Disclosure to Promote the Right To Information

Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public.

इंटरनेट मानक

“!ान $ एक न' भारत का +नम-ण”Satyanarayan Gangaram Pitroda

“Invent a New India Using Knowledge”

“प0रा1 को छोड न' 5 तरफ”Jawaharlal Nehru

“Step Out From the Old to the New”

“जान1 का अ+धकार, जी1 का अ+धकार”Mazdoor Kisan Shakti Sangathan

“The Right to Information, The Right to Live”

“!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता है”Bhartṛhari—Nītiśatakam

“Knowledge is such a treasure which cannot be stolen”

“Invent a New India Using Knowledge”

है”ह”ह

IS 11470 (1985): Coconut Oil for Cosmetic Industry [PCD 19:Cosmetics]

IS :11470 - 1985

hdiun Standard SPECIFICATION FOR

COCONUT OIL FOR COSMETIC INDUSTRY

Cosmetics Sectional Committee, PCDC 19 Chairman Represenling

DR S. S. GOTHOS~AR Directorate General of Health Services, New Delhi

Members

SHRI C. D. ANAND Directorate General of Technical Development, New Delhi

SHRI N. K. AG~ARWAL ( Alternate ) ASSISTANT DIRECTOR Food & Drug Administration, Maharashtra State,

Bombay DR P. D. PILA~K.~R ( Alternate )

SHRI B. S. B~RVE Lakme Ltd, Bombay SHRI S. M. SHANBHAG ( Alternate )

DR S. G. BEAT Tata Oil Mills Co Ltd, Bombay SHRI F. E. DARUWALLA ( Alternate )

DR D. CHHIBBA Hindustan Lever Ltd, Bombay SHRI R. GOVERNOR ( Alternate )

SHRI V. G. DESHPANDF. Hindustan Ciba-Geigy Ltd, Bomhay DR S. S. KAR~IARKAR ( Alternate )

DR A. S. DIVATIA Consumer Educatiou and Research Centre, Ahmadabad

KUMARI RANI ADVA~I ( Alternate ) SHRIMATI T. JACOB Lady Irwin College, Nrw Delhi S HRI P. MAZUMDAR National Test House, Calcutta

SHRI P. K. CHAKRABORTY ( Alternate ) SHRI R. C. MEHT.~ Drugs Control Administration, Government of

Gujarat, Ahmadabad SHRI J. P. GANATR A ( Alternate )

SHRI A. MINHAZUDDIN Millet Rochas Pvt Ltd, Madras KUMARI NASRIN BEGAM ( Alternate )

SHRI S. M. MODY DR S. S. NISHAT

Johnson &Johnson Ltd, Bombay Hygienic Research Institute, Bombay

SHRI KAILASH S. CH~ABR,~ ( Alternate ) DR S. G. PATNERAR Perfumes & Flavours Association of India, Bombay

SHRI SCDHIR J AID ( Altert~atc ) SHRI K. S. RAO Swastik Household and Industrial Products Pvt Ltd,

Bombay ( Alternate ) SHRI C. R. KRISHNAD~OORTHY

( Continued on page 2 )

@ Copvright 1986

INDIAN STANDAR~DS INSTITUTION

This publication is protected under the Indian Copyright Acf ( XIV of 1957 ) and reproduction in whole or in part by any means except with written permission of the publisher shall be deemed to be an infringement of copyright under the said Act.

IS : 11470 - 1985

( Continued from page 1 )

A4embers Refiresenting

SHRI A. c. ROY Indian -Soap and Toiletries Makers Association, Bombay

DR S. K. ROY Central Drugs Laboratory, Calcutta DR A. C. DAS GUPTA ( Alternate )

?&RI P. ROY Bengal Chemical & Pharmaceutical Works Ltd, Calcutta

DR A. N. BASU ( A[ternatc ) SHRI V. SITARAM Basic Chemicals, Pharmaceuticals & Cosmetics

SHRI I. SUNDARICSN ( Alternate ) Export Promotion Council, Bombay

SHRIMATI USRA SUKTHANEAR Consumer’s Guidance Societv. Bombav , I SHRIMATI USHA KAMERKAR ( Alternate )

SHRI M. S. THAKUR Godrej Soaps Ltd, Bombay Srrlt~ N. G. IYER ( Ahmzatc )

SHRI M. S. SAXFN.4, Director General, ISI ( Ex-o&o Member ) Director ( P & C)

Secretary

( DR ) SHRIMATI VIJAY MALIK Assistant Director ( P & C ), IS1

Raw Materials and GRAS List Subcommittee, PCDC 19 : 1

Conuener

DR G. L. MZDN

Members

Shaw Wallace & Co Ltd, Calcutta

ASSISTANT C o M ICI I s s 1 o N E n Food & Drug Administration, Maharashtra State, ( COSMETICS ) Bombay

Se~ron SCIENTIFIC OFFICEI% CLASS I ( cmiv ) ( Alternate)

SHRI B. S. BARVE Lakme Ltd, Bombay SHRI S. M. SHANB~AQ ( Alternate )

DR S. G. EHAT Tata Oil Mills Co Ltd, Bombay S~IRI F. E. DARUWALLA ( Alternate )

SRRI D. GIIHIBB.4 Hindustan Lever Ltd, Bombay SRRT R. GOVERNOX< ( Ahernate )

SHRI V. G. DBSHPANDE Hindustan Ciba-Geigy Ltd, Bombay SHI~J J. P. G_ZNATRA Drug3 Control Administration, Gujarat State,

Ahmadabad SHRI R. D. DEO~XA~ ( Alternate )

SHRI S. M. Moov Johnson & Johnson Ltd, Bombay SHRI S. D. PARANJAPE ( Alternate )

SHRI K. S. Rao Swastik Household & Industrial Products Pvt Ltd, Bombay

SRRT C. R. KI~~SHXAMOORTHY ( Alternate ) SRRI V. R. RATHI Sudershan Chemical Industries Ltd, Pune

SHRI U. N. LIXAYE ( Alternate )

( Continued on page 8 )

COCONUT

IS : 11470 - 1985

Indian Standard SPECIFICATION FOR OIL FOR COSMETIC INDUSTRY

0. FOREWORD

0.1 This Indian Standard was adopted by the Indian Standards Institution on 15 October 1985, after the draft finalized by the Cosmetics Sectional Committee had been approved by the Petroleum, Coal and Related Products Division Council.

0.2 IS : 542-1968* covers a number of grades of coconut oil used in a variety of industries. The present standard has been drawn up speci- fically to cater to the needs of the cosmetic industry.

0.3 Both the types of oil expressed and solvent extracted, are covered in the present standard. All other changes considered necessary to align the standard with others in the series for raw material and finished cosmetic have been included.

0.4 For the purpose of deciding whether a particular requirement of this standard is complied with, the final value, observed or calculated, expre- ing the result of a test or analysis, shall be rounded off inaccordance with IS : 2-19607. The ~number of significant places retained in the rounded off value should be the same as that of the specified value in this standard.

1. SCOPE

1.1 This standard prescribes the requirements and the methods of sampling and test for coconut oil used for cosmetic industry.

2. TYPES

2.1 The material shall be of two types, namely:

Type 1 - Refined oil, and

7-_ype 2 --Raw expeller oil.

*Specification for coconut oil ( second reoisinn )_ .fRules for rounciing oTf numerical values ( wised ).

3

IS : 11470 - 1985

3. REQUIREMENTS

3.1 Description

3.1.1 Type 1 - The material shall be coconut oil obtained from clean and sound copra ( Cocos nucifera Linn., fam. Palmae ) or good quality copra cake by a process of expression or solvent extraction using solvent hexane conforming to IS : 3470-1966*. The oil shall have been refined by neutralisation with alkali, bleached with bleaching earth or activated carbon or both, and deodourised with steam. The oil shall be practically odourless or have a very mild odour characteristic of coconut oil.

3.1.2 Type 2 - The material shall be the genuine coconut oil obtained from clean and sound copra ( Cocos nucifera Linn., fam. Palmae ) by a process of expression. The oil shall have the characteristic odour of coconut oil.

3.2 The material shall pass the clarity test as given in Appendix A. The material, when tested as prescribed in Appendix A, shall have a turbi- dity value ( in terms of silica units ) not more than 10.

3.3 Admixture with Other Oils - The material shall be free from admixture with other oils when tested according to the methods prescri- bed in IS : 548 ( Part 2 )-1976t.

3.4 The material shall also comply with the requirements given in Table 1.

4. PACKING

4.1 The material shall be supplied in suitable well-closed containers which do not deteriorate the product, in quantities as agreed to between the purchaser and the supplier.

5. MARKING

5.1 The container shall be marked w-ith the following:

a> b) C)

4 e)

Name and type of the material;

Manufacturer’s name and/or his recognized trade-mark, if any;

Net mass of the material in the containers;

Month and year of manufacture; and

Code number to enable the lot of manufacture to be traced back from records.

*Specification for hexane food grade. thlethods of sampling and test for oils and fats: Part 2 Purity tests ( third revision ).

4

IS:11470 - 1985

SL NO.

(1)

i)

ii)

iii) iv) v)

vi)

vii) viii)

ix)

x)

xi)

TABLE 1 REQUIBEMENTS FOR COCONUT OIL FOR COSMETIC INDUSTRY

( Clauses 3.4 and 7.1 )

CH.-\RACTERISTICS

(2) Moisture and insoluble impuri-

ties, percent by mass, Max Colour in a 1” cell on the lovi-

bond scale, expressed as Y + 5R, not deeper than

Refractive index at 40°C Relative density at 30”/3O”C Saponification value, Min Iodine value ( Wij’s )

Acid value, Max Unsaponifiable matter, per-

cent by mass, Max Polenske value, Min

Flash point ( Pensky Marten ) ( closed ), “C, Min

Test for rancidity

REQUIREMENTS FOR ~~~~~h~~_~~

Type 1 Type 2

(3) (4)

0’1 0.2

2 10

1.448 0 to 1’449 0 0.915 to 0.920 250 250 7.5 to 7.5 to

10.0 10.0 0.5 2.0 0.5 0.8

13.0 13.0

225 -

shall be free from rancidity

METHOD OF TEST, REF TO CL No.

(5)

5 and 6j 13 j

I 10 / 0f 1s : 11 ;548 15 , ( Part I )- 14 1 1964’

81 i

13J P : 21 of IS : 1448t Appendix B

*Methods of sampling and test for oils and fats: Part 1 Sampling, physical and chemical tests ( revised ).

tMethods of test for petroleum and its products: P :21 Flash point ( closed ) by Pensky-Marten apparatus (first rcoision ).

5.2 In addition, words ‘NOT FOR DIRECT EDIBLE CONSUMP- TION’ ( either printed on the label affixed to the container or lithographed or stencilled thereon with indelible ink ) in a type size of not less than 50 mm shall be marked.

5.2.1 The containers may also be marked with the IS1 Certification Mark.

Nrr~a: -- The use of the IS1 Certification Mark is governed by the provisions of the indian Standards Institution ( Certification Marks ) Act and the Rules and Regu- lations made thereunder. The IS1 Mark on products covered by an Indian Standard conveys the assurance that they have been produced to comply with the require- ments of that standard under a well-defined system of inspection, testing and quality control which is devised and supervised by IS1 and operated by the producer. ISI marked products are also continuously checked by ISI for conformity to that standard as a further safeguard. Details of conditions under which a licence for the use of the ISI Certification Mark may be granted to manufacturers or processors, may be ob:ained from the Indian Standards Institution.

5

IS:11470 -1985

6. SAMPLING

6.1 Representative samples of the material shall be drawn as prescribed under 3 of IS : 548 ( Part 1 )-1964*.

7. TESTS

7.1 Testsshall be carried out as prescribed in IS : 548( Part 1 )-1964* and P:21 of IS : 1448-1970t. Reference to the relevant clauses of these standards is given in co1 5 of Table 1.

7.2 Quality of Reagents - Unless specified otherwise, pure chemicals and distilled water ( see IS : 1070-1977: ) shall be used in the tests.

NOTE - ‘Pure chemicals’ shall mean chemicals that do not contain impurities which affect the results of analysis.

A

DETERMINATION

A-l. TERMINOLOGY

PPENDIX A ( Clause 3.2 )

OF TURBIDITY OF SILICA SCALE

A-l.1 For the purpose of this test, the following definition shall apply.

A-1.1.1 Silica Scale Unit - Turbidity imparted by 1 mg of fullers’ earth when suspended in 1 000 ml of distilled water.

A-2. PREPARATION OF TURBIDITY STANDARDS

A-2.1 Mix slowly with constant stirring 5,000 g of fullers’ earth, previously dried and sieved through 75 pm IS sieve [see IS : 460 ( Part 1 )- 19785 ] with distilled water and dilute it to 1000 ml. Agitate intermitte- ntly for one hour and then allow to stand for 24 hours. Withdraw the supernatant liquid without disturbing the sediment Evaporate about 50 ml of the removed liquid, dry the residue at 105” &- 2°C and weigh the residue to determine the amount of clay in suspension. Prepare turbi- dity standards with this standardized stock suspension with distilled water. A drop of saturated mercuric chloride solution may be added as preservative. The standards are stable for 3 months.

*Methods of sampling and test for oils and fats: Part 1 Sampling, physical and chemical tests ( revised ).

+Methods of test for petroleum and its products: P:21 Flash point ( closed ) by Pensky-Marten apparatus (jirst revision ).

ISpecification for water for general laboratory use ( second revision ), $Specification for test sieves: Part 1 Wire cloth test sieves ( second r&ion ).

6

IS:11470-1985

A-3. PROCEDURE

A-3.1 Pour the sample after thorough shaking into a clear glass bottle of suitable capacity, say, one litre. Compare it -with the turbidity standards contained in similar bottles, holding them against a suitable background and using a source of light which illuminates them-equally and is to be placed in a Dosition that no rays reach the eye directly. The sample and the standards shall be shaken simultaneously immediately before comparison.

A-3.1.1 Report - Record the turbidity readings inthe range 1 to 10 to the nearest unit and in the range 11 to 100 to the nearest 5 units.

APPENDIX B [ Table 1, Item (xi) ]

B-l. TEST FOR RANCIDITY

B-l.1 Reagents

B-1.1.1 Phloroglucinol Solution - IXsscJve 0.1 g of phloroglucinol in 100 ml of diethyl ether.

B-1.2 Procedure - Shake 10 ml of the material, melt if necessary, with 10 ml of concentrated hydrochloric acid and 10 ml of phloroglucinol solution. Shake for 1 minute.

B-1.2.1 The material shall be taken have passed the test if no pink colour develops.

IS:11470 -1985

( Continued from page 2 )

Members Representing

DR S. K. ROY Central Drugs Laboratory, Calcutta DR A. %. DAS GUPTA ( Alternate )

DR M. P. SAHAKARI Italab Pvt Ltd, Bombay SHRI M. R. PAREKH ( Ahmate I ) SHRI K. S. SANTHANAM ( Alternate II )

DR N. D. SHAH Geoffrey Manners & Co Ltd, Bombay DR M. M. DOSHI ( Alternate )

SERI NAVINCEANDRA R. SHAH Devarsons Pvt Ltd, Ahmadabad SHRI VINODCEIANDRA K. MEHTA ( Alfrmate )

SHRI M. S. TH~KUR Godrej Soaps Ltd, Bombay SRRI N. G. IYER ( Alternate )

8