
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EPA 8270C SIM Preparation Techniques: Extraction, microwave; Extraction, ultrasonic; Extraction, soxhlet; Extraction, separatory funnel liquid-liquid
(LLE);
Program Method Analyte Matrix Primary SOP
RCRP EPA 8270C n-Nitrosodi-n-propylamine NPW MN
RCRP EPA 8270C n-Nitrosodimethylamine SCM MN
RCRP EPA 8270C n-Nitrosodimethylamine NPW MN
RCRP EPA 8270C n-Nitrosodiphenylamine SCM MN
RCRP EPA 8270C n-Nitrosodiphenylamine NPW MN
RCRP EPA 8270C Naphthalene SCM MN
RCRP EPA 8270C Naphthalene NPW MN
RCRP EPA 8270C Nitrobenzene SCM MN
RCRP EPA 8270C Nitrobenzene NPW MN
RCRP EPA 8270C Pentachlorophenol NPW MN
RCRP EPA 8270C Pentachlorophenol SCM MN
RCRP EPA 8270C Phenanthrene NPW MN
RCRP EPA 8270C Phenanthrene SCM MN
RCRP EPA 8270C Phenol SCM MN
RCRP EPA 8270C Phenol NPW MN
RCRP EPA 8270C Pyrene SCM MN
RCRP EPA 8270C Pyrene NPW MN
RCRP EPA 8270C Pyridine NPW MN
RCRP EPA 8270C Pyridine SCM MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 8270C SIM Benzo(a)anthracene NPW MN
RCRP EPA 8270C SIM Benzo(a)anthracene SCM MN
RCRP EPA 8270C SIM Benzo(a)pyrene NPW MN
RCRP EPA 8270C SIM Benzo(a)pyrene SCM MN
RCRP EPA 8270C SIM Benzo(j)fluoranthene SCM MN
RCRP EPA 8270C SIM Benzo(j)fluoranthene NPW MN
RCRP EPA 8270C SIM Benzo(k)fluoranthene NPW MN
RCRP EPA 8270C SIM Benzo(k)fluoranthene SCM MN
RCRP EPA 8270C SIM Benzo[b]fluoranthene SCM MN
RCRP EPA 8270C SIM Benzo[b]fluoranthene NPW MN
RCRP EPA 8270C SIM Dibenz(a,h) anthracene NPW MN
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EPA 8270D Preparation Techniques: Extraction, ultrasonic; Extraction, continuous liquid-liquid (LLE); Extraction, EPA 1311 TCLP, non-
volatiles; Extraction, soxhlet; Extraction, separatory funnel liquid-liquid (LLE); Extraction, EPA 1312 SPLP, non-volatiles;
Program Method Analyte Matrix Primary SOP
RCRP EPA 8270C SIM Dibenz(a,h) anthracene SCM MN
RCRP EPA 8270C SIM Fluoranthene SCM MN
RCRP EPA 8270C SIM Fluoranthene NPW MN
RCRP EPA 8270C SIM Indeno(1,2,3-cd) pyrene NPW MN
RCRP EPA 8270C SIM Indeno(1,2,3-cd) pyrene SCM MN
RCRP EPA 8270C SIM Pyrene SCM MN
RCRP EPA 8270C SIM Pyrene NPW MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 8270D 1,2,4-Trichlorobenzene SCM MN
RCRP EPA 8270D 1,2,4-Trichlorobenzene NPW MN
RCRP EPA 8270D 1,2-Dichlorobenzene SCM MN
RCRP EPA 8270D 1,2-Dichlorobenzene NPW MN
RCRP EPA 8270D 1,2-Diphenylhydrazine SCM MN
RCRP EPA 8270D 1,2-Diphenylhydrazine NPW MN
RCRP EPA 8270D 1,3-Dichlorobenzene SCM MN
RCRP EPA 8270D 1,3-Dichlorobenzene NPW MN
RCRP EPA 8270D 1,4-Dichlorobenzene NPW MN
RCRP EPA 8270D 1,4-Dichlorobenzene SCM MN
RCRP EPA 8270D 2,4,5-Trichlorophenol SCM MN
RCRP EPA 8270D 2,4,5-Trichlorophenol NPW MN
RCRP EPA 8270D 2,4,6-Trichlorophenol SCM MN
RCRP EPA 8270D 2,4,6-Trichlorophenol NPW MN
RCRP EPA 8270D 2,4-Dichlorophenol SCM MN
RCRP EPA 8270D 2,4-Dichlorophenol NPW MN
RCRP EPA 8270D 2,4-Dimethylphenol SCM MN
RCRP EPA 8270D 2,4-Dimethylphenol NPW MN
RCRP EPA 8270D 2,4-Dinitrophenol NPW MN
RCRP EPA 8270D 2,4-Dinitrophenol SCM MN
RCRP EPA 8270D 2,4-Dinitrotoluene (2,4-DNT) NPW MN
RCRP EPA 8270D 2,4-Dinitrotoluene (2,4-DNT) SCM MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 8270D 2,6-Dinitrotoluene (2,6-DNT) NPW MN
RCRP EPA 8270D 2,6-Dinitrotoluene (2,6-DNT) SCM MN
RCRP EPA 8270D 2-Chloronaphthalene SCM MN
RCRP EPA 8270D 2-Chloronaphthalene NPW MN
RCRP EPA 8270D 2-Chlorophenol SCM MN
RCRP EPA 8270D 2-Chlorophenol NPW MN
RCRP EPA 8270D 2-Methylnaphthalene SCM MN
RCRP EPA 8270D 2-Methylnaphthalene NPW MN
RCRP EPA 8270D 2-Methylphenol (o-Cresol) NPW MN
RCRP EPA 8270D 2-Methylphenol (o-Cresol) SCM MN
RCRP EPA 8270D 2-Nitroaniline NPW MN
RCRP EPA 8270D 2-Nitroaniline SCM MN
RCRP EPA 8270D 2-Nitrophenol NPW MN
RCRP EPA 8270D 2-Nitrophenol SCM MN
RCRP EPA 8270D 3,3'-Dichlorobenzidine SCM MN
RCRP EPA 8270D 3,3'-Dichlorobenzidine NPW MN
RCRP EPA 8270D 3-Methylcholanthrene NPW MN
RCRP EPA 8270D 3-Methylcholanthrene SCM MN
RCRP EPA 8270D 3-Methylphenol (m-Cresol) SCM MN
RCRP EPA 8270D 3-Methylphenol (m-Cresol) NPW MN
RCRP EPA 8270D 3-Nitroaniline NPW MN
RCRP EPA 8270D 3-Nitroaniline SCM MN
RCRP EPA 8270D 4,6-Dinitro-2-methylphenol NPW MN
RCRP EPA 8270D 4,6-Dinitro-2-methylphenol SCM MN
RCRP EPA 8270D 4-Bromophenyl phenyl ether NPW MN
RCRP EPA 8270D 4-Bromophenyl phenyl ether SCM MN
RCRP EPA 8270D 4-Chloro-3-methylphenol SCM MN
RCRP EPA 8270D 4-Chloro-3-methylphenol NPW MN
RCRP EPA 8270D 4-Chloroaniline SCM MN
RCRP EPA 8270D 4-Chloroaniline NPW MN
RCRP EPA 8270D 4-Chlorophenyl phenylether NPW MN
RCRP EPA 8270D 4-Chlorophenyl phenylether SCM MN
RCRP EPA 8270D 4-Methylphenol (p-Cresol) SCM MN
RCRP EPA 8270D 4-Methylphenol (p-Cresol) NPW MN
RCRP EPA 8270D 4-Nitroaniline SCM MN
RCRP EPA 8270D 4-Nitroaniline NPW MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 8270D 4-Nitrophenol SCM MN
RCRP EPA 8270D 4-Nitrophenol NPW MN
RCRP EPA 8270D Acenaphthene SCM MN
RCRP EPA 8270D Acenaphthene NPW MN
RCRP EPA 8270D Acenaphthylene SCM MN
RCRP EPA 8270D Acenaphthylene NPW MN
RCRP EPA 8270D Anthracene NPW MN
RCRP EPA 8270D Anthracene SCM MN
RCRP EPA 8270D Benzidine NPW MN
RCRP EPA 8270D Benzidine SCM MN
RCRP EPA 8270D Benzo(a)anthracene NPW MN
RCRP EPA 8270D Benzo(a)anthracene SCM MN
RCRP EPA 8270D Benzo(a)pyrene NPW MN
RCRP EPA 8270D Benzo(a)pyrene SCM MN
RCRP EPA 8270D Benzo(g,h,i)perylene SCM MN
RCRP EPA 8270D Benzo(g,h,i)perylene NPW MN
RCRP EPA 8270D Benzo(k)fluoranthene SCM MN
RCRP EPA 8270D Benzo(k)fluoranthene NPW MN
RCRP EPA 8270D Benzo[b]fluoranthene NPW MN
RCRP EPA 8270D Benzo[b]fluoranthene SCM MN
RCRP EPA 8270D Benzoic acid SCM MN
RCRP EPA 8270D Benzoic acid NPW MN
RCRP EPA 8270D Benzyl alcohol NPW MN
RCRP EPA 8270D Benzyl alcohol SCM MN
RCRP EPA 8270D bis(2-Chloroethoxy)methane NPW MN
RCRP EPA 8270D bis(2-Chloroethoxy)methane SCM MN
RCRP EPA 8270D bis(2-Chloroethyl) ether SCM MN
RCRP EPA 8270D bis(2-Chloroethyl) ether NPW MN
RCRP EPA 8270D bis(2-Chloroisopropyl) ether SCM MN
RCRP EPA 8270D bis(2-Chloroisopropyl) ether NPW MN
RCRP EPA 8270D Butyl benzyl phthalate NPW MN
RCRP EPA 8270D Butyl benzyl phthalate SCM MN
RCRP EPA 8270D Carbazole SCM MN
RCRP EPA 8270D Carbazole NPW MN
RCRP EPA 8270D Chrysene SCM MN
RCRP EPA 8270D Chrysene NPW MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 8270D Di(2-ethylhexyl) phthalate (bis(2-Ethylhexyl)phthalate, DEHP)
NPW MN
RCRP EPA 8270D Di(2-ethylhexyl) phthalate (bis(2-Ethylhexyl)phthalate, DEHP)
SCM MN
RCRP EPA 8270D Di-n-butyl phthalate SCM MN
RCRP EPA 8270D Di-n-butyl phthalate NPW MN
RCRP EPA 8270D Di-n-octyl phthalate NPW MN
RCRP EPA 8270D Di-n-octyl phthalate SCM MN
RCRP EPA 8270D Dibenz(a,h) anthracene SCM MN
RCRP EPA 8270D Dibenz(a,h) anthracene NPW MN
RCRP EPA 8270D Dibenzofuran SCM MN
RCRP EPA 8270D Dibenzofuran NPW MN
RCRP EPA 8270D Diethyl phthalate SCM MN
RCRP EPA 8270D Diethyl phthalate NPW MN
RCRP EPA 8270D Dimethyl phthalate SCM MN
RCRP EPA 8270D Dimethyl phthalate NPW MN
RCRP EPA 8270D Fluoranthene NPW MN
RCRP EPA 8270D Fluoranthene SCM MN
RCRP EPA 8270D Fluorene SCM MN
RCRP EPA 8270D Fluorene NPW MN
RCRP EPA 8270D Hexachlorobenzene NPW MN
RCRP EPA 8270D Hexachlorobenzene SCM MN
RCRP EPA 8270D Hexachlorobutadiene SCM MN
RCRP EPA 8270D Hexachlorobutadiene NPW MN
RCRP EPA 8270D Hexachlorocyclopentadiene SCM MN
RCRP EPA 8270D Hexachlorocyclopentadiene NPW MN
RCRP EPA 8270D Hexachloroethane SCM MN
RCRP EPA 8270D Hexachloroethane NPW MN
RCRP EPA 8270D Indeno(1,2,3-cd) pyrene NPW MN
RCRP EPA 8270D Indeno(1,2,3-cd) pyrene SCM MN
RCRP EPA 8270D Isophorone SCM MN
RCRP EPA 8270D Isophorone NPW MN
RCRP EPA 8270D n-Nitrosodi-n-propylamine SCM MN
RCRP EPA 8270D n-Nitrosodi-n-propylamine NPW MN
RCRP EPA 8270D n-Nitrosodimethylamine NPW MN
RCRP EPA 8270D n-Nitrosodimethylamine SCM MN
RCRP EPA 8270D n-Nitrosodiphenylamine SCM MN
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EPA 8270D SIM Preparation Techniques: Extraction, microwave; Extraction, ultrasonic; Extraction, soxhlet; Extraction, separatory funnel liquid-liquid
(LLE);
Program Method Analyte Matrix Primary SOP
RCRP EPA 8270D n-Nitrosodiphenylamine NPW MN
RCRP EPA 8270D Naphthalene NPW MN
RCRP EPA 8270D Naphthalene SCM MN
RCRP EPA 8270D Nitrobenzene NPW MN
RCRP EPA 8270D Nitrobenzene SCM MN
RCRP EPA 8270D Pentachlorophenol NPW MN
RCRP EPA 8270D Pentachlorophenol SCM MN
RCRP EPA 8270D Phenanthrene NPW MN
RCRP EPA 8270D Phenanthrene SCM MN
RCRP EPA 8270D Phenol NPW MN
RCRP EPA 8270D Phenol SCM MN
RCRP EPA 8270D Pyrene NPW MN
RCRP EPA 8270D Pyrene SCM MN
RCRP EPA 8270D Pyridine SCM MN
RCRP EPA 8270D Pyridine NPW MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 8270D SIM 1-Methylnaphthalene SCM MN
RCRP EPA 8270D SIM 1-Methylnaphthalene NPW MN
RCRP EPA 8270D SIM 2-Chloronaphthalene NPW MN
RCRP EPA 8270D SIM 2-Chloronaphthalene SCM MN
RCRP EPA 8270D SIM 2-Methylnaphthalene SCM MN
RCRP EPA 8270D SIM 2-Methylnaphthalene NPW MN
RCRP EPA 8270D SIM Acenaphthene SCM MN
RCRP EPA 8270D SIM Acenaphthene NPW MN
RCRP EPA 8270D SIM Acenaphthylene SCM MN
RCRP EPA 8270D SIM Acenaphthylene NPW MN
RCRP EPA 8270D SIM Anthracene SCM MN
RCRP EPA 8270D SIM Anthracene NPW MN
RCRP EPA 8270D SIM Benzo(a)anthracene NPW MN
RCRP EPA 8270D SIM Benzo(a)anthracene SCM MN
RCRP EPA 8270D SIM Benzo(a)pyrene SCM MN
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EPA 8280B Preparation Techniques: Extraction, separatory funnel liquid-liquid (LLE);
Program Method Analyte Matrix Primary SOP
RCRP EPA 8270D SIM Benzo(a)pyrene NPW MN
RCRP EPA 8270D SIM Benzo(g,h,i)perylene SCM MN
RCRP EPA 8270D SIM Benzo(g,h,i)perylene NPW MN
RCRP EPA 8270D SIM Benzo(k)fluoranthene SCM MN
RCRP EPA 8270D SIM Benzo(k)fluoranthene NPW MN
RCRP EPA 8270D SIM Benzo[b]fluoranthene SCM MN
RCRP EPA 8270D SIM Benzo[b]fluoranthene NPW MN
RCRP EPA 8270D SIM Chrysene SCM MN
RCRP EPA 8270D SIM Chrysene NPW MN
RCRP EPA 8270D SIM Dibenz(a,h) anthracene SCM MN
RCRP EPA 8270D SIM Dibenz(a,h) anthracene NPW MN
RCRP EPA 8270D SIM Dibenzofuran NPW MN
RCRP EPA 8270D SIM Dibenzofuran SCM MN
RCRP EPA 8270D SIM Fluoranthene NPW MN
RCRP EPA 8270D SIM Fluoranthene SCM MN
RCRP EPA 8270D SIM Fluorene NPW MN
RCRP EPA 8270D SIM Fluorene SCM MN
RCRP EPA 8270D SIM Indeno(1,2,3-cd) pyrene SCM MN
RCRP EPA 8270D SIM Indeno(1,2,3-cd) pyrene NPW MN
RCRP EPA 8270D SIM Naphthalene SCM MN
RCRP EPA 8270D SIM Naphthalene NPW MN
RCRP EPA 8270D SIM Phenanthrene NPW MN
RCRP EPA 8270D SIM Phenanthrene SCM MN
RCRP EPA 8270D SIM Pyrene SCM MN
RCRP EPA 8270D SIM Pyrene NPW MN
RCRP EPA 8270D SIM Quinoline SCM MN
RCRP EPA 8270D SIM Quinoline NPW MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 8280B 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)
NPW MN
RCRP EPA 8280B 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)
SCM MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 8280B 1,2,3,4,6,7,8,9-Octachlorodibenzofuran(OCDF)
NPW MN
RCRP EPA 8280B 1,2,3,4,6,7,8,9-Octachlorodibenzofuran(OCDF)
SCM MN
RCRP EPA 8280B 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)
NPW MN
RCRP EPA 8280B 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)
SCM MN
RCRP EPA 8280B 1,2,3,4,6,7,8-Heptachlorodibenzofuran(1,2,3,4,6,7,8-hpcdf)
SCM MN
RCRP EPA 8280B 1,2,3,4,6,7,8-Heptachlorodibenzofuran(1,2,3,4,6,7,8-hpcdf)
NPW MN
RCRP EPA 8280B 1,2,3,4,7,8,9-Heptachlorodibenzofuran(1,2,3,4,7,8,9-hpcdf)
SCM MN
RCRP EPA 8280B 1,2,3,4,7,8,9-Heptachlorodibenzofuran(1,2,3,4,7,8,9-hpcdf)
NPW MN
RCRP EPA 8280B 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,4,7,8-Hxcdd)
SCM MN
RCRP EPA 8280B 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,4,7,8-Hxcdd)
NPW MN
RCRP EPA 8280B 1,2,3,4,7,8-Hexachlorodibenzofuran(1,2,3,4,7,8-Hxcdf)
NPW MN
RCRP EPA 8280B 1,2,3,4,7,8-Hexachlorodibenzofuran(1,2,3,4,7,8-Hxcdf)
SCM MN
RCRP EPA 8280B 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,6,7,8-Hxcdd)
SCM MN
RCRP EPA 8280B 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,6,7,8-Hxcdd)
NPW MN
RCRP EPA 8280B 1,2,3,6,7,8-Hexachlorodibenzofuran(1,2,3,6,7,8-Hxcdf)
SCM MN
RCRP EPA 8280B 1,2,3,6,7,8-Hexachlorodibenzofuran(1,2,3,6,7,8-Hxcdf)
NPW MN
RCRP EPA 8280B 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin(1,2,3,7,8,9-Hxcdd)
NPW MN
RCRP EPA 8280B 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin(1,2,3,7,8,9-Hxcdd)
SCM MN
RCRP EPA 8280B 1,2,3,7,8,9-Hexachlorodibenzofuran(1,2,3,7,8,9-Hxcdf)
NPW MN
RCRP EPA 8280B 1,2,3,7,8,9-Hexachlorodibenzofuran(1,2,3,7,8,9-Hxcdf)
SCM MN
RCRP EPA 8280B 1,2,3,7,8-Pentachlorodibenzo-p-dioxin(1,2,3,7,8-Pecdd)
SCM MN
RCRP EPA 8280B 1,2,3,7,8-Pentachlorodibenzo-p-dioxin(1,2,3,7,8-Pecdd)
NPW MN
RCRP EPA 8280B 1,2,3,7,8-Pentachlorodibenzofuran(1,2,3,7,8-Pecdf)
NPW MN
RCRP EPA 8280B 1,2,3,7,8-Pentachlorodibenzofuran(1,2,3,7,8-Pecdf)
SCM MN
RCRP EPA 8280B 2,3,4,6,7,8-Hexachlorodibenzofuran SCM MN
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EPA 8290 Preparation Techniques: Extraction, soxhlet; Extraction, separatory funnel liquid-liquid (LLE);
Program Method Analyte Matrix Primary SOP
RCRP EPA 8280B 2,3,4,6,7,8-Hexachlorodibenzofuran NPW MN
RCRP EPA 8280B 2,3,4,7,8-Pentachlorodibenzofuran NPW MN
RCRP EPA 8280B 2,3,4,7,8-Pentachlorodibenzofuran SCM MN
RCRP EPA 8280B 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)
SCM MN
RCRP EPA 8280B 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)
NPW MN
RCRP EPA 8280B 2,3,7,8-Tetrachlorodibenzofuran SCM MN
RCRP EPA 8280B 2,3,7,8-Tetrachlorodibenzofuran NPW MN
RCRP EPA 8280B Total HpCDD NPW MN
RCRP EPA 8280B Total HpCDD SCM MN
RCRP EPA 8280B Total HpCDF SCM MN
RCRP EPA 8280B Total HpCDF NPW MN
RCRP EPA 8280B Total HxCDD SCM MN
RCRP EPA 8280B Total HxCDD NPW MN
RCRP EPA 8280B Total HxCDF SCM MN
RCRP EPA 8280B Total HxCDF NPW MN
RCRP EPA 8280B Total PeCDD NPW MN
RCRP EPA 8280B Total PeCDD SCM MN
RCRP EPA 8280B Total PeCDF SCM MN
RCRP EPA 8280B Total PeCDF NPW MN
RCRP EPA 8280B Total TCDD NPW MN
RCRP EPA 8280B Total TCDD SCM MN
RCRP EPA 8280B Total TCDF SCM MN
RCRP EPA 8280B Total TCDF NPW MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 8290 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)
NPW MN
RCRP EPA 8290 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)
TISSUE MN
RCRP EPA 8290 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)
SCM MN
RCRP EPA 8290 1,2,3,4,6,7,8,9-Octachlorodibenzofuran(OCDF)
TISSUE MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 8290 1,2,3,4,6,7,8,9-Octachlorodibenzofuran(OCDF)
SCM MN
RCRP EPA 8290 1,2,3,4,6,7,8,9-Octachlorodibenzofuran(OCDF)
NPW MN
RCRP EPA 8290 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)
SCM MN
RCRP EPA 8290 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)
NPW MN
RCRP EPA 8290 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)
TISSUE MN
RCRP EPA 8290 1,2,3,4,6,7,8-Heptachlorodibenzofuran(1,2,3,4,6,7,8-hpcdf)
NPW MN
RCRP EPA 8290 1,2,3,4,6,7,8-Heptachlorodibenzofuran(1,2,3,4,6,7,8-hpcdf)
TISSUE MN
RCRP EPA 8290 1,2,3,4,6,7,8-Heptachlorodibenzofuran(1,2,3,4,6,7,8-hpcdf)
SCM MN
RCRP EPA 8290 1,2,3,4,7,8,9-Heptachlorodibenzofuran(1,2,3,4,7,8,9-hpcdf)
NPW MN
RCRP EPA 8290 1,2,3,4,7,8,9-Heptachlorodibenzofuran(1,2,3,4,7,8,9-hpcdf)
SCM MN
RCRP EPA 8290 1,2,3,4,7,8,9-Heptachlorodibenzofuran(1,2,3,4,7,8,9-hpcdf)
TISSUE MN
RCRP EPA 8290 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,4,7,8-Hxcdd)
TISSUE MN
RCRP EPA 8290 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,4,7,8-Hxcdd)
NPW MN
RCRP EPA 8290 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,4,7,8-Hxcdd)
SCM MN
RCRP EPA 8290 1,2,3,4,7,8-Hexachlorodibenzofuran(1,2,3,4,7,8-Hxcdf)
SCM MN
RCRP EPA 8290 1,2,3,4,7,8-Hexachlorodibenzofuran(1,2,3,4,7,8-Hxcdf)
NPW MN
RCRP EPA 8290 1,2,3,4,7,8-Hexachlorodibenzofuran(1,2,3,4,7,8-Hxcdf)
TISSUE MN
RCRP EPA 8290 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,6,7,8-Hxcdd)
SCM MN
RCRP EPA 8290 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,6,7,8-Hxcdd)
TISSUE MN
RCRP EPA 8290 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,6,7,8-Hxcdd)
NPW MN
RCRP EPA 8290 1,2,3,6,7,8-Hexachlorodibenzofuran(1,2,3,6,7,8-Hxcdf)
TISSUE MN
RCRP EPA 8290 1,2,3,6,7,8-Hexachlorodibenzofuran(1,2,3,6,7,8-Hxcdf)
NPW MN
RCRP EPA 8290 1,2,3,6,7,8-Hexachlorodibenzofuran(1,2,3,6,7,8-Hxcdf)
SCM MN
RCRP EPA 8290 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin(1,2,3,7,8,9-Hxcdd)
NPW MN
RCRP EPA 8290 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin(1,2,3,7,8,9-Hxcdd)
TISSUE MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 8290 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin(1,2,3,7,8,9-Hxcdd)
SCM MN
RCRP EPA 8290 1,2,3,7,8,9-Hexachlorodibenzofuran(1,2,3,7,8,9-Hxcdf)
SCM MN
RCRP EPA 8290 1,2,3,7,8,9-Hexachlorodibenzofuran(1,2,3,7,8,9-Hxcdf)
TISSUE MN
RCRP EPA 8290 1,2,3,7,8,9-Hexachlorodibenzofuran(1,2,3,7,8,9-Hxcdf)
NPW MN
RCRP EPA 8290 1,2,3,7,8-Pentachlorodibenzo-p-dioxin(1,2,3,7,8-Pecdd)
NPW MN
RCRP EPA 8290 1,2,3,7,8-Pentachlorodibenzo-p-dioxin(1,2,3,7,8-Pecdd)
SCM MN
RCRP EPA 8290 1,2,3,7,8-Pentachlorodibenzo-p-dioxin(1,2,3,7,8-Pecdd)
TISSUE MN
RCRP EPA 8290 1,2,3,7,8-Pentachlorodibenzofuran(1,2,3,7,8-Pecdf)
SCM MN
RCRP EPA 8290 1,2,3,7,8-Pentachlorodibenzofuran(1,2,3,7,8-Pecdf)
TISSUE MN
RCRP EPA 8290 1,2,3,7,8-Pentachlorodibenzofuran(1,2,3,7,8-Pecdf)
NPW MN
RCRP EPA 8290 2,3,4,6,7,8-Hexachlorodibenzofuran NPW MN
RCRP EPA 8290 2,3,4,6,7,8-Hexachlorodibenzofuran TISSUE MN
RCRP EPA 8290 2,3,4,6,7,8-Hexachlorodibenzofuran SCM MN
RCRP EPA 8290 2,3,4,7,8-Pentachlorodibenzofuran TISSUE MN
RCRP EPA 8290 2,3,4,7,8-Pentachlorodibenzofuran NPW MN
RCRP EPA 8290 2,3,4,7,8-Pentachlorodibenzofuran SCM MN
RCRP EPA 8290 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)
SCM MN
RCRP EPA 8290 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)
NPW MN
RCRP EPA 8290 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)
TISSUE MN
RCRP EPA 8290 2,3,7,8-Tetrachlorodibenzofuran SCM MN
RCRP EPA 8290 2,3,7,8-Tetrachlorodibenzofuran NPW MN
RCRP EPA 8290 2,3,7,8-Tetrachlorodibenzofuran TISSUE MN
RCRP EPA 8290 Total Heptachlorodibenzo-p-dioxin (HpCDD, Total)
TISSUE MN
RCRP EPA 8290 Total Heptachlorodibenzofuran (HpCDF,Total)
TISSUE MN
RCRP EPA 8290 Total Hexachlorodibenzo-p-dioxin (HxCDD, Total)
TISSUE MN
RCRP EPA 8290 Total Hexachlorodibenzofuran (HxCDF,Total)
TISSUE MN
RCRP EPA 8290 Total Hpcdd NPW MN
RCRP EPA 8290 Total Hpcdd SCM MN
RCRP EPA 8290 Total Hpcdf NPW MN
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EPA 8290A Preparation Techniques: Extraction, soxhlet; Extraction, separatory funnel liquid-liquid (LLE);
Program Method Analyte Matrix Primary SOP
RCRP EPA 8290 Total Hpcdf SCM MN
RCRP EPA 8290 Total Hxcdd NPW MN
RCRP EPA 8290 Total Hxcdd SCM MN
RCRP EPA 8290 Total Hxcdf SCM MN
RCRP EPA 8290 Total Hxcdf NPW MN
RCRP EPA 8290 Total Pecdd SCM MN
RCRP EPA 8290 Total Pecdd NPW MN
RCRP EPA 8290 Total Pecdf SCM MN
RCRP EPA 8290 Total Pecdf NPW MN
RCRP EPA 8290 Total Pentachlorodibenzo-p-dioxin(PeCDD, Total)
TISSUE MN
RCRP EPA 8290 Total Pentachlorodibenzofuran (PeCDF,Total)
TISSUE MN
RCRP EPA 8290 Total TCDD SCM MN
RCRP EPA 8290 Total TCDD NPW MN
RCRP EPA 8290 Total TCDF SCM MN
RCRP EPA 8290 Total TCDF NPW MN
RCRP EPA 8290 Total Tetrachlorodibenzo-p-dioxin (TCDD, Total)
TISSUE MN
RCRP EPA 8290 Total Tetrachlorodibenzofuran (TCDF,Total)
TISSUE MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 8290A 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)
SCM MN
RCRP EPA 8290A 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)
TISSUE MN
RCRP EPA 8290A 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)
NPW MN
RCRP EPA 8290A 1,2,3,4,6,7,8,9-Octachlorodibenzofuran(OCDF)
NPW MN
RCRP EPA 8290A 1,2,3,4,6,7,8,9-Octachlorodibenzofuran(OCDF)
SCM MN
RCRP EPA 8290A 1,2,3,4,6,7,8,9-Octachlorodibenzofuran(OCDF)
TISSUE MN
RCRP EPA 8290A 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)
TISSUE MN
RCRP EPA 8290A 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)
NPW MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 8290A 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)
SCM MN
RCRP EPA 8290A 1,2,3,4,6,7,8-Heptachlorodibenzofuran(1,2,3,4,6,7,8-hpcdf)
TISSUE MN
RCRP EPA 8290A 1,2,3,4,6,7,8-Heptachlorodibenzofuran(1,2,3,4,6,7,8-hpcdf)
NPW MN
RCRP EPA 8290A 1,2,3,4,6,7,8-Heptachlorodibenzofuran(1,2,3,4,6,7,8-hpcdf)
SCM MN
RCRP EPA 8290A 1,2,3,4,7,8,9-Heptachlorodibenzofuran(1,2,3,4,7,8,9-hpcdf)
NPW MN
RCRP EPA 8290A 1,2,3,4,7,8,9-Heptachlorodibenzofuran(1,2,3,4,7,8,9-hpcdf)
SCM MN
RCRP EPA 8290A 1,2,3,4,7,8,9-Heptachlorodibenzofuran(1,2,3,4,7,8,9-hpcdf)
TISSUE MN
RCRP EPA 8290A 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,4,7,8-Hxcdd)
NPW MN
RCRP EPA 8290A 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,4,7,8-Hxcdd)
SCM MN
RCRP EPA 8290A 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,4,7,8-Hxcdd)
TISSUE MN
RCRP EPA 8290A 1,2,3,4,7,8-Hexachlorodibenzofuran(1,2,3,4,7,8-Hxcdf)
TISSUE MN
RCRP EPA 8290A 1,2,3,4,7,8-Hexachlorodibenzofuran(1,2,3,4,7,8-Hxcdf)
SCM MN
RCRP EPA 8290A 1,2,3,4,7,8-Hexachlorodibenzofuran(1,2,3,4,7,8-Hxcdf)
NPW MN
RCRP EPA 8290A 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,6,7,8-Hxcdd)
NPW MN
RCRP EPA 8290A 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,6,7,8-Hxcdd)
SCM MN
RCRP EPA 8290A 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,6,7,8-Hxcdd)
TISSUE MN
RCRP EPA 8290A 1,2,3,6,7,8-Hexachlorodibenzofuran(1,2,3,6,7,8-Hxcdf)
TISSUE MN
RCRP EPA 8290A 1,2,3,6,7,8-Hexachlorodibenzofuran(1,2,3,6,7,8-Hxcdf)
NPW MN
RCRP EPA 8290A 1,2,3,6,7,8-Hexachlorodibenzofuran(1,2,3,6,7,8-Hxcdf)
SCM MN
RCRP EPA 8290A 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin(1,2,3,7,8,9-Hxcdd)
TISSUE MN
RCRP EPA 8290A 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin(1,2,3,7,8,9-Hxcdd)
SCM MN
RCRP EPA 8290A 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin(1,2,3,7,8,9-Hxcdd)
NPW MN
RCRP EPA 8290A 1,2,3,7,8,9-Hexachlorodibenzofuran(1,2,3,7,8,9-Hxcdf)
TISSUE MN
RCRP EPA 8290A 1,2,3,7,8,9-Hexachlorodibenzofuran(1,2,3,7,8,9-Hxcdf)
NPW MN
RCRP EPA 8290A 1,2,3,7,8,9-Hexachlorodibenzofuran(1,2,3,7,8,9-Hxcdf)
SCM MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 8290A 1,2,3,7,8-Pentachlorodibenzo-p-dioxin(1,2,3,7,8-Pecdd)
TISSUE MN
RCRP EPA 8290A 1,2,3,7,8-Pentachlorodibenzo-p-dioxin(1,2,3,7,8-Pecdd)
NPW MN
RCRP EPA 8290A 1,2,3,7,8-Pentachlorodibenzo-p-dioxin(1,2,3,7,8-Pecdd)
SCM MN
RCRP EPA 8290A 1,2,3,7,8-Pentachlorodibenzofuran(1,2,3,7,8-Pecdf)
NPW MN
RCRP EPA 8290A 1,2,3,7,8-Pentachlorodibenzofuran(1,2,3,7,8-Pecdf)
SCM MN
RCRP EPA 8290A 1,2,3,7,8-Pentachlorodibenzofuran(1,2,3,7,8-Pecdf)
TISSUE MN
RCRP EPA 8290A 2,3,4,6,7,8-Hexachlorodibenzofuran NPW MN
RCRP EPA 8290A 2,3,4,6,7,8-Hexachlorodibenzofuran SCM MN
RCRP EPA 8290A 2,3,4,6,7,8-Hexachlorodibenzofuran TISSUE MN
RCRP EPA 8290A 2,3,4,7,8-Pentachlorodibenzofuran NPW MN
RCRP EPA 8290A 2,3,4,7,8-Pentachlorodibenzofuran SCM MN
RCRP EPA 8290A 2,3,4,7,8-Pentachlorodibenzofuran TISSUE MN
RCRP EPA 8290A 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)
SCM MN
RCRP EPA 8290A 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)
TISSUE MN
RCRP EPA 8290A 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)
NPW MN
RCRP EPA 8290A 2,3,7,8-Tetrachlorodibenzofuran SCM MN
RCRP EPA 8290A 2,3,7,8-Tetrachlorodibenzofuran NPW MN
RCRP EPA 8290A 2,3,7,8-Tetrachlorodibenzofuran TISSUE MN
RCRP EPA 8290A Total Heptachlorodibenzo-p-dioxin (HpCDD, Total)
NPW MN
RCRP EPA 8290A Total Heptachlorodibenzo-p-dioxin (HpCDD, Total)
SCM MN
RCRP EPA 8290A Total Heptachlorodibenzofuran (HpCDF,Total)
SCM MN
RCRP EPA 8290A Total Heptachlorodibenzofuran (HpCDF,Total)
NPW MN
RCRP EPA 8290A Total Hexachlorodibenzo-p-dioxin (HxCDD, Total)
NPW MN
RCRP EPA 8290A Total Hexachlorodibenzo-p-dioxin (HxCDD, Total)
SCM MN
RCRP EPA 8290A Total Hexachlorodibenzofuran (HxCDF,Total)
NPW MN
RCRP EPA 8290A Total Hexachlorodibenzofuran (HxCDF,Total)
SCM MN
RCRP EPA 8290A Total HpCDD TISSUE MN
RCRP EPA 8290A Total HpCDF TISSUE MN
RCRP EPA 8290A Total HxCDD TISSUE MN
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EPA 9095B Preparation Techniques: N/A
EPA 8015B Preparation Techniques: Extraction, ultrasonic; Extraction, separatory funnel liquid-liquid (LLE); Purge and trap;
EPA 8015C
Program Method Analyte Matrix Primary SOP
RCRP EPA 8290A Total HxCDF TISSUE MN
RCRP EPA 8290A Total PeCDD TISSUE MN
RCRP EPA 8290A Total PeCDF TISSUE MN
RCRP EPA 8290A Total Pentachlorodibenzo-p-dioxin(PeCDD, Total)
SCM MN
RCRP EPA 8290A Total Pentachlorodibenzo-p-dioxin(PeCDD, Total)
NPW MN
RCRP EPA 8290A Total Pentachlorodibenzofuran (PeCDF,Total)
NPW MN
RCRP EPA 8290A Total Pentachlorodibenzofuran (PeCDF,Total)
SCM MN
RCRP EPA 8290A Total TCDD TISSUE MN
RCRP EPA 8290A Total TCDF TISSUE MN
RCRP EPA 8290A Total Tetrachlorodibenzo-p-dioxin (TCDD, Total)
NPW MN
RCRP EPA 8290A Total Tetrachlorodibenzo-p-dioxin (TCDD, Total)
SCM MN
RCRP EPA 8290A Total Tetrachlorodibenzofuran (TCDF,Total)
NPW MN
RCRP EPA 8290A Total Tetrachlorodibenzofuran (TCDF,Total)
SCM MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 9095B Paint Filter Liquids Test SCM MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 8015B Diesel range organics (DRO) NPW MN
RCRP EPA 8015B Diesel range organics (DRO) SCM MN
RCRP EPA 8015B Gasoline range organics (GRO) SCM MN
RCRP EPA 8015B Gasoline range organics (GRO) NPW MN
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Preparation Techniques: Extraction, ultrasonic; Extraction, separatory funnel liquid-liquid (LLE); Purge and trap;
EPA 8021B Preparation Techniques: Purge and trap;
EPA 8260B Preparation Techniques: Extraction, EPA 1312 SPLP, zero headspace (ZHE); Extraction, EPA 1311 TCLP, zero headspace (ZHE);
Purge and trap;
Program Method Analyte Matrix Primary SOP
RCRP EPA 8015C Diesel range organics (DRO) NPW MN
RCRP EPA 8015C Diesel range organics (DRO) SCM MN
RCRP EPA 8015C Gasoline range organics (GRO) SCM MN
RCRP EPA 8015C Gasoline range organics (GRO) NPW MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 8021B 1,2,4-Trimethylbenzene NPW MN
RCRP EPA 8021B 1,2,4-Trimethylbenzene SCM MN
RCRP EPA 8021B 1,3,5-Trimethylbenzene SCM MN
RCRP EPA 8021B 1,3,5-Trimethylbenzene NPW MN
RCRP EPA 8021B Benzene SCM MN
RCRP EPA 8021B Benzene NPW MN
RCRP EPA 8021B Ethylbenzene NPW MN
RCRP EPA 8021B Ethylbenzene SCM MN
RCRP EPA 8021B m+p-xylene SCM MN
RCRP EPA 8021B m+p-xylene NPW MN
RCRP EPA 8021B Methyl tert-butyl ether (MTBE) NPW MN
RCRP EPA 8021B Methyl tert-butyl ether (MTBE) SCM MN
RCRP EPA 8021B o-Xylene SCM MN
RCRP EPA 8021B o-Xylene NPW MN
RCRP EPA 8021B Toluene SCM MN
RCRP EPA 8021B Toluene NPW MN
Program Method Analyte Matrix Primary SOP
RCRP EPA 8260B 1,1,1,2-Tetrachloroethane NPW MN
RCRP EPA 8260B 1,1,1,2-Tetrachloroethane SCM MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 8260B 1,1,1-Trichloroethane SCM MN
RCRP EPA 8260B 1,1,1-Trichloroethane NPW MN
RCRP EPA 8260B 1,1,2,2-Tetrachloroethane SCM MN
RCRP EPA 8260B 1,1,2,2-Tetrachloroethane NPW MN
RCRP EPA 8260B 1,1,2-Trichloro-1,2,2-trifluoroethane(Freon 113)
SCM MN
RCRP EPA 8260B 1,1,2-Trichloroethane SCM MN
RCRP EPA 8260B 1,1,2-Trichloroethane NPW MN
RCRP EPA 8260B 1,1-Dichloroethane SCM MN
RCRP EPA 8260B 1,1-Dichloroethane NPW MN
RCRP EPA 8260B 1,1-Dichloroethylene NPW MN
RCRP EPA 8260B 1,1-Dichloroethylene SCM MN
RCRP EPA 8260B 1,1-Dichloropropene NPW MN
RCRP EPA 8260B 1,1-Dichloropropene SCM MN
RCRP EPA 8260B 1,2,3-Trichlorobenzene NPW MN
RCRP EPA 8260B 1,2,3-Trichlorobenzene SCM MN
RCRP EPA 8260B 1,2,3-Trichloropropane NPW MN
RCRP EPA 8260B 1,2,3-Trichloropropane SCM MN
RCRP EPA 8260B 1,2,4-Trichlorobenzene NPW MN
RCRP EPA 8260B 1,2,4-Trichlorobenzene SCM MN
RCRP EPA 8260B 1,2,4-Trimethylbenzene SCM MN
RCRP EPA 8260B 1,2,4-Trimethylbenzene NPW MN
RCRP EPA 8260B 1,2-Dibromo-3-chloropropane (DBCP) SCM MN
RCRP EPA 8260B 1,2-Dibromo-3-chloropropane (DBCP) NPW MN
RCRP EPA 8260B 1,2-Dibromoethane (EDB, Ethylenedibromide)
NPW MN
RCRP EPA 8260B 1,2-Dibromoethane (EDB, Ethylenedibromide)
SCM MN
RCRP EPA 8260B 1,2-Dichlorobenzene NPW MN
RCRP EPA 8260B 1,2-Dichlorobenzene SCM MN
RCRP EPA 8260B 1,2-Dichloroethane (Ethylene dichloride) NPW MN
RCRP EPA 8260B 1,2-Dichloroethane (Ethylene dichloride) SCM MN
RCRP EPA 8260B 1,2-Dichloropropane SCM MN
RCRP EPA 8260B 1,2-Dichloropropane NPW MN
RCRP EPA 8260B 1,3,5-Trimethylbenzene NPW MN
RCRP EPA 8260B 1,3,5-Trimethylbenzene SCM MN
RCRP EPA 8260B 1,3-Dichlorobenzene SCM MN
RCRP EPA 8260B 1,3-Dichlorobenzene NPW MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 8260B 1,3-Dichloropropane SCM MN
RCRP EPA 8260B 1,3-Dichloropropane NPW MN
RCRP EPA 8260B 1,4-Dichlorobenzene SCM MN
RCRP EPA 8260B 1,4-Dichlorobenzene NPW MN
RCRP EPA 8260B 1,4-Dioxane (1,4- Diethyleneoxide) SCM MN
RCRP EPA 8260B 1,4-Dioxane (1,4- Diethyleneoxide) NPW MN
RCRP EPA 8260B 2,2-Dichloropropane SCM MN
RCRP EPA 8260B 2,2-Dichloropropane NPW MN
RCRP EPA 8260B 2-Butanone (Methyl ethyl ketone, MEK) NPW MN
RCRP EPA 8260B 2-Butanone (Methyl ethyl ketone, MEK) SCM MN
RCRP EPA 8260B 2-Chloroethyl vinyl ether NPW MN
RCRP EPA 8260B 2-Chloroethyl vinyl ether SCM MN
RCRP EPA 8260B 2-Chlorotoluene SCM MN
RCRP EPA 8260B 2-Chlorotoluene NPW MN
RCRP EPA 8260B 2-Hexanone NPW MN
RCRP EPA 8260B 2-Hexanone SCM MN
RCRP EPA 8260B 2-Methylnaphthalene SCM MN
RCRP EPA 8260B 2-Nitropropane NPW MN
RCRP EPA 8260B 4-Chlorotoluene SCM MN
RCRP EPA 8260B 4-Chlorotoluene NPW MN
RCRP EPA 8260B 4-Isopropyltoluene (p-Cymene) SCM MN
RCRP EPA 8260B 4-Isopropyltoluene (p-Cymene) NPW MN
RCRP EPA 8260B 4-Methyl-2-pentanone (MIBK) NPW MN
RCRP EPA 8260B 4-Methyl-2-pentanone (MIBK) SCM MN
RCRP EPA 8260B Acetone SCM MN
RCRP EPA 8260B Acetone NPW MN
RCRP EPA 8260B Acetonitrile NPW MN
RCRP EPA 8260B Acrolein (Propenal) NPW MN
RCRP EPA 8260B Acrolein (Propenal) SCM MN
RCRP EPA 8260B Acrylonitrile SCM MN
RCRP EPA 8260B Acrylonitrile NPW MN
RCRP EPA 8260B Allyl chloride (3-Chloropropene) NPW MN
RCRP EPA 8260B Allyl chloride (3-Chloropropene) SCM MN
RCRP EPA 8260B Benzene NPW MN
RCRP EPA 8260B Benzene SCM MN
RCRP EPA 8260B Bromobenzene NPW MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 8260B Bromobenzene SCM MN
RCRP EPA 8260B Bromochloromethane SCM MN
RCRP EPA 8260B Bromochloromethane NPW MN
RCRP EPA 8260B Bromodichloromethane SCM MN
RCRP EPA 8260B Bromodichloromethane NPW MN
RCRP EPA 8260B Bromoform NPW MN
RCRP EPA 8260B Bromoform SCM MN
RCRP EPA 8260B Carbon disulfide NPW MN
RCRP EPA 8260B Carbon disulfide SCM MN
RCRP EPA 8260B Carbon tetrachloride NPW MN
RCRP EPA 8260B Carbon tetrachloride SCM MN
RCRP EPA 8260B Chlorobenzene NPW MN
RCRP EPA 8260B Chlorobenzene SCM MN
RCRP EPA 8260B Chlorodibromomethane NPW MN
RCRP EPA 8260B Chlorodibromomethane SCM MN
RCRP EPA 8260B Chloroethane (Ethyl chloride) NPW MN
RCRP EPA 8260B Chloroethane (Ethyl chloride) SCM MN
RCRP EPA 8260B Chloroform SCM MN
RCRP EPA 8260B Chloroform NPW MN
RCRP EPA 8260B Chloroprene (2-Chloro-1,3-butadiene) NPW MN
RCRP EPA 8260B cis & trans-1,2-Dichloroethene SCM MN
RCRP EPA 8260B cis-1,2-Dichloroethylene NPW MN
RCRP EPA 8260B cis-1,2-Dichloroethylene SCM MN
RCRP EPA 8260B cis-1,3-Dichloropropene NPW MN
RCRP EPA 8260B cis-1,3-Dichloropropene SCM MN
RCRP EPA 8260B cis-1,4-Dichloro-2-butene NPW MN
RCRP EPA 8260B Di-isopropylether (DIPE) SCM MN
RCRP EPA 8260B Dibromomethane (Methylene bromide) SCM MN
RCRP EPA 8260B Dibromomethane (Methylene bromide) NPW MN
RCRP EPA 8260B Dichlorodifluoromethane (Freon-12) SCM MN
RCRP EPA 8260B Dichlorodifluoromethane (Freon-12) NPW MN
RCRP EPA 8260B Diethyl ether NPW MN
RCRP EPA 8260B Diethyl ether SCM MN
RCRP EPA 8260B Ethanol NPW MN
RCRP EPA 8260B Ethanol SCM MN
RCRP EPA 8260B Ethyl acetate NPW MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 8260B Ethyl methacrylate NPW MN
RCRP EPA 8260B Ethyl-t-butylether (ETBE) (2-Ethoxy-2-methylpropane)
SCM MN
RCRP EPA 8260B Ethyl-t-butylether (ETBE) (2-Ethoxy-2-methylpropane)
SCM MN User Defined S-MN-O-521 Rev. 27
RCRP EPA 8260B Ethyl-t-butylether (ETBE) (2-Ethoxy-2-methylpropane)
NPW MN User Defined S-MN-O-521 Rev. 27
RCRP EPA 8260B Ethylbenzene SCM MN
RCRP EPA 8260B Ethylbenzene NPW MN
RCRP EPA 8260B Hexachlorobutadiene SCM MN
RCRP EPA 8260B Hexachlorobutadiene NPW MN
RCRP EPA 8260B Iodomethane (Methyl iodide) SCM MN
RCRP EPA 8260B Iodomethane (Methyl iodide) NPW MN
RCRP EPA 8260B Isobutyl alcohol (2-Methyl-1-propanol) NPW MN
RCRP EPA 8260B Isobutyl alcohol (2-Methyl-1-propanol) SCM MN
RCRP EPA 8260B Isopropyl alcohol (2-Propanol,Isopropanol)
SCM MN
RCRP EPA 8260B Isopropyl alcohol (2-Propanol,Isopropanol)
NPW MN
RCRP EPA 8260B Isopropylbenzene NPW MN
RCRP EPA 8260B Isopropylbenzene SCM MN
RCRP EPA 8260B m+p-xylene NPW MN
RCRP EPA 8260B m+p-xylene SCM MN
RCRP EPA 8260B Methacrylonitrile NPW MN
RCRP EPA 8260B Methyl bromide (Bromomethane) SCM MN
RCRP EPA 8260B Methyl bromide (Bromomethane) NPW MN
RCRP EPA 8260B Methyl chloride (Chloromethane) SCM MN
RCRP EPA 8260B Methyl chloride (Chloromethane) NPW MN
RCRP EPA 8260B Methyl methacrylate NPW MN
RCRP EPA 8260B Methyl tert-butyl ether (MTBE) SCM MN
RCRP EPA 8260B Methyl tert-butyl ether (MTBE) NPW MN
RCRP EPA 8260B Methylene chloride (Dichloromethane) NPW MN
RCRP EPA 8260B Methylene chloride (Dichloromethane) SCM MN
RCRP EPA 8260B n-Butyl alcohol (1-Butanol, n-Butanol) NPW MN
RCRP EPA 8260B n-Butylbenzene SCM MN
RCRP EPA 8260B n-Butylbenzene NPW MN
RCRP EPA 8260B n-Hexane SCM MN
RCRP EPA 8260B n-Hexane NPW MN
RCRP EPA 8260B n-Propylbenzene SCM MN
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Program Method Analyte Matrix Primary SOP
RCRP EPA 8260B n-Propylbenzene NPW MN
RCRP EPA 8260B Naphthalene SCM MN
RCRP EPA 8260B Naphthalene NPW MN
RCRP EPA 8260B o-Xylene SCM MN
RCRP EPA 8260B o-Xylene NPW MN
RCRP EPA 8260B Propionitrile (Ethyl cyanide) NPW MN
RCRP EPA 8260B sec-Butylbenzene SCM MN
RCRP EPA 8260B sec-Butylbenzene NPW MN
RCRP EPA 8260B Styrene SCM MN
RCRP EPA 8260B Styrene NPW MN
RCRP EPA 8260B T-amylmethylether (TAME) NPW MN User Defined S-MN-O-521 Rev. 27
RCRP EPA 8260B T-amylmethylether (TAME) SCM MN User Defined S-MN-O-521 Rev. 27
RCRP EPA 8260B tert-Butyl alcohol NPW MN
RCRP EPA 8260B tert-Butyl alcohol SCM MN
RCRP EPA 8260B tert-Butylbenzene SCM MN
RCRP EPA 8260B tert-Butylbenzene NPW MN
RCRP EPA 8260B Tetrachloroethylene (Perchloroethylene) SCM MN
RCRP EPA 8260B Tetrachloroethylene (Perchloroethylene) NPW MN
RCRP EPA 8260B Tetrahydrofuran (THF) SCM MN
RCRP EPA 8260B Tetrahydrofuran (THF) NPW MN
RCRP EPA 8260B Toluene SCM MN
RCRP EPA 8260B Toluene NPW MN
RCRP EPA 8260B trans-1,2-Dichloroethylene SCM MN
RCRP EPA 8260B trans-1,2-Dichloroethylene NPW MN
RCRP EPA 8260B trans-1,3-Dichloropropylene SCM MN
RCRP EPA 8260B trans-1,3-Dichloropropylene NPW MN
RCRP EPA 8260B trans-1,4-Dichloro-2-butene SCM MN
RCRP EPA 8260B trans-1,4-Dichloro-2-butene NPW MN
RCRP EPA 8260B Trichloroethene (Trichloroethylene) SCM MN
RCRP EPA 8260B Trichloroethene (Trichloroethylene) NPW MN
RCRP EPA 8260B Trichlorofluoromethane(Fluorotrichloromethane, Freon 11)
NPW MN
RCRP EPA 8260B Trichlorofluoromethane(Fluorotrichloromethane, Freon 11)
SCM MN
RCRP EPA 8260B Vinyl acetate SCM MN
RCRP EPA 8260B Vinyl acetate NPW MN
RCRP EPA 8260B Vinyl chloride NPW MN
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EPA RSK-175 (GC/FID) Preparation Techniques: N/A
EPA 180.1 Preparation Techniques: N/A
EPA 300.0 Preparation Techniques: N/A
EPA 353.2 Preparation Techniques: N/A
Program Method Analyte Matrix Primary SOP
RCRP EPA 8260B Vinyl chloride SCM MN
RCRP EPA 8260B Xylene (total) SCM MN
Program Method Analyte Matrix Primary SOP
RCRP EPA RSK-175 (GC/FID) Ethane NPW MN
RCRP EPA RSK-175 (GC/FID) Ethene NPW MN
RCRP EPA RSK-175 (GC/FID) Methane NPW MN
Safe Drinking Water Program
Program Method Analyte Matrix Primary SOP
SDWP EPA 180.1 Turbidity DW MN
Program Method Analyte Matrix Primary SOP
SDWP EPA 300.0 Chloride DW MN
SDWP EPA 300.0 Fluoride DW MN
SDWP EPA 300.0 Nitrate DW MN
SDWP EPA 300.0 Nitrite DW MN
SDWP EPA 300.0 Sulfate DW MN
Program Method Analyte Matrix Primary SOP
SDWP EPA 353.2 Nitrate DW MN
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SM 2320 B-97 Preparation Techniques: N/A
SM 2340 B-97 Preparation Techniques: N/A
SM 2510 B-97 Preparation Techniques: N/A
SM 2540 C-97 Preparation Techniques: N/A
SM 4500-Cl G-93 Preparation Techniques: N/A
Program Method Analyte Matrix Primary SOP
SDWP EPA 353.2 Nitrite DW MN
Program Method Analyte Matrix Primary SOP
SDWP SM 2320 B-97 Alkalinity as CaCO3 DW MN
Program Method Analyte Matrix Primary SOP
SDWP SM 2340 B-97 Hardness DW MN
Program Method Analyte Matrix Primary SOP
SDWP SM 2510 B-97 Conductivity DW MN
Program Method Analyte Matrix Primary SOP
SDWP SM 2540 C-97 Residue-filterable (TDS) DW MN
Program Method Analyte Matrix Primary SOP
SDWP SM 4500-Cl G-93 Total chlorine DW MN
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SM 4500-CN¯ E-97 Preparation Techniques: Distillation, micro; Distillation, macro; Distillation, MIDI;
SM 4500-CN¯ G-97 Preparation Techniques: Distillation, micro; Distillation, macro; Distillation, MIDI;
SM 4500-F¯ C-97 Preparation Techniques: N/A;
SM 4500-H+ B-96 Preparation Techniques: N/A
SM 4500-NO2¯ B-93 Preparation Techniques: N/A
SM 4500-P E-97 Preparation Techniques: N/A
Program Method Analyte Matrix Primary SOP
SDWP SM 4500-CN¯ E-97 Cyanide DW MN
Program Method Analyte Matrix Primary SOP
SDWP SM 4500-CN¯ G-97 Cyanide DW MN
Program Method Analyte Matrix Primary SOP
SDWP SM 4500-F¯ C-97 Fluoride DW MN
Program Method Analyte Matrix Primary SOP
SDWP SM 4500-H+ B-96 pH DW MN
Program Method Analyte Matrix Primary SOP
SDWP SM 4500-NO2¯ B-93 Nitrite DW MN
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EPA 200.8 Preparation Techniques: Digestion, hotplate or HotBlock;
EPA 245.1 Preparation Techniques: N/A
SM 9215 B (R2A)-94 Preparation Techniques: N/A
Program Method Analyte Matrix Primary SOP
SDWP SM 4500-P E-97 Orthophosphate as P DW MN
Program Method Analyte Matrix Primary SOP
SDWP EPA 200.8 Aluminum DW MN
SDWP EPA 200.8 Antimony DW MN
SDWP EPA 200.8 Arsenic DW MN
SDWP EPA 200.8 Barium DW MN
SDWP EPA 200.8 Beryllium DW MN
SDWP EPA 200.8 Cadmium DW MN
SDWP EPA 200.8 Chromium DW MN
SDWP EPA 200.8 Copper DW MN
SDWP EPA 200.8 Lead DW MN
SDWP EPA 200.8 Manganese DW MN
SDWP EPA 200.8 Nickel DW MN
SDWP EPA 200.8 Selenium DW MN
SDWP EPA 200.8 Silver DW MN
SDWP EPA 200.8 Thallium DW MN
SDWP EPA 200.8 Uranium DW MN
SDWP EPA 200.8 Zinc DW MN
Program Method Analyte Matrix Primary SOP
SDWP EPA 245.1 Mercury DW MN
Program Method Analyte Matrix Primary SOP
SDWP SM 9215 B (R2A)-94 Heterotrophic plate count DW MN
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SM 9223 B (Colilert®)-97 Preparation Techniques: N/A
EPA 1613 Preparation Techniques: Extraction, solid phase (SPE); Extraction, automated soxhlet; Extraction, separatory funnel liquid-liquid
(LLE);
EPA 524.2 Preparation Techniques: Purge and trap;
Program Method Analyte Matrix Primary SOP
SDWP SM 9223 B (Colilert®)-97 Escherichia coli DW MN
SDWP SM 9223 B (Colilert®)-97 Total coliforms DW MN
Program Method Analyte Matrix Primary SOP
SDWP EPA 1613 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)
DW MN
Program Method Analyte Matrix Primary SOP
SDWP EPA 524.2 1,1,1,2-Tetrachloroethane DW MN
SDWP EPA 524.2 1,1,1-Trichloroethane DW MN
SDWP EPA 524.2 1,1,2,2-Tetrachloroethane DW MN
SDWP EPA 524.2 1,1,2-Trichloroethane DW MN
SDWP EPA 524.2 1,1-Dichloroethane DW MN
SDWP EPA 524.2 1,1-Dichloroethylene DW MN
SDWP EPA 524.2 1,1-Dichloropropene DW MN
SDWP EPA 524.2 1,2,3-Trichlorobenzene DW MN
SDWP EPA 524.2 1,2,3-Trichloropropane DW MN
SDWP EPA 524.2 1,2,4-Trichlorobenzene DW MN
SDWP EPA 524.2 1,2,4-Trimethylbenzene DW MN
SDWP EPA 524.2 1,2-Dichlorobenzene DW MN
SDWP EPA 524.2 1,2-Dichloroethane (Ethylene dichloride) DW MN
SDWP EPA 524.2 1,2-Dichloropropane DW MN
SDWP EPA 524.2 1,3,5-Trichlorobenzene DW MN
SDWP EPA 524.2 1,3-Dichlorobenzene DW MN
SDWP EPA 524.2 1,4-Dichlorobenzene DW MN
SDWP EPA 524.2 2,2-Dichloropropane DW MN
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Program Method Analyte Matrix Primary SOP
SDWP EPA 524.2 2-Chlorotoluene DW MN
SDWP EPA 524.2 4-Chlorotoluene DW MN
SDWP EPA 524.2 Benzene DW MN
SDWP EPA 524.2 Bromobenzene DW MN
SDWP EPA 524.2 Bromochloromethane DW MN
SDWP EPA 524.2 Bromodichloromethane DW MN
SDWP EPA 524.2 Bromoform DW MN
SDWP EPA 524.2 Bromomethane DW MN
SDWP EPA 524.2 Carbon tetrachloride DW MN
SDWP EPA 524.2 Chlorobenzene DW MN
SDWP EPA 524.2 Chlorodibromomethane DW MN
SDWP EPA 524.2 Chloroethane (Ethyl chloride) DW MN
SDWP EPA 524.2 Chloroform DW MN
SDWP EPA 524.2 cis-1,2-Dichloroethylene DW MN
SDWP EPA 524.2 cis-1,3-Dichloropropene DW MN
SDWP EPA 524.2 Dibromomethane (Methylene bromide) DW MN
SDWP EPA 524.2 Dichlorodifluoromethane (Freon-12) DW MN
SDWP EPA 524.2 Ethylbenzene DW MN
SDWP EPA 524.2 Hexachlorobutadiene DW MN
SDWP EPA 524.2 Isopropylbenzene DW MN
SDWP EPA 524.2 Methyl chloride (Chloromethane) DW MN
SDWP EPA 524.2 Methyl tert-butyl ether (MTBE) DW MN
SDWP EPA 524.2 Methylene chloride (Dichloromethane) DW MN
SDWP EPA 524.2 n-Butylbenzene DW MN
SDWP EPA 524.2 n-Propylbenzene DW MN
SDWP EPA 524.2 Naphthalene DW MN
SDWP EPA 524.2 sec-Butylbenzene DW MN
SDWP EPA 524.2 Styrene DW MN
SDWP EPA 524.2 tert-Butylbenzene DW MN
SDWP EPA 524.2 Tetrachloroethylene (Perchloroethylene) DW MN
SDWP EPA 524.2 Toluene DW MN
SDWP EPA 524.2 Total Trihalomethanes DW MN
SDWP EPA 524.2 trans-1,2-Dichloroethylene DW MN
SDWP EPA 524.2 trans-1,3-Dichloropropylene DW MN
SDWP EPA 524.2 Trichloroethene (Trichloroethylene) DW MN
SDWP EPA 524.2 Trichlorofluoromethane(Fluorotrichloromethane, Freon 11)
DW MN
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WI(95) DRO Preparation Techniques: N/A
EPA TO-15 Preparation Techniques: N/A
Program Method Analyte Matrix Primary SOP
SDWP EPA 524.2 Vinyl chloride DW MN
SDWP EPA 524.2 Xylene (total) DW MN
Underground Storage Tank Program
Program Method Analyte Matrix Primary SOP
USTP WI(95) DRO Diesel range organics (DRO) SCM MN
USTP WI(95) DRO Diesel range organics (DRO) NPW MN
USTP WI(95) DRO Diesel range organics (DRO) SCM MN User Defined S-MN-O-466 Rev. Rev.21
USTP WI(95) DRO Diesel range organics (DRO) NPW MN User Defined S-MN-O-466 Rev. Rev.21
Program Method Analyte Matrix Primary SOP
USTP EPA TO-15 1,1,1-Trichloroethane AIR MN
USTP EPA TO-15 1,1,2,2-Tetrachloroethane AIR MN
USTP EPA TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane(Freon 113)
AIR MN
USTP EPA TO-15 1,1,2-Trichloroethane AIR MN
USTP EPA TO-15 1,1-Dichloroethane AIR MN
USTP EPA TO-15 1,1-Dichloroethylene AIR MN
USTP EPA TO-15 1,2,4-Trichlorobenzene AIR MN
USTP EPA TO-15 1,2,4-Trimethylbenzene AIR MN
USTP EPA TO-15 1,2-Dibromoethane (EDB, Ethylenedibromide)
AIR MN
USTP EPA TO-15 1,2-Dichloro-1,1,2,2-tetrafluoroethane(Freon-114)
AIR MN
USTP EPA TO-15 1,2-Dichlorobenzene AIR MN
USTP EPA TO-15 1,2-Dichloroethane (Ethylene dichloride) AIR MN
USTP EPA TO-15 1,2-Dichloropropane AIR MN
USTP EPA TO-15 1,3,5-Trimethylbenzene AIR MN
USTP EPA TO-15 1,3-Butadiene AIR MN
USTP EPA TO-15 1,3-Dichlorobenzene AIR MN
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Program Method Analyte Matrix Primary SOP
USTP EPA TO-15 1,4-Dichlorobenzene AIR MN
USTP EPA TO-15 1-Propene AIR MN
USTP EPA TO-15 2-Butanone (Methyl ethyl ketone, MEK) AIR MN
USTP EPA TO-15 2-Hexanone AIR MN
USTP EPA TO-15 4-Ethyltoluene AIR MN
USTP EPA TO-15 4-Methyl-2-pentanone (MIBK) AIR MN
USTP EPA TO-15 Acetone AIR MN
USTP EPA TO-15 Benzene AIR MN
USTP EPA TO-15 Benzyl chloride AIR MN
USTP EPA TO-15 Bromodichloromethane AIR MN
USTP EPA TO-15 Bromoform AIR MN
USTP EPA TO-15 Carbon disulfide AIR MN
USTP EPA TO-15 Carbon tetrachloride AIR MN
USTP EPA TO-15 Chlorobenzene AIR MN
USTP EPA TO-15 Chlorodibromomethane AIR MN
USTP EPA TO-15 Chloroethane (Ethyl chloride) AIR MN
USTP EPA TO-15 Chloroform AIR MN
USTP EPA TO-15 cis-1,2-Dichloroethylene AIR MN
USTP EPA TO-15 cis-1,3-Dichloropropene AIR MN
USTP EPA TO-15 Cyclohexane AIR MN
USTP EPA TO-15 Dichlorodifluoromethane (Freon-12) AIR MN
USTP EPA TO-15 Ethanol AIR MN
USTP EPA TO-15 Ethyl acetate AIR MN
USTP EPA TO-15 Ethylbenzene AIR MN
USTP EPA TO-15 Hexachlorobutadiene AIR MN
USTP EPA TO-15 Isopropyl alcohol (2-Propanol,Isopropanol)
AIR MN
USTP EPA TO-15 m+p-xylene AIR MN
USTP EPA TO-15 Methyl bromide (Bromomethane) AIR MN
USTP EPA TO-15 Methyl chloride (Chloromethane) AIR MN
USTP EPA TO-15 Methyl tert-butyl ether (MTBE) AIR MN
USTP EPA TO-15 Methylene chloride (Dichloromethane) AIR MN
USTP EPA TO-15 n-Heptane AIR MN
USTP EPA TO-15 n-Hexane AIR MN
USTP EPA TO-15 Naphthalene AIR MN
USTP EPA TO-15 o-Xylene AIR MN
USTP EPA TO-15 Styrene AIR MN
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WI(95) GRO Preparation Techniques: N/A
WI(95) GRO Preparation Techniques: N/A
Note: Method beginning with "SM" refer to the approved editions of Standard methods for the Examination of Water and Wastes. Approved
methods are listed in the applicable parts of Title 40 of the Code of Federal Regulations (including its subsequent Federal Register updates),
MN Statutes and Rules, and state-issued permits.
Program Method Analyte Matrix Primary SOP
USTP EPA TO-15 Tetrachloroethylene (Perchloroethylene) AIR MN
USTP EPA TO-15 Tetrahydrofuran (THF) AIR MN
USTP EPA TO-15 Toluene AIR MN
USTP EPA TO-15 trans-1,2-Dichloroethylene AIR MN
USTP EPA TO-15 trans-1,3-Dichloropropylene AIR MN
USTP EPA TO-15 Trichloroethene (Trichloroethylene) AIR MN
USTP EPA TO-15 Trichlorofluoromethane(Fluorotrichloromethane, Freon 11)
AIR MN
USTP EPA TO-15 Vinyl acetate AIR MN
USTP EPA TO-15 Vinyl chloride AIR MN
USTP EPA TO-15 Xylene (total) AIR MN
Program Method Analyte Matrix Primary SOP
USTP WI(95) GRO Gasoline range organics (GRO) NPW MN
USTP WI(95) GRO Gasoline range organics (GRO) SCM MN
Program Method Analyte Matrix Primary SOP
USTP WI(95) GRO Petroleum Volatile Organic Compounds(PVOC)
SCM MN
USTP WI(95) GRO Petroleum Volatile Organic Compounds(PVOC)
NPW MN
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Potable drinking water samples for determining lead content in water were obtained using 950 cubic centimeters (0.95 liters) plastic bottles to collect water. The collection bottles were provided by the analyzing laboratory; Pace Analytical. First draw samples were collected after each potable drinking water source was not used for a minimum of six hours prior to sample collection. Sample were collected from the cold water side if the faucets had both hot and cold water. Prior to collecting water samples, nitrile gloves were donned by the person collecting the water sample to prevent cross contamination. The cap was removed from the 950 cc sample bottle and the bottle was filled with water at the rate it would be used by the consumer. The bottle was not allowed to overfill. The bottle was closed tightly with the cap and a unique sample number was written on the side of the sample bottle. The sample number was recorded on the chain of custody and stored in a cooler for transport to the analyzing laboratory. Field notes documented each sample number, type of fixture, the location and any additional comments. Pace Analytical Services (PACE) analyzed the potable drinking water samples for lead content. PACE used EPA Method 200.8 to analyze for lead concentrations in each water sample. EPA Method 200.8 is a well-established method promulgated by the U.S. Environmental Protection Agency (EPA) for the analysis of ground waters, surface waters, drinking waters, and wastewaters by inductively coupled plasma mass spectrometry (ICP-MS). The method was first published in 1990 to support the National Primary Drinking Water Regulations (NPDWR), which specified maximum contaminant levels (MCL) for 12 primary elemental contaminants in public water systems as part of the Safe Drinking Water Act (SDWA) of 1986. There have been many iterations of Method 200.8, including the addition of 9 secondary contaminants under the National Secondary Drinking Water Regulations (NSDWR). The version in use today is Revision 5.4 of the Method, which was approved for drinking water in 1994 and became effective in January, 1995. In addition, Method 200.8 was also recommended in 1992 for the monitoring of wastewaters under the National Pollutant Discharge Elimination System (NPDES) permit program to control the discharge of pollutants into navigable water systems, as part of the amended Clean Water Act (CWA) of 1977. It was approved on a nation-wide basis for this matrix in 2007.1
1 http://www.perkinelmer.com/CMSResources/Images/44-134581APP_NexION300Q-US-EPA200-8-Drinking-Water.pdf
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Introduction to Lead
Page 1 of 1
Lead naturally occurs in small amounts in nature and is found in soil, rocks and water. However, lead can be toxic to humans in higher concentrations when ingested or inhaled. Lead exposure occurs from lead containing products such as fossil fuels, plumbing, paint, batteries, ammunition and cosmetics. Lead from industrial manufacturing sites contaminates the environment and workers when using incorrect work practices, using inadequate personal protective equipment, and improper handing lead containing waste products. Industrial facilities, automobiles, and small aircraft release lead in to the atmosphere which settles on surfaces; contaminating structures, soil, and water. Federal and state regulatory standards have reduced lead content in products and significantly decreased lead exposure in humans.
Lead exposure poses the greatest risk for children since Lead is more easily absorbed and incorporated into their growing bodies. At high concentrations, lead interferes with growth, results in hearing problems, mental development, behavior problems, and lower intelligence. Children may absorb 50% of the lead from an exposure. Lead ingested or inhaled from contaminated soil in their playground, lead dust in the paint on their house or toys, and lead contaminated water are a few sources that children are exposed to lead. Adults are less affected by lead since physical growth has generally stopped. With the exception of pregnant mothers and their unborn child, adults do not absorb lead as readily as children may only absorb 25% of the lead from an exposure. However, lead exposure at higher concentrations for adults can cause health symptoms such as nerve disorders, decreased kidney function and cardiovascular deficiencies, Organic lead compounds, such as tetraethyl lead and tetramethyl lead (TEL) which is an additive to avgas, behave as gases in the respiratory tract and are absorbed to a greater extent than are inorganic lead particles. Organic lead compounds are also absorbed through the skin of both humans and experimental animals.
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