Investigating high strain rate effect on FRHSC of Steel and Polyethelene

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    Department of Civil and Environmental Engineering

    Investigating the high strain rate effect on high strength concrete

    reinforced with Steel and Polyethylene fibers

    InterimReportVanceKang

    U094742A

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    Table of Contents

    TABLE OF CONTENTS................................................................................................................2

    1. INTRODUCTION: ...................................................................................................................3

    1.1. OBJECTIVES AND SCOPE........................................................................................................3

    1.2. BACKGROUND..........................................................................................................................4

    1.2.1. FIBRE REINFORCED CONCRETE (FRC)...........................................................................................4

    1.2.2. SPLIT HOPKINSON PRESSURE BAR(SHPB).................................................................................4

    2. PRELIMINARY EXPERIMENTAL STUDY....................................................................5

    2.1. MIX DESIGN..............................................................................................................................5

    2.2. RESULTS....................................................................................................................................6

    2.2.1.STATIC TEST RESULTS.........................................................................................................................6

    2.2.2 DYNAMIC TEST RESULTS......................................................................................................7

    3. COURSE FOR FUTURE:....................................................................................................13

    APPENDIX.................... .................. .................. ................. .................. .................. .................. ........14

    A1 FIBRE-REINFORCED CONCRETE.........................................................................................14

    A2 STEEL AND POLYPROENLENE FIBERS...............................................................................14

    A3 ASSUMPTIONS WITH SHPB.................................................................................................16

    4. BIBLIOGRAPHY..................................................................................................................23

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    1.Introduction:

    1.1.Objectives and scope

    The objective of this experiment is to investigate the properties of a fibre reinforced

    high strength concrete (FRHSC) at varying high strain rates that are between

    80-300s-1. The FRHSC is of strength 80-90MPa. The fibres used are a combination of

    Steel and Polyethylene of which ratio of its volume to concrete is 0.375% and 0.125%

    respectively. A Split Hopkinson Pressure bar (SHPB) is used to deliver the high strain

    rate to the material. Failure patterns of the samples as well as the compressive

    strength!, critical strain

    !and Youngs modulus from SHPB tests will be

    investigated and discussed. The later three properties will be used hopefully as a

    means to acquire a Dynamic increase factor (DIF) relationship. DIF is a factor used to

    express the increase in the physical property of the concrete when subjected to high

    strain rate with respect to quasi-static loading.

    The SHPB test however has limitations that need to be acknowledged. Firstly, for a

    consistent and apt material characterization, it is desired to achieve constant strain rate

    and dynamic stress equilibrium within the specimen)(Chen & Song, 2011). These

    properties are not easily achieved. Other problems include the fact that the Hopkinson

    bar is assumed to be 1-dimensional when in reality is not which results in dispersion.

    Experimental errors such as having gaps between the specimen and the SHPB bar that

    are hard to eliminate are also causes for concern. As shown briefly, there are

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    complexities involved in SHPB test and therefore deduction of results obtained from

    experiment has to be analysed with these factors in mind. Therefore in this

    dissertation, the different methods proposed by various academicians will be also

    explored and reviewed.

    1.2. Background

    1.2.1. Fibre reinforced concrete (FRC)

    More information about the FRC is in the appendix section

    1.2.2. Split Hopkinson Pressure Bar (SHPB)

    The SHPB set up is as shown. A gas tank on the right fires a projectile 0.5m long that

    impacts the input bar producing a strain wave. The strain wave is then measured by

    the strain gauges positioned in the middle of the input and output bar that are both 5m

    long. The wave initiated at the input bar is called the incident wave !() and the

    wave that is transmitted through the specimen and into the output bar is called the

    transmitted wave!(). The wave that is reflected at the input bar and specimeninterface is called the reflected wave!(). These 3 time-dependent waves are used tocalculate the strain rate and stress experienced by the specimen.

    The 2 approaches used to calculate them using this theory are the 1-wave and 3-wave

    equations. They will not be covered in depth in this report but in short 1-wave

    equation uses !() and !() to calculate strain rate and stress respectively while the

    Figure2SplitHopkinsonPressurebarequipmenttakenfromSHPBusermanual0501

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    3-wave equation uses all 3 types of strains to calculate stress and strain

    rate! , !() and !().

    There are a number of assumptions taken when using the SHPB but due to the

    limitation in length of report, it is placed in the appendix section.

    2.Preliminary Experimental study

    2.1.Mix design

    Table 1 Concrete Mix

    Mix proportion (kg/m3)

    Cement Water C.A. Sand Fiber SP

    500 175 900 71729.25

    101.21

    Table 2 Fiber Properties

    % by

    VolumeType

    Length

    (mm)

    Diameter

    (m)

    Aspect ratio

    (length/diameter)

    Young's

    modulus

    (GPa)

    Tensile

    strength

    (MPa)0.375 Steel (SF) 13 160 81 200 2500

    0.125 Polyethylene (PE) 12 39 308 66 2610

    The mix design is as shown in the tables above. The water to cement (w/c) ratio is

    0.35 and the fiber content is 0.5% by volume of which 0.375% is SF and 0.125% is

    PE. Superplasticizer is added to improve the workability of the mix. The Vebe time is

    7 seconds for this mix.

    The fibers used are steel and polyethylene both of which are approximately the same

    length however the aspect ratio of PE is much higher than that of SF. The tensile

    strength of PE is approximately the same as SF but the modulus of SF is almost 4

    times as high as that of PE.

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    2.2. Results

    2.2.1. Static test results

    Cylinders of length to diameter ratio of 2 and of diameter 100mm were used to

    determine Poisson ratiowhile compressive strengthfyand Youngs modulusE

    were determined from the SHPB specimens with length 38mm and diameter 75mm.

    Linear variable differential transformer (LVDT) is used to measure bulk deformation,

    which is then used to determine the shape of the curve after failure of specimen while

    strain gauge used measures value local deformation in the middle of specimen pre-

    failure shape of curve andE.

    Table 3 Static test results

    Ultimate strengthfy (MPa) E(GPa) Poisson ratio

    98.8 39.2 0.188

    Figure 3 Static Stress vs. Strain curves

    0

    20

    40

    60

    80

    100

    120

    -0.01 0 0.01 0.02 0.03 0.04 0.05 0.06 0.07

    Str

    ess(MPa)

    Strain

    LVDT

    StrainGauge

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    2.2.2.DynamicTestresults

    Figure4Incidentstrainpulsegeneratedby0.5mstriker

    These3pulseshereshowthedifferenceinmagnitudeofstrainpulseinthe

    incidentbardifferentamountofpressureisdelivered.Theperiodofpulsewhich

    isdependentuponthestrikerlengthapproximatelythesameasexpectedand

    thevelocityoftheprojectileisapproximatelyproportionatethemagnitudeof

    stresspulsewhichisgenerated.

    Pressure(Bar)Velocityof0.5m

    Projectile(ms-1)

    (MPa)

    14 7.2 851 173

    20 10.6 1111 226

    26 12.5 1360 276

    -1,600

    -1,400

    -1,200

    -1,000

    -800

    -600

    -400

    -200

    0

    200

    400

    0.00E+00 1.00E-04 2.00E-04 3.00E-04 4.00E-04 5.00E-04

    Strain()

    Time(s)

    14Bar

    16Bar14Bar

    26Bar

    20Bar

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    Figure 5 Strain measured with time as measured at the middle of the input and out put bar after impact

    This is a time dependent strain gauge response for a specimen subjected to a 31 bars

    of pressure, which corresponds to approximately 13.5ms-1 striker speed("NUS RD-

    SHPB 0501 user manual," 2006). Only the first 3 waves of are used.

    Figure 6 Strain waves after shifting

    The strain waves at the specimen bar-interface (which is used to input into the

    equations) are assumed to be the same after propagation to the centre of the input and

    output bar where the strain gauges are. Therefore the waves are shifted using the

    -1,800

    -1,300

    -800

    -300

    200

    700

    1,200

    0.00E+00 1.00E-03 2.00E-03 3.00E-03 4.00E-03 5.00E-03 6.00E-03

    Strain()

    Time(s)

    Inputbar

    output bar

    -2,000

    -1,500

    -1,000

    -500

    0

    500

    1,000

    1,500

    2,000

    1.00E-04 1.50E-04 2.00E-04 2.50E-04 3.00E-04 3.50E-04 4.00E-04 4.50E-04

    Strain()

    Time(s)

    Incident

    Reflected

    Transmitted

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    speed of the wave and the length travelled by the wave to find the strains experienced

    by the specimen. Theoretically speaking the period of the incident, reflected and

    transmitted wave ought to be the same but it can be hypothesized due to energy loss

    in cracking up, wave reverberations in specimen, imperfect contact surface between

    the bar and specimen as well as other factors that it has resulted in shorter period in

    the transmitted wave.

    The stress strain curve has many oscillations instead of a smooth curve due to reason as

    discussed earlier. The 3-wave theory shows a more erroneous result as can be seen that

    the stress pulse, which is supposed to be compressive, peaks with a tensile stress of

    almost 60MPa. This cannot be right, as the strain incident pulse is negative and therefore

    cannot possibly generate a tensile pulse. The reason for this is will be elaborated bellow.

    -80

    -60

    -40

    -20

    0

    20

    40

    60

    80

    100

    120140

    0 10,000 20,000 30,000 40,000 50,000 60,000 70,000

    Stress(MPa)

    Strain()

    1 wave

    3 wave

    Figure7DynamicStressvsStrainwithapplicationof1-Dwaveequations

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    The dynamic strength is taken from the peak of the curve.

    Figure8Stress/ Strain rate vs Time curves applying 1-wave equation

    The strain rate against time experienced by the specimen is shown to be constantly

    changing and since there is a need to specify a strain rate for each test, a general guide

    is employed by Wang to use the average value of strain rate experienced by the

    specimen in the time between the 80% values of the stress of the specimen (as shown

    above)(Wang, 2011). This portion of the strain rate curve comes after the highest

    peak of strain rate during which the stress has yet to rise and is more consistent. This

    high peak is unreliable due to experimental limitations as mentioned before and hence

    should not be considered.

    Both 1-wave and 3-wave theory shows a delay in rise time of the stress wave as

    compared to the strain rate (the 3-wave theory differs only by going negative before

    rising). This is due to the delay in transmitted strain !() as observed in the Strain vs.

    Time curve as both methods use !() to calculate stress. Therefore the initial portion

    of the curve should not be considered for both methods. More experiments have to be

    -100.00

    -50.00

    0.00

    50.00

    100.00

    150.00

    200.00

    250.00

    300.00

    350.00

    400.00

    450.00

    0.E+00 1.E-04 2.E-04 3.E-04 4.E-04 5.E-04 6.E-04 7.E-04

    Stress(MPa)/Strainrate(

    s-1)

    Time(s)

    stress

    strainrate

    80%stressvalue

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    conducted to evaluate further the reason for this significant delay but for now it is

    hypothesized that it is an experimental error mainly due to the specimen-bar interface.

    The data collected for this specimen is summarized below.

    Table 4 Dynamic test results

    ID Bar Strength( MPa) DIF Strain rate (s-

    )

    1 wave 3 wave 1 wave 3 wave 1 wave 3 wave

    8A-1-1 30.5 125 123 1.27 1.25 264 272

    Figure9Typicalfailurepatternforspecimen

    Figure9Strainvs.Time(withD30x1mmpulseshaper)aftershifting .

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    The pulses observed for a setup using pulse shaper is seen to comparatively much

    lesser oscillations (noise) as compared to Figure 6. This is due to absorption of high

    frequency components of the wave. The rise up time of the incident pulse is also

    delayed which helps the specimen to achieve stress equilibrium before failure as well

    as reduce inertia effects(Parry, Walker, & Dixon, 1995).

    Figure10StressvsStrain-ratecurveusing1-waveequation

    Figure11StressvsStrain-ratecurveusing3-waveequation

    Thedatapointsobtainedfromexperimentaltestsasofpresentdoesnot

    establishaclearDIFrelationshipbetweenstressandstrain-rate.Thiscouldbe

    duetothelackofdatapointsandthepresenceofanomalousdatapoints.

    0

    20

    40

    60

    80100

    120

    140

    160

    180

    0 50 100 150 200 250 300

    UltStress(MPa)

    StrainRate(s-1)

    1wave

    020

    40

    60

    80

    100

    120

    140

    160

    180

    0 50 100 150 200 250 300

    UltStress(MPa)

    StrainRate(s-1)

    3wave

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    Courseforfuture:

    2.3.Investigation in the limitation of SHPB

    With the limitations of SHPB in mind, more effort will be put into evaluating which

    portion of the stress-strain curve is useful, how to evaluate the strain-rate of the

    material (which is not universally established) and also if the Youngs Ecan actually

    be used from dynamic tests (debatable in literature if it is of any use (Gama,

    Lopatnikov, & Gillespie, 2004)).

    The transmitted wave as shown is a cause of problem in determining the strain-rate as

    well as the stress versus strain curve. As of now, the deviance in results obtained is

    predicted to be due to the experimental error but more investigation has to be done in

    that respect. If experimental error cannot be eliminated time shifting may not be the

    best approach in getting start of pulse and other methods should be employed such as

    the high accuracy forward finite-divided difference formula (discussed in the

    appendix)

    2.4.Investigation of the failure mode of the specimen.

    Failure mode of the concrete matrix has not been discussed much in the report but it

    can be of useful information. It can tell at high strain rate if the matrix fails due to

    fiber pull out or fracture which will better inform the user on the geometrical

    properties to consider for future mixes. Therefore surface of the specimen will be

    looked at and investigated further

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    Appendix

    A1 Fibre-reinforced concrete

    Concrete is a brittle material with very little ductility and toughness. That is to say

    that ordinary concrete cannot take much stress after the maximum is reached. With

    fibres in the concrete matrix, the concrete is able to achieve much higher post

    cracking ductility and toughness. One must note that the main purpose of fibres is not

    to increase ultimate strength of the concrete (which will be more economically done

    by adjusting w/c ratio and adding admixtures such as silica fume) (Papworth, 1997).

    The main role of the fibres is controlling cracking of concrete matrix allowing the

    concrete mass to be able to withstand significant stresses over relatively large strain

    capacity in the strain-softening stage (Mindess, 2003). Another important fact to note

    is that concrete is a strain-rate dependent material(Soroushian & Obaseki, 1986).

    Studies have shown that concrete subjected to higher strain rates tend to have higher

    strength and Youngs modulus(Wang, Zhang, & Quek, 2012).

    A2 Steel and Polyethylene fibers

    There are different kinds of fibres that can be used. The most common of which is

    steel fibers (SF) which has been used for many years of which its known advantages

    are high modulus of elasticityE, high strengthfy , relatively higher bonding with the

    matrix than other fibers resulting in increase in post cracking strength and therefore

    toughness to the matrix. All these help to minimise cracking due to changes in

    temperature and relative humidity and also increase its resistance against dynamic

    loading (A. Benturt & Mindess, 2007). The disadvantage of SF is that they have the

    common problem of balling which would reduce the workability of the fresh concrete

    and uniformity in distribution of the fiber. This is further aggravated when higher

    bond is desired (for smooth steel fiber) and so higher aspect ratio of the fiber is

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    employed to increase the surface area in contact. However higher aspect ratio and

    higher ratio in volume of fiber promote the occurrence of balling(A. Benturt &

    Mindess, 2007).

    Polymeric fibres have also become more and more common with different kinds

    being designed to serve different purposes. Polyethylene (PE), a polymer fiber is

    known to be able to control plastic shrinkage cracking well. Other notable advantages

    of it include their alkali resistance and low price(A. Benturt & Mindess, 2007). In

    addition, supplementing of PE as proven by Benturt (et. al ?) that while it only had a

    small effect on the toughness in static loading, it had a much bigger influence on the

    ductility in impact. Also, the addition of these fibers to (A. Benturt, Banthia, &

    Mindess, 1986) high strength concrete(HSC) yielded much better results in terms of

    toughness during impact testing as compared to normal strength concrete and

    therefore would be more efficient when applied to HSC.

    Having a hybrid in the mix is also an option. If employed effectively, it aims to utilize

    the advantageous properties of both fibers as well as to make the concrete mix more

    economical and thereby attaining synergy. Synergy is the term used to describe

    fibers that work together in a combination to provide performance exceeding that of

    individual fibers(Al Hazmi, Al Hazmi, Shubaili, & Sallam, 2012).

    As concluded by Hazmi through testing, high strength concrete with the hybrid of SF

    and polypropylene (PP) showed the superior compressive strength, tensile strength

    and flexural toughness over SF and PP acting alone. The reason could be that during

    hardened stage, SF being stiffer provides first crack strength, while PP having lower E

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    provides the improved toughness and strain capacity in the post crack zone(Al Hazmi

    et al., 2012).

    A3 Assumptions with SHPB

    The SHPB is used to deliver high strain rate to specimens in the order of 50s -1 to 104s-

    1(Gama et al., 2004). The fundamental assumptions when using 1 dimensional wave

    theory to calculate stress and strain of specimen are as follows:

    i. Material of bar remains linear elastic when loaded with stress pulsesii. Neutral axis is straight

    iii. Axial stress distribution is uniform across the cross sectioniv. System of bars are linear and dispersion freev. Stress equilibrium of specimen assumed and inertia effects ignored

    vi.

    Bar-specimen interface imperfection ignored

    i. Material of bar remains linear elastic

    This condition is satisfied as the stress pulse required for the experiment is much less

    than the elastic limit of the bar.

    ii. Neutral axis is straight

    The bars are as straight as it can possibly be made and error with respect to that is

    insignificant. However the specimen in contact with the bar may not be perfectly flat

    against the bar and is a cause for concern as will be touched on in point 4.

    iii. Axial stress distribution is uniform across the cross section

    This assumption is important as strain gauges that measure the strains are placed at

    the surface of the bars and if the axial stress distribution is not uniform across the

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    cross-section then the result obtained is greatly flawed. For strains recorded in the

    middle of the bar, this assumption is valid. However this assumption is not so valid at

    the bar ends as shown by Wang (2007). The figure shows near the bar end, the stress

    in the middle is higher by about 15% than the stress on the surface. This indicates that

    the stress experienced by the specimen at the bar end is not completely uniform.

    Figure 13 Axial stress distribution over the cross section 0.5D frombar end (Reproduced from Wang (2007))

    iv. System of bars are linear and dispersion freeWhen the striker hits the input bar, stress pulses of varying frequencies are generated

    due to the two dimensional nature of wave propagation; contrary to the assumption of

    1D wave propagation (waves travel at a constant speed c = E/. Pulses of higher

    frequencies travel slower than those of lower frequencies that results in the

    undesirable phenomena known as wave dispersion. Wave dispersion is reflected in

    the noise (oscillation of the wave) observed in the data.

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    Figure 14 Wave dispersion (reference?)

    This graph shows the incident and reflected pulse after the pulse wave generated by

    the striker propagates from the strain gauge to the free end of the incident bar and

    back. Since the same strain gauge is used to measure the pulses, any difference in

    shape of pulse is not caused by the fault of the recording system. From the

    comparison of both pulses it is can be concluded that due to the difference in speed of

    waves, the reflected wave gets more distorted with distance travelled and hence the

    difference in shape from the incident pulse.

    This can be corrected using Fourier Transform(Follansbee & Frantz, 1983) or by

    using a softer object placed between the input bar and the striker which acts as a pulse

    shaper. The pulse shaper helps to absorb high frequency components of the wave

    resulting in a pulse with lesser noise (can be seen in the Results section where a

    smoother curve is obtained).

    v. Stress equilibrium of specimen assumed and inertia effect ignoredStress equilibrium is achieved not instantaneously but after a certain number of

    reverberations within the specimen. It is proposed by Davies that the number is

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    -times(Gama et al., 2004). It is important that the specimen be able to reach stress

    uniformity before failure in order to obtain useful data.

    Inertia effect gets more pronounced when the specimen size gets longer in length in

    the axial direction. A thinner specimen will also allow for a shorter time for specimen

    to reach equilibrium (due to the shorter distance travelled by wave). It is

    recommended by Davies and Hunter that the optimum Length/ Diameter ratio is

    approximately 0.43 and since specimen used in this experiment has a ratio of 0.5,

    inertia effect can be an issue. The specimen length cannot be reduced too much due to

    requirements by the code to meet the minimum dimensions that is affected by the

    maximum aggregate size. Reducing the specimen length too much will result in

    failure to record the bulk property of the concrete matrix.

    vi. Bar-specimen interface imperfection ignoredThere is an uncertainty as the stress wave propagates from the incident bar to the

    specimen and then towards the transmission bar. The impedanceIin 1-D stress wave

    theory is defined as the ratio of the force applied to the point mass to the velocity of

    the point mass and theoretically it is purely influenced by density , areaA and wave

    velocity c.

    =cA

    1-D theory goes on to show that when there is an impedance mismatch, part of the

    stress wave will not be transmitted but be reflected. M. A. Kaiser proposed a

    coefficient to represent this ratio introducing as the transmission coefficient,

    =!

    !

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    Based on energy conservation, wave that is not transmitted is reflected at any given

    boundary. Based on the specimen and bar properties our transmission coefficient is

    as such (subscripts 12 and 23 represent incident bar-specimen interface and specimen-

    output bar interface):

    This show that only 20% of the incident wave that reaches the specimen would be

    transmitted and 75% of that transmitted wave will be transmitted to the output bar.

    This means that the remaining 25% of the wave within the specimen is reflected back

    into the specimen. Part of this portion of the wave is trapped within the specimen

    and will eventually die off after a period known as the stress bleed-off period. The

    phenomenon of bleed-off contributes to the noise of the strain recorded.

    In determining the start of the dynamic stress-strain curve, the start of the pulse

    should be identified properly. Currently the method employed is time-based meaning

    the start of the strain pulse is based on the shifting of the reflected and the transmitted

    pulse using the velocity of the wave though the bar and then through the specimen.

    There are 2 problems with this approach. Firstly the velocity of the wave through

    specimen is very rough estimate due to its high anisotropic nature and secondly there

    is a high degree of uncertainty of the time for wave propagation at the specimen-bar

    interface known as the transit time (which is completely ignored in our 1-D wave

    theory). This uncertainty is due to the gap between specimen and the bar due to the

    finishing of the specimen not being completely smooth and also the concrete

    specimen having small holes that if not filled with grease is filled with air. Both air

    12 0.20

    23 0.75

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    and grease introduces uncertainties to the experiment and negatively affect the strain

    pulse recorded when using time to determine the start of pulse.

    Kaiser proposes a mathematical solution as an alternative to the identification of the

    start of the pulse, which is not dependent on time. For a perfect strain history, the

    strain rate leading up to the pulse edge should be zero. Since the measured strain,

    though close to zero is never zero due to noise, this algorithm searches for a number

    of consecutive derivatives of the same sign and there is not change then the start of

    the pulse is determined. This numerical derivative algorithm is as follows

    ! ! = !!! + 4 !!! 3 !

    2

    Where i is the index referring to the data point and h is the sample rate of the signal.

    This method though currently not employed here can be considered to deal with

    uncertainty for the initial portion of the strains recorded in this experiment(Kaiser,

    Wilson, Wicks, & Swantek, 2000) .

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    # 20#

    Wave$equations:$#

    #

    1-wave equation:! ! =

    !

    !!

    !!! !

    ! ! =

    2!!

    !!

    !!

    !

    ! ! = ! !

    !

    !

    !"

    2-wave equation:

    ! ! =

    !! !!

    !!

    =

    !!

    !!

    [!! ! !! ! !! !

    ! ! = ! !

    !

    !

    !"

    ! ! =

    !!

    2!![!! ! + !! ! + !! ! ]

    ! ! : Time-dependent stress

    ! ! : Time-dependent strain rate

    ! ! :!Time-dependent strain!! ! :!Time-dependent incident strain!!

    ! :!Time-dependent reflected strain!!(!): Time-dependent transmitted strain

    !!: Wave speed in bar (!! =E/= 5090ms-1)

    !!: Length of specimen

    !!: Area of specimen

    !: Area of bar

    E: Youngs modulus of bar

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    3.Bibliography

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