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Glass Interposer Substrates: Fabrication,
Characterization and Modeling
Aric B. Shorey, PhD
Manager of Commercial Technology
Semiconductor Glass Wafers/Corning, Incorporated
5 September 2013
© 2013 Corning Incorporated
Outline
• Glass Substrates
• Strength
• Via Process
• Cu Filling and RDL Process
• Glass and Si Interposer Test Vehicle
Performance
• Summary
© 2013 Corning Incorporated
What is Needed for 3D-IC?
High Quality Substrates
• A substrate that can support a silicon
device wafer during the thinning and
stacking process as a carrier
• A substrate that can be used in
interposer applications
High Value Attributes
• Smooth & clean surface
• Low TTV
• Low warp / bow
• Strength & reliability
• CTE matching Si
• Good chemical durability
• Good electrical properties
© 2013 Corning Incorporated
Corning’s Strategic Intent in Semiconductor Glass
Advanced Optical Melting Fusion
Sheet Forming Process
Optimized
Expansion
Pristine Surface
Profoundly
Flat
Thin & Strong
Innovative Aluminosilicate
Glass Compositions
© 2013 Corning Incorporated
Corning® Willow™ Glass: Ultra-slim Flexible Substrates
• Ultra-slim flexible glass from the fusion
process makes an ideal substrate for TGV
– Pristine surface with low TTV
– Opportunity to provide materials that do not
require post-form finishing
– Glass is not susceptible to dislocations
© 2013 Corning Incorporated
Potential Methods for Creating TGV
• Product Requirements:
– Hole dimensions
– Hole quality (cracks)
– Substrate size
– Scaling
– Cost
Through or Blind Via
Wet Etching & DRIE
Photo-Sensitive
Glass
Mechanical Drilling
Laser Ablation
Electrical Discharge
© 2013 Corning Incorporated
Corning’s Process: Current Capabilities
• Through and blind holes
• Glass size
– Wafers 100mm → 300mm wafers
– Panels up to 500mm
• Thickness
– 100µm→700µm
© 2013 Corning Incorporated
Via Dimensions
Diameter > 20mm | Thickness > 100mm
20mm diameter 100mm diameter
Side B
Side A
100mm thick
60mm vias
100mm pitch
300mm thick
50mm vias
100mm pitch
700mm thick
25mm vias
100mm pitch
© 2013 Corning Incorporated
Varying Pitch and Pattern
15mm diameter
50mm pitch
30mm diameter
100mm pitch
30mm diameter
400mm pitch
Pitch down to 50 mm
Square Array
~ 6 holes/mm2 Square Array
~ 100 holes/mm2
HCP Array
~140 holes/mm2
Densities : <1 hole/mm2 >250 holes / mm2
© 2013 Corning Incorporated
Vias in High Quality Glass Substrates Full Characterization of
Hole Diameter, Circularity
Capabilities up to 300 mm wafers and panels up to 0.5M
30 µm Diameter Blind
Holes
Fully Patterned Wafers
With
100,000s of holes
Blind Via Diameter ~ 27 µm
2,500 holes 11,716 holes
Not just making holes in glass – fully patterned wafers/panels
with 100% inspection
© 2013 Corning Incorporated
Strength Performance
10010
95
80
50
20
5
2
1
Kgf
Pe
rce
nt
With Holes - A
With Holes - B
P lain Glass
V ariable
Weibull
0.923, 0.957, 0.956
C orrelation C oefficient
Glass Strength With and Without Holes
Weibull
© 2013 Corning Incorporated
Typical Breakage of a Via Sample
Break Origin
Picture of ROR broken glass sample with 5x5 via array.
Note that breakage did not originate at via array.
© 2013 Corning Incorporated
Filled Vias
• Demonstrated ability to fill vias with good adhesion properties (ITRI).
– Vias passed hatch test demonstrating good adhesion
• Development of additional downstream processes in progress
– Redistribution Layers (RDL)
– Thinning/finishing blind vias
Cu filling performance with TGV substrate based on
Corning fusion glass
(top diameter ~ 30 µm, total depth ~ 180 µm)
© 2013 Corning Incorporated
Glass and Silicon Interposer Test Vehicles
• Glass and Si test vehicles fabricated by Industrial Technology
Research Institute (ITRI) using Corning glass interposer
substrates.
Source: Industrial Technology Research Institute (ITRI)
© 2013 Corning Incorporated
Insertion Loss Measurement Comparison
• Si resulted in much insertion loss compared to glass based on surface (line) measurement.
• Signal lost ~50% if S21 = -3dB.
Microstrip Line CPW
© 2013 Corning Incorporated
Measurement of TSV and TGV combining microstrip line (L=570um)
Condition (line + via) Measurement
• Si resulted in much insertion loss compared to glass (based on line+via measurement)
• Signal lost ~50% if S21 = -3dB.
© 2013 Corning Incorporated
Corning Active Participation LGIP Program at Georgia Tech PRC
• Work will demonstrate:
– Decreased hole size and substrate thickness
– Ability to process/handle thin glass substrates (<100 µm)
– Performance/Reliability of glass interposers with different CTE
• Electrical and mechanical characterization
© 2013 Corning Incorporated
Model-to-Measurement Correlation
0 1 2 3 4 5 6 7 8 9 10
-0.6
-0.5
-0.4
-0.3
-0.2
-0.1
0
0.1
Frequency (GHz)
Insert
ion L
oss |S
21| (d
B)
2 Via Transition
Simulated
4 Via Transition
Simulated
6 Via Transition
Simulated
0 1 2 3 4 5 6 7 8 9 10
-0.6
-0.5
-0.4
-0.3
-0.2
-0.1
0
0.1
Frequency (GHz)
Insert
ion L
oss |S
21| (d
B)
2 Via Transition
Simulated
4 Via Transition
Simulated
6 Via Transition
Simulated
0 1 2 3 4 5 6 7 8 9 10
-0.6
-0.5
-0.4
-0.3
-0.2
-0.1
0
0.1
Frequency (GHz)In
sert
ion L
oss |S
21| (d
B)
2 Via Transition
Simulated
4 Via Transition
Simulated
6 Via Transition
Simulated
CPW Line
CPW Line
Glass TP
V
TP
V
CPW Line
Glass Glass
Glass Glass Glass 0 1 2 3 4 5 6 7 8 9 10
-0.5
-0.45
-0.4
-0.35
-0.3
-0.25
-0.2
-0.15
-0.1
-0.05
0
Frequency (GHz)
Insert
ion L
oss |S
21| (d
B)
2 Via Transition
Simulated
4 Via Transition
Simulated
6 Via Transition
Simulated
© 2013 Corning Incorporated
Finite Element analysis on package warp
Material
Elastic Modulus
(MPa)
Poisson Ratio
CTE (ppm/C)
Silicon See Table 2 below NA 2.6
Interposer (Glass
A, B)
73600 (A), 71700
(B) 0.23 (A), 0.21 (B) 3.17 (A), 8.35 (B)
Substrate
x,z = 29647-
39.438T
y = 12962-17.168T
xy,zy = 0.39,
xz=0.11
16 (in-plane), 84
(out-of-plane)
Microbump and
Underfill Effective
Properties
20705 0.3 40
C4 joints and
Underfill Effective
Properties
8517.8 0.35 25
Constant C11=C22 C12 C13 C33 C44 C55 C66
Value [GPa] 194.5 35.7 64.1 165.7 79.6 79.6 50.9
© 2013 Corning Incorporated
FEA Results indicate the ability to adjust CTE important lever for reliability
• Example of the warpage from the
package
• Effect of interposer thickness and
CTE on warpage
0 100 200 300 400 500200
220
240
260
280
300
320
340
360
Warp
age (
Mic
rons)
Interposer Thickness (Microns)
Silicon Interposer
Glass with CTE of 3.17 ppm/C
Glass with CTE of 8.35 ppm/C
© 2013 Corning Incorporated
Substantial opportunities for glass interposers readiness
• Electrical properties provide substantial
opportunity in many applications (particularly RF)
10010
95
80
50
20
5
2
1
Kgf
Pe
rce
nt
With Holes - A
With Holes - B
P lain Glass
V ariable
Weibull
0.923, 0.957, 0.956
C orrelation C oefficient
Glass Strength With and Without Holes
Weibull
• Ability to manufacture glass interposers with
excellent performance demonstrated
• Ability to adjust properties such as CTE can have
significant impact in device reliability
• Substantial opportunities to leverage the ability to
form 1) at thickness and 2) in different form factors
(wafer/panel) can substantially impact cost
© 2013 Corning Incorporated
Conclusion
• Glass is a versatile and robust material with a long track record &
strong potential as an enabling material in electronics.
• The key attributes to be delivered are in the areas of flatness,
surface quality, thermal behavior, electrical behavior, thinness, and
strength.
• There is opportunity to adjust glass composition to tailor
properties.
• We can make high quality through and blind vias in a variety of
glass compositions. Via diameters down to 20 µm diameter have
been achieved, with glass thickness of 100µm → 700µm.
• Filled vias with good adhesion.
• Thermal, mechanical, electrical and overall process (cost)
performance continue to be demonstrated