17
ORIGINAL PAPER Experimental Study on Guabirotuba’s Soil Stabilization Using Extreme Molding Conditions Jair de Jesu ´s Arrieta Baldovino . Ronaldo Luis dos Santos Izzo . Fernanda Feltrim . E ´ rico Rafael da Silva Received: 26 November 2018 / Accepted: 23 December 2019 / Published online: 3 January 2020 Ó Springer Nature Switzerland AG 2020 Abstract The porosity/cement ratio (g/C iv ) was employed in this research to study the evolution of unconfined compressive strength (UCS or q u ) and split tensile strength (STS or q t ) of a silty soil stabilized with cement in several molding conditions not shown in the literature. Five molding moisture contents (x) fixed between 14.67 and 33.34%, three dry unit weight of molding between 13 and 16 kN/m 3 , four cement contents (C) between 3 and 9% (by dry mass of the natural soil) and a curing time of 28 days were used to study the influence of g/C iv on q t and q u under normalized conditions. With the increase in dry molding unit weight and cement content, as well as reducing the initial porosity of the samples, q u and q t strengths increase for all mixtures. On the other hand, q u and q t also increase potentially depending on the g/ C iv ratio, adjusted to an exponent of 0.44, which remained constant for all molding conditions. The g/ C iv ratio was able to establish empirical ratios between q t /q u , which obtained values between 0.135 and 0.163 and which depended on the moisture content used during compaction. Regarding molding moisture content, there was an augment in q u and q t , with an increased molding moisture content up to 28% (con- verting into an optimum value) using the g/C iv ratio in normalized terms. After x = 28%, the strength of the mixtures was reduced. Finally, two equations to dose and estimate q t and q u were obtained, set to 96.5%, and with a 6% error. Thus, all strengths showed the same normalized potential trend as a function of x, compatible with the value of g/C iv 0.44 = 35. Keywords Ground improvement Porosity/cement ratio Split tensile Unconfined compressive Molding conditions Empirical relationships List of Symbols D 50 Mean particle diameter D 10 Effective size C Cement content (expressed in relation to mass of dry soil) C iv Volumetric cement content (expressed in relation to the total specimen volume) B iv Volumetric binder content (expressed in relation to the total specimen volume) q u Unconfined compressive strength q t Split tensile strength J. J. A. Baldovino R. L. S. Izzo (&) F. Feltrim E ´ . R. da Silva Department of Civil Construction, Federal University of Technology- Parana ´, Street Deputado Heitor Alencar Furtado, 5000, Campus Curitiba, Ecoville, Parana ´ ZIP: 81280-340, Brazil e-mail: [email protected] J. J. A. Baldovino e-mail: [email protected] F. Feltrim e-mail: [email protected] E ´ . R. da Silva e-mail: [email protected] 123 Geotech Geol Eng (2020) 38:2591–2607 https://doi.org/10.1007/s10706-019-01171-x

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Page 1: Experimental Study on Guabirotuba’s Soil Stabilization ... · Experimental Study on Guabirotuba’s Soil Stabilization Using Extreme Molding Conditions Jair de Jesu´s Arrieta Baldovino

ORIGINAL PAPER

Experimental Study on Guabirotuba’s Soil StabilizationUsing Extreme Molding Conditions

Jair de Jesus Arrieta Baldovino . Ronaldo Luis dos Santos Izzo .

Fernanda Feltrim . Erico Rafael da Silva

Received: 26 November 2018 / Accepted: 23 December 2019 / Published online: 3 January 2020

� Springer Nature Switzerland AG 2020

Abstract The porosity/cement ratio (g/Civ) was

employed in this research to study the evolution of

unconfined compressive strength (UCS or qu) and split

tensile strength (STS or qt) of a silty soil stabilized

with cement in several molding conditions not shown

in the literature. Five molding moisture contents (x)fixed between 14.67 and 33.34%, three dry unit weight

of molding between 13 and 16 kN/m3, four cement

contents (C) between 3 and 9% (by dry mass of the

natural soil) and a curing time of 28 days were used to

study the influence of g/Civ on qt and qu under

normalized conditions. With the increase in dry

molding unit weight and cement content, as well as

reducing the initial porosity of the samples, qu and qtstrengths increase for all mixtures. On the other hand,

qu and qt also increase potentially depending on the g/Civ ratio, adjusted to an exponent of 0.44, which

remained constant for all molding conditions. The g/Civ ratio was able to establish empirical ratios between

qt/qu, which obtained values between 0.135 and 0.163

and which depended on the moisture content used

during compaction. Regarding molding moisture

content, there was an augment in qu and qt, with an

increased molding moisture content up to 28% (con-

verting into an optimum value) using the g/Civ ratio in

normalized terms. After x = 28%, the strength of the

mixtures was reduced. Finally, two equations to dose

and estimate qt and qu were obtained, set to 96.5%, and

with a 6% error. Thus, all strengths showed the same

normalized potential trend as a function of x,compatible with the value of g/Civ

0.44 = 35.

Keywords Ground improvement � Porosity/cement

ratio � Split tensile � Unconfined compressive �Molding conditions � Empirical relationships

List of Symbols

D50 Mean particle diameter

D10 Effective size

C Cement content (expressed in relation to

mass of dry soil)

Civ Volumetric cement content (expressed in

relation to the total specimen volume)

Biv Volumetric binder content (expressed in

relation to the total specimen volume)

qu Unconfined compressive strength

qt Split tensile strength

J. J. A. Baldovino � R. L. S. Izzo (&) � F. Feltrim �E. R. da Silva

Department of Civil Construction, Federal University of

Technology- Parana, Street Deputado Heitor Alencar

Furtado, 5000, Campus Curitiba, Ecoville,

Parana ZIP: 81280-340, Brazil

e-mail: [email protected]

J. J. A. Baldovino

e-mail: [email protected]

F. Feltrim

e-mail: [email protected]

E. R. da Silva

e-mail: [email protected]

123

Geotech Geol Eng (2020) 38:2591–2607

https://doi.org/10.1007/s10706-019-01171-x(0123456789().,-volV)( 0123456789().,-volV)

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qu�norm Normalized unconfined compressive

strength

qt�norm Normalized split tensile strength

cd Dry unit weight

g Porosity

x Moisture content

r Value of a given adjusted porosity/cement

css Unit weight of soil

csc Unit weight of cement

n Tensile/compressive strength ratio

R2 Coefficient of determination

1 Introduction

Cement is one of the most widely used binders in the

world, especially in the engineering sector in the

construction of buildings, rigid pavements, founda-

tions, channels, among other infrastructure works.

Besides these applications, cement is also widely used

for soil stabilization (Baldovino et al. 2019a). When

the cement is mixed with soil in the presence of water

and then compressed, it is known as soil–cement. The

soil–cement reaches higher strength than soil under

normal conditions, and, in a short time, cement helps

in workability, reduces expansion, decreases porosity

and increases the durability of the mixture when it is

used (Henzinger et al. 2018; Baldovino 2018). The

cement benefits on the properties mentioned are due to

the substantial amount of cement used or the high

compaction energy used. Therefore, the volume of

cement used and the initial porosity in the soil–cement

are vital variables to stabilize soil with cement, as it

can be observed in recent studies (Festugato et al.

2017; Consoli et al. 2017d; Diambra et al. 2018;

Henzinger et al. 2018; Baldovino and Izzo 2019).

Consoli et al. (2007) used the g/Civ ratio to study

the qu strength of a clayey sandy soil mixed with high

early strength cement. In the study, the same density

(19 kN/m3) and several molding moistures (4 up to

14%) were set, and the molding moisture content

(x) = 10%was the value at which the mixtures had the

highest strengths under non-normalized conditions,

and without considering g/Civ, only evaluating the

cement content used (2–12% regarding the dry soil

mass). For the set value of x = 10%, the molding

density also varied, obtaining strengths close to

5 MPa, after 7 curing days. Consoli et al. (2009a)

concluded that, for a sandy lean clay soil mixed with

lime and cement, using the same dry density (18 kN/

m3), the x molding moisture (between 10 and 16%)

had no significant effects on qu strength of any mixture

(soil–lime or soil–cement) under non-normalized

conditions and without the use of g/Civ. In a study,

Consoli et al. (2011) applied strengths normalization

to study the effects of the dry unit weight of molding,

porosity and molding moisture on the mechanical

behavior of silt mixed with cement, using different

unsaturated molding conditions: and x varying

between 17 and 23%, cement between 3 and 9% and

cd between 14 and 16 kN/m3. With the normalization

of qu strength as a function of g/Civ, it was found that

the strength increased linearly from x = 17 to

x = 23%. Stracke et al. (2012) mixed sandy soil with

cement to verify the effects of molding moisture

(between 6 and 14%) and void ratios (e) on the

compressive and tensile strength of samples after 7

curing days. It was concluded that, for this type of soil,

moisture reduction increased mechanical resistance,

being 6% the value of x in which the samples reached

maximum values of qu and qt as a function of g/Civ.

Finally Consoli et al. (2016a), used the g/Civ ratio to

study the strength of silt mixed with high early

strength cement, using several molding conditions:

moisture between 17 and 23%, molding dry unit

weight between 14 and 16 kN/m3 and using 7 curing

days. In the study, normalized equations were devel-

oped to estimate qu and qt as a function of x and g/Civ,

and potential growth in strength was observed between

17 and 23%.

Under normalized conditions, Consoli et al.

(2011, 2016a) and Stracke et al. (2012) did not

establish the limits in which the molding moisture

content increases or decreases the strength of stabi-

lized soils in terms of g/Civ. Thus, this study

determines these limits, using several molding condi-

tions and expanding the experimental program of the

previously mentioned studies. For this purpose,

molding moistures were studied from 14.67 to

33.34%, and the dry unit weight of molding from 13

to 16 kN/m3, using silt from the Guabirotuba Forma-

tion of Curitiba/Brazil, stabilized with cement con-

tents from 3 to 9%, at 28 curing days. Other aspects

approached in this study were: calculation of equa-

tions that control qu and qt as a function of g/Civ;

calculation of empirical ratios between

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tensile/compression (qt/qu) of the mixtures, for each

moisture content used; and determination of dosage

equations to estimate the strength of the mixtures.

2 Background

The porosity/binder (g/Biv) ratio is a relationship

between void and binder volumes in a blend with the

soil. Porosity/binder ratio is a rational criterion to

study the mechanical properties (unconfined compres-

sive-UCS, split tensile, stiffness, and shearing) of

lime–soil, soil–cement, lime–soil–fly ash, soil–ce-

ment–fibers, and crushed reclaimed asphalt pave-

ment–lime mixes, among others (Henzinger et al.

2018). The relationship g/Biv was introduced in the

literature by Consoli et al. (2007) to study the

evolution of UCS for soil–cement mixes. The g/Biv

was extended to study the initial shear modulus and the

effective Mohr–Coulomb strength parameters of an

artificially cemented sand (Consoli et al. 2009c), the

strength parameters of a sandy clay treated with lime

and cement (Consoli et al. 2009a), the compressive

properties of sand–cement blends (Rios et al. 2012),

the study of Jet Grouting mechanicals properties

(Tinoco et al. 2012), the influence of grain size and

mineralogy on the porosity/cement ratio and the

correlation of this ratio with the mechanical behavior

of different soils (Rios et al. 2013), the compressive

strength of residual soil–fly ash–lime blends (da Rocha

et al. 2014), the compressive properties of lime

stabilized sandy clay using distinct molding moisture

content (Consoli et al. 2014; Baldovino et al. 2018b),

the shear behavior of an artificially cemented soil

(Rios et al. 2014), the UCS of zeolite and cement

addition on a sandy soil (Mola-Abasi and Shooshpasha

2016), the UCS and split tensile strength for non-

plastic clayey sand–cement mixes reinforced with

polypropylene fibers (Festugato et al. 2017), the

theoretical derivation of artificially cemented granular

soils strength (Diambra et al. 2017), the effect of water

salinity in lime-fly ash treated sand (Karim et al.

2017), the split tensile/compressive ratio of long-term

lime–soil mixes (Baldovino et al. 2018a), the uncon-

fined compressive strength evolution of sedimentary

silt-roof tiles waste mixes (Moreira et al. 2019a), the

equations controlling split tensile/compressive

indexes for silts-cement compacted blends using

different compaction efforts (Baldovino et al.

2019a, 2019b), the strength of homogeneous and

non-homogeneous mixtures of fine-grained soil with

lignite fly ash (Henzinger et al. 2018) and the strength

of reclaimed asphalt pavement–fly ash–carbide lime

blends (Consoli et al. 2018b). The g/Biv is also a

parameter to study durability properties of soil-binder

mixes: sandy soils stabilized with waste glass and

carbide lime (Consoli et al. 2018c), compacted gold

tailings—cement mixes (Consoli et al. 2018a) and

compacted clay-industrial wastes blends (Consoli

et al. 2017a). In all the above-mentioned studies, g/Biv is a suitable parameter to predict the unconfined

compressive, split tensile, stiffness, and durability of

stabilized soils. The general equation (Eq. 1) for

studying the evolution of these properties (compres-

sive and split tensile, mainly) is given by:

qu _ qt ¼ Ag

Civð ÞC

" #�B

ð1Þ

where A, B, and C are empirical constants, with A

having the same units as qu and qt (in kPa). When the

mixtures are evaluated depending on the cure time,

‘‘A’’ values usually increase (Consoli et al. 2014;

Baldovino et al. 2018a).

Recent studies have addressed B and C values

under normalized conditions for various soil types.

Consoli et al. (2017c) used seven different silty/clayey

soils (London clay, Dispersive clay, Botucatu resid-

ual soil, Organic soft clay, Red silty clay, Silt Gold

tailings, and Coal fly ash) mixed with early strength

Portland cement (1–9% cement content regarding the

dry weight of the soil) and different dry molding unit

weights (5–19 kN/m3) at curing periods ranging from

3 to 28 days. For all silty/clayey soils studied,

B = 3.85 and C = 0.28 were calculated. Then, Consoli

et al. (2017b) studied the UCS for four different fine-

grained soils: Botucatu residual soil, Osorio sand with

10% fines (crushed sand), Osorio sand with 30% fines

(crushed sand), and Osorio sand with 50% fines

(crushed sand), mixed with high early strength Port-

land cement—Type III ? Fibre (6 mm, 12 mm, and

24 mm) using different molding void ratio (0.34–0.66)

at 7 curing days, obtaining values for B = 2.45 and

C = 0.28. Finally, Consoli et al. (2016b) studied the

UCS and the tensile strength of four different sand

types: well-graded granitic sand, poorly graded sand

made from crushed basalt, silica sand obtained as a by-

product of agate polishing, and eolic, uniform Osorio

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sand, stabilized with general-purpose cement, early

strength cement, and low heat of hydration cement

(1–12% cement content regarding to the dry weight of

the sands) using curing periods from 2 to 28 days. For

sandy soils, B has taken a value of 1.38 and C of 1.00.

Thus, C value depends on the soil and type of binder

and takes values between 1.00 and 0.01. Values for C

close to 1.00 are most found for granular soils, where

the parameters g and Biv have the same magnitude

over qu and qt, and proportional variations in the

values of g and Civ cause qu and qt values to remain

constant [e.g., Consoli et al. (2007, 2017a)]. Values for

C close to 0.01 mean the influence of porosity (g) andvoids of the soil–binder mixture exerts a more

significant effect on qu and qt than the volumetric

content of binder so that an increase in porosity of a

proportionally higher binder content get bigger to

compensate the increased voids due to lack of

compaction and to maintain a constant mechanical

resistance (e.g., Consoli et al. 2009b, 2014; Baldovino

et al. 2018c). The empirical constant ‘‘B’’ assumes

negative values, which means that increases in

mechanical resistance are potential. Thus, it can be

verified how efficient parameter B has been to study

different types of soil stabilized with different types of

binders under different molding conditions (e.g.,

compaction efforts, water content, cure time, dry unit

weight).

3 Experimental Program

The experimental program was defined over the

previous study by Consoli et al. (2016a, 2017d);

Baldovino et al. (2018a) and according to the Brazilian

experience in cement–soil and soil–lime mixes

(Stracke et al. 2012; da Rocha et al. 2014; Festugato

et al. 2017). Thus, the experimental program was

divided into two stages. The first stage involved soil

and cement characterization tests. The soil granulom-

etry curve was obtained under ASTM D2487 (ASTM

2011a) and by laser analyzer for fine fraction.

Atterberg limits of the soil following ASTM 4318

(ASTM 2010), the specific gravity of the soil accord-

ing to ASTM D854 (ASTM 2014). One-dimensional

consolidation properties of soil using the ASTM

D2435/D2435M-11 (ASTM 2011b). The compaction

properties [Maximum Dry Density (MDD) and Opti-

mum Moisture Content (OMC)] of soil (in the three

efforts: standard, intermediate, and modified) were

conducted in agreement with Brazilian NBR 7182

(ABNT 2016). The direct soil shear parameters

(internal angle and cohesion) in the natural state were

obtained according to ASTM D3080-11 (2011c), and

the specific gravity of the cement according to NBR

16605 (ABNT 2017). The second stage consisted of

molding, curing, and rupture of the specimens sub-

jected to unconfined compressive and split tensile

tests. The unconfined compressive strength and split

tensile strength are the most commonly used mechan-

ical properties to study improved soils (or ground

improvement) according to recent studies (Mola-

Abasi and Shooshpasha 2016; Diambra et al. 2018;

Henzinger et al. 2018). The characteristics of the

materials and the methodology used in this article are

shown below.

3.1 Materials: Soil, Cement, and Water

In the present study, silty sedimentary soil, early

strength Portland cement, and distilled water were the

three materials used.

The soil sample was manually collected, in an

undeformed and deformed state, southeast of Curitiba

(Brazil), in the city of Sao Jose dos Pinhais (metropoli-

tan area of Curitiba), avoiding possible contamination,

and was taken in enough quantity to perform all the

tests. The soil was collected on a road slope and

extracted from a depth of about 2–2.5 m. The soil

belongs to the second layer of the Guabirotuba

Formation. The soils of the Guabirotuba geological

formation are located in Curitiba and its metropolitan

region and are predominantly fine-grained (clays and

silts). The undeformed samples were collected for

unconfined compressive, split tensile, one-dimen-

sional consolidation, and direct shear tests in the

natural state. The soil in its natural state presented

hygroscopic moisture of 40% and a dry unit weight of

11.60 kN/m3.

An early strength Portland cement (Type V in

Brazil) [ASTM C150 (ASTM 2016)] mainly com-

posed of calcium oxide (CaO), Silicon dioxide (SiO2),

and aluminum oxide (Al2O3), produced and sold in

southern Brazil, was used for the study.

To prevent undesired reactions and limit the

number of variables, distilled water at 24 ± 2 �Cwas used to conduct all characterization tests of soil

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and soil–cement mixtures as well as to mold the test

specimens.

The 10%, 30%, 50%, 60% and 90% finer particle

diameters of soil were measured as D10 = 0.003 mm,

D30 = 0.01 mm, D50 = 0.025 mm, D60 = 0.038 mm

and D90 = 0.3 mm. Moreover, the uniformity coeffi-

cient (Cu) and coefficient of curvature (Cc) were

measured as Cu = 8.33 and Cc = 1.33, from which the

soil was characterized as elastic silty with sand (MH)

in accordance with the Unified Soil Classification

System (USCS) criterion. The results of the soil and

cement characterization tests, performed as described

in the experimental program, are presented in Tables 1

and 2, respectively. Table 1 shows that the largest soil

size corresponds to 60% silt. The specific gravity is

2.62 and 3.11 to soil sample and cement, respectively.

The predominant color of the soil is yellow due to the

oxidation and important presence of goethite in the

subtropical climate in southern Brazil (Baldovino

et al. 2019a). In addition, the total quantitative

chemical composition of soil was acquired by

energy-dispersive X-ray spectroscopy (EDX) using

Table 1 Properties of the soil sample

Properties Value Standard

Liquid limit (%) 50.82 ASTM 4318 (ASTM 2010)

Plastic limit (%) 35.96

Plastic index (%) 14.86

Specific gravity of soil (Gs) 2.62 ASTM 854 (ASTM 2014)

Coarse sand (0.6 mm\ diameter\ 2 mm) (%) 5 NBR 6502 (ABNT 1995)

Medium sand (0.2 mm\ diameter\ 0.6 mm) (%) 12

Fine sand (0.06 mm\ diameter\ 0.2 mm) (%) 18

Silt (0.002 mm\ diameter\ 0.06 mm) (%) 60

Clay (diameter\ 0.002 mm) (%) 5

Effective size (D10) (mm) 0.003

Mean particle diameter (D50) (mm) 0.038

Uniformity coefficient (Cu) 8.33

Coefficient of curvature (Cc) 1.33

Classification (USCS) MH

UCS-natural state (kPa) 104.58

STS-natural state (kPa) 16.62

STS/UCS ratio-natural state 0.16

Preconsolidation pressure (r0c) (kPa) 300 D2435/D2435M-11 (ASTM 2011b)

Coefficient of consolidation (Cv) (cm2/s) 0.02

Internal friction angle-natural state (/) (degrees) 26 ASTM D3080-11 (ASTM 2011c)

Cohesion-natural state (kPa) 23

Color Yellow

Table 2 Chemical composition and some physical properties

of cement

Property Value

Al2O3 (%) 4.30

SiO2 (%) 18.96

Fe2O3 (%) 2.95

CaO (%) 60.76

MgO (%) 3.26

SO3 (%) 3.18

Insoluble residue (%) 0.77

Strength at 7 days (MPa) 44.7

Strength at 28 days (MPa) 54.2

Fineness (%) 0.04

Specific gravity 3.11

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an energy-dispersive X-ray fluorescence spectrometer.

Table 3 exhibits the chemical composition of the soil

sample, mainly SiO2, Al2O3, and Fe2O3, which are

usually found in sedimentary soils and participate

actively in the soil chemical stabilization process

(Moreira et al. 2019b).

3.2 Split Tensile and Unconfined Compressive

Strength Program

To define the molding points, the soil compaction tests

were carried out in three efforts: normal, intermediate

and modified, in accordance with the Brazilian

standard NBR 7182 (ABNT 2016) to find the

compaction properties (optimum moisture content

and maximum dry unit weight) of the soil, and the

results are presented in Fig. 1. The molding points

were established after plotting the compaction soil. In

order to study the influence of the dry molding unit

weight, moisture content, and porosity on the mechan-

ical strength of the cement-improved soil, the molding

points were delimited according to Fig. 1 and Table 4.

Variating the molding conditions gets the voids and

porosity to vary, and then changes in mechanical

properties of compacted soils. These molding points

were strategically defined considering possible field

conditions, without exceeding the modified energy

and optimum moisture content of all efforts. During

the mixing process, it was verified that the lowest

moisture percentage in which the specimens could be

molded was superior to 14%. The first attempts were

made with x = 10%, but the specimens broke effort-

lessly because the soil–cement particles in the pres-

ence of so little water could not adhere enough.

Therefore, the first molding point was chosen at

x = 14.67%, with variations of 4.67% up to

x = 33.34%. To study the effects of these non-optimal

compaction conditions on the mechanical strength of

soil–cement mixes, 28 curing period was chosen.

Figure 2 shows the experimental program chart.

3.3 Molding Specimens for Split Tensile

and Unconfined Compressive Tests

Test specimens, with a 100 mm height and 50 mm

diameter, were molded for unconfined compressive

and split tensile tests. The soil was dried in a heating

chamber at a temperature of 100 ± 5 �C and divided

into evenly distributed portions to be mixed with

different cement contents. The percentages of cement

chosen for this research were: 3, 5, 7, and 9% to the dry

mass of the soil, taking into account current literature

and Brazilian experience (Consoli et al. 2016a). Thus,

a quantity of dry cement was added to achieve the four

different addition contents (Fig. 3a). The mixture of

soil and cement was prepared to be homogenous to the

maximum extent. Subsequently, a percentage of water

was added, determined regarding the water content of

the molding points (i.e., non-optimal conditions of

compaction) shown in Table 4.

The samples for molding the test specimens were

statically compacted with a 50 mm internal diameter,

100 mm height, and 5 mm thick stainless-steel mold.

12.00

12.50

13.00

13.50

14.00

14.50

15.00

15.50

16.00

16.50

17.00

0 3 6 9 12 15 18 21 24 27 30 33 36 39

Dry

Uni

t Wei

ght (

kN/m

3 )

Moisture content, ω (%)

Standard effort

Intermediate effort

Modify effort

S=100%

Molding points

A1

A2

A3 B3C3

B2 C2 D3

D2

B1

C1 D1 E1

E2

Fig. 1 Compaction properties of soil sample and split tensile

and unconfined compressive strength program (molding points).

S degree of saturation of soil

Table 3 Soil sample chemical composition

Compost Concentration by weight (%)

SiO2 48.78

Al2O3 44.51

Fe2O3 0.61

K2O 0.84

TiO2 0.92

SO3 4.12

LOI 0.16

LOI loss on ignition

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The specimens were extruded from their molds using a

hydraulic device. An example of compacted specimens

is presented in Fig. 3b. To ensure the maximum dry

density obtained during the compaction tests, the mold

volume and weight of the wet mixture necessary for

each test specimen were calculated. The time taken to

prepare, mix, and compact the specimens were always

lower than 10 min, to avoid the early reactions of

cement in water’s presence. The test specimens were

weighed on a 0.01 g precision scale, and the dimensions

were measured using a caliper with a 0.01 mm error.

Three wet samples of the mixture were taken to check

the mold moisture by oven drying. Thus, the initial

specimen�s porosity was calculated using Eq. (2)

g ¼ 100�100cd

1þ C=100ð Þ

� �� 1

cSSþ C=100

cSC

� �� �ð2Þ

where cSS and cSC are the specific gravity of the soil

and cement grains, respectively. Equation (2) was

previously defined by Baldovino et al. (2019a) and

Fig. 2 Experimental program chart

Table 4 Molding points for soil–cement mixes

Molding point Dry unit weight (kN/m3) Moisture content (%) Degree of saturation/% Specimens (for qt and qu)

A1-Line A 13.00 14.67 0.37 24

A2-Line A 14.50 14.67 0.46 24

A3-Line A 16.00 14.67 0.58 24

B1-Line B 13.00 19.33 0.49 24

B2-Line B 14.50 19.33 0.62 24

B3-Line B 16.00 19.33 0.78 24

C1-Line C 13.00 24.00 0.61 24

C2-Line C 14.50 24.00 0.77 24

C3-Line C 16.00 24.00 0.98 24

D1-Line D 13.00 28.67 0.73 24

D2-Line D 13.75 28.67 0.83 24

D3-Line D 14.50 28.67 0.94 24

E1-Line E 13.00 33.34 0.86 24

E2-Line E 13.75 33.34 0.96 24

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Consoli et al. (2018a). The extracted test specimens

were wrapped in a transparent plastic film to maintain

the moisture content. Finally, the test specimens were

stored in a humidity chamber for the curing process for

27 days, at an average temperature of 25 ± 3 �C and

relative humidity above 95%, to prevent significant

changes in the moisture until the testing day. After 27

curing days, the specimens were submerged in a

distilled water tank for 24 h (1 day), expecting to

saturate the samples prior to compression and tensile

tests and trying to minimize the possibility that suction

would influence the final strength value. This proce-

dure has been used in the current literature to reduce

the effect of suction (Consoli et al. 2007; da Rocha

et al. 2014). Additionally, the moisture content in the

soil–cement mixes was cross-checked by oven drying

after the completion of the UCS and STS tests.

The following maximum errors were taken into

account when conducting the unconfined compressive

and split tensile tests for the samples: sample dimen-

sions with a diameter of ± 0.5 mm and height of ±

1 mm, dry unit weight (cd) of ± 1%, and water

content (x) of ± 0.5% (Consoli et al. 2009b, 2018c;

Baldovino et al. 2018a). For each molding point and

cement content, three test specimens were molded.

Three replicate samples were tested for each com-

paction state to verify repeatability in UCS and STS

results. 168 test specimens were molded for each of

the tests (unconfined compressive and split tensile),

making a total of 336 samples.

3.4 Split Tensile and Unconfined Compressive

Tests

To perform the unconfined compressive and split

tensile tests, an automatic press was used along with

rings calibrated for a 30 kN axial load. The tests were

conducted using an automated system at a test speed of

1 mm/min to measure the applied force with a

resolution of 2.5 N and strain with a sensitivity of

0.01 mm. The procedures for the unconfined com-

pressive tests followed ABNT (2007). UCS is the

maximum rupture load of the material or the pressure

corresponding to the load at which a specific defor-

mation to the 20%-soil test specimen occurs when the

axial stress–strain curve does not exhibit a maximum

peak. When the axial stress–strain curve exhibited a

maximum peak in a test, the UCS (qu) was selected by

the following expression:

qu ¼PR

AT

ð3Þ

where PR is the rupture load at the peak of the axial

stress–strain curve, and AT is the corrected cross-

sectional area of the test specimen. Tensile strength is

an essential parameter in predicting the suitability of a

subgrade material in pavement construction. The split

tensile strength tests comply with the Brazilian

standard NBR 7222 (ABNT 2011). Split tensile

strength qt was adopted according to the following

expression:

qt ¼2PRd

pDHð4Þ

Fig. 3 a Raw materials. b Soil–cement specimens for UCS and STS tests

123

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where PRd is the rupture load at the peak of the

diametrical stress–strain curve, and D and H are the

diameter and height of the test specimen, respectively

(Baldovino et al. 2018a). The split tensile test, also

known as the indirect tensile test or Brazilian Test, was

developed independently in Brazil and Japan in 1943.

The test is performed by applying a compression load

in a cylindrical specimen positioned between two

rectangular pieces with dimensions determined as a

function of the specimen diameter and positioned

diametrically opposite from each other. The test

mechanism is carried out as follows: in addition to

causing compression, the conditions imposed by the

load on elastic materials also produce a practically

uniform tensile stress over a significant area of the

diametrical plane containing the applied load.

4 Results and Discussion

4.1 Effects of Porosity/Cement Ratio

on Unconfined Compressive and Split Tensile

Strength

The porosity/volumetric cement content ratio (g/Civ)

was used in this study to verify the evolution of

unconfined compressive strength and split tensile

strength. The g/Civ ratio is defined regarding the

voids of soil–cement and the volume of cement used in

the mixture under the initial molding conditions

previously defined (Fig. 1 and Table 4). Porosity is

calculated as an initial condition of the soil–cement

matrix at a pre-established dry unit weight cd and the

desired moisture content. Therefore, the mechanical

resistance of the soil–cement matrix might happen as a

direct relation of the specimens’ porosity, as well as a

function of the inverse of the volumetric content of

cement (1/Civ), as demonstrated by Consoli et al.

(2009b) and Henzinger et al. (2018). To find a direct

and compatible alignment between g and Civ as a

mathematical ratio and convert the two variables as a

dependency for qu and qt, Civ value should be set as an

exponent C between 0.01 and 1.00 with variations of

0.01, as observed in the current literature (Festugato

et al. 2017; Consoli et al. 2017d; Diambra et al. 2018).

In this way, the C value that best fits the values of quand qt for this experimental program was 0.44. This

value means that the influence of porosity (g) and the

voids in the soil–cement mixture has more significant

impact in UCS and STS than the cement volumetric

content so that an increase in porosity needs a

proportionally more substantial increase in cement

content, in order to compensate the increase in voids

due to lack of compaction and to maintain constant

strength (Leon 2018). Values for C close to 1.00 are

most commonly found for granular soils, where the

parameters g and Civ exert the same magnitude on quand qt, in which proportional variations in g and Civ

values cause constant qu and qt values (Rios et al.

2013). In other words, to ensure high strength to

cement mixtures with granular soils, both the voids

and the volume of cement have the key to reach a

specific value for qu and qt. However, for cement

mixtures with fine-grained soils (silts and clay), the

crucial to achieving high strength is to apply high

compaction energy or significantly increase the

cement amount.

Figures 4, 5, 6, 7 and 8 show the influence of g/Civ

ratio (adjusted to 0.44) on unconfined compressive

strength and split tensile strength for the samples with

molding moisture contents of 14.67, 19.33, 24.00,

28.67, and 33.34%, respectively. The g/Civ0.44 ratio

0

500

1000

1500

2000

2500

3000

3500

20 25 30 35 40 45 50

q tan

d q u

(kPa

)

η/Civ0.44

UCSSTS

: qu= 51×106(η/Civ0.44)-3.30 (R2=0.97)

: qt= 6.9×106 (η/Civ0.44)-3.30 (R2=0.95)

qt/qu =0.135

Fig. 4 Influence of porosity/volumetric cement content (g/Civ)

ratio on split tensile strength (qt) and unconfined compressive

strength (qu) for silty soil–cement mixes, considering all studied

dry unit weights, distinct cement contents, and moisture content

of 14.67% (Line A)

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influences qu and qt directly under all molding

conditions, presenting a potential trend of g/Civ-quand g/Civ-qt. So, when the g/Civ values decrease due

to the voids reduction or the cement volume increase

in the mixture, the strength values of the specimens

increase. As noted in Figs. 4, 5, 6, 7 and 8, to increase

qu by 1000 kPa, g/Civ should be reduced by 5%. As

for qt, this same reduction might generate a significant

increase of 150 kPa.

Figure 4 shows the results for qu and qt in the

molding line A (x = 14.67%), with maximum value

for qu of 2110 kPa and 320 kPa for qt. For molding

line B (x = 19.33%), maximum values of 2560 and

400 kPa were attained for qu and qt, respectively, as

presented in Fig. 5. Ultimately, for line C

(x = 24.00%), maximum strengths for qu and qt of

3000 and 500 kPa were obtained, respectively

(Fig. 6). The maximum values for qu and qt (Line A,

B, and C) were obtained for the same value of g/Civ

0.44 = 21 (or g/Civ = 9.4). That is, there was an

increase in both qu and qt as the amount of water added

in the mixture increased to a set value of g/Civ and the

same variation of cd (Table 4) between 14.67% and

0

500

1000

1500

2000

2500

3000

3500

20 25 30 35 40 45 50

q tan

d q u

(kPa

)

η/Civ0.44

UCS

STS

: qu= 64.6×106(η/Civ0.44)-3.30 (R2=0.97)

: qt= 8.9×106 (η/Civ0.44)-3.30 (R2=0.95)

qt/qu =0.138

Fig. 5 Influence of porosity/volumetric cement content (g/Civ)

ratio on split tensile strength (qt) and unconfined compressive

strength (qu) for silty soil–cement mixes, considering all studied

dry unit weights, distinct cement contents, and moisture content

of 19.33% (Line B)

0

500

1000

1500

2000

2500

3000

3500

20 25 30 35 40 45 50

q tan

d q u

(kPa

)

η/Civ0.44

UCS

STS

: qu= 76×106(η/Civ0.44)-3.30 (R2=0.95)

: qt= 12.4×106 (η/Civ0.44)-3.30 (R2=0.99)

qt/qu =0.163

Fig. 6 Influence of porosity/volumetric cement content (g/Civ)

ratio on split tensile strength (qt) and unconfined compressive

strength (qu) for silty soil–cement mixes, considering all studied

dry unit weights, distinct cement contents, and moisture content

of 24% (Line C)

0

500

1000

1500

2000

2500

3000

3500

20 25 30 35 40 45 50

q tan

d q u

(kPa

)

η/Civ0.44

UCSSTS

: qu= 80×106(η/Civ0.44)-3.30 (R2=0.98)

: qt= 12.7×106 (η/Civ0.44)-3.30 (R2=0.99)

qt/qu =0.159

Fig. 7 Influence of porosity/volumetric cement content (g/Civ)

ratio on split tensile strength (qt) and unconfined compressive

strength (qu) for silty soil–cement mixes, considering all studied

dry unit weights, distinct cement contents, and moisture content

of 28.67% (Line D)

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24.00%. For line D (x = 28.67%), the maximum

values of 1720 and 331 kPa were observed for qu e qt,

respectively (Fig. 7) (for g/Civ = 11.7). Finally, for

line E (x = 33.34%), maximums of 1080 and 175 kPa

were found for qu and qt, respectively, for a defined

value of g/Civ = 13.2 (Fig. 8).

According to the molding points established in

Table 4, the g/Civ0.44 ratio was limited between the

values of 22 and 46.5 for molding moisture contents

between 14.67 and 24% (between lines A and C). As

for Lines D and E, the g/Civ0.44 range of the specimens

was (25–46.5) and (27.2–46.5), respectively. The g/Civ value increased due to the reduction in the dry unit

weight of the samples. Although there was a change in

the g/Civ ratio, its potential growth trend was main-

tained due to the change in moisture and the

water/compaction cement ratio. The potential trend

was excellently set for the experimental points, which

was demonstrated by the elevated determination

coefficient values higher than 0.92 (see Figs. 4, 5, 6,

7, 8).

It was observed that, in Figs. 4, 5, 6, 7 and 8, the

potential equations that describe the growth of qu and

qt follow the form: qu ¼ A� gCciv

h i�B

and

qt ¼ A� gCciv

h i�B

, respectively, where A, B, and C

are constants. The value of A might depend on curing

time, molding moisture as well as cementing or

binding agent (e.g., lime, cement, and fly-ash). For this

study, A value changes depending on the molding

moisture, with moisture contents in the following

order: A (x = 14.67%)\A (x =19.33%)\A

(x =24.00%)\A (x =28.63%)[A (x =33.34%). The equa-

tions presented in Figs. 4, 5, 6, 7 and 8 obtained the

same value for C and B, both for qu and qt. The only

difference between these equations is the value of A

(in the same units if qu and qt - kPa). For compressive

values, A ranges from 51 9 106 and 80 9 106 kPa

(variation of 57%) and, for tensile values, it ranges

from 6.9 9 106 and 12.7 9 106 kPa (variation of

84%). This means that the strength of the soil–cement

mixtures has more considerable additions in terms of

tensile strength than unconfined compression.

Figures 4, 5, 6, 7 and 8 show that, for the same

value of g/Civ, qu gets a different value for each

molding moisture content, and the highest values were

obtained in line D, followed by Line C, Line E, Line B,

and Line A, which demonstrates the superiority of the

28%moisture to provide greater silty soil strength. For

(Rios et al. 2012; Mola-Abasi and Shooshpasha 2016;

Festugato et al. 2017; Diambra et al. 2018), the g/Civ

ratio proved to be an excellent setting parameter to

describe the unconfined compressive behavior of

cement-stabilized soils.

4.2 Empirical Relationships Between Unconfined

Compressive And Split Tensile Strength

An empirical relation between compressive and split

tensile strengths can be calculated in terms of molding

moisture of soil–cement samples. This relation can be

called n ¼ qt

quand is independent of the g

Civð Þ0:44 ratio.

Thus, the equations that describe the growth of qu and

qt as a function ofg

Civð Þ0:44 (see Figs. 4, 5, 6, 7, 8) can be

expressed as a direct ratio of qt/qu for each molding

moisture content outlined in Table 5. The qt/qu ratio

ensures a decimal constant, calculated in Table 5,

which also shows the equations representing the

increase of qu and qt, with a potential trend for each

value ofx. Therefore, n gets values between 0.135 and0.163 (variation of 3%). The calculated values of n

0

500

1000

1500

2000

2500

3000

3500

20 25 30 35 40 45 50

q tan

d q u

(kPa

)

η/Civ0.44

UCSSTS

: qu= 71×106(η/Civ0.44)-3.30 (R2=0.92)

: qt= 9.9×106 (η/Civ0.44)-3.30 (R2=0.96)

qt/qu =0.139

Fig. 8 Influence of porosity/volumetric cement content (g/Civ)

ratio on split tensile strength (qt) and unconfined compressive

strength (qu) for silty soil–cement mixes, considering all studied

dry unit weights, distinct cement contents, and moisture content

of 33.34% (Line E)

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grow from x = 14.67 to x = 24.00% and decrease

from x = 28.67 to x = 33.34%, as shown in Fig. 9.

Thus, qt proves to be a percentage of 13.5, 13.8, 16.3,

15.9, and 13.9% of the value of qu for lines A, B, C, D,

and E, respectively.

According to Diambra et al. (2018), in artificially

cemented sandy soils, the existence of a tensile/com-

pressive strength ratio (qt/qu) is independent of the

curing time. The ratio is mainly ruled by the tensile

strengths (or properties of friction) of cement. Authors

such as Consoli et al. (2016a, b) calculated a qt/qu ratio

of 0.13 for compacted fine-grained soil-Portland

cement blends using molding moisture contents of

17, 20, and 23%, and dry unit weights between 14 and

16 kN/m3. Festugato et al. (2017) mixed sandy soil

with cement and monofilament polypropylene fiber;

they calculated a n value of 0.10 for the non-fiber soil

and the fiber-reinforced soil they found a value of

n = 0.15, using a ratio of g

Civð Þ0:28. Other authors such

as Anggraini et al. (2015) determined a direct ratio of

n = 0.16 for soft, coconut-fiber-reinforced, lime-

treated soil. For Correia et al. (2015), there is a

decrease in the qt/qu ratio (from 0.20 to 0.24) with

increasing amounts of cement-slag-fiber in the same

mixture. Finally, Muntohar et al. (2013) studied the qt/

qu ratio for lime-stabilized and fiber-reinforced soil.

The addition of fibers to the stabilized soil slightly

increased the n value from about 0.11 to 0.13,

increasing the fiber content from 0.1 to 1.2%. Thus,

the ratio of strength n for cemented/reinforced soils

varies between 10 and 20% on average. Consequently,

the empirical qt and qu ratios reported in this study are

within these ranges.

4.3 Normalization of qt and qu Strengths to Assess

the Optimum Moisture Content of the Mix

in g/Civ Ratio

The equations shown in Table 5 can be normalized in

terms of g/Civ for equal molding moisture values.

Potential equations describing the growth of qu and qtas a function of g/Civ can be divided by the same value

of 106 � g

Civð Þ0:44� ��3:30

, thus, ensuring a constant

calculated for its corresponding molding moisture

value, both for qu and qt. Therefore, if the moisture

correlates with its respective normalized constant (qu

divided by 106 � g

Civð Þ0:44� ��3:30

or qt divided by

Table 5 Equations controlling split tensile/compressive

strength ratio of silty soil–cement mixes for distinct molding

moisture contents

Moisture content (%) Equations for qt-qu and qt/qu ratio

14.67

n ¼ qt

qu¼

6:9�106g

Civð Þ0:44

" #�3:30

51�106g

Civð Þ0:44

" #�3:30 ¼ 0:135

19.33

n ¼ qt

qu¼

8:9�106g

Civð Þ0:44

" #�3:30

64:6�106g

Civð Þ0:44

" #�3:30 ¼ 0:138

24.00

n ¼ qt

qu¼

12:4�106g

Civð Þ0:44

" #�3:30

76�106g

Civð Þ0:44

" #�3:30 ¼ 0:163

28.67

n ¼ qt

qu¼

12:7�106g

Civð Þ0:44

" #�3:30

80�106g

Civð Þ0:44

" #�3:30 ¼ 0:159

33.34

n ¼ qt

qu¼

9:9�106g

Civð Þ0:44

" #�3:30

71�106g

Civð Þ0:44

" #�3:30 ¼ 0:139

0

0.05

0.1

0.15

0.2

0 5 10 15 20 25 30 35 40

ξ=q t

/qu

ω ω (%)

Fig. 9 Variation of unconfined compressive strength (qu)-split

tensile strength (qt) ratio (n = qt/qu) with distinct molding

moisture content (x)

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106 � g

Civð Þ0:44� ��3:30

), a point is found on the Carte-

sian plane. Thus, the variation of qu and qt normalized

depends on the moisture content (Fig. 10). This

variation follows a polynomial trend represented by

the form:

qu _ qt ¼ �aix3 þ aiix

2 � aiiixþ aiv� �

kg

Civð ÞC

" #�B

ð5Þ

where ai, aii, aiii and aiv are constants that depend on

the polynomial trend, x is the molding moisture

content, and k is a normalization-dependent constant,

which, in this case, is equal to 106. Thus, the equations

that allow calculating qu and qt strengths for any

molding condition limited by the variables of this

study are defined as:

qu ¼ � 0:0088x3 þ 0:46x2 � 5:11xþ 54:37� �� 106

g

Civð Þ0:44

" #�3:30

R2 ¼ 0:96� �

ð6Þ

qt ¼ � 0:0041x3 þ 0:25x2 � 4:43xþ 30:90� �� 106

g

Civð Þ0:44

" #�3:30

R2 ¼ 0:97� �

ð7Þ

Equations (6) and (7), which estimated the

strengths of the mixtures for any value of x, g, andCiv, have excellent coefficients of determination

R2 = 0.96 and R2 = 0.97, for qu and qt, respectively,

when validated to the real values of the 336 specimens

(real 9 calculated). Statistical analysis was per-

formed with real values and the estimated equations.

Themean absolute percentage error (MAPE, in%) and

the normalized root-mean-square error (NRMSE, in

%) were analyzed to validate the equations and the

coefficient of determination. For the 118 unconfined

compression data, percentages of 2.68% and 1.64%

were calculated for MAPE and NRMSE, respectively.

For the 118 tensile samples, percentages of 3.18% and

1.60% were calculated for MAPE and NRMSE,

respectively. Overall, the statistical analysis shows

excellent fits and high quality of the normalized model

used in this study. TheMAPE and NRMSE parameters

indicate an error close to 3% of the model. The (g) andvolumetric content of cement (cement volume in terms

of the sample volume) are optimal predictor variables

of the mechanical resistance for cement-compacted

silt. Parameter R2 had average results of 96.5% in all

developed equations and, simultaneously with other

statistical parameters, indicates that the molding

values and the soil–cement mixtures conditions [dry

unit weight, binder content, curing time, moisture, and

curing temperature] are excellent to estimate qu and qtin any of these molding situations.

Conversely, in Fig. 10, there is an ‘‘optimum’’

normalized maximum of qt and qu divided by

106 9 (g/Civ0.44)-3.30, where the maximum strengths

of the soil–cement mixtures are obtained. Thus, from

the first partial found from Eqs. (6) to (7), the

‘‘normalized optimal moisture content’’ can be calcu-

lated as a function of g/Civ0.44. The normalized

optimum value for any molding condition for qu isx�28% and x � 28% for qt; therefore, an empirical ratio

of n = 0.16 was also achieved (See Fig. 9). Although a

higher value for the equation qu _ qt ¼ A� gCciv

h i�B

is

found at point x = 28% (A achieves a value of 81�106

qu = [-0.0088ω3+0.46ω2 -5.11ω +54.37]×106[η/Civ

0.44]-3.30

qt = [-0.0041ω3 +0.25ω2 -4.43ω +30.97]×106[η/Civ

0.44]-3.30

0

10

20

30

40

50

60

70

80

90

10 15 20 25 30 35

q tan

d q u

divi

ded

by 1

06 (η/C

iv0.

44)-3

.30

Moisture content, ω (%)

Opt

imum

moi

stur

e co

nten

t to

mix

at

η/(C

iv0.

44)0.

33in

dex

→ω

=28%

Fig. 10 Variation in normalized unconfined compressive

strength (qu) and split tensile strength (qt) with distinct molding

moisture content (x)

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for qu and of 13�106 for qt), there is a limitation

regarding the degree of saturation reaching real

strengths. Even though a theoretical 28% humidity

molding line could get higher strengths, they would be

limited by the reduction of gCciv

with a maximum of

cd = 15.25 kN/m3. Therefore, in theory [applying

Eqs. (6) and (7)], the maximum value reached in this

point would be of 2474 kPa and 415 kPa for qu and qt,

respectively, at 28 curing days and with 9% cement

added. As for point x = 23% (maximum of cd-= 16 kN/m3), the strengths of 3112 kPa (increase of

25% regarding x = 28%) and 492 kPa (increase of

18% regarding x = 28%) for qu and qt could be

achieved under the same conditions since they would

not be limited by the dry molding unit weight provided

in this study. Nevertheless, it should be mentioned that

changes in real field molding conditions could lead to a

higher/lower construction cost, such as pavement

layers, foundation supports, reinforcement of slopes

and dams.

4.4 Normalization of qt and qu Strengths to Assess

the Single Mixing Trend at g/Civ0.44 Ratio

The normalization (division) of the strengths is used to

find an equation able to estimate qu and qt as a function

of normalized g/Civ in a single potential trend.

According to Consoli et al. (2016b), to find an

equation to estimate cement-stabilized silty/argilla-

ceous soil using the g/Civ ratio, firstly, all normaliza-

tion strengths must be determined using a particular

value of g/Civ0.44 = r for each variable on which the

strengths depend (in this case, the molding moisture).

The particular value of r to normalize the strengths

can be chosen within the range reported in this

research, between 20 and 50, for each molding

moisture value of the soil–cement, both for split

tensile (qt-norm) and unconfined compression (qu-norm).

So, for this study, the value ofg/Civ0.44 = r = 35 was

chosen. The number r = 35 was replaced in the

equations that control qu and qt (shown in Table 5 and

in Figs. 4, 5, 6, 7, 8) to calculate normalization

strengths for each value of molding moisture (x). Thenormalization strengths for qu-norm with x values of

14.67 (Line A), 19.33 (Line B), 24.00 (Line C), 28.67

(Line D), and 33.34% (Line E), are 409.4, 518.6,

610.1, 642.2 and 569.9 kPa, respectively. The nor-

malization strengths for qt-norm with x values of 14.67

(Line A), 19.33 (Line B), 24.00 (Line C), 28.67 (Line

D), e 33.34% (Line E), are 55.4, 71.4, 99.5, 101.9 and

79.5 kPa, respectively. After calculating normaliza-

tion strengths, the strengths should be normalized over

the reported unconfined compressive and indirect

tensile values, which result in dividing the value of

unconfined compressive and tensile strength of each

specimen by the value of normalization strength of its

corresponding molding moisture (both for qu and qt).

Thus, normalization is obtained dividing Eq. (1) by

specific and arbitrary values of unconfined compres-

sive and tensile strengths, corresponding to a defined

porosity value g/CivC = r, which leads to:

qu

qu�normg

CC

iv

¼ r� _ qt

qt�normg

CC

iv

¼ r�

¼A g=CC

iv

� ��B

A rð Þ�B¼ rð ÞB g=CC

iv

� ��B ð8Þ

Therefore, with the value of r = 35, Eq. (8) is

converted into:

qu

qu�normg

C0:44

iv

¼ 35

� _ qt

qt�normg

C0:44

iv

¼ 35

� ¼ 124:5� 103 g=C0:44

iv

� ��3:30 ð9Þ

Normalized values of qu/qu norm e qt/qt-norm of all

specimens tested for unconfined compressive and

tensile strength of the type V PC in different moisture

contents acquire the same potential trend described in

Eq. (9). Values corresponding to normalized qu/qu-

norm e qt/qt-norm are shown in Fig. 11 with the

respective trend. The normalized values for the

mechanical resistance obtain a coefficient of determi-

nation of 0.95, being a single trend for all experimental

and normalized points, and for all moisture contents in

which the specimens were molded. Thus, if the sample

values of B and C are applied in Eq. (9), the expression

to estimate the mechanical behavior through tensile

and compressive tests for the studied silty soil and the

cement type used is converted into the form described

by Eq. (10)

qu

qu�normg

C0:44

iv

¼ r� _ qt

qt�normg

C0:44

iv

¼ r�

¼ rð Þ3:30 g=C0:44iv

� ��3:30 ð10Þ

123

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with ther value of a soil specimen studied and mixed

with cement and its respective result of qu e qt in a

determined curing time and moisture value, qu e qtbehavior can be estimated for any value of g/Civ, and

this equation may be used to conduct soil–cement

mixtures projects without the need for broad testing

programs, which demand time and money.

5 Concluding Remarks

According to the type of soil, cement, the methodol-

ogy, the presentation, and analyses of results used in

this study, the following conclusions can be drawn:

1. For all studied soil–cement mixtures, the reduc-

tion in initial molding porosity and the increase in

the quantity of cement caused an increase in split

tensile and unconfined compression strengths after

28 curing days.

2. In normalized terms of porosity/volumetric

cement content, the compressive and tensile

strengths of all soil–cement mixtures increased

up to 28%moldingmoisture (between Lines C and

D). Afterward, they decreased until 33.34% of

moisture (Line E).

3. It was possible to calculate the equations that

control qu and qt as a function of g/Civ (to the

power of 0.44) and the empirical ratios between

qu/qt. Empirical ratios varied depending on the

molding moisture used, from 0.135 to 0.163

(Table 5).

4. There is a single normalized potential trend of quand qt as a function of molding moisture and

apparent dry unit weights used. The single trend

(Eq. 9) can be extended to any high early strength

cement stabilized silty soil molding condition in

this study.

Acknowledgements The authors are thankful to the Federal

University of TechnologyParana and to the financial support

given by Coordination for the Improvement of Higher

Education Personnel (CAPES), Fundacao Araucaria do Parana

and National Council for Scientific and Technological

Development (CNPq) in Brazil. Finally, authors would like to

thank the anonymous reviewers for their in-depth comments,

suggestions, and corrections, which have greatly improved the

manuscript.

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