Disclosure to Promote the Right To Information

Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public.

इंटरनेट मानक

“!ान $ एक न' भारत का +नम-ण”Satyanarayan Gangaram Pitroda

“Invent a New India Using Knowledge”

“प0रा1 को छोड न' 5 तरफ”Jawaharlal Nehru

“Step Out From the Old to the New”

“जान1 का अ+धकार, जी1 का अ+धकार”Mazdoor Kisan Shakti Sangathan

“The Right to Information, The Right to Live”

“!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता है”Bhartṛhari—Nītiśatakam

“Knowledge is such a treasure which cannot be stolen”

“Invent a New India Using Knowledge”

है”ह”ह

IS 6552 (1987): straight mineral high demulsibility oils[PCD 3: Petroleum, Lubricants and their Related Products]

IS : 6552 - 1987

Indian Standard SPECIFICATION FOR

STRAIGHT MINERAL HIGH DEMULSIBILITY OILS

( First Revision )

Lubricants and Related Products Sectional Committee, PCDC 4

Chairman Representing

DR P. K. MUKROPADHYAY Indian Oil Corporation Ltd ( R & D Centre ), Faridabad

Members

SRRI J. R. NANDA ( Alternate to Dr P. K. Mukhopadhyay )

DR N. T. BADDI Association of Manufacturers of Petroleum

SHRI S. CHATTERJEE ( Alternate ) Specialities, Bombay

SRRI N. P. BAKHSHI Indian Oil Corporation Ltd ( Marketing Division ), Bombay

SHRI K. K. RAI ( Alternate ) SIIRI M. BHADRA Inter-Plant Standardization in Steel Industry, Sub-

SHRI A. MAZUMDAR ( Alternate ) committee on Oils and Lubricants, IPSS 1 : 9

SRRI M. K. BHAR~AVA Petroleum Re-refiners Association of India, Madras SHRI SHANTILAL DAYA ( Alternate )

SRRI S. R. BHATNAQAR Indrol Lubricants & Specialities Ltd, Bombay SHRI N. SETEURAMAN ( Alternate )

DR K. S. BI~ATACHARYA SHRI S. PANDEY ( Alternate )

Ministry of Defence ( DGI )

SHRI B. K. CRAPRA Central Institute of Road Transport ( Training & Research ), Pune

SHRI T. B. DAS GUPTA Indian Oil Corporation Ltd ( Refinery & Pipelines Division ), New Delhi

SHRI B. N. BANSAL ( Alternate ) CHI~MIST & METALLUROIST-II Ministry of Railways

ASSW~~NT RESEARCH OFFICER ( CHEM-I ), RDSO, LUCKNOW ( Alternate )

Srrnr V. K. DESHPAND~ Srmr K. P. S~HI ( Alternate )

Oil Co-ordination Committee, New Delhi

( Continued on @age 2 )

I @ Copyright 1987

BUREAU OF INDIAN STANDARDS

This publication is protected under the Indian Co&right Act ( XIV of 1957 ) and reproduction in whole or in part by any means except with written permission of the publisher shall be deemed to be an infringement of copyright under the said Act.

c

IS-:6552 -1987

( Continued from page 1 )

Mem hers

SHRI P. K. GOEL

Rcprcscnting

Petroleum Conservation __ -_.. Research Association, New Uelhl

LT GOPAL BHARTI Naval Headquarters, New Delhi SHRI G. C. GWWAMI Assam Oil Division, Bombay

SHRI I. P. BARIJA ( Alternate ) SHRI P. K. GUPTA Hindustan Fertilizers Corporation Ltd, New Delhi SHRI J. D. HARIDAS Tata Engineering & Locomotive Co Ltd, Jamshed-

pur SHRI B. GOSWA~Y ( Altcrnatc )

SHRI H. JAFFREY Petrosil Oil Co Ltd, Bombay SHRI M. A. PAES ( Ahrnatc )

DR G. JAYARAMA RAO Ministry of Petroleum & Natural Gas, Rourkela Steel Plant, Rourkela

SHRI S. S. JHA ( A&rnatc ) SARI 0. K. JUNEJA -Bharat Petroleum Corporation Ltd, Bombay

San1 P. P. NAGAI~KAX ( Alternate ) SHRI S. K. KALE Bhilai Steel Plant, Bhilai

SHI~I J. L. GILOVEI~ ( Alternate ) SHRI R. KULASEKARAN Ministry of_Defence ( DPIN )

SHRI R. N. PADDY ( Ahnate ) SHRI P. MA~UMDAR National Test House, Calcutta

SHRI P. K. CHAKRA~ORTY ( Alternate ) SHRI C. MISHRA Tata Iron & Steel Co Ltd, Jamshedpur

SHRI S. PANIGRAHI ( Alternate ) SHRI S. R. MEHTA Hindustan Petroleum Corporation Ltd, Bombay

SHRI A. B. PAI ( Altdrnate ) SERI J. P. NIGAM Development Commissioner, Small Scale Industries,

New Delhi SHRI J. C. PASRIJA ( Ahnatc )

SHRI M. NIRMAL KUMAR Ashok Leyland Ltd, Madras SHRI S. K. RAJU ( Alternate )

SHRI R. A. RAO Lubrizol India Limited, Bombay SRRI K. L. MALLIK ( Ahrnatc )

SHRI P. K. ROY Indian Oil Blending Limited, Bombay SHRI R. MUEHERJEE ( Aftcrnatc )

SHRI K. SADASIVA CHETTY Madras Refineries Ltd, Madras SHRI E. S. R. RAO ( A&‘?‘n& )

SHRI S. V. SASTRY Automotive Research Association of India, Pune SRRI B. GHOSH ( Alt8rnUtc )

SHRI D. K. SINGH Bharat Heavy Electricals Ltd, Bhopal SHRI R. K. GUPTA ( Alternate I ) SHRI T. R. SUNDERRAJAN ( Ahernatc II )

SHRI SUDHIR SINGHAL Indian Institute of Petroleum, Dehra Dun SHW B. P. PUNDIR ( Ahnat )

Dn R. M. THAKICAII. Gujarat Petrosynrhese Ltd, Bombay SARI N. SU~YANARAYANA ( Ahwtc )

DR P. S. VENKATARAMANI Ministry of Defence ( DMSRDE ) DR R. D. SRIVAST~LVA ( Alt8rnUt8 )

SHRI M. S. SAXENA, Director General, BIS ( Ex-o&o Member ) Director (P & C )

Secretary

SHRI M. A. U. KHAN Joint Director ( P & C ), BIS

( Continued on page 6 )

2

IS:6552- 1987

Indian Standard SPECIFICATION FOR

STRAIGHT MINERAL HIGH DEMULSIBILITY OILS

( First Revision )

0. FOREWORD

0.1 This Indian Standard ( First Revision ) was adopted by the Rureau of Indian Standards on 10 July 1987, after the draft finalized by the Lubricants and Related Products Sectional Committee had been appro- ved by the Petroleum, Coal and related Products Division Council.

0.2 A number of rolling mills turning out accurate profiles are using oil film bearing on the back up and/or on the main rolls. These bear- ings need a high grade bearing oil possessing excellent water separating properties because of the peculiar feature of water contamination which is so common in these systems. This standard was originally issued in 1972 and the same is being revised to align the standard with the latest JPSS standard with a view to enabling the steel plants to procure the right type of material suited to their needs.

0.3 For the purpose of deciding whether a particular requirement of this standard is complied with, the final value, observed or calculated, ex- pressing the result of a test or analysis, shall be rounded off in accor- dance with IS : 2-1960”. The number of significant places retained in the rounded off value should be the same as that of the specified value in this standard.

+

1. SCOPE

1.1 This standard prescribes the requirements and methods of sampling and test for high grade straight mineral high demulsibility oils used on oil film bearings employed in steel mills and other similar applications.

2. GRADES

2.1 The material shall be of nine grades depending on its kinematic viscosity

*Rules for rounding off numerical values ( reuiscd ).

3

IS : 6552 - 1987

3. REQUIREMENTS

3.1 General - The material shall be bright, clear and free from water, clay, dirt or any suspended impurities.

3.2 Composition - The material shall consist of paraffinic base oils having a high chemical stability. Use of viscosity index (VI) improvers is not permitted.

3.3 The material shall also comply with the requirements given in Table 1, when tested according to the appropriate methods prescribed in IS : 1448”. Reference to methods of test in ‘P’ series given in co1 12 of Table 1.

4. PACKING AND <MARKING

4.1 Packing - The material shall be packed in suitable metal containers as agreed to between the purchaser and the supplier.

4.2 Marking - The containers shall be securely closed and marked with the name of manufacturer, name, grade and mass of the material; recog- nized trade-mark, if any; and identification in code or otherwise to enable the lot of consignment or manufacture to be traced back from records.

4.2.1 The containers may also be marked with the Standard Mark.

NOTE - The use of the Standard Mark is governed by the provisions of the Bureau of Indian Standards Act, 1986 and the Rules and Regulations made thereunder. The Standard Mark on products covered by an Indian Standard conveys the assurance that they have been produced to comply with the requirements of that standard under a well defined system of inspection, testing and quality control which is devised and supervised by BIS and operated by the producer. Standard marked products are also continuously checked by BE for conformity to that standard as a further safeguard. Details of conditions under which a licence for the use of the Standard Mark mav be granted to manufacturers or porcessors may be obtained from the Bureau of Indian Standards.

5. SAMPLING

5.1 Representative samples of the material shall be drawn as prescribed in IS : 1447-1966t.

c

*Methods of test for petroleum and its products. tMethods of sampling of petroleum and its products.

4

TABLE 1 REQUIREMENTS FOR STRAIGHT MINERAL HIGH DEMULSIBILITY OILS

SL CHARACTERISTIC No.

( Clause 3.3 )

REQUIRKMENTFOR METHOD OF ~-------____---_ h-_--_-___---__-, TEST,RE~E~

Grade Grade Grade Grade Grade Grade Grade Grade Grade TO IS : 1448* VG 32 VG 46 VG 68 VG 100 VG 150 VG 220 VG 320 VG 460 VG 680

(1) i)

ii) iii)

iv)

v) vi)

u1 vii)

viii)

ix)

(‘4 Kinematic viscosity at 4O”C,

mm2/S

Viscosity index, Min

(3) (4) (5) (6) (7) (8) (9) (10) (11) 28.8 41.4 61.2 90 135 198 288 414 612

3;; 569s 728 1: 16”5 2f:2 3502 56”s 7g

90 90. 90 90 90 80 80 80 80

Total acidity ( mg of KOH per +_-_---_-___-_-O’lO__- -__--_____ ---j g of the oil ), Max

Copper strip corrosion for 3 h at .+ -___ -___-Not worse than No. l___- --_-___---+ 100°C

Pour point, “C, Max c--------__--__ 6 ----_------__-___+ Ash, percent by mass? Max .+--_--_-----__-- o.ooj--_______--_____-, Foaming characteristm

Foaming stability Volume in ml of foam after 10 minutes, Max

a) at 24°C -1 b) at 93°C ) c------ Not limited, but to be reported ---- -------3 c) at 24°C after testing at 93% 1

Flash ( open )

De’Jkibiiit p$ntk~;eveland y at 54 f 1°C ( for

190 190 190 190 200 200 200 250 250

c--- 40 - 37 - 3 ( 20 minutes ) -- + 40-37-3 ( 40 minutes VG 32,46, and 68 ) and at

)

82 f 1°C ( for other grades )

Demulsibility if 82 & 1°C

a) Percent water, MQX + _ ____ --- _______ 1*5----__--- ---__-___3 b) Free water, ml, k&r +-___-_-- --__-__ r_30---_-___-_--___a c) Emulsion, ml, MUX f- -_-_ - -____-_ -_l’O--____._____-_____+

(12) P : 25

P : 56

P:2

P : 15

P: 10 P:4 P : 67

P : 69

P: 91

*Methods of test for petroleum and its products. $Under preparation. Till such time it is published, methods given under ASTM D 2711-1974 may be followed. ti

IS : 6552 - 1987

( Continued jiom page ‘2 )

Turbine, Compressor and Hydraulic Oils Subcommittee, PCDC 4 : 11

COW3lGY

DR S. P. S~VASTAVA

Members

Representing

Indian Oil Corporation Limited ( R & D Centre ), Faridabad

SHRI K. C. JAYAPRAKASH ( Alternate to Dr S. P. Srivastava )

SILBI V. B. AR~RA DR. N. T. BADDI

Associated Engineering Services, New Delhi Association of Manufactures of Petroleum

SHRI S. CHATTERJEE ( Alternate ) Specialities, Bombay

SHEX M. K. BHAR~AVA Petroleum Re-Refiners Association of India, Madras SHRI SHAXYI LAL DAYA ( Altsmatc 1

’ Snar S. R. BH .YTNAGAR Indrol Lubricants & Specialities Ltd, Bombay SHRI N. SETHURAMAN ( Altern& )

SHRI B. K. CIIAPRA Central Institute of Road Transport ( Training &

SIXRI N. C. COATTERJEE DR R. B. DESIIPANDE DIRECTOR oV MINES SAFETY

SHRI D. SA HA ( Alternate ) SHRI HAR~IR SINGH

SHRI A. P. GOEL ( Alternate ) SRRI S. K. JAIN SHRI H. JAFFRXY

SHRI M. A. F’AES ( Alternate ) SHRI S. S. JHA SHRI 0. K. JUNEJA

Research ), Pune National Test House, Calcutta Maruti Udyog Limited, Gurgaon Directorate General of Mines Safety, Dhanbad

Naval Headquarters, New Delhi

Indian Institute of Petroleum, Debra Dun Petrosil Oil Co Ltd, Bombay

Rourkela Steel Plant, Rourkela Bharat Petroleum Corporation Ltd, Bombay \

SHRI P. P. NAGARICAR ( Alternate, SRRI S. R. MIHTA Hindustan Petroleum Corporation Ltd, Bombay

S FTRI P. KRISHNAMOORTHY ( Alternate ) SHRI A. K. MISHRA Bokaro Steel Plant, Bokaro

SHRI M. P. PATHAX ( Alternate ) SHRI S. PANI)EY Ministry of Defence ( DGI )

SHRI A. G. BHATTACHARYA ( Alternate ) SHRI K. K. RAI Indian 0:l Corporation Limited ( Marketing

Division ), Bombay SJ~RI F~TCIRA SINGH ( Alternate )

SHRI V. R~MA~HANDRAN Brakes India Limited: Madras SHRI R. KRISHNAMOOKTHY ( Alternate )

SHRI RANJITIGAI H. R~THOD Swastik Oil Products Mfg Co, Bombay SJTRI S. R. RATHOD ( Alternate )

SHIEI 1’. I~. ROY Indian Oil Blending I,td, Bombay SHV.I S. R. SIII\H ( Afternate)

SHRI B. SANGH.IVI Lubrizol India Ltd, Bombay SHRI R. A. Rao ( Alternate)

SRRI A. SHANTHAlLAM HMT Ltd. Bangalore SHRI D. K. SING11 Bharat Heavy Llectricals Ltd, IIyderahad

SKRI L. PUNU~REEK ( Altdrnate 1 ) SHRI B. S. SXIVASTAVA ( Alternnte II )

SHRI K. B. SI~IVASTAVA Tide Water Oil Co ( India ) Ltd, Calcutta SHRI ,J, NAIX ( Alternate I ) SHRI N. C. MITTAL ( Alternate II )

Dn R. D. SILIVAS’rAVA Ministry of Defence ( DMSRDE ) SHRI RAJENDRA SINGH ( Alternate )

SHRI T. V. VA~~GHESE Madras Refineries Limited, Madras SARI V. K. GOPINATH ( Alternate )

6

L