72
TestAmerTca HE ..AD:r \ ENV. r’rA ANALYTICAL REPORT Job Number: 680-63734-1 Job Description: Hattiesburg Carbon Filter MWO8 12/2/10 For: Ashland Inc. 500 Hercules Road Wilmington, DE 19894 Attention: Timothy Hassett Approved for release. 1 (A-LL. 24 r I 12117/2010 44B PM Lidya Gulizia Project Manager I [email protected] 12/17/2010 cc: Caleb Dana Mr. Charlie Jordan Mr. Chris Waters The test results in this report meet NELAP requirements for parameters for which accreditation is required or available. [ Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the person who signed this report. L Savannah Certifications and ID #s: A2LA: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT: PHOI6I; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KYUST; LA DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GAOO6; Ml: 9925; MS; NFESC: 249; NV: GA00006; L NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LA000244; SC: 98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV DHHR: 9950 C; WI DNR: 999819810; WYJEPAR8: 8TMS-Q TestAmerica Laboratories, Inc. TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404 Tel (912) 354-7858 Fax (912) 352-0165 w.testarneicainccoin thheladc Page 1 of 20

Job Number: 680-63734-1 ANALYTICAL REPORT For: 500

  • Upload
    others

  • View
    3

  • Download
    0

Embed Size (px)

Citation preview

TestAmerTcaHE ..AD:r \ ENV. r’rA

ANALYTICAL REPORT

Job Number: 680-63734-1

Job Description: Hattiesburg Carbon Filter MWO8 12/2/10

For:Ashland Inc.

500 Hercules Road

Wilmington, DE 19894

Attention: Timothy Hassett

Approved for release.

1 (A-LL. 24 r I

12117/2010 44B PM

Lidya GuliziaProject Manager I

[email protected]

12/17/2010

cc: Caleb DanaMr. Charlie JordanMr. Chris Waters

The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.

[ Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report

may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the

person who signed this report.

L Savannah Certifications and ID #s: A2LA: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT:

PHOI6I; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KYUST; LA

DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GAOO6; Ml: 9925; MS; NFESC: 249; NV: GA00006;

LNJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LA000244; SC:

98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV

DHHR: 9950 C; WI DNR: 999819810; WYJEPAR8: 8TMS-Q

TestAmerica Laboratories, Inc.

TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404

Tel (912) 354-7858 Fax (912) 352-0165 w.testarneicainccoin thheladcPage 1 of 20

Job Narrative68043734-1

ReceiptAll samples were received in good condition within temperature requirements.

J MetalsNo analytical or quality issues were noted.

General Chemistry

j No analytical or quality issues were noted.

CommentsNo additional comments.

2zJ

LiLi

0LiLi

METHOD SUMMARY

TALSAV SW8466010B

TAL SAV SW846 3050B

TAL SAV SW846 7471A

TAL SAV SW846 7471A

pH

TAL SAV

TAL SAV

TAL SAV

TAL SAV

TAL SAV

TAL SAV

SW846 6010B

SW846 7471A

SW846 1010

SW846 9045C

SW846 3050B

SW846 7471A

b Client: Ashland Inc.Job Number: 680-63734-1

] Description Lab Location Method Preparation Method

Matrix Solid

1 Metals (ICP)

j Preparation, Metals

Mercury (CVAA)

1 Preparation, Mercury

- Matrix Waste

Metals (ICP)

J Preparation, Metals

Mercury (CVA)

Preparation, Mercury

] Ignitability, Pensky-Martens Closed-Cup Method

Lab References:

TAL SAV = TestAmerica Savannah

Method References:

SW846 = “Test Methods For Evaluating Solid Waste, Physical/Chemical Methods”, Third Edition, November 1986 And Its

Updates.

ii

I0UElElEl

o[1o TestAmerica Savannah Page 3 of 20

METHOD I ANALYST SUMMARY

Client: Ashland Inc.Job Number: 680-63734-1

Method Analyst Analyst ID

SW846 6010B Bland, Brian BCB

SW846 7471A Vasquez, Juana JV

SW846 1010 Jackson, Michelle S MSJ

SW846 9045C Robinson, Tiffany TR

TestAmerica Savannah

Page 4 of 20

SAMPLE SUMMARY

Client: Ashland Inc. Job Number: 680-63734-1

DatelTime DatelTime

Lab Sample ID Client Sample ID Client Matrix Sampled Received

680-63734-1 ASH-MWO8-CF-1 2022010 Solid 12/02/2010 1420 12/04/2010 1023

680-63734-2 ASF-l-MWO8-CF-12022010 Waste 12/02/2010 1435 12/04/2010 1023

TestAmerica Savannah Page 5 of 20

1oI

]

]SAMPLE RESULTS

Ii

LiI]

000 TestAmerica Savannah

Page 6 of 20

Analytical Data

Client: Ashland Inc. Job Number: 680-63734-1

Client Sample ID: ASI-f-MWO8-CF-12022010

Lab Sample ID: 680-63734-1 Date Sampled: 12/02/2010 1420

Client Matnx: Solid Date Received: 12/04/2010 1023

60108 Metals (ICP)

Method: 6010B Analysis Batch: 680-188613 Instrument ID: ICPD

Preparation: 3050B Prep Batch: 680-188073 Lab File ID: 120910104750.chr

Dilution: 1.0 Initial WeightNolume: 1.09 g

Date Analyzed: 12/10/2010 1047 Final WeighlfVolume: 100 mL

Date Prepared: 12/06/2010 1457

Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL

Arsenic 34 1.8

Barium 40 0.92

Cadmium <0.46 0.46

Lead 1.9 0.92

Selenium <2.3 2.3

Silver <0.92 0.92

Method: 6010B Analysis Batch: 680-189108 Instrument ID: ICPD

Preparation: 3050B Prep Batch: 680-188734 Lab File ID: 12141015195.chr

J Dilution: 1.0 Initial WeightNolume: 1.08 g

Date Analyzed: 12115/2010 0738 Final Weight/Volume: 100 mL

Date Prepared: 12/13/2010 1003

Analyte DryVVt Corrected: N Result (mg/Kg) Qualifier RL

Chromium 4.0 0.93

7471A Mercury (CVAA)

Method: 7471A Analysis Batch: 680-189039 Instrument ID: LEEMAN1

Preparation: 7471A Prep Batch: 680-188335 Lab File ID: b121410a.chr

Dilution: 1.0 Initial WeightNolume: 0.51 g

Date Analyzed: 12/14/2010 1534 Final Weight/Volume: 50 mL

Date Prepared: 12/08/2010 1405

Analyte - DryWt Corrected: N Result (mg/Kg) Qualifier RL

Mercury - <0.020 0.020

TestAmerica Savannah Page 7 of 20

Analytical Data

Client: Ashland Inc.Job Number: 680-63734-1

Client Sample ID: ASH-MWO8-CF-1 2022010

Lab Sample ID: 680-63734-2Date Sampled: 12/02/2010 1435

Client Matrix: WasteDate Received: 12/04/2010 1023

6010B Metals (ICP)

Method: 601DB Analysis Batch: 680-188613 Instrument ID: ICPD

j Preparation: 305DB Prep Batch: 680-188402 Lab File ID: 120910104750.chr

Dilution: 1.0Initial WeightNolume: 1.01 g

Date Analyzed: 12/10/2010 1117 Final WeightNolume: 100 mL

Date Prepared: 12/09/2010 0841

Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL

Arsenic <2.0 2.0

Barium <0.99 0.99

Cadmium <0.50 0.50

Chromium <0.99 0.99

Lead <0.99 0.99

Selenium<2.5 2.5

J Silver <0.99 0.99

7471A Mercury (CVAA)

Method: 7471A Analysis Batch: 680-189039 Instrument ID: LEEMAN1

Preparation: 7471A Prep Batch: 680-188335 Lab File ID: b121410a.chr

Dilution: 1.0Initial WeightNolume: 0.52 g

Date Analyzed: 12/14/2010 1537 Final WeightNolume: 50 mL

Date Prepared: 12/08/2010 1405

Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL

Mercury <0.019 0.019

TestAmerica Savannah Page 8 of 20

Analytical Data

Client: Ashland Inc.Job Number: 680-63734-1

General Chemistry

Client Sample ID: ASH-MW08-CF-1 2022010

Lab Sample ID: 680-63734-2Date Sampled: 12/0212010 1435

Client Matrix: WasteDate Received: 12104/2010 1023

Analyte Result Qual Units Dil Method

j Flashpoint >140 Degrees F 1.0 1010

Analysis Batch: 680-1 89278 Date Analyzed: 12/16/2010 1230 DryWt Corrected: N

pH 7.49 SU 1.0 9045C

Analysis Batch: 680-1 881 08 Date Analyzed: 12/06/2010 1649 DryWt Corrected: N

]

PI

ULiLiLiiLiLi0Li

TestAmerica Savannah Page 9 of 20

] QUALITY CONTROL RESULTS

]

LiElULi

00LI TestAmerica Savannah

Page 10 of 20

Quality Control Results

Client: Ashland Inc.

QC Association SummaryReport

Job Number: 680-63734-1

Prep Batch: 680-188073

LCS 680-188073110-A

MB 680-1 8807319-A

680-63734-1

Prep Batch: 680-188335

j MB 680-188335/1-A

LCS 680-188335/2-A

680-63734-1

680-63734-2

Prep Batch: 680-188402

LCS 680-1 88402/7-A

MB 680-1 8840216-A

680-63734-2

Lab Control Sample

Method BlankASH-MWO8-CF-1 2022010

T Waste

T Waste

T Waste

3050B305DB305DB

pAnalysis Batch:680-188613

LCS 680-188073/10-A

MB 680-188073/9-A

LCS 680-1 88402/7-A

MB 680-18840216-A

680-63734-1

Li 680-63734-2

[JPrep Batch: 680-188734

LCS 680-1 88734/24-A

MB 680-188734/23-A

680-63734-1

Analysis Batch:680-1 89039

MB 680-188335/1-A

LCS 680-188335/2-A

680-63734-1

680-63734-2

Method BlankLab Control Sample

ASH-MWO8-CF-1 2022010

ASH-MW08-CF-1 2022010

T Solid

T Waste

T Solid

T Waste

7471A7471A7471A7471A

680-188335

680-188335

680-188335

680-188335

Analysis Batch:680-189108

n LCS 680-188734/24-A

MB 680-188734/23-A

680-63734-1

Report Basis

T = Total

TestAmenca Savannah

Metals

Lab Samole ID Client Sample ID Basis Client Matrix Method Prep Batch

Lab Control Sample T Solid 3050B

Method Blank T Solid 30508

ASH-MWO8-CF-1 2022010 T Solid 305DB

Method Blank T Solid 7471A

Lab Control Sample T Waste 7471A

ASH-MWO8-CF-1 2022010 T Solid 7471A

ASH-MWO8-CF-1 2022010 T Waste 7471A

Lab Control Sample T Solid 6010B 680-188073

Method Blank T Solid 6010B 680-1 88073

Lab Control Sample T Waste 601DB 680-188402

Method Blank T Waste 6010B 680-1 88402

ASH-MWO8-CF-12022010 T Solid 6010B 680-188073

ASH-MWD8-CF-12022010 T Waste 601DB 680-188402

Lab Control Sample T Solid 305DB

Method Blank T Solid 305DB

ASH-MWO8-CF-1 2022010 T Solid 305DB

Lab Control Sample T Solid 6010B 680-188734

Method Blank T Solid 6010B 680-188734

ASH-MWO8-CF-12022010 T Solid 60108 680-188734

Page 11 of 20

Quality Control Results

Client: Ashland Inc.Job Number: 680-63734-1

QC Association SummaryReport

Lab Sample ID Client Sample ID Basis Client Matrix Method Prep Batch

General Chemistry

Analysis Batch:680-188108

LCS 680-188108/1 Lab Control Sample T Waste 9045C

680-63734-2 ASH-MWO8-CF-12022010 T Waste 9045C

680-63734-2DU Duplicate T Waste 9045C

Analysis Batch:680-1 89278

J LCS 680-18927812 Lab Control Sample T Waste 1010

MB 680-189278/1 Method Blank T Waste 1010

680-63734-2 ASH-MWO8-CF-12022010 T Waste 1010

680-63734-2DU Duplicate T Waste 1010

Report Basis

T = Total

TestAmerica Savannah

Page 12 of 20

Quality Control Results

Client: Ashland Inc.

Method Blank - Batch: 680-188073

Job Number: 680-63734-1

Method: 601DB

Preparation: 3050B

Lab Sample ID: MB 680-188073/9-A

J Client Matrix: Solid

Dilution: 1.0

Date Analyzed: 12/10/2010 0941

Date Prepared: 12/06/2010 1457

Analysis Batch: 680-188613

Prep Batch: 680-188073

Units: mg/Kg

Instrument ID: ICPD

Lab File ID: 12091 0104750.chr

Initial WeightNolume: 1.00 g

Final WeightNolume: 100 mL

Method: 6010B

Preparation: 305DB

Lab Sample ID: LCS 680-188073(10-A

Client Matrix: Solid

Dilution: 1.0

Date Analyzed: 12/10/2010 0946

Date Prepared: 12/06/2010 1457

Analysis Batch: 680-188613

Prep Batch: 680-188073

Units: mg/Kg

Instrument ID: ICPD

Lab File ID: 12091 01 04750.chr

Initial WeightNolume: 1.00 g

Final WeightlVolume: 100 mL

Analyte Spike Amount Result % Rec. Limit Qual

Arsenic 200 215 108 75-125

Barium 200 207 103 75-125

Cadmium 5.00 5.51 110 75- 125

Lead 50.0 54.5 109 75-125

Selenium 200 216 108 75-125

Silver 5.00 5.38 108 75- 125

QualAnalyte Result

J Arsenic <2.0

Barium <1.0

Cadmium <0.50

Lead<1.0

Selenium <2.5

Silver <1.0

Lab Control Sample - Batch: 680-188073

RL

2.01.00.501.02.51.0

TestAmerica Savannah Page 13 of 20

Quallty Control Results

Client: Ashland Inc.Job Number: 680-63734-1

Method Blank - Batch: 680-188402Method: 6010B

Preparation: 3050B

Lab Sample ID: MB 680-188402/6-A Analysis Batch: 680-188613 Instrument ID: ICPD

Client Matrix: Waste Prep Batch: 680-188402 Lab File ID: 120910104750.chr

Dilution: 1.0 Units: mg/Kg Initial WeightNolume: 1.00 g

Date Analyzed: 12/10/2010 1106Final Weight)Volume: 100 mL

Date Prepared: 12109/2010 0841

AnalyteResult Qual RL

Arsenic<2.0 -

2.0

Barium<1.0

1.0

Cadmium <0.500.50

Chromium<1.0

1.0

Lead<1.0

1.0

Selenium <2.52.5

Silver<1.0

1.0

Lab Control Sample - Batch: 680-188402 Method: 6010B

Preparation: 3050B

Lab Sample ID: LCS 680-188402/7-A Analysis Batch: 680-188613 Instrument ID: ICPD

Client Matrix: Waste Prep Batch: 680-188402 Lab File ID: 120910104750.chr

[ Dilution: 1.0 Units: mg/Kg Initial WeightNolume: 1.00 g

Li Date Analyzed: 12/10/2010 1111 Final Weight/Volume: 100 mL

Date Prepared: 12/09/2010 0841

Analyte Spike Amount Result % Rec. Limit Qual

UArsenic 200 219 110 75-125

Barium 200 214 107 75-125

Cadmium 5.00 5.81 116 75- 125

Chromium 20.0 22.5 113 75- 125

O Lead 50.0 55.9 112 75-125

Selenium 200 221 111 75-125

Silver 5.00 5.44 109 75- 125

TestAmerica SavannahPage 14 of 20

Quality Control Results

Chent: Ashland Inc.Job Number: 680-63734-1

Method Blank - Batch: 680-188734 Method: 60108

Preparation: 3050B

Lab Sample ID: MB 680-188734/23-A Analysis Batch: 680-189108 Instrument 1D: ICPD

Client Matrix: Solid Prep Batch: 680-188734 Lab File ID: 12141015195.chr

Dilution: 1.0 Units: mg/Kg Initial WeightNolume: 1.00 g

Date Analyzed: 12/15/2010 0516 Final WeightNolume: 100 mL

Date Prepared: 12)13/2010 1003

Analyte Result Qual RL

Arsenic <2.0 2.0

Barium <1.0 1.0

Cadmium <0.50 0.50

Chromium <1.0 1.0

Lead <1.0 1.0

Selenium <2.5 2.5

Silver <1.0 1.0

Lab Control Sample - Batch: 680-188734 Method: 6010BPreparation: 3050B

Lab Sample ID: LCS 680-188734/24-A Analysis Batch: 680-189108 Instrument ID: ICPD

Client Matrix: Solid Prep Batch: 680-188734 Lab File ID: 12141015195.chr

Dilution: 1.0 Units: mg/Kg Initial WeightNolume: 1.00 g

Date Analyzed: 12)15/2010 0521 Final WeightNolume: 100 mL

Date Prepared: 12/13/2010 1003

Analyte Spike Amount Result % Rec. Limit Qual

Arsenic 200 205 102 75-125

Barium 200 207 103 75-125

Cadmium 5.00 5.09 102 75- 125

Chromium 20.0 21.2 106 75- 125

flLead 50.0 52.3 105 75-125

Selenium 200 204 102 75 - 125

Silver 5.00 5.19 104 75- 125

TestAmerica Savannah Page 15 of 20

Quality Control Results

Client: Ashland Inc.

Method Blank - Batch: 680-188335

Job Number: 680-63734-1

Method: 7471A

Preparation: 7471A

Lab Sample ID: MB 680-188335/1-A

j Client Matrix: Solid

Dilution: 1.0

Date Analyzed: 12/1412010 1348

Date Prepared: 1210812010 1405

Analysis Batch: 680-189039

Prep Batch: 680-188335

Units: mg/Kg

Instrument ID: LEEMAN1

Lab File ID: b121410a.chr

Initial Weight/Volume: 0.50 g

Final WeightNolume: 50 mL

Result Qual RL

Mercury <0.020 0.020Analyte

TestAmerica Savannah Page 16 of 20

Quality Control Results

Client: Ashland Inc.Job Number: 680-63734-1

Method Blank - Batch: 680-189278 Method: 1010Preparation: N!A

Lab Sample ID: MB 680-189278/1 Analysis Batch: 680-189278 Instrument ID: No Equipment Assigned

j Client Matrix: Waste Prep Batch: N/A Lab File ID: N/A

Dilution: 1.0 Units: Degrees F Initial WeightNolume:

Date Analyzed: 12116/2010 1230 Final WeightNolume: 1.0 mL

Date Prepared: N/A

AnaMeResult Qual NONE

J Flashpoint >140

Lab Control Sample - Batch: 680-189278 Method: 1010Preparation: NIA

Lab Sample ID: LCS 680-189278/2 Analysis Batch: 680-189278 Instrument ID: No Equipment Assigned

J Client Matrix: Waste Prep Batch: N/A Lab File ID: N/A

Dilution: 1.0 Units: Degrees F Initial WeightNolume:

Date Analyzed: 12/16/2010 1230 Final WeightiVolume: 1.0 mL

Date Prepared: N/A

Analyte Spike Amount Result % Rec. Limit Qual

Flashpoint 80.0 80.0 100 97.53- 102.47

Duplicate - Batch: 680-189278 Method: 1010Preparation: N/A

ULab Sample ID: 680-63734-2 Analysis Batch: 680-189278 Instrument ID: No Equipment Assigned

Client Matrix: Waste Prep Batch: N/A Lab File ID: N/A

Dilution: 1.0 Units: Degrees F Initial WeightNolume:

Date Analyzed: 12/16/2010 1230 Final Weight/Volume: 1.0 mL

Date Prepared: N/A

UAnalyte Sample ResultlQual Result RPD Limit Qual

Flashpoint >140 >140 NC

TestAmerica Savannah Page 17 of 20

Quality Control Results

Lab Control Sample - Batch: 680-188108 Method: 9045C

Preparation: NIA

Lab Sample ID:

Client Matrix:

Dilution:

Date Analyzed:

Date Prepared:

LCS 680-188108/1

Waste

1.012/0612010 1649

N/A

Analysis Batch: 680-188108

Prep Batch: N/A

Units: SU

Instrument ID: No Equipment Assigned

Lab File ID: N/A

Initial Weight/Volume: 20 mL

Final Weight/Volume: 20 mL

Analyte Spike Amount Result % Rec. Limit Qual

pH 7.00 6.970 100 63-158

Duplicate - Batch: 680-188108 Method: 9045C

Preparation: NIA

1 Lab Sample ID: 680-63734-2

j Client Matrix: Waste

Dilution: 1.0

Date Analyzed: 1210612010 1649

Date Prepared: N/A

Analysis Batch: 680-188108

Prep Batch: N/A

Units: SU

Instrument ID: No Equipment Assigned

Lab File ID: N/A

Initial WeightNolume: 20 mL

Final Weight/Volume: 20 mL

Analyte Sample ResultlQual Result RPD Limit Qual

pH 7.49 7.520 0.4 40

Client: Ashland Inc.Job Number: 680-63734-1

TestAmerica Savannah Page 18 of 20

EE

lL

EJçjZ

JL

E]

LE

E]

L_

Ji

LZ

JL

..

LJ

_J

L.J

C_-J

L.

LJ

J&

L_J

Serial

Num

ber

•M

ob

ile

ww

w.t

est

am

eri

cain

c.c

om

Tes

tirn

eric

ac31

900

Lak

esi

de

Dri

ve

Ph

on

e:

(251)

666-6

633

IVio

bile

Mobil

e,A

L36693

Fax

:(2

51)

66

6-6

69

6

TH

EL

EA

DE

RIN

EN

ViR

ON

ME

NT

AL

TE

ST

ING

Alt

ern

ate

Lab

ora

tory

Nar

rie/

Loca

tion:

0P

hone:

TA

L-8

240(

1007

)A

NA

LY

SIS

RE

QU

ES

TA

ND

CH

AIN

OF

CU

ST

OD

YR

EC

OR

DF

ax:

‘RO

JEC

TR

EF

ER

EN

CE

PR

OJE

CT

NO

PR

OJE

CT

LO

CA

TIO

NM

ATR

IX—

PAG

EO

F

(ST

AT

E)

fr-

TY

PE-

—R

EQ

UIR

ED

AN

AL

YSE

S—

LA

B)

PR

OJE

CT

MA

NA

GE

RP.

0.

NU

MB

ER

CO

NT

RA

CT

NO

.ST

AN

DA

RD

RE

PO

RT

1—’J

-C-.1

.A..

DE

LIV

ER

Y

CL

IEN

T(S

FT

E)P

CL

IEN

TP

HO

NE

CL

IEN

TFA

X--.

DA

TF

DU

E

.(1

7I

21

>\

Iyv’

flW

Ifr

•?I

•f•C

W)tJ

JE

XPE

DIT

ED

RE

PO

RT

CL

IEN

TN

AM

EC

LIE

NT

EMA

IL.

.‘j-

DE

LIV

ER

Y

jj

oC

LIE

NT

AD

DR

ESS

a:L

K,-i

4:-

-w

—T

——

—N

UM

SE

RO

FC

OO

LE

FIS

CO

MPA

NY

CO

NT

RA

CT

ING

TH

ISW

OR

KS

AM

PL

ER

rtT

US

UB

Mrr

rED

PE

RSH

IPM

EN

T:

(Ifc

aM

aj SA

MPL

ESA

MPL

EID

EN

TIF

ICA

TIO

NN

UM

BE

RO

FC

ON

TA

INE

RS

SUB

MIT

TE

DR

EM

AR

KS

DA

TETI

ME

Ocn

<z

2’2-2

)424

?A

---i

-i7

øL

Z1oi

--

-J

ii.€

fk

i4i)

Z--

j43

A$4-tg

—flZ

zz

--

Ij

J_—

—lf

r);

RE

LIN

QU

ISH

ED

BY:

(SIG

NA

TU

RE

)D

AT

ET

IME

RE

LIN

UTSI

-)BY

:(S

IGU

RE

)D

AT

ET

IME

RE

LIN

QU

ISH

Y:(S

RE

)D

AT

ET

IME

—_

__

__

__

__

__

__

__

)Z

z?

1f4

kR

EC

EIV

ED

BY:

(SIG

NA

TU

RE

)D

AT

ET

IME

RE

CE

IVE

DB

Y:

(SIG

NA

TU

RE

)D

AT

ET

IME

RE

CE

JED

BI1

NA

TU

RE

)D

AT

ET

IME

.1

?4

I3

._____

:•

:,U

Oo

yS

dN

Lv

(‘&

-tiI

f1E

OE

JVE

DFO

BL

A&

RA

TO

RY

BYlA

TTI

ME

0US

rbO

YN

TA

CT

C1J

1OD

VLO

GN

O.7

1AB

QR

AtO

FWR

EM

1<S

IIp

Nd-1

DI to ID 0 0

JJ

Ori

gin

al-

Ret

urn

toL

abora

tory

wit

hS

ample

(s)

Login Sample Receipt Check List

Client: Ashland Inc.Job Number: 680-63734-1

Login Number: 63734List Source: TestAmerica Savannah

Creator: Daughtry, Beth

List Number: I

QuestionTI Ft NA Comment

Radioactivity either was not measured or, if measured, is at or below N/A

backgroundThe cooleis custody seal, if present, is intact. True

The cooler or samples do not appear to have been compromised or True

tampered with.Samples were received on ice. True

Cooler Temperature is acceptable. True

J Cooler Temperature is recorded. True 0.8 C

COC is present.True

COC is filled out in ink and legible. True

COC is filled out with all pertinent information. True

Is the Field Samplers name present on COG? True

There are no discrepancies between the sample lDs on the containers and True

the COG.

J Samples are received within Holding Time. True

Sample containers have legible labels. True

‘Containers are not broken or leaking. True

Sample collection date/times are provided. True

Appropriate sample containers are used. True

Sample bottles are completely filled. True

Sample Preservation Verified N/A

There is sufficient vol. for all requested analyses, mci. any requested True

MS/MSD5

fl VOA sample vials do not have headspace or bubble is <6mm (114”) in N/A

U diameter.If necessary, staff have been informed of any short hold time or quick TAT True

needs

U Multiphasic samples are not present. N/A

Samples do not require splitting or compositing. N/A

TestAmerica Savannah Page 20 of 20

ZJ

EL

LL

-—

Ua

0

BO

NN

ER

AN

AL

.Y11

CA

LT

EST

ING

(OM

PA

NY

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

SU

RA

NC

ED

ATA

DIO

XA

ThIO

N! D

IOX

ENET

I-II

ON

1-IP

ICA

NA

.YSI

SD

ATA

Clie

ntA

shla

ndC

hem

ical

Col

lect

ed:

1210

3/20

1009

55C

lIent

Sam

ple

Type

:W

ater

Sam

ple

ID:

ASH

-MW

I7-1

2032

010

Ext

ract

ed:

1210

6/20

1013

00V

CT

Ext

ract

ion

Met

hod:

SW84

635

10C

Flle

#:10

1204

7-01

Ana

lyze

d:12

1131

2010

2041

DG

AA

naly

sisM

etho

d;M

odif

iedS

W84

6

Dat

eA

naly

st

SAM

PLE

M’T

HO

DBU

AN

KLa

bC

ontro

lM

ATR

IXSP

IKE

Det

ecte

dS)

4Ke

Det

ecte

d—

pike

Det

ecte

dSp

ike

Det

ecte

d

POL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugIL

ugfl

Am

ount

%ug

hA

mou

n%

ugim

LA

mou

nt%

uglm

LA

mou

nt%

(ppb

)(p

pb)

ugIL

Rec

over

y(p

pb)

ugIL

Rec

over

y(p

pm)

ugIm

LR

ecov

ery

(ppm

)ug

lmL

Rec

over

y

Dio

xene

thlo

n0.

400

3045

ND

8.9

10.0

897.

110

.071

..

0.40

023

.7N

D9,

910

.099

8.8

10.0

88

Dio

xath

ron

(dc)

0.40

04.

2N

D9.

610

.098

7.9

10.0

79

Dio

xalh

ion

(han

s)

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

r’R

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

lene

*25

.110

.00

251

7.1

10.0

071

7.2

10.0

072

7.2

10.0

072

9-ug

hsu

rn,g

ate

reco

very

due

toin

terf

eren

ce

Cer

flie

dby

:M

icha

elS.

Bon

ner,

Ph.D

BO

NN

ER

AN

ALV

TIC

AL

TEST

ING

CO

MPA

NY

LL

ji

___

___

BO

NN

ER

AN

AL

YT

ICA

L.

TE

ST

ING

C)M

PAN

Y

QU

AN

TITA

ThFE

RE

SUL

TS

AN

DQ

UA

L1TV

AS

UR

AN

CE

DA

TA

DIO

XA

THIO

NI D

IOX

ENET

hIO

NH

PLC

AN

AY

SIS

DA

TA

Cli

ent

Ash

land

Che

mic

alC

olle

cted

:12

1031

2010

1005

Clie

ntS

ampl

eT

ype:

Wat

er

Sam

ple

ID:

ASH

-RS4

-120

3201

0E

xtra

cted

:12

1061

2010

1300

VC

TE

xtre

cuon

Met

hod:

SW84

635

1CC

Fil

et

1012

047-

02A

naly

zed:

1211

3120

1021

05D

GA

AP

eth

od

Mod

ifie

dSW

B46

(lat

eA

naly

st

SAM

PLE

ME

TH

OD

BLL

NK

Lab

Con

trol

MA

TRIX

SPIK

E

Det

ecte

dSp

ike

Det

ecte

dpl

keD

etec

ted

Det

ecte

d

POL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugh

ugIL

Am

ount

%ug

ILA

mou

nt%

ugim

LA

mou

nt%

ugIm

LA

mou

nt%

(ppb

)(p

pb)

ugh

Rec

over

y(p

pb)

ugIL

Rec

oven

j(p

pm)

uglm

LR

ecov

ery

(ppm

)ug

lmL

Rec

over

y

Dio

xene

thio

n0.

400

2.9

ND

8.9

10.0

897.

110

.071

.

0.40

0N

DN

D9.

910

.099

8.8

10.0

88

Dio

xath

ion

(cia

)

0.40

0N

DN

D9.

610

.096

7.9

10.0

79

Dio

xath

ion

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

lene

7.5

10.0

075

7.1

10.0

071

7.2

10.0

072

7.2

10.0

072

itif

iad

byf Mic

hael

S.B

onne

r,Ph

.DB

ON

NER

AN

ALY

11C

AL.

TES1

1NG

CO

MPA

NV

EEEJ

EL

_J

LJ

0

BO

NN

ER

AN

AL

YT

ICA

LT

ES

TiN

GL

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

St

DIO

XA

THIO

N! D

IOX

ENET

hIO

NH

PLC

AN

OM

PAN

Y;U

RA

NC

ED

ATA

LYSI

SD

ATA

C.p

rtif

ierl

hr

Clie

ntA

shla

ndC

hem

ical

Col

lect

ed:

1210

3120

1010

40C

lient

LS

ampl

eTy

pe:

Wat

er

Sam

ple

ID:

ASH

-MW

18-1

2032

010

Ext

ract

ed:

12/0

6/20

1013

00V

CT

Exa

cUon

Met

hod:

SW84

635

10C

File

#:10

1204

7-03

Anal

ed:

1211

3120

1021

28D

GA

]A

naly

sis

Met

hod:

Mod

ified

SW84

6

Dat

eA

naly

sti

SAM

PLE

MET

HO

DB

IAN

I(L

abC

ontro

lM

ATR

IXSP

IKE

Det

ecte

dD

etec

ted

—Sp

ike

Det

ecte

dSp

ike

Det

ecte

d

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugIL

ugIL

Am

ount

%Ug

ILA

mou

n%

ug/m

LA

mou

nt%

uglm

LA

mou

nt%

(ppb

)(p

pb)

ugh

Rec

over

y(p

pb)

ugh.

Rec

over

y(p

pm)

uglm

LR

ecov

ery

(ppm

)ug

/mL

Rec

over

y

Dlo

xeri

ethi

on0.

400

ND

ND

8.9

10.0

897.

110

.071

..

0.40

02.

6N

D9.

910

.099

8.8

10.0

88

Dio

xath

ion

(cis

)

0.40

05.

6N

D9.

610

.096

7.9

10.0

79

Dio

xath

ion

(tra

ris)

Det

ecte

dSp

Iked

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

SUR

RO

GA

TE

CO

MPO

UN

DS

Anl

ount

Am

ount

Rec

over

yA

mou

ntA

mou

rR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

lene

56

10.0

058

7.1

10.0

071

7.2

10.0

072

7.2

10.0

072

MIc

flae

iS

.on

ner,

1’n.

vB

ON

NE

RA

NA

LYTi

CA

LTE

STIN

GC

OM

PAN

Y

____

____

____

____

•iz

zit

L_J

L_2

BO

NN

ER

AN

AL

YT

ICA

LT

ES

TIN

GC

QU

AN

TIT

A1W

ER

ESU

LT

SA

ND

QU

ALI

TYA

SID

IOX

AT

hIO

N!

DIO

XEN

ETH

ION

HPI

CA

NA

MP

AN

YU

RA

NC

ED

ATA

YSI

SD

ATA

Cer

tifie

dby

:l.4pø’4

i.p.i

irrr

mpj.

i.ip

Cli

ent

Ash

land

Chem

ical

Col

lect

ed:

12/0

3120

1011

15C

lient

-Sa

mpl

eTy

pe:

Wat

er

Sam

ple

ID:

ASH

-MW

2O-1

2032

010

Ext

ract

ed:

12/0

6120

1013

00V

CT

[-E

xtra

ctio

nM

etho

d:SW

846

3610

C

File

1012

047-

04A

naly

zed:

1211

3/20

1021

52O

GA

j-A

naly

sis

Met

hod:

Mod

ified

SW84

6

Dat

eA

naly

stj

SAM

PLE

MET

HO

DB

LN

KL

abC

ontro

lM

ATR

IXSP

IKE

Det

ecte

dpi

keD

etec

ted

POL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugh

ugJL

Am

ount

%ug

/LA

mou

nt%

uglm

LA

mou

nt%

ug/m

LA

mou

nt%

(ppb

)(p

pb)

ug/L

Rec

over

y(p

pb)

ugh

Rec

over

y(p

pm)

ug/m

LR

ecov

ery

(ppm

)ug

/mL

Rec

over

y

Dlo

xene

thio

n0.

400

3.4

ND

8.9

10.0

897.

110

.071

..

.0.

400

0.68

ND

9.9

10.0

998.

810

_c88

Dio

xath

iori

(rs}

0.40

06.

1N

D9.

610

.096

7.9

10.0

79

Dio

xath

ion

(tra

ris)

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

rnou

nR

ecov

ejy

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

httla

lene

4.7

10.0

047

7.1

10.0

071

7.2

10.0

072

7.2

10.0

072

Mlc

flael

SB

onne

r,Ih

.0B

ON

NE

RA

NA

LYTI

CA

LTE

STIN

GC

OM

PAN

Y

c5E

Dc

LJ

__

.

0

BO

NN

ER

AN

AL

YT

ICA

LT

EST

ING

C

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

S;

DIO

XA

THIO

NID

IOX

ENET

HIO

NH

PLC

AN

A

)MPA

NY

UR

AN

CE

DA

TAY

SIS

DA

TA

Cer

tifie

dby

;-

Clie

nt:

Ash

land

Che

mic

alC

olle

cted

:12

1031

2010

1155

Clie

nt-

Sam

pleT

ype:

Wat

er

Sam

ple

ID:

ASH

-MW

21-1

2032

010

Ext

ract

ed:

1210

6120

1013

00V

CT

-E

xtra

ctio

nM

etho

d:SW

846

351D

C

FiIe

#:10

1204

7-05

Ana

lyze

d:12

113/

2010

2216

DG

AA

naly

sis

Met

hod:

Mod

ified

SW64

6

Dat

eA

naly

st

SAM

PLE

MET

HO

DB

INK

Lab

Con

trol

MA

TRIX

SPIK

E

Det

ecte

dS

pike

Det

ecte

dpi

keD

etec

ted

Det

ecte

dSp

ike

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ug/L

ugIL

Am

ount

%ug

iLA

mou

nt%

ugim

LA

mou

nt%

ugfm

LA

mou

nt%

(ppb

)(p

pb)

ug/L

Rec

over

y(p

pb)

ug/L

Rec

over

y(p

pm)

uglm

LR

ecov

ery

(ppm

)ug

/ml.

Rec

over

y

Dlo

xene

ttiio

n0.

400

10.2

ND

8.9

10.0

897.

110

.071

.

0.40

0N

DN

D9.

910

.099

8.8

10.0

88

Dro

xath

lon

(cis

)

0.40

0N

DN

D9.

810

.086

7.9

10.0

79

Dio

xath

ion

(Ira

ns)

Det

ecte

dSp

iked

%D

etec

tedii

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

nR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

lone

13.7

10.0

013

77.

110

.00

717.

210

.00

727.

210

.00

72

Mlc

nael

i.ir

onne

r,I-’

fl.LJ

BO

NN

ER

AN

ALY

TIC

AL

TEST

ING

CO

MPA

NY

c5I

-

__

_

-

SO

NN

ER

AN

ALY

TIC

AL

TE

ST

ING

C)M

PAN

YQ

UA

NTI

TATi

VE

RE

SUL

TS

AN

DQ

UA

UTY

AS

IJR

AN

CE

DA

TAD

IOX

ATH

ION

ID

IOX

ENET

HIO

NH

PLC

AN

/Y

SIS

DA

TA

Clie

ntA

sh’a

ndC

hem

Ical

Col

lect

ed:

12/0

3120

1013

00C

lient

-Sa

mpl

eT

ype

Wat

er

Sam

ple

ID;

ASH

-M1N

22-1

2032

010

Ext

ract

ed:

12/0

6/20

1013

00V

CT

-E

xtra

ctio

nM

etho

d:SW

846

3510

C

FiIe

#:10

1204

7-06

Ana

lyze

d:12

/13/

2010

2240

DG

A-

Ana

lysi

sM

etho

d:

Dat

eA

iit

SAM

PLE

MET

HO

DB

NK

Lab

Con

trol

MA

TRIX

SPIK

E

Det

ecte

dD

etec

ted

Pike

Det

ecte

dD

etec

ted

Spik

e

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ug!L

ug/L

Am

ount

%ug

ILA

mou

nt%

uglm

LA

mou

nt%

ugim

LA

mou

nt%

(ppb

)(p

pb)

ug!L

Rec

over

y(p

pb)

ugIL

Rec

over

y(p

pm)

uglm

LR

ecov

ery

(ppm

)ug

imL

Rec

over

y

Dio

xene

thio

n0.

400

8.2

ND

8.9

10.0

697.

110

.071

..

0.40

0N

DN

D9.

910

.099

8.8

10.0

88D

ioxa

thio

n(a

s)

0.40

0N

DN

D9.

610

.096

7.9

10.0

79

Dio

xath

ion

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

Spic

ed%

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

lene

10.3

10.0

010

37.

110

.00

717.

210

.00

727.

210

.00

72

ertit

led

S.B

onne

r.B

ON

NER

AN

Al.

YTI

CA

LTE

STIN

GC

OM

PAN

Y

c5E

ZL

L_J

L

__

.—

BO

NN

ER

AN

AL

YT

ICA

LT

ES

TIN

GC

OM

PA

NY

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

AU

TYA

SSU

RA

NC

ED

ATA

DIO

XA

THIO

NI

DIO

XEN

EThI

ON

HPL

CA

NA

LYSI

SD

ATA

Clie

ntA

shla

ndC

hem

ical

Col

lect

ed:

1210

3120

1012

20C

lIent

Sam

ple

Type

:W

aler

Sam

ple

ID:

ASH

-MW

23-1

2032

010

Ext

ract

ed:

1210

6120

1013

00V

CT

Ext

ract

ion

Met

hod:

SW84

635

10C

File

#:10

1204

7-07

Ana

lyze

d:12

1131

2010

2304

DG

AA

naly

sis

Met

hod:

Mod

ified

SW84

6

Dat

eA

naly

st

SAM

PLE

MET

HO

DBL

AN

KLa

bC

ontro

lM

ATR

IXSP

IKE

Det

ecte

dSp

ike

Det

ecte

dSp

ike

Det

ecte

dSp

ike

Det

ecte

dSp

ike

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

uglL

ugiL

Am

ount

%ug

hA

mou

nt%

uglm

LA

mou

nt%

ug!m

LA

mou

nt%

(ppb

)(p

pb)

ugh

Rec

over

y(p

pb)

ugh

Rec

over

y(p

pm)

uglm

LR

ecov

ery

(ppm

)ug

lmL

Rec

over

y

Dio

xene

thlo

n0.

400

ND

ND

8.9

10.0

897.

110

.071

..

.0.

400

ND

ND

9.9

10.0

998.

810

.088

Dio

xath

ion

(cia

)

0.40

0N

DN

D9,

610

.096

7.9

10.0

79

Dio

xath

ion

(ban

s)

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

lene

42.9

10.0

042

97.

110

.00

717.

210

.00

727.

210

.00

72

*HIg

hsu

rrog

ate

reco

very

Clue

toin

terf

eren

ce

1rt

ifid

byM

lcna

eI.

tionn

er.

-‘ni

)B

ON

NE

RA

NA

LYTI

CA

LT

EST

ING

CO

MPA

NY

UL

JL

..,

C)

BO

NN

ER

AN

AL

YT

ICA

LT

ES

TIN

G(O

IVIP

AN

Y

QU

AN

TITA

TiV

ER

ESU

LT

SA

ND

QU

ALI

TYA

SU

RA

NC

ED

ATA

D1O

XA

TIII

ON

/DIO

XEN

ETH

ION

HPL

CA

NA

LYSI

SD

ATA

Clie

ntA

shla

nd

Chem

ical

Col

lect

ed:

1210

3120

10C

lient

Sam

pleT

ype:

Wat

er

Sam

ple

ID:

ASR

.FD

3-12

0320

10E

xtra

cted

:12

1061

2010

1300

VC

TE

xtra

ctto

nM

etho

d:SW

B4S

aslo

c

Fiie

#:10

1204

7-08

Ana

lyze

d:12

1131

2010

2328

DG

Aj

Ana

lysi

sM

etho

d:M

odifi

edSW

846

Dat

eA

naiY

st}

SAM

PLE

MT

HO

DBI

IAN

KLa

bC

ontro

lM

4ThI

XSP

IKE

Det

ecte

dD

etec

ted

Sp1

kD

etec

ted

Spik

eD

etec

ted

POL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugh.

ugh

Am

ount

%ug

hA

mou

r%

uglm

LA

mou

nt%

uglm

LA

mou

nt%

(ppb

)(p

pb)

ugh

Rec

over

y(p

pb)

ugIL

Rec

over

y(p

pm)

uglm

LR

ecov

ery

(ppm

)ug

lmL

Rec

over

y

Olo

xene

thio

n0.

400

1.9

ND

8.9

10.0

897.

110

.071

0.40

0N

DN

D8.

910

.099

8.8

10.0

88

Dlo

xath

lon

(cis

)

0.40

08.

4N

D9.

610

.096

7.9

10.0

79

Dio

xath

ion

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

I&II

%D

etec

ied

Spik

ed%

Det

ecte

dSp

iked

%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

n(R

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

lene

5.1

10.0

051

7.1

10.0

071

7.2

10.0

072

7.2

10.0

072

Cer

tIfie

dby

:ic

haeI

S.B

onne

r,B

ON

NE

RA

NA

LYTI

CA

LTE

STiN

GC

OM

PAN

Y

E

0Y

OU

RC

OM

PA

NY

NA

ME

:

YO

UR

CO

MP

AN

YA

DD

RE

SS

:

NA

ME

OF

PE

RS

ON

TO

CO

NT

AC

T:

CO

NT

AC

TP

ER

SO

N’S

PH

ON

E:

CO

NT

AC

TP

ER

SO

N’S

EM

AIL

:

ZiZ

JzJz

.

6)

-F

AX

:

LJ

LJj

__

o

BO

NN

ERA

NA

LY

TICA

LTE

STIN

GC

OM

PAN

Y

2703

Oak

Grove

Ro

ad

,H

auie

.cbur

g,M

S3

94

02

____

____

____

_

Phone:

(601

)-264-2854

Fax

:(60

I}-26R

-7084

Em

ail:

ba1

co

ba(co

.co

m

WW

W.B

AT

CO

.CO

M

PAR

AM

ET

ER

SFO

RA

NA

LYSI

SLA

BORA

TORY

USE

CL

IEN

TP

RO

JEC

TN

O.

CL

IEN

TP

.O.#

CL

IEN

TP

RO

JEC

TN

UM

BE

R

SAM

PLE

DE

SC

RIP

TIO

ND

AT

ET

IME

MA

TR

IX

LI)

Turn

Aro

und

Tim

ea:

Ui z

,-z 0

z0

0P

rn(e

ctN

umbe

rU

.

Ui

Lii

.4)

1A f1i2/1

a:

(Z

1

AS

-4-j-

I2G

3Zcz

*)z

--2

.X

f._

—±

BT

2

A3

(4--

-i2

zIZ

$?6-

2)lØj

—BT

I3

-jzøi

--7ø

)tt

4J

—ST

‘k3-

4Z

t-Z

3zq

z-?a

1Ii

—BT

A5.1t

-H

i-JZ

j-

)lQ

iII5

.I

BT

6-

il1zz

-

-i

/1

—BT

-3z

-.

J2—

——

ST

—i---B

T

L_..

BT

10

ST

SA

MP

LE

CO

LL

EC

TO

R/R

EL

INQ

UIS

HE

DB

Y:

DA

TE

TIM

ER

EC

EIV

ED

BY

::L

INO

UIS

HE

DB

Y:

DA

TE

TIM

ER

EC

EIV

ED

BY

:

t7e

ME

ThO

DO

FS

HIP

ME

NT

(It

Any

)R

EL

INQ

UIS

HE

DB

Y:

DE

TIM

ER

EC

EIV

ED

FO

RB

AT

CO

BY

:D

ATE

/TIM

E

RE

MA

RK

S-

jR

EQ

UE

ST

BA

TC

OT

OD

ISP

OS

EO

FA

LL

SA

MP

LE

RE

MA

IND

ER

S

-

(Sig

natu

re)

RE

VIS

ION

NO

1.2

.

ISA

MPL

EIS

DE

TE

RM

INE

DT

OB

EH

AZ

AR

DO

US

,A

MIN

IMU

MA

DD

ITIO

NA

L03

1221

01

ClA

RG

EO

F$

30

.00

PE

RSA

MPL

EW

ILL

BE

AS

SE

SS

ED

.

L:J

JJ

jJj

JJ

JL

J

BO

NN

ER

AN

AL

YT

ICA

LT

EST

ING

OM

PA

NY

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

SU

RA

NC

ED

ATA

DIO

XA

THIO

NI

DIO

XEN

ETH

ION

HPL

CA

NLY

SIS

DA

TA

Clie

ntA

shla

nd

Ch

emic

alC

olle

cted

:12

1011

2010

Clie

nt-

Sam

ple

Type

:W

ater

Sam

ple

ID:

ASH

-FD

I-12

0120

10E

xtra

cted

:12

1022

010

1300

VC

T—

Ext

ract

ion

Met

hod:

SW84

635

10C

Flle

#:10

1202

4.01

Ana

lyze

d:12

1141

2010

1529

DG

A—

Ana

lysi

sMet

hod:

Mod

ified

SW84

6D

ate

An

aty

SAM

PLE

ME

TH

OD

BLA

NK

Lab

COnt

rOl

MA

TRIX

SPIK

ED

etec

ted

Splk

eD

etec

ted

Spik

eD

etec

ted

Det

ecte

dSp

ike

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugIL

ugIL

Am

ount

%ug

ILA

mou

i%

uglm

LA

mou

nt%

uglm

LA

mou

nt%

(ppb

)(p

pb)

ugIL

Rec

over

y(p

pb)

ug/L

Rec

over

y(p

pm)

ugim

LR

ecov

ery

(ppm

)ug

!mL

Rec

over

y

Dlo

xene

thio

n0.

400

15.5

ND

9.13

10.0

917.

1110

.071

..

0.40

0N

DN

D9.

4310

.094

8.07

10.0

81D

ioxa

thio

n(o

s)

0.40

0N

DN

D8.

8410

.088

8.22

10.0

82O

loxa

thio

n(t

rans

)

Det

ecte

dSp

iked

%D

etec

ted

Splk

e%

Det

ecte

dSp

iked

%D

etec

ted

Splk

ed%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

rR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

titha

lene

6.6

10.0

066

6.77

10.0

068

7.71

10.0

077

7.80

10.0

078

Cer

tifie

dby

:er

,Ph

.DB

ON

NE

RA

NA

LYTI

CA

LT

EST

ING

CO

MPA

NY

cE

JL

zJ

L

_

II

_

——

.

00

BO

NN

ER

AN

ALY

TIC

AL

TE

STIN

GO

MPA

NY

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

SU

RA

NC

ED

ATA

DIO

XA

THIO

NI

DIO

XEN

ETH

ION

HPL

CA

N.

LYSI

SD

ATA

Cli

ent

Ash

land

Ch

emic

alC

olle

cted

:12

1011

2010

1055

Clie

ntS

ampl

eT

ype:

Wat

er

Sam

ple

ID;

ASH

-MW

1O-1

2012

010

Ext

iact

ed:

1210

2120

1013

00V

CT

Extra

ctio

nM

etho

d:SW

846

3510

C

Fil

et

1012

024-

02A

naly

zed:

1211

4120

1015

53D

GA

—ly

sis

Met

hod:

Mod

ifIed

SW84

6

Dat

eA

naIy

s-

SAM

PLE

ME

TH

OD

BIA

NK

Lab

Con

trol

MA

TRIX

SPIK

E

Det

ecte

dD

etec

ted

Spik

eD

etec

ted

Spik

eD

etec

ted

POL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugIL

ugIL

Am

ount

%ug

lLA

mou

ri%

uglm

LA

mou

nt%

uglm

l.A

mou

nt%

(ppb

)(p

pb)

ugIL

Rec

over

y(p

pb)

ugh

Rec

over

y(p

pm)

ugi’m

LR

ecov

ery

(ppm

)ug

ImL

Rec

over

y

Dio

xene

thlo

n0.

400

ND

ND

9.13

10.0

9171

110

.071

..

.0.

400

ND

ND

9.43

10.0

948.

0710

.081

Dio

xeth

ion

(cia

)

0.40

0N

DN

D8.

8410

.088

6.22

10.0

62

Dio

xath

lon

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

%D

etec

ted

Splic

ed%

Det

ecte

dSp

iked

%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

xnow

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Am

ount

Am

ount

Rec

over

y

Nap

htha

lene

6.9

10.0

069

6.77

10.0

088

7.71

10.0

077

7.80

10.0

078

Cer

tifie

dby

:M

icha

elS.

Bon

ner,

Ph.D

BO

NN

ER

AN

ALY

TIC

AL

TE

STIN

GC

OM

PAN

Y

_

LI

_

00

0

BO

NN

ER

AN

AL

YT

ICA

LT

EST

ING

OM

PAN

Y

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

SU

RA

NC

ED

ATA

DIO

XA

THIO

NID

IOX

ENET

HIO

NH

PLC

Al’

.YSI

SD

ATA

Clie

ntA

shla

nd

Chem

ical

Col

lect

ed:

1210

1120

1011

50C

lIent

—Sa

mpl

eTy

pe:

Wat

er

Sam

ple

ID:

ASH

-MW

O4-

1201

2010

Ext

ract

ed:

1210

2120

1013

00V

CT

Ext

ract

ion

Met

hod:

SW84

635

1CC

FIl

et10

1202

4-03

Ana

lyze

d:12

1141

2010

1617

DG

AM

&ys

Ir,te

thod

:M

odIf

iedS

W84

6

Dat

eA

naly

s

SAM

PLE

MET

HO

DB

LAN

Kla

bC

ontro

lM

ATR

IXSP

IKE

Det

ecte

dSp

ike

Det

ecte

d—

Spik

eD

etec

ted

Det

ecte

dSp

rke

POL

Am

ount

Am

ount

Am

ount

Am

ou

nt

CO

MPO

UN

DS

uC!L

ugII

.A

mou

nt%

ugIL

Am

oun

%ug

lmL

Am

ount

%ug

ImL

Am

ount

%

(ppb

)(p

pb)

ugIL

Rec

over

y(p

pb)

ugIL

Rec

over

y(p

pm)

uglm

LR

ecov

ery

(ppm

)ug

lmL

Rec

over

y

Dio

xene

thio

n0.

400

22.2

ND

913

10.0

917.

1110

.071

.

0.40

0N

DN

D9.

4310

.094

8.07

10.0

81

Dio

xath

ion

(cis)

0.40

0N

DN

D8.

8410

.088

8.22

10.0

82

Dio

xath

ion

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

rnou

nR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

httr

alen

e8.

210

.00

626.

7710

.00

687.

7110

.00

777.

8010

.00

78

Cer

tifie

dby

:M

icha

elS.

Ban

ner,

P11.

0

BO

NN

ER

AN

ALY

TIC

AL

TEST

ING

CO

MPA

NY

EE

EZ

ZL

i_..j

1._

iL

__J

00

0

BO

NN

ER

AN

AL

YT

ICA

LT

ES

TIN

GO

MP

AN

Y

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

SU

RA

NC

ED

ATA

DIO

XA

THIO

N!

DIO

XEN

ETI-I

ION

HPL

CAI

-LLY

SIS

DA

TA

Clie

nt:

Ash

land

Che

mic

alC

olle

cted

:12

/01/

2010

1230

ClIe

ntSa

mpl

eTy

pe:

Wat

er

Sam

ple

ID:

ASH

-MW

11-1

2012

010

Ext

ract

ed:

1210

2120

1013

00V

CT

Ext

ract

ion

Met

hod:

swe

3510

C

FIIe

#:10

1202

4-04

Ana

lyze

d:12

1141

2010

1641

DG

AA

naly

sis

Met

hod:

Mod

ified

SW84

6

Dat

eA

naIy

s

SAM

PLE

MET

HO

DBL

AN

KLa

bC

ontr

olM

ATR

IXSP

IKE

Det

ecte

dSp

ike

Det

ecte

dSp

ike

Det

ecte

dD

etec

ted

Spik

e

POL

Am

ount

Am

ount

Am

ounl

Am

ount

CO

MPO

UN

DS

ug/L

ug/L

Am

ount

%ug

ILA

mou

i%

ug!m

LA

mou

nt%

ugi’m

LA

mou

nt%

(ppb

)(p

pb)

ugh

Rec

over

y(p

pb)

ugIL

Rec

over

y(p

pm)

uglm

LR

ecov

ery

(ppm

>ug

fmL

Rec

over

y

Dio

xene

thlo

n0.

400

1.00

ND

9.13

10.0

917.

1110

.071

0.40

0N

DN

D9.

4310

.094

8.07

10.0

81

Dio

xath

ion

(cia

)

0.40

0N

DN

D8.

8410

.088

8.22

10.0

82

Dio

xath

ion

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

Spik

e-

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

niou

niR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

titha

lene

44

10.0

044

6.77

10.0

068

7.71

10.0

077

7.80

10.0

078

Cer

tifie

dby

:M

icha

elS.

Bon

ner.

Ph.D

BO

NN

ERA

NA

LYTI

CA

LT

EST

ING

CO

MPA

NY

rz:

LL

J

00

BO

NN

ER

AN

AL

YT

ICA

LT

ES

TIN

G(

)MPA

NY

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

SU

RA

NC

ED

ATA

DIO

XA

ThIO

N/D

IOX

EN

ET

hIO

NH

PLC

AN

AY

SIS

DA

TA

Cli

ent

Ash

land

Che

mic

alC

olle

cted

:12

/01/

2010

1215

Cte

ntSa

mpl

eTy

pe:

Wat

er

Sam

ple

ID:

ASH

-RS2

-120

1201

0E

xtra

cted

:12

1021

2010

1300

VC

T-

Ext

ract

ion

Met

hod:

SW84

635

1c)C

PIIe

#10

1202

4-05

Ana

lyze

d:12

1141

2010

1705

DG

A:

AnaiI

sMeth

:M

odlI

ledS

W84

6

Dat

eA

naly

st

SAM

PLE

MrT

I-IO

I)BL

IANK

Lab

Con

trol

MA

TRIX

SPIK

E

Det

ecte

dSp

ike

Det

ecte

dSp

ike

Dete

cD

etec

ted

Spik

e

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugIL

ugIL

Am

ount

%ug

hA

mou

n%

uglm

LA

mou

nt%

ug/m

LA

mou

nt%

(ppb

)(p

pb)

ug/L

Rec

over

y(p

pb)

ugh

Rec

over

y(p

pm)

ug/m

LR

ecov

ery

(ppm

)ug

/mL

Rec

over

y

Dio

xene

thio

n0.

400

ND

ND

9.13

10.0

917.

1110

.071

..

.0.

400

ND

ND

9.43

10.0

948.

0710

.081

Dio

xath

ion

(cis

)

0.40

0N

DN

D8.

8410

.088

6.22

10.0

82

Dio

xath

ion

(tra

ns)

Det

ecte

dSp

iked

%D

etec

tedid

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

nR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

lene

73

10.0

073

6.77

10,0

068

7.71

10.0

077

7.80

10.0

078

Cer

tifie

dby

:M

icha

elS.

Bon

ner,

Ph.D

BO

NN

ER

AN

ALY

TIC

AL

TE

STIN

GC

OM

PAN

Y

E—

EL

Jr

_

00

C)

BO

NN

ER

AN

ALY

TIC

AL

TE

STIN

GO

MPA

NY

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

UR

AN

CE

DA

TA

DIO

XA

THIO

N!

DIO

XEN

ETH

ION

FIPL

CAN

LYSI

SD

ATA

Clie

nt:

Ash

land

Chem

ical

Col

lect

ed:

1210

1120

1013

00C

lIent

Sam

ple

Type

:W

ater

Sam

ple

ID:

ASH

-MW

O5-

1201

2010

Ext

ract

ed:

12)0

2/20

1013

00V

CT

Met

hod:

SW84

635

10C

Fil

e#10

1202

4-08

Ana

lyze

d:12

1141

2010

1729

DG

A—

Ana

lysi

sMet

hod:

Mod

ifie

dSW

846

Dat

eA

naly

s

SAM

PLE

MET

HO

DN

KLa

bC

ontr

olM

ATR

IXSP

IKE

Det

ecte

dSp

ike

Det

ecte

dSp

ike

Det

ecte

dD

etec

ted

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugIL

ug!L

Am

ount

%ug

ILA

mou

n%

uglm

LA

mou

nt%

uglm

LA

mou

nt%

fppb

)(p

pb)

UgI

LR

ecov

ery

(ppb

)ug

hR

ecov

ery

(ppm

)ug

lmL

Rec

over

y(p

pm)

ughn

LR

ecov

ery

Dio

xene

thlo

n0.

400

ND

NO

9.13

10.0

917.

1110

.071

.*

0.40

00.

74N

D9.

4310

.094

8.07

’10

.081

Dlo

xath

ion

(cis

)

.0.

400

0.56

ND

8.84

10.0

888.

2210

.082

Dio

xath

pon

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

Spi

ke-

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

nR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

lene

45

10.0

048

6.77

10.0

068

7.71

10.0

077

7.80

10.0

078

Cer

Ufle

dby

Mic

hael

S.B

orin

er,

Ph.D

BO

NN

ER

AN

ALY

TIC

AL

TE

STIN

GC

OM

PAN

Y

EL

J.

_

00

0

BO

NN

ER

AN

AL

YT

ICA

LT

ES

TIN

GI

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

St

DIO

XA

TIII

ON

ID

!OX

ENET

hIO

NH

PLC

ANA

OM

PAN

YU

RA

NC

ED

ATA

LYSI

SD

ATA

Cer

tifie

db

Clie

ntA

shla

ndC

hem

ical

Col

lect

ed:

1210

1/20

1014

15C

lient

Sam

ple

Typ

e:W

ater

Sam

ple

ID:

ASH

-MW

12-1

2012

010

Ext

ract

ed:

1210

2120

1013

00V

CT

—E

xtra

cton

Met

hod

SW84

6ss

ioc

File

#:10

1202

4.07

Ana

lyze

d:12

1141

2010

1753

DG

AA

flaly

SiS

Met

hod

Mod

ified

SW84

6

Dat

eA

nalv

si]

SAM

PLE

MT

HO

DD

tiN

KLa

bC

ontr

olM

ATR

IXSP

IKE

Det

ecte

dD

etec

ted

—Sp

ike

Det

ecte

dD

etec

ted

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugIL

ug/L

Am

ount

%ug

ILA

mou

n%

ug!m

LA

mou

nt%

ug/m

LA

mou

nt%

(jpb

)(p

pb)

ug/L

Rec

over

y(p

pb)

ugh

Rec

over

y(j

pm)

uglm

LR

ecov

ery

(ppm

)ug

tmL

Rec

over

y

Dio

xene

tNon

0.40

00.

75N

D9.

1310

.091

7.11

10.0

71

.0.

400

ND

ND

9.43

10.0

946.

0710

.061

Dio

xath

ion

(cis

)

0.40

0N

DN

D8.

8410

.088

822

10.0

62

Dio

xath

ion

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

iid

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

ovei

yA

mou

ntA

mou

nR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

lene

7.0

10.0

070

6.77

10.0

068

7.71

10.0

077

7.80

10.0

078

Mic

hael

S.B

onne

r.Ph

.DB

ON

NE

RA

NA

LYTI

CA

LTE

STIN

GC

OM

PAN

Y

JL

PL

_ij

I

__

_

00

0

BO

NN

ER

AN

AL

YT

ICA

LT

ES1

1NG

OM

PA

NY

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

SU

RA

NC

ED

ATA

DIO

XA

TI-II

ON

IDIO

XEN

ETH

ION

l-IPL

CA

NA

LYSI

SD

ATA

Cli

ent

Ash

land

Chem

ical

Col

lect

ed:

12/0

1/20

1014

00C

lient

Sam

pleT

ype:

Wat

er

Sam

ple

ID:

ASH

-MW

O6-

1201

2010

Extra

cted

:12

102/

2010

1300

VC

T-

Ext

ract

ion

Met

hod:

SW84

835

10C

File

#:10

1202

408

Ana

lyze

d:12

114/

2010

1817

DG

A—

Ana

lysi

sM

etho

d:M

odifi

edSW

846

Dat

eA

naly

st1

SAM

PLE

MET

HO

DB

IIAN

KLa

bC

ontro

lM

ATR

IXSP

IKE

Det

ecte

dD

etec

ted

olk

eD

etec

ted

Det

ecte

dSo

ike

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

uglL

ugIL

Am

ount

%ug

itA

mou

n%

ug/m

LA

mou

nt%

uglm

LA

mou

nt%

(ppb

)(p

pb)

VgA

.R

ecov

ery

(ppb

)ug

/LR

ecov

ery

(ppm

)ug

lmL

Rec

over

y(p

pm)

uglm

LR

ecov

ery

Dio

xene

thlo

n0.

400

ND

ND

10.0

917.

1110

.071

..

0.40

0N

DN

D9.

4310

.094

8.07

10.0

81

Oox

athi

on(c

ia)

0.40

0N

DN

D8.

8410

.088

8.22

10.0

82

Dio

xath

ion

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%

SUR

RO

GA

TEC

OM

POU

ND

SA

mou

ntA

mou

ntR

ecov

ery

Am

ount

Am

oun

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Am

ount

Am

ount

Rec

over

y

Nap

htha

lene

6.9

10.0

069

6.77

10.0

068

7.71

10.0

077

7.80

10.0

078

Cer

tifie

d

BO

NN

ERA

NA

LYTI

CA

LTE

STIN

GC

OM

PAN

Y

EE

lE

EE

EE

ED

.L

EJc

-_

BO

NN

ER

AN

AL

YT

ICA

LT

EST

ING

OM

PAN

Y

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

SU

RA

NC

ED

ATA

DIO

XA

TI-II

ON

IDIO

XEN

ETH

ION

HPL

CA

N1L

YSI

SD

ATA

Clie

ntA

shla

ndC

hem

ical

Col

lect

ed:

12/0

1/20

1014

45C

lient

-Sa

mpl

eTy

pe:

Wat

et

Sam

ple

ID:

ASH

-MW

O7-

1201

2010

Ext

ract

ed:

1210

2120

1013

00V

CT

I—

EX

traC

tIO

flM

etho

d:SW

846

3510

C

File

#:10

1202

4-09

Ana

lyze

d:12

/141

2010

1841

DG

AA

naly

sis

Met

hod:

Mod

ified

Sld

46

Dat

eA

naly

s

SAM

PLE

MET

HO

DB

tAN

KLa

bC

ontro

lM

ATR

IXSP

IKE

Det

ecte

dSp

ike

Det

ecte

doke

Det

ecte

dSo

ilce

Det

ecte

d

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugiL

ugIL

Am

ount

%ug

ILA

niou

i%

ug/m

i.A

mou

nt%

ugIm

LA

mou

nt%

(ppb

)(p

pb)

ugh

Rec

over

y(p

pb)

ug/L

Rec

over

y(p

pm)

ug/m

LR

ecov

ery

(ppm

)ug

lmL

Rec

over

y

Dio

xene

thio

n0.

400

ND

ND

9.13

10.0

917.

1110

.071

..

0.40

0N

DN

D9.

4310

.094

8.07

10.0

81

D,o

xath

ion

(cs)

0.40

0N

DN

D8.

8410

.088

8.22

10.0

82

Dio

xath

ion

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

ii&

i%

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

niou

nlR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

titha

lene

5.1

10.0

051

5.77

10.0

968

7.71

10.0

077

7.80

10.0

078

Cer

thle

db

Mic

hael

S.B

onne

r.Ph

.DB

ON

NE

RA

NA

LYTI

CA

LTE

STIN

GC

OM

PAN

Y

EZ

JL

EI

LZ

JL

JcJ

L..J

LL

.JL

JL

JL

JL

)L

._.J

LJ

LJ

BO

NN

ER

AN

AL

YT

ICA

LT

EST

ING

CO

MPA

NY

OU

AN

TITA

TTV

ER

ESU

LT

SA

ND

OU

AU

TY

ASU

RA

NC

ED

ATA

DIO

XA

THIO

N) D

IOX

ENET

NIO

NH

FLC

AN

ALY

SIS

DA

TA

Cli

ent

Ash

land

Ch

emic

alC

olle

cted

:12

1011

2010

1525

Clie

ntSa

mpl

eTy

pe:

Wat

er

Sam

ple

ID:

ASH

-MW

24-1

2012

010

Ext

ract

ed:

1210

2120

1013

00V

CT

E,t

iori

Met

hod:

SW84

635

10C

File

#:10

1202

4-10

Ana

Lyze

d:12

1141

2010

1905

DG

AA

naly

sis

Met

hod:

Mod

ified

SW84

6

Dat

eA

naly

st

SAM

PLE

MET

HO

DB

NK

Lab

Con

trol

MA

JRIX

SPIK

E

Det

ecte

dSp

ike

Det

ecte

d1i

Plke

Det

ecte

dSp

ike

Det

ecte

d

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

uglL

ugIL

Am

ount

%U

9)L

Am

ou,

%ug

!mL

Am

ount

%ug

lmL

Am

ount

%

(ppb

)(p

pb)

ugIL

Rec

over

y(p

pb)

ugJL

Rec

over

y(p

pm)

uglm

LR

ecov

ery

(ppm

)ug

/mL

Rec

over

y

Dio

xene

thio

n0.

400

0.46

ND

9.13

10.0

917.

1110

.071

.0.

400

ND

ND

9.43

10.0

948.

0710

.081

Dio

xath

ion

(cls

)

0.40

0N

DN

D8.

8410

.088

8.22

10.0

82

Dio

xath

ion

(lie

ns)

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

nR

ecov

er’

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

lene

6.0

10.0

060

6.77

10.0

068

7.71

10.0

077

7.80

10.0

078

by

:,

Mic

hael

S.B

onne

r.Ph

.DB

ON

NE

RA

NA

LYTI

CA

LT

EST

ING

CO

MPA

NY

I•W

LJ

LL

_

LL

_J

00

Ahb

44J

Q.ke

A.-’-

r2JY

OU

RC

OM

PAN

YN

AM

E:

YO

UR

CO

MPA

NY

AD

DR

ES

S:

NA

ME

OF

PE

RS

ON

TO

CO

NT

AC

T:

CO

NT

AC

TP

ER

SO

N’S

PH

ON

E:

CO

NT

AC

TP

ER

SO

N’S

EMA

IL:

&--.p___

FAX

:-____

I

BO

NN

ERA

NA

LY

TICA

LTE

STIN

GC

OM

PAN

Y

2703

Oak

Gro

veRo

ad.H

aLtic

.sbur

g,M

S39

402

Phon

e:(6

01)-

264-

2854

Fax:

(601

)-26

8-70

84Em

ail:

baic

ocith

atcu

.coi

n

WW

W.B

AT

CO

.CO

M

CU

EN

TP

RO

JEC

TN

O.

CL

IEN

TP.

0.11

CL

IEN

TP

RO

JEC

TN

UM

BE

R

PAR

AM

ET

ER

SFO

RA

NA

LY

SIS

SAM

PLE

DE

SC

RIP

TIO

N

I

LABO

RATO

RYU

SE

DA

TET

IME

MA

TRIX

-

LI)

Turn

Aro

und

lim

ew z

.

z—

0z

—C.

)0

Pmle

ctN

umbe

rL

L

j 3D

0z

a-F

iIeI

D

11’4

vJ’

@-i

2øzz

a,,

)2Z

-cp

itqyz

IB

T____________

2p

4-

fr1v

)SI2

(azarq

2--ø

Z..-

2hZ

’3t

—BT

5L

z-Z

c?2-a

øiq

12-z

-j4ct

IBT

As--t2.L

ac

z-as

a-2w

tit

/—

4-

14jM

3.-

(2Z

Z(Q

.cz

-z-a

jya

1.241W

-I

—BT

6Ms

14-

-

1Z35

&1

BT

‘,1

S.ti-

fpa

-1z

øZ2t

iiø2Z

’ZcD

ie—

,..j

-‘

BT

84J

—M

ia--

/j

—ST

A44

V—

——

)—

ST

10ST

SAM

PLE

CO

LL

EC

TO

RIR

EL

INQ

UIS

HE

DB

Y:

DA

TET

IME

RE

CE

IVE

DB

Y:

EL

INQ

UIS

HE

DBY

:D

ATE

TIM

ER

EC

EIV

ED

BY:

ckw

eu

ME

TH

OD

OF

SHIP

ME

NT

(IfA

ny)

RE

LIN

QU

ISH

ED

BY:

DA

TET

IME

RE

CE

IVE

DF

OR

BA

TC

OBY

:O

ATE

ITIM

E

RE

MA

RK

S:]

RE

QU

ES

TB

AIC

OT

OD

ISP

OS

EO

FA

LLSA

MPL

ER

EM

AIN

DE

RS

(Sig

natu

re)

RE

VIS

ION

NO

1.2

-

ISA

MPL

EIS

DE

TE

RM

INE

DTO

BE

HA

ZA

RD

OU

S,A

MIN

IMU

MA

DD

ITIO

NA

L03

/22/

01

lAR

GE

OF

$30.

00P

ER

SAM

PLE

WIL

LB

EA

SS

ES

SE

D.

CL

_J

LJ

L_J.

00

BO

NN

ER

AN

AL

YT

ICA

LT

ES

TIN

GG

OM

PA

NY

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYF%

S4U

RA

NC

ED

ATA

DIO

XA

THIO

N1

DIO

XEN

ETH

ION

HPL

CA

NA

YSI

SD

ATA

Clie

ntA

shla

nd

Chem

ical

Col

lect

ed:

1113

0120

1011

35C

lient

Sam

ple

Type

:W

ater

Sam

ple

ID:

ASI

I-M

WO

3-11

3020

10E

xtra

cted

:12

)02)

2010

0830

VC

T-

Extra

ctio

nM

etho

d:SW

848

3510

C

File

#:10

1135

7-01

Ana

lyze

d:12

1131

2010

2009

DG

A1.

Ana

lysi

sM

etho

d:M

odifi

edSW

846

Dat

eAn

alystT

SAM

PLE

ME1

1-IO

DB(

IANK

Lab

Con

trol

MA

TRIX

SPIK

E

Det

ecte

dSp

ike

Det

ecte

dp

ikB

Det

ecte

dSo

ike

Det

ecte

d

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugR

ugh.

Am

ount

%U9

ILA

mou

ri%

uglm

LA

mou

nt%

uglm

LA

mou

nt%

(ppb

)(p

pb)

ugIL

Rec

over

y(p

pb)

ugL

Rec

over

y(p

pm)

uglm

LR

ecov

ery

(ppm

)ug

lmL

Rec

over

y

Dio

xene

thio

n0.

400

ND

ND

8.9

10.0

697.

110

.071

.0.

400

ND

ND

9.9

10.0

998.

810

.088

Dio

xath

ion

(cia

)

0.40

0N

DN

D9.

610

.096

7.9

10.0

79

Dio

xath

ion

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

Det

ecte

dSp

lked

%D

etec

ted

Spik

ed%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

nR

ecov

ep’

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

lene

7.2

10.0

072

7.1

10.0

071

7.2

10.0

072

7.2

10.0

072

Cer

tifie

dby_

______

Mic

hael

S.B

anne

r,Ph

.DB

ON

NE

RA

NA

LYTI

CA

LTE

STIN

GC

OM

PAN

Y

•.

J

__

__

__

——

00

BO

NN

ER

AN

AL

YT

ICA

LT

ES

TIN

GO

MP

AN

Y

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QIJ

AU

TYA

SSU

RA

NC

ED

ATA

DIO

XA

THIO

NI

DIO

XEN

ETH

ION

HPL

CA

NA

LYSI

SD

ATA

Clie

ntA

shla

nd

Chem

ical

Col

lect

ed:

1113

0120

1011

25C

lient

-Sa

mpl

eT

ype:

Wat

er

Sam

ple

ID:

ASH

-RSI

-113

0201

0E

xtra

cted

:12

I022

010

0830

VC

T-

Ext

ract

ion

Met

hod

SW84

635

10C

File

#10

1135

7-02

Ana

lyze

d:12

1131

2010

2033

DG

AI

Ana

lysi

sM

etho

d:M

odifi

edSW

846

Dat

eA

naly

sti

SAM

PLE

ME

ThO

DBI

IANK

Lab

Con

trol

MA

TRIX

SPIK

E

Det

ecte

dSp

ike

Det

ecte

dIs

Pike

Det

ecte

dD

etec

ted

S13&

e

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugIL

ugiL

Am

ount

%ug

hA

mou

n%

uglm

lA

mou

nt%

uglm

LA

mou

nt%

(ppb

)(p

pb)

ugh

Rec

over

y(p

pb)

ugh

Rec

over

y(p

pm)

uglm

LR

ecov

ery

(ppm

)ug

/mL

Rec

over

y

Dio

xene

thio

n0.

400

0.55

ND

8.9

10.0

897.

110

.071

..

0.40

0N

DN

D9.

910

.099

8.8

10.0

88

Dro

xath

on(c

is)

0.40

0N

DN

D9.

610

.096

7.9

10.0

79

Dio

xath

ion

(tran

s)

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

Rec

over

”A

mou

ntA

mou

ntR

ecov

ery

Am

ount

Am

ount

Rec

over

y

Nap

htha

lene

7.2

10.0

072

7.1

10.0

071

7.2

10.0

072

7.2

10.0

072

Cer

tifie

dby, M

chae

l S.

Sonr

,er.

Ph.D

BO

NN

ER

AN

ALY

TIC

AL

TEST

ING

CO

MPA

NY

i:•

LL

JL

J—

ocb

o

BO

NN

ER

AN

ALY

TIC

AL

TE

ST

ING

£)M

PAN

Y

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

SIU

RA

NC

ED

ATA

D1O

XA

TI-II

ON

!D

IOX

ENET

HIO

NH

PLC

AN

AY

SIS

DA

TA

Clie

nt:

Ash

land

Che

mic

alC

ofle

cted

:11

130(

2010

1222

Clie

nt-

Sam

ple

Typ

e:W

ater

Sam

ple

ID:

ASH

-MW

O2-

1130

2010

Ext

ract

ed:

1210

2120

1008

30V

CT

-E

xtra

ctio

nM

etho

d:SW

B4B

3510

C

FU

e10

1135

7-03

Ana

Lyze

d:12

1131

2010

2057

DG

A-

Ana

iyst

sMet

hod:

Mod

Ifie

dSW

B4B

Dat

eA

naly

st

SAM

PLE

M°T

hOO

MA

NK

Lab

Con

trol

MA

TRIX

SPIK

E

Det

ecte

dSp

ike

Det

ecte

d-Lke

Det

ecte

dSp

ike

Det

ecte

dSp

ike

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugiL

ugfl.

Am

ount

%rig

/I.A

mou

n%

uglm

LA

mou

nt%

u9nL

Am

ount

%

(ppb

)(p

pb)

ugIL

Rec

over

y(p

pb)

rig/I.

Rec

over

y(p

pm)

uglm

LR

ecov

ery

(ppm

)ug

lmL

Rec

over

y

Dio

xene

thio

n0.

400

ND

ND

8.9

10.0

897.

110

.071

..

0.40

0N

DN

D9.

910

.099

8.8

10.0

88

Dio

xath

ion

(cis

)

0.40

0N

DN

D9.

610

.096

7.9

10.0

79

Dio

xath

ion

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

riR

ecov

er’

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

lene

8.3

10.0

083

7.1

10.0

071

7.2

10,0

072

7.2

10.0

072

Cer

tifie

dby

:M

icha

elS.

Bon

ner,

Ph.D

BO

NN

ERA

NA

LYTI

CA

LTE

STIN

GC

OM

PAN

Y

0•C)

YO

UR

CO

MPA

NY

NA

ME:

YO

UR

CO

MPA

NY

AD

DR

ESS

:i4pt

4.tJes

gA.

NA

ME

OF

PER

SON

TOC

ON

TAC

T:

CO

NTA

CT

PER

SON

’SPH

ON

E:

CO

NTA

CT

PER

SON

’SEM

AIL

:

Tvv

I44

LJ‘

=:•

_

BO

NN

ERA

NA

LY

TICA

LTE

STIN

GC

OM

PAN

Y

2703

Oak

Gro

veRo

ad, H

auic

sbur

g,M

S39

402

Phon

c:(6

01)-2

64—

2R54

Fax:

(60)

)268

-708

4Em

ail:

baic

o(àb

atco

,cor

n

WW

W.B

AT

CO

.CO

M

___

FAX

:

CLI

ENT

PRO

JEC

TN

O.

CLI

ENT

P.O

..C

LIEN

TPR

OJE

CT

NU

MB

ER

PAR

AM

ET

ER

SFO

RA

NA

LYSI

S

SAM

PLE

DE

SCR

IPT

ION

DA

TE

LABO

RATO

RYU

SE

TIM

EM

ATR

IX

II

Tu

mA

rou

nd

Tim

e

*,..

wI

.-

9-

4fcL

,z 0

z 0Pm

ject

Num

ber

;U

-0

<

-cr

.

;; N.

Fil

eID

:/t

--Z

GU

35

V

2M

iI’

--

tI-3

cD”2

Obj’

VJ

—BT

Au

-M

wa2

-1I;

pza,,

(vt/

M)

uizø

IZ.Z

-2/

3BT

4‘

BT

5BT

6BT

7BT

8BT

9.

BT

10BT

SA

MP

LE

CO

LL

EC

TO

R/R

EL

INQ

UIS

HE

DB

Y:

DA

TE

TiM

ER

EC

EIV

ED

EL

INQ

UIS

HE

DB

Y:

DA

TET

IME

RE

CE

IVE

DB

Y:

-ti

j3-2t

1315

(I

ME

TH

OD

OF

SH

IPM

EN

T(I

IA

ny)

RE

LIN

QU

ISH

ED

BY

DT

IME

RE

CE

IVE

DF

OR

BA

TC

OB

YD

ATE

/1’IM

E

RE

MA

RK

S:

-

]R

EQ

UE

ST

BA

TC

OT

OD

ISP

OS

EO

FA

LL

SA

MP

LE

RE

MA

IND

ER

S

(Slg

natw

e)

RE

VIS

ION

NO

1,2

.

IS

AM

PL

EIS

DE

TE

RM

INE

DT

OB

EH

AZ

AR

DO

US

,A

MIN

IMU

MA

DD

ITIO

NA

L03

/22/

01

-..

lAR

GE

OF

$30.0

0P

ER

SA

MP

LE

WIL

L.

BE

AS

SE

SS

ED

.

LJ

LL

.?

00

BO

NN

ER

AN

AL

YT

ICA

LT

ES

TIN

GC

MP

AN

Y

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

SU

RA

NC

ED

ATA

DIO

XA

TI-II

ON

/DIO

XEN

ETII

ION

HPL

CA

NA

LYSI

SD

ATA

Clie

ntA

shla

ndC

hem

ical

Col

lect

ed:

1112

9/20

1014

45C

lient

Sam

ple

Type

:W

ater

Sam

ple

ID:

ASI

I-C

MO

5-1

1282

010

Ext

ract

ed:

1210

2120

1008

30V

CT

IEx

tract

ion

Met

hod:

SW84

635

10C

Fil

e#10

1134

4-01

Ana

lyze

d:12

)131

2010

1408

DG

Af

Ana

lysi

sMet

liod:

Mod

ifte

dSW

84s

Dat

eA

naly

stj

SAM

PLE

ME

ThO

DB

NK

Lab

Con

trol

MA

TRIX

SPIK

E

Det

ecte

dD

et

Spik

eD

eci

Det

ecte

dSp

lice

POL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugIL

ugJL

Am

ount

%ug

iLA

mou

nt%

uglm

LA

mou

nt%

uglm

LA

mou

nt%

(ppb

)(p

pb)

ug/L

Rec

over

y(p

pb)

uoJL

Rec

over

y(p

pm)

ugfm

l.R

ecov

ery

(ppm

)ug

lmL

Rec

over

y

Dio

xene

thio

n1.

9N

D8.

910

.089

7.1

10.0

71

..

0.40

0N

DN

D9.

910

.099

8.8

10.0

88

Dio

xath

ion

(cr5

)

0.40

0N

DN

D9.

610

.096

7.9

10.0

79

D,o

xath

ion

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

Splk

edl

%D

etec

ted

Spik

ed%

Det

ecte

dSp

liced

%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

rnou

nR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

lene

6.9

10.0

089

7.1

10.0

071

7.2

10.0

072

7.2

10.0

072

Cer

lifie

dby

:M

icha

elS.

Bon

ner,

Ph.D

BO

NN

ER

AN

ALY

TIC

AI

TEST

ING

CO

MPA

NY

EE

J11

Li.

_

00

BO

NN

ER

AN

AL

YT

iCA

LT

ES

TIN

GC

)MP

AN

Y

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

SSU

RA

NC

ED

ATA

DIO

XA

THIO

N!D

IOX

ENET

HIO

NH

PLC

AN

4YS

ISD

ATA

ClI

ent

Mhla

nd

Chem

ical

Col

lect

ed;

1112

9120

1014

50C

lient

Sam

ple

Typ

e:W

ater

Sam

ple

ID:

ASH

-CM

O4-

1129

2010

Ext

ract

ed:

12I0

2120

1008

30V

CT

Ext

ract

ion

Met

hod:

SW84

635

10C

Fil

e#10

1134

4-02

Ana

lyze

d:12

1131

2010

1429

DG

A—

Ana

lysi

sM

etho

d:t.4

odif

iedS

W84

6

Dat

eA

naly

st

SAM

PLE

MFT

HO

DB’

IAN

KLa

bC

ontro

lM

ATR

IXSP

IKE

Det

ecte

dSp

ike

Det

ecte

d—

plke

Det

ecte

dD

etec

ted

Spik

e

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugIL

ugh.

Am

ount

%ug

/LA

mou

n%

uglm

LA

mou

nt%

uglm

LA

mou

nt%

(ppb

)(p

pb)

ugIL

Rec

over

y(p

pb)

ugIL

Rec

over

y(p

pm)

ugIm

LR

ecov

ery

(ppm

)ug

ImL

Rec

over

y

Die

net

hlo

n0.

400

1.5

ND

8.9

10.0

897.

110

.071

0.40

0N

DN

O9.

910

.099

8.8

10.0

86

Dio

xath

ion

(cis

)

0.40

00.

62N

D9.

610

.098

7.9

10.0

79

Dio

xatti

ion

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

nR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

lene

6.3

10.0

063

7.1

10.0

071

7.2

10.0

072

7.2

10.0

072

Cer

tifie

dby

:M

icha

elS.

Bon

net,

Ph.D

BO

NN

ER

AN

ALV

TIC

AL

TES1

1NG

CO

MPA

NY

Li

00

o

BO

NN

ER

AN

AL

YT

ICA

LT

ES

TIN

GC

OM

PA

NY

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

AL

IWA

SSU

RA

NC

ED

ATA

DIO

XA

THIO

NJD

IOX

ENET

HIO

NH

PLC

AN

ALY

SIS

DA

TA

Clie

ntA

shla

nd

Chem

ical

Col

lect

ed:

1112

9120

1015

00C

lient

Sam

ple

Type

:W

ater

Sam

ple

ID:

ASH

-CM

O3-

1129

2010

Ext

ract

ed:

1210

2120

1008

30V

OT

Extra

ctio

nM

etho

d:SW

646

3510

C

File

#:10

1134

4.03

Ana

lyze

d:12

)131

2010

1609

OG

A—

Ana

lysi

sMet

hod:

Mod

ified

SW84

6

Dat

eA

naly

st

SAM

PLE

MET

I-IO

DBI

IAN

I(t.a

bC

ontro

lM

ATR

IXSP

IKE

Det

ecte

dD

etec

ted

Spik

eD

etec

ted

Det

ecte

dSp

ike

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugfl

ug/L

Am

ount

%ug

!LA

mou

r%

uglm

LA

mou

nt%

uglm

LA

mou

nt%

(ppb

)(p

pb)

ug!L

Rec

over

y(p

pb)

ugh

Rec

over

y(p

pm)

uglm

LR

ecov

ery

(ppm

)ug

lmL

Rec

over

y

Dlo

xene

tliio

n0.

400

0.49

ND

8.9

10.0

897.

110

.071

.

0,40

0N

DN

D9.

910

.099

8.8

10.0

88

Dio

xath

ion

(Cis

)

0.40

0N

DN

D9.

610

.096

7.9

10.0

79

Dio

xa(h

ion

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

Spik

ea%

Det

ecte

dSp

iked

ID

etec

ted

Spik

ed%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

nR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

iene

6.9

10.0

069

7.1

10.0

071

7.2

10.0

072

7.2

10.0

072

Cer

tifie

dby

:M

icha

elS.

Bon

ner,

Ph.D

BO

NN

ERA

NA

LYTI

CA

LTE

STIN

GC

OM

PAN

Y

I.‘J

1

EL

JL

JL

Li

_

-

_

O0

BO

NN

ER

AN

ALY

TIC

AL

TE

STIN

GC

MPA

NY

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

OU

AL

ITt’

ASS

RA

NC

ED

ATA

DIO

XA

THIO

NI

DIO

XEN

EThI

ON

HPL

CA

NA

LYSI

SD

ATA

Clie

ntA

shla

ndC

hem

ical

Col

lect

ed:

11/2

9/20

1015

05C

lIent

Sam

ple

Type

:W

ater

Sam

ple

ID:

ASH

-CM

O2-

1129

2010

Ext

ract

ed:

12/0

2120

1008

30V

CT

TE

xtra

ctio

nM

etho

d:SW

B46

3510

C

File

W10

1134

4-04

Ana

lyze

d:12

1131

2010

1633

DG

Ar

Ana

lyst

sM

etho

d:M

oddi

eci

SW84

6

Dat

eA

naly

st

SAM

PLE

-

MtT

KO

DB

NK

Lab

Con

trol

MA

TRIX

SPIK

E

Det

ecte

dSp

ike

Def

ecte

dpi

keD

etec

ted

Spik

eD

etec

ted

Spik

e

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugIL

ugIL

Am

ount

%ug

itA

mou

nt%

uglm

LA

mou

nt%

uglm

LA

mou

nt%

(ppb

)(p

pb)

ug/L

Rec

over

y(p

pb)

ug/L

Rec

over

y(p

pm)

ughn

LR

ecov

ery

(ppm

)ug

lmL

Rec

ovei

y

Dio

xene

thlo

n0.

400

ND

ND

8.9

10.0

897.

110

.071

.0.

400

ND

ND

9.9

10.0

998.

810

.088

Dio

xath

lon

(as)

0.40

0N

DN

D9.

610

.096

7.9

10.0

79

Olo

xath

ion

(han

s)

Det

ecte

dSp

iked

%D

etec

ted

Ied

%D

etec

ted

SpH

ed%

Det

ecte

dSp

iked

%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

nR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecoy

pry

Nap

htha

iene

8.1

10.0

081

7.1

10.0

071

7.2

10.0

072

7.2

10.0

072

Cer

tifie

dby

Mic

hael

S.B

onne

r,Ph

.DB

ON

NER

AN

ALY

TIC

AL

TEST

ING

CO

MPA

NY

II

00

BO

NN

ER

AN

ALY

TIC

AL

TE

STIN

GC

OM

PAN

Y

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

S4U

RA

NC

ED

ATA

DIO

XA

THIO

NI

DIO

XEN

ETH

ION

HPL

CA

*Y

SIS

DA

TA

Clie

nt:

Ash

land

Chem

ical

Col

lect

ed:

1112

9120

1015

20C

lIent

Sam

ple

Type

:W

ater

Sam

ple

ID:

ASH

.CM

O1-

1129

2010

Ext

ract

ed:

1210

2120

1008

30V

CT

JEx

tract

ion

Met

hod:

SW84

635

10C

File

#:10

1134

4-05

Ana

lyze

d:12

1131

2010

1657

DG

kLA

naly

sis

Met

hod:

Mod

ified

SW84

8

Dat

eA

nalY

st]

SAM

PLE

MET

HO

DB

LAN

K1.

abC

ontro

lM

ATR

IXSP

IKE

Det

ecte

dSp

ike

Det

ecte

d—

Spik

eD

etec

ted

Spik

øD

etec

ted

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

uglL

ugh

Am

ount

%ugh

Am

oun

%ug

lmL

Am

ount

%ug

lml.

Am

ount

%

(ppb

)(p

pb)

ugIL

Rec

over

y(p

pb)

ug&

Rec

over

y(p

pm)

uglm

LR

ecov

ery

(ppm

)ug

fmL

Rec

over

y

Dio

xene

thlo

n0.

400

NO

ND

8.9

10.0

897.

110

.071

..

0.40

0N

DN

D9.

910

.099

8.8

10.0

86

Dio

xallu

ori (

os)

0,40

0N

DN

D9.

610

.096

7.9

10.0

79

Dio

xath

ion

(tra

ns)

Det

ecte

dSp

iked

%D

etec

tedie

-%

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

n-

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Am

ount

Am

ount

Rec

over

y

Nap

htha

lenG

7.1

10.0

071

7.1

10.0

071

7.2

10.0

072

7.2

10.0

072

Cer

tUIe

dbM

icha

elS.

Bon

ner,

Ph.D

BO

NN

ER

AN

ALY

TIC

AL

TEST

ING

CO

MPA

NY

D

__

__

__

do

BO

NN

ER

AN

ALY

TIC

AL

TE

ST

ING

(.O

MP

AN

Y

QU

AN

TITA

TIV

ER

ESI

JL.T

SA

ND

QU

ALI

TYA

SU

RA

NC

ED

ATA

DIO

XA

ThI

ON

/DIO

XEN

ETH

ION

HPL

CA

Nd

YSI

SD

ATA

Cil

ent

Ash

land

Che

mic

alC

olle

cted

:11

/291

2010

1525

Clie

nt-

Sam

pleT

ype:

Wat

er

Sam

ple

ID:

ASH

-CM

OO

-112

9201

0E

xtra

cted

:12

1021

2010

0630

VC

T-

Ext

ract

ion

Met

hod:

swse

3510

C

Fii

e#10

1134

4-06

Ana

lyze

d:12

113/

2010

1721

DG

A-

Ana

lysi

sMei

hod:

Mod

iIle

dSW

846

Dat

eA

naly

s

SAM

PLE

MFT

hOD

B’N

I<L

abC

ontro

lM

ATR

IXSP

IKE

Det

ecte

dSp

ike

Det

ecte

d—

Spik

eD

etec

ted

Spik

eD

etec

ted

Spik

e

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugIL

uglL

Am

ount

%ug

hA

mou

r%

uglm

LA

mou

nt%

uglm

LA

mou

nt%

(ppb

)(p

pb)

ugIL

Rec

over

y(p

pb)

ug/L

Rec

over

y(p

pm)

uglm

LR

ecov

ery

(ppm

)ug

lmL

Rec

over

y

Dio

xene

thlo

n0.

400

ND

ND

8.9

10.0

897.

110

.071

0.40

0N

DN

D9.

910

.099

8.8

10.0

88

Dio

xath

ion

(dC

)

0.40

0N

DN

D9.

610

.096

7.9

10.0

79

Dio

xath

ion

(tran

s)

Det

ecte

dSp

iked

%D

etec

ted

%D

etec

ted

Spik

ed%

Det

ecte

dSp

liced

%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

litha

lene

6.9

10.0

069

7.1

10.0

071

7.2

10.0

072

7.2

10.0

072

Cer

tifie

dby

:M

icha

elS.

Bon

ner,

Ph.D

BO

NN

ER

AN

ALY

TiC

AL

TEST

ING

CO

MPA

NY

LAB

OR

A1O

FIY

USE

Turn

Aro

und

Tim

e

Prri

,ecI

Num

ber

(1) o 0

0U

-

____________

o<

____________

File

113

I-B

T

IB

T

I—

BT

I—

BT

I—

BT

I—

BT BT

______________

BT

BT

BT

DA

TETI

ME

RE

CE

IVE

DBY

:

UE

EJ

LJ

L

__

__

____

BO

NN

ERA

NA

LYTI

CA

LTE

STIN

GC

OM

PAN

Y

________

2703

Oak

Gro

veRo

ad,H

atiie

sbur

g,M

S39

402

________

________—

Phon

y:(6

011-

264-

2854

Pax:

(601

)-26

)i-70

84Em

ail:

baic

o’w

hatc

o.co

rn

YO

UR

CO

MPA

NY

NA

ME:

______

YO

UR

CO

MPA

NY

AD

DR

ESS

:

_______

NA

ME

OF

PER

SON

TOC

ON

TAC

T:

_____

CO

NTA

CT

PE

RS

ON

SPH

ON

E:

‘1_-_3

42..

Z7’%

__________

CO

NTA

CT

PE

RS

ON

SEM

AIL

:

CLI

ENT

PRO

JEC

TN

O.

CLI

ENT

P.O

.#C

LIEN

TPR

OJE

CT

NU

MB

ER

FAX

:

II

PAR

AM

ET

ER

SFO

RA

NA

LYSI

S

LSA

MPL

ED

ESC

RIP

TIO

N

--

2/5

Jf-

Q,1

-

1A

5U

-’viø

-I!

z920’®

i_/4

tMøZ

-12

’Z.c

VW

SC

...Q

f—II

V?Z

Ø1Ø

6-

(A-v

1øG

-I(

zqza;q

DA

TETI

ME

MA

TRIX

ij9-2ti

ø1

445

if--

2W

øi4

ca

7ra2

D(Ø

IS’c

Zxb

r.4

________________

•(-Z

JtD

1ø5

u-z

q-2

d,4

_52$

______________

_

JSA

MPL

EC

OL

LE

CT

OR

/RE

LIN

QU

ISH

ED

BY:

DA

TEli

ME

RE

CE

IVE

DBY

:EL

INQ

UIS

HED

BY:

1W8L

Jl1

-2W)

ME

TH

OD

OF

SHIP

ME

NT

(ItA

ny)

RE

LIN

QU

ISH

ED

BY:

II

-.—

,—-

..,—

.—-l

_..

•-7

-—

—---—

I

ID

ATE

TIM

ER

EC

EIV

ED

FOR

BA

TCO

BY:

DA

TE/T

IME

REM

AR

KS:

.R

EQ

UE

STB

AT

CO

TO

DIS

POSE

OF

ALL

SAM

PLE

RE

MA

IND

ER

S

F(S

igna

ture

)R

EVIS

ION

NO

1.2

-

IISA

MPL

EIS

DE

TE

RM

INE

DTO

BE

HA

ZAR

DO

US,

AM

INIM

UM

AD

DIT

ION

AL

03/2

2/01

IHA

RG

EO

F$3

0.00

PER

SAM

PLE

WiL

LB

EA

SSE

SSE

D.

I_i

cL

LJ

_

_

-

aa

C

BO

NN

ER

AN

AL

YT

ICA

LT

EST

ING

CM

PAN

Y

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

AL

1r’A

SSLR

.ANC

ED

ATA

DIO

XA

TH1O

NI D

IOX

ENET

HIO

NH

PLC

AN

AY

SIS

DA

TA

Clie

ntA

shla

nd

Chem

ical

Col

lect

ed:

1210

2(20

1009

50C

lIent

[Sa

mpl

eT

ype:

Wat

er

Sam

ple

ID:

ASH

-MW

I6-1

2022

010

Ext

ract

ed:

1210

4/20

1008

00V

CT

Extra

ctio

nM

etho

d:SW

846

3510

C

FiIe

#:10

1204

2-01

Ana

lyze

d:12

115/

2010

0104

E)G

A:

Mal

ysis

Met

hod:

Mod

ified

SW84

6

Dat

eA

naly

st

SAW

PLE

M’T

HO

DB

iN

Kla

bC

ontr

olM

ATR

IXSP

IKE

Det

ecte

dSp

ike

Det

ecte

dpd

ceD

etec

ted

Det

ecte

dSp

ike

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugIL

ugh.

Am

ount

%ug

ILA

mou

nt%

ug/m

LA

mou

nt%

ugir

nlA

mou

nt%

(ppb

)(p

pb)

ug/L

Rec

over

y(p

pb)

ugIL

Rec

over

y(p

pm)

ugim

LR

ecov

ery

(ppm

)ug

ftnL

Rec

over

y

Dio

xene

thio

n0.

400

ND

ND

9.13

100

917.

1110

.071

.

0.40

01.

6N

D9.

4310

.094

8.07

10.0

81

Dio

xath

ion

(cis

)

0.40

0N

DN

D8.

5410

.088

822

10.0

82

Dio

xath

ion

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

lene

5.7

10.0

057

6.77

10.0

068

7.71

10.0

077

7.80

10.0

078

Cer

tifie

dby:_

____

___________________

Mic

hael

S.B

onne

r,Ph

.DB

ON

NE

RA

NA

LYTI

CA

LTE

STIN

GC

OM

PAN

Y

—tJ

LJ

LJ

1J

.L

ZJ

Ki

LJ

0&

BO

NN

ER

AN

AL

YT

ICA

LT

EST

ING

OM

PAN

YQ

UA

NTI

TATI

VE

RE

SUL

TS

AN

DQ

UA

LITY

AS

UR

AN

CE

DA

TAD

IOX

ATH

ION

!D

IOX

ENET

HIO

NH

PLC

AN

LYSI

SD

ATA

Cli

ent

Ash

land

Che

mic

alC

olle

cted

:12

1021

2010

1030

Clie

ntI

Sam

ple

Typ

e:W

ater

Sam

ple

ID:

ASH

-MW

15-1

2022

010

Ext

ract

ed:

1210

4120

1005

00V

CT

Ext

ract

ion

Met

hod:

SW84

635

10C

File

#:10

1204

2-02

Ana

lyze

d:12

1151

2010

0127

DG

AA

naly

sis

Met

hod:

Mod

t8ed

SW84

6D

ate

Ana

lys

SAM

PLE

MET

HO

DB

IAN

KL

abC

ontro

lM

ATR

IXSP

IKE

Det

ecte

dSp

ike

Det

ecte

dSo

ike

Det

ecte

dSp

ike

Det

ecte

dSp

ike

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugIL

ugIL

Am

ount

%ug

!LA

mou

n%

uglm

LA

mou

nt%

uglm

LA

mou

nt%

(ppb

)(p

pb)

ugIL

Rec

over

y(p

pb)

ugh

Rec

over

y(p

pm)

uglm

LR

ecov

ery

(ppm

)ug

lmL

Rec

over

y

Dio

xene

thio

n0.

400

ND

ND

9.13

10.0

917.

1110

.071

..

.0.

400

2.9

ND

9.43

10.0

948.

0710

.081

Dio

xattv

on(c

is)

0.40

02.

8N

D8.

8410

.088

8.22

10.0

82D

ioxa

thio

n(t

rans

)

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

nR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

titha

tene

6.2

10.0

062

6.77

10.0

068

7.71

10.0

077

7.80

10.0

078

Cer

lille

dby

:M

icha

ela

Bor

lner

,P

hi)

BO

NN

ER

AN

ALY

TIC

AL

TE

STIN

GC

OM

PAN

Y

__

__

__

___

__

EL

LL

•i

__

0a

C

BO

NN

ER

AN

AL

YT

ICA

LT

EST

ING

OM

PAN

Y

QU

AN

TITA

TIV

ER

ESU

LTS

AN

DQ

UA

LIV

(AS

IJRA

NCE

DATA

DIO

XA

TI-H

ON

ID

IOX

ENET

HIO

NH

PLC

AN

PLY

SIS

DA

TA

Clie

ntA

shla

ndC

hem

ical

Col

lect

ed:

1210

2120

1010

40C

lIent

—Sa

mpl

eTy

pe:

Wal

er

Sam

ple

ID:

ASH

-RS3

-120

2201

0E

xtra

cted

:12

1041

2010

0800

VC

TE

xtin

ctio

nM

etho

d:SW

846

3510

C

Fite

#:10

1204

2-03

Ana

lyze

d:12

1151

2010

0151

OG

A—

Ana

lysi

sM

etho

d:M

odifi

edSW

846

Dat

eA

na

1

SAM

PLE

MET

HO

D81

.AN

KLa

bC

ontro

lM

ATR

IXSP

IKE

Det

ecte

dSp

ike

Det

ecte

dSp

ike

Det

ecte

dD

etec

ted

POL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugIL

UgIL

Am

ount

%ug

ILA

mou

ri%

uglm

LA

mou

nt%

uglm

LA

mou

nt%

(ppb

)(p

pb)

U9I

LR

ecov

ery

(ppb

)ug

h.R

ecov

ery

(ppm

)ug

lmL

Rec

over

y(p

pm)

ugim

LR

ecov

ery

Dlo

xene

thio

n0.

400

1.3

ND

9.13

10.0

917.

1110

.071

.

0.40

0N

DN

D9.

4310

.094

8.07

10.0

81

Dro

xath

ion

(cia

)

0.40

00.

89N

D8.

8410

.088

8.22

10.0

82

Dlo

xath

lon

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

Spi

ke4

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecoy

er’

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

lene

7.4

10.0

074

6.77

10.0

068

7.71

10.0

077

7.80

10.0

078

Cer

tifie

dby

:M

icha

elS.

Bon

ner,

Ph.D

BO

NN

ER

AN

ALY

TIC

AL

TEST

ING

CO

MPA

NY

_

_

.J

_

0L

Io

BO

NN

ER

AN

ALY

TIC

AL

TE

ST

ING

CM

PAN

Y

(2U

AN

TITA

T1V

ER

ESU

LT

SA

ND

QU

ALI

TYA

SLJR

AN

CE

DA

TA

DIO

XA

TI-II

ON

!DIO

XEN

ETH

ION

HPL

CA

NA

LYSI

SD

ATA

Clie

nt:

Ash

land

Chem

ical

Col

lect

ed:

12)0

2120

1011

20C

lient

-

Sam

ple

Type

:W

ater

Sam

ple

ID:

ASH

.MW

I4-1

2022

010

Ext

ract

ed:

12/0

4/20

1008

00V

CT-

Extra

ctio

nM

etho

d:sw

aess

ioc

FiIe

#:10

1204

2-04

Ana

lyze

d:12

/15/

2010

0215

DG

A—

Ana

lysi

sMet

hod:

Mod

lfie

dSW

B46

Dat

eA

naly

st

SAM

PLE

MIE

THO

DB

NK

lab

Con

trol

MA

TRIX

SPIK

E

Det

ecte

dD

etec

ted

—Sp

ike

Dat

eced

Spik

eD

etec

ted

PQL

Am

ount

Am

ount

—A

mou

ntA

mou

nt

CO

MPO

UN

DS

ugIL

ugh.

Am

ount

%ug

/LA

mov

n%

uglm

LA

mou

nt%

ugim

LA

mou

nt%

(ppb

)(p

pb)

ug/L

Rec

over

y(p

pb)

ug/L

Rec

over

y(p

pm)

uglm

LR

ecov

ery

(ppm

)ug

/mL

Rec

over

y

Dio

xene

thlo

n0.

400

ND

ND

9.13

10.0

917.

1110

.071

..

0.40

05.

1N

D9.

4310

.094

8.07

10.0

81

Dia

xath

ion

(cis

)

0.40

01.

0N

D8.

8410

.088

8.22

10.0

82

Dio

xath

ion

(tm

ns)

Det

ecte

dSp

Iked

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

rR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

httr

alen

e7.

610

.00

766.

7710

.00

687.

7110

.00

777.

8010

.00

76

Cei

lifie

clby

:M

icha

elS.

Bon

ner,

Ph.D

BO

NN

ERA

NA

LYTI

CA

LTE

STIN

GC

OM

PAN

Y

EE

EE

EE

JL

_L

LJ

0u

BO

NN

ER

AN

AL

YT

ICA

LT

ES

TIN

G

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

St

DIO

XA

ThIO

NID

IOX

ENET

HIO

NH

PLC

AN

OM

PAN

YU

RA

NC

ED

ATA

LYSI

SD

ATA

Cer

tifie

dby

:

-

Clie

ntA

shla

ndC

hem

ical

Col

lect

ed:

1210

2120

1012

00C

lient

ISa

mpl

eTy

pe:

Wat

er

Sam

ple

ID:

ASH

-MW

13-1

2022

010

Ext

ract

ed:

1210

4120

1008

00V

CTi

Extra

ctiO

nM

etho

d:sw

se35

10C

File

#10

1204

2-05

Ana

lyze

d:12

1151

2010

0239

DG

A—

Ana

lysi

SM

etho

d:M

odifi

edSW

846

Dat

eA

naly

st

SAM

PLE

MET

HO

DIIA

NK

Lab

Con

trol

MA

TRIX

SPIK

E

Det

ecte

dD

etec

ted

Spik

eD

etec

ted

Spi

keD

etec

ted

POL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugIL

ugiL

Am

ount

%ug

ILA

mou

n%

uglr

nlA

mou

nt%

uglm

LA

mou

nt%

(ppb

)(p

pb)

ugIL

Rec

over

y(p

pb)

ugIL

Rec

over

y(p

pm)

ug/m

LR

ecov

ery

(ppm

)ug

lmL

Rec

over

y

Dio

xene

thio

n0.

400

6.6

ND

9.13

10.0

917.

1110

.071

Dio

xath

ion(

cis)

0.40

01.

5N

D9.

4310

.094

8.07

10.0

81

0.40

00.

60N

D6.

8410

.088

8.22

10.0

82

Dio

xalti

lon

(tra

na)

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed)

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

njR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

lene

10.0

10.0

010

06.

7710

.00

687.

7110

.00

777.

8010

.00

78

Mhae

lS.

Bon

ner,

P11.

0B

ON

NE

RA

NA

LYTI

CA

LTE

STIN

GC

OM

PAN

Y

_

LZ

hL

Ji

_

BO

NN

ER

AN

AL

YT

ICA

LT

ES

TIN

GO

MPA

NY

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

SU

RA

NC

ED

ATA

DIO

XA

TIII

ON

ID

IOX

ENET

hIO

NK

PLC

A.X

SIS

DA

TA

Clie

ntA

shla

ndC

hem

ical

Col

lect

ed:

1210

2/20

1012

35C

uent

Sam

ple

Type

:W

ater

Sam

ple

ID:

ASI

-l-M

WI9

-120

2201

0E

xtra

cted

:12

/04/

2010

0800

VC

TI

Ext

ract

ion

Met

hod:

SW84

635

10C

File

#10

1204

2-06

Ana

lyze

d:12

/15/

2010

0303

DG

AA

naly

sis

Met

hod:

Mod

ified

SW84

6

Dat

eA

naly

s

SAM

PLE

MFr

I-IO

0B

LAN

KL

abC

ontr

olM

ATR

IXSP

IKE

Det

ecte

dSp

ike

Det

ecte

d—

jSpl

keD

etec

ted

Det

ecte

dSp

ike

FQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ug/L

ugh

Am

ount

%ug

hA

mou

n%

ug/m

LA

mou

nt%

ug/m

LA

mou

nt%

(ppb

)(p

pb)

ugh

Rec

over

y(p

pb)

ugIL

Rec

over

y(p

pm)

ug!m

LR

ecov

ery

(ppm

)ug

lmL

Rec

over

y

Dio

xene

thio

n0.

400

ND

ND

9.13

10.0

917.

1110

.071

..

0.40

079

.6N

D9.

4310

.094

8.07

10.0

81

Dio

xath

ion

(CIS

)

0.40

05.

1N

D8.

8410

.088

8.22

10.0

82

Dio

xath

ion

(fra

nc)

Det

ecte

dSp

iked

%D

etec

ted

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

nlR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

liflia

lene

9.9

10.0

099

6.77

10.0

068

7.71

10.0

077

7.80

10.0

078

Cer

tifie

dM

icha

elS.

Bon

net,

Ph.D

BO

NN

ERA

NA

LYTI

CA

LTE

STIN

GC

OM

PAN

Y

ira

LJ

——

0t

0

BO

NN

ER

AN

AL

YT

ICA

LT

ES

TIN

GC

OM

PA

NY

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

SU

RA

NC

ED

ATA

DIO

XA

THIO

N/ D

IOX

ENET

HIO

NH

PLC

ANd

.YSJ

SD

ATA

Cha

ntA

shla

ndC

hem

ical

Col

lect

ed:

1210

2)20

10C

lient

—S

ampl

eT

ype:

Wat

er

Sam

ple

ID:

ASI

-I-F

02-1

2022

010

Ext

ract

ed:

12)0

4120

1008

00V

CT

Extr

acti

on

Met

hod:

SW84

635

10C

Flle

#:10

1204

2-07

Ana

lyze

d:W

0327

OG

A:

IsM

e:

Mod

ified

SW84

6

Dat

eM

alys

SPLM

PLE

MET

HO

DB

NK

lab

Con

trol

MA

TRIX

SPIK

E

Det

ecte

dD

etec

ted

Solk

eD

etec

ted

Solk

eD

etec

ted

P01

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugIL

ugIL

Am

ount

%ug

hA

rnou

n%

ug,tn

LA

mou

nt%

uglm

lA

mou

nt%

(ppb

)(p

pb)

ugh

Rec

over

y(p

pb)

ugh

Rec

over

y(p

pm)

uglm

LR

ecov

ery

(ppm

)ug

ImI

Rec

over

y

Dio

xene

ttilo

n0.

400

8.3

ND

9.13

10.0

917.

1110

.071

..

0.40

0N

DN

D9.

4310

.094

8.07

10.0

81

Dio

xath

ion

(cis

)

0.40

0N

DN

D8.

8410

.088

8.22

10.0

82

Dio

xath

ion

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

d%

Det

ecte

dSp

iked

%D

etec

ted

Spik

ed%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

riR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

rnD

unt

Rec

over

y

Nap

htha

lene

9.4

10.0

094

6.77

10.0

066

7.71

10.0

077

7.80

10.0

078

Cer

tifie

dby

:M

icha

elS.

Ban

ner,

Ph.D

BO

NN

ER

AN

ALY

TIC

AL

TEST

ING

CO

MPA

NY

_J

cz

LJ.

__

__

CC

BO

NN

ER

AN

AL

YT

ICA

LT

EST

ING

CM

PAN

Y

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

S!R

AN

CE

DA

TA

DIO

XA

THIO

N!

DIO

XEN

ETII

ION

HPL

CA

NA

YSI

SD

ATA

Clie

ntA

shla

ndC

hem

ical

Col

leC

ted:

12/0

2)20

1013

35C

lient

ISa

mpl

eTy

pe:

Wat

er

Sam

ple

ID:

ASH

-MW

O9-

1202

2010

Ext

ract

ed:

1210

4/20

1008

00V

CT

[.Ex

txac

flon

Met

hod:

SW84

635

10C

File

#10

1204

2-08

Ana

lyze

d:12

115/

2010

0351

OG

Ai:

Ana

lysi

sM

etho

d:M

odifi

edSW

848

Dat

eA

naly

st

SAM

PLE

MET

HO

DB

LAN

KLa

bC

ontro

lM

ATR

IXSP

IKE

Det

ecte

dD

etec

ted

—D

ike

Det

ecte

dD

etec

ted

Spik

e

P01

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ugIL

ugL

Am

ount

%ug

hA

mou

nt%

ugIm

l.A

mou

nt%

ug!m

LA

mou

nt%

(ppb

)(p

pb)

ugh

Rec

over

y(p

pb)

ugIL

Rec

over

y(p

pm)

ugim

LR

ecov

ery

(ppm

)ug

ImL

Rec

over

y

Dlo

xene

thio

n0.

400

ND

ND

9.13

10.0

917.

1110

.071

0.40

06.

6N

D9.

4310

.094

8.07

10.0

81

Dio

xath

ion

(cis

)

0.40

01.

2N

D8.

8410

.088

8.22

10.0

82

Dio

xath

ion

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

ieu

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

rR

ecov

ery

Am

ount

Am

ount

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Nap

htha

lene

8.2

10.0

052

6.77

10.0

068

7.71

10.0

077

7.80

10.0

078

Cer

tifIe

dM

icha

elS.

Bon

ner.

Ph.D

BO

NN

ERA

NA

LY11

CA

LTE

STIN

GC

OM

PAN

Y

00

BO

NN

ER

AN

AL

YT

ICA

LT

EST

ING

CP

MP

AN

Y

QU

AN

TITA

TIV

ER

ESU

LT

SA

ND

QU

ALI

TYA

SSU

RA

NC

ED

ATA

DIO

XA

THIO

N!

DIO

XEN

ETI-

IIO

NH

PLC

AN

4YS

ISD

ATA

Cfl

ent

Ash

land

Chem

ical

Col

lect

ed;

1210

2/20

1014

10C

IIL

Sam

ple

Type

:w

ater

Sam

ple

ID:

ASI

-i-M

WO

B-1

2022

010

Ext

ract

ed:

12/0

4/20

1008

00V

CT

LEx

tract

ion

Met

hod:

SW84

635

100

File

#:10

1204

2-09

Ana

lyze

d:12

115/

2010

0415

OG

AA

naly

sis

Met

hod:

Mod

ified

SW84

6

Dat

eA

naly

st

SAM

PLE

MT

HO

DBL

AN

KL

abC

ontro

lM

ATR

IXSP

IKE

Det

ecte

dSp

ike

Det

ecte

dSp

ike

Det

ecte

dD

etec

ted

Spik

e

PQL

Am

ount

Am

ount

Am

ount

Am

ount

CO

MPO

UN

DS

ug!L

ug/L

Am

ount

%U

p/I

Arn

oun

%up

lmL

Am

ount

%ug

imL

Am

ount

%

(ppb

)(p

pb)

ugtL

Rec

over

y(p

pb)

up/I

Rec

over

y(p

pm)

ugIm

LR

ecov

ery

(ppm

)ug

/mL

Rec

over

y

Dio

xene

tllio

n0.

400

310

ND

9.13

10.0

917.

1110

.071

..

0.40

04.

3N

D9.

4310

.094

8.07

10.0

81

Dio

xath

ion

(cia

)

0.40

060

.1N

O8.

8410

.088

8.22

10.0

82

Dio

xath

lon

(tra

ns)

Det

ecte

dSp

iked

%D

etec

ted

iied

%D

etec

ted

Spik

ed%

Det

ecte

dSp

iked

%

SUR

RO

GA

TE

CO

MPO

UN

DS

Am

ount

Am

ouni

Rec

over

yA

mou

ntA

moe

Rec

over

yA

mou

ntA

mou

ntR

ecov

ery

Am

ount

Am

ount

Rec

over

y

Nap

htha

iene

*35

.910

.00

359

6.77

10.0

068

7.71

10.0

077

7.80

10.0

078

*111

gbsu

rrog

ate

reco

very

due

toIn

terf

eren

ce

Cer

llfi

edb

Mic

hi

S.B

oñnè

r,Ph

.D-

BO

NN

ER

AN

ALY

TIC

AL

TEST

ING

CO

MPA

NY

LJ

L-‘-

— (I)

LI’ z 1) U 0 cc Ui

D z

••E

LL7

UU

YO

UR

CO

MPA

NY

NA

ME:

YO

UR

CO

MPA

NY

AD

DR

ESS

:

NA

ME

OF

PER

SON

TOC

ON

TAC

T:

______

______

CO

NTA

CT

PER

SON

’SPH

ON

E:

_______

CO

NTA

CT

PE

RS

ON

SEM

AIL

:

_________

_______

_____

___________

•L

_1__

L?_

FAX

:

i’jyi’__—

-

BO

NN

ERA

NA

LYTI

CA

LTE

STIN

GC

OM

PAN

Y

2703

Oak

Gro

veR

oad.

Hat

ticsb

urg.

MS

3940

2

Phonc:

(601

)-264-2

854

Fax

:(6

0I )

-26X

-7084

Eid

:hai

coii

i)hat

cu.c

om

WW

W.B

AT

CO

.CO

M

CLI

ENT

PRO

JEC

TN

O.

CLI

ENT

P0,4

CL

IEN

TP

RO

JEC

TN

UM

BE

R

PA

RA

ME

TE

RS

FO

RA

NA

LY

SIS

SA

MP

LE

DE

SC

RIP

TIO

ND

AT

E

LABO

RATO

RYU

SE

TIM

EM

AT

RIX

Turn

Aro

und

Tim

e

Proj

ect N

umbe

r

!oio

iLf

File

ID

4i4

-FP

1-

IZ-c

Vl-

2•

,i..j

/—

iBT

24’

--12)I2ciø

Ii-)I-2r’iø

1055

&if

r4

/I

—BT

3M’

I-

,‘i‘4

4-

,-ct

aI

5’Q

1—

BT

-!4

.c)

Il12.

(D?24

),2-3

)/

—BT

-Z

.--øi-

tøk-

i/

IBT

6A

+-

-zøia

aii

cp

Z-c

p-iaiip

-,I

—BT

-_________

7/4fr141L

-IZ

&24

?(cP

-4I-

2zt

,14

,çj

I—

BT

8j4

i4c

/)

—BT

-ii

-ii_uiu’

ii-ci-

144c

BT

10A

i-t1

i4Z

4)-

IZ

ØI

2ø’Ø

7-O

(-2a

wj

1625

6i-1

/I

BT

SA

MP

LE

CO

LL

EC

TO

R/R

EL

INQ

UIS

HE

DB

Y:

DA

TE

TIM

ER

EC

EIV

ED

BY

:E

LIN

QU

ISI-

IED

B’v

DA

TE

TIM

ER

EC

EIV

ED

BY

:

IIO

Q

ME

TH

OD

OF

SH

IPM

EN

T(I

fA

ny)

RE

LIN

QU

ISH

ED

BY

:D

ATE

TIM

ER

EC

EIV

ED

FOR

BA

TCO

BY:

DA

TE/T

IME

RE

MA

RK

S:

—-

]R

EQ

UE

ST

BA

TC

OT

OD

ISP

OS

EO

FA

LL

SA

MP

LE

RE

MA

IND

ER

S

-

(Sig

nat

ure

)R

EV

ISIO

NN

O1.

2

-

IS

AM

PL

EIS

DE

TE

RM

1NE

DT

OBE

HA

ZA

RD

OU

S,

AM

INIM

UM

AD

DIT

ION

AL

03/2

2/01

ClA

RG

EO

F$30.0

0P

ER

SA

MP

LE

WIL

LB

EA

SS

ES

SE

D.

-fl APPENDIX CCONCENTRATION TREND GRAPHS

0[1

00IL]

VOC CONCENTRATION TRENDS AT MW-08

Hercules Incorporated

Hattiesburg, Mississippi

20,000

18,000 —---——--—------——-———

—-—-——-———--Benzene

16,000 -—

_______

————-— —— —___________

_________

14,000

———-——-

______-___________

_______

12,000 ——-—-

-

-——--—-—-

- —

o.ooo--—-—-

———-—-—--—

_________

8,000 —

_________ _______ _______________

2 :: L

_____

7/

2,000 —\ -

1J 0

— (5.Opg/L)

400

350

______

——Chlorobenzene

300 —---—--

--——--—-———-—

_______——--—---—

250 —______

_______________——-—-—-—--—-—-—————-—-

-

_______

• 200 —-—-——-—

—--—-——--—

—-— —________

150 -—--—---——----

—--—

———---—--—

TRG

100 ——— - (l00tWL)

50 -—-—-—--————-—

—-——-—

—---—

—-•——-------—

-•--

______

0

Page 1 of 3

2,500

2,250

2,000

1,750

1,500

1,250

0.

1,000

0•C) 750

500

250

0

HLO

‘LiH

VOC CONCENTRATION TRENDS AT MW-08

Hercules Incorporated

Hattiesburg, Mississippi

18,000

16,000

14,000

12,000

10,000

j 8,0000.

6,000

E 4,000

2,000

,.‘

——Chloroform

-

[kG(5.0 .tg/L)

TRC(0.155 tgIL.)

Page 2 of 3

VOC CONCENTRATION TRENDS AT MW-08

Hercules Incorporated

Hattiesburg, Mississippi

450

400 -

Toluene

350 ——— ——-—--———--——--—-——-—-——-—-----

_______

—-—--—-——-—______

_____

300-—-—-______

________—

250 —---

___

I, 200 —

—-—-——--—------——---—--——----—

—-—-—_______

J 150

______________——————--—--____ ______ _____________

100

50 -

___________________—---——-—-------—--—-—-

——-

______

0

700

600

__________________________

- Methylene Chlorid[_

500 —_____________________________—

_______________________

400 7/ --

_____

I

0(O ig/L)

——

Page 3 of 3

VOC CONCENTRATION TRENDS AT MW-09

Hercules Incorporated

Hattiesbuig, Mississippi

L\ZZE1ZZLZZZLnZE

40

__ ___

TRG

0

cSv@

Page 1 of 1

VOC CONCENTRATION TRENDS AT MW-13

Hercules Incorporated

Hattiesburg, Mississippi

2,800

_______________________

2,600—Benzene

2,400

2,200

2,000

1,800 —________

______

‘‘ 1,600—-

*2

1,400-

1,200 —----———--—-——-—-—-—----—-———————--—________________ ——---——-—--- —

1,000 —-——--

_______- _________—

—-— —-——— —

E800 ———————

——-—-

_________________________

—____________________

_________________

4,500

I

________

——-Carbon

______

b4,000 —

—-—-

__________

_______

03,500 —————

/

3,000

U

_

____

_______

Cl

_

__

• 1,500 -——-—---—-————--——--______—-———

___________________—

ci 1,000

500 —-———-—- ——-—-

________

Cl -

0r (5.0 Ig/L)

O c;’ ‘

. . .

H

LIci

VOC CONCENTRATION TRENDS AT MW-13

Hercules Incorporated

Hattiesburg, Mississippi

2,000

1.800

1,600—---———--—-— -—--—---—-—---—--—-—_______

1,400

1,200—-

— —-

i,ooo ——--——--—--—————--—————-—-—-——-

__________

0)

800 —-—----—

C) 600

400 —--——-—__________

____________________________________—

_______

200 —

___________________—

TRG

0 - — - - - -I—- - -‘

(0.155 xgIL)

£ ‘

Z0

cici

11L

0Liu

9,000

8,000

7,000

6,000

5,000

4,000

3,000

2,000

1,000

1,400

1,200

1,000

800

0

i: 600

400

200

VOC CONCENTRATION TRENDS AT MW-17

Hercules Incorporated

Hattiesburg, MissLc$ppi

0ço o c? \

.:‘ ‘

., ., .

TRG(5.0 iL)

TRG(100 ig)L)

110

U0UU

Page 1 of 3

VOC CONCENTRATION TRENDS AT MW-17

Hercules Incorporated

Hattiesburg, Mississippi

60,000

—-—Carbon Tetrachioride

50,000 —

—-—---1

o,ooo

,,/\\

________________

30,000

//

_______________

______________________

E 20,000 —j--—--——--—-—--—————-----—

10,000

TRG

0—m—--- (5.OpgJL)

çO ç c? c’ ‘

9,000

5,000 —-——-—-—-—-—-—---—--——

_______

___________________

____________—

0)

4,000

3,000-

2,000 —-

____________________

1,000TRG

0—-———-—-—-——-—-—r (0.lSSpgIL)

c’ c ? c? c’ & ‘

S’ S’

Page2 of 3

VOC CONCENTRATION TRENDS AT MW-17

Hercules Incorporated

Hattiesburg, Mississippi

1,000

900—_________

800

700 ——_____

‘ 600

300 ———--—————-

_____________________

—-———-—-—————---———

200 —

100

0

5? ‘ ‘

‘, .,,

ULiUEl

0H

Page3 of 3

LI

VOC CONCENTRATION TRENDS AT MW-19

Hercules Incorporated

Hattiesburg, Mississippi

70

Benzene

30

________________________

____

20

10 TRG(5.OjigIL)

0ço c’ c’ &

p5.0_

_

_

_

_

——-Choroform

TRG

0.0.

(0.155 Ig/L)

riLi

LiPage 1 of 1

LI