58
FIDAMAT 5E-P, -AP, -G Gas analyzers for Measurement of Total Hydrocarbon Content 7MB1420-... Instruction Manual Order no. C79000-B5276-C131-03

FIDAMAT 5E-P, -AP, -G Gas analyzers for Measurement of ......FIDAMAT 5E-G 15 psig FIDAMAT 5E-P 18 psig Position of use Front panel vertical Change in display through influencing variables

  • Upload
    others

  • View
    0

  • Download
    0

Embed Size (px)

Citation preview

  • FIDAMAT 5E-P, -AP, -G Gas analyzersfor Measurement of Total Hydrocarbon Content7MB1420-...

    Instruction Manual

    Order no. C79000-B5276-C131-03

  • Contents Page

    1 Introduction 41.1 General 41.2 Staff Qualifications 4

    2 Application 5

    3 Design 6

    4 Mode of Operation 7

    5 Technical Data 8

    6 Installation 116.1 Mounting 116.2 Gas Supply 116.3 Electric Connections 12

    7 Startup, Calibration 157.1 Startup 157.2 Calibration 157.2.1 FIDAMAT 5E-G without zero and calibration gas connections, FIDAMAT 5E-AP 157.2.2 FIDAMAT 5E-P without zero and calibration gas connections 16

    8 Operation 178.1 Description of Control Panel 178.2 Input Example 188.3 Coding and Organization of Operating Function Groups 198.4 Organization of Data Storage 20

    9 Warnings and Error Messages 219.1 Warnings 219.2 Faults 22

    10 Spare Parts and Accessories 2410.1 FIDAMAT 5E-AP 2410.2 FIDAMAT 5E-P 2610.3 FIDAMAT 5E-G 29

    11 Appendix A-111.1 Gas Flow Diagrams A-111.2 Layout Diagrams of Important Electronic Components A-411.3 Summary of Operating Functions A-511.4 Special Sheet for Storage of Current Coding A-23

    2

  • Note

    Your attention is drawn to the fact that the contents of this Instruction Manual are not part of aprevious or existing agreement, commitment or statutory right and do not change these. Allcommitments on the part of Siemens are contained in the respective sales contract which alsocontains the complete and solely applicable warranty conditions. These warranty conditions in thecontract are neither extended nor limited by the contents of this Instruction Manual.

    Also note that for clarity reasons this Instruction Manual cannot describe every possible problem inconjunction with the use in systems. Should you require further information, or should particularproblems occur which are not handled in sufficient depth in this Manual, help can be requestedthrough your local Siemens office or representative.

    Terms with the following meanings are used in this Instruction Manual and in the warning informationon the product:

    Danger in the sense of this Manual and the warning information on the product itself means thatdeath, severe personal injury and/or substantial damage to property will occur if the appropriatesafety precautions are not observed.

    Warning in the sense of this Manual and the warning information on the product itself means thatdeath, severe personal injury and/or substantial damage to property can occur if the appropriatesafety precautions are not observed.

    Caution in the sense of this Manual and the warning information on the product itself means thatslight personal injury and/or damage to property can occur if the appropriate safety precautionsare not observed.

    A note in the sense of this Manual is important information on the product or the respective part ofthe Manual to which particular attention should be paid.

    3

  • 1 Introduction

    1.1 General

    Warning! Certain parts in this electrical device contain dangerous voltages duringoperation.

    Failure to observe the warnings could therefore result in severe personalinjury and/or damage to property.

    Only suitably qualified staff should work on this device or in its vicinity. Theseshould be thoroughly familiar with all warnings and maintenance measuresaccording to this Manual.

    Correct and safe operation of this device is dependent on proper handling,installation, operation and maintenance.

    This device has left the factory in a perfect condition as regards safety. The notes and warnings inthis Manual must be observed by the user if this state is to be maintained and hazard-free operationof the device assured.

    1.2 Staff Qualifications

    A qualified person in the sense of this Instruction Manual and the warning information is one whois familiar with the installation, construction and operation of the device and who has the appropriatequalifications, e.g.:

    – is trained and authorized to energize, de-energize, ground and tag circuits and devices inaccordance with established safety practices;

    – is trained in the proper care and use of protective equipment in accordance with establishedsafety practices;

    – is trained in first aid.

    4

  • 2 Application

    The FIDAMAT 5E is an analyzer for measuring the concentration of total hydrocarbons. It operatesaccording to the principle of flame ionization.

    The analyzer is suitable for the measurement of all gaseous hydrocarbons. The connection of aheated line is provided in order to prevent condensation and adsorption in the gas supply line.

    Caution! Explosive gas mixtures must not be measured using the FIDAMAT. The ana-lyzer must not be used in potentially explosive atmospheres.

    Order No. Device type

    7MB1420-5.. FIDAMAT 5E-P rack-mounted device for process measurements, combustion gas H2

    7MB1420-7.. FIDAMAT 5E-AP rack-mounted device for car exhaust measurements, combustion gas H2/He

    7MB1420-8.. FIDAMAT 5E-G rack-mounted or benchtop devices for measurementsof gases of highest-grade purity,combustion gas H2/He

    5

  • 3 Design

    The device is available for installation in a 19-inch rack or 19-inch cabinet, the FIDAMAT 5E-G alsoals benchtop unit.

    The FIDAMAT comprises two main sections, the analyzer section and the electronics with front panelcontrols.

    Analyzer section

    The analyzer section consists of the oven with detector chamber and various restrictors. The ovenis accessible from the side to enable modifications or repairs to be carried out in the installedcondition without loosening the electric connections or gas piping connections.

    The analyzer section also contains pressure regulators, solenoid valves, pressure sensors and aflow sensor.

    Electronics

    The electronics consist of the input board which is integrated into the front panel, the motherboardwith preamplifier board and the control board.

    The motherboard contains the EPROMs for the software, the EEPROM for the parameter sets andthe switch for the write-protected area on the EEPROM.

    6

  • 4 Mode of Operation

    Electrons are released when hydrocarbons are combusted in a hydrogen flame. These electronsare collected at an electrode by means of an electric field and measured using a highly sensitiveamplifier. The current is proportional to the quantity of organically-bound C atoms in the samplegas.

    The sample gas is passed into the measuring chamber via an obstruction-resistant fused silicarestrictor. The sample gas is mixed in the measuring chamber with hydrogen or hydrogen/he-lium (4:6) or hydrogen and a specific amount of air and routed via the nozzle into the combustionchamber.

    The hydrogen pressure is held constant by a pressure regulator. The balanced system of restrictorsand pressure regulators ensures that the sample gas pressure is kept constant.

    The FIDAMAT operates largely automatically. If the parameters (pressures, temperatures) are set,the device starts up automatically when switched on and ignites when the setpoint temperature hasbeen reached. The hydrogen and combustion air pressures are measured when switching on, andthe control panel indicates if they are incorrectly set.

    1 Flame2 Quartz nozzle3 Combustion air4 Sample gas5 H2/He or H26 Measuring electrode7 Amplifier

    Fig. 4 Principle of flame ionization detector (FID)

    -200 V DC

    6

    7

    2

    3

    4

    5

    1

    7

  • 5 Technical Data

    Number of measuring ranges Max. 4, freely parameterizable

    Switching ratio Optional

    Autoranging SelectableHysteresis:– Switchover to larger range at 90 % of span of

    smaller range– Switchover to smaller range at 80 % of span of

    smaller range

    Output signals At terminal strips X1 and X3.A cable with a plug connector (Order No. W79070-U1610-M25) can be connected to these terminal strips

    Analog 0/2/4 to 20 mA, max. resolution 0.1 %, max. load 750 Ω

    Digital RS232 serial interface as V.24 or TTY (20 mA)

    Programming facilities (for setting of device-specific parameters using control panel) Measuring ranges, measured-value storage, time constant, 3-stage code for protection against

    unauthorized and unintentional use etc.

    Device output see Section 6.3electrical connections

    Measured-value display Digital concentration display (5 digits with floating decimal point)

    Resolution of digital display 0.1 % of measured value

    Ripple of output signal

  • Response time (T90 time) with time constant 0 s, set using function 13

  • FIDAMAT 5E rack-mounted unit

    FIDAMAT 5E-G as bench top unit

    Fig. 5.1 Dimension drawings

    465

    146 222

    483

    4

    442

    430360

    Caution! Only mount FIDAMAT 5E on sliding rails or angled rails

    Sample gas connection:

    1/4" screw connection

    Sample gas outlet:

    3/8" PVDF screw connection

    Auxiliary gas connections:

    1/4" screw connecction

    All measures are in millimeters (mm)

    493 430

    334

    10

  • 6 Installation

    6.1 Mounting

    The FIDAMAT 5E should be installed or mounted in a vibration-free location.

    Warning! The device must not be used to measure explosive gases. Operation in poten-tially explosive atmospheres is not permitted. The permissible ambient tem-perature (Section 5, Technical Data) must be observed during operation.

    The FIDAMAT 5E must only be mounted on sliding rails or angled rails.See Section 5 for dimensional drawings.

    6.2 Gas Supply

    Warning! When measuring toxic gases, the exhaust gas must be routed such that thereis no danger to the environment. Gases which may lead to explosive mixturesmust not be measured using the FIDAMAT.

    A gas-tight hose or steel piping can be used for the sample gas inlet and outlet depending on theappliction, and must be connected leak-free to the gas connection.

    The sample gas must be supplied with a pressure of 10 psig (5E-AP) or 15 psig (5E-P, -G), the supplygases with a pressure of 30 psig. The exhaust line from the FIDAMAT 5E must always be routedwith a downward gradient since water condenses in it.

    Fig. 6.1 Rear panel of FIDAMAT 5E-AP

    X3

    X1

    comb. air

    Mains120 V

    sample gas

    H2 - He

    11

  • Fig. 6.2 Rear panel of FIDAMAT 5E-P

    Fig. 6.3 Rear panel of FIDAMAT 5E-G

    6.3 Electric Connections

    Warning! The following must be observed for the electric connections:VDE 0100 “Regulations for the installation of power systems with mainsvoltages below 1000 V”.A mains disconnection device must be provided in the building installation(see rating plate for loading capacity).

    – Check that the local power supply agrees with that specified on the rating plate of the device.

    – Connect the required signal cables to the 25-pin trapezoidal plugs X1 and X3 (FID 5E-AP) orX1, X2 and X3 (FID 5E-P, -G) according to the pin assignment diagrams.

    X2

    X1

    zero gas

    Mains120 V/230 V

    sample gas H2

    X3

    cal. gas 1

    comb. air

    X2

    X1

    zero gas

    Mains120 V/230 V

    sample gas

    H2

    X3

    cal. gas 1

    comb. air

    12

  • Pin assignment diagram FIDAMAT 5E-P, -G

    Measure

    CalibrateStatussignal

    VacantMR 3

    Ready

    Not Ready

    Measuring range identificationContact closed = MR active

    Statussignal

    13

    12

    13

    25

    24

    23

    15

    22

    21

    20

    19

    17

    16

    14

    Analog current –

    MR 4

    11

    10

    9

    8

    2

    7

    6

    5

    4

    18

    3

    1

    Connection sideDevice side

    Pin

    Connection sideDevice side

    PinAnalog current +

    MR 2

    MR 4

    MR 1

    X1

    X2

    Calibrate span (funct. 8)

    Calibrate zero (funct. 5)

    Analog current –

    12 E2

    11

    10

    9

    13

    Connection sideDevice side

    Pin

    Valve for hydrogen

    E1 closed triggers a single autocalibration

    E2 closed = E1 is activated13

    25

    24

    23

    15

    22

    21

    20

    19

    18

    16

    14

    No warning

    Connection sideDevice side

    Pin

    Warning17Valve for sample gas

    Valve for calibration gas 1

    E1

    Contactopen =valve closed(whenoff)

    Ground

    Vacant

    8

    2

    7

    6

    5

    4

    3

    1 Valve for zero gas

    X3

    25

    RXD–

    24

    10

    9

    TXD–

    TXD+

    RXD+

    2

    7

    3

    1

    TXD

    GND

    V24

    Screen

    TTY

    RXD

    13

  • Pin assignment diagram FIDAMAT 5E-AP

    Calibrate span

    Measure

    CalibrateStatussignal

    Signal contact “Calibrate” (contactopen = calibration being carried out

    Calibrate zero

    VacantMR 3

    Ready

    No warning

    Measuring range identificationContact closed = MR active

    Statussignal

    13

    12

    13

    25

    24

    23

    15

    22

    21

    20

    19

    17

    16

    14

    Analog current –

    MR 4

    11

    10

    9

    8

    2

    7

    6

    5

    4

    18

    3

    1PinPin

    Analog current +

    MR 2

    MR 4

    MR 1

    X1Device side Connection sideDevice sideConnection side

    Not Ready

    X3

    25

    RXD–

    24

    10

    9

    TXD–

    TXD+

    RXD+

    2

    7

    3

    1

    TXD

    GND

    V24

    Screen

    TTY

    RXD

    14

  • 7 Startup, Calibration

    7.1 Startup

    You should be acquainted with the operation of the FIDAMAT 5! (see Section 8)

    A prerequisite for correct startup is the presence of hydrogen/helium or hydrogen and combustionair with the appropriate inlet pressure of 30 psig and the sample gas with an inlet pressure of 10 psig(5E-AP) or 15 psig (5E-P, -G).

    The settling time differs depending on the previous use of the device. It should be 2 to 3 hours fordevices which have been used normally. The time is longer for the initial startup or with contaminateddevices.

    The device indicates the current software version when the power supply is connected. “Start” thenappears in the display. The device is in the status “Not ready”.

    The hydrogen/helium and sample gas/combustion air pressures are checked immediately at thebeginning and when the oven temperatures have been reached. If the device has already been usedcorrectly, the startup is usually carried out without readjustment of the pressure regulators (adjus-table screws on front panel).

    If the message “H2" appears in the display, the hydrogen pressure must be adjusted to 1000 mbar(980 to 1020 mbar) by means of function 35 and using the adjustable screw on the front panel. Thedevice automatically returns to ”Start" at the end of function 35.

    If the message “Air” appears in the display, it must first be made sure, that combustion air (30 psig)and sample gas (10 psig with FID 5E-AP, 15 psig with FID 5E-P and -G) are supplied with the correctpressures. Then the sample gas pressure (combustion air pressure) inside the device must beadjusted to 340 mbar by means of function 36 and using the adjustable screw on the front panel.The device then automatically returns to “Start”.

    Once the temperatures have been reached, the device automatically ignites the flame. If there is anappropriate sample gas pressure (10 psig with FID 5E-AP, 15 psig with FID 5E-P and -G) the deviceautomatically switches to the measure mode. If there is no pressure at all or insufficient pressurethe device switches to the stand-by mode and waits until there is sufficient sample gas pressure.

    7.2 Calibration

    The calibration should be carried out using gases which represent the gas to be measured as closelyas possible. Zero will always be calibrated using function 5, span using function 8.

    7.2.1 FIDAMAT 5E-G without zero and calibration gas connections, FIDAMAT 5E-AP

    The calibration is carried out via the sample gas line where the calibration gas pressure must be18 psig (FID 5E-AP) or 15 psig (FID 5E-G). The setpoint for the sensitivity (function 7) must be enteredprior to the calibration. This value can be checked using function 6 - one value must always beentered for function 7. Once the contacts have been closed for longer than 1 sec. the calibration isstarted and finished after approx. 20 sec. The adjustment by floating contacts is only possible in the“meas” mode.

    15

  • 7.2.2 FIDAMAT 5E-P without zero and calibration gas connections

    The sample gas pressure must be lower than the pressures for zero and calibration gas. Duringcalibration the excess zero and calibration gas flows back through the sample gas line.

    16

  • 8 Operation

    8.1 Description of Control Panel

    Fig. 8.1 Control panel of FIDAMAT 5E

    (1) Display of selected measuring range 1 to 4

    (2) Large display: concentration display, parameter display, fault display, status display

    (3) Small display: display of selected function codes; if the small display is dark, the largedisplay outputs the measured value

    (4) Clear key to return to basic status or to delete faulty input

    (5) Display of operating states and concentration units:"ppm C1“ etc. = display of concentration unit”warning" = common status for warnings"autocal" = the LED lights up when “autocal” is activated,

    the LED flashes during the automatic calibration"lim" = limit value exceeded"not ready" = common status for error messages

    (6) Function table for the most important functions

    (7) Switchover from measurement to calibration mode and simultaneous signalling of thesestatuses via a contact

    2

    3

    4

    C

    1

    1

    8

    3

    Limit No.

    not ready

    lim

    ppm C6

    2

    36 Display and adjust sample gas pressure

    09 Display limit (lim)

    08 Calibrate sensitivity to setpoint

    07 Set sensitivity setpoint

    06 Display sensitivity setpoint

    05 Calibrate zero

    02 Display measuring range

    01 Switch over measuring range

    35 Display and adjust H2 pressure

    warning

    Manual adjustment

    Setpoint

    Time

    MEAS

    Identifier

    Range No.

    Relay No.

    5

    CAL

    Off/On

    ENTER

    5

    2

    8

    4

    1

    CL

    6

    3

    9

    79

    6

    0

    7

    12

    1110

    4

    autocal

    mg/m 3

    ppm C3

    ppm C1

    17

  • (8) Operator prompting: the corresponding LED flashes here if further inputs are required for the entered functions

    (9) Every input must be terminated by the “ENTER” key apart from the code number

    (10) Flame monitor: The LED lights up when the flame is alight and goes out when the flame is off.

    (11) LED “Autoranging” lights up when the corresponding function (20) is active.

    (12) Dot key with the following meaning:– Decimal point– Change of sign when entering values– Start point of code entries

    8.2 Input Example

    You wish to switch over the measuring range

    Every input - apart from the codes - must be terminated by “ENTER”. Press the CL key in the event of a faulty input.

    The analyzer is in measurement mode. This means:The green LED lights up for “MEAS” next to “MEAS/CAL”.

    Input: .111Since the desired function is in function group 1, it is not necessary to enter any further codes.

    Input: press the MEAS/CAL keyThe green LED lights up next to “CAL”.The calibration status is thus signalled via pins 24/25 on plug X1.

    Input: 1The 1 appears in the small display and thus confirms the input.

    Input: ENTERThe measured value disappears in the large display, and a line appears on the right.The green LED lights up in field 6 in front of “Switch over measuring range”.The green LED simultaneously flashes in front of “Range No.” in field 8 and thus requests theinput of the new range number.

    Input: 3Measuring range 3 is selected. The input is output in the large display.

    Input: ENTERThe measured value appears in the large display.The LED “3” lights up in field 1 and indicates that range 3 is active.

    Input: press the MEAS/CAL keyThe green LED lights up next to “MEAS”.If a control panel is present, the status “Measure” is signalled to it.

    18

  • 8.3 Coding and Organization of Operating Function Groups

    The functions are combined into groups according to their type:

    To prevent important parameters from being deleted or modified by mistake, there are severalfunction levels which can only be accessed using special codes. Note that the decimal point keymust be pressed before entering a code.

    The factory settings for the codes of the three levels are:

    Level 1 .111Level 2 .222Level 3 .333

    The codes can be redefined using function 50. Function 50 also enables the device protection bycodes to be switched off for a certain time or permanently.

    Code 1 can also be set to zero so that it is omitted. The CAL key must be pressed to signal anintervention on the device to the control room if applicable.

    The device is automatically recoded by pressing the MEAS key.

    All operations permissible for a level can be carried out if you are in level 1, 2 or 3. Higher functionlevels also include the lower function levels. For example, from function level 3 you can execute alloperations of levels 0 to 3, and from level 2 all operations of levels 0 to 2.

    A description of the operation functions is provided in the appendix.

    Function groups

    0

    1

    2

    3

    Types of function

    Display functions

    Calibration and adjustment functions

    Functions for input of application parameters

    Functions for input of device parameters

    19

  • 8.4 Organization of Data Storage

    The EPROM and the EEPROM contain three parameter sets:Basic factory-set dataUser-specific dataCurrent data.

    All parameters required to operate the FIDAMAT 5E are stored in the EPROM and are protected byhardware (basic factory-set data). These data can be loaded into the current parameter memoryusing function 53. The user-specific data set is overwritten in the process, however. The basicfactory-set data can only be overwritten by a hardware intervention.

    A second parameter set (user-specific data) is present in an area of the EEPROM which can beoverwritten. The user can store a standard parameter set for his application here (see functions 55and 57).

    The third data set (current data) is the set which is automatically loaded when the analyzer isswitched on. This data set is modified according to the inputs. Note therefore when switching offthe analyzer and restarting that it is the current data set which was parameterized when the analyzerwas switched off which is loaded and not the user-specific data set.

    Fig. 8.2 Organization of data storage

    User-specificdata

    EEPROM

    Program

    RAMEPROM

    Basic factory-set data

    Currentdata

    Currentdata

    Function 57

    Automaticallywhen required

    Restart

    Function 53

    Function 55

    20

  • 9 Warnings and Error Messages

    9.1 Warnings

    The symbol precedes each warning.

    The LED “warning” flashes on the control panel. The cause of the warning can be scanned using“ENTER”. Further measurements are possible in this state. The analyzer may fail if the cause of thewarning is not eliminated.

    Number in display

    71

    73

    77

    78

    79

    80

    81

    82

    83

    84

    86

    88

    Cause of warning

    Pt100 temperature of physical section faultyor outside the limits

    Temperature of electronics section outsidethe limits (0 to 80 ˚C) or sensor faulty

    Control air flow too low

    Temperature of physical section outside thelimits (0 to 80 ̊ C)

    Hydrogen pressure outside the limits

    Sample gas pressure outside the limits

    Flame out

    Difference between actual and former zeroadjustment >6 % of full-scale value

    Output current 1 used for internal value

    Measured value exceeds full-scale value oflargest measuring range

    Incorrect device configuration (’autocal’ only)

    Incorrect measured value

    Causes, notes

    The limits defined in function 37have been violated.Hydrogen input pressure is toohigh or too low; this warning mayalso be produced if the limits aretoo close and there are extremevariations in atmosph. pressure.

    The limits defined in function 38have been violated.Combustion (control) air press-ure is too high or too low; sam-ple gas inlet faulty (filter lines);this warning may also be pro-duced if the limits are too closeand there are extreme variationsin atmospheric pressure.

    See function 62.

    Call function 96 to eliminate war-ning.

    define full-scale value (funct. 12).

    Inform service.

    Recalibrate device usingfunction(s) 5 and/or 8.

    21

  • 9.2 Faults

    The symbol precedes each fault.

    The LED “not ready” flashes on the control panel. One of the following error messages appearswhen you press “ENTER”.

    Number in display

    1

    2

    3

    4

    8

    9

    19

    40

    44

    47

    48

    49

    50

    53

    57

    60

    Error message

    Slave faulty

    Hardware fault

    Heating has switched off

    EEPROM jumper must be set

    Parameter storage test not carried out

    EPROM faulty

    Sensitivity too low

    Oven temperature outside limits or Pt100faulty

    Flame monitor faulty

    Sample gas pressure too high or too low orpressure sensor faulty

    Hydrogen pressure too high or too low orpressure sensor faulty

    High-voltage outside limits

    Operating voltages outside setpoints

    Oven temperature setpoint exceeded orfallen below

    Combustion air/sample gas pressure too low

    Flame does not ignite (30 min)

    Comment

    Pull mains plug immediately,inform service

    Inform service

    RESET

    Inform service

    See u8, next page

    Order replacement from manufacturer

    Incorrect calibration gas, incorrect measuring range, see functions 2 and 6

    Check contacts

    Check contacts

    Check cylinder pressure, readjust, check pressure sensor

    Check cylinder pressure, readjust, check pressure sensor

    Check whether high-voltage lineis connected

    Check power supply and con-nections on transformer

    Combustion air line interrupted

    Check gas flows

    22

  • Number in display

    8

    234

    5

    11

    12

    1516

    1718

    20

    21

    22

    37

    38

    200

    201

    202

    203

    204

    Cause of error

    Parameter storage test not carried out

    A: Analyzer does not react to ENTER

    B: One of the following error numbers is dis-played when you press ENTER. A further num-ber may be displayed when the error has beeneliminated.

    Cause

    Code 1Code 2Code 3

    Assignment of current output 1

    Number of measuring ranges

    Measuring range

    Sensitivity adjustmentSensitivity setpoint

    Start-of-scale valueFull-scale value

    Limits

    Zero

    Sensitivity

    Limits of time constant T90

    Dynamic noise rejection

    Baud rate

    Transmission procedure

    Start, end, don’t care characters

    Calibration of analog current

    Adjustment of preamplifier

    Comment

    Press dot key for 30 sec untilfunction 50 appears in the smalldisplay; recode the analyzer.Then reload basic data into RAMusing function 53 or 55.

    Correct the value in the corrre-sponding function using the fol-lowing table.

    Check/input using function No.

    505050

    62, identifier 0

    51

    1

    17 7

    1112

    18 / 19

    5

    17 / 7 / 8

    13

    14

    80

    81

    82

    Contact service

    Contact service

    23

  • 10 Spare Parts and Accessories

    10.1 FIDAMAT 5E-AP

    Order No.

    Flame ionization detector, complete C79451-A3405-B578

    FID cover complete with thermocouple line C79451-A3405-B501

    Quartz nozzle for FIDAMAT 5E-AP C79402-Z1282-C2

    Clamping screw in the FID C79211-A3003-C15

    Nut for M5 connection C79451-A3040-D126

    Outer ring for M5 connection C79451-A3040-D121

    Graphite gasket for M5 connection C79451-A3040-D102

    Clamping ring for M5 connection C79451-A3040-D112

    Nut for M7 x 0.75 connection, tube 1.5 to 3.0 C79451-A3040-D127

    Outer ring for M7 x 0.75 connection, tube 1.5 to 3.0 C79451-A3040-D122

    Graphite gasket for M7 x 0.75 connection, pipe 1.5 C79451-A3040-D103

    Clamping ring for M7 x 0.75 connection, pipe 1.5 C79451-A3040-D113

    Graphite gasket for M7 x 0.75 connection, pipe 3.0 C79451-A3040-D105

    Clamping ring for M7 x 0.75 connection, pipe 3.0 C79451-A3040-D115

    Coarse filter C79451-A3405-C169

    Sample gas restrictor (fused silica), complete, 5E-AP C79451-A3405-B190

    Crimp restrictor 1, hydrogen, 5E-AP C79451-A3405-C163

    Crimp restrictor 2, combustion air, 5E-AP C79451-A3405-C226

    Crimp restrictor 3, auxiliary air, 5E-AP C79451-A3405-C224

    Crimp restrictor 4, exhaust, 5E-AP C79451-A3405-C227

    Crimp restrictor 5, sample gas, 5E-AP C79451-A3405-C192

    Temperature sensor, complete, FID oven and physical section C79451-A3405-B103

    Flat heater element, FID oven, top C79451-A3405-B102

    Flat heater element, FID oven, bottom C79451-A3405-B101

    Cable connector for input signal C79451-A3405-B109

    Cable connector for FID voltage C79451-A3405-B110

    24

  • Order No.

    Cable connector for pressure sensor for combustion air C79451-A3405-B105

    Cable connector for pressure sensor for hydrogen C79451-A3405-B106

    Solenoid valve for combustion air, complete C79451-A3040-B210

    Solenoid valve for H2, sample gas, combustion air complete C79451-A3040-B206

    Solenoid valve for control air, combustion air, H2 C79402-Z871-A5

    Gasket, diameter 4 mm C79451-A3040-C331

    Gasket, diameter 6 mm C79451-A3040-C354

    Gasket, diameter 10 mm C79451-A3040-C353

    O-ring, diameter 10 mm F79402-E871-A1

    Pressure controller, hydrogen, combustion air/sample gas C79451-A3405-B20

    PTFE gasket for M7 x 0.75 connection, tube 1.5 C79451-A3040-D101

    Elbow compression gland C75304-Z1209-C2

    Union nut for pipe R1/4" available only as set Clamping ring, front, pipe R1/4" of parts, order no.Clamping ring, rear, pipe R1/4" C79451-A3405-D62

    Analyzer fuse, T 6.3 A/120 V W79054-L1011-T630

    Motherboard C79451-A3405-B507

    Preamplifier board C79451-A3405-B508

    Control board C79451-A3405-B509

    ROM, motherboard position D3, 5E-AP, master S79610-G152-A901

    ROM, motherboard position D4, 5E-AP, slave S79610-G152-A902

    Display board (front panel) C79451-A3210-A502

    Touch pad keyboard with labels, German C79451-A3405-D52

    Touch pad keyboard with labels, English C79451-A3405-D53

    Touch pad keyboard with labels, French C79451-A3405-D54

    Touch pad keyboard with labels, Spanish C79451-A3405-D55

    Touch pad keyboard with labels, Italian C79451-A3405-D56

    25

  • 10.2 FIDAMAT 5E-P

    Order No.

    Flame ionization detector, complete C79451-A3405-B510

    FID cover complete with thermocouple line C79451-A3405-B501

    Quartz nozzle for FIDAMAT 5E-P C79402-Z1282-C1

    Clamping screw in the FID C79211-A3003-C15

    Nut for M5 connection C79451-A3040-D126

    Outer ring for M5 connection C79451-A3040-D121

    Graphite gasket for M5 connection C79451-A3040-D102

    Clamping ring for M5 connection C79451-A3040-D112

    Nut for M7 x 0.75 connection, tube 1.5 to 3.0 C79451-A3040-D127

    Outer ring for M7 x 0.75 connection, tube 1.5 to 3.0 C79451-A3040-D122

    Graphite gasket for M7 x 0.75 connection, pipe 1.5 C79451-A3040-D103

    Clamping ring for M7 x 0.75 connection, pipe 1.5 C79451-A3040-D113

    Sample gas filter, complete C79451-A3405-B21

    Gasket, sample gas filter C79451-A3405-C43

    Gasket, sample gas filter C79451-A3405-C44

    Filter cylinder 3 µm C79127-Z970-C1

    Spring washer for sample gas filter C79451-A3405-C47

    Sample gas restrictor (fused silica), complete, 5E-P C79451-A3405-B173

    Crimp restrictor 1, hydrogen, 5E-P C79451-A3405-C152

    Crimp restrictor 2, combustion air, 5E-P C79451-A3405-C153

    Crimp restrictor 3, auxiliary air, 5E-P C79451-A3405-C154

    Crimp restrictor 4, exhaust, 5E-P C79451-A3405-C155

    Crimp restrictor 5, zero gas, calibration gas(es), 5E-P C79451-A3405-C223

    Temperature sensor, complete, FID oven and physical section C79451-A3405-B103

    Flat heater element, FID oven, bottom C79451-A3405-B101

    Flat heater element, FID oven, top C79451-A3405-B102

    26

  • Order No.

    Cable connector for pressure sensor for combustion air C79451-A3405-B105

    Cable connector for pressure sensor for hydrogen C79451-A3405-B106

    Cable connector for input signal C79451-A3405-B109

    Cable connector for FID voltage C79451-A3405-B110

    Flow monitor C79451-A3407-B53

    Solenoid valve for control air, complete C79451-A3405-B210

    Solenoid valve for H2, combustion air, complete C79451-A3040-B206

    Solenoid valve for zero gas/calibration gas, complete C79451-A3405-B37

    Solenoid valve for control air, H2, combustion air C79402-Z871-A5

    Solenoid valve for for zero gas, calibration gas C79402-Z871-A7

    Gasket, diameter 4 mm C79451-A3040-C331

    Gasket, diameter 6 mm C79451-A3040-C354

    Gasket, diameter 10 mm C79451-A3040-C353

    O-ring, diameter 10 mm F79402-E871-A1

    Pressure controller, hydrogen, combustion air/sample gas C79451-A3405-B20

    Union nut for pipe 6 available only as set Clamping ring, front, pipe 6 of parts, order no.Clamping ring, rear, pipe 6 C79451-A3405-D60

    Union nut for pipe 8 available only as set Clamping ring, front, pipe 8 of parts, order no.Clamping ring, rear, pipe 8 C79451-A3405-D61

    Union nut for pipe R1/4" available only as set Clamping ring, front, pipe R1/4" of parts, order no.Clamping ring, rear, pipe R1/4" C79451-A3405-D62

    PTFE gasket for M7 x 0.75 connection, tube 1.5 C79451-A3040-D101

    Analyzer fuse, T 4.0 A/250 V W79054-L1011-T400

    Analyzer fuse, T 6.3 A/250 V W79054-L1011-T630

    27

  • Order No.

    Motherboard C79451-A3405-B507

    Preamplifier board C79451-A3405-B508

    Control board C79451-A3405-B509

    ROM, motherboard D3, 5E-P S79610-G142-A901

    ROM, motherboard D4, 5E-P S79610-G142-A902

    Display board (front panel) C79451-A3210-A502

    Touch pad keyboard with labels, German C79451-A3405-D52

    Touch pad keyboard with labels, English C79451-A3405-D53

    Touch pad keyboard with labels, French C79451-A3405-D54

    Touch pad keyboard with labels, Spanish C79451-A3405-D55

    Touch pad keyboard with labels, Italian C79451-A3405-D56

    28

  • 10.3 FIDAMAT 5E-G

    Order No.

    Flame ionization detector, complete C79451-A3405-B510

    FID cover complete with thermocouple line C79451-A3405-B501

    Quartz nozzle for FIDAMAT 5E-G C79402-Z1282-C1

    Clamping screw in the FID C79211-A3003-C15

    Nut for M5 connection C79451-A3040-D126

    Outer ring for M5 connection C79451-A3040-D121

    Graphite gasket for M5 connection C79451-A3040-D102

    Clamping ring for M5 connection C79451-A3040-D112

    Nut for M7 x 0.75 connection, tube 1.5 to 3.0 C79451-A3040-D127

    Outer ring for M7 x 0.75 connection, tube 1.5 to 3.0 C79451-A3040-D122

    Graphite gasket for M7 x 0.75 connection, pipe 1.5 C79451-A3040-D103

    Clamping ring for M7 x 0.75 connection, pipe 1.5 C79451-A3040-D113

    Graphite gasket for M7 x 0.75 connection, pipe 3.0 C79451-A3040-D105

    Clamping ring for M7 x 0.75 connection, pipe 3.0 C79451-A3040-D115

    Coarse filter C79451-A3405-C169

    Sample gas restrictor (fused silica), complete, 5E-G C79451-A3405-B174

    Crimp restrictor 1, hydrogen, 5E-G C79451-A3405-C152

    Crimp restrictor 2, combustion air, 5E-G C79451-A3405-C153

    Crimp restrictor 3, auxiliary air, 5E-G C79451-A3405-C222

    Crimp restrictor 4, exhaust, 5E-G C79451-A3405-C155

    Crimp restrictor 5, sample gas, 5E-G C79451-A3405-C223

    Temperature sensor, complete, FID oven and physical section C79451-A3405-B103

    Flat heater element, FID oven, bottom C79451-A3405-B101

    Flat heater element, FID oven, top C79451-A3405-B102

    Cable connector for input signal C79451-A3405-B109

    Cable connector for FID voltage C79451-A3405-B110

    Cable connector for pressure sensor for combustion air C79451-A3405-B105

    29

  • Order No.

    Cable connector for pressure sensor for hydrogen C79451-A3405-B106

    Flow monitor C79451-A3407-B53

    Solenoid valve for H2, combustion air, complete C79451-A3040-B206

    Solenoid valve for zero gas, calibration gas, sample gas, compl. C79451-A3405-B38

    Solenoid valve for control air, H2, C79402-Z871-A5

    Solenoid valve for for zero gas, calibration gas, sample gas C79402-Z871-A7

    Gasket, diameter 4 mm C79451-A3040-C331

    Gasket, diameter 6 mm C79451-A3040-C354

    Gasket, diameter 10 mm C79451-A3040-C353

    O-ring, diameter 10 mm F79402-E871-A1

    Pressure controller, hydrogen, combustion air, sample gas C79451-A3405-B20

    PTFE gasket for M7 x 0.75 connection, tube 1.5 C79451-A3040-D101

    Elbow compression gland, 5E-G C79304-Z1209-C2

    Union nut for pipe 6 available only as set Clamping ring, front, pipe 6 of parts, order no.Clamping ring, rear, pipe 6 C79451-A3405-D60

    Union nut for pipe R1/4" available only as set Clamping ring, front, pipe R1/4" of parts, order no.Clamping ring, rear, pipe R1/4" C79451-A3405-D62

    Analyzer fuse, T 4.0 A/230 V W79054-L1011-T400

    Analyzer fuse, T 6.3 A/230 V W79054-L1011-T630

    Motherboard C79451-A3405-B507

    Preamplifier board C79451-A3405-B508

    Control board C79451-A3405-B509

    ROM, motherboard D3, 5E-G S79610-G168-A901

    ROM, motherboard D4, 5E-G S79610-G168-A902

    Display board (front panel) C79451-A3210-A502

    30

  • Order No.

    Touch pad keyboard with labels, German C79451-A3405-D52

    Touch pad keyboard with labels, English C79451-A3405-D53

    Touch pad keyboard with labels, French C79451-A3405-D54

    Touch pad keyboard with labels, Spanish C79451-A3405-D55

    Touch pad keyboard with labels, Italian C79451-A3405-D56

    31

  • 32

  • 11 Appendix

    11.1 Gas Flow Diagram

    Fig. 11.1 FIDAMAT 5E-P for process measurements

    Measuringchamber

    RestrictorFused silica

    Pressuresensor

    optional

    Pressure regulator

    Flowmonitor

    outlet(atmosphericpressure)

    external solenoid valve,controllable viapins 3 and 4 of plug X2

    zero gas, inlet pressure 18 psig

    Solenoidvalve

    Combustion gas(H2/He), inletpressure 30 psig

    Solenoid valve

    Pressureregulastor

    1

    2

    Solenoid valve

    Pressuresensor

    combustion air,inlet pressure 30 psig

    Restrtictors

    calibration gas 1,inlet pressure 18 psig

    sample gas,inlet pressure 15 psig

    Coarse filter

    A-1

  • Fig. 11.2 FIDAMAT 5E-AP for car exhaust measurements

    Measuringchamber

    RestrictorFused silica

    Pressuresensor

    Restrtictors

    191 ˚C

    Pressure regulator

    Pressuresensor

    outlet(atmosphericpressure)

    combustion air,inlet pressure 30 psig

    sample gas,inlet pressure 10 psig

    Solenoidvalve

    Combustion gasinlet pressure 30 psig

    Solenoid valve

    Pressureregulastor

    1

    3

    2

    Solenoid valve

    A-2

  • Fig. 11.3 FIDAMAT 5E-G for measurements of gases of highest-grade purity

    Measuringchamber

    RestrictorFused silica

    Pressuresensor

    Pressure regulator

    Flowmonitor

    outlet(atmosphericpressure)

    zero gas, inlet pressure 15 psig

    Solenoidvalve

    Combustion gas(H2/He), inletpressure 30 psig

    Solenoid valve

    Pressureregulastor

    1

    2

    Pressuresensor

    combustion air,inlet pressure 30 psig

    Restrtictors

    calibration gas 1,inlet pressure 15 psig

    sample gas,inlet pressure 15 psig

    Coarse filter

    A-3

  • 11.2 Layout Diagrams of Important Electronic Components

    Fig. 11.4 Motherboard (top) and control board

    Control board

    Heat sink Potentiometer foradjustment of flow sensor

    Terminal strips

    Motherboard

    Slave

    EEPROM protection switch

    Master

    Cooling rail

    A-4

  • 11.3 Summary of Operating Functions

    Symbols in the sequence diagrams

    Display of set value and possible adjustmnet for a new value.When entering values make sure to enter the sign first!

    ENTER key (importing of numbers)

    Display output in large display (the measured value is displayed again after approx. 3 s)

    Input

    Function protected by code 1 (function level 1)

    Function protected by codes 1 and 2 (function level 2)

    Function protected by codes 1, 2 and 3 (function level 3)

    Symbols in the display

    Enter identifier

    The MEAS/CAL key must be pressed

    Illegal code, illegal identifier, non-existent function number entered

    Enter code according to function level

    Error message

    Warning

    Remarks

    The input can be interrupted at any time using the CL key; the old values are then retained and thesystem returns to the start of the function or partial function.

    ******

    CAL

    ILL

    cod

    A-5

  • Survey of operating functions

    * 96 Switch over between mg/m3 and ppm

    2 Display measuring range

    * 1 Switch over measuring range

    Display and switch over measuring ranges, switch over displayA

    * 8 Calibrate sensitivity to setpoint

    * 7 Adjust sensiitivity setpoint

    6 Display sensitivity setpoint

    * 5 Calibrate zero

    Calibration of measuring rangesB

    Temperatures, pressures, flow, limits D

    * 36 Display, set sample gas pressure

    * 35 Display, set H2 or H2/He pressure

    ** 34 Display, set max. temperature deviation

    * 38 Enter tolerance for sample gas pressure

    * 37 Enter tolerance for hydrogen or hydrogen/helium pressure

    ** 20 Autoranging “on/off”

    A-6

  • Time constantsE

    Adjustment and calibration functions

    *** 73 Compensation of temperature influence on measured value

    *** 71 Compensation of temperature influence on zero

    ** 14 Set dynamic time constant TD (dynamic noise rejection)

    ** 13 Set time constant T90

    Measured-value memory, current output

    ** 24 Set current output

    ** 21 Measured-value memory on/off

    Redefine measuring ranges

    ** 12 Define full-scale values of measuring ranges

    ** 11 Define start-of-scale values of measuring ranges

    ** 51 Select number of valid measuring ranges

    Further display functions

    60 Display internal values

    15 Display compensated background current (zero calibration)

    61 Display measured variables

    F

    G

    I

    K

    A-7

  • Reprogram, activate, deactivate codes

    *** 78 Suppression of negative measured values

    *** 77 Suppression of brief noise signals

    69 LED check, software no.

    *** 68 RESET

    *** 99 Switch analyzer on/off

    * 92 Display warnings and brief errors

    *** 67 Ignite flame

    *** 62 Reproduce internal values on analog signal, channel 1

    *** 50 Reprogram, activate/deactivate codes

    Test functions, RESET, switch-off

    *** 57 Store user-specific data

    M

    L

    *** 53 Load basic factory-set data

    ** 49 Switch valves individually

    * 29 Measure during warm-up phase

    *** 55 Load user-specific data

    * 94 Switch over between mg/m3 and ppm

    A-8

  • * 5 Calibrate zero

    2 Display measuring range

    * 1 Switch over measuring range

    A

    B

    A

    ** 12 Define full-scale values of measuring ranges G

    ** 11 Define start-of-scale values of measuring ranges G

    * 8 Calibrate sensitivity to setpoint B

    * 7 Adjust sensitivity setpoint B

    6 Display sensitivity setpoint B

    D

    * 29 Measure during warm-up phase L

    ** 24 Set current output F

    ** 21 Measured-value memory on/off F

    ** 20 Autoranging on/off A

    15 Display compensated background current (zero calibration) I

    ** 14 Set dynamic time constant TD (dynamic noise rejection) E

    ** 13 Set time constant T90 E

    * 36 Display, set sample gas pressure

    * 35 Display, set H2 or H2/He pressure

    ** 34 Display, set max. temperature deviation

    * 38 Enter tolerance for sample gas pressure

    * 37 Enter tolerance for hydrogen or hydrogen/helium pressure

    D

    M

    D

    G** 51 Select number of valid measuring ranges

    *** 50 Reprogram, activate/deactivate codes

    ** 49 Switch valves individually

    D

    L

    D

    A-9

  • *** 62 Reproduce internal values on analog signal, channel 1

    61 Display measured variables

    60 Display internal values

    *** 57 Store user-specific data

    *** 55 Load user-specific data

    *** 53 Load basic factory-set data

    *** 73 Compensation of temperature influence on measured value

    *** 71 Compensation of temperature influence on zero

    *** 67 Ignite flame

    *** 99 Switch analyzer on/off

    * 92 Display warnings and brief errors

    *** 78 Suppression of negative measured values

    *** 77 Suppression of brief noise signals

    69 LED check, software no.

    *** 68 RESET

    L

    L

    L

    L

    L

    L

    I

    I

    L

    L

    L

    L

    K

    K

    L

    96 Display ∆ zero adjustment

    L

    * 94 Switch over between mg/m3 and ppm A

    A-10

  • AA Display and switch over measuring ranges

    The start-of-scale and full-scale values of the measuring range are output in succession in thedisplay.

    There are four measuring ranges. The measu-ring range which is switched on is indicated tothe right of the display. The number of activemeasuring ranges can be defined using function51.The start-of-scale and full-scale values of themeasuring range can be freely selected.

    Factory setting: 1

    * 1 Switch over measuring range

    Measuring range No.

    CL

    1

    2 Display measuring range

    Display

    Measuring range No.

    CL

    2

    This function only applies to the recorder output(see plug connector X1). The current measuredvalue is always output on the display even if itexceeds the current measuring range.The displayed value flashes when the measuringrange(s) is exceeded.

    Factory setting: 0

    ** 20 Autoranging on/off

    Manual switchover

    Autoranging

    0

    2 1

    CL

    0

    The LED on the right of the display indicates theconcentration unit of the display.

    Factory setting: 0

    * 94 Switch over between mg/m3 and ppm

    ppm C3

    mg C/m3

    3

    9

    2

    CL

    4

    1

    0

    ppm C6

    ppm C1

    A-11

  • BB Calibration of measuring ranges

    Zero gas valve opens after pressing 5 and EN-TER. If there is no such valve, zero gas must befeeded via the sample gas line. After havingpressed the ENTER key once more the calibra-tion will be carried out and the zero gas valve (ifpresent) will be closed.

    * 5 Calibrate zero (FIDAMAT 5E-AP only)

    5

    The setpoint is displayed which was used for thelast calibration. The measuring range in whichthe setpoint is present is output to the right ofthe display.

    * 5 Calibrate zero (FIDAMAT 5E-P only)

    5 Display

    Identifier: 1 = calibration gas 1 for range 1 (to 4)

    The setpoint must be reset when the calibrationgas is changed.All four ranges are calibrated using the samecalibration gas.

    * 7 Adjust sensitivity setpoint

    SetpointIdentifier

    7

    CL

    n

    The sequence is analogous to function 5.

    A calibration gas is used to calibrate measuringrange 1. The other measuring ranges are alsocalibrated.

    * 8 Calibrate sensitivity to setpoint

    Prior to the activation of this function zero gasmust be applied via the sample gas input. 20 s.after activation of function 5 the calibration willbe carried out automatically.

    6 Display sensitivity setpoint

    Measuring range No.

    CL

    6 Display

    A-12

  • Temperatures, pressures, flow, limits DD

    The entered pressure deviation, usually 30 to100 mbar, specifies the maximum permissibledeviation from the setpoint which has been setusing function 36.A warning is output if the sample gas pressureexceeds or falls below this value.

    Factory setting: 30

    * 38 Enter tolerance for sample gas pressure

    3

    Pressure deviationin mbar (0 - 255)

    CL

    8

    The sample gas pressure is output on the dis-play in mbar and can be adjusted using thebottom screw on the front panel. The technicaldata refer to an overpressure of 340 mbar (FID5E-AP) or 500 mbar (FID 5E-P and 5E-G). The pressures will be less if there is no samplegas or combustion air.

    * 36 Display, set sample gas pressure

    Display 63

    The hydrogen/helium pressure is output on thedisplay in mbar and can be adjusted using thetop screw on the front panel. The technical datarefer to an overpressure of 1000 mbar.

    * 35 Display, set H2/He or H2 pressure

    This function defines how far the oven tempera-tures may deviate upwards or downwards fromthe setpoint temperature. A warning is output ifthe temperature deviates by more than this va-lue for one of the four heaters.

    Factory setting: 5

    ** 34 Display, set max. temperature deviation

    3

    temperature deviation in ˚C

    2 to 10

    CL

    4

    The entered pressure deviation, usually 50 to100 mbar, specifies the maximum permissibledeviation from the setpoint which has been setusing function 35.A warning is output if the hydrogen pressureexceeds or falls below this value.

    Factory setting: 50

    * 37 Enter tolerance for hydrogen pressure

    3

    Pressure deviationin mbar(0 - 255)

    CL

    7

    Display53

    A-13

  • EE

    Measured-value memory, current output FF

    If the measured-value memory is switched on,the last measured value is stored when the CALkey is pressed. It is then present at the mA outputuntil the analyzer is reset to the measurementstatus by pressing the MEAS key.The measured value is also stored in the displayin the event of an error.

    Factory setting: 0

    ** 21 Measured-value memory on/off

    Off

    On

    0

    2 1

    CL

    1

    The time constant TD applies to small changesin signal without a defined range ∆ (in % ofrespective f.s.v.). The time T90 defined infunction 13 applies to larger changes in signal.TD must be larger than T90. In this manner, noiseis optimally suppressed in the case of smallchanges; in the case of larger changes (> ∆ ), the modified signal is recorded faster byautomatic switching over to the time constantT90.

    Factory setting: 3.0/1.0

    The time constant T90 (0.1 to 100 s) is used toreduce the noise. The signal delay increaseswith increasing T90.

    Factory setting: 0.0

    ** 14 Set dynamic time constant TD (dynamic noiserejection)

    ** 13 Set time constant T90

    4

    Identifier ∆ (% of f.s.v.)0.0 to 100.0

    CL

    1

    2

    1

    TD (0.0 to 100 s)Identifier

    Time constants

    1

    T90 0.0 to 100 seconds

    CL

    3

    Status0 0 to 20 mA1 2 to 20 mA2 4 to 20 mA

    Factory setting: 2

    CL

    4

    Status

    2

    ** 24 Set current output

    A-14

  • GG Redefine measuring ranges

    The full-scale values can be set as desired. Theonly condition is that the start-of-scale value setusing function 11 is greater than the full-scalevalue set here. The unit displayed when the setting is madeapplies as the unit to the value entered here.

    Factory setting: 10/50/200/1000

    ** 12 Define full-scale values of measuring ranges

    CL

    Range

    21

    Full-scale value

    The start-of-scale values can be set as desired.The only condition is that the full-scale value setusing function 12 is greater than the start-of-sca-le value set here. The unit displayed when the setting is madeapplies as the unit to the value entered here.

    Factory setting: 0

    ** 11 Define start-of-scale values of measuring ranges

    CL

    Range

    11

    Start-of-scale value

    The number of valid measuring ranges is se-lected. Autoranging (function 20) only takesplace within the selected ranges.

    Identifier:1 = measuring range 12 = measuring ranges 1 and 23 = measuring ranges 1, 2 and 34 = measuring ranges 1, 2, 3 and 4

    Factory setting: 4

    CL

    n

    Identifier

    5 1

    ** 51 Select number of valid measuring ranges

    A-15

  • II Further display functions

    The current compensated in the zero is display-ed here in pA.

    15 Display compensated background current (zero calibration)

    Identifier:1 = Oven temperature (100 to 200 ˚C)2 = Physical section temperature

    (10 to 60 ˚C)

    7 = Flame temperature (230 to 300 ˚C)9 = Temperature of board (10 to 70 ˚C)

    11 = Pressure of sample gas/combustion air (mbar abs.)

    12 = Hydrogen/helium pressure (~1000 mbar absolute)

    14 = FID voltage (200 V)15 = +15 V16 = – 15 V17 = +24 V

    Identifier: n =0 = Measured value1 = Raw measured value (pA)2 = Analog current 3 = Current following adjustment of

    preamplifier4 = Current following zero adjustment

    Terminating this function via CL key sets theidentifier automatically to 0.

    Identifier n notequal to 0

    6

    CL

    n

    1

    Identifier

    n

    61 Display measured variables

    6

    CL

    Display0

    Identifier

    * 60 Display internal values

    Display51

    A-16

  • KK Adjustment and calibration functions

    Iden-tifier Value

    1 Basic temperature(Temperature 0)

    (Value 2 - Value 0)2 * 1000

    (Temp. 2 – Temp. 0)

    (Value 0 - Value 1)3 * 1000

    (Temp. 0 – Temp. 1)

    Service staff only!

    Iden- Setpointtifier

    1 Temperature of analyzer section withaverage ambient temperature (in ˚C;see function 60, identifier 2)

    2 Change in display with increase in temperature (function 61, identifier 4)

    3 Change in display with reduction in temperature (function 61, identifier 4)

    Procedure

    1. Calibrate zero of basic temperature(function 5)

    2. Switch on measuring range 13. Select function 71 and enter a value of

    zero for identifiers 2 and 34. Measure (see example)5. Enter identifier and setpoints under

    function 71

    Caution! Function 71 might influence zero!

    *** 71 Compensation of temperature influence onzero

    CL

    7 1

    Identifier value

    n

    Example:Value 1 with Temp. 1 < Temp. 0

    Value 0, 1, 2 is the measured value (asindicated under function 61, identifier 4)

    Value 0 with Temp. 0

    Value 2 with Temp. 2 > Temp. 0

    Zero at average ambient temperature(e. g. 25 ˚C)

    A-17

  • KK Adjustment and calibration functions

    Iden-tifier Value

    1 Basic temperature(Temperature 0)

    (Value 2 - Value 0)2 * 1000

    (Temp. 2 – Temp. 0)

    (Value 0 - Value 1)3 * 1000

    (Temp. 0 – Temp. 1)

    Service staff only!

    Iden- Setpointtifier

    1 Temperature of analyzer section withaverage ambient temperature (in ˚C;see function 60, identifier 2)

    2 Change in display with increase in temperature

    3 Change in display with reduction in temperature

    Procedure

    1. Calibrate sensitivity at basic temperature (function 8)

    2. Switch on measuring range matching the calibration gas used

    3. Select function 73 and enter a value of zero for identifiers 2 and 3

    4. Measure (see example)5. Enter identifier and setpoints under

    function 73

    *** 73 Compensation of temperature influence onmeasured value

    CL

    7 3

    Identifier value

    n

    Example:Value 1 with Temp. 1 < Temp. 0

    Value 0 with Temp. 0

    Value 2 with Temp. 2 > Temp. 0

    Zero at average ambient temperature(e. g. 25 ˚C)

    Value 0, 1, 2 is the measured value

    A-18

  • LL

    *** 55 Load user-specific data

    55

    *** 57 Store user-specific data

    75

    *** 53 Load basic factory-set data

    35

    Test functions, RESET, switch-off

    The measured signal can be observed duringthe warming-up phase.

    Factory setting: 0

    ** 29 Measure during warming-up phase

    Off

    On

    0

    2 1

    CL

    9

    The various gas valves can be switched indivi-dually independent of the operating mode “au-tocal”.

    Identifier:1 = hydrogen/helium or hydrogen2 = combustion air/control air supply3 = control air valve (FID 5E-P, -AP)

    sample gas valve (FID 5E-G)4 = zero gas valve (FID 5E-P, -G)5 = calibration gas valve (FID 5E-P, -G)

    Note that all valves are closed when off. Thismeans that purging is possible in the switched-off status. It is also possible that a small quantityof air might flow back through the sample gasline.

    ** 49 Switch valves individually

    4

    Open

    CL

    n

    Identifier Closed

    0

    1

    9

    The application parameters present in the basicdata memory can be transferred to the mainmemory.The device carries out a restart when thisfunction is triggered.

    A parameter configuration defined by the usercan be held in the memory. This data set isloaded automatically each time the device isswitched on.

    Programming with original data (status whendelivered from factory).Servicing function!The device carries out a restart when thisfunction is triggered.

    Identifier: n =

    0 = Measured value (depends on actualmeasuring range)

    1 = Oven temperature (0 – 300 ˚C)7 = Flame temperature (0 – 800 ˚C)9 = Temperature of board (0 – 80 ˚C)

    11 = Pressure of sample gas/combustion air (0 – 3000 mbar abs.)

    12 = Hydrogen pressure (0 – 3000 mbar abs.)

    14 = FID voltage (0 – 1500 V)15 = +15 V (14 – 16 V)16 = –15 V (–14 – –16 V)17 = +24 V (22 – 26 V)

    18/19/20/21/22/23= –1/0/4/10/20/21 mA

    24 = raw current (depends on actual measuring range)

    Display

    CL

    6 2Identifier

    *** 62 Reproduce internal values on analog signal, channel 1

    A-19

  • LL LL

    *** 68 RESET

    86

    *** 69 LED check, software no.

    96

    The analyzer attempts to ignite the flame forapprox. 20 minutes.

    The ignition process can be terminated by ente-ring “0".

    The procedure is terminated automatically whenthe flame is ignited.

    Factory setting: 0

    *** 67 Ignite flame

    Ignition on

    Ignition off

    1

    6 0

    CL

    7

    This function must be used in the event of faultsin the program sequence. The analyzer is set tothe status of the warming-up phase.

    The entered time corresponds to a dead timewhich will be effective only if the measured valueexceeds the value entered under function 14,identifier 2. The originally entered value remainsuntil the measured value falls below the valueentered under function 14, identifier 1. If thevalue is 0, the dynamic time constant enteredunder function 14, identifier 2, is active (normaloperation)

    Factory setting: 0

    CL

    7 7

    Time in seconds (0.0 to 10.0 s)

    *** 77 Suppression of brief noise signals

    All LEDs light up. After 5 seconds, the two soft-ware versions appear in succession in thedisplay.

    The display and output of negative values canbe suppressed using this function. The analyzerthen displays a value of 0.00 in these cases.

    Factory setting: 0

    *** 78 Suppression of negative measured values

    Negative values are alsodisplayed

    No negative values

    0

    7 1

    CL

    8

    Test functions, RESET, switch-off

    The measured value is displayed if function 92is switched on. The function number 92 appearsin the small display. The measured value isdeleted in the large display when an error oc-curs, and the error code is displayed.

    No other function can be called when function92 is active.

    * 92 Display warnings and brief errors

    Display measured value or

    error/warning if present

    9

    CL

    2

    A-20

  • Test functions, RESET, switch-off LL

    Identifier 1 switches off the device in a controlledmanner. The hydrogen and sample gas suppliesare interrupted. Combustion air is supplied for afurther 30 seconds.

    The device startup is initiated using identifier 0.

    Factory setting: 0

    *** 99 Switch analyzer on/off

    Switch off

    On

    1

    9 0

    CL

    9

    This function can be used to automatically com-pare the previous and new zero and sensitivitycalibrations. A warning is output if the differencebetween the two calibrations is > 6 %. Thevalues can be viewed using identifiers 3 and 4.The warning LED is cancelled when function 96is called, and the status signal at plug X2 is setto "No warning" again.

    96 Display ∆ of zero adjustment

    ∆ zero

    off

    3

    9

    2

    CL

    6

    1

    0

    ∆ span

    ON

    A-21

  • MM Reprogram, activate and deactivate codes

    Identifiers

    1 = codes are active

    2 = codes are not active; all operating functions are freely accessible. The codes are automatically reactivated if a function is not selected within 15 minutes.

    3 = codes are permanently inactive. They are activated again by identifier 1.

    4 = reprogram codes (see special sheet in appendix).

    Factory setting: 1

    *** 50 Reprogram, activate/deactivate codes

    Identifier

    4

    5

    3

    CL

    0

    2

    1

    Special operatorprompting

    Identifier

    Identifier

    Identifier

    A-22

  • This sheet should be removed from the Instruction Manual and stored separately.

    11.4 Special Sheet for Storage of Current Coding

    FIDAMAT 5E gas analyzer

    Remarks

    *** 50 Reprogram of codes

    0 Code 25

    05

    Smalldisplay

    1. Function 50 is only accessible via the current codes (1 to 3)

    2. Code 1 is omitted if it is programmed to 000.

    3. The current codes can be bypassed using a time function if they are no longer known and thus reprogrammed.

    Current codes

    Code 2

    Press for approx. 30 s

    222

    Code 3Code 1

    Code 1

    333111

    Code 3

    Function and code

  • FIDAMAT 5E Data Sheet: Parameters and Measured Values

    Meas. range

    1

    2

    3

    4

    Function 11 Function 12 FIDAMAT 5E: ___________

    Order no.: ________________________________ _ _ _ _

    Fab. no.: _________________________________ _ _ _ _ _ _ _ _ _ _ _ ____

    SW Release no.: Master: ______ Slave: _________

    Mains voltage: V AC________________________ _ _ _ _ _ _ _ _ _ _ ______

    Designation

    Internal values in measurementmode

    Ambient temperature

    = ____________ ˚C

    Internal values in stand-bymode

    Display measured varisbles (pA)using zero gas

    Compensation of temperatureinfluence on zero

    Compensation of temperatureinfluence on span

    Suppression of noise signals

    Suppression of negative measured values

    Unit of measured value

    Display ∆ zero calibration

    Function no.

    60, ident. 1

    60, ident. 2

    60, ident. 3

    60, ident. 4

    60, ident. 5

    60, ident. 6

    60, ident. 7

    60, ident. 8

    60, ident. 9

    60, ident. 10

    60, ident. 11

    60, ident. 12

    60, ident. 13

    60, ident. 14

    60, ident. 10

    60, ident. 11

    61, ident. 1

    71, ident. 1

    71, ident. 2

    71, ident. 3

    73, ident. 1

    73, ident. 2

    73, ident. 3

    77

    78 1 on0 off

    94

    96 1 on0 off

    2, 3 values

    Parameter/measured value

    Designation

    Set time constant

    Dynamic noisesuppression

    Total calibration

    Individual calibration

    Autoranging

    Measured-valuememory

    Autocal

    Limit monitoring

    Current output(mA)

    Set temperatureoven ˚C

    Set temperaturepump ˚C

    Set temperatureheated line ˚C

    Set temp. samplegas probe ˚C

    Max. temperaturedeviation

    Tolerance of H2pressure (mbar)

    Tolerance samplegas press. (mbar)

    Codes 1/2/3

    Number of validmeas. ranges

    Function no.

    13

    14, ident. 1

    14, ident. 2

    17, ident. 0

    17, ident. 1

    20 1 on0 off

    21 1 on0 off

    22 1 on0 off

    23 1 on0 off

    24

    30

    31

    32

    33

    34

    37

    38

    50

    51

    Date Signature

  • FIDAMAT 5E Data Sheet: Parameters and Measured Values

    Meas. range

    1

    2

    3

    4

    Function 11 Function 12 FIDAMAT 5E: ___________

    Order no.: ________________________________ _ _ _ _

    Fab. no.: _________________________________ _ _ _ _ _ _ _ _ _ _ _ ____

    SW Release no.: Master: ______ Slave: _________

    Mains voltage: V AC________________________ _ _ _ _ _ _ _ _ _ _ ______

    Designation

    Internal values in measurementmode

    Ambient temperature

    = ____________ ˚C

    Internal values in stand-bymode

    Display measured varisbles (pA)using zero gas

    Compensation of temperatureinfluence on zero

    Compensation of temperatureinfluence on span

    Suppression of noise signals

    Suppression of negative measured values

    Unit of measured value

    Display ∆ zero calibration

    Function no.

    60, ident. 1

    60, ident. 2

    60, ident. 3

    60, ident. 4

    60, ident. 5

    60, ident. 6

    60, ident. 7

    60, ident. 8

    60, ident. 9

    60, ident. 10

    60, ident. 11

    60, ident. 12

    60, ident. 13

    60, ident. 14

    60, ident. 10

    60, ident. 11

    61, ident. 1

    71, ident. 1

    71, ident. 2

    71, ident. 3

    73, ident. 1

    73, ident. 2

    73, ident. 3

    77

    78 1 on0 off

    94

    96 1 on0 off

    2, 3 values

    Parameter/measured value

    Designation

    Set time constant

    Dynamic noisesuppression

    Total calibration

    Individual calibration

    Autoranging

    Measured-valuememory

    Autocal

    Limit monitoring

    Current output(mA)

    Set temperatureoven ˚C

    Set temperaturepump ˚C

    Set temperatureheated line ˚C

    Set temp. samplegas probe ˚C

    Max. temperaturedeviation

    Tolerance of H2pressure (mbar)

    Tolerance samplegas press. (mbar)

    Codes 1/2/3

    Number of validmeas. ranges

    Function no.

    13

    14, ident. 1

    14, ident. 2

    17, ident. 0

    17, ident. 1

    20 1 on0 off

    21 1 on0 off

    22 1 on0 off

    23 1 on0 off

    24

    30

    31

    32

    33

    34

    37

    38

    50

    51

    Date Signature

  • Siemens AGAutomation DivisionProcess AnalyticsAUT V351D-76181 Karlsruhe, Germany

    Order No.: C79000-B5276-C131-03Printed in GermanyAG 0698 0.055 Sr 56 En

    Siemens Aktiengesellschaft

    Subject to technical modifications

    Copyright © Siemens AG 1994Progressin Automation.Siemens

    FIDAMAT 5E-P, -AP, -G Gas analyzersIntroductionGeneralStaff Qualifications

    ApplicationDesignMode of OperationTechnical DataInstallationMountingGas SupplyElectric Connections

    Startup, CalibrationStartupCalibrationFIDAMAT 5E-G without zero and calibration gas connections, FIDAMAT 5E-APFIDAMAT 5E-P without zero and calibration gas connections

    OperationDescription of Control PanelInput ExampleCoding and Organization of Operating Function GroupsOrganization of Data Storage

    Warnings and Error MessagesWarningsFaults

    Spare Parts and AccessoriesFIDAMAT 5E-APFIDAMAT 5E-PFIDAMAT 5E-G

    AppendixGas Flow DiagramLayout Diagrams of Important Electronic ComponentsSummary of Operating FunctionsSurvey of operating functionsSpecial Sheet for Storage of Current CodingData Sheet: Parameters and Measured Values