Group06_Evalstage2

CL 459 - Design Project

Compound Phthalic Anhydride C6H4(CO)2O

Date - 19/02/2015

Group No. - 6

1) Yash Khemka (110020010)

2) Amit Bhadoriya (110020056)

3) Ajay Kumar (110020060)

4) Nachiket Kuntla (110020014)

5) Jaydeep Panchal (11D020010)

Reaction Path

Catalytic oxidation of o-xylene to phthalic anhydride

EVALUATION STAGE 2

Assumptions

Feed:

95% by weight o-xylene feed Filtered air (approximately 23% oxygen and 77% nitrogen gas) Sulphur dioxide (0.5-2.5% by weight of xylene)

Note:

Only o-xylene can form PAN PAN plant production capacity is 90,000 metric tons per year Weight ratio of air to xylenes is 25, equivalently 1 mole % xylene (

Assumptions

Conversion in Reactor:

All are with respect to 1 kg of 95% o-xylene feed

1.01 kg of PAN (Theoretical max = 1.03) 0.08 kg of Maleic Anhydride 0.007 kg of Benzoic Acid 0.5 kg of Carbon Dioxide 0.15 kg of Carbon Monoxide

Mass balance will give you amount of Water produced

Data taken from literature, based on actual BASF plant operation

Assumptions

Purification in Pretreatment tank:

Exhaust from Tank contains (wrt input of same component)

0.5% of PAN - lost in exhaust 5% of Maleic Anhydride 100% of Water

Purification in Stripper:

Liquid output from bottom of Stripper contains (wrt input of same component)

99.5% of PAN - retained 5% of Maleic Anhydride

Assumptions

Purification in Rectifier:

Condensed Output from top of Rectifier contains (wrt input of same component)

99.9% of PAN - retained

Note:

All other particulate impurities are removed here

No Maleic Anhydride is lost in this stage

Final purity is 99.8% PAN (0.2% by weight of Maleic Anhydride)

Mass Balance-MANUAL

CompoundsReactor Feed

(4)

Reactor

Product (5)

Input to

Condensor (6)

Crude

Product (7)

Condensor

off-gas (8')

Scrubber

Feed (8)

Pretreatment

Tank Feed (11)

Sulphur Dioxide 421989.2 421989.2 421989.2 421989.2 421989.2

Carbon Monoxide 13561817.3 13561817.3 13561817.3 13561817.3

Carbon Dioxide 46834614.2 46834614.2 46834614.2 46834614.2

Nitrogen 1743611132 1743611132 1743611132 426939.2 1743184193.1 1743184193.1 426939.2

Oxygen 529702877.7 406138003.5 406138003.5 406138003.5 406138003.5

Phthalic Anhydride 93031913.4 93031913.4 90961567.5 2070345.9 2070345.9 90961567.5

Maleic Anhydride 7323554.6 7323554.6 3420463.8 3903090.8 3903090.8 3420463.8

Benzoic Acid 641027.6 641027.6 388576.6 252451.0 252451.0 388576.6

o-Xylene 87845529.9

m- & p-Xylene 4140691.7

Particulate 421989.2 421989.2 421989.2 421989.2

Water 24710499.8 78446679.5 78446679.5 26999884.1 51446795.4 78446679.5 26999884.1

Total (kg/hr) 2390432721 2390432721 2390432721 122619420.4 2267813300 2294813184 122619420.4

Mass Balance

CompoundsPretreament

Exhaust (12)

Pretreament

Crude (13)

Stripper

Feed (13)

Stripper waste

to Incinerator

Rectifier

Feed (16)

Rectifier waste to

Incinerator (19)

Refined

PAN (20)

Sulphur Dioxide

Carbon Monoxide

Carbon Dioxide

Nitrogen 426939.2

Oxygen

Phthalic Anhydride 393526.6 90568040.9 90568040.9 477676.9 90090364.0 90363.9 90000000

Maleic Anhydride 180675.7 3239788.1 3239788.1 3077798.7 161989.4 161989.4

Benzoic Acid 388576.57 388576.57 388576.57

o-Xylene

m- & p-Xylene

Particulate 421989.2 421989.2 421989.2 421989.205

Water 26999884.1

Total (kg/hr) 28001025.6 94618394.8 94618394.8 3944052.2 90674342.6 512327.07 90162016

ASPEN FLOWSHEET

DSTWU-RADFRAC COLUMN-DISTILL-1

TEMPERATURE V/S STAGE FOR DISTILL-1

TEMPERATURE V/S STAGE FOR DISTILL-2

VAPOUR COMPOSITION V/S STAGE FOR DISTILL-1

LIQUID COMPOSITION V/S STAGE FOR DISTILL-1

VAPOUR COMPOSITION V/S STAGE FOR DISTILL-2

LIQUID COMPOSITION V/S STAGE FOR DISTILL-2

Units 1 2 3 4 5 6 7 8 9 10

From COMP1 HEATER1 MIX-1 REACT1 COOLER1 FLASH1 FLASH1 COOLER2

To COMP1 HEATER1 MIX-1 MIX-1 REACT1 COOLER1 FLASH1 COOLER2 MIX-2 FLASH2

Substream: MIXED

Phase: Vapor Liquid Vapor Vapor Vapor Vapor Vapor Vapor Liquid Mixed

Component Mole Flow

WATER KMOL/HR 0.00 0.00 0.00 0.00 0.00 347.09 347.09 345.50 1.59 345.50

O-XYL-01 KMOL/HR 0.00 99.17 0.00 99.17 99.17 0.00 0.00 0.00 0.00 0.00

OXYGE-01 KMOL/HR 471.06 0.00 471.06 0.00 471.06 0.00 0.00 0.00 0.00 0.00

CARBO-01KMOL/HR 0.00 0.00 0.00 0.00 0.00 39.67 39.67 39.67 0.00 39.67

MALEI-01 KMOL/HR 0.00 0.00 0.00 0.00 0.00 9.92 9.92 8.53 1.39 8.53

PHTHA-01 KMOL/HR 0.00 0.00 0.00 0.00 0.00 69.42 69.42 20.37 49.05 20.37

CARBO-02KMOL/HR 0.00 0.00 0.00 0.00 0.00 158.67 158.67 158.65 0.02 158.65

BENZE-01 KMOL/HR 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

NITRO-01 KMOL/HR 1884.22 0.00 1884.22 0.00 1884.22 1884.22 1884.22 1884.19 0.04 1884.19

M-XYL-01 KMOL/HR 0.00 2.61 0.00 2.61 2.61 2.61 2.61 2.58 0.03 2.58

P-XYL-01 KMOL/HR 0.00 2.61 0.00 2.61 2.61 2.61 2.61 2.58 0.03 2.58

TOLUE-01 KMOL/HR 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

ETHYL-01 KMOL/HR 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

BENZO-01 KMOL/HR 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

PHTHA-02 KMOL/HR 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

Mole FlowKMOL/HR 2355.28 104.39 2355.28 104.39 2459.67 2514.21 2514.21 2462.06 52.15 2462.06

Mass FlowKG/HR 67856.85 11082.72 67856.85 11082.72 78939.57 78939.57 78939.57 71501.79 7437.78 71501.79

Volume FlowL/MIN 969062.00 210.52 563606.00 33388.57 641740.00 989624.00 731262.00 503410.00 105.14 646283.00

TemperatureC 24.85 24.85 141.17 300.00 178.73 380.00 210.00 170.00 170.00 110.00

Pressure BAR 1.00 1.00 2.40 2.40 2.40 2.30 2.30 3.00 3.00 2.00

Vapor Fraction 1.00 0.00 1.00 1.00 1.00 1.00 1.00 1.00 0.00 0.99

Liquid Fraction 0.00 1.00 0.00 0.00 0.00 0.00 0.00 0.00 1.00 0.01

Solid Fraction 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

Molar EnthalpyCAL/MOL -2.97 -5621.38 810.75 16455.83 1474.74 -14109.88 -15623.74 -14537.10 -99871.09 -15166.74

Mass EnthalpyCAL/GM -0.10 -52.95 28.14 155.00 45.95 -449.40 -497.61 -500.56 -700.22 -522.25

Enthalpy FlowCAL/SEC -1942.27 -163000.00 530431.00 477169.00 1007600.00 -9854200.00 -10912000.00 -9942000.00 -1446700.00 -10373000.00

Molar EntropyCAL/MOL-K 1.00 -106.80 1.58 -56.03 -0.43 3.89 1.21 0.63 -67.89 -0.09

Mass EntropyCAL/GM-K 0.03 -1.01 0.05 -0.53 -0.01 0.12 0.04 0.02 -0.48 0.00

Molar DensityMOL/CC 0.00 0.01 0.00 0.00 0.00 0.00 0.00 0.00 0.01 0.00

Mass DensityGM/CC 0.00 0.88 0.00 0.01 0.00 0.00 0.00 0.00 1.18 0.00

Average Molecular Weight 28.81 106.17 28.81 106.17 32.09 31.40 31.40 29.04 142.63 29.04

Units 11 12 13 14 15 18 19 20 21

From FLASH2 FLASH2 MIX-2 HEATER2 DIST1 DIST1 DIST1 DIST2 DIST2

To MIX-2 HEATER2 DIST1 DIST2

Substream: MIXED

Phase: Liquid Vapor Mixed Mixed Vapor Liquid Liquid Liquid Liquid

Component Mole Flow

WATER KMOL/HR 2.00 343.50 3.60 3.60 3.53 0.07 0.00 0.00 0.00

O-XYL-01 KMOL/HR 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

OXYGE-01 KMOL/HR 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

CARBO-01KMOL/HR 0.00 39.67 0.00 0.00 0.00 0.00 0.00 0.00 0.00

MALEI-01 KMOL/HR 3.08 5.45 4.47 4.47 2.41 1.46 0.60 0.54 0.06

PHTHA-01 KMOL/HR 19.26 1.11 68.31 68.31 0.00 0.00 68.31 2.00 66.30

CARBO-02KMOL/HR 0.01 158.64 0.03 0.03 0.03 0.00 0.00 0.00 0.00

BENZE-01 KMOL/HR 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

NITRO-01 KMOL/HR 0.01 1884.18 0.04 0.04 0.04 0.00 0.00 0.00 0.00

M-XYL-01 KMOL/HR 0.03 2.55 0.06 0.06 0.06 0.00 0.00 0.00 0.00

P-XYL-01 KMOL/HR 0.03 2.55 0.05 0.05 0.05 0.00 0.00 0.00 0.00

TOLUE-01 KMOL/HR 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

ETHYL-01 KMOL/HR 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

BENZO-01 KMOL/HR 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

PHTHA-02 KMOL/HR 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

Mole FlowKMOL/HR 24.42 2437.64 76.57 76.57 6.13 1.53 68.91 2.55 66.36

Mass FlowKG/HR 3197.71 68304.08 10635.49 10635.49 314.35 144.43 10176.71 350.39 9826.32

Volume FlowL/MIN 43.01 ######## 155.14 172.77 3753.70 2.04 160.47 5.23 150.73

TemperatureC 110.00 110.00 151.96 190.00 174.02 174.02 279.76 221.81 255.02

Pressure BAR 2.00 2.00 2.00 2.00 1.00 1.00 1.00 0.50 0.50

Vapor Fraction 0.00 1.00 0.00 0.00 1.00 0.00 0.00 0.00 0.00

Liquid Fraction 1.00 0.00 1.00 1.00 0.00 1.00 1.00 1.00 1.00

Solid Fraction 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

Molar EnthalpyCAL/MOL ######## -14305.55 ######## -98202.98 -68500.90 ######## -94485.42 -98687.45 -96057.55

Mass EnthalpyCAL/GM -772.32 -510.54 -721.90 -706.99 -1334.79 -1076.15 -639.80 -718.13 -648.72

Enthalpy FlowCAL/SEC ######## ######## ######## ######## ######## -43174.96 ######## -69895.76 ########

Molar EntropyCAL/MOL-K -70.29 0.61 -68.49 -63.83 -12.44 -48.09 -56.61 -58.54 -59.79

Mass EntropyCAL/GM-K -0.54 0.02 -0.49 -0.46 -0.24 -0.51 -0.38 -0.43 -0.40

Molar DensityMOL/CC 0.01 0.00 0.01 0.01 0.00 0.01 0.01 0.01 0.01

Mass DensityGM/CC 1.24 0.00 1.14 1.03 0.00 1.18 1.06 1.12 1.09

Average Molecular Weight130.95 28.02 138.90 138.90 51.32 94.32 147.68 137.42 148.07

010

20

30

40

50

60

70

0 50 100 150 200 250

MO

LA

R F

LO

W R

AT

E

TEMPERATURE(C)

FLASH-1

MAL-V PTH-L

MOLAR FLOW RATE V/S TEMPERATURE

05

10

15

20

25

0 20 40 60 80 100 120 140

Mola

r F

low

Temperature

Flash-2

MAL-V

PTH-L

MOLAR FLOW RATE V/S TEMPERATURE

Row/CaseStatus stream 18 stream 19 stream15

VARY 1 MAVAP PAVAP MALIQ PALIQ MAVAP1 PAVAP1

DIST1

1

P-SPEC PRES

BAR KMOL/HR KMOL/HR KMOL/HR KMOL/HR KMOL/HR KMOL/HR

1 OK 0.2 1.49165342 1.39E-14 0.60483 68.30635 2.375104 1.23E-15

2 OK 0.328571429 1.48330447 7.68E-14 0.604829 68.30635 2.383453 7.86E-15

3 OK 0.457142857 1.47679637 2.48E-13 0.604829 68.30635 2.389961 2.80E-14

4 OK 0.585714286 1.47133548 6.10E-13 0.604829 68.30635 2.395422 7.43E-14

5 OK 0.714285714 1.46656806 1.27E-12 0.604829 68.30635 2.40019 1.65E-13

6 OK 0.842857143 1.4623006 2.38E-12 0.604829 68.30635 2.404457 3.24E-13

7 OK 0.971428571 1.45841412 4.10E-12 0.604829 68.30635 2.408344 5.84E-13

8 OK 1 1.45759105 4.59E-12 0.604829 68.30635 2.409167 6.60E-13

9 OK 1.1 1.45482964 6.64E-12 0.604828 68.30635 2.411929 9.86E-13

10 OK 1.22857143 1.45149163 1.03E-11 0.604828 68.30635 2.415267 1.58E-12

11 OK 1.35714286 1.4483597 1.53E-11 0.604827 68.30635 2.4184 2.43E-12

12 OK 1.48571429 1.44540227 2.21E-11 0.604827 68.30635 2.421358 3.61E-12

13 OK 1.61428571 1.44259599 3.10E-11 0.604826 68.30635 2.424165 5.22E-12

14 OK 1.74285714 1.43992158 4.27E-11 0.604826 68.30635 2.42684 7.36E-12

15 OK 1.87142857 1.4373634 5.76E-11 0.604825 68.30635 2.429399 1.02E-11

16 OK 2 1.4349087 7.64E-11 0.604824 68.30635 2.431854 1.38E-11

SENSITIVITY W.R.T PRESSURE DISTILL-1

SENSITIVITY W.R.T PRESSURE DISTILL-1

Row/Case Status stream18 stream 19 stream15


DIST1

COL-SPEC

MOLE-RR

KMOL/HR KMOL/HR KMOL/HR KMOL/HR KMOL/HR KMOL/HR

1 OK 0.2 0.748687 0.732838 1.527923 67.38325 2.194976 0.190264

2 OK 0.614286 1.375287 0.08544 0.703049 68.20813 2.39325 0.012783

3 OK 1.028571 1.457591 6.76E-11 0.604827 68.30635 2.409168 9.74E-12

4 OK 1.442857 1.457593 1.07E-11 0.604828 68.30635 2.409165 1.55E-12

5 OK 1.779 1.457593 4.58E-12 0.604829 68.30635 2.409165 6.59E-13

6 OK 1.857143 1.457593 3.92E-12 0.604829 68.30635 2.409165 5.64E-13

7 OK 2.271429 1.457593 2.01E-12 0.604829 68.30635 2.409165 2.90E-13

8 OK 2.685714 1.457593 1.24E-12 0.604829 68.30635 2.409165 1.78E-13

9 OK 3.1 1.457593 8.47E-13 0.604829 68.30635 2.409164 1.22E-13

10 OK 3.514286 1.457593 6.24E-13 0.604829 68.30635 2.409164 8.98E-14

11 OK 3.928571 1.457593 4.83E-13 0.604829 68.30635 2.409164 6.96E-14

12 OK 4.342857 1.457593 3.89E-13 0.604829 68.30635 2.409164 5.59E-14

13 OK 4.757143 1.457593 3.22E-13 0.604829 68.30635 2.409164 4.63E-14

14 OK 5.171429 1.457593 2.72E-13 0.604829 68.30635 2.409164 3.92E-14

15 OK 5.585714 1.457593 2.35E-13 0.604829 68.30635 2.409164 3.38E-14

16 OK 6 1.457593 2.05E-13 0.604829 68.30635 2.409164 2.95E-14

SENSITIVITY W.R.T REFLUX RATIO DISTILL-1

Row/Case Status Stream18 Stream19 stream 15


DIST1

14

FEEDS STAGE


1 OK 2 1.056122 0.415502 1.097925 67.81325 2.31754 0.077593

2 OK 3 1.375441 0.085281 0.702869 68.20831 2.393277 0.012759

3 OK 4 1.445206 0.012868 0.619559 68.29162 2.406822 0.001862

4 OK 5 1.455911 0.001747 0.606829 68.30435 2.408847 0.000252

5 OK 6 1.457371 0.000233 0.605096 68.30608 2.409121 3.35E-05

6 OK 7 1.457564 3.08E-05 0.604865 68.30631 2.409158 4.44E-06

7 OK 8 1.457589 4.08E-06 0.604834 68.30634 2.409163 5.88E-07

8 OK 9 1.457593 5.41E-07 0.60483 68.30635 2.409164 7.79E-08

9 OK 10 1.457593 7.20E-08 0.60483 68.30635 2.409164 1.04E-08

10 OK 11 1.457593 9.61E-09 0.60483 68.30635 2.409164 1.38E-09

11 OK 12 1.457593 1.30E-09 0.60483 68.30635 2.409164 1.87E-10

12 OK 13 1.457593 1.81E-10 0.60483 68.30635 2.409164 2.60E-11

13 OK 14 1.457593 2.68E-11 0.604829 68.30635 2.409164 3.86E-12

14 OK 15 1.457593 4.58E-12 0.604829 68.30635 2.409165 6.59E-13

15 OK 16 1.457593 1.03E-12 0.604822 68.30635 2.409172 1.48E-13

16 OK 17 1.457596 4.13E-13 0.604759 68.30635 2.409233 5.94E-14

17 OK 18 1.421642 0.037375 0.646849 68.26351 2.403095 0.005468

18 OK 19 1.060632 0.411247 1.080893 67.81816 2.330061 0.076947

SENSITIVITY W.R.T FEED STAGE DISTILL-1

Row/Case Status Stream18 Stream19 stream 15


DIST1

PARAM

NSTAGE


1 OK 3 0.366795 1.13125 2.147829 66.55261 1.956963 0.622487

2 OK 4 0.438994 1.05673 1.953396 66.75027 2.079196 0.49935

3 OK 5 0.456787 1.038371 1.910106 66.79414 2.104693 0.473836

4 OK 6 0.459985 1.035086 1.902419 66.80192 2.109183 0.469343

5 OK 7 0.460625 1.034394 1.90108 66.80329 2.109882 0.468666

6 OK 8 0.460682 1.034353 1.900843 66.80353 2.110062 0.468469

7 OK 9 0.460695 1.03434 1.900813 66.80356 2.110079 0.468453

8 OK 10 0.460697 1.034337 1.900806 66.80356 2.110083 0.468448

9 OK 11 0.460698 1.034336 1.900804 66.80357 2.110085 0.468446

10 OK 12 0.460698 1.034337 1.900804 66.80357 2.110085 0.468447

11 OK 13 0.460698 1.034337 1.900804 66.80357 2.110085 0.468447

12 OK 14 0.460698 1.034336 1.900804 66.80357 2.110085 0.468446

13 OK 15 0.460698 1.034337 1.900804 66.80357 2.110085 0.468447

14 OK 16 1.060493 0.411366 1.081062 67.81799 2.330032 0.076996

15 OK 17 1.421638 0.037379 0.646854 68.2635 2.403095 0.005469

16 OK 18 1.457596 2.36E-11 0.604759 68.30635 2.409233 3.39E-12

17 OK 19 1.457593 7.78E-12 0.604822 68.30635 2.409172 1.12E-12

18 OK 20 1.457593 4.58E-12 0.604829 68.30635 2.409165 6.60E-13

SENSITIVITY W.R.T THEORETICAL STAGES DISTILL-1

Row/Case Status

VARY 1 PTHIN MALIN MALD PTHD PTHB MALB PTHB/(MA

DIST2 LB+PTHB)

COL-SPEC

MOLE-RR


1 OK 2 68.30635 0.604829 0.261921 2.287792 66.01856 0.342907 0.994832734

2 OK 2.928571 68.30635 0.604829 0.341472 2.20824 66.09811 0.263356 0.99603149

3 OK 3.857143 68.30635 0.604829 0.421331 2.128382 66.17797 0.183498 0.997234872

4 OK 4.785714 68.30635 0.604829 0.499026 2.050687 66.25566 0.105803 0.998405656

5 OK 5.43 68.30635 0.604829 0.544676 2.005036 66.30131 0.060152 0.999093567

6 OK 5.714286 68.30635 0.604829 0.560422 1.98929 66.31706 0.044406 0.999330842

7 OK 6.642857 68.30635 0.604829 0.590454 1.959259 6.63E+01 0.014375 0.999783388

8 OK 7.571429 68.30635 0.604829 0.600299 1.949413 6.64E+01 0.004529 0.999931749

9 OK 8.5 68.30635 0.604829 0.603266 1.946447 6.64E+01 0.001562 0.999976455

10 OK 9.428571 68.30635 0.604829 0.604225 1.945488 6.64E+01 0.000604 0.999990904

11 OK 10.35714 68.30635 0.604829 0.60457 1.945143 6.64E+01 0.000259 0.999996098

12 OK 11.28571 68.30635 0.604829 0.604707 1.945006 6.64E+01 0.000122 0.999998168

13 OK 12.21429 68.30635 0.604829 0.604767 1.944946 6.64E+01 6.17E-05 0.99999907

14 OK 13.14286 68.30635 0.604829 0.604795 1.944917 6.64E+01 3.34E-05 0.999999496

15 OK 14.07143 68.30635 0.604829 0.604809 1.944903 6.64E+01 1.91E-05 0.999999712

16 OK 15 68.30635 0.604829 0.604817 1.944896 6.64E+01 1.15E-05 0.999999826

Reflux ratio variation


Row/Case Status

VARY 1 PTHIN MALIN MALD PTHD PTHB MALB PTHB/(MA MALD/MAL

DIST2 LB+PTHB) IN

19

FEEDS STAGE


1 OK 5 68.30635 0.604829 0.555713 1.993999 6.63E+01 0.049115 0.999259883 0.918794788

2 OK 6 68.30635 0.604829 0.556206 1.993507 66.31284 0.048623 0.999267304 0.919608937

3 OK 7 68.30635 0.604829 0.556193 1.99352 66.31283 0.048636 0.999267105 0.919587193

4 OK 8 68.30635 0.604829 0.556101 1.993611 66.31274 0.048727 0.99926573 0.919436271

5 OK 9 68.30635 0.604829 0.55598 1.993733 66.31262 0.048849 0.999263902 0.919235643

6 OK 10 68.30635 0.604829 0.555842 1.993871 66.31248 0.048987 0.999261818 0.919007062

7 OK 11 68.30635 0.604829 0.555677 1.994036 66.31231 0.049152 0.999259331 0.918734207

8 OK 12 68.30635 0.604829 0.555478 1.994235 66.31211 0.04935 0.999256338 0.9184058

9 OK 13 68.30635 0.604829 0.555242 1.99447 66.31188 0.049586 0.999252785 0.918015993

10 OK 14 68.30635 0.604829 0.554963 1.994749 66.3116 0.049865 0.999248584 0.917555023

11 OK 15 68.30635 0.604829 0.554634 1.995079 66.31127 0.050195 0.999243617 0.917010037

12 OK 16 68.30635 0.604829 0.554243 1.99547 66.31088 0.050586 0.999237721 0.916363151

13 OK 17 68.30635 0.604829 0.55378 1.995933 66.31042 0.051049 0.99923075 0.915598306

14 OK 18 68.30635 0.604829 0.553229 1.996483 66.30987 0.051599 0.999222452 0.914687814

15 OK 19 68.30635 0.604829 0.552576 1.997136 66.30921 0.052252 0.999212613 0.913608278

16 OK 20 68.30635 0.604829 0.551796 1.997917 66.30843 0.053033 0.999200852 0.91231789

17 OK 21 68.30635 0.604829 0.550866 1.998847 66.3075 0.053963 0.999186836 0.910780097

18 OK 22 68.30635 0.604829 0.549747 1.999966 66.30638 0.055082 0.999169972 0.908929779

19 OK 23 68.30635 0.604829 0.548402 2.001311 66.30504 0.056427 0.999149706 0.906706199

20 OK 24 68.30635 0.604829 0.546766 2.002946 66.3034 0.058062 0.999125063 0.904002367

21 OK 25 68.30635 0.604829 0.544775 2.004938 66.30141 0.060054 0.999095051 0.900709445

22 OK 26 68.30635 0.604829 0.542312 2.007401 66.29895 0.062517 0.999057939 0.896637583

23 OK 27 68.30635 0.604829 0.539248 2.010465 66.29588 0.06558 0.999011769 0.891571803

24 OK 28 68.30635 0.604829 0.535356 2.014357 66.29199 0.069473 0.998953112 0.885136007

25 OK 29 68.30635 0.604829 0.530341 2.019371 66.28698 0.074487 0.99887755 0.876845429

26 OK 30 68.30635 0.604829 0.52359 2.026123 66.28023 0.081239 0.998775814 0.865682974

27 OK 31 68.30635 0.604829 0.514429 2.035284 66.27107 0.0904 0.998637767 0.850536491

28 OK 32 68.30635 0.604829 0.50125 2.048463 66.25789 0.103579 0.998439169 0.828746492

FEEDS STAGE Vary


Row/Case Status No of theo stages

VARY 1 PTHIN MALIN MALD PTHD PTHB MALB PTHB/(MA MALD/MAL

DIST2 LB+PTHB) IN

PARAM

NSTAGE


1 OK 10 68.30635 0.604829 0.371011 2.178702 66.12765 0.233818 0.996476604 0.61341492

2 OK 11 68.30635 0.604829 0.370987 2.178726 66.12762 0.233842 0.99647624 0.61337491

3 OK 12 68.30635 0.604829 0.370992 2.17872 66.12763 0.233836 0.996476328 0.613384538

4 OK 13 68.30635 0.604829 0.370991 2.178722 66.12763 0.233838 0.996476303 0.613381794

5 OK 14 68.30635 0.604829 0.370991 2.178722 66.12763 0.233837 0.996476307 0.613382286

6 OK 15 68.30635 0.604829 0.370991 2.178721 66.12763 0.233837 0.996476308 0.613382428

7 OK 16 68.30635 0.604829 0.370991 2.178721 66.12763 0.233837 0.996476308 0.613382427

8 OK 17 68.30635 0.604829 0.370991 2.178721 66.12763 0.233837 0.996476308 0.613382398

9 OK 18 68.30635 0.604829 0.370991 2.178721 66.12763 0.233837 0.996476308 0.613382399

10 OK 19 68.30635 0.604829 0.370991 2.178721 66.12763 0.233837 0.996476308 0.613382401

11 OK 20 68.30635 0.604829 0.370991 2.178722 66.12763 0.233837 0.996476308 0.613382384

12 OK 21 68.30635 0.604829 0.370991 2.178722 66.12763 0.233837 0.996476308 0.61338237

13 OK 22 68.30635 0.604829 0.370991 2.178722 66.12763 0.233837 0.996476308 0.613382358

14 OK 23 68.30635 0.604829 0.370991 2.178722 66.12763 0.233837 0.996476308 0.613382345

15 OK 24 68.30635 0.604829 0.370991 2.178722 66.12763 0.233837 0.996476308 0.613382331

16 OK 25 68.30635 0.604829 0.370991 2.178722 66.12763 0.233837 0.996476308 0.613382317

17 OK 26 68.30635 0.604829 0.445639 2.104073 66.20228 0.159189 0.997601182 0.736802978

18 OK 27 68.30635 0.604829 0.480881 2.068831 66.23752 0.123947 0.998132239 0.795070304

19 OK 28 68.30635 0.604829 0.5013 2.048412 66.25794 0.103528 0.998439935 0.828830554

20 OK 29 68.30635 0.604829 0.514471 2.035242 66.27111 0.090358 0.998638398 0.850605785

21 OK 30 68.30635 0.604829 0.523624 2.026088 66.28026 0.081204 0.998776334 0.865740034

22 OK 31 68.30635 0.604829 0.530287 2.019425 66.28692 0.074541 0.998876737 0.876756146

23 OK 32 68.30635 0.604829 0.535318 2.014394 66.29195 0.06951 0.99895255 0.885074291

24 OK 33 68.30635 0.604829 0.539128 2.010585 66.29576 0.065701 0.999009954 0.89137269

25 OK 34 68.30635 0.604829 0.542218 2.007495 66.29885 0.06261 0.999056524 0.89648226

26 OK 35 68.30635 0.604829 0.544694 2.005019 66.30133 0.060135 0.999093833 0.900575849


THANK YOU

Documents

Group06_Evalstage2