43
Era WEST COAST TeCHNlCAL S6RV1CG INC. INDUSTRIAL CATEGORY f SAMPLE ID 30F-1 LAB ID 22049V1 DATE INJECTED 8/28/81 STD ID BFB52 VOA176 CONC. FACTOR ———— - Volaules 2V iqj.ijIMii''""""'""" 3V acrylonitrile 4V benzene 6V carbon tetrachloride 7V chlorobenzene 10V l^rfr^iCiyrt^-iiftoiiiiAra 11 V 1,1 , i-trichloroethane 13V 1-dichloroethane 14V 1,1, 2-trichloroethane 15V 1. 1,2,2-tetrachloroethane 16V chloroethane j D j t ' J L Y Y \ S ) IftXfiXlXssiy flftj\JtvW\lX)X /^JwwwuA X XX) 19V 2-chloroethylvinyl ether 23V mtomrfrinTTif 29V 1 , 1-dichloroethylene 30V 1 , 2-trans-dichloroethyiene 32V 1 , 2-dichloropropane 33V 1 , 3-dichloropropylene 38V ethylbenzene 44V fti^^it'^'UgffMab^ 45V methyl chloride 46V methyl bromide 47V bromoform 48V dichlorobromome thane 49V trichlorofluoromethane 50V dichlorodifluoromethane 51V chlorodibromomethane 85V tetrachloroethylene 86V toluene 87V trichloroethylene 88V vinyl chloride ug/l 26 ND NO ND ND 19 ND ND ND ND ND XXXXXX ND 32 ND * ND NO NO 19 ND . NO _.ND. ND NO HP __.. - ND * ND * ^ f|D. ** SAMPLE ID____ LAB ID______ DATE EXTRACTED^ DATE INJECTED^ STD ID CONC. FACTOR Pesticides 30M TRACE #4423 8/28/81 8/31/81 JRACE_*4422 100 89P aldrin 9QP._._ dleldrin__ 91P chlordane 92P ' -DOT 93P 4.4'-DP£ ._____ 94P_4.4'-DPD_______ 95P alpha-endosulfan 96P beta-endosulfan 97P endosulfan sulfate 9gP _endrin_________ 99P_ endrin aldehyde lOQP _heptachlor______ IQjP_ heptachlor epoxide 102P alpha-BHCL 103P beta-BHC_______ 104P gamma-BHC._____ lQ5P_._d_eha-BHC..____ 106P PCB-1242 ^_____ 1Q7P PCB-1254____ 1Q8P PCB-1221____ 109P PCB-123_2_. 110P PCB-1248 ' 111P PCB-126Q_______ 112P PCB-I016_______ 113P toxaphene * * Less than 10 ug/l (pesticides less than 5 ug/l) ND = Not detected ** * Not confirmed by GCMS M ND ••VfVH _N_P_ Nj J!2, J!L M NO ID _ND_ jjD_ IL M ML r ND tjD M. ND m ML CM O ND 'iflPi.WBlaiff,.

f G INC. INDUSTRIAL CATEGORY - US Environmental … · west coasera t technlcal s6rv1cf g inc.industrial category • sample id 30f-1 lab id 22049v1 date injected 8/28/81 std id bfb52

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Page 1: f G INC. INDUSTRIAL CATEGORY - US Environmental … · west coasera t technlcal s6rv1cf g inc.industrial category • sample id 30f-1 lab id 22049v1 date injected 8/28/81 std id bfb52

EraW E S T COAST T e C H N l C A L S 6 R V 1 C G I N C . I N D U S T R I A L C A T E G O R Yf• S A M P L E I D 3 0 F - 1

L A B I D 22049V1D A T E I N J E C T E D 8 / 2 8 / 8 1S T D I D B F B 5 2 V O A 1 7 6C O N C . F A C T O R — — — — -

V o l a u l e s2 V i q j . i j I M i i ' ' " " " " ' " " "3V a c r y l o n i t r i l e4V benzene6V carbon t e t r a c h l o r i d e7V c h l o r o b e n z e n e10V l^rfr^iCiyrt^-iiftoiiiiAra11 V 1,1 , i - t r i c h l o r o e t h a n e13V 1» 1 - d i c h l o r o e t h a n e14V 1 , 1 , 2 - t r i c h l o r o e t h a n e15V 1. 1 , 2 , 2 - t e t r a c h l o r o e t h a n e16V c h l o r o e t h a n e

j D j t ' J L Y Y \ S ) I f t X f i X l X s s i y f l f t j \ J t v W \ l X ) X /^JwwwuA X X X )19V 2 - c h l o r o e t h y l v i n y l e t h e r23V m t o m r f r i n T T i f29V 1 , 1 - d i c h l o r o e t h y l e n e30V 1 , 2 - t r a n s - d i c h l o r o e t h y i e n e32V 1 , 2 - d i c h l o r o p r o p a n e33V 1 , 3 - d i c h l o r o p r o p y l e n e38V e t h y l b e n z e n e44V f t i ^ ^ i t ' ^ ' U g f f M a b ^45V m e t h y l c h l o r i d e46V m e t h y l b r o m i d e47V b r o m o f o r m48V d i c h l o r o b r o m o m e t h a n e49V t r i c h l o r o f l u o r o m e t h a n e50V d i c h l o r o d i f l u o r o m e t h a n e51V c h l o r o d i b r o m o m e t h a n e85V t e t r a c h l o r o e t h y l e n e86V t o l u e n e87V t r i c h l o r o e t h y l e n e88V v i n y l c h l o r i d e

u g / l26

N DN ON DN D19

N DN DN DN DN D

X X X X X XN D32

N D*

N DN ON O19

N D .N O

_ . N D .N DNOHP

__.. - ND*N D*

^ f|D.

**

S A M P L E ID____L A B ID______D A T E E X T R A C T E D ^D A T E I N J E C T E D ^S T D I DC O N C . F A C T O R

P e s t i c i d e s

30MTRACE #44238 / 2 8 / 8 18 / 3 1 / 8 1

J R A C E _ * 4 4 2 2100

89P a l d r i n9QP._._ d l e l d r i n _ _91P c h l o r d a n e92P ' -DOT9 3 P 4 . 4 ' - D P £ ._____9 4 P _ 4 . 4 ' - D P D _ _ _ _ _ _ _9 5 P a l p h a - e n d o s u l f a n96P b e t a - e n d o s u l f a n9 7 P e n d o s u l f a n s u l f a t e9gP _endrin_________99P_ e n d r i n a l d e h y d elOQP _ h e p t a c h l o r _ _ _ _ _ _I Q j P _ h e p t a c h l o r e p o x i d e102P a l p h a - B H C L103P b e ta-BHC_______104P g a m m a - B H C . _ _ _ _ _l Q 5 P _ . _ d _ e h a - B H C . . _ _ _ _106P P C B - 1 2 4 2 ^_____1Q7P P C B - 1 2 5 4 _ _ _ _1Q8P P C B - 1 2 2 1 _ _ _ _109P PCB-123_2_.110P P C B - 1 2 4 8 '111P PCB-126Q_______112P PCB-I016_______113P t o x a p h e n e

* * L e s s t h a n 10 u g / l( p e s t i c i d e s l e s s than 5 u g / l )

N D = N o t d e t e c t e d** * Not c o n f i r m e d by GCMS

MN D

••VfVH

_N_P_N j

J!2,J!LM

N OID_ N D _j j D _ILMMLr N D

tjDM.

N D

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' i f l P i . W B l a i f f , .

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11.5- E N V I R O N M E N T A L P R O T E C T I O N A G E N C Y - H W 1 S a m p l e Management O f f i c eP.O. G o x S I S - A l e x a n d r i a , V i r g i n i a 22313 - 7 0 3 / 5 5 7 - Z 4 9 0 / F T S - 3 - 5 5 7 - 2 4 9 Q

A N A L Y S I S D A T A S H E E T

L A B O R A T O R Y N A M E ^Versar jnc^L A B S A M P L E I D N O . _ _

S A M P L £

1. A l u m i n u m2* Chromium3« Sarium4. Bervil ium5. Cadmium6. C o b a l t

CoooerS. I r o n9.

QC R E T O R T NO*TASK 1

u g / 1to be i d e n t i f i e d and measured)

10- N i c k e J u g / I1U12.13.1*.15.16.17.

Manganese ? < .Zinc <*/<?-Boron t*i&.V a n a d i u m <* fO.Calcium ?3t 3O&Maenes ium S, $ £>O>S o d i u m 3$f,$OO*

— r-^rK^COo— o

«•«»

TA5K 2 (lUements to b« i d e n t i f i e d and measured)

u g / 1i.2.3«a.

Arsenic ^IU*A n t i m o n y < 2 .S e l e n i u m <V£).T h a l l i u m <"/O.

5, MercurvTin

7. Silver

u g / 1

TASK 3 ( K l e m e s T t s to be i d e n t i f i e d and measured)

I* Ammonia•2. F l u o r ide3. SuJflde m«/l

Cvanide5- pH

TOCU n i t s

mi/1

C O M M E N T S : a)b )c)d )e) average of two replieate dete srujjat ic i iS£) insuf f i c i ent J3an$>le aliquot

with a detecticn Luuit ofwith a detecfcicn Ijjnit ofwith a detection Umit ofanalyzed on a sample aliqunt X T i t h H G 1 fron F / p H bottle

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Page 3: f G INC. INDUSTRIAL CATEGORY - US Environmental … · west coasera t technlcal s6rv1cf g inc.industrial category • sample id 30f-1 lab id 22049v1 date injected 8/28/81 std id bfb52

W € S T C O A S T T € C H N I C A l S 6 R V I C 6 I N CO R G A N I C S A N A L Y S I S D A T A S H E E T - Page 3QC Report No; S a m p l e N u m b e r

A . S U R R O G A T E S P I K E R E S U L T S

C O M P O U N DBenzene - dol-Chloro»2-BromopropamT o l u e n e - d82 - F l u o r o p h e n o iP h e n o l - d5N i t r o b e n z e n e - d52 - F l u o r o b i B h e n v lN a p h t h a l e n e - 0 8

F r a c t i o nVOAVOA

|_ VOAA C I DA C I DB/Nif^B / N

C o n c . ( u q / l )59535887

1009697

NA '

C S u r r o g a t e s o n l y )S p i k e 1 IAdded (uoVI ) ! Recovery5050SOtoo

103101100

N A

118106116

87100

9597

N A8 . T E N T A T I V E L Y I D E N T I F I E D C O M P O U N D S

1.2.3.4.5.6.7.8.9.10,11.12.13.14.15.16.17.18.19.20.

CAS K C O M P O U N D N A M EE T H A N O L

C H L O R O P R O P 1 N ET E T R A H Y D R Q F U R A NT E T R A H Y D R O - 3 - M F T H Y L -

2 H - P Y R A NU N K N O W NU N K N O W NH Y D R O C A R B O NU N K N O W NU N K N O W NU N K N O W NU N K N O W NU N K N O W N

.

F R A C T I O NVOA #53VOA #87VOA 1109

VOA #239B / N #193B/N *366A C I D £ 5 9A C I D 1108A C I D 1140A C I D 0157A C I D 0277A C I D # 8 3

% M a x i m u m S c o r e A t t a i n e dM a s s M a t c h i n g R o u t i n e : F I T( s p e c i f y )

915G E N E R A L F I T934

914N O 600D F I TN O G O O D F I TG E N E R A L F I TN O G O O D F I T

• N O G O O D F I T• N O G O O D F I T

N O t t O O D F I TN O 6000 F I T

o

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$.iit i*0 Cemios, California 90701 j t

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A W & . N C T - M W I S d / n p / c M f l i t a g c m c m O f i i e *P.O, &QX m - A l e x a n d r i a , V i r g i n i a 223 U • 703/ 5 5 7 - 2 * 9 0 / F T S - 6 . 5 5 7 - 2 * 5 0I N O R G A N I C S A N A L Y S E D A T A 5 H E S T $+A\ \ '

L A B O R A T O R Y N A M E m m r Inc.LAS SAMPLE tD NO. &13&

1. A l u m i n u m2.3. Barium

Co co AT*- Iran9.

TASK I (B«m«nta

SAMPLS NO. SGfJ M_QC REPORT NO.

b* id«ntt f i«d and10. Nicfcaiu.

ZincSoronVanadium

1.5. C a J c u mI S . Magnes ium

20

y^^ f l f l .

«I/i

CDOo

TASK 2 to b« i d a n t t f i e c f and m«tusurmi}

i<2.3-f t .

A r s e n i cAntimenvS e l a n i u mT h a l l i u m

</Q_,

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7. S i l v e r

ug/1

TA5K 3 (Elegants to be i d e n t i f i e d and measured}

1. A m m c n i a•2- F i u p r i d e3. S u i f i d e

m g / I Cvanidep H

mu/1 TOG

r n g / IU n i t s

C O M M E N T S ^ a) with a detection limit ofb) with a dstectioi liait ofc) with a detection l i jn i t ofd) analysed on a sample ali^ot preserved w i f c l i Hd frc tn F/pH sample isottlee) anȣase of two replicate dstatminatiensf) insuf fici^it satple aliquot

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A H A L Y W IL A B O A A T O A Y * f C T I O M - H O U I T O N t f t A N C M1

t1I

t•(

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" ^ • ^ < ' ' ' * y ^ J /M ^ ^ * ' ^ \ • ,V . . - - , - , . ,

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A c i d Con p o u n d s21A 2 , £ . 6 - t r i c h l o r o p h e n o I22A p-chloro*m*cresol2 £ A 2 - c h l o r o p h e n o l31A 2 , £ * d i c h l o r o p h e n o l3 £ A 2 , £ - d i m e t h y l p h e n o lS 7 A 2 * n i t r o p h e n o l5 f l A £ * n i t r o p h e n o l$9A 2 , £ * d i n i t r o p h c n o t60A 6,6^dinitro-o«cre$ol6 £ A p e n t a c h l o r o p h e n o l

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B a t f l / H e u t r a l C o m p o u n d s

I B ac enaphthene______SB benzldine______88 l , 2 , £ - t r l c h l o r o b e n z e n e9B h e x a c h l o r o b e n z e n e128 hexachloroe thane____18B b i g ( 2 - c h l o r o e t h y l ) e t h e r20B 2 - c h i o r o n a p t h a l e n e2$B l , 2 * d l c h l o r o b e n z e n e26 B 1,3-d ic h lor pbg n_ze n ^

2 8 8 3 > 3 ' ' - d i c h l o r o b e n z > d i j i e _ _35B 2 ,4~d in i t r o t o lu ene36B 2 , 6 - d i n l t r o t Q l u e n G37B 1 , 2 - d i p h e n y l h y d r a z i n e

( a s a z o b e n z e n e )

J1Q.MLJO.J J 1

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S A M P L E E D 3 O F . 2L A B I D 2204483D A T E E X T R A C T E D 8 / 2 9 / f i lD A T E I N J E C T E D « / t / 8 1S T D I D 8 E H Z 4 G 3 8 M S T D 4 2 0C O N C F A C T O R 1000

B a s e / N e u t r a l C o m p o u n d s u<£18 4~bromophtnyl p h e n y l e t h e r£28 b i s < 2 - c h l o r o i s o p r o p y l ) e t h e r£38 bis ( 2 - c h l o r o e t h o x y ) me thaneS2B h e x a c h l o r o b u t a d i e n e53 B h e x a c h l o r o c y c l o p e n t a d i e n e5^8 U o p h o r o n e558 n a p h t h a l e n e568 n i t r o b e n z e n e618 N - n i t r o f o d i m e t h y t a m i n e628 N - n i t r o s o d i p h e n y l a m i n e638 N - n i t r o s o d i - n - p r o p v l a m i n e

e / iH OH OHOHON ON OH OHO"PN pH P

66B b i s ( 2 - e t h y l h e x y l ) p h t h a i a t e *6 7 8 b u t y l b e n z y l p h t h a l a t e68 B d i - n - b u t y l p h t h a i a t e

W*

698 di-n-octyl p h t h a i a t e MO708 d i e t h y l p h t h a i a t e *7 1 8 d i m e t h y l p h t h a i a t e N O72B b e n z o ( a ) a n t h r a c e n e738 b e n z o ( a ) p y r e n c7 £ B 3 t £ - b e n z o f l u o r a n t h e n e75B b e n z o ( k ) f l u o r a n t h e n e763 e h r y s e n e77B a c e j i a j > h t h y l e n e78B a n t h r a c e n e7 9 B b e n z o f g h i ) p e r y l e n eSOB f t u o r e n e81B p h e n a n t h r e n e

H P"CN OMON DN OH PN ON HN n _

8 2 B d i b e n z o ( a , h ) a n t h r a c e n e N nS 3 B i n d e n o ( 1 . 2 , 3 - e d ) p y r e n e8iB p y r e n e

N f iN O

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— ."•• — — . ... . — 1". - ^' C S S P J W 6 S T C O A S T T O T N I C A L S E R V I C E I N C I N D U S - T O T ^ C A T E G O R Y

S A M P L E I D 3 0 F - 2L A B I D 2 2 Q 4 9 V 1 8D A T E I N J E C T E D 8 / 3 G / S 1S T D I D B F E 5 4 V O A 1 7 7C O N C . F A C T O R ........

V o l a t i l e s2V acro l e in3V a c r y l o n i t r i l e4V benzene6V carbon t e t r a c h l o r i d e7V e h l c r o b e n z e n e

11V 1,1. 1 - t r i c h l o r o f i t h a n e13V 1 » 1 - d i c h l o r o e t h a n e14V 1 , 1 , 2-trich l oroe thane15V 1 f 1 , 2, 2 - t e t r a c h l o r o e t h a n e16V c h l o r o e t h a n e

JCP51X X XXX X I K K2 ft t £ XttXlftJQCX X^h^MC X X X X >19V 2 - c h l o r o e t h y l v i n v l e t h e r23V j M ^ . M u i i i w i i -29V 1 , i - d i c h l o r o e t h y l e n e30V 1 , 2 - t r a n s - d i c h l o r o e t h y l e n e32V 1 , 2 - d i c h l o r o p r o p a n e33V 1 , 3 - d i c h l o r o p r o p y l e n e38V e t h y l b e n z e n e/ / \t •ua tk i . 1 . _ ^. *_U * . ^ , J A

45V m e t h y l c h l o r i d e46V m e t h y l b r o m i d e47V b r o m o f o r m48V d i e h l o r o b r o m o m e t h a n e49V t r i c h l o r o f l u o r o m e t h a n e50V d i e h l o r o d i f l u o r o m e t h a n e51V c h i o r o d i b r o m o m e t h a n e85V t s t r a c h l o r o e t h y l e n e86V t o l u e n e8 7 V j t t ^ r — ' i r l i L j ,88V v i n y l c h l o r i d e

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P e s t i c i d e s89P a i d r i n90P d l e l d r i n91P c h l o r d a n e9 2 P 4 . 4 ' - D D T9 3 P 4 , 4 ' - D D E9 4 P 4 , 4 ' - D D D95? a l p h a - e n d o s u l f a n96? b e t a - e n d o s u l f a n9 7 P e n d o t u l f a n s u l f a t e98P e n d r i n9 9 P e n d r i n a l d e h y d e100P h e p t a c h l o r101P h e p t a c h l o r e p o x i d e102P a l p h a - B H CI 0 3 P b e t a - B H C104P g a m m a - B H C105P d e l t a - B H C106P P C B - 1 2 4 2107P P C B - 1 2 5 4108P P C B » 1 2 2 1109P PCB-1232H O P P C B - 1 2 4 81 1 1 P P C B - I 2 6 01 1 2 P P C B - 1 0 1 6113P t o x a p h e n e

* « Les s t h a n 10 u g / 1( p e s t i c i d e s l e s s than 5 u g / 1 )

N D « N o t d e t e c t e d** e Not c o n f i r m e d by GCMS

N ON ON DN DS ONON ON DNON DN DN ON ON pN DN DN ON pH PN PH PN PN DN ON P

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I ' - 5 . E N V I R O N M E N T A L P R O T E C T I O N A G E N C Y - H W 1 S a m p l e Management O l / i c *P.O. p o x S I S - A l e x a n d r i a , V i r g i n i a 22313 - 703/ 5 5 7 - 2 4 9 0 / / T S - 8 - 5 5 7 - 2 4 9 0

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TASK 1 - ( E l e i t i e T t s to be ident i f i ed and measured)4 U g / 1 U g / 1<£<?£. 10. N i c k e l ^ O-

<10, 11. Maji^aneae 2^7A 12- Zir.C <* / . ,r\

4. ServLnum <"£. 13. Boron 3O* to5. Cadmiumo* C c f a s i t7. CcooerS. I r a n

<"£ - 14. Vanadium 'C IL). ^<lQ, 1^. Calcium 351^300. o<5^), 16. M a z n e s i u m 2,900.

90. 17. S o d i u m IQIOO.9. Laad ^ ^0*

TASK 2 (Element!, to b« i d e n t i f i e d and measured)

u g / 1 f ' u g / 11. A r s « f i i c ^ /O' 5* Mcrcurv /2- Antimony3- Sel en ium

<2.O. 5. Tin ^^C).< / 0 - 7. S i l v e r <20 .

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1. Ammonia1 -Z, F i u c r i d e

3. S u l f i d e

TASK 3 (Elements to be i d en t i f i ed and measured)

ms/1 4. Cvanide m « / Im ? / l 5* pH U n i t sms/1 fi* TOC • m e / 1

C O M M E N T S t a )b)c)d )e)£)

with a detecticn limit of £&O. .with a d f i ta c t i cn liitiit of -with a detection l i jni t ofanalysed on a sarrole aliquot preserved with HC1 fron F/pH sarrple bottleaverage of two repHcata detaoiinatior^insuf f i c i ent sample aliquot i

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**4-- V ' _ i ' ^ > ' - . v , -".

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• ."" 41©Jig} west COAST TemwiCAu SGRVHS A M P L E I D 3 0 F - 6f * ft f tSL A o l u ? ? H d Q A < 3D A T E E X T R A C T E D f t / ^ f l / A lD A T E I N J E C T E D q / ? / f US T D I D _ _ _ _ _ S E N S l f l l P H P N . 1 5 f l _C O N C F A C T O R 1000

A c i d C o m p o u n d s21 A 2 , 4 , 6 - t r i c h l o r o p h e n o l22A p-chloro-m-cre so l24A 2 - c h I o r o p h e n o l31 A 2 , 4 - d i c h l o r o p h e n o l34 A 2 , 4 - d i m e t h y l p h e n o l57A 2-n i t r opheno l58A 4 - n i t r o p h e n c l59 A 2 , 4 - d i n i t r o p h e n o l60A 4 ,6-d in i t ro-o- cr e s o l64 A p e n t a c h l o r o p h e n o l65A p h e n o l

B a s e / N e u t r a l C o m p o u n d s

18 a c e n a p h t h e n eS B b e n z i d i n eSB 1 , 2 , 4 - t r i c h l o r o b e n z e n e9B h exa ch l o rob enz ene1 2 B h e x a c h l o r o e t h a n e

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1 8 B U W - f r ' * " ' 1 " " 1 i l i r i n n l i r T — — — — T T *2 0 B 2 - c h l o r o n a p t h a l e n e N D25B 1 f 2 - d i c h l o r o b e n z e n e26B 1 ,3-dichlorobenzene27B 1 , 4 - d i c h l o r o b e n z e n e

N D_.- . ND

N D28B 3 » 3 ' - d i c h l o r o b e n z i d i n e «n35B 2 , 4 - d i n i t r o t o l u e n e36B 2 , 6 - d i n i t r o t o l u e n e

. _ ND.__ . ND

37B 1 , 2 - d i p h e n y l h y d r a z i n e( a s a z o b e n z e n e ) N H

39B f l u o r a n t h e n e40B 4 - c h l o r o p h e n y l p h e n y l

NOe t h e r N D

B a s e / N e u t r a l C o m p o u n d s41B42B43B52B53B54B55B56B61B62 B63B66B67B68B69B70 B71B72873B74B75B76 B77B78B79880881 B82B83B84B

4-bromophenyl p h e n y l e therb i s ( 2 - c h l o r o i s o p r o p y l ) e t h e rb i s ( 2 - c h l o r o e t h o x y ) m e t h a n eh e x a c h l o r o b u t a d i e n eh e x a c h l o r o c y c l o p e n t a d i e n ei s ophoronen a p h t h a l e n en i t r o b e n z e n eN - n i t r o s o d i m e t h y l a m i n eN - n i t r o s o d i p h e n y l a m i n eN - n i t r o s o d i - n - p r o p v l a m i n eb i s ( 2 - e t h y l h e x y l ) p h t h a i a t eb u t y l b enzyl p h t h a i a t ed i - n - b u t y l p h t h a i a t ed i - n - o c t y l p h t h a l r . t ed i e t h y l p h t h a i a t ed i m e t h y l p h t h a i a t eb e n z o ( a ) a n t h r a c e n eb e n z o ( a ) p y r e n e3 , 4 - b e n z o f l u o r a n t h e n eb e n z o ( k ) f l u o r a n t h e n ec h r y s e n ea c e n a p h t h y l e n ea n t h r a c e n e •b e n z o ( g h i ) p e r y l e n ef l u o r e n ep h e n a n t h r e n ed i b e n 2 o ( a , h ) a n t h r a c e n ei n d e n o ( l , 2 , 3 - c d ) p y r e n ep y r e n e

gU^nn.

N DN DN DN DN DN DN DN ON ON ON D*N O***

N DN ON DN ON ON O

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1298 2 , 3 , 7 * 8 - t e t r a c h l o r o d i b e n z o -p - d i o x i nr- . _, -^-. . ,^-_-———-—.._,. . _ _ _ _ _ _ _._. . . . . ND_.

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W 6 S T C O A S T T e m N I C A iS A M P L E I D 3 0 F - 6L A B I D 22049V8D A T E I N J E C T E D 8 / 2 8 / 8 1

S T D I D 8 F B 5 2 V O A 1 7 6f * A H f e A r ^ r i t ?V » u N L » r A l w i U K

V o l a t i l e s2 V I M B i i i i l g E J i J M l l i i i m i i i i i a i i i H H i i i i i i i i i i i i i M i i i i i3V a e r y l o n i t r i l e6V b enzene6V carbon t e t r a c h l o r i d e7V c h i o r o b e n z e n e1 0 V j j l i i M i i i h l i f U U L U l l i l l L -11V 1 , 1 , 1 - t r i c h l o r o e t h a n e13V 1 , 1 - d i c h l o r o e t h a n eUV 1, 1 , 2 - t r i c h l o r o e t h a n e15V 1,1 , 2 , 2 - t e t r a c h l o r o e t h a n e16V c h l o r o e t h a n emnwinmiu&mtzm&mftmun19V 2 - c h l o r o e t h y l v i n y l e ther23V r t a n m f j M ^ r29V 1 , 1 - d i c h l o r o e t h y l e n e30V 1 , 2 - t r a n s - d i c h l o t ' o e t h y l e n e32V 1 , 2 - d i c h l o r o p r o p a n e33V 1 , 3 - d i c h l o r o p r o p y l e n e38V e t h y l b e n z e n e

45V m e t h y l c h l o r i d e/»6V m e t h y l b r o m i d e47V b r o m o f o r m48V d i c h l o r o b r o m o m e t h a n e49V t r i c h l o t o f l u o r o m e t h a n e50V d i c h l o r o d i f l u o r o m e t h a n e51V c h l o r o d i b r o m o m e t h a n e85V t e t r a c h l o r o e t h y l e n e86V t o l u e n e87V t r i c h l o r o e t h y l e n e

- S 6 R V I

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1P1^ - h . g f i j g c f t l o r e p o x i d e102P a l p h a - B H C _ _ _ _ _ _103P beta-BHC_______1Q4_P_. _ g a _ m m a ~ B H C _.1Q5P d e l t a - B H C106P P C B - 1 2 ^ 21Q7P PCB-12541Q8P PCB-1221_______109P PCB-1232H O P . PCB~m8111P PCB-1260H 2 P PCB-1016_______113P t o x a p h e n e

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N D « N o t d e t e c t e d** « Not c o n f i r m e d by GCMS

88V v i n y l c h l o r i d e NO.

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W 6 S T COAST T E C H N I C A L S 6 R V I C 6 I N CO R G A N I C S A N A L Y S I S D A T A S H E E T - P a g e 3QC Repor t No: S a m p l e N u m b e r

3 OF-6A . S U R R O G A T E S P I K E R E S U L T S ' — — — — — '

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F r a c t i o nVOAVOAVOA

_ _ A C I DA C I DB / NB / NB / N

C o n c _ J i u 5 A L L61

1 526097

1238197N A

( S u r r o q a t e s o n l y )S p i k eA d d e d ( u q / 1 )505050

100103101100

N A

*Recovery122 :104I f l L ^ - .

971208097N A

8 . T E N T A T I V E L Y I D E N T I F I E D C O M P O U N D S

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2 H - P Y R A NU N K N O W NU N K N O W NU N K N O W NU N K N O W NU N K N O W NU N K N O W NH Y D R O C A R B O NU N K N O W NU N K N O W NU N K N O W NU N K N O W NU N K N O W N

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' N O GOOD F I TG E N E R A L F I TN O G O O D F I TN O G O O D F I TN O G O O D F I TN O GOOD F I TN O G O O D F I T

INIrt* P .1

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I N O R G A N I C S A N A L Y S I S D A T A S H E E T

L A B O R A T O R Y NAME Versar Inc. SAMPLS NO, 30 f bF\L A S S A M P L E I D

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; s-9.

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OirsmiumBariumS e r v l l i u r r sCadmiumC c b a J tCoooerIronL^ad

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A m m c n i aF l u c r i d eS u i f l d e

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NO. S313>- - QC REPORT NO.TASK 1 ( E f & n e n t s td b« i d e n t i f i e d and measured)

- - " S / 1

<$>60. 10, Nicke l <2A•^ 10. U. Manganese ^ (9,

9(2, 12. Zinc ^?A<5* 13. S o r o n 3^

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*Z 2$. 16. Magnes ium J?, *$OO.. . J/O. 17. S o d i u m l%^/00-**?

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ug/1<"/A 5. M«rcurv • < ' / .< - 6, Tin 5 ,</£>. 7. SUvef < ).

<7o.TASK 3 (Elements to be ident i f i ed and measured)

me/I *. Cvanidem t ? / l J . p Km«/l 6. TOC

a) with a detection limit of ££O,b) with a cetectioi limit ofc) with a detection limit ofd) analyzed en a ssrrple aliquot preserved with Hd from F/pHe) mirage of two replicate detanrtinaticKsf ) insuf f i c i ent sanple aliquot

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A N A L Y S I S B E Q U E S T / R E P O RU A S O a A T O R Y S E C T I O N - H O U S T O N B R A N C HS . A N D A . D I V I S I O N - R E G I O N V M J . S . E . P . A .

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0 9 £ 8 0 CE N V I R O N M E N T A L P R O T E C T I O N A G E N C Y

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(£21i) W € S T C O A S T I t J I l dS A M P L E I D 3 0 F - 7

I C A L S € R V I C € I N C i N D U S T ^ K c A l G D R Y .

L A B I D 2 2 0 4 9 A 1 0D A T E E X T R A C T E D 8 / 1 0 / 8 1D A T E I N J E C T E D 9 / ^ / 8 1S T D I D S E N S 1 8 1C O N C F A C T O R 1000

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B a s e / N e u t r a l C o m p o u n d s

I B a c e n a n h t h e n eS B b e n z i d i n e8B l » 2 , 4 - t r i c h l o r o b e n 2 e n e9B h e x a c h l o r o b e n z e n e1 2 B h e x a c h l o r o e t h a n e18B b i s ( 2 - c h l o r o e t h y l ) e t h e r20B 2 - e h l o r o n a p t h a l e n e25B \ , 2 - d i c h l o r o b e n z e n e26B 1 , 3 - d i c h l o r o b e n z e n e27B 1 , 4 - d i c h l o r o b e n z e n e2 8 B 3 t 3 ' - d i c h l o r o b e n z i d i n e35B 2 , 4 - d i n i t r o t o l u e n e36B 2 , 6 - d i n i t r o t o l u e n e37B 1 , 2 - d i p h e n y l h y d r a z i n e

( a s a z o b e n z e n e )39B f l u o r a n t h e n e40B 4-chlorophenyl p h e n y l

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. S T D I D B E N Z 4 0 5 B N S T D 4 2 1C O N C F A C T O R 10QO

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6 7 B b u t y l b e n z y l p h t h a l a t e6 8 B d i - n - b u t y l p h t h a l a t e6 9 B d i - n - o c t y l p h t h a l a t e7 0 8 d i e t h y l p h t h a l a t e7 1 B d i m e t h y l p h t h a i a t e7 2 B b e n z o ( a ) a n t h r a c e n e73B b e n z o ( a ) p y r e n e74B 3 > 4 - b e n z o f l u o r a n t h e n e753 b e n z o ( k ) f l u o r a n t h e n e76B chry s ene77B a c e n a p h t h y l e n e/ 8 B a n t h r a c e n e79B b e n 2 o ( g h i ) p e r y l e n eSOB f l u o r e n e81B p h e n a n t h r e n e828 d i b e n z o ( a , h) a n t h r a c e n e

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