Lampiran 1. Surat Keterangan Determinasi Daun Pare ...eprints.unwahas.ac.id/1467/7/File 8 (LAMPIRAN).pdf · Surat Keterangan Determinasi Daun Pare (Momordica charantia L.) 46 Lampiran

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Lampiran 1. Surat Keterangan Determinasi Daun Pare (Momordica charantia L.)

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Lampiran 1. Lanjutan...

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Lampiran 1. Lanjutan..

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Lampiran 2. Surat keterangan telah Selesai Melakukan Penelitian di Universitas

Wahid Hasyim Semarang

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Lanjutan Lampiran 2. Surat keterangan telah Selesai Melakukan Penelitian di

Universitas Wahid Hasyim Semarang

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Lampiran 3. Gambar Alat yang digunakan dalam Penelitian

Timbangan listrik (HENHERR) Oven (MEMMERT) Blender (MASPION)

Moisture balance (OHAUS) Bejana maserasi Rotary evaporator

(HEIDOLPH)

Volumenomete Timbangan analitik (OHAUS) Corong stainless stell

Lampiran 3. Lanjutan…

Friability tester (ERWEKA) Single punch (KORSCH) Hardness tester

(ERWEKA)

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Lampiran 4. Hasil Pemeriksaan Kecepatan Alir Granul

Replikasi

Formula ( gram/detik)

I II III IV V

1 12,05 14,28 13,16 12,50 13,51

2 13,89 12,19 12,50 12,84 13,15

3 13,51 14,08 12,66 14,31 12,20

13 13,79 14,09 13,48 16,83

SD 0,97 1,15 0,34 0,96 0,67

Formula I

Formula II

Formula III

53


Formula IV

Formula V

54

Lampiran 5. Hasil Pemeriksaan Sudut Diam Granul

Replikasi Formula ( º )

I II III IV V

1 26,10 27,02 27,92 29,68 27,02

2 27,02 31,79 26,10 28,54 28,81

3 29,24 27,83 29,24 28,81 30,11

27,45 28,88 27,75 29,01 28,64

SD 1,61 2,55 1,57 0,59 1,55

Formula I

1. D1 = 12 cm D rata-rata = 12,25 cm H = 3 cm

D2 = 12,5 cm R = 6,125 cm

26,10 º

2. D1 = 12,5 cm D rata-rata = 12,5 cm H = 3,2 cm

D2 = 12,5 cm R = 6,25 cm

27,02 º

3. D1 = 12 cm D rata-rata = 12,5 cm H = 3,5 cm

D2 = 13 cm R = 6,25 cm

29,24 º

Formula II


D2 = 13 cm R = 6,625 cm

27,02 º

55



D2 = 12,5 cm R = 6,125 cm

31,79 º


D2 = 12 cm R = 6 cm

27,83 º

Formula III


D2 = 13,5 cm R = 6,75 cm

27,92 º

2. D1 = 12,5 cm D rata-rata = 12,25 cm H = 3 cm

D2 = 12 cm R = 6,125 cm

26,10 º


D2 = 12,5 cm R = 6,375 cm

29,24 º

Formula IV

1. D1 = 12,5 cm D rata-rata = 13 cm H = 3,7 cm

D2 = 13,5 cm R = 6,5 cm

29,68 º

56


D2 = 12 cm R = 6,25 cm


28,54 º


D2 = 13,5 cm R = 6,75 cm

28,81 º

Formula V


D2 = 13 cm R = 6,325cm

27,02 º


D2 = 13,5 cm R = 6,425 cm

28,81 º


D2 = 13,7 cm R = 6,55 cm

30,11 º

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Lampiran 6. Hasil Pemeriksaan Kompresibilitas Granul

Replikasi

Formula (%)

I II III IV V

1 15,00 18,00 17,00 16,00 17,00

2 17,00 18,00 20,00 15,00 13,00

3 16,00 16,00 18,00 15,00 14,00

16 17,33 18,33 15,33 14,66

SD 1 1,15 1,52 0,57 2,08

Formula I

1. Vo = 100 mL

Vf = 85 mL

15%

2. Vo = 100 mL

Vf = 83 mL

17 %

3. Vo = 100 mL

Vf = 84 mL

16 %

Formula II

1. Vo = 100 mL

Vf = 82 mL

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18 %

2. Vo = 100 mL


Vf = 84 mL

16 %

3. Vo = 100 mL

Vf = 83 mL

17 %

Formula III

1. Vo = 100 mL

Vf = 83 mL

17 %

2. Vo = 100 mL

Vf = 80 mL

20 %

3. Vo = 100 mL

Vf = 82 mL

18 %

Formula IV

1. Vo = 100 mL

Vf = 84 mL

16 %

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2. Vo = 100 mL

Vf = 85 mL

15 %

3. Vo = 100 mL


Vf = 85 mL

15 %

Formula V

1. Vo = 100 mL

Vf = 83 mL

17 %

2. Vo = 100 mL Vf = 87 mL

13 %

3. Vo = 100 mL Vf = 86 mL

14 %

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Lampiran 7. Hasil Pemeriksaan Keseragaman Bobot Tablet Hisap

No

Bobot tablet (gram)

F I F II F III F IV F V

1 1,049 1,009 1,016 0,949 1,011

2 1,051 1,02 1,032 0,964 1,003

3 1,042 1,008 1,015 1,054 1,019

4 1,029 1,008 1,022 0,994 1,016

5 1,029 1,014 1,004 0,969 1,009

6 1,026 1,027 1,003 1,057 1,005

7 1 1,007 1,02 1,019 1,016

8 1,05 1,011 1,003 1,028 1,007

9 1,043 1,018 1,007 1,011 1,018

10 1 1,002 1 1,002 1,012

11 1,011 1,018 0,99 1,013 1,006

12 1,012 1,022 1,013 0,992 1,002

13 1 1,008 1,032 0,975 0,995

14 1,016 1,021 0,999 1,053 1,013

15 1,024 1,01 1,017 0,985 1,028

16 1,018 1,004 0,998 1,031 1,023

17 1,02 1,032 1,002 1,014 1,006

18 1,004 1,02 1,015 1,006 0,997

19 1,048 1,024 1,002 1,027 1,009

20 1,003 1,025 1,035 1,022 1,015

1,02 1,01 1,01 1,01 1,01

SD 0,01 0,01 0,01 0,03 0,01

CV

(%) 0,98 0,99 0,99 2,97 0,99

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Formula I

Bobot rata-rata 20 tablet = 1,003 gram

Jadi berat tablet = 1,003 gram ± 0,050 gram

= 0,953-1,053 gram


= 0,903-1,103 gram

Formula II



=0,974-1,076 gram


= 0,923-1,127 gram

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Formula III




= 0,984-1,086 gram


= 0,932-1,138 gram

Formula IV



= 0,971-1,073 gram


= 0,92-1,124 gram

Formula V



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= 0,964-1,066 gram


= 0,914-1,116 gram


Hasil Uji Statistik Keseragaman Bobot Tablet

Keseragaman bobot

Test of Homogeneity of Variances

Keseragaman

Bobot

Levene Statistic df1 df2 Sig.

10.592 4 95 .000

Tests of Normality

Formu

lasi

Kolmogorov-Smirnova Shapiro-Wilk

Statistic Df Sig. Statistic df Sig.

Keseraga

man Bobot

F1 .141 20 .200* .908 20 .059

F2 .150 20 .200* .955 20 .454

F3 .168 20 .139 .942 20 .258

F4 .086 20 .200* .972 20 .803

F5 .071 20 .200* .990 20 .999

a. Lilliefors Significance Correction

*. This is a lower bound of the true significance.

64


Kruskal Wallis

Keseragaman Bobot

Test Statisticsab

Keseragama

n Bobot

Chi-Square 7.361

Df 4

Asymp.

Sig. .118

a. Kruskal Wallis Test

b. Grouping Variable:

keseragaman bobot

FI dan FII

Test Statisticsb

keseragaman

bobot

Mann-Whitney U 153.500

Wilcoxon W 363.500

Z -1.259

Asymp. Sig. (2-tailed) .208

Exact Sig. [2*(1-tailed

Sig.)] .211a

a. Not corrected for ties.

b. Grouping Variable: FORMULASI

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FI dan FIII

Test Statisticsb

keseragaman

bobot


Wilcoxon W 332.000

Z -2.112



Sig.)] .035a



FI dan FIV

Test Statisticsb

keseragaman

bobot


Wilcoxon W 354.500

Z -1.502



Sig.)] .134a



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FI dan FV

Test Statisticsb

keseragaman

bobot


Wilcoxon W 327.000

Z -2.247



Sig.)] .024a



FII dan FIII

Test Statisticsb

keseragaman

bobot


Wilcoxon W 353.500

Z -1.530



Sig.)] .127a



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FII dan FIV

Test Statisticsb

keseragaman

bobot


Wilcoxon W 383.500

Z -.717



Sig.)] .478a


b. Grouping Variable: FORMULA

FII dan FV

Test Statisticsb

keseragaman

bobot


Wilcoxon W 347.500

Z -1.692



Sig.)] .091a



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FIII dan FIV

Test Statisticsb

keseragaman

bobot


Wilcoxon W 400.000

Z -.271



Sig.)] .799a



FIII dan FV

Test Statisticsb

keseragaman

bobot


Wilcoxon W 406.000

Z -.108



Sig.)] .925a



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FIV dan FV

Test Statisticsb

keseragaman

bobot


Wilcoxon W 408.500

Z -.041



Sig.)] .968a



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Lampiran 8. Hasil Pemeriksaan Kekerasan Tablet Hisap

Replikasi Kekerasan (Kg)


1 6,5 8 7,7 7,9 10,9

2 6,3 7,7 6,1 6,9 10,5

3 5,9 7 5,9 8 9,8

4 5,7 7,9 6,6 7,7 9,4

5 5,7 7,4 6,6 6,9 9,1

6,02 7,6 6,58 7,48 9,94

SD 0,36 0,40 0,69 0,54 0,75

Hasil Uji Statistik Kekerasan Tablet

ANOVA

Kekerasan

Sum of

Squares Df Mean Square F Sig.

Between

Groups 44.990 4 11.247 34.312 .000

Within Groups 6.556 20 .328

Total 51.546 24

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Multiple Comparisons

Kekerasan

Tukey HSD

(I)

kesera

gaman

bobot

(J)

kesera

gaman

bobot

Mean

Difference (I-

J) Std. Error Sig.

95% Confidence Interval

Lower

Bound Upper Bound

FI FII -1.5800* .3621 .002 -2.664 -.496

FIII -.5600 .3621 .546 -1.644 .524

FIV -1.4600* .3621 .005 -2.544 -.376

FV -3.9200* .3621 .000 -5.004 -2.836

FII FI 1.5800* .3621 .002 .496 2.664

FIII 1.0200 .3621 .071 -.064 2.104

FIV .1200 .3621 .997 -.964 1.204

FV -2.3400* .3621 .000 -3.424 -1.256

FIII FI .5600 .3621 .546 -.524 1.644

FII -1.0200 .3621 .071 -2.104 .064

FIV -.9000 .3621 .134 -1.984 .184

FV -3.3600* .3621 .000 -4.444 -2.276

FIV FI 1.4600* .3621 .005 .376 2.544

FII -.1200 .3621 .997 -1.204 .964

FIII .9000 .3621 .134 -.184 1.984

FV -2.4600* .3621 .000 -3.544 -1.376

FV FI 3.9200* .3621 .000 2.836 5.004

FII 2.3400* .3621 .000 1.256 3.424

FIII 3.3600* .3621 .000 2.276 4.444

FIV 2.4600* .3621 .000 1.376 3.544

*. The mean difference is significant at the 0.05 level.

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Lampiran 9. Hasil Pemeriksaan Kerapuhan Tablet Hisap

Replikasi Kerapuhan (%)


1 0,01 0,05 0,14 0,03 0,10

2 0,04 0,45 0,32 0,12 0,13

3 0,01 0,03 0,02 0,16 0,05

0,02 0,17 0,16 0,10 0,10

SD 0,01 0,23 0,15 0,06 0,04

Formula I

Formula II

73


Formula III

Formula IV

74


Formula V

Hasil Uji Statistik Kerapuhan Tablet

Kruskal Wallis

Kerapuhan

Test Statisticsab

kerapuhan tab

Chi-Square 4.767

Df 4

Asymp.

Sig. .312



formulasi

75


FI VS FII

Test Statisticsb

kerapuhan tab


Wilcoxon W 7.000

Z -1.528



Sig.)] .200a


b. Grouping Variable: formulasi

FI VS FIII

Test Statisticsb

kerapuhan tab


Wilcoxon W 7.000

Z -1.528



Sig.)] .200a



76


FI VS FIV

Test Statisticsb

kerapuhan tab


Wilcoxon W 7.000

Z -1.528



Sig.)] .200a



FI VS FV

Test Statisticsb

kerapuhan tab

Mann-Whitney U .000

Wilcoxon W 6.000

Z -1.964



Sig.)] .100a



77


FII VS FIII

Test Statisticsb

kerapuhan tab


Wilcoxon W 10.000

Z -.218



Sig.)] 1.000a



FII VS FIV

Test Statisticsb

kerapuhan tab


Wilcoxon W 10.000

Z -.218



Sig.)] 1.000a



78


FII VS FV

Test Statisticsb

kerapuhan tab


Wilcoxon W 9.000

Z -.655



Sig.)] .700a



FIII VS FIV

Test Statisticsb

kerapuhan tab


Wilcoxon W 10.000

Z -.218



Sig.)] 1.000a



79


FIII VS FV

Test Statisticsb

kerapuhan tab


Wilcoxon W 9.000

Z -.655



Sig.)] .700a



FIV VS FV

Test Statisticsb

kerapuhan tab


Wilcoxon W 10,000

Z -,218

Asymp, Sig, (2-tailed) ,827

Exact Sig, [2*(1-tailed

Sig,)] 1,000a

a, Not corrected for ties,

b, Grouping Variable: formulasi

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Lampiran 10. Hasil Pemeriksaan Waktu Melarut Tablet Hisap

Responden Waktu Melarut (menit)


1 6 8 9 8 13

2 10 9 8 7 10

3 12 7 8 11 8

4 11 10 7 9 7

5 8 9 10 10 8

6 7 12 9 8 9

7 8 8 9 9 8

8 11 9 7 6 8

9 11 9 9 10 8

10 10 10 9 8 6

11 10 7 8 7 7

12 9 10 8 9 7

13 10 8 7 9 6

14 12 9 11 7 8

15 7 8 8 7 9

16 7 8 8 7 9

17 8 7 6 7 7

18 9 10 9 10 8

19 7 10 9 9 9

20 9 9 8 7 9

9,1 8,85 8,35 8,25 8,2

SD 1,80 1,26 1,13 1,37 1,54

81


Data Statistik Waktu Melarut

Kruskal Wallis

Waktu Melarut’

Test Statisticsab

waktu melarut

tab

Chi-Square 5.838

Df 4

Asymp. Sig. .212



formulasi

FI VS FII

Test Statisticsb

waktu melarut

tab


Wilcoxon W 392.500

Z -.482



Sig.)] .640a



82


FI VS FIII

Test Statisticsb

waktu melarut

tab


Wilcoxon W 361.000

Z -1.352



Sig.)] .192a



FI VS FIV

Test Statisticsb

waktu melarut

tab


Wilcoxon W 354.000

Z -1.545



Sig.)] .134a



83


FI VS FV

Test Statisticsb

waktu melarut

tab


Wilcoxon W 349.000

Z -1.679



Sig.)] .102a



FII VS FIII

Test Statisticsb

waktu melarut

tab


Wilcoxon W 365.500

Z -1.247



Sig.)] .231a



84


FII VS FIV

Test Statisticsb

waktu melarut

tab


Wilcoxon W 360.500

Z -1.375



Sig.)] .183a



FII VS FV

Test Statisticsb

waktu melarut

tab


Wilcoxon W 346.000

Z -1.782



Sig.)] .086a



85


FIII VS FIV

Test Statisticsb

waktu melarut

tab


Wilcoxon W 398.000

Z -.335



Sig.)] .758a



FIII VS FV

Test Statisticsb

waktu melarut

tab


Wilcoxon W 384.500

Z -.717



Sig.)] .495a



86


FIV VS FV

Test Statisticsb

waktu melarut

tab


Wilcoxon W 400.500

Z -.264



Sig.)] .799a


b, Grouping Variable: formulasi

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Lampiran 11. Angket Tanggapan Responden

ANGKET TANGGAPAN RASA

PETUNJUK PENGISIAN ANGKET

Berilah tanda cek list (√) pada kolom angket sesuai dengan rasa dari tablet hisap

ekstrak etanol daun Pare

PERTANYAAN

1. Bagaimana pendapat anda mengenai rasa dari tablet hisap ekstrak etanol daun

Pare untuk produk I, II, III, IV, V Diskripsikan pendapat anda !

Tingkat

kemanisan


Manis

Kurang Manis

Pahit

Sangat Pahit

Catatan :

2. Berdasarkan rasa dari kelima produk tablet hisap ekstrak etanol daun Pare

tersebut, produk mana yang dapat diterima? (Pilih salah satu)

I II III IV V

Formula yang dapat

diterima

IDENTITAS RESPONDEN

Nama :

Pekerjaan :

Umur :

Alamat :

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Lampiran 12. Perhitungan % Uji Tanggap Rasa

Formula I

= X 20 Responden = 17 Responden X 100% = 85%


Formula II



Formula III




Formula IV



Formula V



Documents

Lampiran 1. Surat Keterangan Determinasi Daun Pare ...eprints.unwahas.ac.id/1467/7/File 8 (LAMPIRAN).pdf · Surat Keterangan Determinasi Daun Pare (Momordica charantia L.) 46 Lampiran