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www. itquima..es LABORATORY OF CATALYSIS AND MATERIALS Institute of Chemical and Enviromental Technologies

LABORATORY OF CATALYSIS AND MATERIALS - Blog UCLM...Mezclado y Agitación (1min) Liofilización - Tiempo de congelación:6h. - Presión de vacío: 0,08 mbar. - Temperatura de bandeja:

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Page 1: LABORATORY OF CATALYSIS AND MATERIALS - Blog UCLM...Mezclado y Agitación (1min) Liofilización - Tiempo de congelación:6h. - Presión de vacío: 0,08 mbar. - Temperatura de bandeja:

wwwitquimaes

LABORATORY OF

CATALYSIS AND MATERIALS

Instituteof Chemical and EnviromentalTechnologies

ITQUIMA UCLMLABORATORY OF CATALYSIS AND MATERIALS

INNOVATION AND

TECHNOLOGICAL DEVELOPMENT

DIFFERENTIAL VALUE

Synthesis and characterization

of Graphene and other carbon

and inorganic nanomaterials

(CNT CNF CNS CrO ZnO

Al2O3 etc)

2

Calentamiento

(81 C) y agitacioacuten

Ultrasonidos(1h)

Mezclado y Agitacioacuten (1min)

Liofilizacioacuten- Tiempo de congelacioacuten6h-Presioacuten de vaciacuteo 008 mbar

-Temperatura de bandeja 35degC-Tiempo del proceso 6+27 h

AguaPVA

AguaMateriales Nanocarbonosos

Synthesis at lab and pilot plant

scale and characterization of

polymer composites and aerogels

doped with nanomaterials

AEROGELGRAPHENE

Thermochemical valorisation of agro-industrial wastes and vegetable and

animal biomass (terrestrial and marine) through pyrolysis combustion and

gasification processes at lab and pilot plant scale

$

Products Ash biofuelgas

M

EnergyBIOMASS VALORIZATION

Thermochemical processesto pilot plant scale

Thermochemical processesat laboartory scale

Dried- Crushed

ITQUIMA UCLM

3

Chemical processes analysis and life cycle assessment (SIMAPRO)

Simulation modelling optimization and basic engineering of

chemical processes

Catalytic and electrocatalytic processes for the transformation of

alcohols ammonia synthesis gas and waste products (CO2) into

higher-added value compounds

LABORATORY OF CATALYSIS AND MATERIALS

Biomass

Air

DRYER

Air

CRUSHER

Air

COMBUSTOR

CYCLONE

Ash

Gas

RANKINE CYCLE

BURNDECOMP

Q

InputGoods

Services

ResourcesProcess

CO2

CO

NOx

CH4

Wastes

4

ITQUIMA UCLM

SERVICES AND TECHNICAL ADVISORY

Physical-chemical tests

bull Turbidity index (TSI)

bull Scanning electron

microscopy (SEM)

bull Fourier transform infrared

spectroscopy (FTIR)

bull Volume and density of

powders foams and bulk

solids

bull Pore size and pore

distribution (Hg porosimetry

and BET)

bull Abrasion test of materials

bull Surface tension

bull Sound absorption analysis

Mechanical tests and Rheology

bull Dynamic mechanical analysis

(DMA)

bull Tensile flexural and compression

bull Shore D hardness

bull Rheology of liquids and

suspensions

bull Curing of adhesives and resins

LABORATORY OF CATALYSIS AND MATERIALS

5

ITQUIMA UCLM

Thermogravimetric and thermal

analysis

bull Differential scanning calorimetry

(DSC)

bull TGA-MS at atmospheric and high

pressure

bull Thermal conductivity of materials

bull Flash pyrolyzer coupled to GC-MS

Sample preparation

bull Extruder

bull Injection moulding

bull Sample cutting press

bull Powder and conductive samples for

SEM analysis

bull Centrifugation orbital mixing and

grinding

bull Solid V-Mixer

LABORATORY OF CATALYSIS AND MATERIALS

6

Catalysis and Electrocatalysis

bull Synthesis of catalysts at lab and bench scale

bull Spin-coater and electrode preparation robot

bull Physical-chemical characterization of

catalysts (BET TPD TPR TPO acidity

chemisorption oxidation by pulses

titrations etc)

bull Electrochemical characterization of

electrocatalysts (rotary disc ECSA analysis

Tafel curves etc)

bull Different catalytic and electrocatalytic

configurations analysis of effluents (GC

microGC and HPLC)

ITQUIMA UCLM

PROCESSES AND PRODUCTS

FROM THE LAB TO THE INDUSTRIAL DEPLOYMENT

LABORATORY OF CATALYSIS AND MATERIALS

7

ITQUIMA UCLM

A SINGLE CENTER FOR ALL THE

TECHNOLOGICAL SERVICES

(SINGLE POINT LAB)

LABORATORY OF CATALYSIS AND MATERIALS

(UCLM)

Development of new materials

BUSINESS

Innovation and support

FROM INNOVATIONTO MARKET IMPLEMENTATION

LABORATORY OF CATALYSIS AND MATERIALS

wwwitquimaes

LABORATORY CATALYSIS AND MATERIALS Institute of Chemical and Environmental

Technologies (ITQUIMA)

University of castilla la Mancha

Avenida Camilo Joseacute Cela sn

13004 Ciudad Real

Tel +34 902 204100 (ext96322)

Responsible for laboratory

M Luz Sanchez Silva Tel +34 926 295 3000|Ext 6307

mariaLuzsanchezuclmes

Page 2: LABORATORY OF CATALYSIS AND MATERIALS - Blog UCLM...Mezclado y Agitación (1min) Liofilización - Tiempo de congelación:6h. - Presión de vacío: 0,08 mbar. - Temperatura de bandeja:

ITQUIMA UCLMLABORATORY OF CATALYSIS AND MATERIALS

INNOVATION AND

TECHNOLOGICAL DEVELOPMENT

DIFFERENTIAL VALUE

Synthesis and characterization

of Graphene and other carbon

and inorganic nanomaterials

(CNT CNF CNS CrO ZnO

Al2O3 etc)

2

Calentamiento

(81 C) y agitacioacuten

Ultrasonidos(1h)

Mezclado y Agitacioacuten (1min)

Liofilizacioacuten- Tiempo de congelacioacuten6h-Presioacuten de vaciacuteo 008 mbar

-Temperatura de bandeja 35degC-Tiempo del proceso 6+27 h

AguaPVA

AguaMateriales Nanocarbonosos

Synthesis at lab and pilot plant

scale and characterization of

polymer composites and aerogels

doped with nanomaterials

AEROGELGRAPHENE

Thermochemical valorisation of agro-industrial wastes and vegetable and

animal biomass (terrestrial and marine) through pyrolysis combustion and

gasification processes at lab and pilot plant scale

$

Products Ash biofuelgas

M

EnergyBIOMASS VALORIZATION

Thermochemical processesto pilot plant scale

Thermochemical processesat laboartory scale

Dried- Crushed

ITQUIMA UCLM

3

Chemical processes analysis and life cycle assessment (SIMAPRO)

Simulation modelling optimization and basic engineering of

chemical processes

Catalytic and electrocatalytic processes for the transformation of

alcohols ammonia synthesis gas and waste products (CO2) into

higher-added value compounds

LABORATORY OF CATALYSIS AND MATERIALS

Biomass

Air

DRYER

Air

CRUSHER

Air

COMBUSTOR

CYCLONE

Ash

Gas

RANKINE CYCLE

BURNDECOMP

Q

InputGoods

Services

ResourcesProcess

CO2

CO

NOx

CH4

Wastes

4

ITQUIMA UCLM

SERVICES AND TECHNICAL ADVISORY

Physical-chemical tests

bull Turbidity index (TSI)

bull Scanning electron

microscopy (SEM)

bull Fourier transform infrared

spectroscopy (FTIR)

bull Volume and density of

powders foams and bulk

solids

bull Pore size and pore

distribution (Hg porosimetry

and BET)

bull Abrasion test of materials

bull Surface tension

bull Sound absorption analysis

Mechanical tests and Rheology

bull Dynamic mechanical analysis

(DMA)

bull Tensile flexural and compression

bull Shore D hardness

bull Rheology of liquids and

suspensions

bull Curing of adhesives and resins

LABORATORY OF CATALYSIS AND MATERIALS

5

ITQUIMA UCLM

Thermogravimetric and thermal

analysis

bull Differential scanning calorimetry

(DSC)

bull TGA-MS at atmospheric and high

pressure

bull Thermal conductivity of materials

bull Flash pyrolyzer coupled to GC-MS

Sample preparation

bull Extruder

bull Injection moulding

bull Sample cutting press

bull Powder and conductive samples for

SEM analysis

bull Centrifugation orbital mixing and

grinding

bull Solid V-Mixer

LABORATORY OF CATALYSIS AND MATERIALS

6

Catalysis and Electrocatalysis

bull Synthesis of catalysts at lab and bench scale

bull Spin-coater and electrode preparation robot

bull Physical-chemical characterization of

catalysts (BET TPD TPR TPO acidity

chemisorption oxidation by pulses

titrations etc)

bull Electrochemical characterization of

electrocatalysts (rotary disc ECSA analysis

Tafel curves etc)

bull Different catalytic and electrocatalytic

configurations analysis of effluents (GC

microGC and HPLC)

ITQUIMA UCLM

PROCESSES AND PRODUCTS

FROM THE LAB TO THE INDUSTRIAL DEPLOYMENT

LABORATORY OF CATALYSIS AND MATERIALS

7

ITQUIMA UCLM

A SINGLE CENTER FOR ALL THE

TECHNOLOGICAL SERVICES

(SINGLE POINT LAB)

LABORATORY OF CATALYSIS AND MATERIALS

(UCLM)

Development of new materials

BUSINESS

Innovation and support

FROM INNOVATIONTO MARKET IMPLEMENTATION

LABORATORY OF CATALYSIS AND MATERIALS

wwwitquimaes

LABORATORY CATALYSIS AND MATERIALS Institute of Chemical and Environmental

Technologies (ITQUIMA)

University of castilla la Mancha

Avenida Camilo Joseacute Cela sn

13004 Ciudad Real

Tel +34 902 204100 (ext96322)

Responsible for laboratory

M Luz Sanchez Silva Tel +34 926 295 3000|Ext 6307

mariaLuzsanchezuclmes

Page 3: LABORATORY OF CATALYSIS AND MATERIALS - Blog UCLM...Mezclado y Agitación (1min) Liofilización - Tiempo de congelación:6h. - Presión de vacío: 0,08 mbar. - Temperatura de bandeja:

ITQUIMA UCLM

3

Chemical processes analysis and life cycle assessment (SIMAPRO)

Simulation modelling optimization and basic engineering of

chemical processes

Catalytic and electrocatalytic processes for the transformation of

alcohols ammonia synthesis gas and waste products (CO2) into

higher-added value compounds

LABORATORY OF CATALYSIS AND MATERIALS

Biomass

Air

DRYER

Air

CRUSHER

Air

COMBUSTOR

CYCLONE

Ash

Gas

RANKINE CYCLE

BURNDECOMP

Q

InputGoods

Services

ResourcesProcess

CO2

CO

NOx

CH4

Wastes

4

ITQUIMA UCLM

SERVICES AND TECHNICAL ADVISORY

Physical-chemical tests

bull Turbidity index (TSI)

bull Scanning electron

microscopy (SEM)

bull Fourier transform infrared

spectroscopy (FTIR)

bull Volume and density of

powders foams and bulk

solids

bull Pore size and pore

distribution (Hg porosimetry

and BET)

bull Abrasion test of materials

bull Surface tension

bull Sound absorption analysis

Mechanical tests and Rheology

bull Dynamic mechanical analysis

(DMA)

bull Tensile flexural and compression

bull Shore D hardness

bull Rheology of liquids and

suspensions

bull Curing of adhesives and resins

LABORATORY OF CATALYSIS AND MATERIALS

5

ITQUIMA UCLM

Thermogravimetric and thermal

analysis

bull Differential scanning calorimetry

(DSC)

bull TGA-MS at atmospheric and high

pressure

bull Thermal conductivity of materials

bull Flash pyrolyzer coupled to GC-MS

Sample preparation

bull Extruder

bull Injection moulding

bull Sample cutting press

bull Powder and conductive samples for

SEM analysis

bull Centrifugation orbital mixing and

grinding

bull Solid V-Mixer

LABORATORY OF CATALYSIS AND MATERIALS

6

Catalysis and Electrocatalysis

bull Synthesis of catalysts at lab and bench scale

bull Spin-coater and electrode preparation robot

bull Physical-chemical characterization of

catalysts (BET TPD TPR TPO acidity

chemisorption oxidation by pulses

titrations etc)

bull Electrochemical characterization of

electrocatalysts (rotary disc ECSA analysis

Tafel curves etc)

bull Different catalytic and electrocatalytic

configurations analysis of effluents (GC

microGC and HPLC)

ITQUIMA UCLM

PROCESSES AND PRODUCTS

FROM THE LAB TO THE INDUSTRIAL DEPLOYMENT

LABORATORY OF CATALYSIS AND MATERIALS

7

ITQUIMA UCLM

A SINGLE CENTER FOR ALL THE

TECHNOLOGICAL SERVICES

(SINGLE POINT LAB)

LABORATORY OF CATALYSIS AND MATERIALS

(UCLM)

Development of new materials

BUSINESS

Innovation and support

FROM INNOVATIONTO MARKET IMPLEMENTATION

LABORATORY OF CATALYSIS AND MATERIALS

wwwitquimaes

LABORATORY CATALYSIS AND MATERIALS Institute of Chemical and Environmental

Technologies (ITQUIMA)

University of castilla la Mancha

Avenida Camilo Joseacute Cela sn

13004 Ciudad Real

Tel +34 902 204100 (ext96322)

Responsible for laboratory

M Luz Sanchez Silva Tel +34 926 295 3000|Ext 6307

mariaLuzsanchezuclmes

Page 4: LABORATORY OF CATALYSIS AND MATERIALS - Blog UCLM...Mezclado y Agitación (1min) Liofilización - Tiempo de congelación:6h. - Presión de vacío: 0,08 mbar. - Temperatura de bandeja:

4

ITQUIMA UCLM

SERVICES AND TECHNICAL ADVISORY

Physical-chemical tests

bull Turbidity index (TSI)

bull Scanning electron

microscopy (SEM)

bull Fourier transform infrared

spectroscopy (FTIR)

bull Volume and density of

powders foams and bulk

solids

bull Pore size and pore

distribution (Hg porosimetry

and BET)

bull Abrasion test of materials

bull Surface tension

bull Sound absorption analysis

Mechanical tests and Rheology

bull Dynamic mechanical analysis

(DMA)

bull Tensile flexural and compression

bull Shore D hardness

bull Rheology of liquids and

suspensions

bull Curing of adhesives and resins

LABORATORY OF CATALYSIS AND MATERIALS

5

ITQUIMA UCLM

Thermogravimetric and thermal

analysis

bull Differential scanning calorimetry

(DSC)

bull TGA-MS at atmospheric and high

pressure

bull Thermal conductivity of materials

bull Flash pyrolyzer coupled to GC-MS

Sample preparation

bull Extruder

bull Injection moulding

bull Sample cutting press

bull Powder and conductive samples for

SEM analysis

bull Centrifugation orbital mixing and

grinding

bull Solid V-Mixer

LABORATORY OF CATALYSIS AND MATERIALS

6

Catalysis and Electrocatalysis

bull Synthesis of catalysts at lab and bench scale

bull Spin-coater and electrode preparation robot

bull Physical-chemical characterization of

catalysts (BET TPD TPR TPO acidity

chemisorption oxidation by pulses

titrations etc)

bull Electrochemical characterization of

electrocatalysts (rotary disc ECSA analysis

Tafel curves etc)

bull Different catalytic and electrocatalytic

configurations analysis of effluents (GC

microGC and HPLC)

ITQUIMA UCLM

PROCESSES AND PRODUCTS

FROM THE LAB TO THE INDUSTRIAL DEPLOYMENT

LABORATORY OF CATALYSIS AND MATERIALS

7

ITQUIMA UCLM

A SINGLE CENTER FOR ALL THE

TECHNOLOGICAL SERVICES

(SINGLE POINT LAB)

LABORATORY OF CATALYSIS AND MATERIALS

(UCLM)

Development of new materials

BUSINESS

Innovation and support

FROM INNOVATIONTO MARKET IMPLEMENTATION

LABORATORY OF CATALYSIS AND MATERIALS

wwwitquimaes

LABORATORY CATALYSIS AND MATERIALS Institute of Chemical and Environmental

Technologies (ITQUIMA)

University of castilla la Mancha

Avenida Camilo Joseacute Cela sn

13004 Ciudad Real

Tel +34 902 204100 (ext96322)

Responsible for laboratory

M Luz Sanchez Silva Tel +34 926 295 3000|Ext 6307

mariaLuzsanchezuclmes

Page 5: LABORATORY OF CATALYSIS AND MATERIALS - Blog UCLM...Mezclado y Agitación (1min) Liofilización - Tiempo de congelación:6h. - Presión de vacío: 0,08 mbar. - Temperatura de bandeja:

5

ITQUIMA UCLM

Thermogravimetric and thermal

analysis

bull Differential scanning calorimetry

(DSC)

bull TGA-MS at atmospheric and high

pressure

bull Thermal conductivity of materials

bull Flash pyrolyzer coupled to GC-MS

Sample preparation

bull Extruder

bull Injection moulding

bull Sample cutting press

bull Powder and conductive samples for

SEM analysis

bull Centrifugation orbital mixing and

grinding

bull Solid V-Mixer

LABORATORY OF CATALYSIS AND MATERIALS

6

Catalysis and Electrocatalysis

bull Synthesis of catalysts at lab and bench scale

bull Spin-coater and electrode preparation robot

bull Physical-chemical characterization of

catalysts (BET TPD TPR TPO acidity

chemisorption oxidation by pulses

titrations etc)

bull Electrochemical characterization of

electrocatalysts (rotary disc ECSA analysis

Tafel curves etc)

bull Different catalytic and electrocatalytic

configurations analysis of effluents (GC

microGC and HPLC)

ITQUIMA UCLM

PROCESSES AND PRODUCTS

FROM THE LAB TO THE INDUSTRIAL DEPLOYMENT

LABORATORY OF CATALYSIS AND MATERIALS

7

ITQUIMA UCLM

A SINGLE CENTER FOR ALL THE

TECHNOLOGICAL SERVICES

(SINGLE POINT LAB)

LABORATORY OF CATALYSIS AND MATERIALS

(UCLM)

Development of new materials

BUSINESS

Innovation and support

FROM INNOVATIONTO MARKET IMPLEMENTATION

LABORATORY OF CATALYSIS AND MATERIALS

wwwitquimaes

LABORATORY CATALYSIS AND MATERIALS Institute of Chemical and Environmental

Technologies (ITQUIMA)

University of castilla la Mancha

Avenida Camilo Joseacute Cela sn

13004 Ciudad Real

Tel +34 902 204100 (ext96322)

Responsible for laboratory

M Luz Sanchez Silva Tel +34 926 295 3000|Ext 6307

mariaLuzsanchezuclmes

Page 6: LABORATORY OF CATALYSIS AND MATERIALS - Blog UCLM...Mezclado y Agitación (1min) Liofilización - Tiempo de congelación:6h. - Presión de vacío: 0,08 mbar. - Temperatura de bandeja:

6

Catalysis and Electrocatalysis

bull Synthesis of catalysts at lab and bench scale

bull Spin-coater and electrode preparation robot

bull Physical-chemical characterization of

catalysts (BET TPD TPR TPO acidity

chemisorption oxidation by pulses

titrations etc)

bull Electrochemical characterization of

electrocatalysts (rotary disc ECSA analysis

Tafel curves etc)

bull Different catalytic and electrocatalytic

configurations analysis of effluents (GC

microGC and HPLC)

ITQUIMA UCLM

PROCESSES AND PRODUCTS

FROM THE LAB TO THE INDUSTRIAL DEPLOYMENT

LABORATORY OF CATALYSIS AND MATERIALS

7

ITQUIMA UCLM

A SINGLE CENTER FOR ALL THE

TECHNOLOGICAL SERVICES

(SINGLE POINT LAB)

LABORATORY OF CATALYSIS AND MATERIALS

(UCLM)

Development of new materials

BUSINESS

Innovation and support

FROM INNOVATIONTO MARKET IMPLEMENTATION

LABORATORY OF CATALYSIS AND MATERIALS

wwwitquimaes

LABORATORY CATALYSIS AND MATERIALS Institute of Chemical and Environmental

Technologies (ITQUIMA)

University of castilla la Mancha

Avenida Camilo Joseacute Cela sn

13004 Ciudad Real

Tel +34 902 204100 (ext96322)

Responsible for laboratory

M Luz Sanchez Silva Tel +34 926 295 3000|Ext 6307

mariaLuzsanchezuclmes

Page 7: LABORATORY OF CATALYSIS AND MATERIALS - Blog UCLM...Mezclado y Agitación (1min) Liofilización - Tiempo de congelación:6h. - Presión de vacío: 0,08 mbar. - Temperatura de bandeja:

7

ITQUIMA UCLM

A SINGLE CENTER FOR ALL THE

TECHNOLOGICAL SERVICES

(SINGLE POINT LAB)

LABORATORY OF CATALYSIS AND MATERIALS

(UCLM)

Development of new materials

BUSINESS

Innovation and support

FROM INNOVATIONTO MARKET IMPLEMENTATION

LABORATORY OF CATALYSIS AND MATERIALS

wwwitquimaes

LABORATORY CATALYSIS AND MATERIALS Institute of Chemical and Environmental

Technologies (ITQUIMA)

University of castilla la Mancha

Avenida Camilo Joseacute Cela sn

13004 Ciudad Real

Tel +34 902 204100 (ext96322)

Responsible for laboratory

M Luz Sanchez Silva Tel +34 926 295 3000|Ext 6307

mariaLuzsanchezuclmes

Page 8: LABORATORY OF CATALYSIS AND MATERIALS - Blog UCLM...Mezclado y Agitación (1min) Liofilización - Tiempo de congelación:6h. - Presión de vacío: 0,08 mbar. - Temperatura de bandeja:

wwwitquimaes

LABORATORY CATALYSIS AND MATERIALS Institute of Chemical and Environmental

Technologies (ITQUIMA)

University of castilla la Mancha

Avenida Camilo Joseacute Cela sn

13004 Ciudad Real

Tel +34 902 204100 (ext96322)

Responsible for laboratory

M Luz Sanchez Silva Tel +34 926 295 3000|Ext 6307

mariaLuzsanchezuclmes