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है”ह”ह

IS 10672 (1983): Mineral Mixtures for Supplementing Sheepand Goat Feeds [FAD 5: Livestock Feeds, Equipment andSystems]

IS : 10672 - 1983

Indian StandardSPECIFICATION FOR

MINERAL MIXTURES FORSUPi4tEMENTING SHEEP AND GOAT FEEDS

UDC 636·087·72:636·32/·39

J5i'

© Copyright 1984

INDIAN STANDARDS INSTITUTIONMANAK BHAVAN, 9 BAHADUR SliAH ZAFAR MARG

NEW DELl-II 110002

Gr 3 Febrl101Y 1984

IS : 10672 • 1983

Indian StandardSPECIFICATION FOR

MINERAL MIXTURES FORSUPPLEMENTING SHEEP AND GOAT FEEDS

Animal Feeds Sectional Committee, AFDC IS

Chtlirman

DR O. N. SINGH

Representing

Ministry of I Agriculture (Department or Pood ],New Delhi

Member.,

DRS. L. ANAOICAR Godrej Soaps Limited, BombayDR G. P. MITHUJI ( Alternate)

DR S. P. ARORA Indian Council of A.riculture Research,NewDelhiDR C. S. BARSAUL C.S.A. University of Agriculture and Technology,

MathuraDR K. M. SHARMA ( Alternate)

SHIU M. K. DATI'ARAJ Roller Flour Millers' Federation of India,New Delhi

SmuK. B. TRIAOAIWAN ( Alternate)DR P. J. GIORGI KUN.JU National Dainr Development Board, AnandDR A. N. GHOSH Animal Husbandry Commissioner (Ministry of

Aariculture), New DelhiSRRI S. S. CHaIRBD ( Alternate )

DR S. S. GILL Punjab Aariculturo University, Ludhiana8HRI M.S. GODllBI Tho Compound Livestock Feeds Manufacturers'

Association of India, Bombay8"-1 VINBBT VII.MANI ( Alternate)

DR GOPAL KRISHNA Haryana Apicultural University, HissarDRM. G. JACUON Govind BallabhPant University of Aariculture and

Technology, Pant NaprDa M. L. VBRMA ( Alternate)

Da ~AR NATR Indian Veterinary R.esearch Institute (leAR),mtnapr

Da D. C. JOSHI ( Alternate)DR K1USHAN KUMAR Directorate General of Technical Development,

New DelhiDa V. D. MtJDOAL NatiolUll Dairy Rellarch Institute (ICAR.), Kamal

D.B.N.GU"A(AhuM~)

( Co"ti".d Oil JJtl8e 2 )

C> Copyrilht 1984INDIAN STANDARDS INSTITUTION

This PUbUcatiOD il protected under the Indian Copyright Act (XIV of 1957 ) andreproCluctioD in whOle or in part by any means except with written penni.ion ofthepubUaher &ball bedeemed to be an infriulcment of copyriaht uader the said Act.

IS : IM'72 • 1983

( Continued from pale 1 )

Da D. V. RANONIKAR

SHIU G. V. 51RUKDR K. SRINIVASAN

DRS. V. VAIDYA (Alter.'.')SaRI T. S.TAMBOLIA The °Mabarashtra . Agro-Industries Development

CorporatioDt Limited, BombayDRS.M.~NALKAR(Ahenwu)

SSRI VINEIT VIRMANJ Jawala Flour MiDs, New DelhiSHRJ ANAND VIRMANI ( AI"'lItIte )

SHRI T. PuaNANANDAM, Director Oeneral~ lSI ( Ex-officio MemHr)Director ( Api a foOd )

Members RepresentingDRS. M. PATEL All India CottonseedCrushers' Association, Bombay

SRaI K. M. PAl ( Alternate) .Da B. C. PIlTNAYAK central Sheep and Wool R.eaearch IDatitute (leAR),

• ~thuDR MANOHAa SINOR ( Alter.t. ) ,

DRD. V. R. PRAKASH RAo LVR Peeds & Minerals Pvt Limited, MadrasSHRI L. R. SIVAPRASAD (Alt,rnate)

DRN. S. RAJAOOPAL Directorate of Vanaspati, Vegetable Oils and Fats( Ministry. of Aaraculture )

Bhartiya Agro-Industrial Foundation, UruliKanchan (.Pune )

DR A. L. JOSHI ( AlterMt' )DR V. R. SADAOOPAN Central AviaaResearch Institute (leAR), lzat~arDR (SHllIMATI) C. K. SAROJINJ • ~ Kaira District Co-operative Milk Producers' Umon

Ltd, AnandDRN. SATAPATHY Tata Oil Mills Co Limited, Bombay

DRS. S. CHHABRA ( Alterna', )BRIO A. S. SBKHON Directorate of Military Panns, Army Headquarters

( Ministry of Defence)81m1 R.. IC. TR.IPATRI( AIt,rntl")

SaRIG. S. SHUKLA Directorate of MarketiDI and Inspection (Ministryor Rural Development)Da S. JAYARAMAN ( Alt,rMt, )Ll

DR P. C. SHUKLA Institute of Agriculture, GUjarat AariculturalUnivenity, Anand

Solvent Extractors Association or India, BombayHindustaD. Lover· Limited, Bombay

Secretary

SRRI LAJINDIR SINGH

Deputy Director ( Alii 4 Food ), lSI

Animal Feeds and Mineral Mixtures Subcommittee, AFDC IS:2

CO",••,

DRS. P. AltoM Indian Councilor Apiculture Research, NewDelhi

( eo"tl".d on JHlI. 11 )

2

AMENDMENT NO. 1 JANUARY 1988

TO

IS: 10672-1983 SI)ECIFlCATION FOR MINERAL MIXTURESFOR SUPPLEMEN'rING SllEEP AND GOAT FEEDS

(Page .10, clauses 8-S.1 and B-5.1.1)Substitute 'R' for 'X'. wherever occurs.(AFDC 15)

Reprography Unit, BIS, New Delhi, India

AMENDMENT NO.2 JULY 1995TO

IS 10'72: 1983 SPECIFICATION FOR MINERALMIXTURES FOR SUPPLEMENTING SHEEP AND

GOAT FEEDS

(Page 6, clause S.z, line 2 ) - Sumtitute 'IS 1070 : 1992' for 'IS: 1070 •19n' and in abe correspOnding Ioot-note, substitute 'Reagentgrade wiler (thirdrevision)' for the existing COol-note.

(FADS)Repro&rapby Unit, BIS,New Delhit ladia

AMENDMENT NO. 3 AUGUST 1'"TO

IS 10672: 1983 SPECIFICATION FOR MINERALMIXTURES FORSUPPLEMENTING SHEEP AND GOAT

FEEDS(Ptlge 6, Appe"dix A, clauseA-I) - Delete 'Bone-meal (sterilized)

( conforming to IS: 1942 -l968t)' Ind 'Calcined bone-meal'.

( Page 6,lootllottwith ct' mark)- Delete.

(FADS)Reprography UBi.. 815, New Delhi, Jndia

IS : 10672 • 1983

Indian StandardSPECIFICATION FOR

MINERAL MIXTURES FORSUPPLEMENTING SHEEP AND GOAT FEEDS

o. FOR E W 0 R 0

0.1 This Indian Standard was adopted by the Indian Standards Institutionon 30 September 1983, after the draft finalized by the Animal FeedsSectional Committee had been approved by the Agricultural and FoodProducts Division Council.

0.2 Mineralshave many vital functions in the body and the vital processesin a living organism are dependent on the presence of the various mineralsalts in proper proportion. In view of the vital role of minerals, to ensureoptimum health and productivity in livestock, it is essential to provideminerals, wherever necessary, in adequate quantity and proportion. It has,therefore, become a sound animal husbandry practice to incorporate therequisiteminerals in the feed ration of animals by the addition of a mixtureof different substances containingthese minerals. It is expected that thisstandard willassist in the manufactureof a mineral mixture of the requiredquality for supplementing sheepand goat feeds.

0.3 The mineral mixture may be fed. on an average, at the rate of 3percent of the concentrate mixture under normal feeding conditions. It isexpected that farmer will add the required amount of common salt inmineral mixture to ensure growth and milk production in animals.

0.4 For the purpose of deciding whether a particular requirement of thisstandard is complied with, the finalvalue, observed or calculated, express­ing the result of a test or analysis, shall be rounded off in accordance with18:2-1960·. The number of significant places retained in the rounded offvalue should be the same as that of the specified value in this standard.

1. SCOPE

1.1 This standard prescribes the requirements and the methods of samplingand test for a mineral mixture for supplementing sheepand goat feeds.

-Rulesfor roundinl off numerical values ( rlvlsed ).

3

IS : 10672 • 1983

2. REQUIREMENTS

2.1 ~ats - Anyof the ingredients Biven in Appendix A shallbeusedfor the preparation of mineral mixture. All insredients used shall be of aquality suitable for animal consumption and shall contain no substancesharmfulto goat and sheep•.

2.2 Delcrlptlol- The mineral mixture shall be in the form of a freeftowina powder, thoroughly mixed and completely homogeneous, It shallhave been groundto such fineness that not less than 70 percent by mass ofthe material shall pass through 106.micron IS Sieve [see IS:460(Part 1)­1978* ].

2.3 The mineral mixture shall be free from adulterants, insect or visible(unlus infestation and undesirable odour.2.4 Mineral mixtures shall alsoconform to the requirements given inTable 1.

2.4.1 Mineral mixtures shall also be free from spores of Bacillusanthracls, Clostridium sp. when tested by method described in 4, 5 and 6 of18:7874(Part 3 )-197St.

3. PACKING AND MARKING3.1 PaeldDl- The material shall be packed in moisture-proof bags. cartonboxes or arums. All containers shall be sound, clean and free fromcausal agents of infections diseases and parasites.

3.2 Marklnl - Each container shall be marked or labelled giving thefollowing information:

a) Name of the material,b) Nameof the manufacturer,c) Batchor code Dumber,d) Net massof contents, ande) Date of manufacture.

3.2.1 Each container shall also have on it the following information.This may also be done by enclosing in each container a leaflet giving thefollowiDI information:

a) Name of the material,b) Insredients,c) Guaranteed composition, andd) Directions for use (the quantity of salt required to be added

before use shallbe inClicatecl )•

•Speciflcation for test sieveS: Part 1 Wirecloth test sieves ( '_COM ,.",1011 ).tMethoda of tests for animal feeds and feediD, std,: Pan 3 Microbiolo.ical

mitbodI.

4

IS : 10fi71·1983

TABLB I REQUIREMENTS I'OR MINERAL MIXTURE I'oaSUPPLEMENTING SHEEP AND GOAT FEEDS

( Clause 2.4 )

SL CHARACTERISTICNo.

RIQ'UlJl8.MENT

METHOD0' TEsT, REF TOCL No. OF

~

(1) (2)

i) Moisture, percent by mass, Max

ii) Calcium (u Ca), percent bymass, Min

jii) Phosphorus (as P), percent byma~, Min

iv) Iron, percentby mass, Min

V) Iodine(as KI), percent by mass,Mill

vi) Copper,percentby mass, Min

vii) Manpnese. percent by mass,Min

viii) Cobalt, percent by mass, Min

ix) Fluorine,percentby mass, Max

x) Zinc, percent by mass, Min

xi) Acid insoluble .h, percent bymass, Max

xii) Sulphur, percentby mus, Min

(3)

S

30

14

oss0'35

0-03

0-08

0'13

(4)

4

10

s

6

7

8

9

10

11

12

13

(6)

A.]

NOTB - The value. specified for characteristics (ii) to (xii) are aD moisture-freebasis.

-Methods of tests Cor animal feeds and reeding stuffs: Part 1General methods.tMethods of tests for animal feeds and feedina stuffs: Part 2 Minerals and trace

elements.:SpeciflcatioD tor limestone for chemical industry(first ,evialon ).

s

IS : 10672-,.

3.2.2 Each container may also be martc:ed with the lSI CertificationMark.

Non - The use o( the lSI Certiflcation Mark is aovemed by the ~rovilionsof the Indian Standards Institudon (CertiftcatioD Marks) Act and the Rulesand RcaulatioDS made thereunder. Tho lSI mark on prOducts covered by aDIndian Standard conveys the ..uranee that they have been produced to complywith the requirements of that standard under a WeD-defined system of inspectiontestiDa and quality control which is devised and supervised by lSI and o~tedby the producer. lSI marked produetl are also continuously checked by lSI forconformity to that standard as a further safepard. Details of conditions underwhich a licence for the use of the lSI Certification Mark may be aranted tomaunfacturers or processors, may be obtained from the Indian StandardsInstitution.

4. SAMPLING

4.1 Representative samples of the materia) for testing conformity to tbisspecification shall be drawn according to the method prescribed inAppendix B.

s, TESTS

5.1 Tests shall be carried out as prescribed in 2.4.1 and the relevantappendicesspecified in col 4 and Sof Table 1.

5.2 QuaUty 01 ReapDt! - Unless specified otherwise, pure chemicals anddistilled water ( seeIS: 1070.1977*) shall be employed in tests.

NorB- 'Pure chemicals' shall mean chemicals that do Dot contain impurideswhich affect the results of analysis.

APPENDIX A

( Clause 2.1 )

INGREDIENTS FOR MINERAL MIXTURES

A-I. The folJowing ingredients shall be used for compoundin. mineralmixtures for supplementing sheep and goat feeds:

Bone-meal (sterilized) (conforming to IS: 1942.1968f)Calcined bone-mealChalk ( calcium carbonate)Common salt

.SpeciftcatiOD for water for aenerallaboratory use ( second r"I,lo1l ).tSpeci8ca&ioA for bone..lDII1u Uveatoek feed IUpp1emeDt (/it'st ,.,1.. ).

6

IS : 10m • 1983

Dicalcium phosphatePotassium iodide or potassium iodateSodium carbonateSodium thiosulphateStarchYellow or red oxide of ironManganese sulphateCopper sulphateCobalt chlorideCobalt sulphateZinc chlorideZinc sulphate

APPENDIX 8

( Clause 4.1 )

SAMPLING OF MINERAL MIXTURE FOR SUPPLEMENTINGSHEEP AND GOAT FEEDS

B-1. GENERAL REQUIREMENTS OF SAMPLING

8-1.0 In drawing, preparing, storing and handling test samples, thefollowing precautions and directions shall be observed.

8-1.1 Samples shall be taken in a protected place, not exposed to dampair, dust or soot.

8-1.3 The samplinginltrument shall be clean, dry and sterile. .

8-1.3 Precautions shall be taken to protect the samples, the material beingsampled, the samplina instrument and the containers for samples fromadventitious contamination.

B-l.4 The samples shall be placed in clean, dry and sterile glass containers,The samplecontainersshall be of such size that they are almost completelyfilled by the sample.

8-1.5 Each container shall besealed air-tight after filling and marked withfull details of sampling, date of sampling, date of manufacture, batchDumber, name of the manufacturer, and other important particulars of theconsilnment.

7

IS : 101i72 • 1983

B-l.6 Samples shall be stored in such a mannerthat the temperature of thematerialdoes Dot vary unduly-Crom the Dormal temperature.

B-I.7 Sampling shallbe done by a penon agreed to between the purchaserand the vendorand in the presence of the purchaser ( or his representative)and the vendor ( or his representative ).

B-2. SCALE OF SAMPLING

a-Zel Lot - All the containers in a single consignment of. tbe materialdrawn from a single batch of manufacture shall constitute a lot. If aconsignment is declared to beconsisting of different batchesof manufacture,the batches shall be grouped separately and the containers in each groupshall constitutea separate lot.

B-2.1.1 Samples shall be tested for each Jot for ascertaining conformityof the material to the requirements of this specification.

8-2.2 The number of containers to be selected from a lot shall depend onthe size of the lot and shall be in accordance with col 1 and 2 of Table2.

TABLE 2 NUMBER OJ' CONTAINERS TO BESELEOTED FOR SAMPLING

Lor SIZE NUMBER O. CoNTAINERS TO BESELICTID 'OR SAMPLING

N

(1)

2 to 1516 to 4041 to 65

66 to 110

III to 250Over 250

n

(2)

2

3

4

5

7

10

8-2.3 The containers to be selected for samplina shaD be chosenat randomfrom the lot and for this purpose a random number table (see IS: 4905­1968.) as agreed to between the purchaser and the vendor shall beused. If such a table is Dot availatile the following procedure shall beadopted:

StartiDg from any container count I, 2. 3, etc, up to , and so ODeEvery rth container shall be withdrawn from the lot to live a.m~efur~R, '

-Methods of raDdom sampUn.. _

8

IS: 10672 • 1983

where

Nr == n'

N being the number of containers in the lot and n the number ofcontainers to be chosen according to Table 2. If r comes out to bea fractional number, its value shall be taken to be as equal to itsintegral parts.

B-3. TEST SAMPLES AND REFEREE SAMPLES

B-3.1 Pre,aradoD of Individual Samples - Draw with an appropriatesampling Instrument equal quantities of the material from different parts ofeach container selected according to Table 2. The total quantity ofmaterial drawn from each container shall be not less than I'S kg. Mix allthe portions of the material drawn from the same container thoroughly.Take out about 0'75 kg of the material and divide it into three equal parts.Each portion thus obtained shall constitute the test sample representingthat particular container and shall be transferred immediately to clean anddry containers and sealed air-tight. These shall be labelled with theparticulars given in 8-1.5. The individual samples so obtained shall bedivided into three sets in such a way that each set has a test samplerepresenting each container selected. One of the sets shall be for thepurchaser, another for the vendor and the third as the referee sample.

11-3.2 Prep.ratioD of Composite Samples - From the mixed material fromeach selected container remaining after the individual samples have beentaken, equal quantities of the material from each container shall be takenand mixed together so as to form a composite sample weighing not lessthan 0·75 kg. This composite sample shall be divided into three equalparts and transferred to clean and dry containers and labelled with theparticulars given in 8-1.5 and sealed air-tight. One of these samples shallbe for the purchaser, another for the vendor and the third as the refereesample.

B-3.3 Referee Samples - Referee samples shall consist of a let of testsamples ( see B-3.1 ) and composite samples ( see 8-3.%) and shall bear theseals of the purchaser and the vendor and shall be kept at a place agreed tobetween the two.

8-4. NUMBER OF TESTS

8-4.1 Tests for calcium shall be conducted individually on each of thesamples constituting the set of test samples ( seeB-3.1 ).

8-4.2 Tests for remaining characteristics specified in 2.4 shall be conductedon the composite samples ( see8-3.2 ).

9

IS : 10672 • 1983

B-5. CRITERION FOR CONFORMITY

8-5.1 Calclam CODteDt - Bach of the test results on individual samples forcalcium content shall be recorded. The mean ( g ) and range ( R) of tbetest results shall be computed as given below:

Sum of the test resultsMean (g) == Number of the test samples

Range ( R) = Difference between the maximum and the minimumvalues of the test results.

8-5.1.1 The lot shall be considered as satisfying this requirement if theexpression ( g -0·4 R) is greater than or equal to 30.8-5.2 The lot shall be declared as conforming to the requirements of thisspecification, if 8-5.1 is satisfied and all the test results on the compositesample satisfY the remaining requirements as given in this specification.

10

IS : 10672 • 1983

( COIItl"IItd/rom JHlIt 2)

M,mbtrs RepresentingSIIRI M. K. DATI'A-RAJ Mysore Feeds Private Limited, Bangalore

SHRI M. K. PANDURANOA SE1TY( Alternate)

Da S. S. GILL Punjab Apicultural Univenity, LudhianaDIl M. G. JACUON Oovind BaUabh Pant University of Aariculture and

TechnololY, NainitalDa M. L. VUMA ( A/terlltlte )

DR T. S. JOHRI Central Avian Research Institute (leAR.), lzatnaprDIt A. K. SRIVASTAVA ( Alternate)

DRD. C. JOSHI Indian Veterinary Research Institute (leAR),lzatnagar

DR S. S. NEGI ( Alternate)DR T. B. MIIlCHANDANI AriesAgro.Vet Industries Private Limited, Bombay

DIl JIMMY MmCHANDANI ( AI,ernate )DR V. D. MuooAL NationalDairy Research Institute(leAR), Karnal

DaB.N.GunA(Ahunak)Da B. C. PATNAYAIC Central Sheepand Wool Research Institute (ICAR),

RajasthanDR MANOHAIl SINOH ( Alternate)

DR S. P. PllADICB Animal Husbandry Department, loneDRD. V. R. PRAKASH RAo LVR Feeds It Minerals Private Limited, Madras

SHRI L. R. SIVAPRASAD ( Alternate)DR S. K. SAlUtAa AnImalFeeds Manufacturers' Association of Eastern

India, CalcuttaDR (SHlUMATI) C. IC. SAROIINI Kaira District Co-operative Milk Producers' Union

Ltd, AnandDa N. SATAPATRY Tata Oil Mins Company Limited, Bombay

DR S. S. CRAB.1tA ( Al"rnate )DIl O. S. SBUIC.LA Directorate of Marketing and Inspection (Ministry

of Rural Development)DRS. JAYA1WtfAN ( Alt,rnate )

Da P. C. SIIUICLA Institute of Agriculture, Oujarat AgricultureUnivenity, Anand

SBRI VINBIT VIRMANI Nandi Provender Mills, New DelhiSHIU ANAND VIRMANI ( Alternate)

Da S. YAMDAONI Hindustan Lever Limited, Bombay

11

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