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Carrier and makeup gas settings selectable for He, H2, N2 and Ar
Turnkey Laboratories Solutions
Gas ChromatographyOptima GC - 3007
Optionaladvanced
autosampler
Sophisticatedsample inlets
EPC/AFC gassystem
Multi-valveand multi-
columntechnology
Column oventemperature-
rampprogrammable
Psi, KPa, Bar units selectable
Pressure control range: 1~150psi, Pressure accuracy: 0.001Psi Programmable pressure ramp RSD < 0.5%
Pressure/flow rate : -400 to 400 kPa/min and -400 to 400 ml/min
Flow rate control range: 0~600ml/min, flow rate accuracy: 0.1ml/minflow rate RSD < 0.1%
Programmable pressure/flow rate ramping: 20 steps
Excellent FIDwide range at<1.5* 10-12 pg/s
" ~450" "
Detector Limit of detection Baselinenoise
Maxoperatingtemp.
Baseline drift(after 2hrsstabilization)
Lineardynamicrange
FID 1.5PgC/s(N-C16)
4.4fg /MI
S: <2.0 x 10-11 g/sP: <5.0 x 10-13 g/sor 2.0 x 1013 g/s
<4 x 10-13 A
<30uV
<2 x 10-14 A/min zH 004 5 x 10-14 A/30min
400 Hz
100 Hz
100 Hz
100 Hz
> 107
> 105
5*104
S > 102
P: > 103
N: > 103
P: > 103
< 100V /30min
< 50uV /30min
S: <2 x 10-13 AP: <8 x 10-13 A
S: <1 x 10-12 A/30minP: <2 x 10-12 A/30min
2 x 10-12 A/30min
TCD
ECD
FPD
NPD
400oC
400oC
400oC
400oC
450oC
Programming temp. - ramp speed : 0-120oC/min
Fast cool down: 450~50oC< 1.5minutes
Temp. Contrl range: RT+5oC ~ 450oC (0.1oC increment)
N: <0.3 x 10-12 g/s(Azobenzene)P: <0.1 x 10-13 g/s(Malathion)
Dataacquisitionrate:
<20uV
Column oven dimension: 278x 310x 165mm=15.5L
Programming ramp : 20 ramp, programing time of 9999.99 mins.
Temp. accuracy: + 0.01℃C (Rapid column oven heating with rates -250oC to +250oC)
< 400pg tidecane/ ml
Clarity workstation feature
Multi-channel and multi-user universal workstation to control all parameter Can collect signal from 4 detectors via RS232 or USB
Basic parameter: max sample-collecting frequency @100Hz/unlimited peak process quantity/integral sensitivity @1µV*s
Batch processing makes machine control, auto sampling sequence collecting, auto integral correction much easierauto integral correction much easier
Fully support FDA-21CFR PART 11, SST AND IQ/OQ
Powerful post-treatment facilitate chromatography comparing, re-correction and data input&output.
Feature like easy to use report publisher, online help and answer, fully compatible with windows 7/10.
Standard setup
Optionalsamplingdevice
Capillary inlet Split/splitless capillary
Packed inlet Packed inlet
Optima-3007 Clarity counter-controlworkstationWorkstation
Injection Value
Headspacesampler
Thermaldesorption
6 - port valve or 10-port valve
Available
Available
16 or 150Auto sampler
Offers minimum sampling time snapshot function, single analysis capability. Automatic and manual peak integration, manipulation, identification, calibration points and levels and manual calibration curve creation, column performance calibration, data comparison function, Capability of connecting micro-bore column of 0.1 mm ID etc.
AFC: split/splitless mode, carrier gas can fulfill constant-pressure, constant-flow, constant-speed, programmable-temperature-rise, programmable-flow-rise andprogrammable-speed-rise to reduce sample decomposition and discrimination whileincrease separation and shorten analysis time.
EPCAFC fulfill digitalization and automatization, only need input column parameters, EPC/AFC can set best flow of column and show digitally.EPC/AFC can fulfill gas leaking self-diagnosis and cut off flow&gas source and alarm at the same time.
Traditional GC(Column temp @140oC) Analysis time 43min
One button access to routine maintenance information.
-rise and programmable-speed-rise; unique constant linear velocity mode for carrier gas.Unlimited valve events to fulfill accurate switching of multi-valve;Outside power & voltage checking system, over-heating protection system and flow monitoring system to make it intellectualized.Vacuum fluorescent display with english/chinese changeable;Multi-function keyboard can set complicated parameters and store 16 chromatography method;FID and FPD can provide reminder for auto ignite and turn-off, TCD with overflow/cut-off protection, flameout detection.Excellent FID wide-range to enhance linear range;Multi-valve and multi-column switch system to make sure complicated analysis at one times injection;PCB system shielding function to reduce interference;Carrier gas saving mode available to reduce cost;Autosampler, headspace and thermal desorption can be incorporated;Clarity workstation can fulfill 3Q certification to meet GMP/GLPstandard.
Instrument feature
AFC characteristic
GC9720(Column temp @140oC) with programmable pressure-rise Analysis time 17min
PCM control module much precise with independent-development AFC system;8-channel high-accuracy temperature control system and 8-channel outside events to fulfill counter-control ;Every gas circuit can achieve constant-pressure, constant-flow, constant-speed, programmable-temperature-rise, programmable-flow
GC should be capable of upgradation to any 3rd detector or mass Detector.Built in display and computer interface, display chromatograms, method parameters like temp., pressure and flow rates etc.ECD complete with 63NI source and low voltage heatersAdvance self Diagnostic function (inbuilt)
Carrier gas saving mode:After injeciton, can proceed low split flow modeautomatically to reduce carrier gas significantly.
13 min.4 11.6min
Traditional GC constant-flow mode Analysis time 13.4min Optima-3007 with programmable pressure-rise Analysis time 17min
Multi-valve and multi-column switch
Adopting AFP pneumatic valve,can setup 3-valve- 4-column and 4-valve- 5- column switch system to fully analyze only atone time sinpetro chemical, coalgas, trace C2H2 inethylene and trace CO and CO2 in ethylene.
Multi-valve and multi-column flow diagram
Clarity workstation is applicable
Multi-channel and multi-user universal workstation to control all parameter
Can collect signal from 4 detectors via RS232 or USB
Basic parameter: max sample-collecting frequency @100Hz/unlimited peak process
quantity/integral sensitivity @1*sμV
Batch processing makes machine control, auto sampling sequence collecting, auto integral
correction much easier
Fully support FDA-21CFR PART11, SSTAND IQ/OQ
Powerful post-treatment facilitate chromatography comparing, re-correction and data
input&output.
1 2 3
4
5
67
8
9
10
1
2
3
4
5
6 1
2
3
4
5
6
1
2
3
4
5
6
PCM
Hayesep Q(Separate )2mCO2, CO and SO2
m2)(A5 block H2, O2 and N2
2ml Hayesep Q pre-column 1
Release
Air block
Port 3 o�
Capillar y Pre-column 2S/SL
5UL Port 2 o�
Out
Port 1 o�
Cap. Al O2 3
TCD
FIDCAP
FL9720 workstation feature
Fully counter-control to set all parameter in workstationEasy operationalMulti-channel signal sampling, multi outside events control
Autosampler for optima-3007 Big displayer with double -tower automatic injection;Tray vial quantity: 16 or 150;Injection volume: 0.1-250uL;Sampling accuracy:+0.01uL;Precision: 0.4%Injection Port: split/splitless capillarycapillary columns: 50, 100, 250, 350 µInjection loop: multiport(0.25ml, 0.5ml and 1ml) Injection repeatability: <0.5%Maximum Temperature: 450oCMaximum pressure: 0-150psi(with EPC)Reproducibility: 0.3% RSD
Temperature set point Resolution: 0.1℃
Column oven dimension: 278x310x165mm=15.5L;
Temp. control range: RT+5℃~450℃(0.1℃ increment);Temperature Ramp: multi-ramp(>14)with plateaus
Wide split ratio setting range: 1 to 4500.Packed injection, capillary injection, flash-evaporationinjection, PTV injection and liquid injection are available;Easy consumables changeover .
Temp. accuracy: ±0.01℃
Programming temp.-ramp speed: 0-120℃/minProgramming temp.-ramp : 20Fast cool down: 450~50℃≤ 5min
Ignition recognition, Hprotection, anti-ponding;Solvent no tailing peak.Dual Temperature control.
Excellent wide range FID design, no ceiling limit for solvent peak;Dual flow rate differential system.Limit of detection can be 1.5*10 -12g/s;
Performance introductionINSTRUMENTS PERFORMANCE IS
INTRODUCED
Excellent qualitative repeateability
[pA]
00.5200.0200.5100.0100.500.0
00.0500.5400.0400.5300.0300.52
[pA]
00.5700.0700.5600.0600.5500.05
200.000
179.500
159.00
158.500
118.00
97.500
77.00
55.500
35.500
15.500
-5.00000.00100.5900.0900.5800.0800.57
[pA]
200.000
179.500
159.00
158.500
118.00
97.500
77.00
55.500
35.500
15.500
-5.000
200.000
179.500
159.00
158.500
118.00
97.500
77.00
55.500
35.500
15.500
-5.000
200.000
179.500
159.00
158.500
118.00
97.500
77.00
55.500
35.500
15.500
-5.000
[pA]
Retention time RSD ≤0.05%
Can incorporate flash-evaporation and high pressure liquid injection
Flash-evaporation injection for gas-liquid mixture, high pressure valve injection for liquid.
PTV sample injectionWith multiple accumulated injection and solvent release, increase temperature program-rise to achieve trace analysis.
300ppm FIDstandard sample
Peak at , no ceiling limit130000
150.000
130.000
110.000
90.000
70.000
50.000
30.000
10.000
-10.000
150.000
130.000
110.000
90.000
70.000
50.000
30.000
10.000
-10.000
150.000
130.000
110.000
90.000
70.000
50.000
30.000
10.000
-10.000
150.000
130.000
110.000
90.000
70.000
50.000
30.000
10.000
-10.000
0.00 2.00 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00 40.00
40.00 42.00 44.00 46.00 48.00 50.00 52.00 54.00 56.00 58.00 60.00 60.00 62.00 64.00 66.00 68.00 70.00 72.00 74.00 76.00 78.00 80.00
[pA] [pA]
[pA][pA]
[pA]
40.000
35.000
30.000
25.000
20.000
15.000
10.000
5.000
0.000
-5.00000.2100.0100.800.600.400.200.0
130000.0
116500.0
103000.0
89500.0
76000.0
62500.0
49000.0
35500.0
22000.0
8500.0
-5000.00.00 2.00 4.00 6.00 8.00 10.00 12.00
[pA]
Excellent quantitative repeatability
Excellent wide-range design makes no ceiling limit of solvent peak
GC-3007 is suitable but no limited to below application: food safety, environmental protection, energy(), medicine Petroleum refining industry and etc.
Typical application
Peak area RSD ≤0.8%
【 】Food safety
[pA]70.000
55.000
40.000
25.000
10.000
-5.00015.00 20.00 25.00 30.00 35.00 40.00 45.00
Setup
Setup
DEHP(Di-(2-ethylhexyl)phthalate)
[pA]500.000
450.000
400.000
350.000
300.000
250.000
200.000
150.000
100.000
50.000
0.000
-50.0000.00 5.00 10.00 15.00 20.00 25.00 30.00 3 5.00 40.00 45.00
Detector: FIDInlet: CapillaryGas control module: 2 setsInjection mode: liquid autosamplerColumn: LZP950 for wineWorkstation: Optima-3007
Setup
Detector: FIDInlet: CapillaryGas control module: 2 setsInjection mode: liquid autosamplerColumn: HP-5 cap.Workstation: Optima-3007
Chinse white wine
200ppb organochlorine in pesticide residue
Setup
Peak sequence:α-BHC,β-BHC,γ-BHC, δ-BHC, op-DDE, pp-DDD, op-DDT, pp-DDT
[mV]
10.00 13.00 16.00 19.00 22.00 25.00 28.00 31.00 34.00
200.000
180.000
160.000
140.000
120.000
100.000
80.000
60.000
40.000
20.000
0.000
-20.000
Detector: ECDInlet: CapillaryGas control module: 2 setsInjection mode: liquid autosamplerColumn: HP-5Workstation: Optima-3007
Setup
Complicated Organochlorine
Setup
100ppb organophosphoruspesticideresidue
60.000
55.000
50.000
45.000
40.000
35.000
30.000
25.000
20.000
15.000
10.000
5.000
0.000
-5.000
30.000
26.600
23.200
19.800
16.400
13.500
9.600
6.200
2.800
-0.600
-4.00030.00 35.00 40.00 45.00 50.00 55.00
】【Environmental protection
Peak sequence: COS, CS2, SO2, Methyl Mercaptan, Ethyl Mercaptan
450.000
400.000
350.000
300.000
250.000
200.000
150.000
100.000
0.00 3.00 6.00 9.00 12.00 15.00 18.00 21.00 24.00
[mV]Setup
[mV]
00.600.200.0 00.8100.6100.4100.2100.0100.800.4
[pA]
Detector: FPDInlet: CapillaryGas control module: 2 setsInjection mode: liquid autosamplerColumn: DB-35Workstation: Optima-3007
Peak sequence: DDVP, methamidophos, acephate, omethoate, dimethoate, parathionmethyl, fenitrothion, parathion, quinalphos, tiguron triazophos
Detector:TCDInlet: PackedGas control module: 2 setsInjection mode: liquid autosamplerColumn: Hayesep QWorkstation: Optima-3007
Detector: ECDInlet: CapillaryGas control module: 2 setsInjection mode: liquid autosamplerColumn: HP-5Workstation: Optima-3007
Peak sequence: CHCl3, CCl4
Setup
Detector: ECDInlet: CapillaryGas control module: 2 setsInjection mode: liquid autosamplerColumn: DM-1Workstation: Optima-3007
【 Energy 】
Petroleum refining
Distillationsimulation
inorganic gas
[mV]
0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00
Hydrocarbon
0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00
47.500
42.500
37.500
32.500
27.500
22.500
17.500
12.500
7.500
2.500
-2.500
[pA]
[pA]
0.00 2.00 4.00 6.00 8.00 10.00 12.00
700.000
629.000
558.000
487.000
416.000
345.000
274.000
203.000
132.000
61.000
-10.000
Setup
Detector:FID+TOCInjector: gas/capillary
Inorganic gas peak sequence: H2, CO2, O2, N2, COHydrocarbon peak sequence: CH4, C2H6, C2H4, C3H6, C3H8, cyclopropane, C2H2, iso-butane,Propadiene, n-butane, trans-2-Butene,, n-butylene, isobutene, cis-2-Butene, isopentane, n-pentane,allylene, 1,3-butadiene, 2-methyl-2-butene, trans-2-Pentene, 1-pentene, cis-2-Pentene, Hexane
4-valve-5-columnGas control module: 4setsValve injection
Column: Hayesep Q packed, 5A packed,AL2O3 capillary, DB-1 capillaryWorkstation: GC-3007
Setup
600.000
500.000
400.000
300.000
200.000
100.000
0.000
-100.000
Detector: FIDInlet: CapillaryGas control module: 2 setsInjection mode: liquid autosamplerColumn: HP-1 cap.Workstation: GC-3007
Aromatic compounds
[pA]
0.00 6.00 12.00 18.00 24.00 30.00 36.00 42.00 48.00 54.00
1750.000
1550.000
1350.000
1150.000
950.000
750.000
550.000
350.000
150.000
-50.000
-250.000
Setup
Detector: FIDInlet: CapillaryGas control module: 2 setsInjection mode: liquid autosamplerColumn: Innowax cap.Workstation: Optima-3007
Peak sequence: Benzene, Toluene, Ethane, P-xylene, M-xylene, P-Ethyltoluene, M-Ethyltoluene,S-Butybenzene, Diethylbenzene, O-diethylbenzene
,
Dimethyl etherinLNG
15.000
13.300
11.600
9.900
8.200
6.500
4.800
3.100
1.400
-0.300
-2.000
[pA]Setup
0.00 2.00 4.00 6.00 8.00 10.00 12.0 0 14.00 16.00 18.00
Setup
Setup
Organic acid
Cresolisomer
100.000
80.000
60.000
40.000
20.000
0.000
-20.0000.00 4.00 8.00 12.00 16.00 20.00 24.00 28.00
700.000
625.000
550.000
475.000
400.000
325.000
250.000
175.000
100.800
25.000
-50.0000.00 2.30 4.60 6.90 9.20 11.50 13.80 1 6.10 18.40 20.70 23.60
【 Medicine】
[pA][pA]
[pA]
Peak sequence:o-cresol, p-cresolm-cresol,
Detector: FID
Peak sequence: acetic acid, propionic acid, butyrate, valeric acid, sovaleric acid, caproic acid, heptylic acid, octanoic acid, n-nonanoic acid,lactic acid, 2-Hydroxy-2-Methylbutyric Acid.
Inlet: CapillaryGas control module: 2 setsInjection mode: liquid autosamplerColumn: DB-FFAPWorkstation: Optima-3007
Detector: FIDInlet: CapillaryGas control module: 2 setsInjection mode: Gas valve injectionColumn: PLOTQ cap.Workstation: Optima-3007
Peak sequence: CH4, C2H2, prepene, propane,methylal, Dimethyl ether, n-butene, cis-bitene,isoamylene, methyl alcohol, n-pentane
Detector: FIDInlet: CapillaryGas control module: 2 setsInjection mode: liquid autosamplerColumn: specialized for cresolWorkstation: Optima-3007
Organic solvent:
VOCS2nd-level solution
50ppb thiopheneinBenzene
0.00 1.90 3.80 5.70 7.80 9.50 11.40 13.00 15.20 17.10 19.00
60.002
53.177
40.352
39.527
32.702
25.877
19.052
12.227
5.402
-1.423
-8.248
[pA]
Peaksequence:methyl alcohol, ethanol,acetone+ isopropanol, acetonitrile,dichloromethane,chloroform, isobutanolCCI4 Benzene, n-heptane, isoamylol,pyridine, toluene, n-amyl alcohol,ethylbenzene, p-xylene, n-Hexanol, o-xylene
Setup
0.00 3.00 6.00 9.00 12.00 15.00 18.00 21.00 24.00 27.00 30.00 33.00
50.000
45.000
40.000
35.000
30.000
25.000
20.000
15.000
10.000
5.000
0.000
-50.000
[pA]
Setup
Detector: FPDInlet: CapillaryGas control module: 2 setsInjection mode: liquid autosamplerColumn: HP-InnowaxWorkstation: Optima-3007
Setup[pA]
30.000
25.000
20.000
15.000
10.000
5.000
0.000
-5.0000.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00
Detector: FPD
Peak sequence: methanol, ethanol,isopropanol, acetone, methyl acetate, n-butyl alcohol, butanone, ethyl acetate,acetic acid isopropyl ester benzene, 1-Methoxy-2-propanol, propyl acetat, 4-methyl-2-pentanone, 1-Ethoxy-2-propanol, toluene, n-butyl acetate,ethylbenzene, o-xylene, styrene
Inlet: CapillaryGas control module: 2 setsInjection mode: liquid autosamplerColumn: PC-VOCOLWorkstation: Optima-3007
Detector: FPDInlet: CapillaryGas control module: 2 setsInjection mode: liquid autosamplerColumn: DB-624 cap.Workstation: Optima-3007
HPLC Servicing :We have team of service engineers who can attend to any make of HPLC promptly @the most affordable cost. :We also take up preventive Maintenace to reduce downtime of HPLC’s Trainings
AMC’s/CMC :We offer user training both in-House and at customer sites on HPLC principles, operations, troubleshooting.Validations :We have protocols for carrying out periodic Validations as per GLP/GMP/U SFDA norms
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VER.17/09-1
