LABORATORY REPORT - United States Environmental · PDF fileQA/QC CRITERIA: All analyses met method criteria, ... LABORATORY REPORT Prepared For: AMEC Geomatrix Consultants, Inc. -

4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602)

454-9303

LABORATORY REPORT

Prepared For: AMEC Geomatrix Consultants, Inc. - AZ - PGAN

8777 E. Via de Ventura, Suite 396

Scottsdale, AZ 85258

Attention: Mike Dempsey Sampled:

Received:

Issued:

05/11/09

05/11/09

05/22/09 09:45

The results listed within this Laboratory Report pertain only to the samples tested in the laboratory. The analyses contained in this report

were performed in accordance with the applicable certifications as noted. All soil samples are reported on a wet weight basis unless

otherwise noted in the report. This Laboratory Report is confidential and is intended for the sole use of TestAmerica and its client. This

report shall not be reproduced, except in full, without written permission from TestAmerica. The Chain of Custody, 1 page, is included and

is an integral part of this report.

This entire report was reviewed and approved for release.

Project: 08-227E

NELAP #01109CA Arizona DHS#AZ0728

CASE NARRATIVE

MATRIXCLIENT IDLABORATORY ID

PSE0580-01 Bd2-05112009 Water

SAMPLE RECEIPT: Samples were received intact, at 3°C, on ice and with chain of custody documentation.

HOLDING TIMES: All samples were analyzed within prescribed holding times and/or in accordance with the TestAmerica

Sample Acceptance Policy unless otherwise noted in the report.

PRESERVATION: Samples requiring preservation were verified prior to sample analysis.

QA/QC CRITERIA: All analyses met method criteria, except as noted in the report with data qualifiers.

COMMENTS: No significant observations were made.

SUBCONTRACTED: No analyses were subcontracted to an outside laboratory.

Reviewed By:

Project Manager

TestAmerica Phoenix

PSE0580

Tina Paulauskas

<Page 1 of 5>

SDMS DOCID#1142197


454-9303

AMEC Geomatrix Consultants, Inc. - AZ - PGAN



Attention: Mike Dempsey

Sampled:

Received:

05/11/09

05/11/09Report Number:

Project ID:

PSE0580

08-227E

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

TOTAL METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSE0580-01 (Bd2-05112009 - Water)

Reporting Units: mg/l

Chromium 5/13/20095/11/2009P9E1132 0.010 1E200.7 0.029

Project Manager

TestAmerica Phoenix

PSE0580

Tina Paulauskas

The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 2 of 5>


454-9303





Sampled:

Received:

05/11/09


Project ID:

PSE0580

08-227E

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS

METHOD BLANK/QC DATA

Data

Qualifiers

Batch: P9E1132 Extracted: 05/11/09

Blank Analyzed: 05/13/2009 (P9E1132-BLK1)

Chromium mg/l0.010ND

LCS Analyzed: 05/13/2009 (P9E1132-BS1)

Chromium 0.500 85-115mg/l0.0100.509 102

LCS Dup Analyzed: 05/13/2009 (P9E1132-BSD1)

Chromium 0.500 2085-115mg/l0.0100.515 103 1

Matrix Spike Analyzed: 05/13/2009 (P9E1132-MS1) Source: PSE0547-03

Chromium 0.500 75-125mg/l0.0100.486 0.00443 96

Matrix Spike Dup Analyzed: 05/13/2009 (P9E1132-MSD1) Source: PSE0547-03

Chromium 0.500 1075-125mg/l0.0100.483 0.00443 96 1

Project Manager

TestAmerica Phoenix

PSE0580

Tina Paulauskas




454-9303





Sampled:

Received:

05/11/09


Project ID:

PSE0580

08-227E

DATA QUALIFIERS AND DEFINITIONS

Relative Percent DifferenceRPD

Analyte NOT DETECTED at or above the reporting limit or MDL, if MDL is specified.ND

Project Manager

TestAmerica Phoenix

PSE0580

Tina Paulauskas




454-9303





Sampled:

Received:

05/11/09


Project ID:

PSE0580

08-227E

Certification Summary

Method Matrix Nelac Arizona

TestAmerica Phoenix

Water XE200.7

Nevada and NELAP provide analyte specific accreditations. Analyte specific information for TestAmerica may be obtained by contacting

the laboratory or visiting our website at www.testamericainc.com

Project Manager

TestAmerica Phoenix

PSE0580

Tina Paulauskas



Test America THE LEADER IN ENVIRONMENTAL TESTING

TAL-0013·550 (12/08)

Client t,me/AddressM /J £ ... ;n,.._ r;JtJ Mv 'lr 1/'e.e.i•J lM E z:. !&~It /fve .~ ~ ») &~f .P~u j/J /J?t:JJir>

Project Manager: jh,:Ae... iJe.7'Je.J

Sampler:

u;_rt.~ Lawrt.-.t.t-Sam pi{ Description

Sample· Matrix

/ld :1 -~~II :ltJIJ1 lit){)

"'~

Container Type

'-~/llllf Q

CHAIN OF CUSTODY FORM

.f\i.Phoenix- 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ. 85040 (602) 437-3340 FAX (602) 454-9303 [ ] Tucson -1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ ] Las Vegas- 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

' Project! PO Number: Analysis Required

tJt-)l? f

j Phone Number:(1?3) {}. 'fCJ -tS {) () £

Fax Number: @I?J) )._ytl-JJJ8 ~~ #of Sampling Sampling

Preservatives ~~

Cont. Date Time

l 1()5/Jt/11 Jtlo f,t>~T , ptY$l"&l't- X - 21

Date/Time: Date/Time: Turnaround Time: ~edBy: ·p~-- (r7eived By: ~.4

/.flitM1_ )Lj}d "/'"~. 7 same day

I 'Relinquisi!€d y Date/Time: Jfeceived By: Date/Time: 24 hours

/ 17/l I ; 48 hours

Relinquished By: Date/Time: ( ~tJtJ Lab By: ..... II Date/Time: Sample Integrity:

0 ll ~'1 /"-t~o .

/ intact

Page l of J

f/8'1Z858o

Special instructions

&s1 •'2.-r£.1-e•ve.. I

(Check)

72 hours

5 days

normal J(" (Check) .3 <.;.\_ 0 a:: . on ice

v .. Note: By rehnqUishmg samples to TestAmerrca, client agrees to pay for the serv1ces requested on th1s cham of custody form and any additiOnal analyses performed on this project. Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.


454-9303

LABORATORY REPORT




Attention: Brian Mcnamara Sampled:

Received:

Issued:

07/15/09

07/15/09

07/30/09 13:27







Project: PGAN 14682.013


CASE NARRATIVE


PSG0914-01 Bld 22-9-07152009 Soil

PSG0914-02 Bld 22-10.1-07152009 Oil

PSG0914-03 Bld 22-10.2-07152009 Soil

PSG0914-04 Bld 22-10.1-07152009 Oil

Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas

<Page 1 of 22>


454-9303




Attention: Brian Mcnamara

Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013






L3-Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery was above the

acceptance limits. Analyte not detected, data not impacted.

N1a- Vinyl Acetate - The MS and/or MSD were above the acceptance limits. See Blank Spike (LCS).

N1a- 2-Butanone - The LCS/LCSD and MSD recovered high and outside of acceptance limits for

2-Butanone. All associated samples are non-detect for 2-Butanone and therefore should not be impacted.



Reviewed By:

Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

EXTRACTABLE FUEL HYDROCARBONS (EPA 3510/8015B)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSG0914-04 (Bld 22-10.1-07152009 - Oil)

Reporting Units: mg/kg

DRO (C10-C22) 7/27/20097/21/2009P9G2113 25000 M397.1EPA 8015D 810000

ORO (C22-C32) 7/27/20097/21/2009P9G2113 75000 M397.1EPA 8015D 320000

Total (C10-C32) 7/27/20097/21/2009P9G2113 1000 0.971EPA 8015D 1100000

* S8Surrogate: o-terphenyl (70-130%)

Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

VOLATILE ORGANICS BY GC/MS (EPA 5035/8260B)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSG0914-01 (Bld 22-9-07152009 - Soil)

Reporting Units: ug/kg

7/16/20097/15/2009SW8260B1,1,1-Trichloroethane 50P9G1560 0.998ND

7/16/20097/15/2009SW8260B1,1,2,2-Tetrachloroethane 50P9G1560 0.998ND


7/16/20097/15/2009SW8260B1,1-Dichloroethane 50P9G1560 0.998ND

7/16/20097/15/2009SW8260B1,1-Dichloroethene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260B1,1-Dichloropropene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260B1,2,3-Trichlorobenzene 100P9G1560 0.998ND

7/16/20097/15/2009SW8260B1,2,3-Trichloropropane 100P9G1560 0.998ND

7/16/20097/15/2009SW8260B1,2,4-Trimethylbenzene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260B1,2-Dibromoethane (EDB) 50P9G1560 0.998ND

7/16/20097/15/2009SW8260B1,2-Dichlorobenzene 50P9G1560 0.998ND


7/16/20097/15/2009SW8260B1,2-Dichloropropane 50P9G1560 0.998ND






7/16/20097/15/2009SW8260B2-Butanone (MEK) 500P9G1560 L30.998ND

7/16/20097/15/2009SW8260B2-Chlorotoluene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260B2-Hexanone 250P9G1560 0.998ND


7/16/20097/15/2009SW8260B4-Methyl-2-pentanone (MIBK) 250P9G1560 0.998ND

7/16/20097/15/2009SW8260BAcetone 500P9G1560 L30.998ND

7/16/20097/15/2009SW8260BBenzene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260BBromobenzene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260BBromochloromethane 50P9G1560 0.998ND

7/16/20097/15/2009SW8260BBromodichloromethane 50P9G1560 0.998ND

7/16/20097/15/2009SW8260BBromoform 50P9G1560 L30.998ND

7/16/20097/15/2009SW8260BBromomethane 250P9G1560 0.998ND

7/16/20097/15/2009SW8260BCarbon tetrachloride 50P9G1560 0.998ND

7/16/20097/15/2009SW8260BChlorobenzene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260BChloroethane 50P9G1560 0.998ND

7/16/20097/15/2009SW8260BChloroform 50P9G1560 0.998ND

7/16/20097/15/2009SW8260BChloromethane 250P9G1560 0.998ND

7/16/20097/15/2009SW8260Bcis-1,2-Dichloroethene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260Bcis-1,3-Dichloropropene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260BDibromochloromethane 50P9G1560 0.998ND

7/16/20097/15/2009SW8260BDichlorodifluoromethane 50P9G1560 0.998ND

7/16/20097/15/2009SW8260BEthylbenzene 50P9G1560 0.998ND

Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSG0914-01 (Bld 22-9-07152009 - Soil) - cont.


7/16/20097/15/2009SW8260Bm,p-Xylenes 100P9G1560 0.998ND

7/16/20097/15/2009SW8260BMethyl-tert-butyl Ether (MTBE) 50P9G1560 0.998ND

7/16/20097/15/2009SW8260BMethylene Chloride 100P9G1560 0.998ND

7/16/20097/15/2009SW8260Bn-Butylbenzene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260Bn-Propylbenzene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260Bo-Xylene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260Bp-Isopropyltoluene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260Bsec-Butylbenzene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260BStyrene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260Btert-Butylbenzene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260BTetrachloroethene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260BToluene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260Btrans-1,2-Dichloroethene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260Btrans-1,3-Dichloropropene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260BTrichloroethene 50P9G1560 0.998ND

7/16/20097/15/2009SW8260BTrichlorofluoromethane 50P9G1560 0.998ND

7/16/20097/15/2009SW8260BVinyl Acetate 50P9G1560 0.998ND

7/16/20097/15/2009SW8260BVinyl chloride 50P9G1560 0.998ND

102 %Surrogate: Dibromofluoromethane (60-130%)

102 %Surrogate: Toluene-d8 (65-125%)

96 %Surrogate: 4-Bromofluorobenzene (65-125%)

Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSG0914-02 (Bld 22-10.1-07152009 - Oil)


7/20/20097/15/2009SW8260B1,1,1-Trichloroethane 2500P9G1560 50ND

7/20/20097/15/2009SW8260B1,1,2,2-Tetrachloroethane 2500P9G1560 50ND

7/20/20097/15/2009SW8260B1,1,2-Trichloroethane 2500P9G1560 50ND

7/20/20097/15/2009SW8260B1,1-Dichloroethane 2500P9G1560 50ND

7/20/20097/15/2009SW8260B1,1-Dichloroethene 2500P9G1560 50ND

7/20/20097/15/2009SW8260B1,1-Dichloropropene 2500P9G1560 50ND

7/20/20097/15/2009SW8260B1,2,3-Trichlorobenzene 5000P9G1560 50ND

7/20/20097/15/2009SW8260B1,2,3-Trichloropropane 5000P9G1560 50ND

7/20/20097/15/2009SW8260B1,2,4-Trimethylbenzene 2500P9G1560 50ND

7/20/20097/15/2009SW8260B1,2-Dibromoethane (EDB) 2500P9G1560 50ND

7/20/20097/15/2009SW8260B1,2-Dichlorobenzene 2500P9G1560 50ND

7/20/20097/15/2009SW8260B1,2-Dichloroethane 2500P9G1560 50ND

7/20/20097/15/2009SW8260B1,2-Dichloropropane 2500P9G1560 50ND

7/20/20097/15/2009SW8260B1,3,5-Trimethylbenzene 2500P9G1560 50ND





7/20/20097/15/2009SW8260B2-Butanone (MEK) 25000P9G1560 L350ND

7/20/20097/15/2009SW8260B2-Chlorotoluene 2500P9G1560 50ND

7/20/20097/15/2009SW8260B2-Hexanone 12000P9G1560 50ND

7/20/20097/15/2009SW8260B4-Chlorotoluene 2500P9G1560 50ND

7/20/20097/15/2009SW8260B4-Methyl-2-pentanone (MIBK) 12000P9G1560 50ND

7/20/20097/15/2009SW8260BAcetone 25000P9G1560 L350ND

7/20/20097/15/2009SW8260BBenzene 2500P9G1560 50ND

7/20/20097/15/2009SW8260BBromobenzene 2500P9G1560 50ND

7/20/20097/15/2009SW8260BBromochloromethane 2500P9G1560 50ND

7/20/20097/15/2009SW8260BBromodichloromethane 2500P9G1560 50ND

7/20/20097/15/2009SW8260BBromoform 2500P9G1560 L350ND

7/20/20097/15/2009SW8260BBromomethane 12000P9G1560 50ND

7/20/20097/15/2009SW8260BCarbon tetrachloride 2500P9G1560 50ND

7/20/20097/15/2009SW8260BChlorobenzene 2500P9G1560 50ND

7/20/20097/15/2009SW8260BChloroethane 2500P9G1560 50ND

7/20/20097/15/2009SW8260BChloroform 2500P9G1560 50ND

7/20/20097/15/2009SW8260BChloromethane 12000P9G1560 50ND

7/20/20097/15/2009SW8260Bcis-1,2-Dichloroethene 2500P9G1560 50ND

7/20/20097/15/2009SW8260Bcis-1,3-Dichloropropene 2500P9G1560 50ND

7/20/20097/15/2009SW8260BDibromochloromethane 2500P9G1560 50ND

7/20/20097/15/2009SW8260BDichlorodifluoromethane 2500P9G1560 50ND

7/20/20097/15/2009SW8260BEthylbenzene 2500P9G1560 50ND

Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSG0914-02 (Bld 22-10.1-07152009 - Oil) - cont.


7/20/20097/15/2009SW8260Bm,p-Xylenes 5000P9G1560 50ND

7/20/20097/15/2009SW8260BMethyl-tert-butyl Ether (MTBE) 2500P9G1560 50ND

7/20/20097/15/2009SW8260BMethylene Chloride 5000P9G1560 50ND

7/20/20097/15/2009SW8260Bn-Butylbenzene 2500P9G1560 50ND

7/20/20097/15/2009SW8260Bn-Propylbenzene 2500P9G1560 50ND

7/20/20097/15/2009SW8260Bo-Xylene 2500P9G1560 50ND

7/20/20097/15/2009SW8260Bp-Isopropyltoluene 2500P9G1560 50ND

7/20/20097/15/2009SW8260Bsec-Butylbenzene 2500P9G1560 50ND

7/20/20097/15/2009SW8260BStyrene 2500P9G1560 50ND

7/20/20097/15/2009SW8260Btert-Butylbenzene 2500P9G1560 50ND

7/20/20097/15/2009SW8260BTetrachloroethene 2500P9G1560 50ND

7/20/20097/15/2009SW8260BToluene 2500P9G1560 50ND

7/20/20097/15/2009SW8260Btrans-1,2-Dichloroethene 2500P9G1560 50ND

7/20/20097/15/2009SW8260Btrans-1,3-Dichloropropene 2500P9G1560 50ND

7/20/20097/15/2009SW8260BTrichloroethene 2500P9G1560 50ND

7/20/20097/15/2009SW8260BTrichlorofluoromethane 2500P9G1560 50ND

7/20/20097/15/2009SW8260BVinyl Acetate 2500P9G1560 50ND

7/20/20097/15/2009SW8260BVinyl chloride 2500P9G1560 50ND

25000 % S8Surrogate: Dibromofluoromethane (60-130%)

19900 % S8Surrogate: Toluene-d8 (65-125%)

20100 % S8Surrogate: 4-Bromofluorobenzene (65-125%)

Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSG0914-03 (Bld 22-10.2-07152009 - Soil)



7/16/20097/15/2009SW8260B1,1,2,2-Tetrachloroethane 50P9G1560 0.992ND



7/16/20097/15/2009SW8260B1,1-Dichloroethene 50P9G1560 0.992ND

7/16/20097/15/2009SW8260B1,1-Dichloropropene 50P9G1560 0.992ND

7/16/20097/15/2009SW8260B1,2,3-Trichlorobenzene 100P9G1560 0.992ND

7/16/20097/15/2009SW8260B1,2,3-Trichloropropane 100P9G1560 0.992ND


7/16/20097/15/2009SW8260B1,2-Dibromoethane (EDB) 50P9G1560 0.992ND









7/16/20097/15/2009SW8260B2-Butanone (MEK) 500P9G1560 L30.992ND


7/16/20097/15/2009SW8260B2-Hexanone 250P9G1560 0.992ND


7/16/20097/15/2009SW8260B4-Methyl-2-pentanone (MIBK) 250P9G1560 0.992ND

7/16/20097/15/2009SW8260BAcetone 500P9G1560 L30.992ND

7/16/20097/15/2009SW8260BBenzene 50P9G1560 0.992ND

7/16/20097/15/2009SW8260BBromobenzene 50P9G1560 0.992ND

7/16/20097/15/2009SW8260BBromochloromethane 50P9G1560 0.992ND

7/16/20097/15/2009SW8260BBromodichloromethane 50P9G1560 0.992ND

7/16/20097/15/2009SW8260BBromoform 50P9G1560 L30.992ND

7/16/20097/15/2009SW8260BBromomethane 250P9G1560 0.992ND

7/16/20097/15/2009SW8260BCarbon tetrachloride 50P9G1560 0.992ND

7/16/20097/15/2009SW8260BChlorobenzene 50P9G1560 0.992ND

7/16/20097/15/2009SW8260BChloroethane 50P9G1560 0.992ND

7/16/20097/15/2009SW8260BChloroform 50P9G1560 0.992ND

7/16/20097/15/2009SW8260BChloromethane 250P9G1560 0.992ND

7/16/20097/15/2009SW8260Bcis-1,2-Dichloroethene 50P9G1560 0.992ND

7/16/20097/15/2009SW8260Bcis-1,3-Dichloropropene 50P9G1560 0.992ND

7/16/20097/15/2009SW8260BDibromochloromethane 50P9G1560 0.992ND

7/16/20097/15/2009SW8260BDichlorodifluoromethane 50P9G1560 0.992ND

7/16/20097/15/2009SW8260BEthylbenzene 50P9G1560 0.992ND

Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSG0914-03 (Bld 22-10.2-07152009 - Soil) - cont.


7/16/20097/15/2009SW8260Bm,p-Xylenes 100P9G1560 0.992ND

7/16/20097/15/2009SW8260BMethyl-tert-butyl Ether (MTBE) 50P9G1560 0.992ND

7/16/20097/15/2009SW8260BMethylene Chloride 100P9G1560 0.992ND

7/16/20097/15/2009SW8260Bn-Butylbenzene 50P9G1560 0.992ND

7/16/20097/15/2009SW8260Bn-Propylbenzene 50P9G1560 0.992ND

7/16/20097/15/2009SW8260Bo-Xylene 50P9G1560 0.992ND

7/16/20097/15/2009SW8260Bp-Isopropyltoluene 50P9G1560 0.992ND

7/16/20097/15/2009SW8260Bsec-Butylbenzene 50P9G1560 0.992ND

7/16/20097/15/2009SW8260BStyrene 50P9G1560 0.992ND

7/16/20097/15/2009SW8260Btert-Butylbenzene 50P9G1560 0.992ND

7/16/20097/15/2009SW8260BTetrachloroethene 50P9G1560 0.992ND

7/16/20097/15/2009SW8260BToluene 50P9G1560 0.992ND

7/16/20097/15/2009SW8260Btrans-1,2-Dichloroethene 50P9G1560 0.992ND

7/16/20097/15/2009SW8260Btrans-1,3-Dichloropropene 50P9G1560 0.992ND

7/16/20097/15/2009SW8260BTrichloroethene 50P9G1560 0.992ND

7/16/20097/15/2009SW8260BTrichlorofluoromethane 50P9G1560 0.992ND

7/16/20097/15/2009SW8260BVinyl Acetate 50P9G1560 0.992ND

7/16/20097/15/2009SW8260BVinyl chloride 50P9G1560 0.992ND

97 %Surrogate: Dibromofluoromethane (60-130%)

85 %Surrogate: Toluene-d8 (65-125%)

80 %Surrogate: 4-Bromofluorobenzene (65-125%)

Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013

SHORT HOLD TIME DETAIL REPORT

Date/Time

Analyzed

Date/Time

Extracted

Date/Time

Sampled

Date/Time

Received

Hold Time

(in days)

Sample ID: Bld 22-9-07152009 (PSG0914-01) - Soil

2 07/15/2009 12:26 07/15/2009 16:54 07/15/2009 17:41 07/16/2009 06:25SW8260B

Sample ID: Bld 22-10.1-07152009 (PSG0914-02) - Soil

2 07/15/2009 14:03 07/15/2009 16:54 07/15/2009 17:41 07/20/2009 16:54SW8260B

Sample ID: Bld 22-10.2-07152009 (PSG0914-03) - Soil

2 07/15/2009 14:06 07/15/2009 16:54 07/15/2009 17:41 07/16/2009 12:49SW8260B

Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

EXTRACTABLE FUEL HYDROCARBONS (EPA 3510/8015B)


Data

Qualifiers

Batch: P9G2113 Extracted: 07/21/09

Blank Analyzed: 07/24/2009 (P9G2113-BLK1)

DRO (C10-C22) mg/kg250ND

ORO (C22-C32) mg/kg750ND

Total (C10-C32) mg/kg1000ND

500 70-130Surrogate: o-terphenyl mg/kg516 103

LCS Analyzed: 07/24/2009 (P9G2113-BS1)

DRO (C10-C22) 2000 70-130mg/kg2502530 126

ORO (C22-C32) 4000 70-130mg/kg7504660 116


LCS Dup Analyzed: 07/24/2009 (P9G2113-BSD1)

DRO (C10-C22) 2000 2070-130mg/kg2502550 127 1

ORO (C22-C32) 4000 2070-130mg/kg7504910 123 5


Matrix Spike Analyzed: 07/27/2009 (P9G2113-MS1) Source: PSG0914-04

DRO (C10-C22) 1940 70-130mg/kg25000872000 M3812000 3060

ORO (C22-C32) 3880 70-130mg/kg75000326000 M3316000 267

485 70-130Surrogate: o-terphenyl mg/kg0.00 S8

Matrix Spike Dup Analyzed: 07/27/2009 (P9G2113-MSD1) Source: PSG0914-04

DRO (C10-C22) 1920 2070-130mg/kg25000788000 M3812000 -1250 10

ORO (C22-C32) 3850 2070-130mg/kg75000289000 M3316000 -716 12

481 70-130Surrogate: o-terphenyl mg/kg0.00 S8

Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



1,1,1-Trichloroethane ug/kg50ND

1,1,2,2-Tetrachloroethane ug/kg50ND

1,1,2-Trichloroethane ug/kg50ND

1,1-Dichloroethane ug/kg50ND

1,1-Dichloroethene ug/kg50ND

1,1-Dichloropropene ug/kg50ND

1,2,3-Trichlorobenzene ug/kg100ND

1,2,3-Trichloropropane ug/kg100ND

1,2,4-Trimethylbenzene ug/kg50ND

1,2-Dibromoethane (EDB) ug/kg50ND

1,2-Dichlorobenzene ug/kg50ND

1,2-Dichloroethane ug/kg50ND

1,2-Dichloropropane ug/kg50ND

1,3,5-Trimethylbenzene ug/kg50ND





2-Butanone (MEK) ug/kg500ND

2-Chlorotoluene ug/kg50ND

2-Hexanone ug/kg250ND

4-Chlorotoluene ug/kg50ND

4-Methyl-2-pentanone (MIBK) ug/kg250ND

Acetone ug/kg500ND

Benzene ug/kg50ND

Bromobenzene ug/kg50ND

Bromochloromethane ug/kg50ND V1

Bromodichloromethane ug/kg50ND

Bromoform ug/kg50ND

Bromomethane ug/kg250ND

Carbon tetrachloride ug/kg50ND

Chlorobenzene ug/kg50ND

Chloroethane ug/kg50ND

Chloroform ug/kg50ND

Chloromethane ug/kg250ND

Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



cis-1,2-Dichloroethene ug/kg50ND

cis-1,3-Dichloropropene ug/kg50ND

Dibromochloromethane ug/kg50ND

Dichlorodifluoromethane ug/kg50ND

Ethylbenzene ug/kg50ND

m,p-Xylenes ug/kg100ND

Methyl-tert-butyl Ether (MTBE) ug/kg50ND

Methylene Chloride ug/kg100ND

n-Butylbenzene ug/kg50ND

n-Propylbenzene ug/kg50ND

o-Xylene ug/kg50ND

p-Isopropyltoluene ug/kg50ND

sec-Butylbenzene ug/kg50ND

Styrene ug/kg50ND

tert-Butylbenzene ug/kg50ND

Tetrachloroethene ug/kg50ND

Toluene ug/kg50ND

trans-1,2-Dichloroethene ug/kg50ND

trans-1,3-Dichloropropene ug/kg50ND

Trichloroethene ug/kg50ND

Trichlorofluoromethane ug/kg50ND

Vinyl Acetate ug/kg50ND

Vinyl chloride ug/kg50ND

1250 60-130Surrogate: Dibromofluoromethane ug/kg1340 107

1250 65-125Surrogate: Toluene-d8 ug/kg1120 90

1250 65-125Surrogate: 4-Bromofluorobenzene ug/kg1170 94


1,1,1-Trichloroethane 1240 75-120ug/kg501280 103

1,1,2,2-Tetrachloroethane 1240 60-125ug/kg501330 107

1,1,2-Trichloroethane 1240 65-125ug/kg501480 119

1,1-Dichloroethane 1240 70-125ug/kg501370 110

1,1-Dichloroethene 1240 50-135ug/kg501160 93

1,1-Dichloropropene 1240 75-120ug/kg501210 97

1,2,3-Trichlorobenzene 1240 55-140ug/kg1001540 124

1,2,3-Trichloropropane 1240 60-130ug/kg1001300 104

Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



1,2,4-Trimethylbenzene 1240 75-120ug/kg501270 103

1,2-Dibromoethane (EDB) 1240 70-120ug/kg501420 115

1,2-Dichlorobenzene 1240 80-120ug/kg501350 108

1,2-Dichloroethane 1240 70-130ug/kg501520 123

1,2-Dichloropropane 1240 80-120ug/kg501460 117

1,3,5-Trimethylbenzene 1240 80-130ug/kg501230 99





2-Butanone (MEK) 1240 40-150ug/kg5002030 L3164

2-Chlorotoluene 1240 80-120ug/kg501190 96

2-Hexanone 1240 20-150ug/kg2501450 117

4-Chlorotoluene 1240 80-120ug/kg501250 101

4-Methyl-2-pentanone (MIBK) 1240 50-130ug/kg2501590 128

Acetone 1240 10-150ug/kg5001690 137

Benzene 1240 75-120ug/kg501280 103

Bromobenzene 1240 80-120ug/kg501310 105

Bromochloromethane 1240 75-125ug/kg501530 V1124

Bromodichloromethane 1240 75-120ug/kg501430 115

Bromoform 1240 60-120ug/kg501500 L3121

Bromomethane 1240 20-140ug/kg2501130 91

Carbon tetrachloride 1240 70-130ug/kg501260 102

Chlorobenzene 1240 80-120ug/kg501290 104

Chloroethane 1240 10-130ug/kg501130 91

Chloroform 1240 75-120ug/kg501420 114

Chloromethane 1240 25-140ug/kg2501020 82

cis-1,2-Dichloroethene 1240 70-125ug/kg501290 104

cis-1,3-Dichloropropene 1240 75-125ug/kg501450 117

Dibromochloromethane 1240 75-120ug/kg501440 116

Dichlorodifluoromethane 1240 10-150ug/kg50676 55

Ethylbenzene 1240 80-120ug/kg501240 100

m,p-Xylenes 1240 60-140ug/kg1001250 101

Methyl-tert-butyl Ether (MTBE) 1240 65-130ug/kg501510 121

Methylene Chloride 1240 65-125ug/kg1001330 107

Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



n-Butylbenzene 1240 65-130ug/kg501250 101

n-Propylbenzene 1240 75-130ug/kg501220 98

o-Xylene 1240 80-120ug/kg501250 101

p-Isopropyltoluene 1240 75-130ug/kg501220 99

sec-Butylbenzene 1240 75-125ug/kg501170 94

Styrene 1240 80-120ug/kg501340 108

tert-Butylbenzene 1240 80-120ug/kg501190 96

Tetrachloroethene 1240 70-130ug/kg501200 97

Toluene 1240 75-120ug/kg501310 106

trans-1,2-Dichloroethene 1240 70-130ug/kg501280 103

trans-1,3-Dichloropropene 1240 65-130ug/kg501500 121

Trichloroethene 1240 80-120ug/kg501300 105

Trichlorofluoromethane 1240 50-150ug/kg501050 85

Vinyl Acetate 1240 35-150ug/kg501490 120

Vinyl chloride 1240 10-150ug/kg50414 33





1,1,1-Trichloroethane 1250 1575-120ug/kg501160 94 9

1,1,2,2-Tetrachloroethane 1250 3060-125ug/kg501190 96 11


1,1-Dichloroethane 1250 2070-125ug/kg501250 101 9

1,1-Dichloroethene 1250 2050-135ug/kg501050 84 10

1,1-Dichloropropene 1250 1575-120ug/kg501050 84 14

1,2,3-Trichlorobenzene 1250 2555-140ug/kg1001310 105 16

1,2,3-Trichloropropane 1250 3060-130ug/kg1001180 95 9

1,2,4-Trimethylbenzene 1250 1575-120ug/kg501150 92 11

1,2-Dibromoethane (EDB) 1250 2070-120ug/kg501310 105 8

1,2-Dichlorobenzene 1250 2080-120ug/kg501200 97 11

1,2-Dichloroethane 1250 2070-130ug/kg501410 114 7

1,2-Dichloropropane 1250 2080-120ug/kg501310 105 11

1,3,5-Trimethylbenzene 1250 1580-130ug/kg501120 90 9



Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers





2-Butanone (MEK) 1250 3540-150ug/kg5001910 L3153 6

2-Chlorotoluene 1250 1580-120ug/kg501090 87 9

2-Hexanone 1250 3520-150ug/kg2501460 117 0

4-Chlorotoluene 1250 1580-120ug/kg501150 92 9

4-Methyl-2-pentanone (MIBK) 1250 3550-130ug/kg2501370 110 15

Acetone 1250 3510-150ug/kg5002010 L3162 17

Benzene 1250 1575-120ug/kg501160 93 10

Bromobenzene 1250 2080-120ug/kg501180 95 10

Bromochloromethane 1250 2075-125ug/kg501410 V1113 9

Bromodichloromethane 1250 1575-120ug/kg501300 105 9

Bromoform 1250 2560-120ug/kg501290 104 15

Bromomethane 1250 3520-140ug/kg2501040 83 8

Carbon tetrachloride 1250 2070-130ug/kg501110 89 13

Chlorobenzene 1250 1580-120ug/kg501190 96 8

Chloroethane 1250 3010-130ug/kg501040 84 8

Chloroform 1250 2075-120ug/kg501320 106 7

Chloromethane 1250 3525-140ug/kg250934 75 8

cis-1,2-Dichloroethene 1250 1570-125ug/kg501210 97 7

cis-1,3-Dichloropropene 1250 1575-125ug/kg501310 105 10

Dibromochloromethane 1250 2075-120ug/kg501370 110 5

Dichlorodifluoromethane 1250 3510-150ug/kg50619 50 9

Ethylbenzene 1250 1580-120ug/kg501140 92 9

m,p-Xylenes 1250 1560-140ug/kg1001150 92 8

Methyl-tert-butyl Ether (MTBE) 1250 2065-130ug/kg501400 112 7

Methylene Chloride 1250 2065-125ug/kg1001200 97 10

n-Butylbenzene 1250 2065-130ug/kg501090 88 14

n-Propylbenzene 1250 1575-130ug/kg501110 89 10

o-Xylene 1250 1580-120ug/kg501140 92 9

p-Isopropyltoluene 1250 1575-130ug/kg501120 90 9

sec-Butylbenzene 1250 1575-125ug/kg501050 84 11

Styrene 1250 1580-120ug/kg501250 101 7

tert-Butylbenzene 1250 1580-120ug/kg501070 86 10

Tetrachloroethene 1250 1570-130ug/kg501130 91 6

Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Toluene 1250 1575-120ug/kg501190 96 10

trans-1,2-Dichloroethene 1250 2070-130ug/kg501180 95 8

trans-1,3-Dichloropropene 1250 2065-130ug/kg501350 109 11

Trichloroethene 1250 1580-120ug/kg501180 95 9

Trichlorofluoromethane 1250 2550-150ug/kg50957 77 10

Vinyl Acetate 1250 3535-150ug/kg501180 95 23

Vinyl chloride 1250 3510-150ug/kg50356 29 15





1,1,1-Trichloroethane 6130 50-125ug/kg2506220 ND 102

1,1,2,2-Tetrachloroethane 6130 50-130ug/kg2506030 ND 98


1,1-Dichloroethane 6130 55-125ug/kg2506680 ND 109

1,1-Dichloroethene 6130 25-140ug/kg2505580 ND 91

1,1-Dichloropropene 6130 55-125ug/kg2505680 ND 93

1,2,3-Trichlorobenzene 6130 35-140ug/kg4907250 ND 118

1,2,3-Trichloropropane 6130 35-140ug/kg4905880 ND 96

1,2,4-Trimethylbenzene 6130 50-130ug/kg2506030 ND 98

1,2-Dibromoethane (EDB) 6130 55-120ug/kg2506670 ND 109

1,2-Dichlorobenzene 6130 60-120ug/kg2506360 ND 104

1,2-Dichloroethane 6130 55-130ug/kg2507200 ND 117

1,2-Dichloropropane 6130 60-120ug/kg2506860 ND 112

1,3,5-Trimethylbenzene 6130 45-135ug/kg2506000 ND 98




2,2-Dichloropropane 6130 45-130ug/kg4905530 ND 90

2-Butanone (MEK) 6130 40-150ug/kg25008720 1140 124

2-Chlorotoluene 6130 60-120ug/kg2505740 ND 94

2-Hexanone 6130 20-150ug/kg12006610 ND 108

4-Chlorotoluene 6130 55-130ug/kg2505970 ND 97

4-Methyl-2-pentanone (MIBK) 6130 40-130ug/kg12007250 ND 118

Acetone 6130 10-150ug/kg25008690 ND 142

Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Benzene 6130 55-120ug/kg2506200 ND 101

Bromobenzene 6130 60-125ug/kg2506180 ND 101

Bromochloromethane 6130 50-135ug/kg2507120 V1ND 116

Bromodichloromethane 6130 60-120ug/kg2506680 ND 109

Bromoform 6130 40-125ug/kg2506440 ND 105

Bromomethane 6130 10-140ug/kg12005650 ND 92

Carbon tetrachloride 6130 40-135ug/kg2506030 ND 98

Chlorobenzene 6130 65-120ug/kg2506340 ND 103

Chloroethane 6130 10-140ug/kg2505770 ND 94

Chloroform 6130 60-125ug/kg2506930 ND 113

Chloromethane 6130 10-140ug/kg12004880 ND 80

cis-1,2-Dichloroethene 6130 55-125ug/kg2506400 ND 105

cis-1,3-Dichloropropene 6130 55-120ug/kg2506850 ND 112

Dibromochloromethane 6130 55-125ug/kg2506980 ND 114

Dichlorodifluoromethane 6130 10-150ug/kg2503110 ND 51

Ethylbenzene 6130 60-125ug/kg2506280 ND 102

m,p-Xylenes 6130 55-125ug/kg4906240 ND 102

Methyl-tert-butyl Ether (MTBE) 6130 50-130ug/kg2506940 95.2 112

Methylene Chloride 6130 50-120ug/kg4906270 ND 102

n-Butylbenzene 6130 40-135ug/kg2505920 ND 97

n-Propylbenzene 6130 55-130ug/kg2505860 ND 96

o-Xylene 6130 60-125ug/kg2506200 ND 101

p-Isopropyltoluene 6130 45-135ug/kg2505870 ND 96

sec-Butylbenzene 6130 50-130ug/kg2505650 ND 92

Styrene 6130 55-125ug/kg2506520 97.6 105

tert-Butylbenzene 6130 55-125ug/kg2505730 ND 93

Tetrachloroethene 6130 60-130ug/kg2506070 ND 99

Toluene 6130 55-125ug/kg2506370 ND 104

trans-1,2-Dichloroethene 6130 50-130ug/kg2506230 ND 102

trans-1,3-Dichloropropene 6130 55-125ug/kg2507090 ND 116

Trichloroethene 6130 40-145ug/kg2506110 ND 100

Trichlorofluoromethane 6130 20-150ug/kg2505170 ND 84

Vinyl Acetate 6130 10-150ug/kg2509860 N1aND 161

Vinyl chloride 6130 10-150ug/kg2502170 ND 35


Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers






1,1,1-Trichloroethane 6190 1550-125ug/kg2506270 ND 101 1

1,1,2,2-Tetrachloroethane 6190 2550-130ug/kg2506490 ND 105 7

1,1,2-Trichloroethane 6190 2555-120ug/kg2507370 819 106 5

1,1-Dichloroethane 6190 2555-125ug/kg2506870 ND 111 3

1,1-Dichloroethene 6190 3525-140ug/kg2505580 ND 90 0

1,1-Dichloropropene 6190 2555-125ug/kg2505740 ND 93 1

1,2,3-Trichlorobenzene 6190 3035-140ug/kg5007100 ND 115 2

1,2,3-Trichloropropane 6190 3535-140ug/kg5006410 ND 104 9

1,2,4-Trimethylbenzene 6190 2050-130ug/kg2506000 ND 97 1

1,2-Dibromoethane (EDB) 6190 2555-120ug/kg2507010 ND 113 5

1,2-Dichlorobenzene 6190 2560-120ug/kg2506530 ND 106 3

1,2-Dichloroethane 6190 2555-130ug/kg2507720 ND 125 7

1,2-Dichloropropane 6190 2560-120ug/kg2507030 ND 114 3

1,3,5-Trimethylbenzene 6190 2045-135ug/kg2505950 ND 96 1


1,3-Dichloropropane 6190 2560-120ug/kg2506800 174 107 4


2,2-Dichloropropane 6190 2545-130ug/kg5005540 ND 90 0

2-Butanone (MEK) 6190 3540-150ug/kg250011100 N1a1140 162 24

2-Chlorotoluene 6190 2060-120ug/kg2505650 ND 91 2

2-Hexanone 6190 3520-150ug/kg12007880 ND 127 18

4-Chlorotoluene 6190 2055-130ug/kg2505980 ND 97 0

4-Methyl-2-pentanone (MIBK) 6190 3040-130ug/kg12007810 ND 126 7

Acetone 6190 3510-150ug/kg25008680 ND 140 0

Benzene 6190 2555-120ug/kg2506210 ND 100 0

Bromobenzene 6190 2560-125ug/kg2506240 ND 101 1

Bromochloromethane 6190 3050-135ug/kg2507330 V1ND 119 3

Bromodichloromethane 6190 2060-120ug/kg2506990 ND 113 5

Bromoform 6190 3540-125ug/kg2506750 ND 109 5

Bromomethane 6190 3510-140ug/kg12005610 ND 91 1

Carbon tetrachloride 6190 3040-135ug/kg2506070 ND 98 1

Chlorobenzene 6190 2065-120ug/kg2506260 ND 101 1

Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Chloroethane 6190 3510-140ug/kg2505660 ND 91 2

Chloroform 6190 2560-125ug/kg2507070 ND 114 2

Chloromethane 6190 3510-140ug/kg12005050 ND 82 3

cis-1,2-Dichloroethene 6190 2555-125ug/kg2506500 ND 105 2

cis-1,3-Dichloropropene 6190 2055-120ug/kg2507180 ND 116 5

Dibromochloromethane 6190 3055-125ug/kg2507110 ND 115 2

Dichlorodifluoromethane 6190 3510-150ug/kg2503350 ND 54 7

Ethylbenzene 6190 2060-125ug/kg2506080 ND 98 3

m,p-Xylenes 6190 2055-125ug/kg5006090 ND 98 2

Methyl-tert-butyl Ether (MTBE) 6190 3550-130ug/kg2507430 95.2 119 7

Methylene Chloride 6190 3050-120ug/kg5006560 ND 106 4

n-Butylbenzene 6190 2540-135ug/kg2505810 ND 94 2

n-Propylbenzene 6190 2055-130ug/kg2505820 ND 94 1

o-Xylene 6190 3060-125ug/kg2506050 ND 98 2

p-Isopropyltoluene 6190 2545-135ug/kg2505770 ND 93 2

sec-Butylbenzene 6190 2050-130ug/kg2505620 ND 91 1

Styrene 6190 2055-125ug/kg2506510 97.6 104 0

tert-Butylbenzene 6190 2555-125ug/kg2505660 ND 91 1

Tetrachloroethene 6190 2060-130ug/kg2505900 ND 95 3

Toluene 6190 3555-125ug/kg2506310 ND 102 1

trans-1,2-Dichloroethene 6190 2550-130ug/kg2506320 ND 102 1

trans-1,3-Dichloropropene 6190 2555-125ug/kg2507420 ND 120 5

Trichloroethene 6190 3540-145ug/kg2506380 ND 103 4

Trichlorofluoromethane 6190 3520-150ug/kg2505250 ND 85 2

Vinyl Acetate 6190 3510-150ug/kg2508780 ND 142 12

Vinyl chloride 6190 3510-150ug/kg2501730 ND 28 22




Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013


L3 The associated blank spike recovery was above method acceptance limits.

M3 The spike recovery value is unusable since the analyte concentration in the sample is disproportionate to the spike

level. The associated blank spike recovery was acceptable.

N1 See case narrative.

S8 The analysis of the sample required a dilution such that the surrogate recovery calculation does not provide usuful

information. The associated blank spike recovery was acceptable.

V1 CCV recovery was above method acceptance limits. This target analyte was not detected in the sample.



ADDITIONAL COMMENTS

For Extractable Fuel Hydrocarbons (EFH, DRO, ORO) :

Unless otherwise noted, Extractable Fuel Hydrocarbons (EFH, DRO, ORO) are quantitated against a Diesel Fuel Standard.

Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas




454-9303





Sampled:

Received:

07/15/09


Project ID:

PSG0914

PGAN 14682.013



TestAmerica Phoenix

OilEPA 8015D

Soil XSW8260B



Project Manager

TestAmerica Phoenix

PSG0914

Tina Paulauskas



Test America I


. ,L){;Phoenix- 4625 E. Gatton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303

THE LEADER IN ENVIRONMENTAL TESTING [ ] Tucson -1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803

Page--lot I [ ] Las Vegas- 2520 E. Sunset, Suite 3, Las Vegas, NV 891.20 (702) 798-3620 FAX (702) 798-3621 TAL-0013-550 (12/08)

Client Name=: Project/ PO Number: Analysis Required

19h-.t.£ fJ:_ *- ]1{, ft?/lV $ 7?? JS ... d Vl'?. .,._ u .. fl'¢4 s- e.

5ufhJJ'J~ /1-l ~t;258 J'f(pt),t11} Project Manager:}jt·ltt"> f!J~ni!il'(Yltill'il Phone Numbe(~J'gJ.U- &Jt3

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Sampler: h J, Fax Number&tgJ''j5- J).'f5 ~~ I --- •. ~JVV' Vtir't. -GJ.v(t..-~~ ~ por~ · J T~t:~ Sam$e Description

Sample Container #of Sampling Sampling Preservatives } Special Instructions Matrix Ty~,e Cont. Date Time ~ ,/'"':i_ I L I

f} fJ 21 ~'1-J?JS') IJJ~ }t;tl ,4/~tr 1. tiJ/6/IYi JJJ6 Jrt~ .... e. )C r__x iCJl rvf---c \ ~ tM.- A-xi-r.:ri w:lft"- lfl rM f/J 1)_-}tp.j -f?lf )b01 Jrw.rd v II I I I '1 tJJ 1 I --6 L ~11fbw f!JT ~11 Jl-J~.).-o?IS 2tJIJCf 1~;( Vr\ Jt- ¥ J lf/J ~ :v· w- ---6 ~- ( uld/.~Y e);,.Pfwdl.fJ. ~ ~~

I

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~~dBy:~ Date/[Time: Received By: Date/Time: Turnaround Time: (Check) . ;...,._,._

t~?/1>/41 J~>Lf(' 7 _.·:/- ~-~.? same day 72 hours

~Ffelinqui~ Date/\Time:

/ -1\eceived By: Date/Time: 24 hours 2( 5 days

I 48 hours normal

Relinquished By: · .Date/\Time: .( -::ivl)~ Date/Time:

/Co(51 Sampl~grity: (Check)

;( /I !SI()Cf intact on ice I ~ I I

Note: By relinqu1shmg samples to TestAmenca, cl1en' agrees to pay for the serv1ces requested on th1s chain of custody form and any additional analyses performed on this project. Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.

- I ___ \!_ ------------'-------------c-~ __ _,_. ---


454-9303

LABORATORY REPORT




Attention: Brian Mcnamara Sampled:

Received:

Issued:

08/21/09

08/21/09

09/14/09 16:03







Project: 14682.013 PGAN


CASE NARRATIVE


PSH1228-01 Bld 1 Tank-08212009 Water

PSH1228-02 TB001-08212009 Water




Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas

<Page 1 of 53>


454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN


HOLDING TIMES: Not all holding times were met. Results were qualified where the sample analysis did not occur within

method specified holding time requirements.

H4-Sample was extracted past required extraction holding time, but analyzed within analysis holding time.





L4-Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery was below

acceptance limits.

N1-8270 - Several analytes recovered low and outside of acceptance limits in the LCS/LCSD. The sample

was re-extracted outside of hold time, but analyzed within hold time to confirm the initial results.

R1-The RPD exceeded the acceptance limit.

S10-Surrogate recovery was above acceptance limits.


SUBCONTRACTED: Refer to the last page for specific subcontract laboratory information included in this report.

Reviewed By:

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSH1228-01 (Bld 1 Tank-08212009 - Water)

Reporting Units: ug/l

9/4/20099/4/2009SW8260B1,1,2,2-Tetrachloroethane 1.0P9I0414 1ND

9/4/20099/4/2009SW8260B1,1-Dichloroethene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260B1,2-Dichloropropane 1.0P9I0414 1ND

9/4/20099/4/2009SW8260B2-Butanone (MEK) 5.0P9I0414 1ND

Acetone 9/4/20099/4/2009P9I0414 200 10SW8260B 280

9/4/20099/4/2009SW8260BBenzene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BCarbon tetrachloride 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BChloroform 1.0P9I0414 1ND

9/4/20099/4/2009SW8260Bcis-1,2-Dichloroethene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BEthylbenzene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260Bm,p-Xylenes 2.0P9I0414 1ND

9/4/20099/4/2009SW8260BMethylene Chloride 2.0P9I0414 1ND

9/4/20099/4/2009SW8260Bo-Xylene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BTetrachloroethene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BToluene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260Btrans-1,2-Dichloroethene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BTrichloroethene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BTrichlorofluoromethane 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BVinyl chloride 1.0P9I0414 1ND

9/4/20099/4/2009SW8260B1,1,1-Trichloroethane 1.0P9I0414 1ND


9/4/20099/4/2009SW8260B1,1-Dichloroethane 1.0P9I0414 1ND

9/4/20099/4/2009SW8260B1,1-Dichloropropene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260B1,2,3-Trichlorobenzene 2.0P9I0414 1ND

9/4/20099/4/2009SW8260B1,2,3-Trichloropropane 2.0P9I0414 1ND


9/4/20099/4/2009SW8260B1,2,4-Trimethylbenzene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260B1,2-Dibromoethane (EDB) 1.0P9I0414 1ND

9/4/20099/4/2009SW8260B1,2-Dichlorobenzene 1.0P9I0414 1ND







9/4/20099/4/2009SW8260B2-Chlorotoluene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260B2-Hexanone 5.0P9I0414 1ND


9/4/20099/4/2009SW8260B4-Methyl-2-pentanone (MIBK) 5.0P9I0414 1ND

9/4/20099/4/2009SW8260BBromobenzene 1.0P9I0414 1ND

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSH1228-01 (Bld 1 Tank-08212009 - Water) - cont.


9/4/20099/4/2009SW8260BBromochloromethane 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BBromodichloromethane 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BBromoform 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BBromomethane 2.0P9I0414 1ND

9/4/20099/4/2009SW8260BChlorobenzene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BChloroethane 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BChloromethane 5.0P9I0414 1ND

9/4/20099/4/2009SW8260Bcis-1,3-Dichloropropene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BDibromochloromethane 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BDichlorodifluoromethane 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BMethyl-tert-butyl Ether (MTBE) 1.0P9I0414 1ND

9/4/20099/4/2009SW8260Bn-Butylbenzene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260Bn-Propylbenzene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260Bp-Isopropyltoluene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260Bsec-Butylbenzene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BStyrene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260Btert-Butylbenzene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260Btrans-1,3-Dichloropropene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BVinyl Acetate 1.0P9I0414 1ND

108 %Surrogate: Dibromofluoromethane (80.3-130%)

102 %Surrogate: Toluene-d8 (88.4-111%)

103 %Surrogate: 4-Bromofluorobenzene (86.5-114%)

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSH1228-02 (TB001-08212009 - Water)


9/4/20099/4/2009SW8260B1,1,2,2-Tetrachloroethane 1.0P9I0414 1ND

9/4/20099/4/2009SW8260B1,1-Dichloroethene 1.0P9I0414 1ND


9/4/20099/4/2009SW8260B2-Butanone (MEK) 5.0P9I0414 1ND

9/4/20099/4/2009SW8260BAcetone 20P9I0414 1ND

9/4/20099/4/2009SW8260BBenzene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BCarbon tetrachloride 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BChloroform 1.0P9I0414 1ND

9/4/20099/4/2009SW8260Bcis-1,2-Dichloroethene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BEthylbenzene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260Bm,p-Xylenes 2.0P9I0414 1ND

9/4/20099/4/2009SW8260BMethylene Chloride 2.0P9I0414 1ND

9/4/20099/4/2009SW8260Bo-Xylene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BTetrachloroethene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BToluene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260Btrans-1,2-Dichloroethene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BTrichloroethene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BTrichlorofluoromethane 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BVinyl chloride 1.0P9I0414 1ND




9/4/20099/4/2009SW8260B1,1-Dichloropropene 1.0P9I0414 1ND


9/4/20099/4/2009SW8260B1,2,3-Trichloropropane 2.0P9I0414 1ND



9/4/20099/4/2009SW8260B1,2-Dibromoethane (EDB) 1.0P9I0414 1ND









9/4/20099/4/2009SW8260B2-Hexanone 5.0P9I0414 1ND


9/4/20099/4/2009SW8260B4-Methyl-2-pentanone (MIBK) 5.0P9I0414 1ND

9/4/20099/4/2009SW8260BBromobenzene 1.0P9I0414 1ND

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSH1228-02 (TB001-08212009 - Water) - cont.


9/4/20099/4/2009SW8260BBromochloromethane 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BBromodichloromethane 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BBromoform 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BBromomethane 2.0P9I0414 1ND

9/4/20099/4/2009SW8260BChlorobenzene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BChloroethane 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BChloromethane 5.0P9I0414 1ND

9/4/20099/4/2009SW8260Bcis-1,3-Dichloropropene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BDibromochloromethane 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BDichlorodifluoromethane 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BMethyl-tert-butyl Ether (MTBE) 1.0P9I0414 1ND

9/4/20099/4/2009SW8260Bn-Butylbenzene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260Bn-Propylbenzene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260Bp-Isopropyltoluene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260Bsec-Butylbenzene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BStyrene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260Btert-Butylbenzene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260Btrans-1,3-Dichloropropene 1.0P9I0414 1ND

9/4/20099/4/2009SW8260BVinyl Acetate 1.0P9I0414 1ND

106 %Surrogate: Dibromofluoromethane (80.3-130%)

100 %Surrogate: Toluene-d8 (88.4-111%)

101 %Surrogate: 4-Bromofluorobenzene (86.5-114%)

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

SEMI-VOLATILE ORGANICS BY GC/MS (EPA 3520C/8270C)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSH1228-04 (Bld 1 Tank-08212009 - Water) D1


9/1/20098/28/2009SW8270CBis(2-chloroethyl)ether 40P9H2840 4ND

9/1/20098/28/2009SW8270CPhenol 40P9H2840 L34ND

9/1/20098/28/2009SW8270C2-Chlorophenol 40P9H2840 4ND

9/1/20098/28/2009SW8270C1,3-Dichlorobenzene 40P9H2840 L34ND

9/1/20098/28/2009SW8270C1,4-Dichlorobenzene 40P9H2840 4ND

9/1/20098/28/2009SW8270C1,2-Dichlorobenzene 40P9H2840 4ND

9/1/20098/28/2009SW8270CBenzyl alcohol 40P9H2840 V1, L44ND

9/1/20098/28/2009SW8270CBis(2-chloroisopropyl)ether 40P9H2840 4ND

9/1/20098/28/2009SW8270C2-Methylphenol 40P9H2840 L44ND

9/1/20098/28/2009SW8270CHexachloroethane 40P9H2840 L34ND

9/1/20098/28/2009SW8270Cn-Nitroso-di-n-propylamine 40P9H2840 4ND

9/1/20098/28/2009SW8270C3&4-Methylphenol 40P9H2840 L44ND

9/1/20098/28/2009SW8270CNitrobenzene 40P9H2840 4ND

9/1/20098/28/2009SW8270CIsophorone 40P9H2840 4ND

9/1/20098/28/2009SW8270C2-Nitrophenol 60P9H2840 4ND

9/1/20098/28/2009SW8270C2,4-Dimethylphenol 40P9H2840 L44ND

9/1/20098/28/2009SW8270CBenzoic acid 100P9H2840 L34ND

9/1/20098/28/2009SW8270CBis(2-chloroethoxy)methane 40P9H2840 4ND

9/1/20098/28/2009SW8270C2,4-Dichlorophenol 40P9H2840 4ND

9/1/20098/28/2009SW8270C1,2,4-Trichlorobenzene 40P9H2840 4ND

9/1/20098/28/2009SW8270CNaphthalene 40P9H2840 4ND

9/1/20098/28/2009SW8270C4-Chloroaniline 40P9H2840 L44ND

9/1/20098/28/2009SW8270CHexachlorobutadiene 40P9H2840 L34ND

9/1/20098/28/2009SW8270C4-Chloro-3-methylphenol 40P9H2840 L44ND

9/1/20098/28/2009SW8270C2-Methylnaphthalene 40P9H2840 4ND

9/1/20098/28/2009SW8270CHexachlorocyclopentadiene 40P9H2840 L34ND

9/1/20098/28/2009SW8270C2,4,6-Trichlorophenol 80P9H2840 4ND

9/1/20098/28/2009SW8270C2,4,5-Trichlorophenol 80P9H2840 4ND

9/1/20098/28/2009SW8270C2-Chloronaphthalene 40P9H2840 4ND

9/1/20098/28/2009SW8270C2-Nitroaniline 40P9H2840 4ND

9/1/20098/28/2009SW8270CAcenaphthylene 40P9H2840 4ND

9/1/20098/28/2009SW8270CDimethyl phthalate 80P9H2840 L34ND

9/1/20098/28/2009SW8270C2,6-Dinitrotoluene 40P9H2840 4ND

9/1/20098/28/2009SW8270CAcenaphthene 40P9H2840 4ND

9/1/20098/28/2009SW8270C3-Nitroaniline 40P9H2840 L44ND

9/1/20098/28/2009SW8270C2,4-Dinitrophenol 200P9H2840 4ND

9/1/20098/28/2009SW8270CDibenzofuran 40P9H2840 4ND

9/1/20098/28/2009SW8270C2,4-Dinitrotoluene 40P9H2840 4ND

9/1/20098/28/2009SW8270C4-Nitrophenol 100P9H2840 L34ND

9/1/20098/28/2009SW8270CFluorene 40P9H2840 4ND

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSH1228-04 (Bld 1 Tank-08212009 - Water) - cont. D1


9/1/20098/28/2009SW8270C4-Chlorophenyl phenyl ether 40P9H2840 4ND

9/1/20098/28/2009SW8270CDiethyl phthalate 40P9H2840 L34ND

9/1/20098/28/2009SW8270C4-Nitroaniline 40P9H2840 L44ND

9/1/20098/28/2009SW8270C4,6-Dinitro-2-methylphenol 200P9H2840 4ND

9/1/20098/28/2009SW8270Cn-Nitrosodiphenylamine 40P9H2840 L44ND

9/1/20098/28/2009SW8270C1,2-Diphenylhydrazine (as Azobenzene) 40P9H2840 4ND

9/1/20098/28/2009SW8270C4-Bromophenyl phenyl ether 40P9H2840 4ND

9/1/20098/28/2009SW8270CHexachlorobenzene 40P9H2840 4ND

9/1/20098/28/2009SW8270CPentachlorophenol 200P9H2840 4ND

9/1/20098/28/2009SW8270CPhenanthrene 40P9H2840 4ND

9/1/20098/28/2009SW8270CAnthracene 40P9H2840 4ND

9/1/20098/28/2009SW8270CDi-n-butyl phthalate 40P9H2840 4ND

9/1/20098/28/2009SW8270CFluoranthene 40P9H2840 4ND

9/1/20098/28/2009SW8270CPyrene 40P9H2840 4ND

9/1/20098/28/2009SW8270CButyl benzyl phthalate 40P9H2840 4ND

9/1/20098/28/2009SW8270C3,3-Dichlorobenzidine 40P9H2840 L44ND

9/1/20098/28/2009SW8270CBenzanthracene 40P9H2840 4ND

9/1/20098/28/2009SW8270CChrysene 40P9H2840 4ND

9/1/20098/28/2009SW8270CBis(2-ethylhexyl)phthalate 40P9H2840 4ND

9/1/20098/28/2009SW8270CDi-n-octyl phthalate 40P9H2840 E7, L34ND

9/1/20098/28/2009SW8270CBenzo(b)fluoranthene 40P9H2840 E7, L34ND

9/1/20098/28/2009SW8270CBenzo(k)fluoranthene 40P9H2840 E7, L34ND

9/1/20098/28/2009SW8270CBenzo(a)pyrene 40P9H2840 E7, L34ND

9/1/20098/28/2009SW8270CIndeno(1,2,3-cd)pyrene 40P9H2840 E7, L34ND

9/1/20098/28/2009SW8270CDibenz(a,h)anthracene 40P9H2840 E7, L34ND

9/1/20098/28/2009SW8270CBenzo(g,h,i)perylene 40P9H2840 E7, L34ND

32 %Surrogate: 2-Fluorophenol (15-65%)

29 %Surrogate: Phenol-d6 (11-47%)

82 %Surrogate: Nitrobenzene-d5 (31-110%)

75 %Surrogate: 2-Fluorobiphenyl (36-94%)

28 % S6Surrogate: 2,4,6-Tribromophenol (41-99%)

67 % S4Surrogate: 4-Terphenyl-d14 (8-56%)

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSH1228-04RE1 (Bld 1 Tank-08212009 - Water) - cont. H4, N1, D1


9/8/20099/3/2009SW8270CBis(2-chloroethyl)ether 40P9I0322 4ND

9/8/20099/3/2009SW8270CPhenol 40P9I0322 4ND

9/8/20099/3/2009SW8270C2-Chlorophenol 40P9I0322 4ND

9/8/20099/3/2009SW8270C1,3-Dichlorobenzene 40P9I0322 4ND



9/8/20099/3/2009SW8270CBenzyl alcohol 40P9I0322 4ND

9/8/20099/3/2009SW8270CBis(2-chloroisopropyl)ether 40P9I0322 4ND

9/8/20099/3/2009SW8270C2-Methylphenol 40P9I0322 4ND

9/8/20099/3/2009SW8270CHexachloroethane 40P9I0322 4ND

9/8/20099/3/2009SW8270Cn-Nitroso-di-n-propylamine 40P9I0322 4ND

9/8/20099/3/2009SW8270C3&4-Methylphenol 40P9I0322 4ND

9/8/20099/3/2009SW8270CNitrobenzene 40P9I0322 4ND

9/8/20099/3/2009SW8270CIsophorone 40P9I0322 4ND

9/8/20099/3/2009SW8270C2-Nitrophenol 60P9I0322 4ND

9/8/20099/3/2009SW8270C2,4-Dimethylphenol 40P9I0322 4ND

9/8/20099/3/2009SW8270CBenzoic acid 100P9I0322 L44ND

9/8/20099/3/2009SW8270CBis(2-chloroethoxy)methane 40P9I0322 4ND

9/8/20099/3/2009SW8270C2,4-Dichlorophenol 40P9I0322 4ND

9/8/20099/3/2009SW8270C1,2,4-Trichlorobenzene 40P9I0322 4ND

9/8/20099/3/2009SW8270CNaphthalene 40P9I0322 4ND

9/8/20099/3/2009SW8270C4-Chloroaniline 40P9I0322 4ND

9/8/20099/3/2009SW8270CHexachlorobutadiene 40P9I0322 4ND

9/8/20099/3/2009SW8270C4-Chloro-3-methylphenol 40P9I0322 4ND

9/8/20099/3/2009SW8270C2-Methylnaphthalene 40P9I0322 4ND

9/8/20099/3/2009SW8270CHexachlorocyclopentadiene 40P9I0322 4ND

9/8/20099/3/2009SW8270C2,4,6-Trichlorophenol 80P9I0322 4ND

9/8/20099/3/2009SW8270C2,4,5-Trichlorophenol 80P9I0322 4ND

9/8/20099/3/2009SW8270C2-Chloronaphthalene 40P9I0322 4ND

9/8/20099/3/2009SW8270C2-Nitroaniline 40P9I0322 4ND

9/8/20099/3/2009SW8270CAcenaphthylene 40P9I0322 4ND

9/8/20099/3/2009SW8270CDimethyl phthalate 80P9I0322 L34ND

9/8/20099/3/2009SW8270C2,6-Dinitrotoluene 40P9I0322 4ND

9/8/20099/3/2009SW8270CAcenaphthene 40P9I0322 4ND


9/8/20099/3/2009SW8270C2,4-Dinitrophenol 200P9I0322 4ND

9/8/20099/3/2009SW8270CDibenzofuran 40P9I0322 4ND

9/8/20099/3/2009SW8270C2,4-Dinitrotoluene 40P9I0322 4ND

9/8/20099/3/2009SW8270C4-Nitrophenol 100P9I0322 4ND

9/8/20099/3/2009SW8270CFluorene 40P9I0322 4ND

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSH1228-04RE1 (Bld 1 Tank-08212009 - Water) - cont. H4, N1, D1


9/8/20099/3/2009SW8270C4-Chlorophenyl phenyl ether 40P9I0322 4ND

9/8/20099/3/2009SW8270CDiethyl phthalate 40P9I0322 4ND


9/8/20099/3/2009SW8270C4,6-Dinitro-2-methylphenol 200P9I0322 4ND

9/8/20099/3/2009SW8270Cn-Nitrosodiphenylamine 40P9I0322 4ND

9/8/20099/3/2009SW8270C1,2-Diphenylhydrazine (as Azobenzene) 40P9I0322 4ND

9/8/20099/3/2009SW8270C4-Bromophenyl phenyl ether 40P9I0322 4ND

9/8/20099/3/2009SW8270CHexachlorobenzene 40P9I0322 4ND

9/8/20099/3/2009SW8270CPentachlorophenol 200P9I0322 4ND

9/8/20099/3/2009SW8270CPhenanthrene 40P9I0322 4ND

9/8/20099/3/2009SW8270CAnthracene 40P9I0322 4ND

9/8/20099/3/2009SW8270CDi-n-butyl phthalate 40P9I0322 4ND

9/8/20099/3/2009SW8270CFluoranthene 40P9I0322 4ND

9/8/20099/3/2009SW8270CPyrene 40P9I0322 4ND

9/8/20099/3/2009SW8270CButyl benzyl phthalate 40P9I0322 4ND

9/8/20099/3/2009SW8270C3,3-Dichlorobenzidine 40P9I0322 4ND

9/8/20099/3/2009SW8270CBenzanthracene 40P9I0322 4ND

9/8/20099/3/2009SW8270CChrysene 40P9I0322 4ND

9/8/20099/3/2009SW8270CBis(2-ethylhexyl)phthalate 40P9I0322 4ND

9/8/20099/3/2009SW8270CDi-n-octyl phthalate 40P9I0322 4ND

9/8/20099/3/2009SW8270CBenzo(b)fluoranthene 40P9I0322 4ND

9/8/20099/3/2009SW8270CBenzo(k)fluoranthene 40P9I0322 4ND

9/8/20099/3/2009SW8270CBenzo(a)pyrene 40P9I0322 4ND

9/8/20099/3/2009SW8270CIndeno(1,2,3-cd)pyrene 40P9I0322 4ND

9/8/20099/3/2009SW8270CDibenz(a,h)anthracene 40P9I0322 4ND

9/8/20099/3/2009SW8270CBenzo(g,h,i)perylene 40P9I0322 4ND

32 %Surrogate: 2-Fluorophenol (15-65%)

24 %Surrogate: Phenol-d6 (11-47%)

58 %Surrogate: Nitrobenzene-d5 (31-110%)

58 %Surrogate: 2-Fluorobiphenyl (36-94%)

66 %Surrogate: 2,4,6-Tribromophenol (41-99%)

53 %Surrogate: 4-Terphenyl-d14 (8-56%)

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

TOTAL METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



8/24/20098/21/2009E200.7Aluminum 0.20P9H2132 1ND

8/24/20098/21/2009E200.7Antimony 0.040P9H2132 1ND

8/24/20098/21/2009E200.7Arsenic 0.10P9H2132 1ND

Barium 8/24/20098/21/2009P9H2132 0.010 1E200.7 0.079

8/24/20098/21/2009E200.7Beryllium 0.0010P9H2132 1ND

Boron 8/24/20098/21/2009P9H2132 0.20 1E200.7 0.29

8/24/20098/21/2009E200.7Cadmium 0.0010P9H2132 1ND

Calcium 8/24/20098/21/2009P9H2132 2.0 1E200.7 88

8/24/20098/21/2009E200.7Chromium 0.010P9H2132 1ND

8/24/20098/21/2009E200.7Cobalt 0.010P9H2132 1ND

Copper 8/24/20098/21/2009P9H2132 0.010 1E200.7 0.012

Iron 8/24/20098/21/2009P9H2132 0.050 1E200.7 0.32

8/24/20098/21/2009E200.7Lead 0.015P9H2132 1ND

Magnesium 8/24/20098/21/2009P9H2132 2.0 1E200.7 9.1

Manganese 8/24/20098/21/2009P9H2132 0.010 1E200.7 0.017

Molybdenum 8/24/20098/21/2009P9H2132 0.010 1E200.7 0.011

Nickel 8/24/20098/21/2009P9H2132 0.010 1E200.7 0.010

Potassium 8/24/20098/21/2009P9H2132 2.0 1E200.7 33

8/24/20098/21/2009E200.7Selenium 0.10P9H2132 1ND

Silica 8/24/20098/21/2009P9H2132 0.21 1E200.7 18

8/24/20098/21/2009E200.7Silver 0.010P9H2132 1ND

Sodium 8/24/20098/21/2009P9H2132 2.0 1E200.7 53

8/24/20098/21/2009E200.7Thallium 0.10P9H2132 1ND

Vanadium 8/24/20098/21/2009P9H2132 0.010 1E200.7 0.011

8/24/20098/21/2009E200.7Zinc 0.050P9H2132 1ND

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

TOTAL METALS BY ICP/MS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



Uranium 8/24/20098/21/2009P9H2135 0.0010 1E200.8 0.0044

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

TOTAL RECOVERABLE METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



9/2/20099/2/2009SW7470AMercury 0.00050P9I0224 1ND

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

MDL

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



8/25/20098/25/2009E314Perchlorate 2.0P9H2523 1ND0.36

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



9/2/20099/2/2009SM4500CN-ETotal Cyanide 0.0209I02126 1ND

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

SW846 8330

Data

QualifiersBatch

Reporting

Limit

Sample

Result


Reporting Units: ug/L

9/6/20098/27/2009SW846 83301,3,5-Trinitrobenzene 0.119239332 1.08ND

9/6/20098/27/2009SW846 83301,3-Dinitrobenzene 0.119239332 1.08ND

9/6/20098/27/2009SW846 83302,4,6-Trinitrotoluene 0.119239332 1.08ND

9/6/20098/27/2009SW846 83302,4-Dinitrotoluene 0.119239332 1.08ND

9/6/20098/27/2009SW846 83302,6-Dinitrotoluene 0.119239332 1.08ND

9/6/20098/27/2009SW846 83302-Amino-4,6-dinitrotoluene 0.229239332 1.08ND

9/6/20098/27/2009SW846 83302-Nitrotoluene 0.549239332 1.08ND

9/6/20098/27/2009SW846 83303-Nitrotoluene 0.549239332 V81.08ND

9/6/20098/27/2009SW846 83304-Amino-2,6-dinitrotoluene 0.119239332 1.08ND

9/6/20098/27/2009SW846 83304-Nitrotoluene 0.549239332 1.08ND

9/6/20098/27/2009SW846 8330HMX 0.119239332 1.08ND

9/6/20098/27/2009SW846 8330Nitrobenzene 0.119239332 1.08ND

9/6/20098/27/2009SW846 8330RDX 0.119239332 1.08ND

9/6/20098/27/2009SW846 8330Tetryl 0.119239332 1.08ND

95 %Surrogate: 3,4-Dinitrotoluene (79-111%)

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

Batch: P9I0414 Extracted: 09/04/09

Blank Analyzed: 09/04/2009 (P9I0414-BLK1)

1,1,2,2-Tetrachloroethane ug/l1.0ND

1,1-Dichloroethene ug/l1.0ND

1,2-Dichloropropane ug/l1.0ND

2-Butanone (MEK) ug/l5.0ND

Acetone ug/l20ND

Benzene ug/l1.0ND

Carbon tetrachloride ug/l1.0ND

Chloroform ug/l1.0ND

cis-1,2-Dichloroethene ug/l1.0ND

Ethylbenzene ug/l1.0ND

m,p-Xylenes ug/l2.0ND

Methylene Chloride ug/l2.0ND

o-Xylene ug/l1.0ND

Tetrachloroethene ug/l1.0ND

Toluene ug/l1.0ND

trans-1,2-Dichloroethene ug/l1.0ND

Trichloroethene ug/l1.0ND

Trichlorofluoromethane ug/l1.0ND

Vinyl chloride ug/l1.0ND

1,1,1-Trichloroethane ug/l1.0ND

1,1,2-Trichloroethane ug/l1.0ND

1,1-Dichloroethane ug/l1.0ND

1,1-Dichloropropene ug/l1.0ND

1,2,3-Trichlorobenzene ug/l2.0ND

1,2,3-Trichloropropane ug/l2.0ND

1,2,4-Trichlorobenzene ug/l1.0ND

1,2,4-Trimethylbenzene ug/l1.0ND

1,2-Dibromoethane (EDB) ug/l1.0ND

1,2-Dichlorobenzene ug/l1.0ND

1,2-Dichloroethane ug/l1.0ND

1,3,5-Trimethylbenzene ug/l1.0ND





Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



2-Chlorotoluene ug/l1.0ND

2-Hexanone ug/l5.0ND

4-Chlorotoluene ug/l1.0ND

4-Methyl-2-pentanone (MIBK) ug/l5.0ND

Bromobenzene ug/l1.0ND

Bromochloromethane ug/l1.0ND

Bromodichloromethane ug/l1.0ND

Bromoform ug/l1.0ND

Bromomethane ug/l2.0ND

Chlorobenzene ug/l1.0ND

Chloroethane ug/l1.0ND

Chloromethane ug/l5.0ND

cis-1,3-Dichloropropene ug/l1.0ND

Dibromochloromethane ug/l1.0ND

Dichlorodifluoromethane ug/l1.0ND

Methyl-tert-butyl Ether (MTBE) ug/l1.0ND

n-Butylbenzene ug/l1.0ND

n-Propylbenzene ug/l1.0ND

p-Isopropyltoluene ug/l1.0ND

sec-Butylbenzene ug/l1.0ND

Styrene ug/l1.0ND

tert-Butylbenzene ug/l1.0ND

trans-1,3-Dichloropropene ug/l1.0ND

Vinyl Acetate ug/l1.0ND

25.0 80.3-130Surrogate: Dibromofluoromethane ug/l25.8 103

25.0 88.4-111Surrogate: Toluene-d8 ug/l24.8 99

25.0 86.5-114Surrogate: 4-Bromofluorobenzene ug/l24.8 99

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 09/04/2009 (P9I0414-BS1)

1,1,2,2-Tetrachloroethane 25.0 70.5-125ug/l1.027.4 110

1,1-Dichloroethene 25.0 81.7-122ug/l1.025.7 103

1,2-Dichloropropane 25.0 85-115ug/l1.025.4 101

2-Butanone (MEK) 25.0 45.6-141ug/l5.029.4 117

Acetone 25.0 22.4-153ug/l2029.8 119

Benzene 25.0 80.7-120ug/l1.025.1 101

Carbon tetrachloride 25.0 82.5-123ug/l1.028.3 113

Chloroform 25.0 80.7-119ug/l1.025.2 101

cis-1,2-Dichloroethene 25.0 83.3-117ug/l1.023.8 95

Ethylbenzene 25.0 85-115ug/l1.025.3 101

m,p-Xylenes 25.0 85-115ug/l2.025.0 100

Methylene Chloride 25.0 79.7-117ug/l2.024.8 99

o-Xylene 25.0 85-115ug/l1.025.6 102

Tetrachloroethene 25.0 85-115ug/l1.024.1 96

Toluene 25.0 85-115ug/l1.025.7 103

trans-1,2-Dichloroethene 25.0 82.3-120ug/l1.025.0 100

Trichloroethene 25.0 85-115ug/l1.026.0 104

Trichlorofluoromethane 25.0 84.5-123ug/l1.027.4 110

Vinyl chloride 25.0 80.9-127ug/l1.025.7 103

1,1,1-Trichloroethane 25.0 83.2-120ug/l1.027.3 109

1,1,2-Trichloroethane 25.0 85-115ug/l1.025.7 103

1,1-Dichloroethane 25.0 78.8-122ug/l1.025.9 104

1,1-Dichloropropene 25.0 82.3-119ug/l1.025.4 102

1,2,3-Trichlorobenzene 25.0 60.4-171ug/l2.022.0 88

1,2,3-Trichloropropane 25.0 76.3-125ug/l2.026.1 104

1,2,4-Trichlorobenzene 25.0 71-136ug/l1.022.8 91

1,2,4-Trimethylbenzene 25.0 78.1-120ug/l1.026.3 105

1,2-Dibromoethane (EDB) 25.0 85-115ug/l1.026.0 104

1,2-Dichlorobenzene 25.0 85-115ug/l1.023.8 95

1,2-Dichloroethane 25.0 79.1-124ug/l1.028.0 112

1,3,5-Trimethylbenzene 25.0 80.1-119ug/l1.026.4 106

1,3-Dichlorobenzene 25.0 83.9-114ug/l1.024.6 99

1,3-Dichloropropane 25.0 85-115ug/l1.025.7 103

1,4-Dichlorobenzene 25.0 85-115ug/l1.024.6 98

2,2-Dichloropropane 25.0 70.8-128ug/l2.028.1 112

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



2-Chlorotoluene 25.0 78.6-120ug/l1.025.2 101

2-Hexanone 25.0 58.5-135ug/l5.027.1 108

4-Chlorotoluene 25.0 80.3-119ug/l1.025.9 104

4-Methyl-2-pentanone (MIBK) 25.0 72-129ug/l5.027.9 111

Bromobenzene 25.0 83.3-116ug/l1.024.3 97

Bromochloromethane 25.0 83-122ug/l1.025.1 100

Bromodichloromethane 25.0 84-117ug/l1.026.7 107

Bromoform 25.0 71.9-131ug/l1.022.7 91

Bromomethane 25.0 56.3-145ug/l2.026.4 106

Chlorobenzene 25.0 82.5-123ug/l1.025.3 101

Chloroethane 25.0 69.5-132ug/l1.027.1 109

Chloromethane 25.0 70.9-123ug/l5.025.9 103

cis-1,3-Dichloropropene 25.0 85-115ug/l1.027.1 108

Dibromochloromethane 25.0 83.2-123ug/l1.027.1 108

Dichlorodifluoromethane 25.0 72.8-130ug/l1.030.7 123

Methyl-tert-butyl Ether (MTBE) 25.0 81.8-118ug/l1.025.1 100

n-Butylbenzene 25.0 74-121ug/l1.025.5 102

n-Propylbenzene 25.0 79.4-120ug/l1.024.8 99

p-Isopropyltoluene 25.0 75.5-116ug/l1.024.2 97

sec-Butylbenzene 25.0 76.7-121ug/l1.025.3 101

Styrene 25.0 85-115ug/l1.026.4 106

tert-Butylbenzene 25.0 78.9-117ug/l1.025.0 100

trans-1,3-Dichloropropene 25.0 82.2-121ug/l1.028.4 113

Vinyl Acetate 25.0 70.5-134ug/l1.033.0 132




Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Dup Analyzed: 09/04/2009 (P9I0414-BSD1)

1,1,2,2-Tetrachloroethane 25.0 2570.5-125ug/l1.026.0 104 5

1,1-Dichloroethene 25.0 2581.7-122ug/l1.026.8 107 4

1,2-Dichloropropane 25.0 2585-115ug/l1.025.1 100 1

2-Butanone (MEK) 25.0 2545.6-141ug/l5.027.2 109 8

Acetone 25.0 2522.4-153ug/l2031.7 127 6

Benzene 25.0 2580.7-120ug/l1.025.0 100 0

Carbon tetrachloride 25.0 2582.5-123ug/l1.028.2 113 0

Chloroform 25.0 2580.7-119ug/l1.026.0 104 3

cis-1,2-Dichloroethene 25.0 2583.3-117ug/l1.025.0 100 5

Ethylbenzene 25.0 2585-115ug/l1.026.2 105 3

m,p-Xylenes 25.0 2585-115ug/l2.025.4 102 2

Methylene Chloride 25.0 2579.7-117ug/l2.025.2 101 1

o-Xylene 25.0 2585-115ug/l1.026.0 104 2

Tetrachloroethene 25.0 2585-115ug/l1.026.0 104 8

Toluene 25.0 2585-115ug/l1.024.9 99 3

trans-1,2-Dichloroethene 25.0 2582.3-120ug/l1.026.4 105 5

Trichloroethene 25.0 2585-115ug/l1.026.1 105 0

Trichlorofluoromethane 25.0 2584.5-123ug/l1.028.8 115 5

Vinyl chloride 25.0 2580.9-127ug/l1.027.8 111 8

1,1,1-Trichloroethane 25.0 2583.2-120ug/l1.027.8 111 2

1,1,2-Trichloroethane 25.0 2585-115ug/l1.024.1 96 7

1,1-Dichloroethane 25.0 2578.8-122ug/l1.026.6 106 3

1,1-Dichloropropene 25.0 2582.3-119ug/l1.025.7 103 1

1,2,3-Trichlorobenzene 25.0 2560.4-171ug/l2.023.2 93 5

1,2,3-Trichloropropane 25.0 2576.3-125ug/l2.026.2 105 0

1,2,4-Trichlorobenzene 25.0 2571-136ug/l1.023.9 96 5

1,2,4-Trimethylbenzene 25.0 2578.1-120ug/l1.026.6 107 1

1,2-Dibromoethane (EDB) 25.0 2585-115ug/l1.025.9 104 0

1,2-Dichlorobenzene 25.0 2585-115ug/l1.024.0 96 1

1,2-Dichloroethane 25.0 2579.1-124ug/l1.028.1 112 0

1,3,5-Trimethylbenzene 25.0 2580.1-119ug/l1.026.9 108 2

1,3-Dichlorobenzene 25.0 2583.9-114ug/l1.024.9 100 1

1,3-Dichloropropane 25.0 2585-115ug/l1.025.6 103 0

1,4-Dichlorobenzene 25.0 2585-115ug/l1.024.4 98 0

2,2-Dichloropropane 25.0 2570.8-128ug/l2.028.2 113 0

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



2-Chlorotoluene 25.0 2578.6-120ug/l1.024.5 98 3

2-Hexanone 25.0 2558.5-135ug/l5.028.2 113 4

4-Chlorotoluene 25.0 2580.3-119ug/l1.026.7 107 3

4-Methyl-2-pentanone (MIBK) 25.0 2572-129ug/l5.026.1 104 7

Bromobenzene 25.0 2583.3-116ug/l1.024.7 99 2

Bromochloromethane 25.0 2583-122ug/l1.025.5 102 2

Bromodichloromethane 25.0 2584-117ug/l1.025.2 101 6

Bromoform 25.0 2571.9-131ug/l1.022.2 89 2

Bromomethane 25.0 2556.3-145ug/l2.027.6 111 4

Chlorobenzene 25.0 2582.5-123ug/l1.025.2 101 0

Chloroethane 25.0 2569.5-132ug/l1.026.9 108 1

Chloromethane 25.0 2570.9-123ug/l5.026.9 108 4

cis-1,3-Dichloropropene 25.0 2585-115ug/l1.026.3 105 3

Dibromochloromethane 25.0 2583.2-123ug/l1.027.8 111 3

Dichlorodifluoromethane 25.0 2572.8-130ug/l1.031.3 125 2

Methyl-tert-butyl Ether (MTBE) 25.0 2581.8-118ug/l1.024.7 99 1

n-Butylbenzene 25.0 2574-121ug/l1.026.3 105 3

n-Propylbenzene 25.0 2579.4-120ug/l1.026.0 104 4

p-Isopropyltoluene 25.0 2575.5-116ug/l1.026.1 104 8

sec-Butylbenzene 25.0 2576.7-121ug/l1.025.7 103 2

Styrene 25.0 2585-115ug/l1.026.1 105 1

tert-Butylbenzene 25.0 2578.9-117ug/l1.025.3 101 1

trans-1,3-Dichloropropene 25.0 2582.2-121ug/l1.026.4 105 7

Vinyl Acetate 25.0 2570.5-134ug/l1.032.0 128 3




Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Analyzed: 09/04/2009 (P9I0414-MS1) Source: PSH1235-02

1,1,2,2-Tetrachloroethane 25.0 70.4-124ug/l1.026.0 ND 104

1,1-Dichloroethene 25.0 82.1-126ug/l1.025.6 ND 102

1,2-Dichloropropane 25.0 81.1-116ug/l1.025.5 ND 102

2-Butanone (MEK) 25.0 41.6-130ug/l5.026.9 ND 108

Acetone 25.0 19.7-131ug/l2037.0 11.0 104

Benzene 25.0 78.4-127ug/l1.025.6 ND 103

Carbon tetrachloride 25.0 80.7-128ug/l1.028.7 ND 115

Chloroform 25.0 77.6-122ug/l1.027.0 ND 108

cis-1,2-Dichloroethene 25.0 80.1-119ug/l1.024.4 ND 97

Ethylbenzene 25.0 83.4-116ug/l1.025.4 ND 102

m,p-Xylenes 25.0 70.8-132ug/l2.025.2 ND 101

Methylene Chloride 25.0 74.6-119ug/l2.026.1 ND 105

o-Xylene 25.0 77.5-122ug/l1.025.8 ND 103

Tetrachloroethene 25.0 77.8-119ug/l1.024.6 ND 98

Toluene 25.0 83-118ug/l1.026.1 ND 104

trans-1,2-Dichloroethene 25.0 81.3-123ug/l1.026.4 ND 106

Trichloroethene 25.0 77.3-120ug/l1.026.3 ND 105

Trichlorofluoromethane 25.0 82.4-132ug/l1.029.2 ND 117

Vinyl chloride 25.0 69.2-143ug/l1.026.2 ND 105

1,1,1-Trichloroethane 25.0 81.4-125ug/l1.028.4 ND 114

1,1,2-Trichloroethane 25.0 77.5-118ug/l1.026.0 3.56 90

1,1-Dichloroethane 25.0 75.7-126ug/l1.026.8 ND 107

1,1-Dichloropropene 25.0 81.4-123ug/l1.025.2 ND 101

1,2,3-Trichlorobenzene 25.0 32.3-117ug/l2.022.7 ND 91

1,2,3-Trichloropropane 25.0 69.8-124ug/l2.025.5 ND 102

1,2,4-Trichlorobenzene 25.0 52.9-145ug/l1.023.0 ND 92

1,2,4-Trimethylbenzene 25.0 75.2-120ug/l1.026.4 ND 105

1,2-Dibromoethane (EDB) 25.0 76.5-120ug/l1.025.6 ND 102

1,2-Dichlorobenzene 25.0 80.6-114ug/l1.024.6 ND 98

1,2-Dichloroethane 25.0 69.4-129ug/l1.029.4 ND 118

1,3,5-Trimethylbenzene 25.0 75.1-123ug/l1.025.6 ND 102


1,3-Dichloropropane 25.0 77.1-119ug/l1.025.8 0.810 100


2,2-Dichloropropane 25.0 66.5-134ug/l2.028.7 ND 115

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



2-Chlorotoluene 25.0 75.2-122ug/l1.025.2 ND 101

2-Hexanone 25.0 57.9-118ug/l5.026.1 ND 104

4-Chlorotoluene 25.0 76.8-120ug/l1.025.2 ND 101

4-Methyl-2-pentanone (MIBK) 25.0 65.6-127ug/l5.025.6 ND 103

Bromobenzene 25.0 79.4-116ug/l1.024.6 ND 98

Bromochloromethane 25.0 75.5-125ug/l1.025.4 ND 102

Bromodichloromethane 25.0 78.1-118ug/l1.027.2 ND 109

Bromoform 25.0 63.7-129ug/l1.021.1 ND 84

Bromomethane 25.0 44.2-155ug/l2.028.1 ND 112

Chlorobenzene 25.0 84.6-110ug/l1.025.0 ND 100

Chloroethane 25.0 68.9-136ug/l1.027.8 ND 111

Chloromethane 25.0 64.1-135ug/l5.027.4 ND 110

cis-1,3-Dichloropropene 25.0 78.6-118ug/l1.026.4 ND 106

Dibromochloromethane 25.0 75.2-123ug/l1.026.9 ND 108

Dichlorodifluoromethane 25.0 71-138ug/l1.032.0 ND 128

Methyl-tert-butyl Ether (MTBE) 25.0 68.8-126ug/l1.025.4 ND 101

n-Butylbenzene 25.0 70.4-119ug/l1.024.4 ND 98

n-Propylbenzene 25.0 76-124ug/l1.025.8 ND 103

p-Isopropyltoluene 25.0 67.9-122ug/l1.026.1 ND 104

sec-Butylbenzene 25.0 73.7-125ug/l1.025.0 ND 100

Styrene 25.0 55-136ug/l1.025.7 ND 103

tert-Butylbenzene 25.0 76.8-119ug/l1.025.5 ND 102

trans-1,3-Dichloropropene 25.0 72.8-123ug/l1.027.5 ND 110

Vinyl Acetate 25.0 50-139ug/l1.030.9 ND 124




Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Dup Analyzed: 09/04/2009 (P9I0414-MSD1) Source: PSH1235-02

1,1,2,2-Tetrachloroethane 25.0 2570.4-124ug/l1.027.3 ND 109 5

1,1-Dichloroethene 25.0 2582.1-126ug/l1.028.5 ND 114 11

1,2-Dichloropropane 25.0 2581.1-116ug/l1.027.4 ND 109 7

2-Butanone (MEK) 25.0 2541.6-130ug/l5.030.2 ND 121 11

Acetone 25.0 2519.7-131ug/l2040.0 11.0 116 8

Benzene 25.0 2578.4-127ug/l1.026.5 ND 106 3

Carbon tetrachloride 25.0 2580.7-128ug/l1.029.8 ND 119 4

Chloroform 25.0 2577.6-122ug/l1.028.9 ND 116 7

cis-1,2-Dichloroethene 25.0 2580.1-119ug/l1.027.4 ND 109 12

Ethylbenzene 25.0 2583.4-116ug/l1.027.5 ND 110 8

m,p-Xylenes 25.0 2570.8-132ug/l2.026.9 ND 107 6

Methylene Chloride 25.0 2574.6-119ug/l2.028.6 ND 114 9

o-Xylene 25.0 2577.5-122ug/l1.027.0 ND 108 5

Tetrachloroethene 25.0 2577.8-119ug/l1.026.1 ND 104 6

Toluene 25.0 2583-118ug/l1.026.6 ND 106 2

trans-1,2-Dichloroethene 25.0 2581.3-123ug/l1.029.1 ND 116 9

Trichloroethene 25.0 2577.3-120ug/l1.027.7 ND 111 5

Trichlorofluoromethane 25.0 2582.4-132ug/l1.031.1 ND 124 6

Vinyl chloride 25.0 2569.2-143ug/l1.029.6 ND 118 12

1,1,1-Trichloroethane 25.0 2581.4-125ug/l1.030.2 ND 121 6

1,1,2-Trichloroethane 25.0 2577.5-118ug/l1.027.4 3.56 95 5

1,1-Dichloroethane 25.0 2575.7-126ug/l1.029.6 ND 118 10

1,1-Dichloropropene 25.0 2581.4-123ug/l1.026.3 ND 105 4

1,2,3-Trichlorobenzene 25.0 2532.3-117ug/l2.023.7 ND 95 5

1,2,3-Trichloropropane 25.0 2569.8-124ug/l2.027.2 ND 109 7

1,2,4-Trichlorobenzene 25.0 2552.9-145ug/l1.024.2 ND 97 5

1,2,4-Trimethylbenzene 25.0 2575.2-120ug/l1.028.3 ND 113 7

1,2-Dibromoethane (EDB) 25.0 2576.5-120ug/l1.027.4 ND 110 7

1,2-Dichlorobenzene 25.0 2580.6-114ug/l1.026.2 ND 105 6

1,2-Dichloroethane 25.0 2569.4-129ug/l1.030.6 ND 122 4

1,3,5-Trimethylbenzene 25.0 2575.1-123ug/l1.027.5 ND 110 7


1,3-Dichloropropane 25.0 2577.1-119ug/l1.027.4 0.810 106 6


2,2-Dichloropropane 25.0 2566.5-134ug/l2.029.8 ND 119 4

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



2-Chlorotoluene 25.0 2575.2-122ug/l1.027.0 ND 108 7

2-Hexanone 25.0 2557.9-118ug/l5.028.3 ND 113 8

4-Chlorotoluene 25.0 2576.8-120ug/l1.027.3 ND 109 8

4-Methyl-2-pentanone (MIBK) 25.0 2565.6-127ug/l5.028.8 ND 115 12

Bromobenzene 25.0 2579.4-116ug/l1.026.3 ND 105 7

Bromochloromethane 25.0 2575.5-125ug/l1.028.3 ND 113 11

Bromodichloromethane 25.0 2578.1-118ug/l1.028.3 ND 113 4

Bromoform 25.0 2563.7-129ug/l1.023.5 ND 94 11

Bromomethane 25.0 2544.2-155ug/l2.030.1 ND 120 7

Chlorobenzene 25.0 2584.6-110ug/l1.027.4 ND 110 9

Chloroethane 25.0 2568.9-136ug/l1.030.9 ND 124 11

Chloromethane 25.0 2564.1-135ug/l5.029.6 ND 118 8

cis-1,3-Dichloropropene 25.0 2578.6-118ug/l1.028.9 ND 116 9

Dibromochloromethane 25.0 2575.2-123ug/l1.029.4 ND 118 9

Dichlorodifluoromethane 25.0 2571-138ug/l1.033.8 ND 135 5

Methyl-tert-butyl Ether (MTBE) 25.0 2568.8-126ug/l1.028.6 ND 114 12

n-Butylbenzene 25.0 2570.4-119ug/l1.027.0 ND 108 10

n-Propylbenzene 25.0 2576-124ug/l1.028.4 ND 114 10

p-Isopropyltoluene 25.0 2567.9-122ug/l1.027.1 ND 108 4

sec-Butylbenzene 25.0 2573.7-125ug/l1.026.7 ND 107 7

Styrene 25.0 2555-136ug/l1.028.4 ND 113 10

tert-Butylbenzene 25.0 2576.8-119ug/l1.027.3 ND 109 7

trans-1,3-Dichloropropene 25.0 2572.8-123ug/l1.028.9 ND 116 5

Vinyl Acetate 25.0 2550-139ug/l1.034.7 ND 139 11




Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

Batch: P9H2840 Extracted: 08/28/09

Blank Analyzed: 09/01/2009 (P9H2840-BLK1)

Bis(2-chloroethyl)ether ug/l10ND

Phenol ug/l10ND

2-Chlorophenol ug/l10ND

1,3-Dichlorobenzene ug/l10ND



Benzyl alcohol ug/l10ND

Bis(2-chloroisopropyl)ether ug/l10ND

2-Methylphenol ug/l10ND

Hexachloroethane ug/l10ND

n-Nitroso-di-n-propylamine ug/l10ND

3&4-Methylphenol ug/l10ND

Nitrobenzene ug/l10ND

Isophorone ug/l10ND

2-Nitrophenol ug/l15ND

2,4-Dimethylphenol ug/l10ND

Benzoic acid ug/l25ND

Bis(2-chloroethoxy)methane ug/l10ND

2,4-Dichlorophenol ug/l10ND

1,2,4-Trichlorobenzene ug/l10ND

Naphthalene ug/l10ND

4-Chloroaniline ug/l10ND

Hexachlorobutadiene ug/l10ND

4-Chloro-3-methylphenol ug/l10ND

2-Methylnaphthalene ug/l10ND

Hexachlorocyclopentadiene ug/l10ND

2,4,6-Trichlorophenol ug/l20ND


2-Chloronaphthalene ug/l10ND

2-Nitroaniline ug/l10ND

Acenaphthylene ug/l10ND

Dimethyl phthalate ug/l20ND

2,6-Dinitrotoluene ug/l10ND

Acenaphthene ug/l10ND


Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



2,4-Dinitrophenol ug/l50ND

Dibenzofuran ug/l10ND



Fluorene ug/l10ND

4-Chlorophenyl phenyl ether ug/l10ND

Diethyl phthalate ug/l10ND


4,6-Dinitro-2-methylphenol ug/l50ND

n-Nitrosodiphenylamine ug/l10ND

1,2-Diphenylhydrazine (as Azobenzene) ug/l10ND

4-Bromophenyl phenyl ether ug/l10ND

Hexachlorobenzene ug/l10ND

Pentachlorophenol ug/l50ND

Phenanthrene ug/l10ND

Anthracene ug/l10ND

Di-n-butyl phthalate ug/l10ND

Fluoranthene ug/l10ND

Pyrene ug/l10ND

Butyl benzyl phthalate ug/l10ND

3,3-Dichlorobenzidine ug/l10ND

Benzanthracene ug/l10ND

Chrysene ug/l10ND

Bis(2-ethylhexyl)phthalate ug/l10ND

Di-n-octyl phthalate ug/l10ND

Benzo(b)fluoranthene ug/l10ND

Benzo(k)fluoranthene ug/l10ND

Benzo(a)pyrene ug/l10ND

Indeno(1,2,3-cd)pyrene ug/l10ND

Dibenz(a,h)anthracene ug/l10ND

Benzo(g,h,i)perylene ug/l10ND

100 15-65Surrogate: 2-Fluorophenol ug/l72.7 S473

100 11-47Surrogate: Phenol-d6 ug/l67.0 S467

100 31-110Surrogate: Nitrobenzene-d5 ug/l78.6 79

100 36-94Surrogate: 2-Fluorobiphenyl ug/l73.3 73

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



100 41-99Surrogate: 2,4,6-Tribromophenol ug/l51.7 52

100 8-56Surrogate: 4-Terphenyl-d14 ug/l65.8 S466

LCS Analyzed: 09/01/2009 (P9H2840-BS1) Q8

Bis(2-chloroethyl)ether 80.0 30-102ug/l1071.5 89

Phenol 80.0 13-56ug/l1055.7 L370

2-Chlorophenol 80.0 39-87ug/l1057.2 72

1,3-Dichlorobenzene 80.0 13-79ug/l1052.9 66



Benzyl alcohol 80.0 29-99ug/l1047.4 V159

Bis(2-chloroisopropyl)ether 80.0 29-98ug/l1067.2 84

2-Methylphenol 80.0 34-85ug/l10ND L4

Hexachloroethane 120 13-72ug/l1076.2 63

n-Nitroso-di-n-propylamine 80.0 30-102ug/l1069.7 87

3&4-Methylphenol 80.0 18-97ug/l10ND L4

Nitrobenzene 80.0 33-111ug/l1075.0 94

Isophorone 80.0 35-111ug/l1064.1 80

2-Nitrophenol 80.0 40-100ug/l1570.9 89

2,4-Dimethylphenol 80.0 41-90ug/l10ND L4

Benzoic acid 200 15-47ug/l25138 L369

Bis(2-chloroethoxy)methane 80.0 31-102ug/l1066.4 83

2,4-Dichlorophenol 80.0 43-93ug/l1053.8 67

1,2,4-Trichlorobenzene 120 22-92ug/l1087.4 73

Naphthalene 80.0 28-107ug/l1065.8 82

4-Chloroaniline 80.0 24-124ug/l10ND L4

Hexachlorobutadiene 80.0 12-73ug/l1056.4 70

4-Chloro-3-methylphenol 80.0 42-97ug/l1039.3 49

2-Methylnaphthalene 80.0 29-100ug/l1064.3 80

Hexachlorocyclopentadiene 80.0 12-74ug/l1053.3 67

2,4,6-Trichlorophenol 80.0 45-98ug/l2061.3 77


2-Chloronaphthalene 120 32-105ug/l1096.4 80

2-Nitroaniline 80.0 31-130ug/l1065.7 82

Acenaphthylene 80.0 35-111ug/l1058.5 73

Dimethyl phthalate 120 16-66ug/l2097.2 L381

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



2,6-Dinitrotoluene 80.0 34-118ug/l1068.1 85

Acenaphthene 80.0 34-114ug/l1066.9 84

3-Nitroaniline 80.0 30-117ug/l1011.4 L414

2,4-Dinitrophenol 120 41-105ug/l5092.5 77

Dibenzofuran 80.0 35-114ug/l1069.3 87


4-Nitrophenol 120 20-57ug/l25125 L3104

Fluorene 80.0 36-117ug/l1070.9 89

4-Chlorophenyl phenyl ether 80.0 32-103ug/l1069.3 87

Diethyl phthalate 80.0 19-86ug/l1068.4 86


4,6-Dinitro-2-methylphenol 120 42-105ug/l50104 87

n-Nitrosodiphenylamine 80.0 31-97ug/l10ND L4

1,2-Diphenylhydrazine (as Azobenzene) 80.0 36-114ug/l1069.4 87

4-Bromophenyl phenyl ether 80.0 33-104ug/l1062.7 78

Hexachlorobenzene 80.0 37-114ug/l1062.5 78

Pentachlorophenol 120 41-110ug/l5090.4 75

Phenanthrene 80.0 38-117ug/l1068.3 85

Anthracene 80.0 37-116ug/l1050.9 64

Di-n-butyl phthalate 80.0 33-105ug/l1069.6 87

Fluoranthene 80.0 39-119ug/l1068.0 85

Pyrene 80.0 39-116ug/l1064.4 80

Butyl benzyl phthalate 80.0 31-100ug/l1069.2 87

3,3-Dichlorobenzidine 80.0 36-111ug/l10ND L4

Benzanthracene 80.0 39-115ug/l1060.6 76

Chrysene 80.0 39-117ug/l1067.3 84

Bis(2-ethylhexyl)phthalate 80.0 35-104ug/l1069.4 87

Di-n-octyl phthalate 80.0 33-102ug/l1082.2 L3103

Benzo(b)fluoranthene 80.0 35-107ug/l1068.9 86

Benzo(k)fluoranthene 80.0 39-115ug/l1083.9 105

Benzo(a)pyrene 80.0 38-113ug/l1047.3 59

Indeno(1,2,3-cd)pyrene 80.0 35-129ug/l1075.7 95

Dibenz(a,h)anthracene 80.0 33-124ug/l1075.1 94

Benzo(g,h,i)perylene 80.0 34-128ug/l1073.6 92

100 20-64Surrogate: 2-Fluorophenol ug/l62.4 62

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers







100 17-61Surrogate: 4-Terphenyl-d14 ug/l59.9 60

LCS Dup Analyzed: 09/01/2009 (P9H2840-BSD1) Q8

Bis(2-chloroethyl)ether 80.0 3530-102ug/l1073.5 92 3

Phenol 80.0 3513-56ug/l1052.5 L366 6

2-Chlorophenol 80.0 3539-87ug/l1056.8 71 1

1,3-Dichlorobenzene 80.0 3513-79ug/l1064.5 L381 20

1,4-Dichlorobenzene 80.0 3515-81ug/l1064.8 81 17


Benzyl alcohol 80.0 3529-99ug/l1016.6 V1, L4, R121 96

Bis(2-chloroisopropyl)ether 80.0 3529-98ug/l1074.5 93 10

2-Methylphenol 80.0 3534-85ug/l10ND L4

Hexachloroethane 120 3513-72ug/l1092.9 L377 20

n-Nitroso-di-n-propylamine 80.0 3530-102ug/l1076.5 96 9

3&4-Methylphenol 80.0 3518-97ug/l10ND L4

Nitrobenzene 80.0 3533-111ug/l1088.5 111 17

Isophorone 80.0 3535-111ug/l1068.9 86 7

2-Nitrophenol 80.0 3540-100ug/l1579.9 100 12

2,4-Dimethylphenol 80.0 3541-90ug/l10ND L4

Benzoic acid 200 3515-47ug/l2596.9 L348 35

Bis(2-chloroethoxy)methane 80.0 3531-102ug/l1072.2 90 8

2,4-Dichlorophenol 80.0 3543-93ug/l1051.1 64 5

1,2,4-Trichlorobenzene 120 3522-92ug/l1097.9 82 11

Naphthalene 80.0 3528-107ug/l1072.1 90 9

4-Chloroaniline 80.0 3524-124ug/l10ND L4

Hexachlorobutadiene 80.0 3512-73ug/l1067.7 L385 18

4-Chloro-3-methylphenol 80.0 3542-97ug/l1030.3 L438 26

2-Methylnaphthalene 80.0 3529-100ug/l1070.5 88 9

Hexachlorocyclopentadiene 80.0 3512-74ug/l1060.4 L375 12

2,4,6-Trichlorophenol 80.0 3545-98ug/l2062.9 79 3


2-Chloronaphthalene 120 3532-105ug/l10104 87 8

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



2-Nitroaniline 80.0 3531-130ug/l1038.1 R648 53

Acenaphthylene 80.0 3535-111ug/l1046.9 59 22

Dimethyl phthalate 120 3516-66ug/l20102 L385 5

2,6-Dinitrotoluene 80.0 3534-118ug/l1070.1 88 3

Acenaphthene 80.0 3534-114ug/l1069.1 86 3

3-Nitroaniline 80.0 3530-117ug/l10ND L4

2,4-Dinitrophenol 120 3541-105ug/l5062.5 R652 39

Dibenzofuran 80.0 3535-114ug/l1072.7 91 5


4-Nitrophenol 120 3520-57ug/l25121 L3101 3

Fluorene 80.0 3536-117ug/l1073.1 91 3

4-Chlorophenyl phenyl ether 80.0 3532-103ug/l1072.1 90 4

Diethyl phthalate 80.0 3519-86ug/l1071.4 L389 4

4-Nitroaniline 80.0 3533-119ug/l103.46 L4, R14 168

4,6-Dinitro-2-methylphenol 120 3542-105ug/l5099.7 83 5

n-Nitrosodiphenylamine 80.0 3531-97ug/l10ND L4

1,2-Diphenylhydrazine (as Azobenzene) 80.0 3536-114ug/l1071.3 89 3

4-Bromophenyl phenyl ether 80.0 3533-104ug/l1067.6 85 8

Hexachlorobenzene 80.0 3537-114ug/l1066.4 83 6

Pentachlorophenol 120 3541-110ug/l5079.2 66 13

Phenanthrene 80.0 3538-117ug/l1070.3 88 3

Anthracene 80.0 3537-116ug/l1044.0 55 15

Di-n-butyl phthalate 80.0 3533-105ug/l1073.2 92 5

Fluoranthene 80.0 3539-119ug/l1069.8 87 3

Pyrene 80.0 3539-116ug/l1067.0 84 4

Butyl benzyl phthalate 80.0 3531-100ug/l1073.5 92 6

3,3-Dichlorobenzidine 80.0 3536-111ug/l10ND L4

Benzanthracene 80.0 3539-115ug/l1062.2 78 3

Chrysene 80.0 3539-117ug/l1071.8 90 6

Bis(2-ethylhexyl)phthalate 80.0 3535-104ug/l1073.8 92 6

Di-n-octyl phthalate 80.0 3533-102ug/l10408 E7, L3, R1510 133

Benzo(b)fluoranthene 80.0 3535-107ug/l10332 E7, L3, R1415 131

Benzo(k)fluoranthene 80.0 3539-115ug/l10401 E7, L3, R1501 131

Benzo(a)pyrene 80.0 3538-113ug/l1095.3 E7, L3, R1119 67

Indeno(1,2,3-cd)pyrene 80.0 3535-129ug/l10359 E7, L3, R1449 130

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Dibenz(a,h)anthracene 80.0 3533-124ug/l10361 E7, L3, R1451 131

Benzo(g,h,i)perylene 80.0 3534-128ug/l10329 E7, L3, R1411 127









Bis(2-chloroethyl)ether ug/l10ND

Phenol ug/l10ND

2-Chlorophenol ug/l10ND




Benzyl alcohol ug/l10ND

Bis(2-chloroisopropyl)ether ug/l10ND

2-Methylphenol ug/l10ND

Hexachloroethane ug/l10ND

n-Nitroso-di-n-propylamine ug/l10ND

3&4-Methylphenol ug/l10ND

Nitrobenzene ug/l10ND

Isophorone ug/l10ND


2,4-Dimethylphenol ug/l10ND

Benzoic acid ug/l25ND

Bis(2-chloroethoxy)methane ug/l10ND

2,4-Dichlorophenol ug/l10ND

1,2,4-Trichlorobenzene ug/l10ND

Naphthalene ug/l10ND

4-Chloroaniline ug/l10ND

Hexachlorobutadiene ug/l10ND

4-Chloro-3-methylphenol ug/l10ND

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



2-Methylnaphthalene ug/l10ND

Hexachlorocyclopentadiene ug/l10ND



2-Chloronaphthalene ug/l10ND


Acenaphthylene ug/l10ND

Dimethyl phthalate ug/l20ND


Acenaphthene ug/l10ND


2,4-Dinitrophenol ug/l50ND

Dibenzofuran ug/l10ND



Fluorene ug/l10ND

4-Chlorophenyl phenyl ether ug/l10ND

Diethyl phthalate ug/l10ND


4,6-Dinitro-2-methylphenol ug/l50ND

n-Nitrosodiphenylamine ug/l10ND

1,2-Diphenylhydrazine (as Azobenzene) ug/l10ND

4-Bromophenyl phenyl ether ug/l10ND

Hexachlorobenzene ug/l10ND

Pentachlorophenol ug/l50ND

Phenanthrene ug/l10ND

Anthracene ug/l10ND

Di-n-butyl phthalate ug/l10ND

Fluoranthene ug/l10ND

Pyrene ug/l10ND

Butyl benzyl phthalate ug/l10ND

3,3-Dichlorobenzidine ug/l10ND

Benzanthracene ug/l10ND

Chrysene ug/l10ND

Bis(2-ethylhexyl)phthalate ug/l10ND

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Di-n-octyl phthalate ug/l10ND

Benzo(b)fluoranthene ug/l10ND

Benzo(k)fluoranthene ug/l10ND

Benzo(a)pyrene ug/l10ND

Indeno(1,2,3-cd)pyrene ug/l10ND

Dibenz(a,h)anthracene ug/l10ND

Benzo(g,h,i)perylene ug/l10ND


100 11-47Surrogate: Phenol-d6 ug/l26.0 26






Bis(2-chloroethyl)ether 80.0 30-102ug/l1048.2 60

Phenol 80.0 13-56ug/l1024.2 30

2-Chlorophenol 80.0 39-87ug/l1048.7 61




Benzyl alcohol 80.0 29-99ug/l1041.3 52

Bis(2-chloroisopropyl)ether 80.0 29-98ug/l1048.9 61

2-Methylphenol 80.0 34-85ug/l1043.3 54

Hexachloroethane 120 13-72ug/l1059.9 50

n-Nitroso-di-n-propylamine 80.0 30-102ug/l1051.9 65

3&4-Methylphenol 80.0 18-97ug/l1038.4 48

Nitrobenzene 80.0 33-111ug/l1051.0 64

Isophorone 80.0 35-111ug/l1047.5 59

2-Nitrophenol 80.0 40-100ug/l1553.4 67

2,4-Dimethylphenol 80.0 41-90ug/l1046.0 57

Benzoic acid 200 15-47ug/l2538.8 19

Bis(2-chloroethoxy)methane 80.0 31-102ug/l1048.9 61

2,4-Dichlorophenol 80.0 43-93ug/l1050.5 63

1,2,4-Trichlorobenzene 120 22-92ug/l1074.0 62

Naphthalene 80.0 28-107ug/l1050.6 63

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



4-Chloroaniline 80.0 24-124ug/l1043.2 54

Hexachlorobutadiene 80.0 12-73ug/l1034.8 43

4-Chloro-3-methylphenol 80.0 42-97ug/l1049.7 62

2-Methylnaphthalene 80.0 29-100ug/l1049.3 62

Hexachlorocyclopentadiene 80.0 12-74ug/l1031.9 40



2-Chloronaphthalene 120 32-105ug/l1080.9 67


Acenaphthylene 80.0 35-111ug/l1051.8 65

Dimethyl phthalate 120 16-66ug/l2085.2 L371


Acenaphthene 80.0 34-114ug/l1052.5 66


2,4-Dinitrophenol 120 41-105ug/l5075.1 63

Dibenzofuran 80.0 35-114ug/l1052.6 66


4-Nitrophenol 120 20-57ug/l2540.8 34

Fluorene 80.0 36-117ug/l1054.1 68

4-Chlorophenyl phenyl ether 80.0 32-103ug/l1052.0 65

Diethyl phthalate 80.0 19-86ug/l1050.7 63


4,6-Dinitro-2-methylphenol 120 42-105ug/l5082.4 69

n-Nitrosodiphenylamine 80.0 31-97ug/l1045.0 56

1,2-Diphenylhydrazine (as Azobenzene) 80.0 36-114ug/l1051.2 64

4-Bromophenyl phenyl ether 80.0 33-104ug/l1049.3 62

Hexachlorobenzene 80.0 37-114ug/l1050.1 63

Pentachlorophenol 120 41-110ug/l5080.8 67

Phenanthrene 80.0 38-117ug/l1052.1 65

Anthracene 80.0 37-116ug/l1052.0 65

Di-n-butyl phthalate 80.0 33-105ug/l1053.7 67

Fluoranthene 80.0 39-119ug/l1053.5 67

Pyrene 80.0 39-116ug/l1051.6 65

Butyl benzyl phthalate 80.0 31-100ug/l1051.0 64

3,3-Dichlorobenzidine 80.0 36-111ug/l1052.8 66

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Benzanthracene 80.0 39-115ug/l1050.6 63

Chrysene 80.0 39-117ug/l1052.5 66

Bis(2-ethylhexyl)phthalate 80.0 35-104ug/l1052.2 65

Di-n-octyl phthalate 80.0 33-102ug/l1049.8 62

Benzo(b)fluoranthene 80.0 35-107ug/l1045.9 57

Benzo(k)fluoranthene 80.0 39-115ug/l1052.6 66

Benzo(a)pyrene 80.0 38-113ug/l1049.8 62

Indeno(1,2,3-cd)pyrene 80.0 35-129ug/l1050.4 63

Dibenz(a,h)anthracene 80.0 33-124ug/l1050.7 63

Benzo(g,h,i)perylene 80.0 34-128ug/l1050.2 63








Bis(2-chloroethyl)ether 80.0 3530-102ug/l1047.0 59 3

Phenol 80.0 3513-56ug/l1021.6 27 11

2-Chlorophenol 80.0 3539-87ug/l1046.6 58 5




Benzyl alcohol 80.0 3529-99ug/l1039.1 49 6

Bis(2-chloroisopropyl)ether 80.0 3529-98ug/l1048.3 60 1

2-Methylphenol 80.0 3534-85ug/l1040.9 51 6

Hexachloroethane 120 3513-72ug/l1048.5 40 21

n-Nitroso-di-n-propylamine 80.0 3530-102ug/l1049.9 62 4

3&4-Methylphenol 80.0 3518-97ug/l1036.7 46 5

Nitrobenzene 80.0 3533-111ug/l1050.8 64 0

Isophorone 80.0 3535-111ug/l1046.7 58 2

2-Nitrophenol 80.0 3540-100ug/l1547.2 59 12

2,4-Dimethylphenol 80.0 3541-90ug/l1046.4 58 1

Benzoic acid 200 3515-47ug/l25ND L4

Bis(2-chloroethoxy)methane 80.0 3531-102ug/l1049.2 61 1

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



2,4-Dichlorophenol 80.0 3543-93ug/l1048.4 60 4

1,2,4-Trichlorobenzene 120 3522-92ug/l1066.5 55 11

Naphthalene 80.0 3528-107ug/l1047.7 60 6

4-Chloroaniline 80.0 3524-124ug/l1046.0 57 6

Hexachlorobutadiene 80.0 3512-73ug/l1027.3 34 24

4-Chloro-3-methylphenol 80.0 3542-97ug/l1048.9 61 2

2-Methylnaphthalene 80.0 3529-100ug/l1046.2 58 6

Hexachlorocyclopentadiene 80.0 3512-74ug/l1026.2 33 20



2-Chloronaphthalene 120 3532-105ug/l1078.2 65 3

2-Nitroaniline 80.0 3531-130ug/l1055.0 69 0

Acenaphthylene 80.0 3535-111ug/l1050.3 63 3

Dimethyl phthalate 120 3516-66ug/l2084.9 L371 0


Acenaphthene 80.0 3534-114ug/l1050.9 64 3


2,4-Dinitrophenol 120 3541-105ug/l5050.8 R642 39

Dibenzofuran 80.0 3535-114ug/l1051.3 64 3


4-Nitrophenol 120 3520-57ug/l2528.1 R623 37

Fluorene 80.0 3536-117ug/l1053.2 67 2

4-Chlorophenyl phenyl ether 80.0 3532-103ug/l1050.6 63 3

Diethyl phthalate 80.0 3519-86ug/l1051.3 64 1


4,6-Dinitro-2-methylphenol 120 3542-105ug/l5078.5 65 5

n-Nitrosodiphenylamine 80.0 3531-97ug/l1046.2 58 3

1,2-Diphenylhydrazine (as Azobenzene) 80.0 3536-114ug/l1052.3 65 2

4-Bromophenyl phenyl ether 80.0 3533-104ug/l1049.7 62 1

Hexachlorobenzene 80.0 3537-114ug/l1051.2 64 2

Pentachlorophenol 120 3541-110ug/l5081.8 68 1

Phenanthrene 80.0 3538-117ug/l1053.5 67 3

Anthracene 80.0 3537-116ug/l1053.3 67 2

Di-n-butyl phthalate 80.0 3533-105ug/l1053.3 67 1

Fluoranthene 80.0 3539-119ug/l1055.3 69 3

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Pyrene 80.0 3539-116ug/l1053.7 67 4

Butyl benzyl phthalate 80.0 3531-100ug/l1051.1 64 0

3,3-Dichlorobenzidine 80.0 3536-111ug/l1053.0 66 1

Benzanthracene 80.0 3539-115ug/l1051.2 64 1

Chrysene 80.0 3539-117ug/l1052.9 66 1

Bis(2-ethylhexyl)phthalate 80.0 3535-104ug/l1054.3 68 4

Di-n-octyl phthalate 80.0 3533-102ug/l1052.5 66 5

Benzo(b)fluoranthene 80.0 3535-107ug/l1047.4 59 3

Benzo(k)fluoranthene 80.0 3539-115ug/l1053.4 67 1

Benzo(a)pyrene 80.0 3538-113ug/l1050.6 63 2

Indeno(1,2,3-cd)pyrene 80.0 3535-129ug/l1051.7 65 3

Dibenz(a,h)anthracene 80.0 3533-124ug/l1052.1 65 3

Benzo(g,h,i)perylene 80.0 3534-128ug/l1051.1 64 2







Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Aluminum mg/l0.20ND

Antimony mg/l0.040ND

Arsenic mg/l0.10ND

Barium mg/l0.010ND

Beryllium mg/l0.0010ND

Boron mg/l0.20ND

Cadmium mg/l0.0010ND

Calcium mg/l2.0ND

Chromium mg/l0.010ND

Cobalt mg/l0.010ND

Copper mg/l0.010ND

Iron mg/l0.050ND

Lead mg/l0.015ND

Magnesium mg/l2.0ND

Manganese mg/l0.010ND

Molybdenum mg/l0.010ND

Nickel mg/l0.010ND

Potassium mg/l2.0ND

Selenium mg/l0.10ND

Silica mg/l0.21ND

Silver mg/l0.010ND

Sodium mg/l2.0ND

Thallium mg/l0.10ND

Vanadium mg/l0.010ND

Zinc mg/l0.050ND

LCS Analyzed: 08/24/2009 (P9H2132-BS1)

Aluminum 1.00 85-115mg/l0.201.00 100

Antimony 0.500 85-115mg/l0.0400.531 106

Arsenic 0.500 85-115mg/l0.100.530 106

Barium 0.500 85-115mg/l0.0100.518 104

Beryllium 0.500 85-115mg/l0.00100.531 106

Boron 0.500 85-115mg/l0.200.488 98

Cadmium 0.500 85-115mg/l0.00100.526 105

Calcium 10.5 85-115mg/l2.010.7 102

Chromium 0.500 85-115mg/l0.0100.517 103

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Cobalt 0.500 85-115mg/l0.0100.531 106

Copper 0.500 85-115mg/l0.0100.520 104

Iron 0.500 85-115mg/l0.0500.513 103

Lead 0.500 85-115mg/l0.0150.532 106

Magnesium 10.5 85-115mg/l2.010.9 104

Manganese 0.500 85-115mg/l0.0100.527 105

Molybdenum 0.500 85-115mg/l0.0100.520 104

Nickel 0.500 85-115mg/l0.0100.531 106

Potassium 10.0 85-115mg/l2.010.2 102

Selenium 0.500 85-115mg/l0.100.538 108

Silica 5.35 85-115mg/l0.215.36 100

Silver 0.500 85-115mg/l0.0100.524 105

Sodium 10.0 85-115mg/l2.010.3 103

Thallium 0.500 85-115mg/l0.100.532 106

Vanadium 0.500 85-115mg/l0.0100.525 105

Zinc 0.500 85-115mg/l0.0500.534 107

LCS Dup Analyzed: 08/24/2009 (P9H2132-BSD1)

Aluminum 1.00 2085-115mg/l0.200.974 97 3

Antimony 0.500 2085-115mg/l0.0400.522 104 2

Arsenic 0.500 2085-115mg/l0.100.523 105 1

Barium 0.500 2085-115mg/l0.0100.512 102 1

Beryllium 0.500 2085-115mg/l0.00100.525 105 1

Boron 0.500 2085-115mg/l0.200.485 97 1

Cadmium 0.500 2085-115mg/l0.00100.520 104 1

Calcium 10.5 2085-115mg/l2.010.7 102 1

Chromium 0.500 2085-115mg/l0.0100.510 102 1

Cobalt 0.500 2085-115mg/l0.0100.523 105 2

Copper 0.500 2085-115mg/l0.0100.513 103 1

Iron 0.500 2085-115mg/l0.0500.515 103 0

Lead 0.500 2085-115mg/l0.0150.523 105 2

Magnesium 10.5 2085-115mg/l2.010.9 103 1

Manganese 0.500 2085-115mg/l0.0100.521 104 1

Molybdenum 0.500 2085-115mg/l0.0100.517 103 1

Nickel 0.500 2085-115mg/l0.0100.523 105 1

Potassium 10.0 2085-115mg/l2.010.2 102 0

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Selenium 0.500 2085-115mg/l0.100.549 110 2

Silica 5.35 2085-115mg/l0.215.32 99 1

Silver 0.500 2085-115mg/l0.0100.518 104 1

Sodium 10.0 2085-115mg/l2.010.3 103 1

Thallium 0.500 2085-115mg/l0.100.525 105 1

Vanadium 0.500 2085-115mg/l0.0100.518 104 1

Zinc 0.500 2085-115mg/l0.0500.528 106 1

Matrix Spike Analyzed: 08/24/2009 (P9H2132-MS1) Source: PSH1198-01

Aluminum 1.00 75-125mg/l0.201.19 0.210 98

Antimony 0.500 75-125mg/l0.0400.534 ND 107

Arsenic 0.500 75-125mg/l0.100.552 ND 110

Barium 0.500 75-125mg/l0.0100.637 0.131 101

Beryllium 0.500 75-125mg/l0.00100.526 ND 105

Boron 0.500 75-125mg/l0.200.705 0.207 100

Cadmium 0.500 75-125mg/l0.00100.517 ND 103

Calcium 10.5 75-125mg/l2.0100 M296.1 38

Chromium 0.500 75-125mg/l0.0100.508 ND 102

Cobalt 0.500 75-125mg/l0.0100.525 ND 105

Copper 0.500 75-125mg/l0.0100.533 ND 107

Iron 0.500 75-125mg/l0.0500.554 ND 111

Lead 0.500 75-125mg/l0.0150.523 ND 105

Magnesium 10.5 75-125mg/l2.042.0 33.3 82

Manganese 0.500 75-125mg/l0.0100.520 ND 104

Molybdenum 0.500 75-125mg/l0.0100.531 0.00786 105

Nickel 0.500 75-125mg/l0.0100.525 ND 105

Potassium 10.0 75-125mg/l2.015.6 5.74 99

Selenium 0.500 75-125mg/l0.100.560 ND 112

Silica 5.35 75-125mg/l0.2114.9 9.87 95

Silver 0.500 75-125mg/l0.0100.527 ND 105

Sodium 10.0 75-125mg/l2.0152 M2153 -8

Thallium 0.500 75-125mg/l0.100.531 ND 106

Vanadium 0.500 75-125mg/l0.0100.522 0.00206 104

Zinc 0.500 75-125mg/l0.0500.538 ND 108

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Aluminum 1.00 75-125mg/l0.200.972 ND 97

Antimony 0.500 75-125mg/l0.0400.533 ND 107

Arsenic 0.500 75-125mg/l0.100.556 ND 111

Barium 0.500 75-125mg/l0.0100.533 0.0262 101

Beryllium 0.500 75-125mg/l0.00100.531 ND 106

Boron 0.500 75-125mg/l0.201.10 0.618 97

Cadmium 0.500 75-125mg/l0.00100.518 ND 104

Calcium 10.5 75-125mg/l2.075.7 M271.1 43

Chromium 0.500 75-125mg/l0.0100.506 ND 101

Cobalt 0.500 75-125mg/l0.0100.522 ND 104

Copper 0.500 75-125mg/l0.0100.576 0.0431 107

Iron 0.500 75-125mg/l0.0500.545 ND 109

Lead 0.500 75-125mg/l0.0150.514 ND 103

Magnesium 10.5 75-125mg/l2.038.6 29.7 85

Manganese 0.500 75-125mg/l0.0100.524 0.00367 104

Molybdenum 0.500 75-125mg/l0.0100.528 0.0104 103

Nickel 0.500 75-125mg/l0.0100.519 ND 104

Potassium 10.0 75-125mg/l2.014.9 4.86 101

Selenium 0.500 75-125mg/l0.100.585 ND 117

Silica 5.35 75-125mg/l0.2132.7 28.3 83

Silver 0.500 75-125mg/l0.0100.530 ND 106

Sodium 10.0 75-125mg/l2.0375 M2390 -156

Thallium 0.500 75-125mg/l0.100.556 ND 111

Vanadium 0.500 75-125mg/l0.0100.527 0.00577 104

Zinc 0.500 75-125mg/l0.0500.555 ND 111

Matrix Spike Dup Analyzed: 08/24/2009 (P9H2132-MSD1) Source: PSH1198-01

Aluminum 1.00 1075-125mg/l0.201.24 0.210 103 5

Antimony 0.500 1075-125mg/l0.0400.537 ND 107 0

Arsenic 0.500 1075-125mg/l0.100.551 ND 110 0

Barium 0.500 1075-125mg/l0.0100.651 0.131 104 2

Beryllium 0.500 1075-125mg/l0.00100.537 ND 107 2

Boron 0.500 1075-125mg/l0.200.726 0.207 104 3

Cadmium 0.500 1075-125mg/l0.00100.530 ND 106 3

Calcium 10.5 1075-125mg/l2.0106 96.1 94 6

Chromium 0.500 1075-125mg/l0.0100.517 ND 103 2

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Cobalt 0.500 1075-125mg/l0.0100.531 ND 106 1

Copper 0.500 1075-125mg/l0.0100.539 ND 108 1

Iron 0.500 1075-125mg/l0.0500.561 ND 112 1

Lead 0.500 1075-125mg/l0.0150.525 ND 105 0

Magnesium 10.5 1075-125mg/l2.043.6 33.3 98 4

Manganese 0.500 1075-125mg/l0.0100.529 ND 106 2

Molybdenum 0.500 1075-125mg/l0.0100.534 0.00786 105 1

Nickel 0.500 1075-125mg/l0.0100.527 ND 105 1

Potassium 10.0 1075-125mg/l2.016.0 5.74 103 2

Selenium 0.500 1075-125mg/l0.100.562 ND 112 0

Silica 5.35 1075-125mg/l0.2115.5 9.87 105 4

Silver 0.500 1075-125mg/l0.0100.530 ND 106 0

Sodium 10.0 1075-125mg/l2.0161 153 83 6

Thallium 0.500 1075-125mg/l0.100.562 ND 112 6

Vanadium 0.500 1075-125mg/l0.0100.527 0.00206 105 1

Zinc 0.500 1075-125mg/l0.0500.541 ND 108 1


Aluminum 1.00 1075-125mg/l0.201.04 ND 104 7

Antimony 0.500 1075-125mg/l0.0400.541 ND 108 1

Arsenic 0.500 1075-125mg/l0.100.562 ND 112 1

Barium 0.500 1075-125mg/l0.0100.538 0.0262 102 1

Beryllium 0.500 1075-125mg/l0.00100.538 ND 108 1

Boron 0.500 1075-125mg/l0.201.12 0.618 101 2

Cadmium 0.500 1075-125mg/l0.00100.525 ND 105 1

Calcium 10.5 1075-125mg/l2.075.6 M271.1 43 0

Chromium 0.500 1075-125mg/l0.0100.514 ND 103 1

Cobalt 0.500 1075-125mg/l0.0100.531 ND 106 2

Copper 0.500 1075-125mg/l0.0100.583 0.0431 108 1

Iron 0.500 1075-125mg/l0.0500.544 ND 109 0

Lead 0.500 1075-125mg/l0.0150.525 ND 105 2

Magnesium 10.5 1075-125mg/l2.038.5 29.7 84 0

Manganese 0.500 1075-125mg/l0.0100.531 0.00367 105 1

Molybdenum 0.500 1075-125mg/l0.0100.533 0.0104 105 1

Nickel 0.500 1075-125mg/l0.0100.526 ND 105 1

Potassium 10.0 1075-125mg/l2.014.9 4.86 100 0

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Selenium 0.500 1075-125mg/l0.100.569 ND 114 3

Silica 5.35 1075-125mg/l0.2133.1 28.3 90 1

Silver 0.500 1075-125mg/l0.0100.534 ND 107 1

Sodium 10.0 1075-125mg/l2.0378 M2390 -127 1

Thallium 0.500 1075-125mg/l0.100.555 ND 111 0

Vanadium 0.500 1075-125mg/l0.0100.532 0.00577 105 1

Zinc 0.500 1075-125mg/l0.0500.563 ND 113 1

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS BY ICP/MS


Data

Qualifiers



Uranium mg/l0.0010ND


Uranium 0.100 85-115mg/l0.00100.106 106


Uranium 0.100 2085-115mg/l0.00100.105 105 0


Uranium 0.100 70-130mg/l0.00100.249 0.135 114


Uranium 0.100 70-130mg/l0.00100.115 0.000124 115


Uranium 0.100 1570-130mg/l0.00100.246 0.135 111 1


Uranium 0.100 1570-130mg/l0.00100.114 0.000124 114 1

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Mercury mg/l0.00050ND


Mercury 0.0100 85-115mg/l0.000500.0101 101


Mercury 0.0100 2085-115mg/l0.000500.00978 98 4


Mercury 0.0100 85-115mg/l0.000500.0103 ND 103


Mercury 0.0100 2085-115mg/l0.000500.00944 ND 94 9

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers



Perchlorate ug/l2.0ND


Perchlorate 25.0 85-115ug/l2.025.8 103


Perchlorate 25.0 1585-115ug/l2.025.7 103 0

Duplicate Analyzed: 08/25/2009 (P9H2523-DUP1) Source: PSH1219-23

Perchlorate 15ug/l2.0ND ND


Perchlorate 25.0 80-120ug/l2.026.5 ND 106


Perchlorate 25.0 1580-120ug/l2.027.6 ND 110 4

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers

Batch: 9I02126 Extracted: 09/02/09

Blank Analyzed: 09/02/2009 (9I02126-BLK1)

Total Cyanide mg/l0.020ND

LCS Analyzed: 09/02/2009 (9I02126-BS1)

Total Cyanide 0.200 90-110mg/l0.0200.211 105

Matrix Spike Analyzed: 09/02/2009 (9I02126-MS1) Source: ISH2516-01

Total Cyanide 0.200 70-115mg/l0.0200.208 ND 104

Matrix Spike Dup Analyzed: 09/02/2009 (9I02126-MSD1) Source: ISH2516-01

Total Cyanide 0.200 1570-115mg/l0.0200.202 ND 101 3

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

SW846 8330


Data

Qualifiers

Batch: 9239332 Extracted: 08/27/09

Blank Analyzed: 09/06/2009 (G9H270000332B) Source:

1,3,5-Trinitrobenzene -ug/L0.1ND

1,3-Dinitrobenzene -ug/L0.1ND

2,4,6-Trinitrotoluene -ug/L0.1ND

2,4-Dinitrotoluene -ug/L0.1ND

2,6-Dinitrotoluene -ug/L0.1ND

2-Amino-4,6-dinitrotoluene -ug/L0.2ND

2-Nitrotoluene -ug/L0.5ND

3-Nitrotoluene -ug/L0.5ND V8

4-Amino-2,6-dinitrotoluene -ug/L0.1ND

4-Nitrotoluene -ug/L0.5ND

HMX -ug/L0.1ND

Nitrobenzene -ug/L0.1ND

RDX -ug/L0.1ND

Tetryl -ug/L0.1ND

2.5 79-111Surrogate: 3,4-Dinitrotoluene ug/L2.4 96

LCS Analyzed: 09/06/2009 (G9H270000332C) Source:

1,3,5-Trinitrobenzene 1 2974-120ug/L0.11.08 108 1

1,3-Dinitrobenzene 1 2972-123ug/L0.11.08 108 1

2,4,6-Trinitrotoluene 1 2869-111ug/L0.11.02 102 0

2,4-Dinitrotoluene 1 3070-119ug/L0.11.02 102 0


2-Amino-4,6-dinitrotoluene 1 2777-123ug/L0.21.09 109 0

2-Nitrotoluene 1 3664-120ug/L0.51.02 102 2

3-Nitrotoluene 1 3167-114ug/L0.50.986 V899 1



HMX 1 3267-115ug/L0.11.12 112 1

Nitrobenzene 1 3169-119ug/L0.11.1 110 1

RDX 1 3268-122ug/L0.11.14 114 1

Tetryl 1 2666-105ug/L0.10.989 99 0


Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

SW846 8330


Data

Qualifiers

Batch: 9239332 Extracted: 08/27/09

LCS Dup Analyzed: 09/06/2009 (G9H270000332L) Source:

1,3,5-Trinitrobenzene 1 2974-120ug/L0.11.08 108 1

1,3-Dinitrobenzene 1 2972-123ug/L0.11.07 107 1

2,4,6-Trinitrotoluene 1 2869-111ug/L0.11.02 102 0





3-Nitrotoluene 1 3167-114ug/L0.50.978 V898 1



HMX 1 3267-115ug/L0.11.1 110 1

Nitrobenzene 1 3169-119ug/L0.11.09 109 1

RDX 1 3268-122ug/L0.11.13 113 1

Tetryl 1 2666-105ug/L0.10.986 99 0


Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN


D1 Sample required dilution due to matrix.

E7 Concentration estimated. Internal standard recoveries did not meet laboratory acceptance criteria.

H4 Sample was extracted past required extraction holding time, but analyzed within analysis holding time.


L4 The associated blank spike recovery was below method acceptance limits.

M2 Matrix spike recovery was low; the associated blank spike recovery was acceptable.


Q8 Insufficient sample received to meet method QC requirements. Batch QC requirements satisfy ADEQ policies

0154.000 and 0155.000.

R1 The RPD/RSD exceeded the method acceptance limit.

R6 LFB/LFBD RPD exceeded the method acceptance limit. Recovery met acceptance criteria.

S10 Surrogate recovery was above laboratory and method acceptance limits. See case narrative.

S4 Surrogate recovery was above laboratory and method acceptance limits. No target analytes were detected in the

sample.

S6 Surrogate recovery was below laboratory and method acceptance limits. Reextraction and/or reanalysis confirms low

recovery caused by matrix effect.


V8 Calibration verification recovery was below the method control limit for this analyte, however the average %

difference or % drift for all the analytes met method criteria.



Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




454-9303





Sampled:

Received:

08/21/09


Project ID:

PSH1228

14682.013 PGAN



TestAmerica Phoenix

Water XE200.7

Water XE200.8

Water XE314

Water XSW7470A

Water XSW8260B

XWater XSW8270C



Subcontracted Laboratories

TestAmerica - Irvine, CA NELAC Cert #01108CA, California Cert #1197, Arizona Cert #AZ0671, Nevada Cert #CA72-2002-63

17461 Derian Ave. Suite 100 - Irvine, CA 92614

Method Performed: SM4500CN-ESamples: PSH1228-03

TestAmerica West Sacramento Arizona Cert #AZ0616

880 Riverside Parkway - West Sacramento, CA 95605

Method Performed: SW846 8330Samples: PSH1228-05

Project Manager

TestAmerica Phoenix

PSH1228

Tina Paulauskas




TAL-0013-550 (12/08)

Client Name I Address: /1n..e-c. . Vv. f,.f",, i ·s-' t }t; t . $?"J? i5 1/t>. el.e 5Lp'ff~ J"' /"{ l'h 1J))f8 ~

Project Manager~~ y[t4>t /fJc.JVe.,..;.q..,.,

Sampler:

1-Pirc., Lw~--tvrt--( Sample gescription Sample Container

Matrix - Typ~

CHAIN OF CUSTODY FOR.M.

A(] Phoenix- 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454~9303 [ 1 Tucson- 1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 80Y-3801 FAX (520) 807~3803 [ 1 Las Vegas - 2520 E. Sunset, Suite 3; Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

Project/ PO Number:

}lf!;i'). ~J) Analysis Required

. f)4fli/ ~

~

Phone Number: q ~II-)..).).-8 J t, J ~ ~ <'l.

~ ~~

~ ~ ~ -~ ~ --...

'l/:,IJ-J it~ -J )._ '15 -..c-..... '-

~~ Fax Number: ~~ ~f"\ ~--~ ~--~~ -.1 ~ ~ #of Sampling Sampling 'J

Cont. Date Time Preservatives

Page__j_ of

?~(lyf /rff Special Instructions

JjJJifFITlk -~!?_J_j)JtJI!f #)I) ~~ X J'8)).J/#1 /);5 ~~ X X f0:\ rJ 1.2 2..~ -- I //}PI I - ~o )f :J/fiJ1 \ V/lf I - - -HLL- X ~ ·2..

' J} I d i h.,)z -oJ d-1 dtYiJ 1 S"rf"" I 'I ) fJ&/)f/1>? I )OS ~ X "X - 5 v u 1 -h~!J -/Jf{::J-1 )/)IJ t1 / 1J:b4- :2. pEj J.//11 /l:Jl hp-;..L" )( -Lj

jJ )J (f ~~-Jz -tJ! )I :W0Cf . ~ ... .r. ~ . 2 13/J-11/P/ }J-t t " ')( ' v ·-s ,,_;' h~nl. /

_...,

Re~~~,~----·· ;1/JJ/;t;J//tJ~ Received By: Date/Time: Turnaround Time: (Check)

15/J ~ 7. same day 72 hours :4".1Y"' .--/

Ri!Mriqu~ Date/Time: ~ceived By: Date/Time: 24 hours 5 days

/ 48 hours normal ID RelinqUished By: Date/Time: (_ ;:e~ Date/Time:

t<::K Sample ll)tegrity: (Check)

-~/Z!/61 intact A on ice X Note: B relin uishin sam les to TestAmerica' client a rees to a for the servic~~ re uested on this chain of c~ftod form and an additional an:alyses performed on this reject.

{ y q g P • g PY q y y p

Payment for services is due within 30 days from the d<)te of invoice. Sample(s) will be disposed of after 30 days.

---------~~-~..,.--~---~----~-'-----~------------~~-~-~---~--


454-9303

LABORATORY REPORT




Attention: Brian Mcnamara 09/01/09

09/01/09

10/27/09 11:21







Sampled:

Received:

Revised:

Project: PGAN 14682.013


CASE NARRATIVE


PSI0067-01 Bld1-47-09012009 Water

PSI0067-02 Bld1-47-09012009 Soil

PSI0067-03 TB001-09012009 Water

PSI0067-04 Bld1 Tank-09012009 Water


Soil sample for volatile analysis was received as an Encore sample.







N1-The MS and/or MSD were above the acceptance limits. See Blank Spike (LCS).

COMMENTS: Results that fall between the MDL and RL are 'J' flagged.


Report revised 10/27/2009 to report full VOC list for sample PSI0067-01 and PSI0067-03 per client's

request.

ADDITIONAL

INFORMATION:

Reviewed By:

Project Manager

TestAmerica Phoenix

PSI0067

Kylie Emily For Tina Paulauskas

<Page 1 of 31>


454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSI0067-01 (Bld1-47-09012009 - Water) Sampled: 09/01/09Reporting Units: ug/l

SW8260B1,1,2,2-Tetrachloroethane P9I1205 1.0 ND E809/12/09 09/12/0910.12

SW8260B1,1-Dichloroethene P9I1205 1.0 ND E809/12/09 09/12/0910.23

SW8260B1,2-Dichloropropane P9I1205 1.0 ND E809/12/09 09/12/0910.15

2-Butanone (MEK) SW8260B P9I1205 315.0 09/12/09 09/12/0911.8

Acetone SW8260B P9I1205 10020 09/12/09 09/12/0913.8

Benzene SW8260B P9I1205 0.571.0 E409/12/09 09/12/0910.15

SW8260BCarbon tetrachloride P9I1205 1.0 ND E809/12/09 09/12/0910.19

SW8260BChloroform P9I1205 1.0 ND E809/12/09 09/12/0910.16

SW8260Bcis-1,2-Dichloroethene P9I1205 1.0 ND E809/12/09 09/12/0910.18

SW8260BEthylbenzene P9I1205 1.0 ND E809/12/09 09/12/0910.16

SW8260Bm,p-Xylenes P9I1205 2.0 ND E809/12/09 09/12/0910.35

SW8260BMethylene Chloride P9I1205 2.0 ND E809/12/09 09/12/0910.50

SW8260Bo-Xylene P9I1205 1.0 ND E809/12/09 09/12/0910.19

SW8260BTetrachloroethene P9I1205 1.0 ND E809/12/09 09/12/0910.23

SW8260BToluene P9I1205 1.0 ND E809/12/09 09/12/0910.35

SW8260Btrans-1,2-Dichloroethene P9I1205 1.0 ND E809/12/09 09/12/0910.22

SW8260BTrichloroethene P9I1205 1.0 ND E809/12/09 09/12/0910.19

Trichlorofluoromethane SW8260B P9I1205 0.671.0 E409/12/09 09/12/0910.17

SW8260BVinyl chloride P9I1205 1.0 ND E809/12/09 09/12/0910.24

SW8260B1,1,1-Trichloroethane P9I1205 1.0 ND E809/12/09 09/12/0910.22


SW8260B1,1-Dichloroethane P9I1205 1.0 ND E809/12/09 09/12/0910.17

SW8260B1,1-Dichloropropene P9I1205 1.0 ND E809/12/09 09/12/0910.19

SW8260B1,2,3-Trichlorobenzene P9I1205 2.0 ND E809/12/09 09/12/0910.27

SW8260B1,2,3-Trichloropropane P9I1205 2.0 ND E809/12/09 09/12/0910.31


1,2,4-Trimethylbenzene SW8260B P9I1205 0.391.0 E409/12/09 09/12/0910.13

SW8260B1,2-Dibromoethane (EDB) P9I1205 1.0 ND E809/12/09 09/12/0910.14

SW8260B1,2-Dichlorobenzene P9I1205 1.0 ND E809/12/09 09/12/0910.12


SW8260B1,3,5-Trimethylbenzene P9I1205 1.0 ND E809/12/09 09/12/0910.16





SW8260B2-Chlorotoluene P9I1205 1.0 ND E809/12/09 09/12/0910.17

SW8260B2-Hexanone P9I1205 5.0 ND E809/12/09 09/12/0910.31


4-Methyl-2-pentanone (MIBK) SW8260B P9I1205 2.65.0 E409/12/09 09/12/0910.43

SW8260BBromobenzene P9I1205 1.0 ND E809/12/09 09/12/0910.15

Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSI0067-01 (Bld1-47-09012009 - Water) - cont. Sampled: 09/01/09Reporting Units: ug/l

SW8260BBromochloromethane P9I1205 1.0 ND E809/12/09 09/12/0910.20

SW8260BBromodichloromethane P9I1205 1.0 ND E809/12/09 09/12/0910.15

SW8260BBromoform P9I1205 1.0 ND E809/12/09 09/12/0910.19

SW8260BBromomethane P9I1205 2.0 ND E809/12/09 09/12/0910.22

SW8260BChlorobenzene P9I1205 1.0 ND E809/12/09 09/12/0910.12

SW8260BChloroethane P9I1205 1.0 ND E809/12/09 09/12/0910.26

SW8260BChloromethane P9I1205 5.0 ND E809/12/09 09/12/0910.20

SW8260Bcis-1,3-Dichloropropene P9I1205 1.0 ND E809/12/09 09/12/0910.17

SW8260BDibromochloromethane P9I1205 1.0 ND E809/12/09 09/12/0910.15

SW8260BDichlorodifluoromethane P9I1205 1.0 ND E809/12/09 09/12/0910.15

SW8260BMethyl-tert-butyl Ether (MTBE) P9I1205 1.0 ND E809/12/09 09/12/0910.18

SW8260Bn-Butylbenzene P9I1205 1.0 ND E809/12/09 09/12/0910.17

SW8260Bn-Propylbenzene P9I1205 1.0 ND E809/12/09 09/12/0910.18

SW8260Bp-Isopropyltoluene P9I1205 1.0 ND E809/12/09 09/12/0910.21

SW8260Bsec-Butylbenzene P9I1205 1.0 ND E809/12/09 09/12/0910.14

SW8260BStyrene P9I1205 1.0 ND E809/12/09 09/12/0910.15

SW8260Btert-Butylbenzene P9I1205 1.0 ND E809/12/09 09/12/0910.17

SW8260Btrans-1,3-Dichloropropene P9I1205 1.0 ND E809/12/09 09/12/0910.097

SW8260BVinyl Acetate P9I1205 1.0 ND E809/12/09 09/12/0910.21

Surrogate: Dibromofluoromethane (80.3-130%) 121 %

Surrogate: Toluene-d8 (88.4-111%) 100 %

Surrogate: 4-Bromofluorobenzene (86.5-114%) 99 %

Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSI0067-03 (TB001-09012009 - Water) Sampled: 09/01/09Reporting Units: ug/l

SW8260B1,1,2,2-Tetrachloroethane P9I1205 1.0 ND E809/12/09 09/12/0910.12

SW8260B1,1-Dichloroethene P9I1205 1.0 ND E809/12/09 09/12/0910.23


SW8260B2-Butanone (MEK) P9I1205 5.0 ND E809/12/09 09/12/0911.8

SW8260BAcetone P9I1205 20 ND E809/12/09 09/12/0913.8

SW8260BBenzene P9I1205 1.0 ND E809/12/09 09/12/0910.15

SW8260BCarbon tetrachloride P9I1205 1.0 ND E809/12/09 09/12/0910.19

SW8260BChloroform P9I1205 1.0 ND E809/12/09 09/12/0910.16

SW8260Bcis-1,2-Dichloroethene P9I1205 1.0 ND E809/12/09 09/12/0910.18

SW8260BEthylbenzene P9I1205 1.0 ND E809/12/09 09/12/0910.16

SW8260Bm,p-Xylenes P9I1205 2.0 ND E809/12/09 09/12/0910.35

SW8260BMethylene Chloride P9I1205 2.0 ND E809/12/09 09/12/0910.50

SW8260Bo-Xylene P9I1205 1.0 ND E809/12/09 09/12/0910.19

SW8260BTetrachloroethene P9I1205 1.0 ND E809/12/09 09/12/0910.23

SW8260BToluene P9I1205 1.0 ND E809/12/09 09/12/0910.35

SW8260Btrans-1,2-Dichloroethene P9I1205 1.0 ND E809/12/09 09/12/0910.22

SW8260BTrichloroethene P9I1205 1.0 ND E809/12/09 09/12/0910.19

SW8260BTrichlorofluoromethane P9I1205 1.0 ND E809/12/09 09/12/0910.17

SW8260BVinyl chloride P9I1205 1.0 ND E809/12/09 09/12/0910.24




SW8260B1,1-Dichloropropene P9I1205 1.0 ND E809/12/09 09/12/0910.19


SW8260B1,2,3-Trichloropropane P9I1205 2.0 ND E809/12/09 09/12/0910.31



SW8260B1,2-Dibromoethane (EDB) P9I1205 1.0 ND E809/12/09 09/12/0910.14









SW8260B2-Hexanone P9I1205 5.0 ND E809/12/09 09/12/0910.31


SW8260B4-Methyl-2-pentanone (MIBK) P9I1205 5.0 ND E809/12/09 09/12/0910.43

SW8260BBromobenzene P9I1205 1.0 ND E809/12/09 09/12/0910.15

Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSI0067-03 (TB001-09012009 - Water) - cont. Sampled: 09/01/09Reporting Units: ug/l

SW8260BBromochloromethane P9I1205 1.0 ND E809/12/09 09/12/0910.20

SW8260BBromodichloromethane P9I1205 1.0 ND E809/12/09 09/12/0910.15

SW8260BBromoform P9I1205 1.0 ND E809/12/09 09/12/0910.19

SW8260BBromomethane P9I1205 2.0 ND E809/12/09 09/12/0910.22

SW8260BChlorobenzene P9I1205 1.0 ND E809/12/09 09/12/0910.12

SW8260BChloroethane P9I1205 1.0 ND E809/12/09 09/12/0910.26

SW8260BChloromethane P9I1205 5.0 ND E809/12/09 09/12/0910.20

SW8260Bcis-1,3-Dichloropropene P9I1205 1.0 ND E809/12/09 09/12/0910.17

SW8260BDibromochloromethane P9I1205 1.0 ND E809/12/09 09/12/0910.15

SW8260BDichlorodifluoromethane P9I1205 1.0 ND E809/12/09 09/12/0910.15

SW8260BMethyl-tert-butyl Ether (MTBE) P9I1205 1.0 ND E809/12/09 09/12/0910.18

SW8260Bn-Butylbenzene P9I1205 1.0 ND E809/12/09 09/12/0910.17

SW8260Bn-Propylbenzene P9I1205 1.0 ND E809/12/09 09/12/0910.18

SW8260Bp-Isopropyltoluene P9I1205 1.0 ND E809/12/09 09/12/0910.21

SW8260Bsec-Butylbenzene P9I1205 1.0 ND E809/12/09 09/12/0910.14

SW8260BStyrene P9I1205 1.0 ND E809/12/09 09/12/0910.15

SW8260Btert-Butylbenzene P9I1205 1.0 ND E809/12/09 09/12/0910.17

SW8260Btrans-1,3-Dichloropropene P9I1205 1.0 ND E809/12/09 09/12/0910.097

SW8260BVinyl Acetate P9I1205 1.0 ND E809/12/09 09/12/0910.21

Surrogate: Dibromofluoromethane (80.3-130%) 114 %

Surrogate: Toluene-d8 (88.4-111%) 101 %

Surrogate: 4-Bromofluorobenzene (86.5-114%) 98 %

Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSI0067-02 (Bld1-47-09012009 - Soil) Sampled: 09/01/09Reporting Units: ug/kg

SW8260B1,1,1-Trichloroethane P9I0228 50 ND E809/02/09 09/06/090.9419

SW8260B1,1,2,2-Tetrachloroethane P9I0228 50 ND E809/02/09 09/06/090.9418

SW8260B1,1,2-Trichloroethane P9I0228 50 ND E809/02/09 09/06/090.9423

SW8260B1,1-Dichloroethane P9I0228 50 ND E809/02/09 09/06/090.9415

SW8260B1,1-Dichloroethene P9I0228 50 ND E809/02/09 09/06/090.9423

SW8260B1,1-Dichloropropene P9I0228 50 ND E809/02/09 09/06/090.9419

SW8260B1,2,3-Trichlorobenzene P9I0228 100 ND E809/02/09 09/06/090.9418

SW8260B1,2,3-Trichloropropane P9I0228 100 ND E809/02/09 09/06/090.9420

SW8260B1,2,4-Trimethylbenzene P9I0228 50 ND E809/02/09 09/06/090.9427

SW8260B1,2-Dibromoethane (EDB) P9I0228 50 ND E809/02/09 09/06/090.9416

SW8260B1,2-Dichlorobenzene P9I0228 50 ND E809/02/09 09/06/090.9421

SW8260B1,2-Dichloroethane P9I0228 50 ND E809/02/09 09/06/090.9429

SW8260B1,2-Dichloropropane P9I0228 50 ND E809/02/09 09/06/090.9419

SW8260B1,3,5-Trimethylbenzene P9I0228 50 ND E809/02/09 09/06/090.9416





SW8260B2-Butanone (MEK) P9I0228 500 ND E809/02/09 09/06/090.94200

SW8260B2-Chlorotoluene P9I0228 50 ND E809/02/09 09/06/090.9415

SW8260B2-Hexanone P9I0228 250 ND E809/02/09 09/06/090.94210

SW8260B4-Chlorotoluene P9I0228 50 ND E809/02/09 09/06/090.9418

SW8260B4-Methyl-2-pentanone (MIBK) P9I0228 250 ND E809/02/09 09/06/090.94170

SW8260BAcetone P9I0228 500 ND E8, V109/02/09 09/06/090.94330

SW8260BBenzene P9I0228 50 ND E809/02/09 09/06/090.9423

SW8260BBromobenzene P9I0228 50 ND E809/02/09 09/06/090.9418

SW8260BBromochloromethane P9I0228 50 ND E809/02/09 09/06/090.9424

SW8260BBromodichloromethane P9I0228 50 ND E809/02/09 09/06/090.9418

SW8260BBromoform P9I0228 50 ND E809/02/09 09/06/090.9420

SW8260BBromomethane P9I0228 250 ND E809/02/09 09/06/090.948.3

SW8260BCarbon tetrachloride P9I0228 50 ND E809/02/09 09/06/090.9420

SW8260BChlorobenzene P9I0228 50 ND E809/02/09 09/06/090.9411

SW8260BChloroethane P9I0228 50 ND E809/02/09 09/06/090.9431

SW8260BChloroform P9I0228 50 ND E809/02/09 09/06/090.9424

SW8260BChloromethane P9I0228 250 ND E809/02/09 09/06/090.9426

SW8260Bcis-1,2-Dichloroethene P9I0228 50 ND E809/02/09 09/06/090.9421

SW8260Bcis-1,3-Dichloropropene P9I0228 50 ND E809/02/09 09/06/090.9415

SW8260BDibromochloromethane P9I0228 50 ND E809/02/09 09/06/090.9411

SW8260BDichlorodifluoromethane P9I0228 50 ND E809/02/09 09/06/090.9419

SW8260BEthylbenzene P9I0228 50 ND E809/02/09 09/06/090.9413

Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSI0067-02 (Bld1-47-09012009 - Soil) - cont. Sampled: 09/01/09Reporting Units: ug/kg

SW8260Bm,p-Xylenes P9I0228 100 ND E809/02/09 09/06/090.9434

SW8260BMethyl-tert-butyl Ether (MTBE) P9I0228 50 ND E809/02/09 09/06/090.9417

SW8260BMethylene Chloride P9I0228 100 ND E809/02/09 09/06/090.9432

SW8260Bn-Butylbenzene P9I0228 50 ND E809/02/09 09/06/090.9418

SW8260Bn-Propylbenzene P9I0228 50 ND E809/02/09 09/06/090.9417

SW8260Bo-Xylene P9I0228 50 ND E809/02/09 09/06/090.9416

SW8260Bp-Isopropyltoluene P9I0228 50 ND E809/02/09 09/06/090.9420

SW8260Bsec-Butylbenzene P9I0228 50 ND E809/02/09 09/06/090.9418

SW8260BStyrene P9I0228 50 ND E809/02/09 09/06/090.9412

SW8260Btert-Butylbenzene P9I0228 50 ND E809/02/09 09/06/090.9420

SW8260BTetrachloroethene P9I0228 50 ND E809/02/09 09/06/090.949.4

SW8260BToluene P9I0228 50 ND E809/02/09 09/06/090.9415

SW8260Btrans-1,2-Dichloroethene P9I0228 50 ND E809/02/09 09/06/090.9418

SW8260Btrans-1,3-Dichloropropene P9I0228 50 ND E809/02/09 09/06/090.9415

SW8260BTrichloroethene P9I0228 50 ND E809/02/09 09/06/090.9421

SW8260BTrichlorofluoromethane P9I0228 50 ND E809/02/09 09/06/090.9432

SW8260BVinyl Acetate P9I0228 50 ND E8, L309/02/09 09/06/090.9426

SW8260BVinyl chloride P9I0228 50 ND E809/02/09 09/06/090.9425

Surrogate: Dibromofluoromethane (60-130%) 104 %

Surrogate: Toluene-d8 (65-125%) 108 %

Surrogate: 4-Bromofluorobenzene (65-125%) 106 %

Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: PSI0067-04 (Bld1 Tank-09012009 - Water) Sampled: 09/01/09Reporting Units: mg/l

SM3500CR-DChromium VI P9I0232 0.010 ND 09/01/09 09/02/0910.0050

Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

SHORT HOLD TIME DETAIL REPORT

Date/Time

Analyzed

Date/Time

Extracted

Date/Time

Sampled

Date/Time

Received

Hold Time

(in days)

Sample ID: Bld1-47-09012009 (PSI0067-02) - Soil

2 09/01/2009 14:55 09/01/2009 16:06 09/02/2009 15:00 09/06/2009 19:20SW8260B

Sample ID: Bld1 Tank-09012009 (PSI0067-04) - Water

1 09/01/2009 15:00 09/01/2009 16:06 09/01/2009 17:00 09/02/2009 14:20SM3500CR-D

Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



1,1,2,2-Tetrachloroethane ug/l1.0ND 0.12

1,1-Dichloroethene ug/l1.0ND 0.23

1,2-Dichloropropane ug/l1.0ND 0.15

2-Butanone (MEK) ug/l5.0ND 1.8

Acetone ug/l20ND 3.8

Benzene ug/l1.0ND 0.15

Carbon tetrachloride ug/l1.0ND 0.19

Chloroform ug/l1.0ND 0.16

cis-1,2-Dichloroethene ug/l1.0ND 0.18

Ethylbenzene ug/l1.0ND 0.16

m,p-Xylenes ug/l2.0ND 0.35

Methylene Chloride ug/l2.0ND 0.50

o-Xylene ug/l1.0ND 0.19

Tetrachloroethene ug/l1.0ND 0.23

Toluene ug/l1.0ND 0.35

trans-1,2-Dichloroethene ug/l1.0ND 0.22

Trichloroethene ug/l1.0ND 0.19

Trichlorofluoromethane ug/l1.0ND 0.17

Vinyl chloride ug/l1.0ND 0.24

1,1,1-Trichloroethane ug/l1.0ND 0.22

1,1,2-Trichloroethane ug/l1.0ND 0.19

1,1-Dichloroethane ug/l1.0ND 0.17

1,1-Dichloropropene ug/l1.0ND 0.19

1,2,3-Trichlorobenzene ug/l2.00.870 E40.27

1,2,3-Trichloropropane ug/l2.0ND 0.31

1,2,4-Trichlorobenzene ug/l1.00.710 E40.18

1,2,4-Trimethylbenzene ug/l1.00.130 E40.13

1,2-Dibromoethane (EDB) ug/l1.0ND 0.14

1,2-Dichlorobenzene ug/l1.0ND 0.12

1,2-Dichloroethane ug/l1.0ND 0.20

1,3,5-Trimethylbenzene ug/l1.0ND 0.16





Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



2-Chlorotoluene ug/l1.0ND 0.17

2-Hexanone ug/l5.0ND 0.31

4-Chlorotoluene ug/l1.0ND 0.15

4-Methyl-2-pentanone (MIBK) ug/l5.0ND 0.43

Bromobenzene ug/l1.0ND 0.15

Bromochloromethane ug/l1.0ND 0.20

Bromodichloromethane ug/l1.0ND 0.15

Bromoform ug/l1.0ND 0.19

Bromomethane ug/l2.0ND 0.22

Chlorobenzene ug/l1.0ND 0.12

Chloroethane ug/l1.0ND 0.26

Chloromethane ug/l5.0ND 0.20

cis-1,3-Dichloropropene ug/l1.0ND 0.17

Dibromochloromethane ug/l1.0ND 0.15

Dichlorodifluoromethane ug/l1.0ND 0.15

Methyl-tert-butyl Ether (MTBE) ug/l1.0ND 0.18

n-Butylbenzene ug/l1.00.490 E40.17

n-Propylbenzene ug/l1.0ND 0.18

p-Isopropyltoluene ug/l1.0ND 0.21

sec-Butylbenzene ug/l1.0ND 0.14

Styrene ug/l1.0ND 0.15

tert-Butylbenzene ug/l1.0ND 0.17

trans-1,3-Dichloropropene ug/l1.0ND 0.097

Vinyl Acetate ug/l1.0ND 0.21




Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



1,1,2,2-Tetrachloroethane ug/l1.026.5 70.5-12525.00.12 106

1,1-Dichloroethene ug/l1.022.7 81.7-12225.00.23 91

1,2-Dichloropropane ug/l1.025.0 85-11525.00.15 100

2-Butanone (MEK) ug/l5.021.9 45.6-14125.01.8 88

Acetone ug/l2029.0 22.4-15325.03.8 116

Benzene ug/l1.023.3 80.7-12025.00.15 93

Carbon tetrachloride ug/l1.024.8 82.5-12325.00.19 99

Chloroform ug/l1.023.8 80.7-11925.00.16 95

cis-1,2-Dichloroethene ug/l1.021.7 83.3-11725.00.18 87

Ethylbenzene ug/l1.024.1 85-11525.00.16 96

m,p-Xylenes ug/l2.023.0 85-11525.00.35 92

Methylene Chloride ug/l2.022.8 79.7-11725.00.50 91

o-Xylene ug/l1.023.5 85-11525.00.19 94

Tetrachloroethene ug/l1.023.8 85-11525.00.23 95

Toluene ug/l1.023.1 85-11525.00.35 93

trans-1,2-Dichloroethene ug/l1.025.1 82.3-12025.00.22 101

Trichloroethene ug/l1.023.9 85-11525.00.19 96

Trichlorofluoromethane ug/l1.021.8 84.5-12325.00.17 87

Vinyl chloride ug/l1.024.2 80.9-12725.00.24 97

1,1,1-Trichloroethane ug/l1.024.4 83.2-12025.00.22 98

1,1,2-Trichloroethane ug/l1.023.2 85-11525.00.19 93

1,1-Dichloroethane ug/l1.024.3 78.8-12225.00.17 97

1,1-Dichloropropene ug/l1.023.5 82.3-11925.00.19 94

1,2,3-Trichlorobenzene ug/l2.021.5 60.4-17125.00.27 86

1,2,3-Trichloropropane ug/l2.025.3 76.3-12525.00.31 101

1,2,4-Trichlorobenzene ug/l1.021.6 71-13625.00.18 86

1,2,4-Trimethylbenzene ug/l1.026.1 78.1-12025.00.13 104

1,2-Dibromoethane (EDB) ug/l1.023.6 85-11525.00.14 94

1,2-Dichlorobenzene ug/l1.025.1 85-11525.00.12 100

1,2-Dichloroethane ug/l1.022.9 79.1-12425.00.20 91

1,3,5-Trimethylbenzene ug/l1.026.9 80.1-11925.00.16 108

1,3-Dichlorobenzene ug/l1.025.6 83.9-11425.00.18 102

1,3-Dichloropropane ug/l1.023.8 85-11525.00.18 95

1,4-Dichlorobenzene ug/l1.024.4 85-11525.00.16 97

2,2-Dichloropropane ug/l2.023.7 70.8-12825.00.18 95

Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



2-Chlorotoluene ug/l1.025.7 78.6-12025.00.17 103

2-Hexanone ug/l5.022.8 58.5-13525.00.31 91

4-Chlorotoluene ug/l1.026.1 80.3-11925.00.15 105

4-Methyl-2-pentanone (MIBK) ug/l5.022.1 72-12925.00.43 88

Bromobenzene ug/l1.025.3 83.3-11625.00.15 101

Bromochloromethane ug/l1.023.3 83-12225.00.20 93

Bromodichloromethane ug/l1.024.2 84-11725.00.15 97

Bromoform ug/l1.021.6 71.9-13125.00.19 86

Bromomethane ug/l2.026.0 56.3-14525.00.22 104

Chlorobenzene ug/l1.023.6 82.5-12325.00.12 94

Chloroethane ug/l1.024.1 69.5-13225.00.26 96

Chloromethane ug/l5.024.6 70.9-12325.00.20 98

cis-1,3-Dichloropropene ug/l1.025.2 85-11525.00.17 101

Dibromochloromethane ug/l1.023.4 83.2-12325.00.15 93

Dichlorodifluoromethane ug/l1.028.2 72.8-13025.00.15 113

Methyl-tert-butyl Ether (MTBE) ug/l1.022.7 81.8-11825.00.18 91

n-Butylbenzene ug/l1.024.3 74-12125.00.17 97

n-Propylbenzene ug/l1.027.3 79.4-12025.00.18 109

p-Isopropyltoluene ug/l1.025.2 75.5-11625.00.21 101

sec-Butylbenzene ug/l1.025.8 76.7-12125.00.14 103

Styrene ug/l1.023.7 85-11525.00.15 95

tert-Butylbenzene ug/l1.025.9 78.9-11725.00.17 104

trans-1,3-Dichloropropene ug/l1.025.3 82.2-12125.00.097 101

Vinyl Acetate ug/l1.030.4 70.5-13425.00.21 122




Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



1,1,2,2-Tetrachloroethane 25ug/l1.025.5 70.5-12525.00.12 102 4

1,1-Dichloroethene 25ug/l1.023.5 81.7-12225.00.23 94 4

1,2-Dichloropropane 25ug/l1.025.8 85-11525.00.15 103 3

2-Butanone (MEK) 25ug/l5.023.8 45.6-14125.01.8 95 8

Acetone 25ug/l2027.3 22.4-15325.03.8 109 6

Benzene 25ug/l1.023.5 80.7-12025.00.15 94 1

Carbon tetrachloride 25ug/l1.025.8 82.5-12325.00.19 103 4

Chloroform 25ug/l1.024.4 80.7-11925.00.16 98 3

cis-1,2-Dichloroethene 25ug/l1.021.8 83.3-11725.00.18 87 1

Ethylbenzene 25ug/l1.024.4 85-11525.00.16 98 2

m,p-Xylenes 25ug/l2.023.5 85-11525.00.35 94 2

Methylene Chloride 25ug/l2.023.6 79.7-11725.00.50 95 4

o-Xylene 25ug/l1.024.4 85-11525.00.19 98 4

Tetrachloroethene 25ug/l1.025.1 85-11525.00.23 101 5

Toluene 25ug/l1.023.9 85-11525.00.35 95 3

trans-1,2-Dichloroethene 25ug/l1.025.7 82.3-12025.00.22 103 2

Trichloroethene 25ug/l1.025.0 85-11525.00.19 100 4

Trichlorofluoromethane 25ug/l1.023.1 84.5-12325.00.17 92 6

Vinyl chloride 25ug/l1.025.6 80.9-12725.00.24 102 5

1,1,1-Trichloroethane 25ug/l1.025.7 83.2-12025.00.22 103 5

1,1,2-Trichloroethane 25ug/l1.025.0 85-11525.00.19 100 7

1,1-Dichloroethane 25ug/l1.024.6 78.8-12225.00.17 98 1

1,1-Dichloropropene 25ug/l1.024.4 82.3-11925.00.19 98 4

1,2,3-Trichlorobenzene 25ug/l2.023.5 60.4-17125.00.27 94 9

1,2,3-Trichloropropane 25ug/l2.024.2 76.3-12525.00.31 97 5

1,2,4-Trichlorobenzene 25ug/l1.023.7 71-13625.00.18 95 9

1,2,4-Trimethylbenzene 25ug/l1.025.3 78.1-12025.00.13 101 3

1,2-Dibromoethane (EDB) 25ug/l1.024.2 85-11525.00.14 97 3

1,2-Dichlorobenzene 25ug/l1.024.6 85-11525.00.12 98 2

1,2-Dichloroethane 25ug/l1.024.4 79.1-12425.00.20 98 7

1,3,5-Trimethylbenzene 25ug/l1.026.1 80.1-11925.00.16 104 3

1,3-Dichlorobenzene 25ug/l1.024.3 83.9-11425.00.18 97 5

1,3-Dichloropropane 25ug/l1.024.1 85-11525.00.18 96 1

1,4-Dichlorobenzene 25ug/l1.024.2 85-11525.00.16 97 1

2,2-Dichloropropane 25ug/l2.024.3 70.8-12825.00.18 97 3

Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



2-Chlorotoluene 25ug/l1.024.4 78.6-12025.00.17 97 6

2-Hexanone 25ug/l5.022.8 58.5-13525.00.31 91 0

4-Chlorotoluene 25ug/l1.025.2 80.3-11925.00.15 101 4

4-Methyl-2-pentanone (MIBK) 25ug/l5.022.6 72-12925.00.43 91 2

Bromobenzene 25ug/l1.024.4 83.3-11625.00.15 97 4

Bromochloromethane 25ug/l1.023.5 83-12225.00.20 94 1

Bromodichloromethane 25ug/l1.024.7 84-11725.00.15 99 2

Bromoform 25ug/l1.021.5 71.9-13125.00.19 86 0

Bromomethane 25ug/l2.026.4 56.3-14525.00.22 106 2

Chlorobenzene 25ug/l1.024.4 82.5-12325.00.12 98 4

Chloroethane 25ug/l1.025.0 69.5-13225.00.26 100 4

Chloromethane 25ug/l5.025.4 70.9-12325.00.20 102 3

cis-1,3-Dichloropropene 25ug/l1.025.7 85-11525.00.17 103 2

Dibromochloromethane 25ug/l1.024.0 83.2-12325.00.15 96 3

Dichlorodifluoromethane 25ug/l1.030.1 72.8-13025.00.15 120 7

Methyl-tert-butyl Ether (MTBE) 25ug/l1.023.9 81.8-11825.00.18 96 5

n-Butylbenzene 25ug/l1.024.4 74-12125.00.17 98 0

n-Propylbenzene 25ug/l1.026.1 79.4-12025.00.18 104 4

p-Isopropyltoluene 25ug/l1.025.1 75.5-11625.00.21 100 0

sec-Butylbenzene 25ug/l1.024.9 76.7-12125.00.14 99 4

Styrene 25ug/l1.024.5 85-11525.00.15 98 3

tert-Butylbenzene 25ug/l1.024.5 78.9-11725.00.17 98 5

trans-1,3-Dichloropropene 25ug/l1.025.2 82.2-12125.00.097 101 0

Vinyl Acetate 25ug/l1.030.6 70.5-13425.00.21 123 1




Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


Matrix Spike Analyzed: 09/12/2009 (P9I1205-MS1) Source: PSI0162-02

1,1,2,2-Tetrachloroethane ug/l1.023.0 70.4-12425.0 ND0.12 92

1,1-Dichloroethene ug/l1.022.2 82.1-12625.0 ND0.23 89

1,2-Dichloropropane ug/l1.025.2 81.1-11625.0 ND0.15 101

2-Butanone (MEK) ug/l5.019.3 41.6-13025.0 ND1.8 77

Acetone ug/l2016.0 19.7-13125.0 E4ND3.8 64

Benzene ug/l1.023.1 78.4-12725.0 ND0.15 92

Carbon tetrachloride ug/l1.023.5 80.7-12825.0 ND0.19 94

Chloroform ug/l1.027.3 77.6-12225.0 1.680.16 103

cis-1,2-Dichloroethene ug/l1.023.2 80.1-11925.0 ND0.18 93

Ethylbenzene ug/l1.022.7 83.4-11625.0 ND0.16 91

m,p-Xylenes ug/l2.022.3 70.8-13225.0 ND0.35 89

Methylene Chloride ug/l2.024.8 74.6-11925.0 ND0.50 99

o-Xylene ug/l1.023.2 77.5-12225.0 ND0.19 93

Tetrachloroethene ug/l1.023.3 77.8-11925.0 ND0.23 93

Toluene ug/l1.023.4 83-11825.0 ND0.35 93

trans-1,2-Dichloroethene ug/l1.025.4 81.3-12325.0 ND0.22 102

Trichloroethene ug/l1.023.6 77.3-12025.0 ND0.19 94

Trichlorofluoromethane ug/l1.021.7 82.4-13225.0 ND0.17 87

Vinyl chloride ug/l1.024.2 69.2-14325.0 ND0.24 97

1,1,1-Trichloroethane ug/l1.024.1 81.4-12525.0 ND0.22 96

1,1,2-Trichloroethane ug/l1.024.2 77.5-11825.0 ND0.19 97

1,1-Dichloroethane ug/l1.025.2 75.7-12625.0 ND0.17 101

1,1-Dichloropropene ug/l1.021.8 81.4-12325.0 ND0.19 87

1,2,3-Trichlorobenzene ug/l2.020.3 32.3-11725.0 ND0.27 81

1,2,3-Trichloropropane ug/l2.022.0 69.8-12425.0 ND0.31 88

1,2,4-Trichlorobenzene ug/l1.020.9 52.9-14525.0 ND0.18 83

1,2,4-Trimethylbenzene ug/l1.024.0 75.2-12025.0 ND0.13 96

1,2-Dibromoethane (EDB) ug/l1.023.1 76.5-12025.0 ND0.14 92

1,2-Dichlorobenzene ug/l1.023.8 80.6-11425.0 ND0.12 95

1,2-Dichloroethane ug/l1.026.0 69.4-12925.0 ND0.20 104

1,3,5-Trimethylbenzene ug/l1.024.0 75.1-12325.0 ND0.16 96





Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



2-Chlorotoluene ug/l1.023.2 75.2-12225.0 ND0.17 93

2-Hexanone ug/l5.017.7 57.9-11825.0 ND0.31 71

4-Chlorotoluene ug/l1.023.9 76.8-12025.0 ND0.15 96

4-Methyl-2-pentanone (MIBK) ug/l5.019.6 65.6-12725.0 ND0.43 78

Bromobenzene ug/l1.024.5 79.4-11625.0 ND0.15 98

Bromochloromethane ug/l1.026.0 75.5-12525.0 ND0.20 104

Bromodichloromethane ug/l1.024.9 78.1-11825.0 ND0.15 100

Bromoform ug/l1.019.3 63.7-12925.0 ND0.19 77

Bromomethane ug/l2.026.8 44.2-15525.0 ND0.22 107

Chlorobenzene ug/l1.023.5 84.6-11025.0 ND0.12 94

Chloroethane ug/l1.024.9 68.9-13625.0 ND0.26 100

Chloromethane ug/l5.025.6 64.1-13525.0 ND0.20 102

cis-1,3-Dichloropropene ug/l1.026.1 78.6-11825.0 ND0.17 104

Dibromochloromethane ug/l1.024.3 75.2-12325.0 ND0.15 97

Dichlorodifluoromethane ug/l1.027.1 71-13825.0 ND0.15 109

Methyl-tert-butyl Ether (MTBE) ug/l1.024.1 68.8-12625.0 ND0.18 96

n-Butylbenzene ug/l1.021.0 70.4-11925.0 ND0.17 84

n-Propylbenzene ug/l1.023.6 76-12425.0 ND0.18 94

p-Isopropyltoluene ug/l1.022.6 67.9-12225.0 ND0.21 90

sec-Butylbenzene ug/l1.022.2 73.7-12525.0 ND0.14 89

Styrene ug/l1.022.0 55-13625.0 ND0.15 88

tert-Butylbenzene ug/l1.022.4 76.8-11925.0 ND0.17 90

trans-1,3-Dichloropropene ug/l1.025.1 72.8-12325.0 ND0.097 100

Vinyl Acetate ug/l1.029.9 50-13925.0 ND0.21 119




Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL


Matrix Spike Dup Analyzed: 09/12/2009 (P9I1205-MSD1) Source: PSI0162-02

1,1,2,2-Tetrachloroethane 25ug/l1.023.4 70.4-12425.0 ND0.12 94 2

1,1-Dichloroethene 25ug/l1.022.0 82.1-12625.0 ND0.23 88 1

1,2-Dichloropropane 25ug/l1.025.8 81.1-11625.0 ND0.15 103 2

2-Butanone (MEK) 25ug/l5.022.0 41.6-13025.0 ND1.8 88 13

Acetone 25ug/l2017.9 19.7-13125.0 E4ND3.8 72 11

Benzene 25ug/l1.023.0 78.4-12725.0 ND0.15 92 0

Carbon tetrachloride 25ug/l1.023.2 80.7-12825.0 ND0.19 93 1

Chloroform 25ug/l1.027.6 77.6-12225.0 1.680.16 103 1

cis-1,2-Dichloroethene 25ug/l1.023.8 80.1-11925.0 ND0.18 95 3

Ethylbenzene 25ug/l1.022.5 83.4-11625.0 ND0.16 90 1

m,p-Xylenes 25ug/l2.022.1 70.8-13225.0 ND0.35 88 1

Methylene Chloride 25ug/l2.025.7 74.6-11925.0 ND0.50 103 4

o-Xylene 25ug/l1.023.0 77.5-12225.0 ND0.19 92 1

Tetrachloroethene 25ug/l1.022.2 77.8-11925.0 ND0.23 89 5

Toluene 25ug/l1.023.3 83-11825.0 ND0.35 93 0

trans-1,2-Dichloroethene 25ug/l1.025.9 81.3-12325.0 ND0.22 104 2

Trichloroethene 25ug/l1.023.0 77.3-12025.0 ND0.19 92 3

Trichlorofluoromethane 25ug/l1.021.7 82.4-13225.0 ND0.17 87 0

Vinyl chloride 25ug/l1.024.3 69.2-14325.0 ND0.24 97 1

1,1,1-Trichloroethane 25ug/l1.024.5 81.4-12525.0 ND0.22 98 2

1,1,2-Trichloroethane 25ug/l1.024.5 77.5-11825.0 ND0.19 98 1

1,1-Dichloroethane 25ug/l1.025.7 75.7-12625.0 ND0.17 103 2

1,1-Dichloropropene 25ug/l1.021.3 81.4-12325.0 ND0.19 85 3

1,2,3-Trichlorobenzene 25ug/l2.023.2 32.3-11725.0 ND0.27 93 13

1,2,3-Trichloropropane 25ug/l2.021.8 69.8-12425.0 ND0.31 87 1

1,2,4-Trichlorobenzene 25ug/l1.022.5 52.9-14525.0 ND0.18 90 8

1,2,4-Trimethylbenzene 25ug/l1.023.5 75.2-12025.0 ND0.13 94 2

1,2-Dibromoethane (EDB) 25ug/l1.023.6 76.5-12025.0 ND0.14 94 2

1,2-Dichlorobenzene 25ug/l1.024.3 80.6-11425.0 ND0.12 97 2

1,2-Dichloroethane 25ug/l1.026.5 69.4-12925.0 ND0.20 106 2

1,3,5-Trimethylbenzene 25ug/l1.023.6 75.1-12325.0 ND0.16 95 1





Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



2-Chlorotoluene 25ug/l1.022.5 75.2-12225.0 ND0.17 90 3

2-Hexanone 25ug/l5.016.9 57.9-11825.0 ND0.31 68 5

4-Chlorotoluene 25ug/l1.023.2 76.8-12025.0 ND0.15 93 3

4-Methyl-2-pentanone (MIBK) 25ug/l5.019.8 65.6-12725.0 ND0.43 79 1

Bromobenzene 25ug/l1.024.3 79.4-11625.0 ND0.15 97 1

Bromochloromethane 25ug/l1.026.2 75.5-12525.0 ND0.20 105 1

Bromodichloromethane 25ug/l1.025.8 78.1-11825.0 ND0.15 103 4

Bromoform 25ug/l1.019.9 63.7-12925.0 ND0.19 80 3

Bromomethane 25ug/l2.026.6 44.2-15525.0 ND0.22 107 0

Chlorobenzene 25ug/l1.023.9 84.6-11025.0 ND0.12 96 1

Chloroethane 25ug/l1.025.2 68.9-13625.0 ND0.26 101 1

Chloromethane 25ug/l5.025.9 64.1-13525.0 ND0.20 104 1

cis-1,3-Dichloropropene 25ug/l1.025.8 78.6-11825.0 ND0.17 103 1

Dibromochloromethane 25ug/l1.024.5 75.2-12325.0 ND0.15 98 1

Dichlorodifluoromethane 25ug/l1.026.1 71-13825.0 ND0.15 104 4

Methyl-tert-butyl Ether (MTBE) 25ug/l1.025.6 68.8-12625.0 ND0.18 102 6

n-Butylbenzene 25ug/l1.021.2 70.4-11925.0 ND0.17 85 1

n-Propylbenzene 25ug/l1.022.9 76-12425.0 ND0.18 91 3

p-Isopropyltoluene 25ug/l1.022.4 67.9-12225.0 ND0.21 89 1

sec-Butylbenzene 25ug/l1.021.9 73.7-12525.0 ND0.14 88 1

Styrene 25ug/l1.021.1 55-13625.0 ND0.15 84 4

tert-Butylbenzene 25ug/l1.022.3 76.8-11925.0 ND0.17 89 1

trans-1,3-Dichloropropene 25ug/l1.025.8 72.8-12325.0 ND0.097 103 3

Vinyl Acetate 25ug/l1.029.8 50-13925.0 ND0.21 119 0




Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



1,1,1-Trichloroethane ug/kg50ND 19

1,1,2,2-Tetrachloroethane ug/kg50ND 18

1,1,2-Trichloroethane ug/kg50ND 23

1,1-Dichloroethane ug/kg50ND 15

1,1-Dichloroethene ug/kg50ND 23

1,1-Dichloropropene ug/kg50ND 19

1,2,3-Trichlorobenzene ug/kg100ND 18

1,2,3-Trichloropropane ug/kg100ND 20

1,2,4-Trimethylbenzene ug/kg50ND 27

1,2-Dibromoethane (EDB) ug/kg50ND 16

1,2-Dichlorobenzene ug/kg50ND 21

1,2-Dichloroethane ug/kg50ND 29

1,2-Dichloropropane ug/kg50ND 19

1,3,5-Trimethylbenzene ug/kg50ND 16





2-Butanone (MEK) ug/kg500ND 200

2-Chlorotoluene ug/kg50ND 15

2-Hexanone ug/kg250ND 210

4-Chlorotoluene ug/kg50ND 18

4-Methyl-2-pentanone (MIBK) ug/kg250ND 170

Acetone ug/kg500ND 330

Benzene ug/kg50ND 23

Bromobenzene ug/kg50ND 18

Bromochloromethane ug/kg50ND 24

Bromodichloromethane ug/kg50ND 18

Bromoform ug/kg50ND 20

Bromomethane ug/kg25053.5 E48.3

Carbon tetrachloride ug/kg50ND 20

Chlorobenzene ug/kg50ND 11

Chloroethane ug/kg50ND 31

Chloroform ug/kg50ND 24

Chloromethane ug/kg250ND 26

Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



cis-1,2-Dichloroethene ug/kg50ND 21

cis-1,3-Dichloropropene ug/kg50ND 15

Dibromochloromethane ug/kg50ND 11

Dichlorodifluoromethane ug/kg50ND 19

Ethylbenzene ug/kg50ND 13

m,p-Xylenes ug/kg100ND 34

Methyl-tert-butyl Ether (MTBE) ug/kg50ND 17

Methylene Chloride ug/kg100ND 32

n-Butylbenzene ug/kg50ND 18

n-Propylbenzene ug/kg50ND 17

o-Xylene ug/kg50ND 16

p-Isopropyltoluene ug/kg50ND 20

sec-Butylbenzene ug/kg50ND 18

Styrene ug/kg5017.0 E412

tert-Butylbenzene ug/kg50ND 20

Tetrachloroethene ug/kg50ND 9.4

Toluene ug/kg50ND 15

trans-1,2-Dichloroethene ug/kg50ND 18

trans-1,3-Dichloropropene ug/kg50ND 15

Trichloroethene ug/kg50ND 21

Trichlorofluoromethane ug/kg50ND 32

Vinyl Acetate ug/kg50ND 26

Vinyl chloride ug/kg50ND 25





1,1,1-Trichloroethane ug/kg501320 75-120125019 105

1,1,2,2-Tetrachloroethane ug/kg501340 60-125125018 108

1,1,2-Trichloroethane ug/kg501180 65-125125023 95

1,1-Dichloroethane ug/kg501240 70-125125015 99

1,1-Dichloroethene ug/kg501300 50-135125023 104

1,1-Dichloropropene ug/kg501270 75-120125019 102

1,2,3-Trichlorobenzene ug/kg1001200 55-140125018 96

Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



1,2,3-Trichloropropane ug/kg1001340 60-130125020 107

1,2,4-Trimethylbenzene ug/kg501250 75-120125027 101

1,2-Dibromoethane (EDB) ug/kg501320 70-120125016 106

1,2-Dichlorobenzene ug/kg501270 80-120125021 102

1,2-Dichloroethane ug/kg501280 70-130125029 102

1,2-Dichloropropane ug/kg501250 80-120125019 100

1,3,5-Trimethylbenzene ug/kg501280 80-130125016 103





2-Butanone (MEK) ug/kg5001360 40-1501250200 109

2-Chlorotoluene ug/kg501270 80-120125015 102

2-Hexanone ug/kg2501180 20-1501250210 94

4-Chlorotoluene ug/kg501250 80-120125018 100

4-Methyl-2-pentanone (MIBK) ug/kg2501270 50-1301250170 102

Acetone ug/kg5001410 10-1501250 V1330 113

Benzene ug/kg501220 75-120125023 97

Bromobenzene ug/kg501220 80-120125018 98

Bromochloromethane ug/kg501180 75-125125024 95

Bromodichloromethane ug/kg501190 75-120125018 96

Bromoform ug/kg501300 60-120125020 105

Bromomethane ug/kg2501320 20-14012508.3 106

Carbon tetrachloride ug/kg501320 70-130125020 106

Chlorobenzene ug/kg501250 80-120125011 100

Chloroethane ug/kg501370 10-130125031 110

Chloroform ug/kg501220 75-120125024 98

Chloromethane ug/kg2501180 25-140125026 94

cis-1,2-Dichloroethene ug/kg501190 70-125125021 95

cis-1,3-Dichloropropene ug/kg501320 75-125125015 106

Dibromochloromethane ug/kg501380 75-120125011 110

Dichlorodifluoromethane ug/kg50960 10-150125019 77

Ethylbenzene ug/kg501250 80-120125013 100

m,p-Xylenes ug/kg1001210 60-140125034 97

Methyl-tert-butyl Ether (MTBE) ug/kg501170 65-130125017 94

Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



Methylene Chloride ug/kg1001210 65-125125032 97

n-Butylbenzene ug/kg501240 65-130125018 100

n-Propylbenzene ug/kg501320 75-130125017 106

o-Xylene ug/kg501170 80-120125016 94

p-Isopropyltoluene ug/kg501220 75-130125020 98

sec-Butylbenzene ug/kg501280 75-125125018 103

Styrene ug/kg501140 80-120125012 92

tert-Butylbenzene ug/kg501250 80-120125020 101

Tetrachloroethene ug/kg501280 70-13012509.4 103

Toluene ug/kg501230 75-120125015 99

trans-1,2-Dichloroethene ug/kg501260 70-130125018 101

trans-1,3-Dichloropropene ug/kg501370 65-130125015 110

Trichloroethene ug/kg501220 80-120125021 98

Trichlorofluoromethane ug/kg501360 50-150125032 109

Vinyl Acetate ug/kg501920 35-1501250 L326 154

Vinyl chloride ug/kg501120 10-150125025 90





1,1,1-Trichloroethane 15ug/kg501360 75-120125019 109 3

1,1,2,2-Tetrachloroethane 30ug/kg501370 60-125125018 109 2

1,1,2-Trichloroethane 30ug/kg501270 65-125125023 102 7

1,1-Dichloroethane 20ug/kg501310 70-125125015 105 6

1,1-Dichloroethene 20ug/kg501300 50-135125023 104 1

1,1-Dichloropropene 15ug/kg501320 75-120125019 106 4

1,2,3-Trichlorobenzene 25ug/kg1001320 55-140125018 106 9

1,2,3-Trichloropropane 30ug/kg1001360 60-130125020 109 1

1,2,4-Trimethylbenzene 15ug/kg501350 75-120125027 108 7

1,2-Dibromoethane (EDB) 20ug/kg501350 70-120125016 108 3

1,2-Dichlorobenzene 20ug/kg501360 80-120125021 109 7

1,2-Dichloroethane 20ug/kg501340 70-130125029 108 5

1,2-Dichloropropane 20ug/kg501290 80-120125019 104 3

1,3,5-Trimethylbenzene 15ug/kg501380 80-130125016 110 7

Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL







2-Butanone (MEK) 35ug/kg5001370 40-1501250200 110 0

2-Chlorotoluene 15ug/kg501330 80-120125015 106 4

2-Hexanone 35ug/kg2501230 20-1501250210 99 5

4-Chlorotoluene 15ug/kg501360 80-120125018 109 9

4-Methyl-2-pentanone (MIBK) 35ug/kg2501310 50-1301250170 105 3

Acetone 35ug/kg5001360 10-1501250 V1330 109 4

Benzene 15ug/kg501280 75-120125023 103 5

Bromobenzene 20ug/kg501340 80-120125018 107 9

Bromochloromethane 20ug/kg501310 75-125125024 105 10

Bromodichloromethane 15ug/kg501300 75-120125018 104 8

Bromoform 25ug/kg501400 60-120125020 112 7

Bromomethane 35ug/kg2501300 20-14012508.3 104 2

Carbon tetrachloride 20ug/kg501370 70-130125020 110 3

Chlorobenzene 15ug/kg501340 80-120125011 108 7

Chloroethane 30ug/kg501390 10-130125031 111 2

Chloroform 20ug/kg501290 75-120125024 103 5

Chloromethane 35ug/kg2501200 25-140125026 96 2

cis-1,2-Dichloroethene 15ug/kg501290 70-125125021 103 8

cis-1,3-Dichloropropene 15ug/kg501400 75-125125015 113 6

Dibromochloromethane 20ug/kg501480 75-120125011 118 7

Dichlorodifluoromethane 35ug/kg50991 10-150125019 79 3

Ethylbenzene 15ug/kg501330 80-120125013 107 7

m,p-Xylenes 15ug/kg1001310 60-140125034 105 8

Methyl-tert-butyl Ether (MTBE) 20ug/kg501240 65-130125017 99 5

Methylene Chloride 20ug/kg1001250 65-125125032 100 4

n-Butylbenzene 20ug/kg501360 65-130125018 109 9

n-Propylbenzene 15ug/kg501390 75-130125017 111 5

o-Xylene 15ug/kg501280 80-120125016 103 10

p-Isopropyltoluene 15ug/kg501310 75-130125020 105 7

sec-Butylbenzene 15ug/kg501350 75-125125018 109 5

Styrene 15ug/kg501210 80-120125012 97 6

Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



tert-Butylbenzene 15ug/kg501310 80-120125020 105 4

Tetrachloroethene 15ug/kg501390 70-13012509.4 111 8

Toluene 15ug/kg501300 75-120125015 104 5

trans-1,2-Dichloroethene 20ug/kg501270 70-130125018 102 1

trans-1,3-Dichloropropene 20ug/kg501470 65-130125015 118 7

Trichloroethene 15ug/kg501290 80-120125021 104 6

Trichlorofluoromethane 25ug/kg501380 50-150125032 110 1

Vinyl Acetate 35ug/kg501860 35-150125026 149 3

Vinyl chloride 35ug/kg501110 10-150125025 89 1





1,1,1-Trichloroethane ug/kg1001250 50-1251250 ND39 100

1,1,2,2-Tetrachloroethane ug/kg1001560 50-1301250 ND36 125

1,1,2-Trichloroethane ug/kg1001390 55-1201250 ND47 112

1,1-Dichloroethane ug/kg1001220 55-1251250 ND30 98

1,1-Dichloroethene ug/kg1001240 25-1401250 ND46 100

1,1-Dichloropropene ug/kg1001340 55-1251250 ND39 108

1,2,3-Trichlorobenzene ug/kg200997 35-1401250 ND36 80

1,2,3-Trichloropropane ug/kg2001670 35-1401250 ND40 134

1,2,4-Trimethylbenzene ug/kg1001260 50-1301250 ND55 101

1,2-Dibromoethane (EDB) ug/kg1001420 55-1201250 ND31 114

1,2-Dichlorobenzene ug/kg1001370 60-1201250 ND42 110

1,2-Dichloroethane ug/kg1001220 55-1301250 ND59 98

1,2-Dichloropropane ug/kg1001320 60-1201250 ND38 106

1,3,5-Trimethylbenzene ug/kg1001240 45-1351250 ND32 99





2-Butanone (MEK) ug/kg10001840 40-1501250 ND400 147

2-Chlorotoluene ug/kg1001360 60-1201250 ND30 109

2-Hexanone ug/kg5001590 20-1501250 ND420 128

Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



4-Chlorotoluene ug/kg1001410 55-1301250 ND36 113

4-Methyl-2-pentanone (MIBK) ug/kg5001690 40-1301250 N1ND340 136

Acetone ug/kg10001550 10-1501250 ND660 124

Benzene ug/kg1001300 55-1201250 ND46 104

Bromobenzene ug/kg1001500 60-1251250 ND36 121

Bromochloromethane ug/kg1001320 50-1351250 ND49 106

Bromodichloromethane ug/kg1001270 60-1201250 ND36 101

Bromoform ug/kg1001280 40-1251250 ND40 102

Bromomethane ug/kg5001030 10-1401250 41.917 79

Carbon tetrachloride ug/kg1001350 40-1351250 ND40 108

Chlorobenzene ug/kg1001270 65-1201250 ND23 102

Chloroethane ug/kg1001140 10-1401250 ND61 91

Chloroform ug/kg1001180 60-1251250 ND48 95

Chloromethane ug/kg500849 10-1401250 ND51 68

cis-1,2-Dichloroethene ug/kg1001240 55-1251250 ND42 100

cis-1,3-Dichloropropene ug/kg1001320 55-1201250 ND30 106

Dibromochloromethane ug/kg1001270 55-1251250 ND23 102

Dichlorodifluoromethane ug/kg100545 10-1501250 ND38 44

Ethylbenzene ug/kg1001380 60-1251250 ND26 111

m,p-Xylenes ug/kg2001400 55-1251250 ND68 112

Methyl-tert-butyl Ether (MTBE) ug/kg1001230 50-1301250 ND35 98

Methylene Chloride ug/kg2001120 50-1201250 ND63 90

n-Butylbenzene ug/kg1001040 40-1351250 16235 71

n-Propylbenzene ug/kg1001360 55-1301250 ND34 109

o-Xylene ug/kg1001370 60-1251250 ND32 110

p-Isopropyltoluene ug/kg1001190 45-1351250 ND40 96

sec-Butylbenzene ug/kg1001250 50-1301250 ND35 100

Styrene ug/kg1001270 55-1251250 ND25 102

tert-Butylbenzene ug/kg1001230 55-1251250 ND41 98

Tetrachloroethene ug/kg1001350 60-1301250 ND19 108

Toluene ug/kg1001340 55-1251250 ND30 107

trans-1,2-Dichloroethene ug/kg1001250 50-1301250 ND37 100

trans-1,3-Dichloropropene ug/kg1001220 55-1251250 ND30 98

Trichloroethene ug/kg1001420 40-1451250 ND42 114

Trichlorofluoromethane ug/kg1001140 20-1501250 ND63 91

Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



Vinyl Acetate ug/kg100946 10-1501250 ND51 76

Vinyl chloride ug/kg100403 10-1501250 ND50 32





1,1,1-Trichloroethane 15ug/kg1001180 50-1251250 ND39 95 5

1,1,2,2-Tetrachloroethane 25ug/kg1001560 50-1301250 ND36 125 0

1,1,2-Trichloroethane 25ug/kg1001340 55-1201250 ND47 107 4

1,1-Dichloroethane 25ug/kg1001160 55-1251250 ND30 93 5

1,1-Dichloroethene 35ug/kg1001230 25-1401250 ND46 98 1

1,1-Dichloropropene 25ug/kg1001210 55-1251250 ND39 97 10

1,2,3-Trichlorobenzene 30ug/kg2001020 35-1401250 ND36 82 2

1,2,3-Trichloropropane 35ug/kg2001570 35-1401250 ND40 125 7

1,2,4-Trimethylbenzene 20ug/kg1001260 50-1301250 ND55 101 0

1,2-Dibromoethane (EDB) 25ug/kg1001260 55-1201250 ND31 101 12

1,2-Dichlorobenzene 25ug/kg1001320 60-1201250 ND42 106 4

1,2-Dichloroethane 25ug/kg1001150 55-1301250 ND59 92 6

1,2-Dichloropropane 25ug/kg1001250 60-1201250 ND38 100 6

1,3,5-Trimethylbenzene 20ug/kg1001240 45-1351250 ND32 99 0





2-Butanone (MEK) 35ug/kg10001710 40-1501250 ND400 137 7

2-Chlorotoluene 20ug/kg1001320 60-1201250 ND30 105 3

2-Hexanone 35ug/kg5001560 20-1501250 ND420 125 2

4-Chlorotoluene 20ug/kg1001340 55-1301250 ND36 107 5

4-Methyl-2-pentanone (MIBK) 30ug/kg5001640 40-1301250 N1ND340 131 4

Acetone 35ug/kg10001270 10-1501250 ND660 102 20

Benzene 25ug/kg1001230 55-1201250 ND46 98 6

Bromobenzene 25ug/kg1001430 60-1251250 ND36 115 5

Bromochloromethane 30ug/kg1001300 50-1351250 ND49 104 1

Bromodichloromethane 20ug/kg1001180 60-1201250 ND36 94 7

Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



Bromoform 35ug/kg1001310 40-1251250 ND40 105 2

Bromomethane 35ug/kg5001080 10-1401250 41.917 83 5

Carbon tetrachloride 30ug/kg1001200 40-1351250 ND40 96 11

Chlorobenzene 20ug/kg1001190 65-1201250 ND23 95 6

Chloroethane 35ug/kg1001160 10-1401250 ND61 93 2

Chloroform 25ug/kg1001140 60-1251250 ND48 92 3

Chloromethane 35ug/kg500947 10-1401250 ND51 76 11

cis-1,2-Dichloroethene 25ug/kg1001200 55-1251250 ND42 96 4

cis-1,3-Dichloropropene 20ug/kg1001230 55-1201250 ND30 98 7

Dibromochloromethane 30ug/kg1001200 55-1251250 ND23 96 6

Dichlorodifluoromethane 35ug/kg100767 10-1501250 ND38 61 34

Ethylbenzene 20ug/kg1001280 60-1251250 ND26 102 8

m,p-Xylenes 20ug/kg2001320 55-1251250 ND68 106 6

Methyl-tert-butyl Ether (MTBE) 35ug/kg1001250 50-1301250 ND35 100 2

Methylene Chloride 30ug/kg2001090 50-1201250 ND63 87 3

n-Butylbenzene 25ug/kg1001020 40-1351250 16235 69 2

n-Propylbenzene 20ug/kg1001330 55-1301250 ND34 106 3

o-Xylene 30ug/kg1001240 60-1251250 ND32 99 10

p-Isopropyltoluene 25ug/kg1001130 45-1351250 ND40 90 6

sec-Butylbenzene 20ug/kg1001270 50-1301250 ND35 101 2

Styrene 20ug/kg1001190 55-1251250 ND25 95 7

tert-Butylbenzene 25ug/kg1001200 55-1251250 ND41 96 2

Tetrachloroethene 20ug/kg1001230 60-1301250 ND19 99 9

Toluene 35ug/kg1001260 55-1251250 ND30 101 6

trans-1,2-Dichloroethene 25ug/kg1001240 50-1301250 ND37 99 1

trans-1,3-Dichloropropene 25ug/kg1001110 55-1251250 ND30 88 10

Trichloroethene 35ug/kg1001270 40-1451250 ND42 101 11

Trichlorofluoromethane 35ug/kg1001080 20-1501250 ND63 87 5

Vinyl Acetate 35ug/kg1001090 10-1501250 ND51 87 14

Vinyl chloride 35ug/kg100406 10-1501250 ND50 32 1




Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

QualifiersMDL



Chromium VI mg/l0.010ND 0.0050


Chromium VI mg/l0.0100.0930 85-1150.1000.0050 93


Chromium VI 20mg/l0.0100.0920 85-1150.1000.0050 92 1


Chromium VI mg/l0.0100.0520 80-1250.100 M2ND0.0050 52


Chromium VI 20mg/l0.0100.0520 80-1250.100 M2ND0.0050 52 0

Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013


E4 Concentration estimated. Analyte was detected below laboratory minimum reporting limit (MRL).

E8 Analyte reported to the MDL per project specification. Target analyte was not detected in the sample.


M2 Matrix spike recovery was low; the associated blank spike recovery was acceptable.





Project Manager

TestAmerica Phoenix

PSI0067





454-9303





Sampled:

Received:

09/01/09


Project ID:

PSI0067

PGAN 14682.013



TestAmerica Phoenix

Water XSM3500CR-D

Soil XSW8260B

Water XSW8260B



Project Manager

TestAmerica Phoenix

PSI0067





TAL-0013-550 (12/08)

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Sam1te Description Sample Container Matrix Type


['l<J:Phoenix- 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303 [ 1 Tucson- 1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ 1 Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

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I"Relin~ Date/Time: 7~edBy: Date/Time: 24 hours 5 days

48 hours normal X Relinquished By: Date/Time: (_ Received~& 4/1/;Jr Jroou

Sample Integrity: (Check)

intact on ice ?\ 'L-

Note: By relinquishing samples to TestAmerica, client agrees to pay for the services requested on this chain of custody form and any additional analyses performed on this project. } 7 Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days. . · , :> DC .

Documents

LABORATORY REPORT - United States Environmental · PDF fileQA/QC CRITERIA: All analyses met method criteria, ... LABORATORY REPORT Prepared For: AMEC Geomatrix Consultants, Inc. -