14
Fecha de reporte: 2019-12-22 Página: 1 de 7 Revisión: AR271-TS-48 Dirección: Km 1 Carr. los Reyes-Jacona S/N Ciudad o Localidad: Los Reyes Estado: Michoacán Código postal: 60330 ab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Ag Información del Cliente Solicitante: ROSALVA OLMOS CERVANTES Empresa: FRUITS GIDDINGS SA DE CV ab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Ag Información de Facturación Razón social: Fruits-Giddings SA de CV RFC: SBM040520QN6 Teléfono: 3545427328 Ext. 133 Correo electrónico: [email protected] Telefono: 3545420170 Ext. SD Correo electrónico: [email protected], [email protected] Domicilio Fiscal: Km. 1 Carretera los Reyes- Jacona Sn Ciudad o Localidad: Los Reyes Estado: Michoacán Código postal: 60330 Fecha de recepción: 2019-12-21 Fecha de inicio: 2019-12-21 Fecha de Término: 2019-12-22 ab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Ag Analisis Multiresidual de Pesticidas ab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Ag Información de la Muestra No. Reg. de Muestra: P-19-28976 Libro de registro: dic-19 Parte analizada: Fruto Estado de la muestra: Fresco Cantidad (peso o volumen): Menos de 1.5kg Nombre común: Zarzamora Nombre científico: Rubus Ulmifoli Variedad: Tupy Lugar de muestreo: EL CARMEN DIRECCION: ZIRACUARETIRO, MICHOACÁN Método de muestreo: Aleatorio RFC de Bodega: SD Productor: BERTA LORENA MORENO RODRIGUEZ Lugar de cosecha: ZIRACUARETIRO Registro SAGARPA: SD Fecha y hora de muestreo: 2019-12-19 Hora: 08:00 Hrs Destino Final: E.U.A, U.E,CANADA Fecha de fabricación: SD Uso comercial: Humano Destino Comercial: Mercado Extranjero Aduana: SD Nombre de quien toma la muestra: MARIA DE LA SALUD JIMENEZ MONTAÑO (Cliente) Código de muestra o No. de Lote: 3899-01 SECTOR 01 Observaciones: SD Temperatura: 20.0 ºC Presentación: BOLSA PLASTICA Fecha de caducidad: SD Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto. Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras. Documento controlado ISO/IEC 17025:2017 Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]

Fecha de reporte: 2019-12-22 Página: Revisión: AR271-TS-48 ...agrolab.fictionsecurity.com/resultados/Files/869A-33D0-2297-474C-8… · ፨ Razón social: Fruits-Giddings SA de CV

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Page 1: Fecha de reporte: 2019-12-22 Página: Revisión: AR271-TS-48 ...agrolab.fictionsecurity.com/resultados/Files/869A-33D0-2297-474C-8… · ፨ Razón social: Fruits-Giddings SA de CV

Fecha de reporte: 2019-12-22 Página: 1 de 7 Revisión: AR271-TS-48

፨ Dirección: Km 1 Carr. los Reyes-Jacona S/N ፨ Ciudad o Localidad: Los Reyes

፨ Estado: Michoacán ፨ Código postal: 60330

Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

Información del Cliente

፨ Solicitante: ROSALVA OLMOS CERVANTES ፨ Empresa: FRUITS GIDDINGS SA DE CV

Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

Información de Facturación

፨ Razón social: Fruits-Giddings SA de CV ፨ RFC: SBM040520QN6

፨ Teléfono: 3545427328 Ext. 133 ፨ Correo electrónico: [email protected]

፨ Telefono: 3545420170 Ext. SD ፨ Correo electrónico: [email protected], [email protected]

፨ Domicilio Fiscal: Km. 1 Carretera los Reyes- Jacona Sn ፨ Ciudad o Localidad: Los Reyes

፨ Estado: Michoacán ፨ Código postal: 60330

Fecha de recepción: 2019-12-21 Fecha de inicio: 2019-12-21 Fecha de Término: 2019-12-22

Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

Analisis Multiresidual de Pesticidas

Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

Información de la Muestra

No. Reg. de Muestra: P-19-28976 Libro de registro: dic-19

፨ Parte analizada: Fruto ፨ Estado de la muestra: Fresco፨ Cantidad

(peso o volumen):Menos de 1.5kg

፨ Nombre común: Zarzamora ፨ Nombre científico: Rubus Ulmifoli ፨ Variedad: Tupy

፨ Lugar de muestreo:EL CARMEN DIRECCION:

ZIRACUARETIRO, MICHOACÁN፨ Método de muestreo: Aleatorio ፨ RFC de Bodega: SD

፨ Productor:BERTA LORENA MORENO

RODRIGUEZ፨ Lugar de cosecha: ZIRACUARETIRO ፨ Registro SAGARPA: SD

፨ Fecha y hora de

muestreo:2019-12-19 Hora: 08:00 Hrs ፨ Destino Final: E.U.A, U.E,CANADA

፨ Fecha de

fabricación:SD

፨ Uso comercial: Humano ፨ Destino Comercial: Mercado Extranjero ፨ Aduana: SD

፨ Nombre de quien toma

la muestra:

MARIA DE LA SALUD JIMENEZ

MONTAÑO (Cliente)

፨ Código de muestra o No.

de Lote:3899-01 SECTOR 01

Observaciones:

SD

፨ Temperatura: 20.0 ºC ፨ Presentación: BOLSA PLASTICA፨ Fecha de

caducidad:SD

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la

representatividad del resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.

Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.

Documento controlado ISO/IEC 17025:2017

Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]

Page 2: Fecha de reporte: 2019-12-22 Página: Revisión: AR271-TS-48 ...agrolab.fictionsecurity.com/resultados/Files/869A-33D0-2297-474C-8… · ፨ Razón social: Fruits-Giddings SA de CV

B B

B B

B B

B B

B B

B B

B BB B

B B

B BB BB BB BB B

B B

B BB BB BB BB BB BB B

B B

B BB BB BB BB B

B B

B B

B B

B B

B B

B B

B B

B BB BB B

B B

B BB B

B B

B B

B B

B V

B B

B B

B BB BB BB B

B B

B B

B B

B B

B B

B B

B B

B B

B B

OXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL

METABOLITE

0.01 0.01

0.02 0.01

0.01

0.2 0.5

0.01 0.01

0.5 2

0.05 0.01

3 1

0.05 0.01

- - - -

1

- - - -

- - - -

- - - -

0.1 0.2

- - - -

0.01 1

1

0.01 0.01

0.01 0.01

0.05 0.01

0.01 0.01

- - - -

0.02 0.01

3 1

0.01 0.01

- - - -

0.01

0.01 1

0.01 0.01

0.01 0.01

0.9 0.7

0.01 0.01

0.5

0.01 0.05

0.01 1

0.1 0.01

0.01 0.01

0.01 1

0.02 0.02

0.01 0.01

- - - -

0.01

0.01 0.01

0.03 0.01

0.01 0.1

0.01 0.01

1 1

- - - -

0.01 0.02

0.01 0.01

1

0.01 0.01

0.01 0.01

0.01 0.01

- -

0.01 0.01

0.01 0.05

20 5

0.01 0.5

THIOPHANATE

 METHYL/ BENOMYL

METABOLITE

0.01

0.01

0.01

- -

0.02

0.01

0.01

7 7

0.01 0.01

1 0.3

0.01 0.01

0.01 0.01

0.01 0.01

0.01 0.01

0.05 0.01

5 3

- - - -

0.05 0.01

0.01 0.01

0.02 0.01

0.01 0.01

0.01 0.01

0.01

0.01 0.01

0.08 0.05

0.01 1

2 1

0.01 0.01

0.01 0.01

0.02 0.01

0.01 0.05

0.01

0.05 0.3

Carbetamide - - 0.01

- - < LCL

Chlordane- a GC/MSMS

- - < LCL

SD

CA EU

< LCL

- - < LCL

- - < LCL

- - < LCL

0.01

0.3 0.1 0.02 < LCL

0.1 0.1 0.02 0.1 0.02 < LCL

Chlorbromuron LC/MSMS

Fecha de reporte: 2019-12-22

Resultados de AnálisisSe han detectado residuos de pesticidas dentro de los límites permitidos

Analizado

mediante

equipo

Uso autorizado

LMR (ppm)

፨ Reg. Sagarpa:

No. Reg. Lab.:

Cantidad obtenida en mg/kg

(ppm)MX US JP CA CHN

Cantidad obtenida en mg/kg

(ppm)Analito Analito

Analizado

mediante

equipo

Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

AR271-TS-48Revisión:

፨ Cliente:

፨ Productor:

Cromatograma GC:

FRUITS GIDDINGS SA DE CV

BERTA LORENA MORENO RODRIGUEZ

P-19-28976 12-21-2019.D

P-19-28976

US JP

1-Naphthol GC/MSMSCARBARYL

METABOLITE

CARBARYL

METABOLITE

CARBARYL

METABOLITE

Uso autorizado

LMR (ppm)

MX US JP CA CHN

CARBARYL

METABOLITECARBARYL METABOLITE < LCL Carbendazim LC/MSMS

THIOPHANATE

 METHYL/

BENOMYL

METABOLITE

THIOPHANATE

 METHYL/ BENOMYL

METABOLITE

THIOPHANATE

 METHYL/

BENOMYL

METABOLITE

THIOPHANATE

 METHYL/ BENOMYL

METABOLITE

THIOPHANATE

 METHYL/

BENOMYL

METABOLITE

EU KOR EU KOR

CARBARYL

METABOLITE

CARBARYL

METABOLITE

THIOPHANATE

 METHYL/ BENOMYL

METABOLITE

2,6 Dichlorobenzonitrilo GC/MSMS - - - - - - - - - - < LCL

2,3 dihydro-2,2dimethylbenzofuran 7- GC/MSMS - - - - - -

2, 4-D Methyl ester GC/MSMS 0.2 0.2 0.1 0.1 0.1 < LCL0.1 0.01

- - - -

- - - -

Abamectin LC/MSMS 0.2 0.2 0.05 0.2 - - < LCL

3-Hydroxy carbofuran LC/MSMS - - - - - -

- - - - < LCL

3,4 Dichloroaniline GC/MSMSLINURON

METABOLITE

LINURON

METABOLITE

LINURON

METABOLITE

LINURON

METABOLITELINURON METABOLITE < LCL

2,6-Dichlorobenzamide LC/MSMS - - - - - - - - - -

LINURON

METABOLITE

Aclonifen GC/MSMS - - - - 0.01 0.1 - - < LCL

Acetochlor LC/MSMS - - - -

0.1 0.50 < LCL

Acetamiprid LC/MSMS 1.6 1.6 2 4 2 < LCL

Acephate LC/MSMS - - - - 0.01

Aldicarb LC/MSMS - - - -

- -- -LC/MSMSAldicarb-sulfoxide (Aldoxicarb)

0.01

0.1 - - < LCL

Alachlor LC/MSMS - - - - 0.01 0.1 - - < LCL

Acrinathrin GC/MSMS - - - - 0.01

0.02 0.01

0.02 0.01

0.01 0.01

Amicarbazone LC/MSMS - - - - 0.01

0.1 - - < LCL

Ametryn GC/MSMS - - - - 0.01 0.1 - - < LCL

Ametoctradin LC/MSMS - - - - 0.01 0.01

0.01 0.01

0.01 0.01

Atrazine-2-hydroxy LC/MSMS - - - - - - - - - - < LCL

Atrazine GC/MSMS - - - - 0.02

Aminocarb LC/MSMS - - - - - - - - - - < LCL- - - -

0.05 0.01

- - - -

Azoxystrobin GC/MSMS 5 5 5 5 - - < LCL

Azinphos-Methyl LC/MSMS - - - - 0.01

0.1 - - < LCL

Azinphos-ethyl LC/MSMS - - - - 0.01 0.1 - - < LCL

Azamethiphos LC/MSMS - - - - 0.01 0.01 0.01

0.02

Benfluralin GC/MSMS - - - - 0.01 0.1 - - < LCL

Bendiocarb LC/MSMS - - - - 0.01

- - - - < LCL

Benalaxyl GC/MSMS - - - - 0.05 0.1 - - < LCL

Baycarb LC/MSMS - - - - - -

Benzoximate LC/MSMS - - - - 0.01 0.1 - - < LCL

Benthiavalicarb-isopropyl LC/MSMS - - - - 0.01

0.1 - - < LCL

Bensulide LC/MSMS - - - - 0.01 0.1 - - < LCL

Bensulfuron-methyl LC/MSMS - - - - 0.01

0.01 0.1

0.01

BHC lindane gamma GC/MSMS 0.5 0.5 0.3 0.1 - - < LCL

BHC lindane delta GC/MSMS 0.5 0.5 0.3

< LCL

BHC lindane beta GC/MSMS 0.5 0.5 0.3 0.1 - - < LCL

BHC lindane alpha GC/MSMS 0.5 0.5 0.3

0.01 0.01

0.01 0.01

0.01

Bifenthrin GC/MSMS 1 1 1

Bifenox GC/MSMS - - - - 0.01 0.1 - - < LCL

Bifenazate LC/MSMS 5 5 7

Boscalid LC/MSMS 10 10 10 6 - - < LCL

Bolstar GC/MSMS - - - - - -

Bitertanol LC/MSMS - - - - 0.05 0.1 - - < LCL

- - - -

10 9

0.1 - -

0.1

Carboxin LC/MSMS - - - -

GC/MSMS - - - - 0.01

- - < LCL

0.1 - - < LCL

0.1 - - < LCL

2 1 < LCL

0.1 - - < LCL

0.1 - - < LCL

- -

LINURON METABOLITE

- - - -

0.1 - - < LCL

- - - - < LCL

1 1 < LCL

5 7 < LCL

0.1

0.1

Carbofuran GC/MSMS - - - -

0.1

- - < LCL

- - - - < LCL

Chlorpyrifos GC/MSMS - - - - 1 0.1

LC/MSMS - -

- - - - - -

0.1 - - < LCL

Chlorantraniliprole LC/MSMS 1.8 1.8 2 0.9 1 < LCL

Chinometionate GC/MSMS - - - - 0.01

- -

- - 0.01 0.1 - - < LCL

Chloroxuron LC/MSMS - - - - 0.01

0.1 - - < LCL

Chloropropylate GC/MSMS - - - - - - - - - - < LCL

Chloroneb GC/MSMS

< LCL- -0.1 0.01 0.01

0.01 0.01

0.01 0.05

Chlortal dimethyl** GC/MSMS - - - - 0.01 0.1 - - < LCL

0.1 - - < LCL

Clomazone LC/MSMS - - - - 0.02 0.1 - - < LCL

Clofentezine LC/MSMS - - - - 0.01

- - - - < LCL

Clodinafop-propargyl LC/MSMS - - - - 0.02 0.1 - - < LCL

Chlorthiophos GC/MSMS - - - - - -

0.1 0.05 < LCL

Crimidine LC/MSMS - - - - - - - - - - < LCL

Coumaphos GC/MSMS - - - - - -

0.1 - - < LCL

Clothianidin LC/MSMS - - - - 0.2 0.1 - - < LCL

Cloquintocet-mexyl LC/MSMS - - - - 0.01

0.02 - - < LCL

Cycloate LC/MSMS - - - - 0.01 0.1 - - < LCL

Cyazofamid LC/MSMS - - - - 0.01

0.1 - - < LCL

Cyantraniliprole LC/MSMS 4 4 0.01 4 - - < LCL

Cyanazine LC/MSMS - - - - 0.01

0.1 - - < LCL

Cyhalothrin (Isomero Lambda

y gamma)**GC/MSMS - - - - 0.5 0.01 0.2 < LCL

Cyfluthrin GC/MSMS - - - - 0.02

0.1 - - < LCL

Cyflumetofen LC/MSMS - - - - 0.01 0.1 - - < LCL

Cyflufenamid GC/MSMS - - - - 0.01

10 10 10 - - < LCL

Cyproconazole LC/MSMS - - - - 0.5

4 - - < LCL

Cypermethrin a (Zeta-

Cypermethrin)**GC/MSMS 0.8 0.8 0.5 0.8 - - 0.038

Cymoxanil LC/MSMS 4 4

0.1 - - < LCL

Cyprodinil

- - - - < LCLDDD-p,p GC/MSMS - - - - - -

0.1 - - < LCL

DDD-o,p GC/MSMS - - - - - - - - - - < LCL

Cyromazine LC/MSMS - - - - 0.01

- - - -

- - < LCL

Bupirimate LC/MSMS - - - - 0.01 0.1 - - < LCL DDE-o,p GC/MSMS - - - - - - - - - - < LCL

Buprofezin GC/MSMS - - - - 0.01 0.1 - - - - - -

- - - -1.5 0.01

0.01

- - < LCL

Butocarboxim* LC/MSMS - - - - 0.01 0.1 - - < LCL DDT-p,p GC/MSMS - - - - - - - - - - < LCL

Butachlor GC/MSMS - - - - 0.01 0.1 - - < LCL

- - < LCL

Buturon LC/MSMS - - - - - - - - - - < LCL Deltamethrin GC/MSMS - - - - 0.1 0.1 - - < LCL

Butocarboxim-sulfoxide LC/MSMS - - - - 0.01 0.1 - - < LCLDEET (Diethyl-m-toluamide,

N,N-)

- -

- - < LCL

Cadusafos GC/MSMS - - - - 0.01 0.1 0.02 < LCL Demeton S GC/MSMS - - - - 0.4 0.1 0.02 < LCL

Butylate GC/MSMS - - - - 0.01 0.1 - - < LCL Demeton O

0.01 0.01

Bromacil

OXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL

METABOLITE< LCL

Carbaryl GC/MSMS 12 12 10 10 - - < LCL Desmedipham LC/MSMS - - - - 0.01 0.1 - - < LCL

Captan GC/MSMS 25 25 0.01 0.1 - - < LCL Demeton-s-methyl-sulfone

Bromuconazole* LC/MSMS - - - - 0.01 0.1 - - < LCL

Bromopropylate GC/MSMS - - - - 2

Bromophos methyl GC/MSMS - - - - 0.01

0.1 - - < LCL

0.1 - - < LCL

0.1

- -0.01 0.01

OXYDEMETON

METHYL

METABOLITE

GC/MSMS - -

GC/MSMS - -

GC/MSMS - -

< LCL DDE-p,p GC/MSMS - -

GC/MSMS 10

LC/MSMS

- - - - - -

DDT-o,p

- - - - - -

- - - - - -

- - - - - -

4

0.05

0.01

< LCL0.05

< LCL- -0.1

0.1 - - < LCL

Chlorobenzilate GC/MSMS - - - - 0.01

0.01

0.01

GC/MSMSAldrin

Carfentrazone ethyl LC/MSMS 0.1 0.1 0.1

0.01

0.1 0.02 < LCL

Aldicarb sulfone LC/MSMS - - - - 0.01 0.1 Chlormequat LC/MSMS - - - - 0.01

Chlorimuron-ethyl LC/MSMS - - - - 0.01

Chloridazon (Pyrazon) LC/MSMS - - - - 0.01

< LCL

0.050.05

0.1 - - < LCL

0.1 - - < LCL

0.1 - - < LCL

0.1 - - < LCL

Chlorfluazuron LC/MSMS - - - - 0.01 0.1 - - < LCL

Chlorfenvinphos LC/MSMS - - - - 0.05

0.02 < LCL

- -0.1

GC/MSMS - -

Página:

፨ Muestra:

፨ Huerto:

Cromatograma LC:

2 de 7

Zarzamora

ZIRACUARETIRO

P-19-28976 12-21-2019.d

10- -- -GC/MSMSChlorothalonil

0.1 0.01 < LCL

Chlorfenapyr GC/MSMS - - - - 0.01 0.1 - - < LCL

Chlordimeform GC/MSMS - - - - 0.01

KOR CHN

Chlorpyrifos methyl GC/MSMS - - - - 0.05 0.1 - - < LCL

Chlorsulfuron LC/MSMS - - - - 0.01 0.1 - - < LCL

MX

0.01- -- -LC/MSMSChlorotoluron

- -0.1

- - < LCL

0.1 - - < LCL

Chlorpropham

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del resultado para el total del producto.

Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto. Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.

Documento controlado ISO/IEC 17025:2017

Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]

*Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado. Las bandas de colores son de apoyo visual basadas en los LMRs de México y no representan un resultado. 1Límite Máximo de Residuos (LMR) expresados en ppm para cada país indicado en código ISO 3166-1 alfa-3. LCL = Lowest Calibration Level (Nivel Mínimo de Calibración) ppm = Partes por millón = mg/kg GC/MSMS =Cromatografía de Gases/Masas/Masas LC/MSMS = Cromatografía de Líquidos/MasasMasas

Autoriza

Lic. Carlos Sepulveda Ibarra IBT. Cesar Arturo Sanchez Espindola Director General Analista de Cromatografia

Page 3: Fecha de reporte: 2019-12-22 Página: Revisión: AR271-TS-48 ...agrolab.fictionsecurity.com/resultados/Files/869A-33D0-2297-474C-8… · ፨ Razón social: Fruits-Giddings SA de CV

B BB BB BB BB BB BB BB BB BB BB BB BB BB B

B B

B BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB B

B B

B B

B B

B B

B B

B BB B

B B

B BB B

B B

B B

B B

B B

B B

B BB B

0.3

0.01

5 6

0.01 0.01

0.01 0.01

1.5 1.5

0.01

0.01 0.01

- -

0.01 0.5

0.01 0.01

0.01

0.01 0.5

0.01

0.01Imazapyr

Imazalil

GC/MSMS 0.05 0.05 0.01 0.1

0.01

- - - -

0.01 0.01

0.03

0.01

5 5

0.01

0.05

0.01 0.01

0.01 0.01

0.01 0.02

0.01 0.01

0.01 0.01

- - - -

0.01 0.01

0.01 0.01

0.03 3

0.01 0.01

- -

0.01

0.01 0.01

0.01 0.01

0.7 0.7

- - - -

0.01 0.01

0.01 0.01

- - - -

0.005 0.01

0.05

0.01

0.05

0.01 5

0.01 5

0.01

0.01

0.01

0.01

0.01

0.05 0.3

0.01 0.01

0.01 0.01

3 0.01

- -

0.01 0.01

0.05 0.01

0.01 0.01

- - - -

- - - -

0.01

0.01 0.01

15

0.01

0.010.05

0.01

0.01

0.05

0.01

0.02

0.01

0.01

0.01

0.5

- -

0.01

0.01 0.01

2

0.01 0.01

0.1 0.01

0.02 0.01

- - - -

0.01 0.01

0.01

0.01 0.03

0.05 0.05

0.05 0.05

0.05 0.05

0.01 0.01

0.05 0.01

0.01 0.01

0.02 0.01

- - - -

0.01

0.01 0.01

1.5 0.5

- - - -

0.01 0.01

0.01 0.01

- - - -

0.01 0.01

0.01 0.01

- - - -

0.01 0.01

0.01 0.01

0.01 0.01

0.05 1

- - - -

0.01 0.01

0.01

EU KOR

0.01 0.01

- - - -

0.01 0.01

0.01 15

0.01 0.01

0.01 0.01- - - -

2

0.01

- -

15

0.3

0.010.01

CHN MX US JP CA

0.01

0.01

- -

Revisión: AR271-TS-48

Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

Resultados de AnálisisSe han detectado residuos de pesticidas dentro de los límites permitidos

Analito

Analizado

mediante

equipo

Uso autorizado

LMR (ppm) Cantidad obtenida en

mg/kg (ppm)Analito

Analizado

mediante

equipo

Uso autorizado

LMR (ppm)

፨ Reg. Sagarpa: SD

No. Reg. Lab.:

CHN

Fecha de reporte:

Cantidad obtenida en

mg/kg (ppm)MX US JP CA

፨ Cliente: P-19-28976

፨ Productor:

Cromatograma GC:

FRUITS GIDDINGS SA DE CV

BERTA LORENA MORENO

RODRIGUEZ

EU

< LCL

Dialifos LC/MSMS - - - - - - - - - - < LCL Fenchlorphos

LC/MSMS - - - - 1 0.1 - -Desmetryn GC/MSMS - - - - 0.01 0.1 - - < LCL Fenbutatin oxide*

< LCL

Dichlofluanid GC/MSMS - - - - 10 0.1 - - < LCL Fenhexamid

LC/MSMS - - - - - - - - - -

< LCL

Diazinon GC/MSMS 0.75 0.75 0.1 0.1 0.1 < LCL Fenfuram

GC/MSMS - - - - 0.01 0.1 - -

< LCL

Dichlorvos GC/MSMS - - - - 0.1 0.1 0.2 < LCL Fenoxaprop-ethyl

GC/MSMS - - - - 0.8 0.1 0.5

< LCL

Dichloran GC/MSMS - - - - 10 10 - - < LCL Fenitrothion

LC/MSMS 20 20 15 20 15

< LCL

Diclofop methyl GC/MSMS - - - - 0.01 0.1 - - < LCL Fenpropathrin

LC/MSMS - - - - 0.05 0.1 - -< LCL

Diclobutrazol* LC/MSMS - - - - - - - - - - < LCL Fenoxycarb

LC/MSMS - - - - 0.1 0.1 - -

< LCL

Dieldrin GC/MSMS 0.05 0.05 0.05 0.1 0.02 < LCL Fenpropimorph

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Dicrotophos LC/MSMS - - - - 0.01 0.1 - - < LCL Fenpropidin

GC/MSMS 12 12 5 12 5

< LCL

Difenoconazole LC/MSMS - - - - 0.01 0.1 - - < LCL Fenson

LC/MSMS - - 3 0.01 0.1 - -

< LCL

Diethofencarb LC/MSMS - - - - 0.01 0.1 - - < LCL Fenpyroximate

LC/MSMS - - - - 0.05 0.1 - -

< LCL

Diflubenzuron* LC/MSMS - - - - 0.01 0.1 - - < LCL Fenthion

GC/MSMS - - - - 0.01 0.1 - -

< LCL

Difenoxuron LC/MSMS - - - - - - - - - - < LCL Fensulfothion

GC/MSMS - - - - - - - - - -

< LCL

Dimefuron LC/MSMS - - - - - - - - - - < LCL Fipronil

LC/MSMS - - - - - - - - - -

< LCL

Diflufenican LC/MSMS - - - - 0.01 0.1 - - < LCL Fenuron

GC/MSMS - - - - 0.01 0.1 0.05

< LCL

Dimethachlor LC/MSMS - - - - 0.01 0.1 - - < LCL Flamprop-isopropyl

LC/MSMS - - - - 0.01 0.1 - -

< LCLGC/MSMS - - - - 0.01 0.1 0.02

Flamprop methyl< LCL- -- -- -- -- -GC/MSMSDimepax

< LCL

Dimethoate GC/MSMS - - - - 1 0.1 - - < LCL Flonicamid

LC/MSMS - - - - 0.1 0.1 - -

< LCL

Dimethenamid LC/MSMS - - - - 0.01 0.1 - - < LCL Flazasulfuron

LC/MSMS - - - - - - - - - -

< LCL

Dimethomorph LC/MSMS - - - - 0.01 0.1 - - < LCL Fluazifop-butyl

LC/MSMS - - - - 0.01 0.1 - -

- -0.080.01- -- -LC/MSMS < LCL

0.7

0.01

< LCL

Diniconazole LC/MSMS - - - - 0.01 0.1 - - < LCL Fluchloralin

LC/MSMS - - - - 0.01 0.1 - -< LCL Flubendiamide 0.01

0.01

Dimethylphenol, 2,4- (2,4-xylenol) - - - - - - - -

< LCL

Dioxathion GC/MSMS - - - - 0.01 0.1 - - < LCL Fludioxonil

GC/MSMS - - - - 0.05 0.1 - -

< LCL

Dinotefuran LC/MSMS - - - - 0.01 0.1 - - < LCL Flucythrinate

GC/MSMS - - - - 0.01 0.1 - -

< LCL

Diphenylamine GC/MSMS - - - - 0.05 0.1 - - < LCL Flufenoxuron

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Diphenamid LC/MSMS - - - - 0.01 0.1 - - < LCL Flufenacet

GC/MSMS 5 5 5 7 - -

< LCL

Disulfoton sulfone GC/MSMS - - - - - - - - - - < LCL Fluometuron

GC/MSMS - - - - 0.01 0.1 - -

< LCL

Disulfoton GC/MSMS - - - - 0.05 0.1 - - < LCL Flumiclorac-pentyl

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Diuron (Karmex) LC/MSMS 0.1 0.1 0.05 0.1 - - < LCL Fluopyram

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Disulfoton sulfoxide GC/MSMS - - - - - - - - - - < LCL Fluopicolide

LC/MSMS - - - - 0.02 0.1 - -

< LCL

Dyfonate GC/MSMS - - - - 0.01 0.1 0.01 < LCL Fluoxastrobin

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Dodemorph LC/MSMS - - - - 0.01 0.1 - - < LCL Fluoroglycofen-ethyl

GC/MSMS 5 5 5 5 - -

< LCL

Emamectin Benzoate LC/MSMS - - - - 0.1 0.1 - - < LCL Fluridone

LC/MSMS 5 5 0.01 5 - -

< LCL

Edifenphos LC/MSMS - - - - 0.01 0.1 - - < LCL Flupyradifurone*

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Endosulfan II (beta isomer) GC/MSMS - - - - 0.5 0.1 - - < LCL Flusilazole

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Endosulfan I (alpha isomer) GC/MSMS - - - - 0.5 0.1 - - < LCL Flurtamone

GC/MSMS - - - - 0.01 0.1 - -

< LCL

Endrin GC/MSMS - - - - 0.01 0.1 0.05 < LCL Flutriafol

GC/MSMS - - - - 0.01 0.1 - -

< LCL

Endosulfan sulfato GC/MSMS - - - - 0.5 0.1 - - < LCL Flutolanil

LC/MSMS - - - - 0.01 0.1 - -

< LCL

EPTC GC/MSMS - - - - 0.1 0.1 - - < LCL Fluxapyroxad

GC/MSMS - - - - - - - - - -

< LCL

Epoxiconazole LC/MSMS - - - - 0.01 0.1 - - < LCL Fluvalinate

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Etaconazole (Etaconazole I y II) LC/MSMS - - - - - - - - - - < LCL Forchlorfenuron

GC/MSMS - - - - 0.01 25 - -

< LCL

Esfenvalerate + Fenvalerate (**) GC/MSMS 1 1 1 0.1 0.2 < LCL Folpet

LC/MSMS 5 5 7 5 - -

< LCL

Ethiofencarb LC/MSMS - - - - 0.01 0.1 - - < LCL Fosthiazate

LC/MSMS - - - - - - - - - -

< LCL

Ethalfluralin GC/MSMS - - - - 0.01 0.1 - - < LCL Formetanate

LC/MSMS - - - - 0.1 0.1 - -

< LCL

Ethirimol LC/MSMS - - - - 0.01 0.1 - - < LCL Furathiocarb

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Ethiofencarb-sulfone LC/MSMS - - - - 0.01 0.1 - - < LCL Fuberidazole

LC/MSMS - - - - 0.05 0.1 - -

< LCL

Ethylan GC/MSMS - - - - - - - - - - < LCL Haloxyfop-methyl

GC/MSMS 0.1 0.1 0.02 0.1 0.02

< LCL

Ethoprop GC/MSMS - - - - 0.01 0.1 0.02 < LCL g Chlordan

LC/MSMS - - - - 0.01 0.1 - -

0.01

< LCL

Etion GC/MSMS - - - - 0.3 0.1 - - < LCL Heptachlor

LC/MSMS - - - - 0.05 0.1 - -

Etoxazole LC/MSMS 1.5 1.5 0.01 1.5 - - < LCL Heptenophos

Etofenprox GC/MSMS 5 5 0.01 0.1 - - < LCLHeptachlor exo-epoxide (isomer

B)1

0.01 0.3

1 0.01 1.5LC/MSMS

Famoxadone LC/MSMS 10 10 10 10 - - < LCL Hexachlorobenzene 0.05 0.01 0.10.01 0.01

0.1 0.02 < LCL Hexaflumuron

LC/MSMS - - - - 0.1 - -

Fenazaquin LC/MSMS 0.7

Fenamiphos Sulfone

Fenarimol LC/MSMS - - - - 1 0.1 - - < LCL

1

0.02 0.01

- - - -

- - - -

0.01 0.1 - -

< LCL

0.01

- - 0.01 0.1

0.02 0.01

< LCL Hexythiazox

LC/MSMS - - - - 0.05 0.1 - -

< LCL

Fenbuconazol LC/MSMS - - - - 0.01 0.1 - - < LCL Imazaquin

LC/MSMS - - - - 0.01 0.1 - -0.01 0.5

0.05 0.01 < LCL

0.7 0.01 0.1 - -

P-19-28976 12-21-2019.D

Página:

፨ Muestra:

፨ Huerto:

Cromatograma LC:

3 de 7

Zarzamora

ZIRACUARETIRO

P-19-28976 12-21-2019.d

GC/MSMS - -LC/MSMS - - - - - - - - - - < LCL Hexazinone

LC/MSMS - -

2019-12-22

GC/MSMS 0.05

GC/MSMS - -

KOR

0.05 0.01

0.01 0.01

0.01

CHNKOR

< LCLLC/MSMS - - - - 0.02 0.1 - -

< LCL

- - 0.01 0.1 - -0.01

0.01

- -

US JP CA EUMX

< LCL

LC/MSMS - - - - 0.01 0.1 - -

< LCL- -

< LCL

< LCL

< LCLGC/MSMS - - - - - - - - - -

< LCL

< LCL

Fenamiphos Sulfoxide LC/MSMS - - - - - - - - - - - -

- - < LCL HexaconazoleFenamidone GC/MSMS - - 0.01 0.01

Fenamiphos LC/MSMS - - - - 0.02

0.01

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El re sultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del

resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.

Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tacha duras o enmendaduras.

Documento controlado ISO/IEC 17025:2017

Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]

*Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado. Las bandas de colores son de apoyo visual basadas en los LMRs de México y no representan un resultado. 1Límite Máximo de Residuos (LMR) expresados en ppm para cada país indicado en código ISO 3166 -1 alfa-3. LCL = Lowest Calibration Level (Nivel Mínimo de Calibración) ppm = Partes por millón = mg/kg GC/MSMS =Cromatografía de Gases/Masas/Masas LC/MSMS = Cromatografía de Líquidos/MasasMasas Trazas/Traces = < 0.010 ppm.

Autoriza

Lic. Carlos Sepulveda Ibarra IBT. Cesar Arturo Sanchez Espindola Director General Analista de Cromatografia

Page 4: Fecha de reporte: 2019-12-22 Página: Revisión: AR271-TS-48 ...agrolab.fictionsecurity.com/resultados/Files/869A-33D0-2297-474C-8… · ፨ Razón social: Fruits-Giddings SA de CV

B BB BB BB BB BB BB BB BB B

B B

B B

B B

B BB BB BB B

B B

B B

B B

B B

B B

B B

B B

B B

B B

B B

B B

B B

B B

B B

B B

B B

B B

B BB BB BB BB BB BB BB BB B

B B

B B

B B

B B

B B

B B

B BB BB BB BB BB BB BB BB BB B

B B

B B

- - - -

0.01 0.01

0.01 0.01

- - - -

0.01 0.01

4 1

0.01 0.01

0.01 0.01

0.01 0.01

0.05 3

0.01 2

0.01 2

- - - -

- - - -

0.01 0.05

0.01 0.05

0.01 0.05

0.01 0.01

0.01 0.01

0.01 0.01

0.01 0.01

0.01 0.01

- -

0.05 0.01

0.01 0.01

0.1 0.2

0.05 0.01

0.05 0.01

QUINTOCENE

(PENTACHLOR

ONITROBENZE

NE)METABOLIT

E

QUINTOCENE

(PENTACHLOR

ONITROBENZE

NE)METABOLIT

E

- - - -

0.02 0.01

0.01 0.01

1 0.01

- - - -

0.1 0.01

- - - -

0.01 0.01

0.01 0.01

0.01 0.01

0.01 0.01

- - - -

0.01 2

0.01 0.01

- - - -

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

0.02 0.01

- - - -

0.1 0.01

0.01 0.01

0.01 0.01

- - - -

- - - -

0.01 0.01

0.01 0.01

0.01 0.01

0.01 0.01

0.01

0.01 1

- - - -

0.01 0.01

0.05 0.01

0.01 0.01

0.01 0.01

- - - -

0.01 5

0.01 30

0.01 0.01

- - - -

0.01 0.01

0.01 0.01

0.01 0.01

0.01 0.01

0.01 0.01

0.01 0.01

< LCL

Metosulam LC/MSMS - - - - 0.01 0.1 - - < LCL

Metobromuron LC/MSMS - - - - 0.01 0.1 - - < LCL

< LCL

Metolachlor

Piperalin LC/MSMS - - - - - - - - - - < LCL

Piperonyl Butoxide LC/MSMS 8 8 8

- - - - 0.01 0.1 0.05 < LCL

Phosalone LC/MSMS - - - - 0.01 0.1 - - < LCL

LC/MSMS

LC/MSMS - - - - 0.01 0.1 - -

Phoxim

LC/MSMS

< LCL

Phosphamidon

Picolinafen LC/MSMS

- - - - 0.02 0.1 0.05

Phorate-sulfoxide LC/MSMS - - - - 0.05 0.024 0.01 < LCL

Ofurace LC/MSMS - - - - - - - - - - < LCL

Omethoate LC/MSMSDIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE< LCL

op Dicofol*** GC/MSMS - - - - 3 0.1

Ovex GC/MSMS

Fecha de reporte: 2019-12-22 Revisión: AR271-TS-48

Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

፨ Reg. Sagarpa: SD

No. Reg. Lab.:፨ Cliente:

፨ Productor:

Cromatograma GC:

FRUITS GIDDINGS SA DE CV

BERTA LORENA MORENO

RODRIGUEZ

P-19-28976 12-21-2019.D

Página:

፨ Muestra:

፨ Huerto:

Cromatograma LC:

4 de 7

Zarzamora

ZIRACUARETIRO

P-19-28976 12-21-2019.d

P-19-28976

US JP CA EUMX CHN

Se han detectado residuos de pesticidas dentro de los límites permitidos

Analito

Analizado

mediante

equipo

Uso autorizado

LMR (ppm) Cantidad obtenida en

mg/kg (ppm)Analito

Analizado

mediante

equipo

Uso autorizado

LMR (ppm)

CHN

Cantidad obtenida

en mg/kg (ppm)MX US JP CA CHN MX US JP CAEU KOR EU KOR

Imidacloprid LC/MSMS 2.5 2.5 4 2.5 - - < LCL N-2,4-Dimethylphenyl

Imiprothrin GC/MSMS - - - - - - - - - - < LCL Neburon

Imidan GC/MSMS - - - -

5 1.5

0.05 0.01

- - - -

< LCL

- -

LC/MSMS 0.1 0.1 0.1 0.10.1 0.1 - - < LCL Napropamide

LC/MSMS - - - - - -

- - - -LC/MSMS - - - -

0.5 0.5

- -

LC/MSMS - - - - 0.01 0.1

GC/MSMS - - - - 0.01 0.1

GC/MSMS

LC/MSMS 0.1 0.1

Iprovalicarb LC/MSMS - - - - 0.01 0.1 - - < LCL

Isazophos LC/MSMS

< LCL

Nitrothal-isopropyl

Norflurazon-Desmethyl

Nicosulfuron

Iprodione GC/MSMS

- -

25 25 12 25 - - < LCL Nitrapyrin

Indoxacarb GC/MSMS - - - - 0.01 0.1

< LCLNorflurazon

- - - - - - - -

Irgarol LC/MSMS - - - - - - - - - -

- - - - 0.01 0.1 0.01

GC/MSMS

Isofenphos LC/MSMS - - - - 0.01 0.1 0.01 < LCL

< LCL< LCL

Isocarbophos GC/MSMS - - - - 0.01 0.1 0.05 < LCL Novaluron* LC/MSMS - - - - 0.01 0.1 - - < LCL

O Phenylphenol GC/MSMS - - - - 0.01 0.1

Isoproturon LC/MSMS - - - - 0.01 0.1 - - < LCL

Isoprothiolane GC/MSMS - - - - 0.01 0.1 - - < LCL

Isoprocarb LC/MSMS - - - - 0.01 0.1 - - < LCL

Kresoxim-methyl LC/MSMS - - - - 0.01 0.1 - - < LCL

Kelthane*** GC/MSMS - - - - 3 0.1 - - < LCL

Isoxaflutole LC/MSMS - - - - 0.01 0.1 - - < LCL0.02 0.01

0.02 0.01

0.01 2

Linuron LC/MSMS - - - - 0.2 0.1 - - < LCL

Leptophos GC/MSMS - - - - - - - - - - < LCL

Lenacil LC/MSMS - - - - 0.3 0.1 - - < LCL0.1 0.01

- - - -

0.01 0.01

Malathion GC/MSMS 8 8 8 8 - - < LCL

Malaoxon LC/MSMSMALATHION

METABOLITE

MALATHION

METABOLITE

MALATHION

METABOLITE

MALATHION

METABOLITE

MALATHION

METABOLITE< LCL

Lufenuron LC/MSMS - - - - 0.01 0.1 - - < LCL0.01 0.3

MALATHION

METABOLITE

MALATHION

METABOLITE

0.02 0.5

Mebendazole LC/MSMS - - - - - - - - - - < LCL

Mandipropamid LC/MSMS - - - - 0.01 0.1 - - < LCL

Mancozeb LC/MSMS - - - - 5 0.1 5 < LCL0.05 7

0.01 0.01

- - - -

Metalaxyl-M (Mefenoxam, R-

enantiomero de metalaxyl)GC/MSMS 0.7 0.7 0.7 0.1 - - < LCL

Mepanipyrim LC/MSMS - - - - 0.01 0.1 - - < LCL

Mecarbam LC/MSMS - - - - 0.01 0.1 - - < LCL0.01 0.01

4 0.01

0.02 0.01

Metconazole LC/MSMS - - - - 0.01 0.1 - - < LCL

Metazachlor LC/MSMS - - - - 0.01 0.1 - - < LCL

Metamitron LC/MSMS - - - - 0.01 0.1 - - < LCL0.1 0.01

0.02 0.01

0.02 0.01

Methidathion LC/MSMS - - - - 0.2 0.1 0.05 < LCL

Methamidophos LC/MSMS - - - - 0.01 0.1 0.05 < LCL

Methabenzthiazuron LC/MSMS - - - - 0.01 0.1 - - < LCL0.01 0.01

0.01 0.1

0.02 0.01

Methiocarb sulfoxide GC/MSMS - - - - 0.05 0.1 - - < LCL

Methiocarb sulfone GC/MSMS - - - - 0.05 0.1 - - < LCL

Methiocarb GC/MSMS - - - - 0.05 0.1 - - < LCL0.2 0.01

0.2 0.01

0.2 0.01

Methoprotryne LC/MSMS - - - - - - - - - - < LCL

Methoprene GC/MSMS - - - - 0.01 0.1 - - < LCL

Methomyl LC/MSMS - - - - 1 0.01 0.2 < LCL0.01 0.01

0.02 0.01

- - - -

LC/MSMS - - - - - - - - - - < LCL

Methoxychlor GC/MSMS - - - - 7 0.1 - - < LCL

Methylpentachlophenyl Sulfide GC/MSMS - - - - - - - - - - < LCL

Methoxyfenozide LC/MSMS 6 6 0.01 6 - - < LCL

0.01

< LCL

Metribuzin GC/MSMS - - - - 0.01 0.1 - - < LCL

Metolcarb LC/MSMS - - - - 0.01 0.1 - -

Metsulfuron-methyl LC/MSMS - - - - 0.01 0.1 - -

Metrafenone LC/MSMS - - - - 0.01 0.1 - - < LCL

Metoxuron

MGK-264 GC/MSMS - - - - - - - - - - < LCL

Mexacarbate LC/MSMS - - - - - - - - - - < LCL

Mevinphos GC/MSMS - - - - 0.01 0.1 - - < LCL

- - - - 0.01 0.1 0.03 < LCL

Molinate LC/MSMS - - - - 0.01 0.1 - - < LCL

Mirex GC/MSMS - - - - 0.01 0.1 0.01 < LCL

Myclobutanil GC/MSMS 2 2 1 2 - - < LCL Pronamide LC/MSMS - - - - - - - - - - < LCL

- - - - - - - - - - < LCL

Monuron LC/MSMS - - - - 0.01 0.1 - - < LCL

Monolinuron LC/MSMS - - - - 0.01 0.1 - - < LCL

Oxamyl LC/MSMS - - - - 0.01 0.1

Monocrotophos LC/MSMS

Oxamyl Oxime LC/MSMS OXAMYL METABOLITEOXAMYL METABOLITEOXAMYL METABOLITEOXAMYL METABOLITE OXAMYL METABOLITE < LCL

Oxadiazon GC/MSMS - - - - 0.01 0.1 - - < LCL

Oxadixyl LC/MSMS - - - - 1 0.1 - - < LCL

0.05 0.01

0.01 0.01

0.01 0.5

OXAMYL METABOLITEOXAMYL METABOLITE

- -

< LCL

- -

- -

- -

< LCL

< LCL

Paraoxon LC/MSMS - - - - - - - - - - < LCL

Oxydemeton-methyl LC/MSMS - - - - 0.02 0.1 - - < LCL

Oxyfluorfen GC/MSMS 0.05 0.05 0.01 0.1 - - < LCL

- -

0.2 0.1 0.02 < LCL

0.01 < LCL

0.1 0.1 - -

- - 0.01 0.1

< LCL

< LCL

- -

- -

< LCL- -

< LCL

- - < LCL

- - < LCL

0.01 0.01

0.05 0.01

0.01 0.01

- - - -

- -

- - - - - -

- -

Resultados de análisis

Paclobutrazol (Bonzi) LC/MSMS - - - - 0.01 0.1 - - < LCL

< LCL

Paraoxon-methyl LC/MSMS - - - - - - - - - - < LCL

Parathion GC/MSMS - - - - 0.5 0.1

Parathion methyl GC/MSMS - - - -

- - 0.05 0.024 0.01

Pentachlorophenol

Penthiopyrad

Permethrin

Phenmedipham

Penconazol LC/MSMS - - - - 0.2 0.1 - -

- - - - 0.01 0.1 - -

0.1 0.1 0.05 0.1 - -

QUINTOCENE

(PENTACHLOR

ONITROBENZE

NE)METABOLIT

E

QUINTOCENE

(PENTACHLOR

ONITROBENZE

NE)METABOLIT

E

QUINTOCENE

(PENTACHLOR

ONITROBENZE

NE)METABOLIT

E

QUINTOCENE

(PENTACHLOR

ONITROBENZE

NE)METABOLIT

E

QUINTOCENE

(PENTACHLOR

ONITROBENZE

NE)METABOLIT

E

- - - -

Phenthoate

Phenyl valerate

Phorate

Phorate-sulfone

LC/MSMS

LC/MSMS

GC/MSMS

GC/MSMS

GC/MSMS

GC/MSMS

GC/MSMS

GC/MSMS

LC/MSMS

LC/MSMS

GC/MSMS

GC/MSMS

LC/MSMS

Pencycuron

Pendimethalin

Pentachloroaniline

Pentachloroanisol

Pentachloronitrobenzene

- - - - 0.01 0.1 - -

- - - - 0.01 0.1 - -

- - 10 0.01 10 - -

- - 0.02 0.1 - -

0.1 1

0.01 0.01

0.01 0.5

0.05 5

0.01 0.5

- - - - 0.05 0.024 0.01

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

- - - - - - - - - -

- -

- - - - 1

- - - - 0.01 0.1 - -

- - - - 0.01 0.1 - - < LCL

Picoxystrobin LC/MSMS - - - - 0.01 0.1 - - < LCL

- - - -

- - 0.01

Piperophos LC/MSMS - - - - 0.01 0.1 - - < LCL

Pirimicarb LC/MSMS - - - - 0.5 0.1 1 < LCL

8 - - < LCL

Primisulfuron-methyl LC/MSMS - - - - 0.01 0.1 - - < LCL

Prochloraz LC/MSMS - - - - 0.05 0.1 - - < LCL

Pirimiphos-ethyl LC/MSMS - - - - 0.01 0.1 - - < LCL

Pirimiphos-methyl LC/MSMS - - - - 0.1 0.1 - - < LCL

< LCL

Procymidone GC/MSMS - - - - 0.01 0.1 - - < LCL

Profenofos GC/MSMS - - - - 0.01 0.1 - - < LCL

- - - -

KOR

Prometon GC/MSMS - - - - - - - - - - < LCL

Prometryn GC/MSMS - - - - 0.01 0.1 - - < LCL

Profluoralin GC/MSMS - - - - - - - - - - < LCL

Promecarb GC/MSMS - - - - - - - - - -

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del

resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.

Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.

Documento controlado ISO/IEC 17025:2017

Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]

*Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado. Las bandas de colores son de apoyo visual basadas en los LMRs de México y no representan un resultado. 1Límite Máximo de Residuos (LMR) expresados en ppm para cada país indicado en código ISO 3166-1 alfa-3. LCL = Lowest Calibration Level (Nivel Mínimo de Calibración) ppm = Partes por millón = mg/kg GC/MSMS =Cromatografía de Gases/Masas/Masas LC/MSMS = Cromatografía de Líquidos/MasasMasas Trazas/Traces = < 0.010 ppm.

Autoriza

Lic. Carlos Sepulveda Ibarra IBT. Cesar Arturo Sanchez Espindola Director General Analista de Cromatografia

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B BB BB BB BB BB BB BB BB BB BB B

B B

B BB BB BB B

B B

B BB BB B

B B

B B

B B

B B

B BB B

B B

B B

B B

B B

B B

B B

B B

B VB VB VB VB VB VB VB VB V

B V

B

BB

B

B

BBB

B

B

B

B

B

BBBB0.01 1 - - < LCLThiamethoxam LC/MSMS 0.35 0.35 0.5 0.5

1 < LCLThiacloprid LC/MSMS - - - - 5 0.1 1 0.7

0.01 0.01 - - < LCLThiabendazole LC/MSMS - - - - 3 0.1

- - < LCLTetramethrin LC/MSMS - - - - 0.01 0.1 0.01 0.01

CAPTAN

METABOLITE

CAPTAN

METABOLITE

CAPTAN

METABOLITE < LCLTetrahydrophthalimide, cis-1,2,3,6-

(THPI)GC/MSMS

CAPTAN

METABOLITE

CAPTAN

METABOLITE

CAPTAN

METABOLITE

CAPTAN

METABOLITE

- - < LCLTetradifon GC/MSMS - - - - 1 0.1 0.01 0.01

0.01 0.01 - - < LCLTetrachlorvinphos, E-isomer GC/MSMS - - - - 0.01 0.1

- - < LCLTerrazole GC/MSMS - - - - - - - - - - - -

0.01 0.01 - - < LCLTerbutryn GC/MSMS - - - - 0.01 0.1

- - < LCLTerbuthylazine-desethyl LC/MSMS - - - - - - - - - - - -

0.05 0.01 - - < LCLTerbuthylazine GC/MSMS - - - - 0.01 0.1

- - < LCLTerbumeton LC/MSMS - - - - - - - - - - - -

0.01 0.01 - - < LCLTerbacil GC/MSMS 0.2 0.2 0.1 0.1

- - < LCLTeflubenzuron LC/MSMS - - - - 0.01 0.1 0.01 2

0.01 0.01 - - < LCLTecnazene GC/MSMS - - - - 0.05 0.1

- - < LCLTebuthiuron LC/MSMS - - - - 0.01 0.1 0.01 0.01

0.01 0.01 - - < LCLTebutam LC/MSMS - - - - 0.01 0.1

- - < LCLTebufenpyrad GC/MSMS - - - - 0.01 0.1 0.05 0.5

0.05 2 - - < LCLTebufenozide LC/MSMS 3 3 3 0.1

- - < LCLTebuconazole GC/MSMS - - - - 0.01 0.1 0.5 0.5

0.02 0.01 - - < LCLSumithrin GC/MSMS - - - - 0.01 0.1

- - < LCLSulfoxaflor LC/MSMS - - 1.5 0.01 0.1 0.01 0.5

0.01 0.01 0.01 < LCLSulfotep LC/MSMS - - - - 0.01 0.1

- - < LCLSulfosulfuron LC/MSMS - - - - 0.01 0.1 0.01 0.01

0.01 0.01 - - < LCLSulfentrazone LC/MSMS 0.15 0.15 0.05 0.15

- - < LCLSpiroxamine LC/MSMS - - - - 0.01 0.1 0.01 0.01

0.1 3 - - < LCLSpirotetramat LC/MSMS - - - - 0.01 2

5 0.1 0.01 0.01 - - < LCL- - < LCL Vinclozolin GC/MSMS - - - -

- - < LCL

Spiromesifen LC/MSMS - - - - 0.01 5 0.02 2

- - - - 0.01 0.1 0.01 0.010.02 1 - - < LCL Vamidothion LC/MSMSSpirodiclofen LC/MSMS - - - - 0.01 0.1

0.01 0.1 0.01 0.01 - - < LCL1 < LCL Uniconazole GC/MSMS - - - -

- - < LCL

Spinosad A LC/MSMS 1 1 1 0.5 1.5 0.5

- - - - - - - - - - - -1 0.7 - - < LCL Trimidal LC/MSMSSpinetoram J LC/MSMS 0.8 0.8 0.7 0.5

0.01 0.1 0.01 0.5 - - < LCL- - < LCL Triforine LC/MSMS - - - -

- - < LCL

S-Metolachlor LC/MSMS 0.1 0.1 0.01 0.1 0.05 0.01

- - - - 0.01 0.1 0.01 0.010.01 0.01 - - < LCL Triflusulfuron-methyl LC/MSMSSimetryn LC/MSMS - - - - 0.01 0.1

0.05 0.1 0.01 0.01 - - < LCL- - < LCL Trifluralin GC/MSMS - - - -

- - < LCL

Simazine GC/MSMS 0.2 0.2 0.2 0.1 0.01 0.01

- - - - 0.02 0.1 0.01 0.010.1 1 - - < LCL Triflumuron LC/MSMSSethoxydim* LC/MSMS 5 5 1 5

0.01 0.1 0.02 2 - - < LCL- - < LCL Triflumizole LC/MSMS - - - -

- - < LCL

Sebuthylazine GC/MSMS - - - - - - - - - - - -

- - - - 0.01 0.1 3 10.01 0.01 - - < LCL Trifloxystrobin LC/MSMSRotenone LC/MSMS - - - - 0.01 0.1

- - - - - - - - - - < LCL- - < LCL Trietazine LC/MSMS - - - -

- - < LCL

Rimsulfuron LC/MSMS 0.01 0.01 0.01 0.01 0.01 0.01

- - - - 0.01 0.1 0.01 0.010.05 0.01 - - < LCL Tricyclazole GC/MSMSQuizalofop-ethyl LC/MSMS - - - - 0.05 0.1

- - - - - - - - - - < LCL- - < LCL Triclocarban LC/MSMS - - - -

- - < LCL

Quinoxyfen LC/MSMS - - - - 0.01 0.1 0.02 0.01

- - - - - - - - - - - -0.01 0.01 - - < LCL Trichloronate GC/MSMSQuinalphos LC/MSMS - - - - 0.02 0.1

0.5 0.1 0.01 0.01 0.2 < LCL- - < LCL Trichlorfon LC/MSMS - - - -

- - < LCL

Pyriproxyfen GC/MSMS 1 1 0.01 0.1 0.05 0.01

- - - - - - - - - - - -15 15 - - < LCL Tributyl phosphate GC/MSMSPyrimethanil LC/MSMS 15 15 10 15

0.01 0.1 0.01 0.01 - - < LCL- - < LCL Tribenuron-methyl LC/MSMS - - - -

- - < LCL

Pyridaphenthion GC/MSMS - - - - 0.01 0.1 0.01 0.01

- - - - 0.01 0.1 0.01 0.010.01 1 - - < LCL Triazophos GC/MSMSPyridalyl GC/MSMS - - - - 0.01 0.1

0.01 0.1 0.05 0.01 - - < LCL- - < LCL Triasulfuron LC/MSMS - - - -

- - < LCL

Pyridaben LC/MSMS - - - - 0.01 0.1 0.01 0.01

- - - - - - - - - - - -0.01 0.01 - - < LCL Triallate GC/MSMSPyrazophos LC/MSMS - - - - 0.01 0.1

0.5 0.1 0.01 0.01 - - < LCL- - < LCL Triadimenol GC/MSMS - - - -

- - < LCL

Pyraclostrobin LC/MSMS 4 4 3 3.5 3 3

- - - - 0.1 0.1 0.01 0.053 0.01 - - < LCL Triadimefon GC/MSMSPymetrozine LC/MSMS - - - - 0.01 0.1

5 0.1 0.02 0.01 5 < LCL- - < LCL Tolyfluanid GC/MSMS - - - -

- - < LCL

Prosulfuron LC/MSMS - - - - 0.01 0.1 0.01 0.01

- - - - 0.1 0.1 0.01 0.010.01 0.01 - - < LCL Tolchlofos methyl GC/MSMSProsulfocarb LC/MSMS - - - - 0.01 0.1

- - - - - - - - - - < LCL- - < LCL Tokution GC/MSMS - - - -

- - < LCL

Propyzamide LC/MSMS 0.05 0.05 0.01 0.1 0.01 0.01

- - - - 3 6 0.1 20.05 0.01 - - < LCL Thiophanate-methyl LC/MSMSPropoxur LC/MSMS - - - - 1 0.1

- - - - - - - - - - < LCL- - < LCL Thionazin LC/MSMS - - - -

- - < LCL

Propiconazole GC/MSMS 1 1 0.05 1 0.01 0.01

- - - - - - - - - - - -0.01 0.01 - - < LCL Thiofanox Sulfoxide LC/MSMSPropetamphos LC/MSMS - - - - 0.01 0.1

1 0.1 0.01 0.01 - - < LCL- - < LCL Thiodicarb LC/MSMS - - - -

< LCL

- - < LCL

Propazin GC/MSMS - - - - 0.01 0.1 0.01 0.01

- - - - 3 0.1 0.01 10.01 0.01 - - < LCL Thiocyclam hydrogen oxalate GC/MSMSPropargite (Omite) LC/MSMS - - - - 0.01 0.1

0.01

0.01 0.1 0.01 0.01 - - < LCL- - < LCL Thiobencarb LC/MSMS - - - -

- - < LCL

Propanil LC/MSMS - - - - 0.1 0.1 0.01 0.01

- - - - 0.01 0.1 0.01 0.010.01 0.01 - -

Cantidad obtenida en

mg/kg (ppm)Analito

Analizado

mediante

equipo

Uso autorizado

LMR (ppm) Cantidad obtenida

en mg/kg (ppm)

Thifensulfuron-methyl LC/MSMSPropamocarb LC/MSMS - - - - 0.01 0.1

0.01 0.1 0.01 0.01 - - < LCL- - < LCL Thidiazuron LC/MSMS - - - -Propachlor LC/MSMS - - - - 0.01 0.1 0.02

KOR CHN

፨ Productor:BERTA LORENA MORENO

RODRIGUEZ፨ Huerto: ZIRACUARETIRO ፨ Reg. Sagarpa: SD

፨ Cliente: FRUITS GIDDINGS SA DE CV ፨ Muestra: Zarzamora No. Reg. Lab.: P-19-28976

CHN MX US JP CA EUMX US JP CA EU KOR

Resultados de análisisSe han detectado residuos de pesticidas dentro de los límites permitidos

Analito

Analizado

mediante

equipo

Uso autorizado

LMR (ppm)

Fecha de reporte: 2019-12-22 Página: 5 de 7 Revisión: AR271-TS-48

JP CA EU KOR CHNAgrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

Cromatograma GC: P-19-28976 12-21-2019.D Cromatograma LC: P-19-28976 12-21-2019.d MX US

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El re sultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del

resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.

Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.

Documento controlado ISO/IEC 17025:2017

Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]

*Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado. Las bandas de colores son de apoyo visual basadas en los LMRs de México y no representan un resultado. 1Límite Máximo de Residuos (LMR) expresados en ppm para cada país indicado en código ISO 3166 -1 alfa-3. LCL = Lowest Calibration Level (Nivel Mínimo de Calibración) ppm = Partes por millón = mg/kg GC/MSMS =Cromatografía de Gases/Masas/Masas LC/MSMS = Cromatografía de Líquidos/MasasMasas Trazas/Traces = < 0.010 ppm.

Autoriza

Lic. Carlos Sepulveda Ibarra IBT. Cesar Arturo Sanchez Espindola Director General Analista de Cromatografia

Page 6: Fecha de reporte: 2019-12-22 Página: Revisión: AR271-TS-48 ...agrolab.fictionsecurity.com/resultados/Files/869A-33D0-2297-474C-8… · ፨ Razón social: Fruits-Giddings SA de CV

0.005

0.010

0.005

0.010

Trimidal

Uniconazole

Vamidothion

Vinclozolin

Haloxyfop-methyl 0.005

Heptachlor 0.010

Formetanate 0.005

Fosthiazate 0.005

Fuberidazole 0.005

Furathiocarb 0.005

g Chlordan 0.010

Flutriafol 0.005

Fluvalinate 0.010

Fluxapyroxad 0.005

Folpet 0.010

Forchlorfenuron 0.005

Flupyradifurone* 0.005

Fluridone 0.010

Flurtamone 0.005

Flusilazole 0.005

Flutolanil 0.010

Fluometuron 0.005

Fluopicolide 0.005

Fluopyram 0.010

Fluoroglycofen-ethyl 0.005

Fluoxastrobin 0.005

Flucythrinate 0.010

Fludioxonil 0.010

Flufenacet 0.005

Flufenoxuron 0.005

Flumiclorac-pentyl 0.010

Flazasulfuron 0.005

Flonicamid 0.010

Fluazifop-butyl 0.005

Flubendiamide 0.010

Fluchloralin 0.010

Fenthion 0.010

Fenuron 0.005

Fipronil 0.020

Flamprop methyl 0.010

Flamprop-isopropyl 0.010

Fenpropidin 0.005

Fenpropimorph 0.005

Fenpyroximate 0.005

Fenson 0.020

Fensulfothion 0.010

Analito LCL (ppm)

Fenitrothion 0.020

Fenoxaprop-ethyl 0.005

Fenoxycarb 0.005

Fenpropathrin 0.010

Methamidophos 0.005 Pentachlorophenol 0.010 Spinosad A 0.005

Metazachlor 0.005 Pentachloroaniline 0.010 Simetryn 0.005

Metamitron 0.005 Pendimethalin 0.005 Simazine 0.010

Metalaxyl-M (Mefenoxam, R-

enantiomero de metalaxyl)0.010 Pencycuron 0.005 Sethoxydim* 0.010 Triflumizole 0.005

Methabenzthiazuron 0.005 Pentachloronitrobenzene 0.010 Spinetoram J 0.005

Mandipropamid 0.005 Paraoxon-methyl 0.005 Quizalofop-ethyl 0.005

Triforine 0.010

Triflumuron 0.010

Trifluralin 0.010

Triflusulfuron-methyl 0.005

Methoxychlor 0.010 Phorate-sulfoxide 0.005 Sulfoxaflor 0.005

Methoprotryne 0.005 Phorate-sulfone 0.005 Sulfotep 0.005

Methiocarb 0.020 Permethrin 0.010 Spiromesifen 0.005

Methiocarb sulfoxide 0.020 Phenthoate 0.005 Spiroxamine 0.005

Methiocarb sulfone 0.010 Phenmedipham 0.005 Spirotetramat 0.005

Analito LCL (ppm)

Dimethomorph 0.005

2,6 Dichlorobenzonitrilo 0.010 Bromuconazole* 0.010 Cyanazine 0.005 Dimethylphenol, 2,4- (2,4-xylenol) 0.010

2,3 dihydro-2,2dimethylbenzofuran

7-ol0.020

Methoprene 0.010 Phorate 0.010 Sulfosulfuron 0.005

Methomyl 0.005 Phenyl valerate 0.010 Sulfentrazone 0.005

Methidathion 0.005 Penthiopyrad 0.010 Spirodiclofen 0.005

Picolinafen 0.005 Tebufenpyrad 0.010

Metobromuron 0.010 Phoxim 0.010 Tebufenozide 0.005

Methylpentachlophenyl Sulfide 0.010 Phosphamidon 0.005 Tebuconazole 0.010

Methoxyfenozide 0.005 Phosalone 0.010 Sumithrin 0.020

Fecha de reporte: 2019-12-22 Página: 6 de 7 Revisión:Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

AR271-TS-48

Analito LCL (ppm)

Dimethenamid 0.005

2, 4-D Methyl ester 0.010 Bromophos methyl 0.010 Coumaphos 0.010 Dimethoate 0.010

1-Naphthol 0.010 Bromacil 0.010 Clothianidin 0.005

Lowest Calibration Level (Nivel Mínimo de Calibración) por analitoAnalito LCL (ppm) Analito LCL (ppm)

Bromopropylate 0.010 Crimidine 0.005

Diniconazole 0.005

3,4 Dichloroaniline 0.010 Buprofezin 0.010 Cyazofamid 0.005 Dinotefuran 0.0052,6-Dichlorobenzamide 0.005 Bupirimate 0.005 Cyantraniliprole 0.005

Dioxathion 0.010

Abamectin 0.005 Butocarboxim* 0.010 Cyflufenamid 0.010 Diphenamid 0.0053-Hydroxy carbofuran 0.005 Butachlor 0.010 Cycloate 0.005

Diphenylamine 0.010

Acetamiprid 0.005 Buturon 0.005 Cyfluthrin 0.010 Disulfoton 0.010Acephate 0.005 Butocarboxim-sulfoxide 0.005 Cyflumetofen 0.005

Disulfoton sulfone 0.010

Aclonifen 0.010 Cadusafos 0.010 Cymoxanil 0.005 Disulfoton sulfoxide 0.010

Acetochlor 0.005 Butylate 0.020Cyhalothrin (Isomero Lambda y

gamma)**0.010

Diuron (Karmex) 0.005

Alachlor 0.005 Carbaryl 0.010 Cyproconazole 0.005 Dodemorph 0.005

Acrinathrin 0.020 Captan 0.010Cypermethrin a (Zeta-

Cypermethrin)**0.010

Dyfonate 0.010

Aldicarb sulfone 0.005 Carbetamide 0.005 Cyromazine 0.005 Edifenphos 0.005Aldicarb 0.005 Carbendazim 0.005 Cyprodinil 0.010

Emamectin Benzoate 0.005

Aldrin 0.010 Carboxin 0.005 DDD-p,p 0.010 Endosulfan I (alpha isomer) 0.010Aldicarb-sulfoxide (Aldoxicarb) 0.005 Carbofuran 0.010 DDD-o,p 0.010

Endosulfan II (beta isomer) 0.010

Ametryn 0.010 Chinometionate 0.010 DDE-p,p 0.010 Endosulfan sulfato 0.010Ametoctradin 0.005 Carfentrazone ethyl 0.005 DDE-o,p 0.010

Endrin 0.010

Aminocarb 0.005 Chlorbromuron 0.005 DDT-p,p 0.010 Epoxiconazole 0.005

Amicarbazone 0.005 Chlorantraniliprole 0.005 DDT-o,p 0.010

EPTC 0.010

Atrazine-2-hydroxy 0.005 Chlordimeform 0.010 Deltamethrin 0.010 Esfenvalerate + Fenvalerate (**) 0.010Atrazine 0.010 Chlordane- a 0.010 DEET (Diethyl-m-toluamide, N,N-) 0.010

Etaconazole (Etaconazole I y II) 0.010

Azinphos-ethyl 0.005 Chlorfenvinphos 0.005 Demeton S 0.010 Ethalfluralin 0.010Azamethiphos 0.005 Chlorfenapyr 0.010 Demeton O 0.010

Ethiofencarb 0.005

Azoxystrobin 0.010 Chloridazon (Pyrazon) 0.005 Desmedipham 0.005 Ethiofencarb-sulfone 0.005Azinphos-Methyl 0.005 Chlorfluazuron 0.005 Demeton-s-methyl-sulfone 0.005

Ethirimol 0.005

Benalaxyl 0.010 Chlormequat 0.005 Dialifos 0.005 Ethoprop 0.010Baycarb 0.005 Chlorimuron-ethyl 0.005 Desmetryn 0.010

Ethylan 0.010

Benfluralin 0.010 Chloroneb 0.010 Dichlofluanid 0.010 Etion 0.010Bendiocarb 0.005 Chlorobenzilate 0.010 Diazinon 0.010

Etofenprox 0.010

Bensulide 0.005 Chlorothalonil 0.010 Dichlorvos 0.010 Etoxazole 0.005Bensulfuron-methyl 0.005 Chloropropylate 0.010 Dichloran 0.010

Famoxadone 0.010

Benzoximate 0.005 Chloroxuron 0.005 Diclofop methyl 0.020 Fenamidone 0.010Benthiavalicarb-isopropyl 0.005 Chlorotoluron 0.005 Diclobutrazol* 0.010

Fenamiphos 0.005

BHC lindane beta 0.010 Dieldrin 0.010 Fenamiphos Sulfone 0.005BHC lindane alpha 0.010 Chlorpropham 0.010 Dicrotophos 0.005

Fenamiphos Sulfoxide 0.005Chlorpyrifos 0.010

BHC lindane gamma 0.010 Difenoconazole 0.005 Fenarimol 0.005BHC lindane delta 0.010 Diethofencarb 0.005Chlorpyrifos methyl 0.010

Chlorsulfuron 0.005

Fenazaquin 0.005

Bifenox 0.020 Chlorthiophos 0.020 Diflubenzuron* 0.005 Fenbuconazol 0.005Bifenazate 0.005 Chlortal dimethyl** 0.010 Difenoxuron 0.005

Fenbutatin oxide* 0.010

Bitertanol 0.005 Clofentezine 0.005 Dimefuron 0.005 Fenchlorphos 0.010Bifenthrin 0.010 Clodinafop-propargyl 0.005 Diflufenican 0.005

Fenfuram 0.005

Boscalid 0.005 Cloquintocet-mexyl 0.005 Dimethachlor 0.005 Fenhexamid 0.005

Bolstar 0.010 Clomazone 0.005 Dimepax 0.010

Analito LCL (ppm)

Heptachlor exo-epoxide (isomer B) 0.020 Metribuzin 0.010 Pirimicarb 0.005 Terbacil 0.010

Analito LCL (ppm) Analito LCL (ppm) Analito LCL (ppm)

Terbumeton 0.005

Hexachlorobenzene 0.010 Mevinphos 0.010 Pirimiphos-methyl 0.005 Terbuthylazine 0.010

Heptenophos 0.005 Metsulfuron-methyl 0.005 Pirimiphos-ethyl 0.005

Terbuthylazine-desethyl 0.005

Hexaflumuron 0.005 MGK-264 0.010 Prochloraz 0.005 Terbutryn 0.010

Hexaconazole 0.005 Mexacarbate 0.005 Primisulfuron-methyl 0.005

Terrazole 0.010

Hexythiazox 0.005 Molinate 0.005 Profenofos 0.010 Tetrachlorvinphos, E-isomer 0.010

Hexazinone 0.010 Mirex 0.010 Procymidone 0.010

Tetradifon 0.010

Imazapyr 0.005 Monolinuron 0.005 Promecarb 0.010Tetrahydrophthalimide, cis-1,2,3,6-

(THPI)0.010

Imazalil 0.005 Monocrotophos 0.005 Profluoralin 0.020

Tetramethrin 0.005

Imidacloprid 0.005 Myclobutanil 0.010 Prometryn 0.010 Thiabendazole 0.005

Imazaquin 0.005 Monuron 0.005 Prometon 0.010

Thiacloprid 0.005

Imiprothrin 0.020 Napropamide 0.005 Propachlor 0.005 Thiamethoxam 0.005

Imidan 0.010N-2,4-Dimethylphenyl formamide

(2,4-DMPF)0.010 Pronamide 0.005

0.005

Indoxacarb 0.010 Neburon 0.005 Propamocarb 0.005

Thiobencarb 0.010

Thidiazuron 0.005

Iprodione 0.010 Nicosulfuron 0.005

Iprovalicarb 0.005 Nitrapyrin 0.010 Propargite (Omite) 0.005

Propanil 0.005 Thifensulfuron-methyl

Propoxur 0.005

Isocarbophos 0.010 Norflurazon-Desmethyl 0.010

Irgarol 0.005 Nitrothal-isopropyl 0.010 Propazin 0.010

Isazophos 0.010 Norflurazon 0.005 Propetamphos

Propiconazole

0.005

0.010

Isofenphos 0.005 Novaluron* 0.010

Isoprothiolane 0.010 Ofurace 0.005 Prosulfocarb 0.005

Isoprocarb 0.005 O Phenylphenol 0.010 Propyzamide 0.005

Isoxaflutole 0.010 op Dicofol*** 0.010 Pymetrozine 0.005

Isoproturon 0.005 Omethoate 0.005 Prosulfuron 0.005

Kresoxim-methyl 0.005 Oxadiazon 0.010 Pyrazophos 0.005

Kelthane*** 0.010 Ovex 0.010 Pyraclostrobin 0.005

Leptophos 0.010 Oxamyl 0.005 Pyridalyl 0.010

Lenacil 0.005 Oxadixyl 0.005 Pyridaben 0.005

Lufenuron 0.005 Oxydemeton-methyl 0.005 Pyrimethanil 0.005

Linuron 0.005 Oxamyl Oxime 0.005 Pyridaphenthion 0.010

Malathion 0.010 Paclobutrazol (Bonzi) 0.005 Quinalphos 0.005

Malaoxon 0.005 Oxyfluorfen 0.010 Pyriproxyfen 0.010

Mancozeb 0.005 Paraoxon 0.005 Quinoxyfen 0.005

Sebuthylazine 0.010

Mecarbam 0.005 Parathion methyl 0.010 Rotenone 0.005

Mebendazole 0.005 Parathion 0.010 Rimsulfuron 0.005

Mepanipyrim 0.010 Penconazol 0.005

Metrafenone 0.005 Piperophos 0.005 Teflubenzuron 0.010

Metconazole 0.005 Pentachloroanisol 0.010 S-Metolachlor 0.005

Metoxuron 0.005 Piperonyl Butoxide 0.005 Tecnazene 0.010

Metosulam 0.005 Piperalin 0.005 Tebuthiuron 0.005

Metolcarb 0.010 Picoxystrobin 0.005 Tebutam 0.005

Metolachlor 0.005

Thiocyclam hydrogen oxalate

Thiodicarb

Thiofanox Sulfoxide

Thionazin

Thiophanate-methyl

Tokution

Tolchlofos methyl

Tolyfluanid

Triadimefon

0.010

0.005

0.005

0.005

0.005

0.010

0.010

0.010

0.010

Triadimenol

Triallate

Triasulfuron

Triazophos

0.010

0.010

0.005

0.010

Trichloronate 0.010

Trichlorfon 0.005

Tributyl phosphate 0.010

Tribenuron-methyl 0.005

Trifloxystrobin 0.005

Triclocarban 0.010

Tricyclazole 0.010

Trietazine 0.005

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la

representatividad del resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.

Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tacha duras o enmendaduras.

Documento controlado ISO/IEC 17025:2017

Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]

ppm = Partes por millón = mg/kg Incertidumbre = 50 % según "Method validation and quality control procedures for pesticide residues analysis in food and feed ". No. de Documento SANCO/10684/2009. Punto 91

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International Maximum Residue Level Database

http://www.mrldatabase.com/

EU Pesticides Database

http://ec.europa.eu/sanco_pesticides/public/index.cfm

Electronic Code of Federal Regulation

http://ecfr.gpoaccess.gov/cgi/t/text/text-idx?

Health Canada

http://pr-rp.hc-sc.gc.ca/mrl-lrm/index-eng.php

Normas Alimentarias FAO/OMS

http://www.codexalimentarius.net/pestres/data/pesticides/search.html

Positive List System for Agricultural Chemical Residues in Foods (Japón)

http://m5.ws001.squarestart.ne.jp/foundation/search.html

Información correspondiente a la página 2, página 3, página 4 y página 5

Información correspondiente a la página 5 y 6

Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

Referencias

Glosario

Trazas = < 0.010 ppm.

MX= México

US= Estados Unidos

JP= Japón

CA= Canadá

EU= Union Europea

KOR=Corea

CHN= China

GC/MSMS = Gases/Masas/Masas AGILENT 225/MS, 240/MS

LC/MSMS = Líquidos/Masas/Masas QQQ (AGILENT 6460)

LCL = Lowest Calibration Level (Nivel Mínimo de Calibración)

LMR = Límite Máximo de Residuos

ppm = Partes por millón = mg/Kg

SD = Sin dato

1. El laboratorio Análisis Técnicos S.A. de C.V. se encuentra acreditado ante la EMA, en el Ensayo de determinación de residuos de pesticidas en frutas, legumbres, alimentos agrícolas y semillas

(incorporando extracción QuEChERS), por cromatografia de GASES/MASAS/MASAS ante el sistema ISO/IEC 17025:2017.

2. El laboratorio Análisis Técnicos S.A. de C.V. se encuentra acreditado ante la EMA, en el Ensayo de determinación de residuos de pesticidas en frutas, legumbres, alimentos agrícolas y semillas

(incorporando extracción QuEChERS), por cromatografia de LÍQUIDOS/MASAS/MASAS ante el sistema ISO/IEC 17025:2017.

3. * = Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado.

4. Uso autorizado del plaguicida en el país correspondiente indicado en código ISO 3166-1 alfa-2. Los LMR de cada país se indican en la misma tabla de resultados.

5. En caso de no haber sido detectado algun pesticida se observa una banda verde fuerte. En caso de haber detectado algun pesticida dentro de los límites permitidos se observa una banda amarilla.

En caso de haber detectado algun pesticida fuera de los límites permitidos se observará una banda roja. En caso de haber detectado algún pesticida prohibido se observará una banda roja.

6. Las bandas de colores son de apoyo visual basadas en los LMRs de cada país y no representan un resultado..Las bandas de colores de cada molécula son de apoyo visual basadas en los LMRs

de cada país y no representan un resultado.

7. ** Se toma el LMR de Isomero Lambda para la molécula Cyhalothrin (Isomero Gamma y Lambda) , para Cypermethrin a (Zeta-Cypermethrin) se toma el LMR de Zeta-Cypermethrin y para el LMR

de Esfenvalerate + Fenvalerate se toma el de Esfenvalerate. Se toma el LMR del sinónimo DCPA para la molécula Chlortal dimethyl.

8. 2 = Para Canadá se considera el default LMR de 0.1 ppm según el punto 5.2.1.4.2 Food and Drug Regulations de Canada Food Inspection Agency http://www.inspection.gc.ca/food/meat-and-

poultry-products/manual-of-procedures/chapter-5/eng/1395150894222/1395150895519?chap=2.

9.El laboratorio Análisis Técnicos S.A. de C.V. se encuentra acreditado ante A2LA en el Ensayo de determinación de residuos de pesticidas en frutas, legumbres, alimentos agrícolas y semillas

(incorporando extracción QuEChERS), por cromatografia de GASES/MASAS/MASAS ante el Metodo de Referencia AOAC 2007.01.

10. El laboratorio Análisis Técnicos S.A. de C.V. se encuentra acreditado ante la A2LA, en el Ensayo de determinación de residuos de pesticidas en frutas, legumbres, alimentos agrícolas y semillas

(incorporando extracción QuEChERS), por cromatografia de LÍQUIDOS/MASAS/MASAS ante el Metodo de Referencia AOAC 2007.01.

***El LMR de Dicofol es la suma de Kelthane(Dicofol) y op Dicofol

1. En las tablas correspondientes se presenta el punto más bajo de la calibración (LCL).

2. Las tablas correspondientes NO REPRESENTAN UN RESULTADO. Son datos informativos de calidad.

3.Incertidumbre = 50 % según "Method validation and quality control procedures for pesticide residues analysis in food and feed". No. de Documento SANCO/10684/2009. Punto 91

Ultima fecha de actualización de LMR :2019/12/16

Límites Máximos de Residuos (LMR) para Zarzamora indicados en El Catálogo Oficial de

Plaguicidas de México 2004.

Límites Máximos de Residuos (LMR) para Zarzamora indicados en Enviromental Protection

Agency (EPA) Estados Unidos.

Límites Máximos de Residuos (LMR) para Zarzamora indicados en Electronic Code of

Federal Regulations, (e-CFR TM) Estados Unidos.

1. El cliente tiene cinco días naturales posteriores a la emisión de resultados**** para poder hacer alguna observación o reclamación al respecto, ya que en caso de no hacerlo en este periodo de

tiempo se considerará este informe como aceptado.

2. Las muestras podrán ser desechadas a los 5 días después de la emisión de resultados****, únicamente las muestras para análisis microbiológico serán desechadas 24 h después de ser

recibidas.

3. La información inscrita en el presente "Informe de resultados de análisis" se trata con estricto apego al aviso de privacidad de Análisis Técnicos S.A. de C.V. acatando a los artículos tercero

transitorio, 16 y 17 de la Ley Federa de Protección de Datos Personales en Posesión de los Particulares, con la finalidad de regular su tratamiento legítimo, controlado e informado, a efecto de

garantizar la privacidad y el derecho a la autodeterminación informativa de las personas.

4. Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas.

5. Análisis Técnicos S.A. de C.V. no se encuentra acreditado en muestreo.

6. Los LMR de los paises son un dato de referencia, solicitando revisar los sitios oficiales de cada país ya que pueden cambiar o modificarse.

7. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V., por lo cual no se hace responsable de la representatividad del resultado para el total del

producto

8. Este formato de interpretación está protegido y registrado ante el Instituto Nacional del Derecho de Autor (INDAUTOR), así mismo, los logotipos y nombre de Agrolab y sus filiales se encuentran

registrados ante el Instituto Mexicano de la propiedad Industrial (IMPI). Se prohibe su reproducción total o parcial, para otro fin que no sea la interpretación de resultados, sin previa autorización.

9. El presente informe de resultados no será válido si presenta raspaduras, tachaduras o enmendaduras.

10. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.

11. El laboratorio Análisis Técnicos S.A. de C.V. no es responsable de la actualización de los LMR's ya que son considerados como un dato informativo. Es responsabilidad del usuario del Informe

revisar los sitios oficiales para LMR de cada país ya que la información puede cambiar o modificarse.

12. La detección del residuo del plaguicida por arriba del límite de cuantificación se reporta como ppm (mg//Kg) , por debajo del límite de cuantificación se reportar como <LCL ppm (mg/Kg) y por

debajo del LD se considera como no detectado.

13.La regla de decisión no incluye la incertidumbre.

14.La muestra se recibió en condiciones para su análisis.

፨ Información proporcionada por el cliente mediante la solicitud de análisis AR6-AC

****La emisión del resultados, contempla el informe final destinado a ser enviado al cliente (PDF). La entrega de resultados al cliente, se encuentra sujeta a confirmación de pago.

Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

Información adicional y complementaria

Información general

Fecha de reporte: 2019-12-22 7 de 7 Revisión:Página:

Final del informe

AR271-TS-48

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El re sultado representa la muestra que fue recibida en las instalaciones de

Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.

Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.

Documento controlado ISO/IEC 17025:2017

Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]

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Report Date: 2019-12-22 Page: 1 of 7 Revision AR272-TS-48

፨ Address: Km 1 Carr. los Reyes-Jacona S/N ፨ City or Town: Los Reyes

፨ State: Michoacán ፨ ZIP Code: 60330

Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

Client Information

፨ Applicant: ROSALVA OLMOS CERVANTES ፨ Company: FRUITS GIDDINGS SA DE CV

Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

Billing Information

፨ Corporate name: Fruits-Giddings SA de CV ፨ RFC SBM040520QN6

Telephone: 3545427328 ፨ Ext. 133 ፨ E-mail: [email protected]

፨ Telephone: 3545420170 ፨ Ext. SD ፨ E-mail: [email protected], [email protected]

፨ Address: Km. 1 Carretera los Reyes- Jacona Sn ፨City or Town: Los Reyes

፨ State: Michoacán ፨ ZIP Code: 60330

Receipt Date: 2019-12-21 Start Date: 2019-12-21 Termination Day: 2019-12-22

Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

Pesticides Multiresidual Analysis

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Sample Information

Sample Reg. No. P-19-28976 Registry Book: dic-19

፨ Analyzed part: Fruit ፨ Sample status: Fresh ፨ Amount (weight or

volume):Less Than 1.5Kg

፨Common Name: Zarzamora ፨ Scientific Name: Rubus Ulmifoli ፨ Variety: Tupy

፨ Sampling Place:EL CARMEN DIRECCION:

ZIRACUARETIRO, MICHOACÁN ፨ Sampling Method: Random ፨Warehouse RFC: SD

፨ Producer:BERTA LORENA MORENO

RODRIGUEZ ፨ Harvest Place: ZIRACUARETIRO ፨ SAGARPA Reg.: SD

፨ Sampling date and

time:2019-12-19 Hora: 08:00 Hrs ፨ Final Destination: U.S.A.,U.E AND CANADA SD

፨ Commercial use: Human ፨ Commercial Destination: Foreign Market ፨Customs House: SD

፨Manufacturing

date:

፨ Name of who takes the

sample:

MARIA DE LA SALUD JIMENEZ

MONTAÑO (Cliente)

፨ Sample code or lot

number:3899-01 SECTOR 01

Observations:

SD

፨ Temperature: 20.0 ºC ፨ Presentation: BOLSA PLASTICA ፨ Expiration

date:SD

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it´s not responsible for the representation of the

result for the total product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.

This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad IntelectualIts total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.

Controlled document ISO/IEC 17025:2017

Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]

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B B

B B

B B

B B

B B

B B

B BB B

B B

B BB BB BB BB B

B B

B B

B B

B BB BB BB BB B

B B

B BB BB BB BB B

B B

B B

B B

B B

B B

B B

B B

B BB BB B

B B

B BB B

B B

B B

B B

B V

B B

B B

B BB BB BB B

B B

B B

B B

B B

B B

B B

B B

B B

B B

KOR CHN

OXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL METABOLITE

- - - -

0.01 0.01

- - - -

- - - -

- - - -

- - - -

- - - -

- - - -

0.1 0.2

- - - -

0.01 0.01

0.01 1

0.02 1

0.2 0.5

0.01

0.02 0.01

3 1

0.5 2

0.05 0.01

3 1

0.05 0.01

- - - -

0.01 0.01

- - 0.01

0.01 1

0.01 0.01

0.01 0.01

0.9 0.7

0.01 0.01

0.01 0.01

0.01

0.01 0.5

0.01 0.05

0.01 1

0.1 0.01

0.02 0.01

0.01 0.01

0.01 1

0.02 0.02

0.01 0.01

- - - -

0.01 1

0.01 0.01

0.01 0.01

0.01 0.05

THIOPHANATE

 METHYL/ BENOMYL

METABOLITE

0.01 0.01

0.01 0.01

0.03 0.01

0.01 0.1

0.01 0.01

1 1

- - - -

0.01 0.02

1.5 0.01

0.01 1

0.01 0.01

0.01 0.01

0.01 0.01

- - - -

20 5

0.01 0.5

THIOPHANATE

 METHYL/

BENOMYL

METABOLITE

0.01

0.01

0.01 0.01

0.01 0.01

7 7

0.01 0.01

1 0.3

0.01 0.01

- - - -

10 9

0.01 0.01

0.05 0.01

0.01 0.01

0.02 0.01

0.01 0.01

0.01 0.01

0.01 0.1

0.01 0.01

0.01 0.01

0.01 0.01

0.01 0.01

0.01 0.01

- - - -

0.05 0.01

- - - -

0.01 0.01

0.02 0.01

0.05 0.3

5 3

0.01 0.01

0.01 0.01

0.02 0.01

0.01 0.05

0.02 0.01

0.02 0.01

0.01 0.01

0.01 0.01

0.01 0.01

0.1 0.01

- - - -

- - - -

- - - -

LINURON

METABOLITELINURON METABOLITE

- - - -

0.08 0.05

0.01 1

2 1

Report Date: 2019-12-22 Page: 2 of 7 Revision: AR272-TS-48

Chromatogram GC: P-19-28976 12-21-2019.D Chromatogram LC: P-19-28976 12-21-2019.d

Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

Analysis Results

፨ Producer: BERTA LORENA MORENO RODRIGUEZ ፨ Orchard: ZIRACUARETIRO ፨SAGARPA Reg.: SD

፨ Client: FRUITS GIDDINGS SA DE CV ፨ Sample: Zarzamora Lab Reg. No.: P-19-28976

US JPMX CA EU

JP CA CHN

1-Naphthol GC/MSMSCARBARYL

METABOLITE

CARBARYL

METABOLITE

CARBARYL

METABOLITE

CARBARYL

METABOLITECARBARYL METABOLITE

US JP CA CHN MX US

Pesticide residues have been detected within the allowed limits

Analyte Analyzed by

Authorized use

MRL (ppm) Obtained amount in mg/kg

(ppm)Analyte Analyzed by

Authorized use

MRL (ppm) Obtained amount in mg/kg

(ppm)MX EU KOR EU KOR

CARBARYL

METABOLITE

CARBARYL

METABOLITE

0.1 - - < LCL

2,3 dihydro-2,2dimethylbenzofuran 7-ol GC/MSMS - - - - - - - - - -

< LCL Carbetamide LC/MSMS - - - - 0.01

THIOPHANATE

 METHYL/

BENOMYL

METABOLITE

THIOPHANATE

 METHYL/ BENOMYL

METABOLITE

< LCL

2, 4-D Methyl ester GC/MSMS 0.2 0.2 0.1 0.1 0.1

< LCL Carbendazim LC/MSMSTHIOPHANATE

 METHYL/ BENOMYL

METABOLITE

THIOPHANATE

 METHYL/

BENOMYL

METABOLITE

THIOPHANATE

 METHYL/ BENOMYL

METABOLITE

0.1 - - < LCL

2,6-Dichlorobenzamide LC/MSMS - - - - - - - - - -

< LCL Carboxin LC/MSMS - - - - 0.01

0.1 0.02 < LCL

2,6 Dichlorobenzonitrilo GC/MSMS - - - - - - - - - -

< LCL Carbofuran GC/MSMS - - - - 0.3

0.1 - - < LCL

3-Hydroxy carbofuran LC/MSMS - - - - - - - - - -

< LCL Chinometionate GC/MSMS - - - - 0.01

0.1 - - < LCL

3,4 Dichloroaniline GC/MSMS LINURON METABOLITELINURON

METABOLITE

LINURON

METABOLITE

LINURON

METABOLITELINURON METABOLITE

< LCL Carfentrazone ethyl LC/MSMS 0.1 0.1 0.1

- - - - < LCL

Acephate LC/MSMS - - - - 0.01 0.1 0.50

< LCL Chlorbromuron LC/MSMS - - - - - -

0.9 1 < LCL

Abamectin LC/MSMS 0.2 0.2 0.05 0.2 - -

< LCL Chlorantraniliprole LC/MSMS 1.8 1.8 2

0.1 0.01 < LCL

Acetochlor LC/MSMS - - - - 0.01 0.1 - -

< LCL Chlordimeform GC/MSMS - - - - 0.01

0.1 0.02 < LCL

Acetamiprid LC/MSMS 1.6 1.6 2 4 2

< LCL Chlordane- a GC/MSMS 0.1 0.1 0.02

0.1 - - < LCL

Acrinathrin GC/MSMS - - - - 0.01 0.1 - -

< LCL Chlorfenvinphos LC/MSMS - - - - 0.05

0.1 - - < LCL

Aclonifen GC/MSMS - - - - 0.01 0.1 - -

< LCL Chlorfenapyr GC/MSMS - - - - 0.01

0.1 - - < LCL

Aldicarb LC/MSMS - - - - 0.01 0.1 0.02

< LCL Chloridazon (Pyrazon) LC/MSMS - - - - 0.01

0.1 - - < LCL

Alachlor LC/MSMS - - - - 0.01 0.1 - -

< LCL Chlorfluazuron LC/MSMS - - - - 0.01

0.1 - - < LCL

Aldicarb-sulfoxide (Aldoxicarb) LC/MSMS - - - - 0.01 0.1 - -

< LCL Chlormequat LC/MSMS - - - - 0.01

0.1 - - < LCL

Aldicarb sulfone LC/MSMS - - - - 0.01 0.1 0.02

< LCL Chlorimuron-ethyl LC/MSMS - - - - 0.01

0.1 - - < LCL

Ametoctradin LC/MSMS - - - - 0.01 0.1 - -

< LCL Chloroneb GC/MSMS - - - - 0.01

0.1 - - < LCL

Aldrin GC/MSMS 0.05 0.05 0.05 0.1 0.05

< LCL Chlorobenzilate GC/MSMS - - - - 0.01

0.1 - - < LCL

Amicarbazone LC/MSMS - - - - 0.01 0.1 - -

< LCL Chlorothalonil GC/MSMS - - - - 10

- - - - < LCL

Ametryn GC/MSMS - - - - 0.01 0.1 - -

< LCL Chloropropylate GC/MSMS - - - - - -

0.1 - - < LCL

Atrazine GC/MSMS - - - - 0.02 0.1 - -

< LCL Chloroxuron LC/MSMS - - - - 0.01

0.1 - - < LCL

Aminocarb LC/MSMS - - - - - - - - - -

< LCL Chlorotoluron LC/MSMS - - - - 0.01

< LCL

0.1 - - < LCL

Atrazine-2-hydroxy LC/MSMS - - - - - - - - - -

< LCL Chlorpropham GC/MSMS - - - - 0.01

Chlorpyrifos GC/MSMS - - - - 1 0.1 - - < LCL0.01 0.01

< LCLAzinphos-ethyl LC/MSMS - - - - 0.01 0.1 - -

- - - -

Azamethiphos LC/MSMS - - - - 0.01 0.1 - - < LCL Chlorpyrifos methyl GC/MSMS - - - - 0.05 0.1 - -

0.1 - -

0.01 0.01

0.05 0.01

0.01 < LCL

Azoxystrobin GC/MSMS 5 5 5 5 - -

< LCL Chlortal dimethyl** GC/MSMS - - - - 0.01Azinphos-Methyl LC/MSMS - - - - 0.01 2 1 0.01

- - - -

0.1 - - < LCL

Benalaxyl GC/MSMS - - - - 0.05 0.1 - -

< LCL Clodinafop-propargyl LC/MSMS - - - - 0.02

< LCL

Baycarb LC/MSMS - - - - - - - - - -

< LCL Chlorthiophos GC/MSMS - - - - - -

- - - -

0.1 - - < LCL

Benfluralin GC/MSMS - - - - 0.01 0.1 - -

< LCL Clomazone LC/MSMS - - - - 0.02

0.1 - - < LCL

Bendiocarb LC/MSMS - - - - 0.01 0.1 - -

< LCL Clofentezine LC/MSMS - - - - 0.01

0.1 - - < LCL

Bensulide LC/MSMS - - - - 0.01 0.1 - -

< LCL Clothianidin LC/MSMS - - - - 0.2

0.1 - - < LCL

Bensulfuron-methyl LC/MSMS - - - - 0.01 0.1 - -

< LCL Cloquintocet-mexyl LC/MSMS - - - - 0.01

- - - - < LCL

Benzoximate LC/MSMS - - - - 0.01 0.1 - -

< LCL Crimidine LC/MSMS - - - - - -

0.1 0.05 < LCL

Benthiavalicarb-isopropyl LC/MSMS - - - - 0.01 0.1 - -

< LCL Coumaphos GC/MSMS - - - - - -

4 - - < LCL

BHC lindane beta GC/MSMS 0.5 0.5 0.3 0.1 - -

< LCL Cyantraniliprole LC/MSMS 4 4 0.01

0.1 - - < LCL

BHC lindane alpha GC/MSMS 0.5 0.5 0.3 0.1 - -

< LCL Cyanazine LC/MSMS - - - - 0.01

0.1 - - < LCL

BHC lindane gamma GC/MSMS 0.5 0.5 0.3 0.1 - -

< LCL Cycloate LC/MSMS - - - - 0.01

0.02 - - < LCL

BHC lindane delta GC/MSMS 0.5 0.5 0.3 0.1 - -

< LCL Cyazofamid LC/MSMS - - - - 0.01

0.1 - - < LCL

Bifenox GC/MSMS - - - - 0.01 0.1 - -

< LCL Cyflumetofen LC/MSMS - - - - 0.01

0.1 - - < LCL

Bifenazate LC/MSMS 5 5 7 5 7

< LCL Cyflufenamid GC/MSMS - - - - 0.01

0.01 0.2 < LCL

Bitertanol LC/MSMS - - - - 0.05 0.1 - -

< LCLCyhalothrin (Isomero Lambda

y gamma)**GC/MSMS - - - - 0.5

0.1 - - < LCL

Bifenthrin GC/MSMS 1 1 1 1 1

< LCL Cyfluthrin GC/MSMS - - - - 0.02

0.8 - - 0.038

Boscalid LC/MSMS 10 10 10 6 - -

< LCLCypermethrin a (Zeta-

Cypermethrin)**GC/MSMS 0.8 0.8 0.5

4 - - < LCL

Bolstar GC/MSMS - - - - - - - - - -

< LCL Cymoxanil LC/MSMS 4 4 4

- - < LCL

Bromophos methyl GC/MSMS - - - - 0.01 0.1 - -

< LCL Cyprodinil GC/MSMS 10 10 10

0.1 - - < LCL

Bromacil GC/MSMS - - - - 0.01 0.1 - -

< LCL Cyproconazole LC/MSMS - - - - 0.5

0.01

0.1 - -

< LCL DDD-o,p GC/MSMS - - - - - -

0.1 - - < LCL

Bromopropylate GC/MSMS - - - - 2 0.1 - -

< LCL Cyromazine LC/MSMS - - - - 0.010.01

0.01 0.01

0.05 0.01

- - - - 0.01 0.1 - -

< LCL DDE-o,p GC/MSMS - - - - - -

- - - - < LCL

Bupirimate LC/MSMS - - - - 0.01 0.1 - -

< LCL DDD-p,p GC/MSMS - - - - - -Bromuconazole* LC/MSMS - - - - 0.01

Butocarboxim* LC/MSMS - - - - 0.01 0.1 - -

< LCL DDT-o,p GC/MSMS - - - - - -

- - - - < LCL

Butachlor GC/MSMS - - - - 0.01 0.1 - -

< LCL DDE-p,p GC/MSMS - - - - - -

< LCL

Buprofezin GC/MSMS

- - 0.01 0.1 0.02

- - < LCL

Buturon LC/MSMS - - - - - - - - - -

< LCLDEET (Diethyl-m-toluamide,

N,N-)GC/MSMS - - - - - -Butocarboxim-sulfoxide LC/MSMS - - - - 0.01 0.1 - - - -

- - - - < LCL< LCL Demeton O

25 0.01 0.1 - -

- - - -

0.1 0.02 < LCL

0.1 - - < LCL

Butylate GC/MSMS - - - - 0.01 0.1 - -

< LCL Deltamethrin GC/MSMS - - - - 0.1

0.01 0.01

0.01 0.05Cadusafos GC/MSMS - -

< LCL Desmedipham LC/MSMS - - - - 0.01

OXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL

METABOLITE

< LCL

< LCL Demeton S GC/MSMS - - - - 0.4

Carbaryl GC/MSMS 12 12 10 10 - -

< LCL Demeton-s-methyl-sulfone LC/MSMSOXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL

METABOLITECaptan GC/MSMS 25

GC/MSMS - -

< LCL

Chlorsulfuron LC/MSMS - - - - 0.01 0.1 - - < LCL

0.1 - - < LCL

- - - - < LCLDDT-p,p GC/MSMS - - - - - -

- - - - < LCL

- - - - < LCL

- - - - < LCL

10

* Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166 -1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued res ult only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it ´s not responsible for the representation of the result for the total product.

Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product. This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or ame ndments.

Controlled document ISO/IEC 17025:2017

Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]

Authorizes

Lic. Carlos Sepulveda Ibarra IBT. Cesar Arturo Sanchez Espindola Directorate Chromatography Analysts

Page 10: Fecha de reporte: 2019-12-22 Página: Revisión: AR271-TS-48 ...agrolab.fictionsecurity.com/resultados/Files/869A-33D0-2297-474C-8… · ፨ Razón social: Fruits-Giddings SA de CV

B BB BB BB BB BB BB BB BB BB BB BB BB BB B

B B

B B

B B

B BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB B

B B

B B

B B

B B

B B

B BB B

B B

B BB B

B B

B B

B B

B B

B B

B BB B

0.01 0.01

0.01 0.01

0.01 0.02

0.05 0.01

0.01 0.01

0.01 0.01

- - - -

0.01 0.01

0.01 0.01

0.01 0.3

0.01 0.01

0.01 0.01

0.5 0.01

0.1

0.1

0.1

0.1

0.01 0.01

0.01 0.01

0.01 0.01

0.01 0.01

- - - -

0.02 0.05

- - - -

0.01 0.5

0.03 3

0.01 0.01

5 5

0.05 0.01

0.05 0.3

0.01 0.01

0.01 0.01

1.5 1.5

0.01 0.01

0.01 0.5

3 0.01

5 6

0.01 0.01

0.01 0.01

- - - -

0.01 0.01

0.01 0.01

- - - -

0.005 0.01

0.01 0.01

- - - -

0.01 0.01

0.03 0.7

0.01 0.01

0.01 0.01

0.01 0.01

- - - -

- - - -

0.02 0.01

0.01 0.5

0.05 0.01

0.01 2

0.01 0.01

- - - -

15 15

0.01 0.3

0.01 0.010.05 0.01

0.01 0.01

0.01 0.01

0.01 0.01

0.7 0.7

0.1 0.01

0.02 0.01

- - - -

0.01 0.01

0.01 1

0.01 0.3

- - - -

- - - -

0.01 0.01

0.01 0.01

0.01 0.01

0.01 0.01

0.01 0.03

0.01

0.01 0.01

0.02 0.01

0.05 0.05

0.01 0.01

0.05 0.01

0.01 0.01

0.02 0.01

- - - -

0.01 0.01

0.01 5

0.01 5

0.05 0.05

0.05 0.05

0.01 0.01

0.05 1

- - - -

0.01 0.01

0.01 2

0.01 0.01

0.01 0.01

0.05 0.01

0.01 0.01

0.01 0.01

1.5 0.5

- - - -

0.01 0.01

0.01 0.01

- - - -

- - - -

0.01 0.01

0.01 0.01

- - - -

0.01 0.01

0.01 15

0.01 0.01

0.01 0.01- - - -

0.05 0.01

0.01 0.01

0.01 0.01

Report Date: 2019-12-22 Page: 3 of 7 Revision: AR272-TS-48

Chromatogram GC: P-19-28976 12-21-2019.D Chromatogram LC: P-19-28976 12-21-2019.d

Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

Analysis Results

፨ Producer:BERTA LORENA MORENO

RODRIGUEZ፨ Orchard: ZIRACUARETIRO ፨SAGARPA Reg.: SD

፨ Client: FRUITS GIDDINGS SA DE CV ፨ Sample: Zarzamora Lab Reg. No.: P-19-28976

US JP CA EUMX

JP CA CHN

Desmetryn GC/MSMS - - - - 0.01 0.1 - -

US JP CA CHN MX US

Pesticide residues have been detected within the allowed limits

AnalyteAnalyzed

by

Authorized use

MRL (ppm) Obtained amount in

mg/kg (ppm)Analyte

Analyzed

by

Authorized use

MRL (ppm) Obtained amount in

mg/kg (ppm)MX EU KOR EU KOR

0.01 0.01

0.1 - - < LCL

Diazinon GC/MSMS 0.75 0.75 0.1 0.1 0.1

< LCL Fenchlorphos GC/MSMS - - - - 0.01

0.1 - - < LCL

Dialifos LC/MSMS - - - - - - - - - -

< LCL Fenbutatin oxide* LC/MSMS - - - - 1

20 15 < LCL

Dichloran GC/MSMS - - - - 10 10 - -

< LCL Fenhexamid LC/MSMS 20 20 15

- - - - < LCL

Dichlofluanid GC/MSMS - - - - 10 0.1 - -

< LCL Fenfuram LC/MSMS - - - - - -

0.1 - - < LCL

Diclobutrazol* LC/MSMS - - - - - - - - - -< LCL Fenoxaprop-ethyl LC/MSMS - - - - 0.1

0.1 0.5 < LCL

Dichlorvos GC/MSMS - - - - 0.1 0.1 0.2

< LCL Fenitrothion GC/MSMS - - - - 0.8

12 5 < LCL

Dicrotophos LC/MSMS - - - - 0.01 0.1 - -

< LCL Fenpropathrin GC/MSMS 12 12 5

0.1 - - < LCL

Diclofop methyl GC/MSMS - - - - 0.01 0.1 - -

< LCL Fenoxycarb LC/MSMS - - - - 0.05

0.1 - - < LCL

Diethofencarb LC/MSMS - - - - 0.01 0.1 - -

< LCL Fenpropimorph LC/MSMS - - - - 0.05

0.1 - - < LCL

Dieldrin GC/MSMS 0.05 0.05 0.05 0.1 0.02

< LCL Fenpropidin LC/MSMS - - - - 0.01

- - - - < LCL

Difenoxuron LC/MSMS - - - - - - - - - -

< LCL Fenson GC/MSMS - - - - - -

0.1 - - < LCL

Difenoconazole LC/MSMS - - - - 0.01 0.1 - -

< LCL Fenpyroximate LC/MSMS - - 3 0.01

0.1 0.05 < LCL

Diflufenican LC/MSMS - - - - 0.01 0.1 - -

< LCL Fenthion GC/MSMS - - - - 0.01

0.1 - - < LCL

Diflubenzuron* LC/MSMS - - - - 0.01 0.1 - -

< LCL Fensulfothion GC/MSMS - - - - 0.01

0.1 0.02 < LCL

Dimepax GC/MSMS - - - - - - - - - -

< LCL Fipronil GC/MSMS - - - - 0.01

- - - - < LCL

Dimefuron LC/MSMS - - - - - - - - - -

< LCL Fenuron LC/MSMS - - - - - -

- - - - < LCL

Dimethenamid LC/MSMS - - - - 0.01 0.1 - -

< LCL Flamprop-isopropyl LC/MSMS - - - - - -

0.1 - - < LCL

Dimethachlor LC/MSMS - - - - 0.01 0.1 - -

< LCL Flamprop methyl LC/MSMS - - - - 0.01

0.1 - - < LCL

Dimethomorph LC/MSMS - - - - 0.01 0.1 - -

< LCL Flonicamid LC/MSMS - - - - 0.01

0.1 - - < LCL

Dimethoate GC/MSMS - - - - 1 0.1 - -

< LCL Flazasulfuron LC/MSMS - - - - 0.1

0.1 - - < LCL

Diniconazole LC/MSMS - - - - 0.01 0.1 - -

< LCL Flubendiamide LC/MSMS - - - - 0.01

0.08 - - < LCL

Dimethylphenol, 2,4- (2,4-xylenol) GC/MSMS - - - - - - - - - -

< LCL Fluazifop-butyl LC/MSMS - - - - 0.01

0.1 - - < LCL

Dioxathion GC/MSMS - - - - 0.01 0.1 - -

< LCL Flucythrinate GC/MSMS - - - - 0.05

0.1 - - < LCL

Dinotefuran LC/MSMS - - - - 0.01 0.1 - -

< LCL Fluchloralin GC/MSMS - - - - 0.01

0.1 - - < LCL

Diphenylamine GC/MSMS - - - - 0.05 0.1 - -

< LCL Flufenacet LC/MSMS - - - - 0.01

7 - - < LCL

Diphenamid LC/MSMS - - - - 0.01 0.1 - -

< LCL Fludioxonil GC/MSMS 5 5 5

0.1 - - < LCL

Disulfoton sulfone GC/MSMS - - - - - - - - - -

< LCL Flumiclorac-pentyl GC/MSMS - - - - 0.01

0.1 - - < LCL

Disulfoton GC/MSMS - - - - 0.05 0.1 - -

< LCL Flufenoxuron LC/MSMS - - - - 0.01

0.1 - - < LCL

Diuron (Karmex) LC/MSMS 0.1 0.1 0.05 0.1 - -

< LCL Fluopicolide LC/MSMS - - - - 0.01

0.1 - - < LCL

Disulfoton sulfoxide GC/MSMS - - - - - - - - - -

< LCL Fluometuron LC/MSMS - - - - 0.02

0.1 - - < LCL

Dyfonate GC/MSMS - - - - 0.01 0.1 0.01

< LCL Fluoroglycofen-ethyl LC/MSMS - - - - 0.01

5 - - < LCL

Dodemorph LC/MSMS - - - - 0.01 0.1 - -

< LCL Fluopyram GC/MSMS 5 5 5

5 - - < LCL

Emamectin Benzoate LC/MSMS - - - - 0.1 0.1 - -

< LCL Flupyradifurone* LC/MSMS 5 5 0.01

0.1 - - < LCL

Edifenphos LC/MSMS - - - - 0.01 0.1 - -

< LCL Fluoxastrobin LC/MSMS - - - - 0.01

0.1 - - < LCL

Endosulfan II (beta isomer) GC/MSMS - - - - 0.5 0.1 - -

< LCL Flurtamone LC/MSMS - - - - 0.01

0.1 - - < LCL

Endosulfan I (alpha isomer) GC/MSMS - - - - 0.5 0.1 - -

< LCL Fluridone GC/MSMS - - - - 0.01

0.1 - - < LCL

Endrin GC/MSMS - - - - 0.01 0.1 0.05

< LCL Flutolanil GC/MSMS - - - - 0.01

0.1 - - < LCL

Endosulfan sulfato GC/MSMS - - - - 0.5 0.1 - -

< LCL Flusilazole LC/MSMS - - - - 0.01

- - - - < LCL

EPTC GC/MSMS - - - - 0.1 0.1 - -

< LCL Fluvalinate GC/MSMS - - - - - -

0.1 - - < LCL

Epoxiconazole LC/MSMS - - - - 0.01 0.1 - -

< LCL Flutriafol LC/MSMS - - - - 0.01

25 - - < LCL

Etaconazole (Etaconazole I y II) LC/MSMS - - - - - - - - - -

< LCL Folpet GC/MSMS - - - - 0.01

5 - - < LCL

Esfenvalerate + Fenvalerate (**) GC/MSMS 1 1 1 0.1 0.2

< LCL Fluxapyroxad LC/MSMS 5 5 7

- - - - < LCL

Ethiofencarb LC/MSMS - - - - 0.01 0.1 - -

< LCL Formetanate LC/MSMS - - - - - -

0.1 - - < LCL

Ethalfluralin GC/MSMS - - - - 0.01 0.1 - -

< LCL Forchlorfenuron LC/MSMS - - - - 0.1

- - < LCL

Ethirimol LC/MSMS - - - - 0.01 0.1 - -

< LCL Fuberidazole LC/MSMS - - - - 0.01

0.1 - - < LCL

Ethiofencarb-sulfone LC/MSMS - - - - 0.01 0.1 - -

< LCL Fosthiazate LC/MSMS - - - - 0.05

0.02 < LCL

Ethylan GC/MSMS - - - - - - - - - -

< LCL g Chlordan GC/MSMS 0.1 0.1 0.02

0.1 - - < LCL

Ethoprop GC/MSMS - - - - 0.01 0.1 0.02

< LCL Furathiocarb LC/MSMS - - - - 0.01

0.01 < LCL

Etofenprox GC/MSMS 5 5 0.01 0.1 - -

< LCL Heptachlor GC/MSMS 0.05 0.05 0.01

0.1 - - < LCL

Etion GC/MSMS - - - - 0.3 0.1 - -

< LCL Haloxyfop-methyl LC/MSMS - - - - 0.05

- - < LCL

Famoxadone LC/MSMS 10 10 10 10 - -

< LCL Heptenophos LC/MSMS - - - - 0.01

- - - - < LCL

Etoxazole LC/MSMS 1.5 1.5 0.01 1.5 - -

< LCLHeptachlor exo-epoxide (isomer

B)GC/MSMS - - - - - -

0.01

0.1 - - < LCL

Fenamiphos LC/MSMS - - - - 0.02 0.1 0.02

< LCL Hexaconazole LC/MSMS - - - - 0.01

0.1 - - < LCL

Fenamidone GC/MSMS - - - - 0.01 0.1 - -

< LCL Hexachlorobenzene GC/MSMS 0.05 0.05 0.01

0.1 - - < LCL

Fenamiphos Sulfoxide LC/MSMS - - - - - - - - - -

< LCL Hexazinone GC/MSMS - - - - 0.01

0.1 - - < LCL

Fenamiphos Sulfone LC/MSMS - - - - - - - - - -

< LCL Hexaflumuron LC/MSMS - - - - 0.01

LC/MSMS 0.7 0.7 0.01 0.1 - -

< LCL Imazalil LC/MSMS - - - - 0.02

1.5 - - < LCL

Fenarimol LC/MSMS - - - - 1 0.1 - -

< LCL Hexythiazox LC/MSMS 1 1 0.01

0.05 0.01

0.01 0.01

CHNKOR

0.1 - - < LCL< LCL Imazaquin LC/MSMS - - - - 0.05

0.1 - - < LCL

Fenbuconazol LC/MSMS - - - - 0.01 0.1 - -

< LCL Imazapyr LC/MSMS - - - - 0.01

0.1 - - < LCL

Fenazaquin

*Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166-1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it́ s not responsible for the representation of the result for the total

product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.

This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.

Controlled document ISO/IEC 17025:2017

Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]

Authorizes

Lic. Carlos Sepulveda Ibarra IBT. Cesar Arturo Sanchez Espindola Directorate Chromatography Analysts

Page 11: Fecha de reporte: 2019-12-22 Página: Revisión: AR271-TS-48 ...agrolab.fictionsecurity.com/resultados/Files/869A-33D0-2297-474C-8… · ፨ Razón social: Fruits-Giddings SA de CV

B BB BB BB BB BB BB BB BB B

B B

B B

B B

B BB BB BB B

B B

B B

B B

B B

B B

B B

B B

B B

B B

B B

B B

B B

B B

B B

B B

B B

B B

B BB BB BB BB BB BB BB BB B

B B

B B

B B

B B

B B

B B

B BB BB BB BB BB BB BB BB BB B

B B

B B

0.01 0.01

0.05 3

0.01 2

0.01 2

- - - -

- - - -

- - - -

0.01 0.01

0.01 0.01

0.01 0.01

0.01 0.01

0.01 0.01

- - - -

- - 0.01

0.01 0.01

4 1

0.01 0.01

0.01 0.01

0.01 0.5

0.05 5

0.01 0.5

- - - -

0.01 0.05

0.01 0.05

0.01 0.05

0.01 0.01

0.01 0.01

0.01 0.01

0.05 0.01

0.01 0.01

- - - -

- - - -

0.05 0.01

0.01 0.01

0.1 0.2

0.05 0.01

0.01 0.01

- - - -

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

0.02 0.01

- - - -

0.05 0.01

0.01 0.01

0.01 0.5

OXAMYL METABOLITEOXAMYL METABOLITE

0.01 5

0.1 0.01

0.01 0.01

0.01 0.01

- - - -

- - - -

0.01 0.01

0.01 0.01

0.01 0.01

- - - -

0.01 0.01

0.01 1

- - - -

0.01 0.01

0.05 0.01

0.01 0.01

0.01 0.01

- - - -

0.02 0.01

0.02 0.01

0.01 0.01

0.01 0.1

0.02 0.01

0.2 0.01

0.2 0.01

0.2 0.01

0.01 0.01

MALATHION

METABOLITE

MALATHION

METABOLITE

0.02 0.5

0.05 7

0.01 0.01

- - - -

0.01 0.01

4 0.01

0.02 0.01

0.1 0.01

0.01 0.01

0.01 0.01

0.01 0.01

0.01 0.01

0.02 0.01

0.02 0.01

0.01 2

0.1 0.01

- - - -

EU KOR EU KOR

5 1.5

0.05 0.01

- - - -

0.5 0.5

0.01 30

0.01 0.01

- - - -

- - - -

0.1 0.01

- - - -

0.01 0.01

0.01 0.01

0.01 0.01

0.01 0.01

Metobromuron LC/MSMS - - - - 0.01 0.1 - - < LCL

Methylpentachlophenyl Sulfide GC/MSMS - - - - - -

ZIRACUARETIRO ፨SAGARPA Reg.:SD

US JP CA EU

Napropamide

Pesticide residues have been detected within the allowed limits

AnalyteAnalyzed

by

Authorized use

MRL (ppm)

MX JP CA CHN

- -

0.01 0.1 - -

25 - -

0.01 0.1 - -

0.01< LCL Nitrothal-isopropyl

0.1< LCL Nitrapyrin - -

- -

< LCL Norflurazon-Desmethyl

- -

- -

- - < LCL

- -

Phorate-sulfoxide LC/MSMS - - - - 0.05 0.024 0.01

Phosalone LC/MSMS

0.1 - -

Analysis Results

AnalyteAnalyzed

by

Authorized use

MRL (ppm) Obtained amount in

mg/kg (ppm)CA CHN

LC/MSMS - - - - - -

Imidan GC/MSMS - - - - 0.1

Iprodione GC/MSMS 25 25 12

Indoxacarb GC/MSMS - - - -

Imiprothrin GC/MSMS

Irgarol

Iprovalicarb LC/MSMS - - - -

- -

< LCL N-2,4-Dimethylphenyl

Report Date: 2019-12-22 Page: 4 of 7 Revision: AR272-TS-48

P-19-28976FRUITS GIDDINGS SA DE CV ፨ Sample: Zarzamora Lab Reg. No.:፨ Client:

፨ Producer:BERTA LORENA MORENO

RODRIGUEZ፨ Orchard:

US JP MX US

Chromatogram GC: P-19-28976 12-21-2019.D Chromatogram LC:

Obtained amount in

mg/kg (ppm)

P-19-28976 12-21-2019.d MXAgrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

0.1 0.1

LC/MSMS - - - - - - < LCL

- - < LCL

0.1

- -LC/MSMS - - - - - -

- -

Imidacloprid LC/MSMS 2.5 2.5 4 2.5 - -

- - < LCL0.1< LCL

- - - -

LC/MSMS 0.10.1

- - - - - - - - - -

0.010.01 LC/MSMS - - - -0.1 - -

< LCL Neburon

< LCL Nicosulfuron < LCL

< LCLLC/MSMS 0.1 0.1 0.1< LCL Norflurazon- -

- - - - < LCLGC/MSMS - - - - - -

Isocarbophos GC/MSMS 0.1- - - - 0.01 0.1 0.05

0.01 0.01

0.01 0.01

- - - -

0.01 2

Isofenphos LC/MSMS - - - - 0.01 0.1 0.01

< LCL Novaluron* < LCLLC/MSMS - -

< LCLGC/MSMS - - - - 0.01

Isazophos LC/MSMS - - - - 0.01 0.1 0.01

0.1 - - < LCLGC/MSMS - - - -

< LCL O Phenylphenol

- -

0.1

- - 0.01

- - < LCLGC/MSMS - - - - 0.01

< LCL Omethoate

< LCL op Dicofol***

< LCL

Isoprothiolane GC/MSMS - - - - 0.01 0.1 - -

< LCL Ofurace LC/MSMS - - - - - -

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE< LCLLC/MSMS

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

Isoprocarb LC/MSMS - - - - 0.01 0.1 - -

Isoxaflutole LC/MSMS - - - - 0.01 0.1 - - < LCL

GC/MSMS - - - - 3

- - < LCL

Isoproturon LC/MSMS - - - - 0.01 0.1 - -

Lenacil LC/MSMS - - - - 0.3 0.1

Kresoxim-methyl LC/MSMS - - - - 0.01 0.1 - - < LCL

Kelthane*** GC/MSMS - - - - 3 0.1

< LCL

Lufenuron LC/MSMS - - - - 0.01 0.1 - - < LCL

Linuron LC/MSMS - - - - 0.2 0.1

Leptophos GC/MSMS - - - - - - - - - - < LCL

0.01 0.01

0.01 0.3

5 < LCL

Mandipropamid LC/MSMS - - - - 0.01 0.1 - - < LCL

Mancozeb LC/MSMS - - - - 5 0.1

MALATHION

METABOLITE< LCL

Malathion GC/MSMS 8 8 8 8 - - < LCL

Malaoxon LC/MSMSMALATHION

METABOLITE

MALATHION

METABOLITE

MALATHION

METABOLITE

MALATHION

METABOLITE

- - < LCL

Metalaxyl-M (Mefenoxam, R-

enantiomero de metalaxyl)GC/MSMS 0.7 0.7 0.7 0.1 - - < LCL

Mepanipyrim LC/MSMS - - - - 0.01 0.1

- - < LCL

Mecarbam LC/MSMS - - - - 0.01 0.1 - - < LCL

Mebendazole LC/MSMS - - - - - - - -

- - < LCL

Methabenzthiazuron LC/MSMS - - - - 0.01 0.1 - - < LCL

Metconazole LC/MSMS - - - - 0.01 0.1

- - < LCL

Metazachlor LC/MSMS - - - - 0.01 0.1 - - < LCL

Metamitron LC/MSMS - - - - 0.01 0.1

< LCL

Methiocarb sulfone GC/MSMS - - - - 0.05 0.1 - - < LCL

Methiocarb GC/MSMS - - - - 0.05 0.1

0.05 < LCL

Methidathion LC/MSMS - - - - 0.2 0.1 0.05 < LCL

Methamidophos LC/MSMS - - - - 0.01 0.1

Methoprotryne LC/MSMS - - - - - - - - - - < LCL

Methoprene GC/MSMS - - - - 0.01 0.1

- - < LCL

Methomyl LC/MSMS - - - - 1 0.01 0.2 < LCL

Methiocarb sulfoxide GC/MSMS - - - - 0.05 0.1

0.02 0.01

LC/MSMS - - - - 0.01 0.1 - -

- - < LCL

Methoxyfenozide LC/MSMS 6 6 0.01 6 - - < LCL

Methoxychlor GC/MSMS - - - - 7 0.1

- - < LCLMetolachlor LC/MSMS - - - - 0.01 0.1

- - < LCL

Metribuzin GC/MSMS - - - - 0.01 0.1 - - < LCL

Metrafenone LC/MSMS - - - - 0.01 0.1

- -

Metoxuron LC/MSMS - - - - - - - - - - < LCL

Metolcarb LC/MSMS - - - - 0.01 0.1 - - < LCL

Metosulam

MGK-264 GC/MSMS - - - - - - - - - - < LCL

Mexacarbate LC/MSMS - - - - - - - -

- - < LCL

Mevinphos GC/MSMS - - - - 0.01 0.1 - - < LCL

Metsulfuron-methyl LC/MSMS - - - - 0.01 0.1

Monolinuron LC/MSMS - - - - 0.01 0.1 - - < LCL

Monocrotophos LC/MSMS - - - - 0.01 0.1

0.01 < LCL

Molinate LC/MSMS - - - - 0.01 0.1 - - < LCL

Mirex GC/MSMS - - - - 0.01 0.1

0.01 0.01

Myclobutanil GC/MSMS 2 2 1 2 - - < LCL

Monuron LC/MSMS - - - - 0.01 0.1 Prometryn GC/MSMS - -0.01 0.01

1 0.01

0.1 - - < LCL

Ovex GC/MSMS - - - - - - - - - - < LCL

- - < LCL - - 0.01 0.1 - -

0.03 < LCL

- - < LCL

< LCL

- - < LCL

- - < LCL

- -

Oxamyl LC/MSMS - - - - 0.01 0.1 - - < LCL

Oxamyl Oxime LC/MSMS OXAMYL METABOLITEOXAMYL METABOLITEOXAMYL METABOLITEOXAMYL METABOLITE OXAMYL METABOLITE < LCL

Oxadiazon GC/MSMS - - - - 0.01 0.1 - - < LCL

Oxadixyl LC/MSMS - - - - 1 0.1 - - < LCL

Paclobutrazol (Bonzi) LC/MSMS - - - - 0.01 0.1 - - < LCL

Paraoxon LC/MSMS - - - - - - - - - - < LCL

Oxydemeton-methyl LC/MSMS - - - - 0.02 0.1 - - < LCL

Oxyfluorfen GC/MSMS 0.05 0.05 0.01 0.1 - - < LCL

Paraoxon-methyl LC/MSMS - - - - - - - - - - < LCL

Parathion GC/MSMS - - - - 0.5 0.1 0.01 < LCL

Parathion methyl GC/MSMS - - - - 0.2 0.1 0.02

- - 10 0.01 10 - -

- - - - - - - -

< LCL

Penconazol LC/MSMS - - - - 0.2 0.1 - - < LCL

- -

- - - - 0.02 0.1 - -

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

QUINTOCENE

(PENTACHLOR

ONITROBENZE

NE)METABOLIT

E

Phorate

Phorate-sulfone

LC/MSMS

LC/MSMS

GC/MSMS

GC/MSMS

GC/MSMS

GC/MSMS

GC/MSMS

GC/MSMS

LC/MSMS

LC/MSMS

GC/MSMS

GC/MSMS

LC/MSMS

Pencycuron

Pendimethalin

Pentachloroaniline

Pentachloroanisol

Pentachloronitrobenzene

Pentachlorophenol

Penthiopyrad

Permethrin

Phenmedipham

Phenthoate

Phenyl valerate

QUINTOCENE

(PENTACHLOR

ONITROBENZE

NE)METABOLIT

E

QUINTOCENE

(PENTACHLOR

ONITROBENZE

NE)METABOLIT

E

QUINTOCENE

(PENTACHLOR

ONITROBENZE

NE)METABOLIT

E

QUINTOCENE

(PENTACHLOR

ONITROBENZE

NE)METABOLIT

E

- - - - 0.01 0.1 - -

0.1 0.1 0.05 0.1 - -

- - - - 0.01 0.1 - -

0.05 0.01

QUINTOCENE

(PENTACHLOR

ONITROBENZE

NE)METABOLIT

E

QUINTOCENE

(PENTACHLOR

ONITROBENZE

NE)METABOLIT

E

- - - -

0.02 0.01

0.01 0.01

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

- - - - - - - - - -

- -

- - - - 1 0.1 1

- - 0.05 0.024 0.01

- - - - 0.01 0.1 - -

- - - - 0.01 0.1 - -

Phoxim LC/MSMS - - - - 0.02 0.1 0.05 < LCL

Picolinafen LC/MSMS - - - - 0.01 0.1 - - < LCL

- - - - 0.05 0.024 0.01

< LCL

< LCL

- -

LC/MSMS - - - - 0.01 0.1 0.05 < LCLPhosphamidon

Piperonyl Butoxide LC/MSMS 8 8 8 8 - - < LCL

Piperophos LC/MSMS - - - - 0.01 0.1 - - < LCL

Picoxystrobin LC/MSMS - - - - 0.01 0.1 - - < LCL

Piperalin LC/MSMS - - - - - - - - - - < LCL

Pirimiphos-methyl LC/MSMS - - - - 0.1 0.1 - - < LCL

Primisulfuron-methyl LC/MSMS - - - - 0.01 0.1 - - < LCL

Pirimicarb LC/MSMS - - - - 0.5 0.1 1 < LCL

Pirimiphos-ethyl LC/MSMS - - - - 0.01 0.1 - - < LCL

- - 0.01 0.1 - - < LCL

Profluoralin GC/MSMS - - - - - - - - - - < LCL

Prochloraz LC/MSMS - - - - 0.05 0.1 - - < LCL

Procymidone GC/MSMS - - - - 0.01 0.1 - - < LCL

CHNKOR

< LCL

Pronamide LC/MSMS - - - - - - - - - - < LCL

Promecarb GC/MSMS - - - - - - - - - - < LCL

Prometon GC/MSMS - - - - - - - - - - < LCL

- - - -

Profenofos GC/MSMS - -

* Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166-1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued res ult only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it ´s not responsible for the representation of the result for the total

product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.

This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amen dments.

Controlled document ISO/IEC 17025:2017

Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]

Authorizes

Lic. Carlos Sepulveda Ibarra IBT. Cesar Arturo Sanchez Espindola Directorate Chromatography Analysts

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B BB BB BB BB BB BB BB BB BB BB B

B B

B BB BB BB BB BB BB BB B

B B

B B

B B

B B

B BB B

B B

B B

B B

B B

B B

B B

B B

B VB VB VB VB VB VB VB VB V

B V

B

B

B

B

B

BBB

B

B

B

B

B

BBBB0.01 1 - - < LCLThiamethoxam LC/MSMS 0.35 0.35 0.5 0.5

1 < LCLThiacloprid LC/MSMS - - - - 5 0.1 1 0.7

0.01 0.01 - - < LCLThiabendazole LC/MSMS - - - - 3 0.1

- - < LCLTetramethrin LC/MSMS - - - - 0.01 0.1 0.01 0.01

CAPTAN

METABOLITE

CAPTAN

METABOLITE

CAPTAN

METABOLITE< LCL

Tetrahydrophthalimide, cis-1,2,3,6-

(THPI)GC/MSMS

CAPTAN

METABOLITE

CAPTAN

METABOLITE

CAPTAN

METABOLITE

CAPTAN

METABOLITE

- - < LCLTetradifon GC/MSMS - - - - 1 0.1 0.01 0.01

0.01 0.01 - - < LCLTetrachlorvinphos, E-isomer GC/MSMS - - - - 0.01 0.1

- - < LCLTerrazole GC/MSMS - - - - - - - - - - - -

0.01 0.01 - - < LCLTerbutryn GC/MSMS - - - - 0.01 0.1

- - < LCLTerbuthylazine-desethyl LC/MSMS - - - - - - - - - - - -

0.05 0.01 - - < LCLTerbuthylazine GC/MSMS - - - - 0.01 0.1

- - < LCLTerbumeton LC/MSMS - - - - - - - - - - - -

0.01 0.01 - - < LCLTerbacil GC/MSMS 0.2 0.2 0.1 0.1

- - < LCLTeflubenzuron LC/MSMS - - - - 0.01 0.1 0.01 2

0.01 0.01 - - < LCLTecnazene GC/MSMS - - - - 0.05 0.1

- - < LCLTebuthiuron LC/MSMS - - - - 0.01 0.1 0.01 0.01

0.01 0.01 - - < LCLTebutam LC/MSMS - - - - 0.01 0.1

- - < LCLTebufenpyrad GC/MSMS - - - - 0.01 0.1 0.05 0.5

0.05 2 - - < LCLTebufenozide LC/MSMS 3 3 3 0.1

- - < LCLTebuconazole GC/MSMS - - - - 0.01 0.1 0.5 0.5

0.02 0.01 - - < LCLSumithrin GC/MSMS - - - - 0.01 0.1

- - < LCLSulfoxaflor LC/MSMS - - 1.5 0.01 0.1 0.01 0.5

0.01 0.01 0.01 < LCLSulfotep LC/MSMS - - - - 0.01 0.1

- - < LCLSulfosulfuron LC/MSMS - - - - 0.01 0.1 0.01 0.01

0.01 0.01 - - < LCLSulfentrazone LC/MSMS 0.15 0.15 0.05 0.15

- - < LCLSpiroxamine LC/MSMS - - - - 0.01 0.1 0.01 0.01

0.1 3 - - < LCLSpirotetramat LC/MSMS - - - - 0.01 2

5 0.1 0.01 0.01 - - < LCL- - < LCL Vinclozolin GC/MSMS - - - -

- - < LCL

Spiromesifen LC/MSMS - - - - 0.01 5 0.02 2

- - - - 0.01 0.1 0.01 0.010.02 1 - - < LCL Vamidothion LC/MSMSSpirodiclofen LC/MSMS - - - - 0.01 0.1

0.01 0.1 0.01 0.01 - - < LCL1 < LCL Uniconazole GC/MSMS - - - -

- - < LCL

Spinosad A LC/MSMS 1 1 1 0.5 1.5 0.5

- - - - - - - - - - - -1 0.7 - - < LCL Trimidal LC/MSMSSpinetoram J LC/MSMS 0.8 0.8 0.7 0.5

0.01 0.1 0.01 0.5 - - < LCL- - < LCL Triforine LC/MSMS - - - -

- - < LCL

S-Metolachlor LC/MSMS 0.1 0.1 0.01 0.1 0.05 0.01

- - - - 0.01 0.1 0.01 0.010.01 0.01 - - < LCL Triflusulfuron-methyl LC/MSMSSimetryn LC/MSMS - - - - 0.01 0.1

0.05 0.1 0.01 0.01 - - < LCL- - < LCL Trifluralin GC/MSMS - - - -

- - < LCL

Simazine GC/MSMS 0.2 0.2 0.2 0.1 0.01 0.01

- - - - 0.02 0.1 0.01 0.010.1 1 - - < LCL Triflumuron LC/MSMSSethoxydim* LC/MSMS 5 5 1 5

0.01 0.1 0.02 2 - - < LCL- - < LCL Triflumizole LC/MSMS - - - -

- - < LCL

Sebuthylazine GC/MSMS - - - - - - - - - - - -

- - - - 0.01 0.1 3 10.01 0.01 - - < LCL Trifloxystrobin LC/MSMSRotenone LC/MSMS - - - - 0.01 0.1

- - - - - - - - - - < LCL- - < LCL Trietazine LC/MSMS - - - -

- - < LCL

Rimsulfuron LC/MSMS 0.01 0.01 0.01 0.01 0.01 0.01

- - - - 0.01 0.1 0.01 0.010.05 0.01 - - < LCL Tricyclazole GC/MSMSQuizalofop-ethyl LC/MSMS - - - - 0.05 0.1

- - - - - - - - - - < LCL- - < LCL Triclocarban LC/MSMS - - - -

- - < LCL

Quinoxyfen LC/MSMS - - - - 0.01 0.1 0.02 0.01

- - - - - - - - - - - -0.01 0.01 - - < LCL Trichloronate GC/MSMSQuinalphos LC/MSMS - - - - 0.02 0.1

0.5 0.1 0.01 0.01 0.2 < LCL- - < LCL Trichlorfon LC/MSMS - - - -

- - < LCL

Pyriproxyfen GC/MSMS 1 1 0.01 0.1 0.05 0.01

- - - - - - - - - - - -15 15 - - < LCL Tributyl phosphate GC/MSMSPyrimethanil LC/MSMS 15 15 10 15

0.01 0.1 0.01 0.01 - - < LCL- - < LCL Tribenuron-methyl LC/MSMS - - - -

- - < LCL

Pyridaphenthion GC/MSMS - - - - 0.01 0.1 0.01 0.01

- - - - 0.01 0.1 0.01 0.010.01 1 - - < LCL Triazophos GC/MSMSPyridalyl GC/MSMS - - - - 0.01 0.1

0.01 0.1 0.05 0.01 - - < LCL- - < LCL Triasulfuron LC/MSMS - - - -

- - < LCL

Pyridaben LC/MSMS - - - - 0.01 0.1 0.01 0.01

- - - - - - - - - - - -0.01 0.01 - - < LCL Triallate GC/MSMSPyrazophos LC/MSMS - - - - 0.01 0.1

0.5 0.1 0.01 0.01 - - < LCL- - < LCL Triadimenol GC/MSMS - - - -

- - < LCL

Pyraclostrobin LC/MSMS 4 4 3 3.5 3 3

- - - - 0.1 0.1 0.01 0.053 0.01 - - < LCL Triadimefon GC/MSMSPymetrozine LC/MSMS - - - - 0.01 0.1

5 0.1 0.02 0.01 5 < LCL- - < LCL Tolyfluanid GC/MSMS - - - -

- - < LCL

Prosulfuron LC/MSMS - - - - 0.01 0.1 0.01 0.01

- - - - 0.1 0.1 0.01 0.010.01 0.01 - - < LCL Tolchlofos methyl GC/MSMSProsulfocarb LC/MSMS - - - - 0.01 0.1

- - - - - - - - - - < LCL- - < LCL Tokution GC/MSMS - - - -

- - < LCL

Propyzamide LC/MSMS 0.05 0.05 0.01 0.1 0.01 0.01

- - - - 3 6 0.1 20.05 0.01 - - < LCL Thiophanate-methyl LC/MSMSPropoxur LC/MSMS - - - - 1 0.1

- - - - - - - - - - < LCL- - < LCL Thionazin LC/MSMS - - - -

- - < LCL

Propiconazole GC/MSMS 1 1 0.05 1 0.01 0.01

- - - - - - - - - - - -0.01 0.01 - - < LCL Thiofanox Sulfoxide LC/MSMSPropetamphos LC/MSMS - - - - 0.01 0.1

1 0.1 0.01 0.01 - - < LCL- - < LCL Thiodicarb LC/MSMS - - - -

< LCL

- - < LCL

Propazin GC/MSMS - - - - 0.01 0.1 0.01 0.01

- - - - 3 0.1 0.01 10.01 0.01 - - < LCL Thiocyclam hydrogen oxalate GC/MSMSPropargite (Omite) LC/MSMS - - - - 0.01 0.1

0.01

0.01 0.1 0.01 0.01 - - < LCL- - < LCL Thiobencarb LC/MSMS - - - -

- - < LCL

Propanil LC/MSMS - - - - 0.1 0.1 0.01 0.01

- - - - 0.01 0.1 0.01 0.010.01 0.01 - -

Obtained amount in

mg/kg (ppm)Analyte

Analyzed

by

Authorized use

MRL (ppm) Obtained amount in

mg/kg (ppm)

Thifensulfuron-methyl LC/MSMSPropamocarb LC/MSMS - - - - 0.01 0.1

0.01 0.1 0.01 0.01 - - < LCL- - < LCL Thidiazuron LC/MSMS - - - -Propachlor LC/MSMS - - - - 0.01 0.1 0.02

KOR CHN

፨ Producer:BERTA LORENA MORENO

RODRIGUEZ፨ Orchard: ZIRACUARETIRO ፨SAGARPA Reg.:SD

፨ Client: FRUITS GIDDINGS SA DE CV ፨ Sample: Zarzamora Lab Reg. No.: P-19-28976

CHN MX US JP CA EUMX US JP CA EU KOR

Analysis ResultsPesticide residues have been detected within the allowed limits

AnalyteAnalyzed

by

Authorized use

MRL (ppm)

Report Date: 2019-12-22 Page: 5 of 7 Revision: AR272-TS-48

JP CA EU KOR CHNAgrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

Chromatogram GC: P-19-28976 12-21-2019.D Chromatogram LC: P-19-28976 12-21-2019.d MX US

* Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166-1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it́ s not responsible for the representation of the result for the total

product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.

This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.

Controlled document ISO/IEC 17025:2017

Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]

Authorizes

Lic. Carlos Sepulveda Ibarra IBT. Cesar Arturo Sanchez Espindola Directorate Chromatography Analysts

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0.005

0.010

Trimidal

Uniconazole

Vamidothion

Vinclozolin

Trifloxystrobin 0.005

g Chlordan 0.010

Haloxyfop-methyl 0.005

Heptachlor 0.010

Forchlorfenuron 0.005

Formetanate 0.005Fosthiazate 0.005Fuberidazole 0.005Furathiocarb 0.005

Flutolanil 0.010

Flutriafol 0.005

Fluvalinate 0.010

Fluxapyroxad 0.005

Folpet 0.010

Fluoxastrobin 0.005

Flupyradifurone* 0.005

Fluridone 0.010

Flurtamone 0.005

Flusilazole 0.005

Flumiclorac-pentyl 0.010

Fluometuron 0.005

Fluopicolide 0.005

Fluopyram 0.010

Fluoroglycofen-ethyl 0.005

Fluchloralin 0.010

Flucythrinate 0.010

Fludioxonil 0.010

Flufenacet 0.005

Flufenoxuron 0.005

Flamprop-isopropyl 0.010

Flazasulfuron 0.005

Flonicamid 0.010

Fluazifop-butyl 0.005

Flubendiamide 0.010

Fensulfothion 0.010

Fenthion 0.010

Fenuron 0.005

Fipronil 0.020

Flamprop methyl 0.010

Fenpropathrin 0.010

Fenpropidin 0.005

Fenpropimorph 0.005

Fenpyroximate 0.005

Fenson 0.020

Analyte LCL (ppm)

Fenitrothion 0.020

Fenoxaprop-ethyl 0.005

Fenoxycarb 0.005

Triclocarban 0.010

Tricyclazole 0.010

Methabenzthiazuron 0.005 Pentachloronitrobenzene 0.010 Spinetoram J 0.005

0.005 Parathion methyl 0.010 Rotenone 0.005

Mandipropamid 0.005 Paraoxon-methyl 0.005 Quizalofop-ethyl 0.005

Trietazine 0.005

Methidathion 0.005 Penthiopyrad 0.010 Spirodiclofen 0.005

Methamidophos 0.005 Pentachlorophenol 0.010 Spinosad A 0.005

Triflumizole 0.005

Triflumuron 0.010

Trifluralin 0.010

Triflusulfuron-methyl 0.005

Triforine 0.010

0.005

0.010

Methiocarb sulfone 0.010 Phenmedipham 0.005 Spirotetramat 0.005

Methiocarb 0.020 Permethrin 0.010 Spiromesifen 0.005

Methomyl 0.005 Phenyl valerate 0.010 Sulfentrazone 0.005

Methiocarb sulfoxide 0.020 Phenthoate 0.005 Spiroxamine 0.005

Methoprotryne 0.005 Phorate-sulfone 0.005 Sulfotep 0.005

Methoprene 0.010 Phorate 0.010 Sulfosulfuron 0.005

Methoxyfenozide 0.005 Phosalone 0.010 Sumithrin 0.020

Methoxychlor 0.010 Phorate-sulfoxide 0.005 Sulfoxaflor 0.005

0.010 Tebufenozide 0.005

Methylpentachlophenyl Sulfide 0.010 Phosphamidon 0.005 Tebuconazole 0.010

Metolcarb 0.010 Picoxystrobin 0.005 Tebutam 0.005

Metolachlor 0.005 Picolinafen 0.005 Tebufenpyrad 0.010

Trichloronate 0.010

Trichlorfon 0.005

Tributyl phosphate 0.010

Tribenuron-methyl 0.005

Report Date 2019-12-22 Page 6 of 7 Revision: AR272-TS-48

Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

Lowest Calibration Level per analyteAnalyte LCL (ppm) Analyte LCL (ppm) Analyte LCL (ppm) Analyte LCL (ppm)

Dimethenamid 0.005

2, 4-D Methyl ester 0.010 Bromophos methyl 0.010 Coumaphos 0.010 Dimethoate 0.0101-Naphthol 0.010 Bromacil 0.010 Clothianidin 0.005

Dimethomorph 0.005

2,6 Dichlorobenzonitrilo 0.010 Bromuconazole* 0.010 Cyanazine 0.005 Dimethylphenol, 2,4- (2,4-xylenol) 0.010

2,3 dihydro-2,2dimethylbenzofuran

7-ol0.020 Bromopropylate 0.010 Crimidine 0.005

Diniconazole 0.005

3,4 Dichloroaniline 0.010 Buprofezin 0.010 Cyazofamid 0.005 Dinotefuran 0.0052,6-Dichlorobenzamide 0.005 Bupirimate 0.005 Cyantraniliprole 0.005

Dioxathion 0.010

Abamectin 0.005 Butocarboxim* 0.010 Cyflufenamid 0.010 Diphenamid 0.0053-Hydroxy carbofuran 0.005 Butachlor 0.010 Cycloate 0.005

Diphenylamine 0.010

Acetamiprid 0.005 Buturon 0.005 Cyfluthrin 0.010 Disulfoton 0.010Acephate 0.005 Butocarboxim-sulfoxide 0.005 Cyflumetofen 0.005

Disulfoton sulfone 0.010

Aclonifen 0.010 Cadusafos 0.010 Cymoxanil 0.005 Disulfoton sulfoxide 0.010

Acetochlor 0.005 Butylate 0.020Cyhalothrin (Isomero Lambda y

gamma)**0.010

Diuron (Karmex) 0.005

Alachlor 0.005 Carbaryl 0.010 Cyproconazole 0.005 Dodemorph 0.005

Acrinathrin 0.020 Captan 0.010Cypermethrin a (Zeta-

Cypermethrin)**0.010

Dyfonate 0.010

Aldicarb sulfone 0.005 Carbetamide 0.005 Cyromazine 0.005 Edifenphos 0.005Aldicarb 0.005 Carbendazim 0.005 Cyprodinil 0.010

Emamectin Benzoate 0.005

Aldrin 0.010 Carboxin 0.005 DDD-p,p 0.010 Endosulfan I (alpha isomer) 0.010Aldicarb-sulfoxide (Aldoxicarb) 0.005 Carbofuran 0.010 DDD-o,p 0.010

Endosulfan II (beta isomer) 0.010

Ametryn 0.010 Chinometionate 0.010 DDE-p,p 0.010 Endosulfan sulfato 0.010Ametoctradin 0.005 Carfentrazone ethyl 0.005 DDE-o,p 0.010

Endrin 0.010

Aminocarb 0.005 Chlorbromuron 0.005 DDT-p,p 0.010 Epoxiconazole 0.005Amicarbazone 0.005 Chlorantraniliprole 0.005 DDT-o,p 0.010

EPTC 0.010

Atrazine-2-hydroxy 0.005 Chlordimeform 0.010 Deltamethrin 0.010 Esfenvalerate + Fenvalerate (**) 0.010Atrazine 0.010 Chlordane- a 0.010 DEET (Diethyl-m-toluamide, N,N-) 0.010

Etaconazole (Etaconazole I y II) 0.010

Azinphos-ethyl 0.005 Chlorfenvinphos 0.005 Demeton S 0.010 Ethalfluralin 0.010Azamethiphos 0.005 Chlorfenapyr 0.010 Demeton O 0.010

Ethiofencarb 0.005

Azoxystrobin 0.010 Chloridazon (Pyrazon) 0.005 Desmedipham 0.005 Ethiofencarb-sulfone 0.005Azinphos-Methyl 0.005 Chlorfluazuron 0.005 Demeton-s-methyl-sulfone 0.005

Ethirimol 0.005

Benalaxyl 0.010 Chlormequat 0.005 Dialifos 0.005 Ethoprop 0.010Baycarb 0.005 Chlorimuron-ethyl 0.005 Desmetryn 0.010

Ethylan 0.010

Benfluralin 0.010 Chloroneb 0.010 Dichlofluanid 0.010 Etion 0.010Bendiocarb 0.005 Chlorobenzilate 0.010 Diazinon 0.010

Etofenprox 0.010

Bensulide 0.005 Chlorothalonil 0.010 Dichlorvos 0.010 Etoxazole 0.005Bensulfuron-methyl 0.005 Chloropropylate 0.010 Dichloran 0.010

Famoxadone 0.010

Benzoximate 0.005 Chloroxuron 0.005 Diclofop methyl 0.020 Fenamidone 0.010Benthiavalicarb-isopropyl 0.005 Chlorotoluron 0.005 Diclobutrazol* 0.010

Fenamiphos 0.005

BHC lindane beta 0.010 Dieldrin 0.010 Fenamiphos Sulfone 0.005BHC lindane alpha 0.010 Chlorpropham 0.010 Dicrotophos 0.005

Fenamiphos Sulfoxide 0.005Chlorpyrifos 0.010

BHC lindane gamma 0.010 Difenoconazole 0.005 Fenarimol 0.005BHC lindane delta 0.010 Diethofencarb 0.005Chlorpyrifos methyl 0.010

Chlorsulfuron 0.005Fenazaquin 0.005

Bifenox 0.020 Chlorthiophos 0.020 Diflubenzuron* 0.005 Fenbuconazol 0.005Bifenazate 0.005 Chlortal dimethyl** 0.010 Difenoxuron 0.005

Fenbutatin oxide* 0.010Bitertanol 0.005 Clofentezine 0.005 Dimefuron 0.005 Fenchlorphos 0.010Bifenthrin 0.010 Clodinafop-propargyl 0.005 Diflufenican 0.005

Fenfuram 0.005

Boscalid 0.005 Cloquintocet-mexyl 0.005 Dimethachlor 0.005 Fenhexamid 0.005

Bolstar 0.010 Clomazone 0.005 Dimepax 0.010

Analyte LCL (ppm)

Heptachlor exo-epoxide (isomer B) 0.020 Metribuzin 0.010 Pirimicarb 0.005 Terbacil 0.010

Analyte LCL (ppm) Analyte LCL (ppm) Analyte LCL (ppm)

Terbumeton 0.005

Hexachlorobenzene 0.010 Mevinphos 0.010 Pirimiphos-methyl 0.005 Terbuthylazine 0.010

Heptenophos 0.005 Metsulfuron-methyl 0.005 Pirimiphos-ethyl 0.005

Terbuthylazine-desethyl 0.005

Hexaflumuron 0.005 MGK-264 0.010 Prochloraz 0.005 Terbutryn 0.010

Hexaconazole 0.005 Mexacarbate 0.005 Primisulfuron-methyl 0.005

Terrazole 0.010

Hexythiazox 0.005 Molinate 0.005 Profenofos 0.010 Tetrachlorvinphos, E-isomer 0.010

Hexazinone 0.010 Mirex 0.010 Procymidone 0.010

Tetradifon 0.010

Imazapyr 0.005 Monolinuron 0.005 Promecarb 0.010Tetrahydrophthalimide, cis-1,2,3,6-

(THPI)0.010

Imazalil 0.005 Monocrotophos 0.005 Profluoralin 0.020

Tetramethrin 0.005

Imidacloprid 0.005 Myclobutanil 0.010 Prometryn 0.010 Thiabendazole 0.005

Imazaquin 0.005 Monuron 0.005 Prometon 0.010

Thiobencarb 0.010

Thiacloprid 0.005

Imiprothrin 0.020 Napropamide 0.005 Propachlor 0.005 Thiamethoxam 0.005

Imidan 0.010N-2,4-Dimethylphenyl formamide

(2,4-DMPF)0.010 Pronamide 0.005

Thidiazuron 0.005

Iprodione 0.010 Nicosulfuron 0.005 Propanil 0.005 Thifensulfuron-methyl 0.005

Indoxacarb 0.010 Neburon 0.005 Propamocarb 0.005

Irgarol 0.005 Nitrothal-isopropyl 0.010 Propazin 0.010Iprovalicarb 0.005 Nitrapyrin 0.010 Propargite (Omite) 0.005

0.005

0.010

Isoprocarb 0.005 O Phenylphenol 0.010 Propyzamide 0.005

Isofenphos 0.005 Novaluron* 0.010 Propoxur 0.005

Isocarbophos 0.010 Norflurazon-Desmethyl 0.010

Isazophos 0.010 Norflurazon 0.005 Propetamphos

Propiconazole

Isoproturon 0.005 Omethoate 0.005 Prosulfuron 0.005

Isoprothiolane 0.010 Ofurace 0.005 Prosulfocarb 0.005

Kelthane*** 0.010 Ovex 0.010 Pyraclostrobin 0.005

Isoxaflutole 0.010 op Dicofol*** 0.010 Pymetrozine 0.005

Lenacil 0.005 Oxadixyl 0.005 Pyridaben 0.005

Kresoxim-methyl 0.005 Oxadiazon 0.010 Pyrazophos 0.005

Linuron 0.005 Oxamyl Oxime 0.005 Pyridaphenthion 0.010

Leptophos 0.010 Oxamyl 0.005 Pyridalyl 0.010

Malaoxon 0.005 Oxyfluorfen 0.010 Pyriproxyfen 0.010

Lufenuron 0.005 Oxydemeton-methyl 0.005 Pyrimethanil 0.005

0.005 Quinoxyfen 0.005

Malathion 0.010 Paclobutrazol (Bonzi) 0.005 Quinalphos 0.005

Metrafenone 0.005 Piperophos 0.005 Teflubenzuron 0.010

Metconazole 0.005 Pentachloroanisol 0.010 S-Metolachlor 0.005

Metoxuron 0.005 Piperonyl Butoxide 0.005 Tecnazene 0.010

Metosulam 0.005

Metobromuron 0.010 Phoxim

Piperalin 0.005 Tebuthiuron 0.005

0.010

0.010

0.005

0.010

Thiocyclam hydrogen oxalate

Thiodicarb

Thiofanox Sulfoxide

Thionazin

Metazachlor 0.005 Pentachloroaniline 0.010 Simetryn 0.005

0.010

Metalaxyl-M (Mefenoxam, R-

enantiomero de metalaxyl)0.010 Pencycuron 0.005 Sethoxydim* 0.010

Tolyfluanid

Triadimefon

Metamitron

0.010

0.005

0.005

0.005

0.005

0.010

0.010

0.010

0.010

Thiophanate-methyl

Tokution

Tolchlofos methyl

0.010

Mepanipyrim 0.010

Triadimenol

Triallate

Triasulfuron

Triazophos

0.005 Pendimethalin 0.005

Mebendazole 0.005 Parathion 0.010 Rimsulfuron

Penconazol 0.005 Sebuthylazine

Simazine

0.005

Mecarbam

Mancozeb 0.005 Paraoxon

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued res ult only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it ´s not responsible for the representation of the result for

the total product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.

This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amen dments.

Controlled document ISO/IEC 17025:2017

Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]

ppm = Parts per million = mg/kg Uncertainty = 50 % according to "Method validation and quality control procedures for pesticide residues analysis in food and feed". No. de Documento SANCO/10684/2009. Punto 91

Page 14: Fecha de reporte: 2019-12-22 Página: Revisión: AR271-TS-48 ...agrolab.fictionsecurity.com/resultados/Files/869A-33D0-2297-474C-8… · ፨ Razón social: Fruits-Giddings SA de CV

Data corresponding to page 2, page 3, page 4 and page 5

Report Date: 2019-12-22 Page: 7 of 7 Revision AR272-TS-48

End of Report

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Additional and complementary information

General Information

1. The customer has five calendar days of issuance of the results**** in order to make any comment or complaint about it, because if not done within this time period will be considered this report

has been accepted.

2. Samples may be disposed within 5 days after the issue of results**** only samples for microbiological analysis shall be discarded 24 hours after being received

3. The information recorded in this "Report test results" is treated with strict adherence to privacy notice Análisis Técnicos S.A. de C.V complying with Articles third transient, 16 and 17 of Law

Protection Federation Personal Data Held by Private Parties, in order to regulate their treatment legitimate, controlled and reported, in order to ensure privacy and the right to self-determination

informative individuals.

4.Análisis Técnicos S.A. de C.V not have the authority, or the right to deny, accept or approve cuts or harvests.

5. Análisis Técnicos S.A. de C.V. is not accredited in sampling.

6. MRLs of the countries are a reference data, requesting check the official sites of each country and that can be changed or modified.

7. The result represents the sample that was received on the premises of Análisis Técnicos S.A. de C.V , which is not responsible for the representation of the result for the total product

8. This form of interpretation is protected and registered with the Instituto Nacional del Derecho de Autor (INDAUTOR), likewise, logos and Agrolab name and its subsidiaries are registered with

the Instituto Mexicano de la Propiedad Intelectual (IMPI). Reproduction is prohibited in whole or in part, for any purpose other than the interpretation of results, without permission.

9. This report is not valid if you have scratches, erasures or amendments.

10. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.

11. Análisis Técnicos S.A. de C.V. It is not responsible for updating the MRL's because they are considered as a piece of information. It is your responsibility to review the report LMR official sites

for each country since the information can be changed or modified.

12. The detection of the pesticide residue above the quantification limit is reported as ppm (mg / kg), below the limit of quantification reported as <LCL ppm (mg / kg) and below the LD is

considered not detected.

13.The decision rule does not include uncertainty.

14.Sample received in conditions for analysis.

፨ Information provided by the client through the AR6-AC analysis request

**** The issuance of the results includes the final report in PDF format. Delivering results to the client, is subject to confirmation of payment.

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References

International Maximum Residue Level Database

http://www.mrldatabase.com/

EU Pesticides Database

http://ec.europa.eu/sanco_pesticides/public/index.cfm

Electronic Code of Federal Regulation

http://ecfr.gpoaccess.gov/cgi/t/text/text-idx?

Health Canada

http://pr-rp.hc-sc.gc.ca/mrl-lrm/index-eng.php

Normas Alimentarias FAO/OMS

http://www.codexalimentarius.net/pestres/data/pesticides/search.html

Positive List System for Agricultural Chemical Residues in Foods (Japón)

http://m5.ws001.squarestart.ne.jp/foundation/search.html

1. The laboratory Análisis Técnicos S.A. de C.V. is accredited before EMA, in the test of determination of residues of pesticides in fruits, vegetables, agricultural food and seeds (incorporating

QuEChERS extraction), by GASS CHROMATOGRAPHY / MASS / MASS to the ISO / IEC 17025:2017.

2. The laboratory Análisis Técnicos S.A. de C.V. is accredited before EMA, in the test of determination of residues of pesticides in fruits, vegetables, agricultural food and seeds (incorporating

QuEChERS extraction), by LIQUID CHROMATOGRAPHY / MASS / MASS to the ISO / IEC 17025:2017.

3. * = Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized.

4.Authorized use of the pesticide in the relevant country code specified in ISO 3166-1 alpha-2. RML for each country are indicated in the same results table.

5. If no pesticide was detected a green band is shown. If a pesticide was detected within the allowed limits a yellow band is shown. If a pesticide was detected outside of the allowed limits a red

band is shown. If a forbidden pesticide was detected a red band is shown.

6. The colored bands are visual aids based on MRLs of each country and are not a result.The color bands of each molecule are visual support based on the MRLs of each country and do not

represent a result.

7. ** The MRL of Isomero Lambda for the molecule Cyhalothrin (Isomero Gamma and Lambda) is taken, for Cypermethrin a (Zeta-Cypermethrin) the MRL for Zeta-Cypermethrin is taken and for

the MRL for Esfenvalerate + Fenvalerate, the one for Esfenvalerate is taken. The MRL of the synonym DCPA is taken for the Chlortal dimethyl molecule.

8. 2 =For Canada the MRL of 0.1 ppm default is considered according to the point 5.2.1.4.2 Food and Drug Regulations of the Canada Food Inspection Agency

http://www.inspection.gc.ca/food/meat-and-poultry-products/manual-of-procedures/chapter-5/eng/1395150894222/1395150895519?chap=2.

9.The laboratory Análisis Técnicos S.A. de C.V. is accredited to A2LA in the Test for the determination of pesticide residues in fruits, legumes, agricultural foods and seeds (incorporating

QuEChERS extraction), by GASS / MASS / MASS chromatography before the AOAC 2007.01 Reference Method.

10. The laboratory Análisis Técnicos S.A. de C.V. is accredited to the A2LA, in the Test for the determination of pesticide residues in fruits, legumes, agricultural foods and seeds (incorporating

QuEChERS extraction), by LIQUID / MASS / MASS chromatography before the AOAC Reference Method 2007.01.

***Dicofol MRL is the sum of Kelthane (Dicofol) and op Dicofol

Information corresponding to page 5 and 6

1. In the corresponding table it´s represented the lower calibration poing (LCL).

2.The correspondig table is NOT A RESULT. It represents quality information data.

3. Uncertainty = 50 % according to "Method validation and quality control procedures for pesticide residues analysis in food and feed". No. de Documento SANCO/10684/2009. point 91

Glosario

GC/MSMS = Gass/Mass/Mass AGILENT 225/MS, 240/MS

LC/MSMS = Liquid/Mass/Mass QQQ (AGILENT 6460)

LCL = Lowest Calibration Level

MRL = Maximum Resuide Limits

ppm = Parts per million = mg/Kg

SD = No Data

Traces = < 0.010 ppm.

MX= Mexico

US= United States

JP= Japan

CA= Canada

EU= European Union

KOR= Korea

CHN= China

Last update date of MRL :2019/12/16

Maximum Residue Limits (MRLs) for Blackberry listed in The Official Catalog of Mexico

Pesticide 2004.

Maximum Residue Limits (MRLs) for Blackberry indicated in Environmental Protection

Agency (EPA) United States.

Maximum Residue Limits (MRLs) for Blackberry indicated in Electronic Code of Federal

Regulations (e-CFR TM) United States.

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A.

de C.V, therefore it´s not responsible for the representation of the result for the total product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.

This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.

Controlled document ISO/IEC 17025:2017

Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]