LABORATORY REPORT Aquatic Testing Laboratories · PDF file07.01.2014 · FATHEAD MINNOW HAZARDOUS WASTE SCREEN BIOASSAY Lab No.: Aquatic Testing Laboratories Client/ID: TEST SUMMARY

LABORATORY REPORT

Date: January 7, 2014

Client: Yolo County District Attorney301 Second StreetWoodland, CA 95695Attn: Heidi D'Agostino

AquaticTesting

Laboratories

Dedicated to providing quality aquatic toxicity testing"

4350 Transport Street, Unit 107Ventura, CA 93003

(805) 650-0546 FAX (805) 650-0756

CA DOES ELAP Cert. No.: 1775

Laboratory No.:Client Sample No.

A-13123001-021/03141A-51A

Sample Control: The samples were received by ATL in new and unopened packaging, with the chainof custody record attached.

Date Received: 12/30/13Date Tested: 01/03/14 to 01/07/14

Sample Analysis: The following analyses were performed on your sample:

CCR Title 22 Fathead Minnow Hazardous Waste Screen Bioassay (Polisini & Miller 1988).

Attached are the test data generated from the analysis of your sample. All testing wasconducted under the direct supervision of Joseph A. LeMay.

Result Summary:Sample ID. Results

41A- A&H 2X Liq Lavender & Linen FAIL (LC50 < 400 mg/1)42A- A&H Liq Det 2X Clean Burst FAIL (LC50 < 400 mg/1)43A- Gain 2X Original Fresh Liq Deterg FAIL (LC50 < 400 mg/1)44A- Soft Scrub w/Lemon FAIL (LC50 < 400 mg/1)45A- Ivory Liquid Hand Soap Original FAIL (LC50 < 400 mg/1)46A- Palmolive Ultra Pure and Clear FAIL (LC50 < 400 mg/1)47A- Gain Liquid Dish Original Scent FAIL (LC50 < 400 mg/1)48A- SSL Liquid Dishwash Lemon FAIL (LC50 < 400 mg/1)49A- Sun 2X LQ Tropical Breeze FAIL (LC50 < 400 mg/1)50A- Sun Burst Clean & Fresh 2X FAIL (LC50 < 400 mg/1)51 A- Sun Lemon Liquid Dish Soap FAIL (LC50 < 400 mg/1)

Quality Control: Reviewed and approved by:

Joseph A.Laboratory

This report pertains only to the samples investigated and does not necessarily apply to other apparently identical or similar materials. This report is submitted for the exclusive use of theclient to whom it is addressed. Any reproduction of this report or use of the Laboratory's name for advertising or publicity purpose without authorization is prohibited.

FATHEAD MINNOW HAZARDOUS WASTESCREEN BIOASSAY

Lab No.: Af3

Client/ID:7.X,. Ufa

' TEST SUMMARYSpecies: Pimephales promelas.Fish weight (gm): av: 0.23; min: 0.21; max: 0.25.Reference Toxicant: SDS conducted monthly.Test chamber volume: 10 liters.Temperature: 20 +/- 2°C.Aeration: none, unless D.O. drops below 5.0 mg/1.Number of replicates: 2.Dilution water: Soft reconstituted water (40-48 mg/1 CaCO3).

11 AquaticTestingLaboratories

Source: Thomas Fish.Regulations: CCR Title 22.Test Protocol: California F&G/DHS 1988.Endpoints: Survival at 96 hrs.Test type: Static.Feeding: None.Number offish per chamber: 10.Photoperiod: 16/8 hrs light/dark.

TEST DATA

Date/Time:

Analyst:

INITIAL

/->-/«/ iiv*

DO PH

24 Hr

DO pH #D

48 Hr

DO PH # D

72 Hr

DO PH #D

96 Hr

DO pH # D

Control A 117 o (17 77 0 ? 0Control B t.o ft* a* 7.7 0 ^77 /ts- O

400 mg/1 A to

400 mg/1 B 'U f. 1° (d

750 mg/1 A t. ft? 9-1 I*

750 mg/1 B

pH Control 71 O £?

Comments: Extraction method: Mechanical shakingNone (aqueous solution)

Dissolved Oxygen (DO) readings in mg/1 O2. Test Aerated: Yes / No pH Control adjusted with HCl/NaOH to pH similar to sample tanks

Initial

Final

CONTROL

Alkalinity

^ ^ mg/1 CaCOj

"J 2- mg/1 CaCO,

Hardness

Y ^ mgA CaC03

y 7 mg/1 CaCO,

HIGH CONCENTRATION

Alkalinity

) 1 mg/lCaCO,

mg/1 CaCO,

Hardness

yjf mg/lCaCO,

— mg/1 CaCOj

Total Number Dead

Control

400 mg/1

750 mg/1

O /20

£o /20

to /20

RESULTS(the checked result applies based on fish survival rates )

Â

/A^

PASSED

FAILED

FAILED

LC50 > 750 mg/1 (<40% dead in 750 mg/1 cone.)

^40% dead in 750 mg/1 (close to passing - definitive test recommended)

LC50 < 400 mg/1 (>60% dead in 400 mg/1 cone.)


Lab No.: Ittoot -

Client/ID:

TEST SUMMARYSpecies: Pimephales promelas.Fish weight (gm): av: 0.23; min: 0.21; max: 0.25.Reference Toxicant: SDS conducted monthly.Test chamber volume: 10 liters.Temperature: 20 +/- 2°C.Aeration: none, unless D.O. drops below 5.0 mg/1.Number of replicates: 2.Dilution water: Soft reconstituted water (40-48 mg/1 CaCO3).

11 AquaticTesting

Laboratories


TEST DATA

Date/Time:

Analyst:

Control A

Control B

400 mg/1 A

400 mg/1 B

750 mg/1 A

750 mg/1 B

pH Control

INITIAL

/"" 5~^V /f¥&

sô c >

b,0

ttf**l*>((4j1

ft 6f i t

DO

*•>

fctH

f'i

*,l„

*-*

pH

*1f-o

it

**

f.rv

*,/

24 Hr

f'V~/<S /A*"

/^°C

ill

nlm(t9

Wd*f*7

DO

^.>

2 y7-\

?>7>^T

pH

?rlf

7^5'f

«,?

M

g-?

^•y

# D

Ô

«7

t<?

^0

Comments: Extraction method: Mechanical shakiNone (aqueous solu

Dissolved Oxygen (DO) readings in mg/1 O2. Test Aerated: '

Initial

Final

48 Hr

/-T-/V //ysr

^&-°c

'T-7't*"

—

——

A?

DO

?.o1iO

f~

-

-

*••

n1R t^.

PH

777,7

—-^

. -9><1

# D

c?o

^

^

-

w

O

72 Hr

l~t>-<<4 ni0

V^-

°C

•&&

\tf

- —

^~

14. k

DO

£f

^^

-

—£.>

PH

?'?

?7

—

—7f

# D

(J

Cs

——c/

96 Hr

I't-ry t.*<^^

°C

ff'6

/r^

A.

"

/ fy

DO

k*

f<\

~

^

^'?

PH

-,(

7, i^/

—'?«r

# D

Oo^

*-

-V

O*P» ««6»M /- As: .zr/5^ ^^x ^^^

¥es / No pH Control adjusted with HCI/NaOH to pH similar to sample tanks

CONTROL HIGH CONCENTRATION

Alkalinity

3 I mg/1 CaCO3

^X mg/1 CaCO3

Hardness Alkalinity

^ & mg/lCaCOj i/o mg/lCaCOj

7 ^ mg/lCaCOj **v mg/lCaCO,

Hardness

U*( mg/1 CaCO3

— mg/1 CaCO,

Total Number Dead

Control

400 mg/1

750 mg/1

0 /2°2o /20

%C> /20

rt/A\J


PASSED

FAILED

FAILED





Lab No.: >7 l~> 1 1 "? tot? A Ol 3

Client/ID: \lo Coî-y 37

TEST SUMMARY

; max:Species: Pimephales promelas.Fish weight (gm): av: ^?-2>Reference Toxicant: SDS conducted per batch.Test chamber volume: 10 liters.Temperature: 20 +/- 2°C.Aeration: none, unless D.O. drops below 5.0 mg/1.Number of replicates: 2.Dilution water: Soft reconstituted water (40-48 mg/1 CaCO3).

11 AquaticTesting

Laboratories

Source: Thomas Fish.Regulations: CCR Title 22.Test Protocol: California F&G/DHS 1988.Endpoints: Survival at 96 hrs.Test type: Static.Feeding: None.Number of fish per chamber: 10.Photoperiod: 16/8 hrs light/dark.

TEST DATA

Date/Time:

Analyst:

Control A

Control B

400 mg/1 A

400 mg/1 B

750 mg/1 A

750 mg/1 B

INITIAL

i't-W l/V<

7

°C

*,«?

*1

ft .7

(f.7

(\1

ft?

DO

A 7

t.i

*(

*i

14f.i,

PH

•* ff

/uÔ

7*?«

M*.*

24 Hr

f-^/V //*5-

^°C

(f '7

r^(^(t/f t?it?

DO

?'7

7-V^^9v»

?/7

So

pH

?-

7^t^D

g-0

&vt<6

# D

oO

to

{*(0

(0

Comments: Extraction method: Mechanical shakiiNone (aqueous solu

Dissolved Oxygen (DO) readings in mg/1

Initial

Final

CONTROL

Alkalinity

2 f mg/1 CaCO,

3J- mg/1 CaCO,

Hardness

y ^ mg/1 CaCO,

Y 7 mg/1 CaCO,

48 Hr

/-r-/«/ /^^r

^°c

ff-7<1.«-

—s-

—

DO

X o70-

.X

^^

tig f^.tion) ^ — .

PH

?'l

27--

—

—

# D

O

c>

,

-

-

72 Hr

I - & — / " IfJ^fJ/\^-

°C

•&.O

If^

—_^

—

DO

£**7

^—

—

——

PH

2?

?^~-

——

^•>A êut v

# D

^

^-

—-

96 Hr

/-7-/<^ ^«^

^°C

^°'f^

^

^

.

S

DO'

^,6

5>r--—-

pH

?-(

1'^

—

-*».

-

# D

C?

£>

—-

—^

-Tte /*w./ 02. Test Aerated: Yes / No

HIGH CONCENTRATION

Alkalinity

) / mg/1 CaCO,

* mg/1 CaCO3

Hardness

Y/ mg/1 CaCO,

•* mg/1 CaCO,

Total Number Dead

Control

400 mg/1

750 mg/1

C> /2°ô /20

<ô /20

x^/^,LX


PASSED

FAILED

FAILED





Lab No.:

AquaticTestingLaboratories

Client/ID:

TEST SUMMARY

f ; max:jg.AT_.Species: Pitnephales promelas.Fish weight (gm): av: /?.2>; min:Reference Toxicant: SDS conducted per batch.Test chamber volume: 10 liters.Temperature: 20 +/- 2°C.Aeration: none, unless D.O. drops below 5.0 mg/1.Number of replicates: 2.Dilution water: Soft reconstituted water (40-48 mg/1 CaCO3).


TEST DATA

Date/Time:

Analyst:

Control A

Control B

400 mg/1 A

400 mg/1 B

750 mg/1 A

750 mg/1 B

INITIAL

I'J-W l/Vf

?

°c

&,<;

*1«.*

(*4fy*ft'

DO

£7t.L

M9.1

to

t'

PH

7?

fo

*•(

*./

M

*•*

24 Hr

t'</-f</ tfV

^2-

°C

(f7diIt'?r?7illit£

D(f

?')

7-Y?->ê;

«•>

f.?

pH

7-Ûfiu

t*>g^jr1<7

# D

6o(JO

fv

1 0

W



Initial

Final

CONTROL

Alkalinity

*) f mg/1 CaCO,

3 X mSfl CaCO,

Hardness

y ^ mg/1 CaCO,

y 7 mg/1 CaCO,

48 Hr

f-S"vy //vs'

^°c

^•7/t^--^

—

DO

7.0

7.0

~

-

x

^

nfi f^.tion) <^ .

PH

7.777

——-

—

# D

^0--

-

-

72 Hr

/-fc-N ;/?^/ 1— '

°c

l^<?/w—__

—

—

DO

b*I

^L~

—. —

—

PH

"T"*)?-?

——

——

-P^c/^^

#D

£>

^)

——*-

-^

96 Hr

/-?-/y A,*r

^°C

ffO

^—-

^

~

DO

£«>

f 'f

—

/-.

X

pH

7,^>-/^^

^^__^

# D

<9

^

-X"

—

-

'•«. A;«,,A^02. Test Aerated: Yes / No

HIGH CONCENTRATION

Alkalinity

~}\1 CaCO,

* mg/1 CaCO,

Hardness

y / mg/1 CaCO,

* mg/1 CaCO,

Total Number Dead

Control

400 mg/1

750 mg/1

0 /20

2o /20

^ /20

>f

yv/


PASSED

FAILED

FAILED





Lab No.: >?/^/3t ~>t9t?t~O

Client/ID: Yo/gIX1~-+\T SUMMARY

Species: Pimephales promelas.Fish weight (gm): av: 0.3.}', min: Q. t / ; max: jReference Toxicant: SDS conducted per batch.Test chamber volume: 10 liters.Temperature: 20 +/- 2°C.Aeration: none, unless D.O. drops below 5.0 mg/1.Number of replicates: 2.Dilution water: Soft reconstituted water (40-48 mg/1 CaCO3).

T ( AquaticTestingLaboratories


TEST DATA

Date/Time:

Analyst:

Control A

Control B

400 mg/1 A

400 mg/1 B

750 mg/1 A

750 mg/1 B

INITIAL

t'J'W l/Vf

?

°C

fc*

*1

(?•'

(itH 7

n.i

DO

*7It

t>t

*•!*.\. i

pH

7?fro

fc?

*Y

J-Y».)

24 Hr

/-*-/v //yr

^°C

0-7it'(v?

ft*<l*(T,*

DO

?J

7,ifft>eo9.1<iO

PH

7.y7$'•r*.**,«^^

#D

O

o(v(0

(0

U



Initial

Final

48 Hr

/-*-•/*' //ys-

^°C

/r7,?j

^^^

DO

?•<*

7-0_

^

-w.

^

"8 ^"-tion) < *1" .

pH

?77.7--

——

#D

^?O^--

—

72 Hr

J-fr-Yf f/?^

/^v

°C

?f

-~

. —

—— .

DO

fc^*^r

fr>^

——

—

pH

??

7-7

——

——

-/•** ,/f.X .

#D

&

~

—-^-

96 Hr

/ - /vy ^>?r

^°c

fTid

rf ^---

• >s

DO

/^

-Cf

"S

<

r

•

pH

^Y

^ D

^^

--

#D

<9

c>

.

-

-

^

aV*,u A.y^.

02. Test Aerated: Yes / No


Alkalinity

7 f mg/1 CaCO,

3 JL mg/1 CaCO,

Hardness Alkalinity

V mg" CaCO, ^ ^ mg/1 CaCO,

y 7 mg/1 CaCO, — mg/1 CaCO,

Hardness

<ja mg/1 CaCO,

— mg/1 CaCO,

Total Number Dead

Control

400 mg/1

750 mg/1

O /20

" 0 /20

ô /20


,4

A^XI/

PASSED

FAILED

FAILED





Lab No.: I">11

Client/ID: Ya/g I$oootf6/t>6

TEST SUMMARY

; max:Species: Pimephales promelas.Fish weight (gm): av: ^ .Jt>; min: Q.Reference Toxicant: SDS conducted per batch.Test chamber volume: 10 liters.Temperature: 20 +/- 2°C.Aeration: none, unless D.O. drops below 5.0 mg/1.Number of replicates: 2.Dilution water: Soft reconstituted water (40-48 mg/1 CaCO3).

T AquaticTestingLaboratories


TEST DATA

Date/Time:

Analyst:

INITIAL

I-}- ti<«

DO PH

24 Hr

rxf pH # D

48 Hr

DO PH # D

72 Hr

DO pH

96 Hr

DO pH #D

Control A I* (f-7 c?Control B 7-7 7-7 O

400 mg/1 A

400 mg/1 B (14 tv

750 mg/1 A it)

750 mg/1 B \U *7 L *•(

Comments: Extraction method: Mechanical shakingNone (aqueous solution) s*~.

Dissolved Oxygen (DO) readings in mg/102. Test Aerated: Yes / No

Initial

Final

CONTROL

Alkalinity

~) f mg/lCaCO,

3J^ mg^CaCO,

Hardness

y £ mg/1 CaCOj

V > mg/1 CaCOj

HIGH CONCENTRATION

Alkalinity

£0 mg/lCaCO,

— mg/1 CaCO,

Hardness

t/ ^ mg/1 CaCOj

~~ mg/1 CaCO3

Total Number Dead

Control

400 mg/1

750 mg/1

0 /2°ô /20

^> /20


A

rf.<X

PASSED

FAILED

FAILED





Lab No.: >?

Client/ID:

TEST SUMMARYSpecies: Pimephales promelas.Fish weight (gm): av: a-H"); min: Q.3L ( ; max:Reference Toxicant: SDS conducted per batch.Test chamber volume: 10 liters.Temperature: 20 +/- 2°C.Aeration: none, unless D.O. drops below 5.0 mg/1.Number of replicates: 2.Dilution water: Soft reconstituted water (40-48 mg/1 CaCO3).

T [ AquaticTestingLaboratories


TEST DATA

Date/Time:

Analyst:

Control A

Control B

400 mg/1 A

400 mg/1 B

750 mg/1 A

750 mg/1 B

INITIAL

l-l'tlf l/Vf

?

°C

*,0

*1

ft*

Mq.1r f <

DO

A 7I.Lt,r

s*<uf, *

PH

?ef

$i0

M*f«,/<.l

24 Hr

/-y-/v tits-

°C

it<7ill1*7hi(14fp

<^DO

7»*Mjtu

21

7^

PH

7,7«f,0^^«0<û

# D

o0

If?(0

\P



48 Hr

1-S--/Y KY*

°c

f?7/f-—-~-

DO

?.<?

7.0

^

^

-

-

n« t^.

pH

7-777-

———

#D

c?0

V

--

^>

72 Hr

l-*b~H \\lf>rj^\c

?00lj* /

—

——

DO

''I

lf*f^^

~

—

—

—

pH

7.7

7.7~-

— -

—

L. — •

#D

O0-

——-

96 Hr

l*7-lf r~VT

--°c

n$(ti—^--

DfT

/^^T-

—--

pH

7.^

?-/

,_

. —

—^

# D

^?

O

—-

-

-

-/="'>* WVt/ -'A. M/M./' ^v/-tion) /"^.


Initial

Final

CONTROL

Alkalinity

^ f mg/1 CaCO,

3JL mg/1 CaCO,

Hardness

y^ mg/ICaCOj

*/ 7 mg/1 CaCOj

HIGH CONCENTRATION

Alkalinity

^ / mg/1 CaCOj

*~ mg/1 CaCO,

Hardness

</ ^ ""g/1 CaCO,

"" mg/1 CaCO3

Total Number Dead

Control

400 mg/1

750 mg/1

0 /20

" 0 /20

2,0 /20


-4^v/

PASSED

FAILED

FAILED





Lab No.:

Client/ID: Va/g

TEST SUMMARY

; max:Species: Pimephales promelas.Fish weight (gm): av: <7-2>; min:Reference Toxicant: SDS conducted per batch.Test chamber volume: 10 liters.Temperature: 20 +/- 2°C.Aeration: none, unless D.O. drops below 5.0 mg/1.Number of replicates: 2.Dilution water: Soft reconstituted water (40-48 mg/1 CaCO3).

V ( AquaticTestingLaboratories


TEST DATA

Date/Time:

Analyst:

Control A

Control B

400 mg/1 A

400 mg/1 B

750 mg/1 A

750 mg/1 B

INITIAL

I'J'W t/Vf

7°c

*,*

*1<?,{(ft(\(<r*

DO

A 7t.l

6tl

f.f

**

*. ?

PH

?f

uf-l,,(M$•(

24 Hr

/-v-/v tlvr

^°c

ft -7rt/(t7<U

(^m

DO

?r^7.Y

?-»777y75-

pH

tf

11

f~0

90

9*

f.O

# D

oo(.0

(0

(t;\



Initial

Final

CONTROL

Alkalinity

~) f mg/1 CaCO,

5 JL mg/1 CaCOj

Hardness

V 6 ms" CaC°3

y > mg/l CaCO,

48 Hr

f-f'tf IKS'

<^°C

T-7( ty^'-^

DO

7i0?.o-,

^_-

ng (^.tion) / *" .

PH

7-7If-

—

—"

# D

d>

0

-•w

l.

-

72 Hr

/-£ -/V H3^

^°c

-zip(tf

——

—

DO

^f

^

—^

— -

pH

7.7

7-7

——

—-FH J*A .

#D

^

^

—

—-

96 Hr

/-7vy /^yr

^°C

^f.°

t*

-

-*

^

DO

^6>ct

—^

^

pH

^/?,^

—•

—^

# D

O^>^^

^ ,

—,-AU ,v*-^<*02. Test Aerated: Yes / No

HIGH CONCENTRATION

Alkalinity

_} mg/1 CaCOj

"~ mg/1 CaCOj

Hardness

(j «- mg/1 CaCO,

— mg/1 CaCO,

Total Number Dead

Control

400 mg/1

750 mg/1

6 /20

^0 /20

2^> /20


S<LX

PASSED

FAILED

FAILED


£40% dead in 750 mg/1 (close to passing - definitive test recommended)



Lab No.: >? /> /3 t

Client/ID: % (a t z if 3 7o »f I

TEST SUMMARY

; max:Species: Pimephales promelas.Fish weight (gm): av: a-H); min: tf>.Reference Toxicant: SDS conducted per batch.Test chamber volume: 10 liters.Temperature: 20 +/- 2°C.Aeration: none, unless D.O. drops below 5.0 mg/1.Number of replicates: 2.Dilution water: Soft reconstituted water (40-48 mg/1 CaCO3).

*T ( AquaticTestingLaboratories


TEST DATA

Date/Time

Analyst:

Control A

Control B

400 mg/1 A

400 mg/1 B

750 mg/1 A

750 mg/1 B

INITIAL

('}•!*/ l/Vf

7

°C

T*,0

*1

(U

(H

rt,£lf.7

DO

£7

1.1,

1.1f>6

%>*l.l,

PH

7?U

h*itr,

?.2

24 Hr

f-f'SY ffYS

^"C

07ftflt*lt-7^7/l(

DO

7->W7+

to»<(&t>

pH

7-f7.^.

$7

>r*-5

# D

ooI*

(«>

(^f o


Dissolved Oxygen (DO) readings in mg/1 <

Initial

Final

48 Hr

^rv*/ //ys^

^°c

ff '7I t - J-

-

-^

DO*

7'°X«

». .--s

IS t^.tion) /-"' .

PH

?.;

7-7._

——

# D

(?

0

^1

--

-

72 Hr

/~£-/H r/5^^-v

°C

Z^

(^—— .

——

DO

^-f

^>

—' —

—

pH

?^

7^—

———

-F--51 A«t.

#D

£>»

^

——

—-

96 Hr

f -? - /y /^y5-

^°C

Orfl

f 4 ^

•H

*~~

-

^

DO

ê>

$;?---

^

pH

?-^

7 ^_ _,--

# D

^>

^

•N

-

-

-

-•/W- l«!t,\, tr



Alkalinity

~> \1 CaCO,

^ **- mg/1 CaCO,

Hardness Alkalinity

y^ mg/1 CaCO, Yj mg/1 CaCO,

«/ 7 mg/1 CaCO, — mg/1 CaCO,

Hardness

y / mg/l CaCO,

— mg/1 CaCO,

Total Number Dead

Control

400 mg/1

750 mg/1

C /20

^0 /20

• o /20


rf

A ,IX

PASSED

^ FAILED

FAILED

LC50 > 750 mg/1 (<40% dead in 750 mg/l cone.)



FATHEAD MINNOW HAZARDOUS WASTESCREEN BIO ASSAY

Lab No.: A 3o»/~O

Client/ID:

TEST SUMMARYSpecies: Pimephales promelas.Fish weight (gm): av: 0.23; min: 0.21; max: 0.25.Reference Toxicant: SDS conducted monthly.Test chamber volume: 10 liters.Temperature: 20 +/- 2°C.Aeration: none, unless D.O. drops below 5.0 mg/1.Number of replicates: 2.Dilution water: Soft reconstituted water (40-48 mg/1 CaCO3).

AT AquaticTesting

Laboratories


TEST DATA

Date/Time:

Analyst:

Control A

Control B

400 mg/1 A

400 mg/1 B

750 mg/1 A

750 mg/1 B

pH Control

INITIAL

'-3-fV INS

^°C

*.o

ItfI1.\

f?.'Ill(T.{

DO

*•?

9,6

*,7

*• >

9 7*•**-y

pH

£79.o

7$

0

<$r,?r./

24 Hr

l~*fv //vs-

^°C

'T-7

'Vf f j tttimft?

DO

7r*

?.y9'7

^c */1 ^r

^/zt

PH

7«7.^Z]

f-o

^7?.?

*>Y

# D

C>^<7

(17

^19

O


Dissolved Oxygen (DO) readings in mg/1 O2. Test Aerated: '

Initial

Final

48 Hr

f- r-/y //y»~

^°c

(77f t ?-"-^

f t ?

DO

7-*r«_-"-^/

ng iX.tion) -^ .V'es / No ]

pH

7'77-7

—-

^

^

#Y

# D

f?

c?x

s

»-

^

6

72 Hr

/-£~Af U";tf^\C

7^

(1-1

— .

—— .

—(^

DO

£-f

*^^^

^

^

—

pH

^?

7-7^

—— .—

7^

# D

£>

£

-

—

—

—&

96 Hr

^7-/y ^y^T

^°C

f^-C

^

-

-

-

/ ty

DO

&0

y-T—---

5-

pH

7.*?(>

—^^-

2C

# D

e?o-

—

—^^

-h ;+.•*! />H 7- ^sH Control adjusted with HCl/NaOH to pH similar to sample tanks

CONTROL

Alkalinity

/ ( mg/1 CaCO,

3 J~ mg/1 CaCO,

Hardness

«/^ mg/1 CaCO,

V7 m^CaCO,

HIGH CONCENTRATION

Alkalinity

U 1 mg/1 CaCO,

— - mg/1 CaCO,

Hardness

Uf mg/1 CaCO,

— mg/1 CaCO,

Total Number Dead

Control

400 mg/1

750 mg/1

O /20

20 /20

ô /20


/4

/•*,\sPASSED

FAILED

FAILED





Lab No.:

Client/ID: Vg/g Ca*«+»

TEST SUMMARY

/ ; max:Species: Pimephales promelas,Fish weight (gm): av: <y.3>; min:Reference Toxicant: SDS conducted per batch.Test chamber volume: 10 liters.Temperature: 20 +/- 2°C.Aeration: none, unless D.O. drops below 5.0 mg/1.Number of replicates: 2.Dilution water: Soft reconstituted water (40-48 mg/1 CaCO3).

*T [ AquaticTestingLaboratories

Source: Thomas Fish.Regulations: CCR Title 22.Test Protocol: California F&G/DHS 1988.Endpoints: Survival at 96 hrs.Test type: Static.Feeding: None.Number of fish per chamber: 10.Photoperiod: 16/8 hrs light/dark.

TEST DATA

Date/Time:

Analyst:

Control A

Control B

400 mg/1 A

400 mg/1 B

750 mg/1 A

750 mg/1 B

INITIAL

('}•«/ l/Vf

7°c

l>,0

*1Mf t *min

DO

A 7£1

fcjr

*.'t,7

&°l

PH

?t

fro

9>>

t.7

*;*?

24 Hr

/-Y-/V ''f5-

<&°c

«T7ffY/K(17

'17tit

DO

?r>7-V^?9'?^.T

^,T

pH

?•*

7*

s.?«•?fc.yV^

# D

0

^1°\. 0

1.0



Initial

Final

CONTROL

Alkalinity

"} f mg/lCaCO,

3^L mg/1 CaCO,

Hardness

y£ mg^CaCO,

*/ 7 "'S'1 CaC°3

48 Hr

I ' f ' f t f /rrs~

^°c

11?nt

—*

*>-

DO

?.07o

^

-

-

-

n* ^.tion) ^" .

pH

>.77.7-

*»

v

s

#D

i?

0

^

-^

»»

•c

72 Hr

/.6>-rv ^3^'> — .

°c

2?^

(^

-

———

DO

^

^—

—— -

—

PH

2?

?7

—

—

—~

- f-'<> A c/Û

#D

^^<2?

——

—

—

96 Hr

I-?-/Y toys'

^"C

(1?n*-^

—

—

DO

t>°

W

-

^

s

pH

?./

7/N

-

-

—

# D

^>

^>

^

-

-•*•

u/.' /*»•'••« 'it/Mi t Aou/'


HIGH CONCENTRATION

Alkalinity

) / mg/1 CaCO,

mg/1 CaCOj

Hardness

Y/ mg/lCaCO,

~~ mg/1 CaCO3

Total Number Dead

Control

400 mg/1

750 mg/1

0 /20

2^ /20

Q*> /20

M/îX


PASSED

FAILED

FAILED




/Â%

Testing Facility

Facility name: Aquatic Testing Laboratories

Facility address: 4350 Transport Street, Unit 107, Ventura, CA93003

LlSample Number

41A

42A

43A

44A

45A

4SA

47A

48A

49A

50A

S1A

52A

53A

S4A

55A

56A

S7A

58A

59A

60A

Description

A&H 2X LIQ LAVENDER & LINEN

A&H LIQ DET 2X CLEAN BURST

GAIN 2X ORIGINAL FRESH LIQ DETERG

SOFT SCRUB W/ LEMON

IVORY LIQUID HAND SOAP ORIGINAL

PALMOLIVE ULTRA PURE AND CLEAR

GAIN LIQUID DISH ORIGINAL SCENT

SSL LIQUID DISHWASH LEMON

SUN 2X LQ TROPICAL BREEZE

SUN BURST CLEAN & FRESH 2X

SUN LEMON LIQUID DISH SOAP

SUN SATIONS AUTO DISH GEL

TIDE LQ PODS OCEAN MIST

LYSOL TOILET BOWL CLEANER

PALMOLIVE ORIGINAL

CLOROX TOILET BOWL CLEANER BLCH G

CLOROX TOILET BOWL GREEN WORKS

DRANO PROFESSIONAL STRENGTH

SNUGGLE BLUE SPARKEL

ALL OXI-ACTIVE STAINLIFTERS WATER

OFFICE OF THE DISTRICT ATTORNEYSAN JOAQUIN COUNTY

222 E Weber Avenue, Suite 678, Stockton, CA 95202P.O. Box 990, Stockton, California 95201

Telephone: (209) 468-2400 Fax: (209) 468-03 1 4

CHAIN OF CUSTODY RECORD

Manufacturer UPC

3320009332

3320009470

3700012784

2340000865

3700040312

3500046106

3700086176

71754411703

7261370896

7261370809

7261316008

7261324025

3700050962

1920002522

3500046112

4460030619

4460000451

1980040109

7261345171

7261345497

Quantity

75 oz

150 oi

5002

24 oz

48 oz

25 oz

24 oz

40 oz188 oz,

125 loads

45.4 oz

20 oz

75 oz27 oz,31 ct

24 oz

25 oz

24 oz

2402

80 oz64 oz,

26 loads

150 oz

Main Ingredient / Or Usage / NOTES

,

S

o

Please send results to:

Name: nvestigator Heidi D'Agostino

Email: [email protected]

Fax: 530-666-8423

Time sampled

Sample containerdescription

Method of sampling:Composite (C) Grab (G)

n/a

n/a

n/a

n/a

n/a

n/a

n/a

n/a

n/a

n/a

n/a

n/a

n/a

n/a

n/a

n/a

n/a

n/a

n/a

n/a

Size of sample container(include units)

200g (min)

200( (min)

200g (min)

200s (min)

200< [mini

200« (mini

200( (min)

200s (min)

200s (mini

2008 (min)

200g (min)

200B (min)

200g (min)

200« (min)

2008 (min)

2008 (min)

2008 (mini

2008 (min)

2008 Imin)

2008 Imin)

ample containerPlastic (P) Metal

r) VOA(V)

•sssill£ a S

P

P

P

P

P

P

P

P

P

P

P

P

P

P

P

P

P

P

P

P

Evidence tape: Yes(Y)No(N)

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

Transported In Iced cooler:Yes(Y) No(N)

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

Requiredanalysis

96-hour fishbloassay

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

NOTE: All Samples were taken at 222 E. Weber Ave.. Room 678. Stockton. CA 95202

NarjA / Title

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Documents

LABORATORY REPORT Aquatic Testing Laboratories · PDF file07.01.2014 · FATHEAD MINNOW HAZARDOUS WASTE SCREEN BIOASSAY Lab No.: Aquatic Testing Laboratories Client/ID: TEST SUMMARY