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Experimental and Numerical Studies of Blast, Fragmentation and Thermal Effects Mitigation of Energetic Materials Detonation By Khurshid Ahmed School of Chemical and Materials Engineering National University of Sciences and Technology 2021

EXPERIMENTAL AND NUMERICAL STUDIES OF BLAST, …

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Page 1: EXPERIMENTAL AND NUMERICAL STUDIES OF BLAST, …

Experimental and Numerical Studies of

Blast, Fragmentation and Thermal

Effects Mitigation of Energetic

Materials Detonation

By

Khurshid Ahmed

School of Chemical and Materials Engineering

National University of Sciences and Technology

2021

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Experimental and Numerical Studies of

Blast, Fragmentation and Thermal

Effects Mitigation of Energetic

Materials Detonation

Name: Khurshid Ahmed

Reg. No: 00000202572

This thesis is submitted as a partial fulfillment of the requirements

for the degree of

Doctor of Philosophy in Energetic Materials Engineering

Supervisor: Dr. Abdul Qadeer Malik

School of Chemical and Materials Engineering (SCME)

National University of Sciences and Technology (NUST)

H-12 Islamabad, Pakistan

June, 2021

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List of Publications

1. Ahmed K, Malik AQ, Ahmad IR. Heterogeneous lightweight configuration

for protection against 7.62 × 39 mm bullet impact. International Journal of

Protective Structures. 2019;10(3):289-305.

https://doi.org/10.1177/2041419619839216

2. Ahmed K, Malik AQ. Experimental studies on blast mitigation capabilities of

conventional dry aqueous foam. AIP Advances. 2020;10(6):065130.

https://doi.org/10.1063/5.0010283

3. Ahmed K, Malik AQ, Hussain A, Ahmad IR, Ahmad I. Lightweight

protective configurations against blast and fragments impact: Experimental

and numerical studies. AIP Advances.2020;10(9):095221.

https://doi.org/10.1063/5.0022982

4. Ahmed, K., Malik, A. Q., Hussain, A., Ahmad, I. R. and Ahmad, I. (2021)

Blast and Fragmentation Studies of a Scaled Down Artillery Shell-Simulation

and Experimental Approaches, The International Journal of Multiphysics,

15(1), pp. 49-71. https://doi.org/10.21152/1750-9548.15.1.49

Under Review

1. Ahmed K, Malik AQ. Experimental investigations of the response of a

heterogeneous container to blast, fragmentation and thermal effects of

energetic materials detonation, International Journal of Protective Structures.

2. Ahmed K, Malik AQ. Protective Container for Combined Blast,

Fragmentation and Thermal Effects of Energetic Materials Detonation,

Central European Journal of Energetic Materials (CEJEM).

International Conference

Ahmed K, Malik AQ, Ahmad IR. Heterogeneous lightweight configuration

for protection against 7.62 × 39 mm bullet impact, 5th

International

Conference on Protective Structures (ICPS5), Poznan, Poland, 19-23 August

2018

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i

DEDICATED TO MY

Dearest Family

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ii

Acknowledgments

All Commendations to Almighty Allah, The Most Beneficent, The Most Merciful,

Who blessed me with intellect and determination to accomplish this task. I would

like to express my deepest and sincere gratitude to my supervisor Dr. Abdul Qadeer

Malik for his valuable guidance and assistance throughout this research work. I can

never forget his keen interest, encouragements and unprecedented support during this

period. My special thanks to my co-supervisor Dr. Iram Raza Ahmad for his

continued technical and moral support to accomplish this work. My thanks are due to

GEC members, Prof. Dr. Arshad Hussain and Dr. Iftikhar Ahmad, for their guidance

and support. The support and cooperation of Dr Ahsan, Dr Sarah, Dr Tayyaba, Ms

Javeria and Ms Ayesha during this period is acknowledged and highly appreciated.

My humble gratitude to Prof. Muhamed Suceska for sharing EXPLO5 calculations

and his unconditional support during these years.

I would like to express my special thanks to Member Technical, PAEC, Mr. Aslam

Hayat and Dr. A. Ghani Akram for providing me this opportunity and their

everlasting support. My thanks to PAEC for meeting the financial requirements and

generous support during experimental work. I would also like to express my thanks

to my friends and colleagues Mr Muhammad Mursaleen, Ahmad Hashmi,

Muhammad Tariq, Mohsan Hassan, Dr. Sultan, Zahoor Sultan, M. Arshad, Khalid

Naeem, Kamran Arif, Fazle Hadi, Sameen Murtaza, Dr. Naveeda, Dr. Javaid, Dr.

Kamran, Kazim Hussain, M. Ashraf, Ajmal Hussain, Nusrat, Kamran and fellow

team members for helping me throughout these years and especially their support

during the experimental work. I also express my thanks to Atif Khurshid for his

assistance in review and computation work. My thanks are also due to Dr Shakeel

Abbas, Mr. Abdul Waheed, Mr Sammiullah and the experimental group for their

generous support in experimental work. I want to thank all the people who helped

and supported me during my PhD.

I would like to express my obedience to my parents and my family whose prayers

have led me to this stage and will accompany me for all future endeavors. It would

not have been easy to complete this work without their sacrifices, cooperation and

prayers.

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Abstract

The detonation of an energetic material (EM) is mainly manifested in the form of

blast, fragmentation and thermal effects. These effects are very destructive and cause

injuries-being fatal-and structural damage as well. The suppression or attenuation of

these effects is a prime focus. The present research is related to the concerted

investigations employing lightweight materials capable of mitigating the blast,

fragmentation and thermal effects of explosive devices including lighter improvised

explosive devices (IEDs). Commercially available shaving foam was characterized

and investigated as a potential mitigating material in combination with Kevlar woven

fabric, laminated glass fiber reinforced polymer (GFRP), Bakelite, Polyurethane

(PU)/expanded Polystyrene (EPS) foams and PU-silica to withstand the impact of

blast wave and explosively driven high velocity fragments.

Various amounts of C4 explosive (82, 104, 250 and 800 grams) were tested in air and

immersed in shaving foam. The shaving foam confinement suppressed the fireball

radius by 80% and quenched the afterburning reactions resulting from an EM

detonation. About 70% reduction in blast overpressure and 62% reduction in positive

impulse were observed for shaving foam confinements weighing 1.0 - 2.05 kg

against C4 explosives of 82 - 250 grams.

Lightweight protective configurations comprising different combinations of Kevlar

woven fabric, laminated GFRP, PU/EPS foams and alumina (Al2O3) tile were tested

against blast, fragments and bullet impact. Multi-layer composition of PU-silica and

a mixture of PU-silica and alumina powder were also studied. The protective

configurations were tested under static detonation of geometrically scaled down 155

mm artillery shell. Fragments weighing up to 4.3 grams with velocities in the range

of 961–1555 m/s were produced and impacted the configurations. The Kevlar woven

fabric, laminated GFRP and PU foam compositions provided significant absorption

and attenuation to impacting fragments. Configurations employing alumina tile were

able to resist perforation of 7.62 mm mild steel core (MSC) bullet and also withstood

the blast and multiple fragments impact without significant backface signatures

(blunt force trauma).

Numerical simulations were performed using ANSYS AUTODYN. SPH (Smoothed

Particle Hydrodynamics) solver was used for characterization of shell fragmentation.

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iv

Coupled SPH -ALE (Arbitrary Lagrangian-Eulerian) approach was used to simulate

the interaction of fragments with protective configurations. A coupled Euler-ALE

approach was employed to simulate blast wave propagation in air and loading on

protective configurations. The fragments mass, initial velocity and spatial

distributions were in good agreement with the experimental findings. The blast wave

parameters showed good match of the arrival time and peak pressure values with

measured data, however, a discrepancy in incident impulse was observed.

On the basis of experimental and simulation studies a model heterogeneous

containment system was developed to counter combined blast, fragmentation and

thermal effects of energetic material detonation of 1.0 kg bare and 0.6 kg of steel

cased TNT equivalent charge. The two layers container provided 97% overpressure

reduction as well as contained the high velocity fragments. The novel combination of

EPS foam, Bakelite and PU-silica layers provided protection against in contact C4

detonation at the base of the container. The upshot of this research work is that,

besides being of academic significance, it provides ample data to design a device to

combat terrorism against lighter time bomb/IEDs placed at public places, high profile

meeting venues and transportation systems (land, air etc.).

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Table of Contents

Acknowledgments ........................................................................................................ ii

Abstract ....................................................................................................................... iii

Table of Contents .......................................................................................................... v

List of Figures .............................................................................................................. ix

List of Tables ............................................................................................................ xvii

List of Acronyms and Symbols .............................................................................. xviii

Introduction........................................................................................... 1 Chapter 1

1.1 Motivation ...................................................................................................... 1

1.2 Energetic Materials ........................................................................................ 2

1.2.1 Low Explosives ...................................................................................... 2

1.2.2 High Explosives ...................................................................................... 2

1.3 The Rankine-Hugoniot Relations................................................................... 4

1.4 Equation of State ............................................................................................ 5

1.5 Formation of Blast Wave ............................................................................... 6

1.6 Scaling Laws .................................................................................................. 8

1.7 Effects of Cased Explosive Detonation ......................................................... 9

1.8 Literature Review ......................................................................................... 11

1.9 Gaps in Literature......................................................................................... 15

1.10 Objectives ................................................................................................. 16

1.11 Thesis Organization .................................................................................. 16

References ................................................................................................................... 17

Materials and Methodology for Blast Mitigation ............................ 21 Chapter 2

2.1 Introduction .................................................................................................. 21

2.2 Aqueous Foam ............................................................................................. 21

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2.2.1 DENIM Shaving Foam ......................................................................... 22

2.2.2 Microscopic and Viscosity Study ......................................................... 22

2.2.3 Sound Speed Measurement................................................................... 24

2.3 C4 Explosive ................................................................................................ 26

2.4 Diagnostic Tools .......................................................................................... 27

2.4.1 High-Speed Photography ...................................................................... 27

2.4.2 Pressure Transducers ............................................................................ 27

2.4.3 Arrival Time Sensors ............................................................................ 29

2.5 Experimental Work ...................................................................................... 30

2.5.1 Blast Mitigation with Shaving Foam .................................................... 30

2.5.2 Effects of Foam Volume and Liquid Content on Mitigation ................ 35

2.5.3 Blast Parameters at Z < 1.0 m/kg1/3

...................................................... 36

2.6 Numerical Modeling and Simulation ........................................................... 39

2.6.1 Material Modeling ................................................................................ 39

2.6.2 Blast Wave Parameters ......................................................................... 40

2.7 Results and Discussion................................................................................. 42

2.7.1 Fireball and Afterburning Suppression ................................................. 44

2.7.2 Peak Pressure and Impulse Reduction .................................................. 46

References ................................................................................................................... 50

Characterization of Shell Fragmentation ......................................... 52 Chapter 3

3.1 Introduction .................................................................................................. 52

3.1.1 Effects of Fragmentation ...................................................................... 53

3.2 Characterization ........................................................................................... 53

3.2.1 Experimental Work ............................................................................... 54

3.3 Numerical Simulation .................................................................................. 58

3.3.1 Material Modeling ................................................................................ 59

3.3.2 Fragmentation of Shell ......................................................................... 59

3.3.3 Blast Parameters for Shell Detonation .................................................. 62

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3.4 Experimental Results ................................................................................... 64

References ................................................................................................................... 71

Protective Configurations against Fragments .................................. 73 Chapter 4

4.1 Protective Mechanisms ................................................................................ 73

4.1.1 Momentum Disruption.......................................................................... 73

4.1.2 Shock Wave Spreading ......................................................................... 74

4.1.3 Shock Energy Absorption ..................................................................... 75

4.2 Protection against Fragments Impact ........................................................... 75

4.2.1 Protective Configurations ..................................................................... 76

4.2.2 Experimental Work ............................................................................... 77

4.3 Protection against Bullet Impact .................................................................. 84

4.3.1 Blunt Force Trauma Test ...................................................................... 85

4.4 Numerical Simulation .................................................................................. 87

4.4.1 Material Modeling ................................................................................ 87

4.4.2 Shell Fragmentation and Impact on Protective Configurations ............ 89

4.4.3 Coupled SPH-ALE Simulation ............................................................. 90

4.4.4 Blast Loading on Protective Configurations ......................................... 98

4.5 Experimental Results ................................................................................. 101

References ................................................................................................................. 107

Containment for Blast, Fragmentation and Thermal Effects .... 109 Chapter 5

5.1 Introduction ................................................................................................ 109

5.2 Materials and Experimental Work ............................................................. 109

5.2.1 Scaled down Container ....................................................................... 109

5.3 Numerical Simulation ................................................................................ 111

5.3.1 C4 Surface Burst Parameters .............................................................. 111

5.3.2 Fragments Impact on Scaled down Container .................................... 114

5.4 Experimental Results ................................................................................. 117

5.4.1 Scaled down Container Test ............................................................... 117

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5.4.2 Container Test with 1.0 kg TNT Equivalent Charge .......................... 122

5.4.3 Container Test with Steel Cased Charge (Pipe-bomb) ....................... 125

References ................................................................................................................. 132

Conclusions and Recommendations ................................................ 133 Chapter 6

6.1 Conclusions ................................................................................................ 133

6.2 Recommendations ...................................................................................... 135

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List of Figures

Figure 1-1 : Fatalities in terrorist violence in Pakistan, (2000-2018) [3] ..................... 1

Figure 1-2 : The detonation wave structure and pressure profile [10] ......................... 3

Figure 1-3 :Shock wave generation in a compressible fluid [12] ................................. 4

Figure 1-4 : Characteristics of a blast wave (a) ambient pressure (b) positive phase

(c) negative phase [13] .............................................................................. 6

Figure 1-5 : Devastating effects of energetic material detonation .............................. 11

Figure 1-6 : Blast inhibitor: 1-Elastic envelope, 2-liquid gas medium, 3-working

space and 4-HE [37] ................................................................................ 13

Figure 1-7: (a) Episafe container and (b) Resnyansky and Delany setup ................... 13

Figure 1-8 : Blastgard trash receptacle [63] ............................................................... 14

Figure 1-9 : TM International blast containment vessel [64] ..................................... 14

Figure 1-10 : Blast Containment Receptacle (BCRs) [65] ......................................... 15

Figure 2-1 : Denim foam-average bubble size (a) 15 µm at 0 hrs (b) 85 µm at 1 hrs 22

Figure 2-2: Denim foam-average bubble size (c) 120 µm at 2 hrs (d) at 24 hrs ........ 23

Figure 2-3: Gillette foam-average bubble size (a) 20 µm at 0 hrs (b) 105 µm at 1 hrs

(c) 155 µm at 2 hrs (d) at 24 hrs .............................................................. 23

Figure 2-4: The graphical representation of bubbles coarsening of conventional

aqueous foams (a) Denim (b) Gillette ..................................................... 24

Figure 2-5: Shear rate vs viscosity plot for shaving foam .......................................... 24

Figure 2-6: Setup for measuring sound speed in air ................................................... 25

Figure 2-7: Setup for measuring sound speed in shaving foam.................................. 25

Figure 2-8: Waveforms (a) in air (b) in shaving foam ................................................ 26

Figure 2-9: (a) Transducers orientation for Pr and Ps measurement (b) Components of

data acquisition (DAQ) system ............................................................... 28

Figure 2-10: (a) Arrival time sensor (b) section view (c) mounted in the fixture ...... 29

Figure 2-11: Comparison of Time of arrival with pressure transducer and

arrival time probe .................................................................................... 29

Figure 2-12: 2D view of Experimental Layout for blast parameters measurement ... 30

Figure 2-13: Test setup for measuring blast parameters for (a) bare charge (b)

immersed in shaving foam(c) Transducer orientation for measuring

reflected pressure .................................................................................... 31

Figure 2-14: High-speed images, 82g bare C4 detonation in air and propagation of

fireball ..................................................................................................... 31

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Figure 2-15: A sequence of events after detonation of charge immersed in shaving

foam ....................................................................................................... 32

Figure 2-16: (a) Reflected overpressure (b) Impulse plots for 82g C4 blast at 0.8 m

for bare charge and covered in shaving foam ........................................ 32

Figure 2-17: Test setup for measuring 82g C4 blast parameters for (a) bare charge (b)

covered in shaving foam at 0.85 m ........................................................ 33

Figure 2-18: (a) Incident overpressure and (b) Impulse profiles for 82g C4 bare and

covered in shaving foam at 0.85 m ........................................................ 33

Figure 2-19: (a) Pressure and (b) Impulse plots for bare 250g C4 blast at 1.0 m and

submerged in shaving foam ................................................................... 34

Figure 2-20: Test setup for measuring 250g C4 blast parameters for bare charge and

covered in 0.05 m3 shaving foam .......................................................... 35

Figure 2-21: Peak incident pressure for 250g Bare C4 and covered in shaving foam at

0.8m ....................................................................................................... 36

Figure 2-22: (a) Perspex channel filled with foam (b) Testing setup within shaving

foam ....................................................................................................... 36

Figure 2-23: Experimental setup for measuring blast parameters for Z < 1 (m/kg1/3

)

(a) sensors fixed inside empty Perspex channel (b & c) shaving foam

filled inside channel ............................................................................... 37

Figure 2-24: High-speed images of 200g C4 detonation inside Perspex channel (a)

just after detonation (b) fireball expansion (c) product gasses expansion

............................................................................................................... 37

Figure 2-25 : Pressure and scaled distance plots for HE detonation in shaving foam

for Z<1 ................................................................................................... 38

Figure 2-26: (a) Pressure and (b) Impulse plots for 200g C4 charge detonated inside

shaving foam at 0.25 and 0.30m from charge face ................................ 38

Figure 2-27: (a) ANSYS AUTODYN model (b) expansion of detonation product

gases after detonation of 250g C4 ......................................................... 41

Figure 2-28: (a) Formation of blast wave and (b) propagation in air ......................... 41

Figure 2-29: Experimental and simulation results for 82g C4 bare blast, (a) Incident

overpressure (b) Impulse at 0.5m and 0.7m from charge center ......... 42

Figure 2-30: Experimental and simulation results for 82g C4 bare blast, incident

overpressure at 0.65 m and 0.85 m ........................................................ 42

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Figure 2-31: Fireball for bare 82 g C4 (a, b) and formation of secondary fireball (c, d,

e, f) ......................................................................................................... 45

Figure 2-32: (a) Fireball formation and (b, c) quenching for 82 g C4 covered in

shaving foam .......................................................................................... 45

Figure 2-33: Fireball for 250 g C4 (a, b, c) bare C4 and (d, e, f) covered in shaving

foam ....................................................................................................... 46

Figure 2-34: Incident pressure and Impulse plots for 82g C4 blast at 0.5 m-for bare

charge and submerged in shaving foam ................................................. 47

Figure 2-35: (a) Peak incident pressure and (b) impulse plots for 250 g Bare C4 and

covered in shaving foam at 0.9 m .......................................................... 47

Figure 2-36: Incident and reflected pressure plot (left) and impulse plot (right) for

250g C4 at 0.8m ..................................................................................... 48

Figure 2-37: Peak pressure and distance plots with and without shaving foam for (a)

82 g C4 (b) 250 g C4 ............................................................................. 49

Figure 3-1: (a) scaled down shells (b) its cut-view (c) standard 155mm shell ........... 54

Figure 3-2: Layout for blast and fragmentation tests of scaled down shell ................ 55

Figure 3-3: (a) Flat Brass probe (b) 3-D view(c) section view (d) Two probes setup 56

Figure 3-4: Flat probes arrangement for fragment velocity measurement (a) test-1 (b)

test-2 ...................................................................................................... 56

Figure 3-5: Testing setup with (a) fiberglass (F/G) sheets and timing probes (b)

plywood sheet ........................................................................................ 57

Figure 3-6: Setup for fragments impact and spatial distribution (a) Test-2 and (b)

Test-3 ..................................................................................................... 57

Figure 3-7: Fiberglass witness sheets (a, b) before and (c) after fragments impacts .. 57

Figure 3-8: Plywood witness sheets (a) before and (b) after the fragments impact ... 58

Figure 3-9: Fragments recovered in the tests .............................................................. 58

Figure 3-10: SPH Model of scaled down shell with gauge points ............................. 60

Figure 3-11: Fragmentation process (a) at 27 s (b) at 48 s (c) venting of product

gases ....................................................................................................... 60

Figure 3-12: Fragmentation process and radial expansion with time (a) at 57 s (b) at

80 s and (c) 150s (d) at 200 s (e) at 250 s ..................................... 61

Figure 3-13: Number of fragments and mass distribution .......................................... 61

Figure 3-14: Fragment velocities of gauge points defined on shell casing (a) with

ALE solver (b) with SPH ....................................................................... 62

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Figure 3-15: Number of fragments and their velocity distribution............................. 62

Figure 3-16: (a) AUTODYN model of shell (b) detonation wave propagation inside

shell (c) Expansion of shell at 20 s ...................................................... 63

Figure 3-17: (a) Venting of pressurized gases in air at t= 40 s and expansion (b) at

t= 61 s (c) at 90 s ............................................................................... 63

Figure 3-18: (a) Blast wave propagation in air at t=0.150ms, (b) at t= 0.604ms and (c)

at t= 0.88ms ........................................................................................... 63

Figure 3-19: Simulated and experimental (a) peak Pressure and (b) Impulse plots for

scaled down shell ................................................................................... 64

Figure 3-20: (a, b) Fragment's velocity measurement from different parts of the shell

(c) timing probe after fragment impact .................................................. 65

Figure 3-21: : (a) Two probes setup (b) Fragment’s impact on timing probe and (c)

arrival time for velocity calculations ..................................................... 65

Figure 3-22: Different positions of shell for fragment velocity calculations ............. 66

Figure 3-23: Fragment impacts and perforation through Fiberglass witness sheets . 67

Figure 3-24: (a, b) Plywood witness sheets (c) Timing probe placed below the shell

base ........................................................................................................ 67

Figure 3-25: Number of fragments and their mass distribution for scaled shell ........ 68

Figure 3-26: : Experimental and simulated peak incident pressure plots at (a) 0.55m

& 0.65m (b) 0.59m & 0.675m ............................................................... 69

Figure 4-1: (a) 7.62 mm bullet impact. (b) Pulverization of alumina disk. (c)

Fragmentation and scattering of alumina .............................................. 74

Figure 4-2 : Alumina tiles used in present work ......................................................... 74

Figure 4-3 : Stress-strain relation of porous material [6] ........................................... 75

Figure 4-4: Fragments penetration and perforation (a) Front side (b) back sides of

the 6 mm thick steel plate ...................................................................... 76

Figure 4-5: Experimental setup for testing protective configurations against

fragments impact ................................................................................... 77

Figure 4-6: (a) Front side (b) back side of C-1 ........................................................... 78

Figure 4-7: (a) Setup for testing C-1 and C-3. (b) Front (c) back sides of C-1 after

fragment’s impact .................................................................................. 78

Figure 4-8: (a, b) Test-2 setup and C-2 view after (c) impacted and (d) perforated

fragments ............................................................................................... 79

Figure 4-9: Assembled view of C-2, (a) front and (b) back sides .............................. 79

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Figure 4-10: (a, b) C-2 testing setup (c) C-2 along with 6 mm thick MS plate .......... 79

Figure 4-11: C-2 (a) front (b) back sides (c) laminated GFRP (d) PU foam after

fragments impact ................................................................................... 80

Figure 4-12: (a) Front and (b) back sides of C-3 ........................................................ 80

Figure 4-13: C-3 front and back sides after fragments impact- first test .................... 80

Figure 4-14: C-3 Second test (a) Front (b) back sides, (c, d) laminated GFRP.......... 81

Figure 4-15: (a, b) Assembled view of C-4 and (c) testing setup for C-4 and C-5 .... 81

Figure 4-16: (a, b) C-4 front and (c, d) back sides after the test ................................. 81

Figure 4-17: C-5 (a) Front side (b) back side ............................................................. 82

Figure 4-18: (a) Front and (b) back sides of C-5 after fragment's impact .................. 82

Figure 4-19: (a, b) A view of C-6 and (c, d) C-7 configurations ................................ 83

Figure 4-20: Testing setup for C-6 and C-7 ................................................................ 83

Figure 4-21: (a, b) front and back sides of C-6 after test, (c, d) front and back sides

of C-7 after test ...................................................................................... 83

Figure 4-22 : Different parts of 7.62x39 mm bullet, (left) steel core, lead filler, and

copper coated steel jacket. (Right) cut sections of bullet [8] ................. 84

Figure 4-23: High speed images of bullet impacting the target configuration ........... 85

Figure 4-24: 7.62 x 39 mm MSC original and plastically deformed recovered bullet

............................................................................................................... 85

Figure 4-25: The testing configuration, including Plastilina clay as backing medium

............................................................................................................... 86

Figure 4-26: High speed photographic images of blunt force trauma test at three

different times ........................................................................................ 86

Figure 4-27: (a) Testing setup (b) 7.62mm bullet impact (c), Rear side of C-5 (d) and

impact on Plastilina clay ........................................................................ 86

Figure 4-28: (a, b) FE model with gauge points defined and Fragment velocities of

gauge points defined on shell casing (c) with ALE solver (d) with SPH

............................................................................................................... 89

Figure 4-29: FE models of (a, b) C-1 and (c, d) C-5 .................................................. 90

Figure 4-30: Isometric view of shell fragmentation with C-1 and C-5, fragments

impacting C-1 & C-5 ............................................................................. 91

Figure 4-31: (a) Fragments penetration through C-1 (b) deformation of Kevlar woven

fabric and (c) Fragments impact on C-5 and bulge on back side of C-5

............................................................................................................... 92

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Figure 4-32: (a) Velocity profile of gauge points before and after impacting C-5 (b)

before and after impacting C-1 .............................................................. 92

Figure 4-33: (a) Fragments impacting on MS plate (b) isometric view ..................... 93

Figure 4-34: Penetration and perforation through (a) MS plate. (b) Close view of MS

plate ........................................................................................................ 93

Figure 4-35: (a) Shell model in SPH (b) radial expansion of fragments and (c)

moving gauges are visible ..................................................................... 94

Figure 4-36: (a) ALE model of C-4 (b, c) Fragments approaching the configurations

............................................................................................................... 95

Figure 4-37: Fragments impact on C-4, (a) front side view, (b, c) back side view .... 95

Figure 4-38: Velocity plot of gauge points (a) before and (b) after impacting C-4 .. 96

Figure 4-39: ALE model of C-2. (a) Grid plot and (b) material plot.......................... 96

Figure 4-40: (a) Isometric view of C-2 and C-4, (b) Fragments perforation through C-

2. (c) Gauge points defined on C-2 ....................................................... 97

Figure 4-41: (a) Fragments penetration through C-2 (b, c) combined view of C-2 and

C-4 ......................................................................................................... 97

Figure 4-42: Velocity profiles of gauge points (a) before and (b) after impacting C-2

............................................................................................................... 98

Figure 4-43: (a) AUTODYN model of shell (b) detonation wave propagation inside

shell (c) Expansion of shell at 20 s ...................................................... 99

Figure 4-44: (a) Expansion of shell at 40 s (b) at 61 s and (c) at t= 90 s ............. 99

Figure 4-45: (a) Blast wave approaching C-2 (b) impacted on C-2 and (c) C-2 before

and (d) after blast impact ....................................................................... 99

Figure 4-46: For gauge point 2 (a) Incident and reflected overpressure (b) Impulse

plots ...................................................................................................... 100

Figure 4-47: (a) Pressure at gauge point 3, (b) Change in Specific internal energy in

PU foam for gauge points 7 and 8 ....................................................... 101

Figure 4-48: Fragments perforation and captured in (a, b) Kevlar and (c, d) GFRP 102

Figure 4-49: (a) C-2, (b) laminated GFRP and (c) PU foam after fragments impact

............................................................................................................. 102

Figure 4-50: (a) Front and (b) back sides of C-3 (c) laminated GFRP after second

test. ....................................................................................................... 103

Figure 4-51: (a) Back side of C-4 (b, c) front and back sides of laminated GFRP

placed behind the ceramic tile ............................................................. 103

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Figure 4-52: (a) Front (b) back sides of C-5 after fragment's impact, (c) recovered

fragment & bullet ................................................................................. 104

Figure 4-53: (a, b) Front and back sides of C-6 (c, d) C-7, after fragments impact . 105

Figure 5-1: (a) Empty container (b) C4 placed at the bottom (c) filled with shaving

foam ..................................................................................................... 110

Figure 5-2: A sketch of testing setup for (a) surface burst (b) detonation inside

cylindrical container ............................................................................ 110

Figure 5-3: Experimental setup for bare C4 charge test (a) close view (b) complete

setup ..................................................................................................... 111

Figure 5-4 (a) Experimental setup for C4 detonation inside container (b) C4 and foam

filled in container ................................................................................. 111

Figure 5-5: (a) AUTODYN model (b) product gases expansion ............................. 112

Figure 5-6: (c) Blast wave formation and (d) propagation in air towards gauge points

............................................................................................................. 112

Figure 5-7: Simulated P(t) history of gauge points for 104g bare C4 surface blast 113

Figure 5-8: (a) AUTODYN Model (b) blast wave reflection from base and walls (c)

blast wave loading on container walls ................................................. 114

Figure 5-9: FE model for shell and container ........................................................... 114

Figure 5-10: (a) Shell fragmentation at 63.93 s and (b) velocity plot of the gauge

points.................................................................................................... 115

Figure 5-11: Isometric view of the fragments, radial dispersion and container ....... 115

Figure 5-12: Fragments penetration into steel liner and its deformation .................. 116

Figure 5-13: Fragments velocity after impacting the container walls ...................... 116

Figure 5-14: High speed images of bare C4 (a) detonator fired (b) t= 0.22 ms after

detonation ............................................................................................ 117

Figure 5-15: High speed images (c) t= 0.320 ms and (d) t= 0.725 ms ..................... 117

Figure 5-16: High speed images of bare C4 detonation ........................................... 118

Figure 5-17: high speed images at (a) t=0.075ms (b) t = 0.800 ms .......................... 118

Figure 5-18: High speed images at (c) t=1.075ms and (d) t=1.475ms ..................... 119

Figure 5-19: C4 charge detonation inside container at (e) 1.80ms and (f) t= 2.675ms

............................................................................................................. 119

Figure 5-20: Contact detonation of 30 g C4 (a) test setup (b) post-test view ........... 120

Figure 5-21: Pressure plots for 104g C4 detonated (a) Surface burst (b) inside

container .............................................................................................. 120

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Figure 5-22: Post-test sights of (a & b) PU-sand composite top and side (c) container

............................................................................................................. 121

Figure 5-23: (a) MS cylinder (b) Inner container ..................................................... 122

Figure 5-24: (a, b) PU-silica disc (c) EPS foam and Bakelite sheet ......................... 122

Figure 5-25: (a) GFRP cylinder (b) inner view of composite container (c) outer

composite container ............................................................................. 123

Figure 5-26: (a) C4 placed inside container (b) shaving foam filled around C4 ...... 123

Figure 5-27: Experimental setup for 800 g C4 detonation inside container ............. 124

Figure 5-28: High-speed images of 800g C4 detonation inside container ............... 124

Figure 5-29: Reflected overpressure-time history for 800g C4 detonation inside

container .............................................................................................. 125

Figure 5-30: Steel cased charge (Pipe-bomb) ........................................................... 125

Figure 5-31: (a) SPH- ALE model for steel cased charge and inner container (b) at 15

s of detonation (c) fragmentation at 40 s ......................................... 126

Figure 5-32: (a) Gauge points location at 58s, (b) radial flight at 105 s .............. 126

Figure 5-33: (a) No. of fragments and mass distribution (b) fragments velocity plot

............................................................................................................. 127

Figure 5-34: (a) Shaving foam filled around steel cased charge (b) experimental setup

............................................................................................................. 127

Figure 5-35: High-speed images of steel cased 565g Comp-B detonation inside

container .............................................................................................. 128

Figure 5-36: Fragments impact and perforation (a) inner layer (b) outer layer of

GFRP ................................................................................................... 128

Figure 5-37: (a, b) Fragments perforation through outer layer of Kevlar fabric (c)

bottom MS disc after second test ......................................................... 129

Figure 5-38: Reflected overpressure -time history for steel cased 565 g Comp-B

charge inside container ........................................................................ 130

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List of Tables

Table 2-1 : Blast parameters for bare charges and covered in shaving foam ............. 35

Table 2-2: JWL parameters of C4, EOS data for Balsa wood and air ........................ 40

Table 2-3: Effect of grid size and discretization error in AUTODYN Simulation .... 40

Table 2-4: Comparison of bare charge tests with Kingrey-Bulmash (KB) results ..... 43

Table 2-5: Fireball radius for C4 detonation in air and with shaving foam ............... 46

Table 3-1: Material and dimensions of scaled down and standard 155mm shell ....... 54

Table 3-2: Johnson Cook damage parameters for Steel-1006 [17] ............................ 59

Table 3-3: Comparison of experimental, numerical and analytical fragments

velocities ................................................................................................... 66

Table 3-4: Measured mass and size of the recovered fragments- comparison with

simulation results ...................................................................................... 68

Table 3-5: Summary of the experimental & simulation Pressure-time values ........... 70

Table 4-1: Constituent materials and dimensions of protective configurations ......... 77

Table 4-2: Protective configuration for bullet impact tests [8]................................... 84

Table 4-3: Measured values of 7.62x39 mm MSC bullet ........................................... 84

Table 4-4: Material properties used in simulation ...................................................... 88

Table 4-5: Summary of the experimental and simulated results .............................. 106

Table 5-1: Simulation results for 104g bare C4 surface blast .................................. 113

Table 5-2: Material and dimensions of pipe-bomb for blast and fragmentation study

................................................................................................................ 126

Table 5-3: Comparison of experimental results with Conwep calculations ............. 130

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List of Acronyms and Symbols

EM Energetic Materials

LE Low Explosives

HE High Explosives

IEDs Improvised Explosive Devices

EPS Expanded Polystyrene

PU Polyurethane

GFRP Glass fiber reinforced polymer

psi pounds per square inch

kPa kilopascal

MSC Mild Steel Cover

SPH Smoothed Particle Hydrodynamics

ALE Arbitrary Lagrangian-Eulerian

TNT Trinitrotoluene

VoD Velocity of Detonation

Ps Incident pressure

Pr Reflected pressure

q Dynamic pressure

ts Positive phase duration

Is positive impulse

P0 ambient pressure

Specific heat capacity ratio

Z Scaled distance

W Charge mass

R distance

UFC Unified Facilities Criteria

m/s meter/second

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kg kilogram

Liquid volume fraction

w/w weight/weight

m micrometer

hrs hours

cP centipoise

W Volume fractions of water

a Volume fractions of air

DAQ Data Acquisition system

ms millisecond

mm millimeter

m meter

s microsecond

FE finite element

Diameter

GSM grams per square meter

Fragment size variable

C/M ratio of explosive to metal mass/unit length

mph miles per hour

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Introduction Chapter 1

1.1 Motivation

Numerous terrorist attacks have caused thousands of deaths and left tens of

thousands injured besides damage to valuable infrastructure and property. In March

2004, several IEDs placed in four commuter trains in Madrid exploded causing 193

deaths and injuries to around 2000 people [1]. In July 2005, 52 died in London

underground train explosions [2]. More than 7500 people have died and over 17000

injured by suicidal attacks in Pakistan between 2007 and 2014. The yearly

breakdown is shown in Figure 1-1. About 5000 civilians lost their lives only in IEDs

attacks in Afghanistan between 2009 and 2014 [3]. In October 2015, a Russian

Metrojet was brought down over Egypt's Sinai peninsula by a bomb, killing all 224

people on board [4]. In April 2017, 11 people were killed and 45 injured in blast on

the St. Petersburg metro [5]. In September 2017, an IED was detonated on a Tube

train in south-west London injured 29 people [6]. These are the direct counts of

deaths in such extreme events. Another aspect of these attacks, which has usually

been ignored, is the indirect fatalities due to health, displacement and malnutrition of

the victimized families. According to Geneva Declaration Secretariat, "a reasonable

average estimate would be a ratio of four indirect deaths to one direct death in

contemporary conflicts” [3]. Therefore, safety against EM detonation is of vital

importance to avoid direct and indirect loss of lives.

Figure 1-1 : Fatalities in terrorist violence in Pakistan, (2000-2018) [3]

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1.2 Energetic Materials

Energetic materials are a class of material which, when suitably ignited by an

external stimulus, release chemical energy stored in their molecular structure at

extremely fast rate. The history of energetic materials goes back to China with the

combustion of the powder mixture of sulfur, charcoal and nitrate salts [7]. These

materials release large amounts of energy and expand rapidly in volume to generate

force in the time scale of microseconds. High explosives, propellants and

pyrotechnics belong to the class of energetic materials. These materials are

commonly used in various military and commercial applications. Based on their

applications, explosives can be classified as low explosives(LE) and high explosives

(HE) [8].

1.2.1 Low Explosives

The decomposition or propagation of reaction rate in these explosives is fast but

subsonic. These explosives are ignited by a spark, flame or impact and this

combustion reaction is termed as deflagration [9]. The deflagration under

confinement turns into explosion. The reaction products move in a direction opposite

to that of reaction propagation. Propellants and pyrotechnics fall in this category of

energetic materials [7]. Propellants are not expected to detonate but combust in a

controlled manner. Propellants are used for the propulsion of different objects

including missiles, rockets, gun bullets etc. [9]. Pyrotechnics produce some special

effects like heat, light, smoke and sound [9].

1.2.2 High Explosives

Once ignited these explosives decompose spontaneously. The propagation of reaction

rate in these materials is supersonic. This type of combustion reaction is termed as

detonation. The unique aspect of detonation is the release of energy at extremely high

rate and production of highly compressed gaseous products [10]. The detonation

creates a shock wave propagating at supersonic speed due to the continuous

exothermic chemical reaction taking place inside the high explosive just behind

detonation front [11]. The point at which the exothermic reaction completes is called

Chapman-Jouguet (C-J) point. Just ahead of C-J point is a narrow pressure spike

known as Von Neumann spike. The thin region between this spike and the C-J point

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is called reaction zone. A release wave propagating downstream into the detonation

products behind the detonation wave is called Taylor wave. [10]. The Von Neumann

spike is attenuated immediately after encountering a metal whereas the Taylor wave

produced the practical impact. The reaction products follow the direction of

propagation. The rate at which the reaction proceeds to the unreacted part of the high

explosive is called detonation velocity (D). It is a function of the density of the

explosive. For commonly used explosives detonation velocity ranges from 3000 to

9000 m/s. The structure of detonation wave and pressure profile is shown in Figure

1-2.

Figure 1-2 : The detonation wave structure and pressure profile [10]

High explosives (HE) are classified as primary and secondary based on their

sensitivity to initiation. Primary explosives are more sensitive and require only a

small amount of energy for initiation but are less powerful. These are mainly used in

detonators. Lead Azides, Mercury fulminate and Lead Styphnate are few examples

[8].

Secondary explosives are less sensitive but more powerful and can be initiated by a

shock wave. Common examples of secondary HE are TNT, C4, Comp-B, RDX

HMX etc. [8]. These explosives create shock waves resulting in shattering,

penetration, lift etc. [9].

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1.3 The Rankine-Hugoniot Relations

The concept of shock wave propagation and the conservation equations can easily be

understood by considering a piston-cylinder configuration as shown in Figure 1-3

[10, 12]. The cross-sectional area of cylinder is taken as unity. The piston is initially

at rest and then pushed into the compressible material at velocity UP. After a time t1,

the compressed region ahead of piston traveled a distance USt1, where US is the

velocity of compressed /disturbed medium ahead of piston. In the meantime, piston

has traveled a distance of UPt1. This process is analogous to snow plow behavior with

US>UP. A very thin layer separates the compressed moving region from stationary

material in the cylinder. The plane separating “moving” from “stationary” fluid in the

cylinder is known as shock front. The initial and final parameters like, pressure,

density, specific internal energy and velocity are shown in the Figure 1-3.

Figure 1-3 :Shock wave generation in a compressible fluid [12]

Now, applying the conservation laws of mass, momentum and energy in the

compressed region, the conservation of mass is expressed as;

𝑈𝑆𝑡1𝜌0 = 𝜌1(𝑈𝑆 − 𝑈𝑃)𝑡1 (1.1)

For any time t, this equation can be written as;

𝜌0𝑈𝑆 = 𝜌1(𝑈𝑆 − 𝑈𝑃) (1.2)

The momentum conservation requires that the difference in the momentum ahead and

behind the shock front is equal to the impulse per unit of cross-sectional area:

𝜌1(𝑈𝑆 − 𝑈𝑃)𝑈𝑃𝑡 − 0 = (𝑃1 − 𝑃0)𝑡

𝜌1(𝑈𝑆 − 𝑈𝑃)𝑈𝑃 = (𝑃1 − 𝑃0)

(1.3)

The equation for conservation of energy requires that the work done by the external

forces is equal to the sum of the increase in both internal and kinetic energy (K.E):

𝐸1[𝜌1(𝑈𝑆 − 𝑈𝑃)𝑡 − 𝐸0[𝜌0𝑈𝑆𝑡] = (𝐸1 − 𝐸0)𝜌0𝑈𝑆𝑡 (1.4)

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The kinetic energy is given by 1

2𝑚𝑣2 , this gives;

1

2𝜌1

(𝑈𝑆 − 𝑈𝑃)𝑈𝑃2𝑡 − 0 =

1

2𝜌1𝑈𝑆𝑈𝑃

2𝑡

(1.5)

For a stationary shock wave, the change in K.E is equal to the change in internal

energy.

𝐸1 − 𝐸0 =

1

2𝑈𝑃

2

(1.6)

The equations (1.2), (1.3) and (1.6) are known as Rankine-Hugoniot relationships for

a material where a pressure discontinuity propagates. The equations applied for a

piston-cylinder configuration with a compressible medium (gas) can be extended to

shock wave propagation into gas, liquid, or solid or to a detonation wave [10]. The

conservation equations for detonation are identical to these three equations with a

change that shock velocity US is replaced by D (detonation velocity). The above

stated three conservation equations have five unknowns US, UP, P1, 1 and E1. By

eliminating US and UP from these equations one can obtain a single equation which is

a function of state variables P1, 1 and E1 [12].

𝐸1 = 𝐸0 +

(𝑃1 + 𝑃0)(𝜌1 − 𝜌0)

2𝜌1𝜌0

(1.7)

This equation (1.7) is known as Hugoniot equation which represents the locus of all

the states that can be reached from an initial density 0 to final compressed density of

1.

1.4 Equation of State

In order to completely define the final state of a system invested by a shock front and

to plot the Hugoniot curve another equation is required. This equation is known as

the equation of state (EOS) of the material [12]. The equation of state of the material

defines a relationship of pressure in terms of internal energy and volume given by;

𝑃 = 𝑓(𝐸, 𝜌). The EOS of a material describes the behavior of a material under shock

wave loading [10]. The above stated three conservation equations together with C-J

condition (D = CCJ + (UP)CJ) and the equation of state of detonation products

completely describe the detonation process. Here, CCJ represents speed of sound at

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the C-J point [10]. A linear relationship of the following form holds for various

materials under shock wave loading without phase change.

𝑈𝑆 = 𝐶0 + 𝑆 𝑈𝑃 (1.8)

Where, C0 is the sound speed of the uncompressed material and S is the slope of the

straight line. The other well-known EOS are ideal gas, Tillotson, Puff, JWL etc.

1.5 Formation of Blast Wave

The detonation of a HE generates hot gases at pressures from 100 to 300 kilobars and

at temperatures about 3000 – 4000oC. The violent expansion of these product gases

forces out the surrounding air. Consequently, a thin layer of highly compressed air- a

blast wave- forms and starts propagating outwards in front of the hot gases. The

pressure falls to ambient as the blast wave moves away from the source. As the

product gases continue to expand, they cool down and their pressure falls below the

ambient pressure. The expansion of these gases results in the reversal of flow

towards the source due to the pressure difference between the atmosphere and these

gases. This causes an under pressure -negative phase- in the pressure-time profile of

the blast wave. Finally, the conditions return to equilibrium as the air and gases

pushed away from the source come back [9]. A typical waveform of the blast wave

is shown in Figure 1-4 [13]. It is pertinent to define blast parameters associated with

a blast wave and loading estimation on an object. These parameters are also

illustrated in Figure 1-4.

Figure 1-4 : Characteristics of a blast wave (a) ambient pressure (b) positive phase (c)

negative phase [13]

Incident pressure (Ps) - Pressure acting on a surface parallel to the direction of blast

wave propagation [14].

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Reflected pressure (Pr) - The pressure as measured front–on to the flow. Peak

reflected pressure is a function of incident pressure and angle of incidence [15].

Dynamic pressure (q) - The pressure due to moving air behind the shock front.

Positive phase duration (ts) - The time for which incident or reflected pressure stays

above the atmospheric pressure.

Incident Impulse (Is) - The area under the incident pressure time plot [16].

Stand-off (R) – The physical distance between the surface of a building or

component, and the center of charge.

The blast wave as shown in Figure 1-4 is a kind of shock wave that represents a

discontinuity in the medium. It is a compressive wave that moves at a speed higher

than the speed of sound in the medium. The blast wave decays immediately after the

peak pressure is reached [17]. The decay rate of the blast wave is given by Modified

Friedlander equation and developed by Thornhill is shown in eq. (1.9) [13, 18].

𝑃(𝑡) = 𝑃𝑠 (1 −

𝑡

𝑡𝑠)𝑒

−𝑏𝑡𝑡𝑠

(1.9)

Where, Ps is peak incident overpressure, ts is positive phase duration and b is a

constant. The blast wave undergoes reflection when the forward moving air

molecules are brought to rest and further compressed upon meeting an obstacle, thus

forming a reflected pressure (Pr) [15]. The reflected pressure depends on the angle

of incidence of the blast wave. For a blast wave impacting perpendicular to the

surface, the reflected pressure is determined by relations shown in eq. (1.10) and

(1.11) [9].

𝑃𝑟 = 2𝑃𝑠 + (𝛾 + 1)𝑞 (1.10)

𝑃𝑟 = 2𝑃𝑠[

7𝑃0 + 4𝑃𝑠

7𝑃0 + 𝑃𝑠]

(1.11)

Where, P0 is ambient pressure, specific heat capacity ratio of air ( = 1.4) and q is

dynamic pressure. The wind associated with the blast wave constitutes the dynamic

pressure (q) and is defined as half the density () times the square of the fluid

velocity (v). The dynamic pressure (q) is given in eq. (1.12). By using the Rankine-

Hugoniot relations q can also be computed by eq. (1.13) [19].

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𝑞 = 1

2𝜌𝑣2 (1.12)

𝑞 =

𝑃𝑠2

2𝛾𝑃0 + (𝛾 − 1)𝑃𝑠

(1.13)

The dynamic pressure is responsible for drag loading on objects [20]. The area under

the pressure time plot for positive phase duration of equation (1.6) determines the

impulse. This impulse is responsible for the transfer of kinetic energy to the structure

which can cause damage to the structure or its components [21]. Impulse is not only

a function of peak pressure and positive phase duration but also a function of decay

rate [22]. The positive or incident impulse (Is) can be computed from the relation

given in eq. (1.14) and (1.15).

𝐼𝑆 = ∫ 𝑃𝑑𝑡

(1.14)

𝐼𝑠 =

𝑃𝑠𝑡𝑠

𝑒 = 0.368𝑃𝑠𝑡𝑠

(1.15)

Kingary-Bulmash [23] empirical equations provide a common approach to determine

the blast loading. The equations describe a range of blast wave parameters for a given

mass of explosive and stand-off distance. The parameters are normalized in terms of

TNT as the explosive and equations are expressed in the form of scaled distances (Z)

[15].

1.6 Scaling Laws

The blast wave parameters are functions of charge mass (W) and standoff distance

(R) [14]. Hopkinson [24] and Cranz [25] independently formulated blast wave

scaling laws which are also known as cube-root scaling. The approach leads to the

specification of scaled distance (Z) defined in eq. (1.16) [9]. The scaled distance (Z)

is widely used to estimate blast related parameters in empirical methods [14].

𝑍 =

𝑅

√𝑊3

(1.16)

For two charge masses W1 and W2 and distances R1 and R2, Z also defines the

constant of proportionality as given in eq. (1.17) and (1.18) [9].

𝑅1 = 𝑍 √𝑊13 (1.17)

𝑅2 = 𝑍 √𝑊23 (1.18)

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Sachs [26] presented scaling laws that incorporate the effect of altitudes where

ambient conditions are significantly different to that of sea level. The overpressure at

an altitude can be computed as given in eq. (1.19).

𝑃𝑆 = 𝑃1

𝑃𝑎𝑡𝑚

𝑃0

(1.19)

Where P1 is the overpressure at sea level [19].

1.7 Effects of Cased Explosive Detonation

The detonation of a cased explosive device or an IED causes damage by following

three main mechanisms [27]:

Blast overpressure

Fragmentation

Thermal effects

The impact of the blast wave induces stresses in the target materials [9]. Compressive

and tensile waves traverse through the material. This wave propagation can result in

several irreversible phenomena including (but not limited to) plastic deformation,

fracture and phase transformation. The damage produced to a structure by a blast

wave depends on its orientation and usually related to a complex combination of the

hydrostatic and dynamic pressure forces. The response of the structure is a function

of the time-history of the blast wave loading [28].

The blast wind resulting from the blast overpressure leads to injuries and fatalities. A

wind speed of 163 mph is associated with a peak overpressure of 5 psi (34.5 kPa)

[20, 29]. The surrounding objects are thrown violently and crushed [29]. Human

beings are sensitive to overpressure, peak pressure rise rate, positive and negative

phase duration of blast wave and the specific impulse. The injuries caused by a blast

wave are categorized as:

Primary injuries

Secondary injuries

Tertiary injuries

Quaternary or Miscellaneous injuries

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Primary blast injuries are caused solely by the direct effect of overpressure on tissue.

Organs containing air like ears, lungs and gastrointestinal track are the most

susceptible to this kind of injury [13]. The minimum pressure for fatal primary blast

injury is 29 psi (200 kPa) [27]. Secondary blast injuries are caused by the flying

objects that strike people. In recent years, nails, screws, ball bearings and other

metallic parts have been used in IEDs to enhance this injury mechanism. Tertiary

blast injury is caused by whole-body displacement at high blast overpressures and

impulses. Any part of the body can be affected by secondary and tertiary injuries. All

other injuries caused by the explosion are included in the quaternary (miscellaneous)

type [27, 30].

The ear is the most sensitive to blast but is not the most critical organ. Threshold for

rupture of human eardrum for a fast rising pulse is 5.0 psi (34.5 kPa). Blast

overpressure at which half of tympanic membranes rupture and the minimum

pressure for lungs damage is 15 psi (103.4 kPa) [27, 31]. Unified Facilities Criteria-

UFC 3-340-02 provides various damage criteria for specific organs of the human

body, equipment and explosives [32].

Fragmentation is one of the dominant threats to personnel from cased explosives or

IEDs. Injuries to personnel due to fragment impact can be classified into primary

fragment and secondary fragment injuries. Primary fragments, which are usually

small and have high-velocities, cause injuries by penetration and perforation of vital

organs of the body [27]. Secondary fragments are usually larger and have much less

velocity upon impact and can cause non-penetrating blunt trauma [33]. Therefore, it

is very difficult to effectively deal with this mechanism. It necessitates higher mass

solution or an expensive lightweight ballistic protection technique.

Thermal effect, burning due to heat and fireball, is another potential injury

mechanism associated with explosives detonation. [33]. The primary thermal hazard

posed by an explosive detonation is less significant than the blast and fragmentation

threats.

Besides these, an energetic material detonation causes damage to the surrounding

objects and structures. A few examples of structural damage caused by energetic

material detonation are shown in Figure 1-5.

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1.8 Literature Review

The highly dynamic nature of the blast wave hampers protective measures. No single

material has been found to provide safety within affordable cost and weight limits.

Sandia National laboratories [34, 35] introduced aqueous foam for mitigation of blast

overpressure. Silnikov et al [36, 37] and Takayama,et al [38] investigated

effectiveness of multiphase material relaxation for blast mitigation in combined

inhibitors and found significant reduction in blast wave parameters. Gelfand et al

[39] studied blast wave mitigation properties of aqueous foam as a function of liquid

fraction. Del Pret et al [40] conducted experimental and numerical studies of HE

detonation inside aqueous foam.

Grujici et al [41] investigated ballistic performance of alumina/S-2 glass combination

against armor piercing (AP) and non- armor piercing projectiles. Poh and Wai [42,

43] investigated multi-layered construction against steel rod at impact velocity of

500 m/s. Zecevic et al [44] compared the fragmentation pattern and effectiveness of

M54 projectile with M107 and concluded that body material and energetic filling

plays important role in fragmentation mass and velocity distribution. Prytz, and

Odegardstuen [45] investigated the fragmentation of a 155 mm artillery shell by

statically detonating the shell and recovering its fragments to analyze the mass

distribution. Fragments’ velocities were estimated with numerical simulation only.

Arnold et al [46] studied the fragmentation behavior of very light and heavier casings

Figure 1-5 : Devastating effects of energetic material detonation

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and found that the circumferential fragments size depends on material strength.

Nystrom and Gylltoft [47] investigated the combined effects of blast and

fragmentation loading on reinforced concrete and concluded that the combined

effects of blast and fragmentation loading are more severe than their separate effects.

Mohammad A. Abdallah [48] conducted fragmentation analysis of OG-7 warhead

using AUTODYN and compared the results with pit test results for OG-7 warhead.

Discrepancy in mass distribution between experimental and numerical data was

observed.

Ramadhan et al [49] studied impact response of sandwich structures based on

Kevlar/epoxy resin and Aluminum alloy laminated panels at impact velocities up to

400 m/s. The sandwich structures exhibited good energy absorbing characteristics

against impact loading. Liverts et al [50] worked specifically on conventional

aqueous foam Gillette using an exploding wire facility for blast wave mitigation.

Carton [51] experimentally investigated the effectiveness of water foam for the

mitigation of blast from HE detonation. Bornstein [15] studied water-filled

containers, numerically and experimentally, against near-field blast loading and

found that the containers provide 65% reduction to steel plate deformation. Alogla et

al [52] studied metallic protective panels against nearby blast loading. The fragments

effect was not studied. Nayak et al [53] studied 7.62 mm AP bullet impact at

velocity of 550 m/s on aramid fabric-epoxy composite laminates. Li et al [54]

introduced a lab scale experimental technique for studying combined loading effects

of blast and fragments, considering only single fragment impact with blast loading.

Lee et al [55] studied ballistic impact behavior of silica impregnated Kevlar against

fragment impact velocity up to 244 m/s. Soydan et al [56] experimentally and

numerically investigated the impact of a 9 mm FMJ bullet, of velocity 400 m/s, on a

three-layer armor configuration consisting of fiber-cement, Kevlar fabric and steel.

Ansari et al [57] investigated laminated GFRP composite plate under blunt projectile

impact at velocities below 50 m/s. Rasico et al [58] simulated the blast and

fragmentation of HE (high explosive) filled, M795 artillery shell IED (improvised

explosive device) buried in soil. The fragments impacted on vehicle hull were

investigated numerically.

Unified Facilities Criteria-UFC 3-340-02 provides blast resistant protective design

criteria for components, glass windows and structures. [32]. The latest version of

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UFC 4-010-01 published in 2013 supersedes its previous versions and defined

different levels of protection [14]. Qi et al investigated mitigation of shock loads

from near field and contact detonations of high explosives using auxetic honeycomb-

cored sandwich panels. The combined shield was effective to protect reinforced

concrete structures against impact and near field blast loadings [59]. Langdon et al

investigated numerically and experimentally the mitigation of damage in aircraft

luggage containers subjected to internal blast loading. It was found that allowing a

venting in containers lengthwise along the aircraft body is more beneficial [60].

A destructible container [37] as shown in Figure 1-6 and liquid blast inhibitors

composed of several elastic envelopes can withstand only the blast effects of 0.5 kg

TNT.

Figure 1-6 : Blast inhibitor: 1-Elastic envelope, 2-liquid gas medium, 3-working space and 4-

HE [37]

Episafe [61] containers comprising a hard inner cylinder and an energy absorbing

outer cylinder made of high performance plastic fiber can contain blasts of cased

charges up to 0.47 kg TNT and equivalent. Episafe container as shown in Figure

1-7(a) is relatively bulky and direction dependent.

Figure 1-7: (a) Episafe container and (b) Resnyansky and Delany setup

a b

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Resnyansky and Delany [62] recorded a large reduction of peak incident pressure by

surrounding 0.5 kg Pentolite with 110 liter of water inside a spherical container. The

setup is shown in Figure 1-7(b). Blastguard technologies Inc. [63] developed trash

receptacles to reduce lethal threats posed by the detonation of an improvised

explosive device (IED). The trash receptacle, shown in Figure 1-8, has a diameter of

30 inches and a height of 36 inches. It can contain a blast of charge up to 0.50 kg of

TNT or equivalent.

Figure 1-8 : Blastgard trash receptacle [63]

TM International [64] developed a steel wired rope blast containment tank for

explosive ordnance disposal (EOD). The vessel shown in Figure 1-9 is employed to

counter emergency scenarios involving an energetic material detonation. The product

is primarily intended to contain fragments but it can also reduce the blast

overpressure by a minimum of 50%.

Figure 1-9 : TM International blast containment vessel [64]

Mistral Security [65] has developed a Blast Containment Receptacle (BCRs) which

provides protection against fragmentation and blast pressure. BCR0.5 weighing 160

kg shown in Figure 1-10 can withstand a blast of 0.5 kg TNT or equivalent and it

costs about USD1800 –USD2000 [66].

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Figure 1-10 : Blast Containment Receptacle (BCRs) [65]

Greenfield et al [67] developed a container for explosive devices comprising inner

and outer containment vessels to contain explosively driven fragments and blast

overpressure. The inner and outer vessels were made of 12.5 mm thick HY80 Steel.

Edberg et al [68] presented a shield formed of one or more sprays of attenuation

material comprising a gas, such as air, disposed as bubbles in a liquid medium for

blast mitigation. Fly-Bag [69] made of multi-layered textiles is fitted inside the

standard aluminum containers that are used for loading luggage can stop a small-to-

medium-sized (200-500g) bomb hidden in a suitcase or a cargo-hold from damaging

the structure. It can only be fitted in narrow body aircrafts. FLY BAG2 [70] has

developed a technology that could allow planes in the future to survive a Lockerbie-

sized explosion. Fly Bag2 is a joint project of 14 European countries.

1.9 Gaps in Literature

Much of the material in this field is restricted or proprietary which makes the

learning inherently difficult. Although aqueous foam barrier is very effective for

blast and shock wave mitigation, it cannot protect against the fragmentation effects

associated with the detonation of cased charges or IEDs. Sembian and Liverts et al

[50, 71] worked specifically on conventional aqueous foam using an exploding wire

facility. The facility, however, lacks generation of detonation products produced in

case of energetic material detonation. Fountain blast inhibitors [36] and destructible

container [37] can only provide safety against blast effects up to 0.5 kg of TNT

equivalent charge. The details of the working medium are not available. Episafe [61]

is relatively bulky and direction dependent. Grujicic et al [41] used encapsulated

ceramic plates and alumina/S-2 glass for protective armor but the shattering of brittle

ceramic plate and resulting secondary fragmentation was not investigated. Alogla et

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al [52] studied metallic protective panels against nearby blast loading. The fragments

effect was not studied. Blastgard trash receptacles, TM International containment

vessels and Mistral Security BCRs [63-65] are good solutions but fairly bulky and

expensive. BCR0.5 that can withstand a blast of 0.5 kg TNT or equivalent costs

about USD1800 –USD2000 [66].

1.10 Objectives

The main objectives of the present work are;

1. To measure the blast wave parameters produced by C4 detonation and its

mitigation.

2. To search, characterize and investigate commercially available materials for

fireball suppression, blast mitigation and fragments containment.

3. To study the response of multi-layered combination of Kevlar fabric, GFRP

and PU/PS foams against high velocity fragments and blast loading.

4. To develop a model container against combined blast, fragmentation and

thermal effects of 1.0 kg TNT equivalent charge detonation.

1.11 Thesis Organization

A brief introduction and literature review of the effects of EM detonation and

mitigation strategies is laid down in Chapter 1. Materials, diagnostic tools and

experimental work applied for blast mitigation are presented in Chapter 2.

Experimental and simulation approaches for characterization of shell fragmentation

and testing of protective configurations are discussed in Chapter 3 and Chapter 4

respectively. Design and testing of a protective container based on the simulated and

experimental data obtained is laid down in Chapter 5. Finally, Chapter 6 presents

conclusions from the current research as well as provides some recommendations

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[58] J. Rasico, C. Newman, M.R. Jensen, MODELING FRAGMENTATION OF

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[63] Blastguard Trash Receptacles. Available from:

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Materials and Methodology for Blast Chapter 2

Mitigation

2.1 Introduction

The chapter covers an introduction of materials used for generation of blast wave and

its mitigation. Characterization of commercially available shaving foam and its blast

mitigation capabilities are presented. The diagnostic tools employed for visual study,

fireball measurement and determination of blast wave parameters are briefly

discussed. Blast wave parameters for C4 explosive detonation in air and covered with

shaving foam are presented in this chapter.

2.2 Aqueous Foam

Aqueous foam is a bi-phase system where air cells are enclosed by thin liquid films.

It consists of a foam concentrate of de-ionized water with a surfactant and a polymer

stabilizer essentially introduced with gas/air component. The aqueous foam is

categorized as dry, wet and bubbly based on the liquid volume fraction () [1].

dry foam: < 0.05

wet foam: 0.05 < < 0.36

bubbly liquid: > 0.36

Aqueous foam in particular has been a subject of research since its first development

at Sandia laboratories in 1983. It was developed to mitigate blast effects and to

capture the hazardous particulate material from unwanted dispersion in the

atmosphere. The blast wave strength can also be significantly attenuated by

surrounding the energetic material with aqueous foam [2, 3].

The aqueous foam developed specifically for blast mitigation may not be available to

the general public which necessitated the search for a commercially available

alternate. Present work addresses the investigation of commonly available health care

product DENIM shaving foam against an energetic material detonation including the

suppression of fireball as well as the overpressure attenuation.

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2.2.1 DENIM Shaving Foam

The composition of the contents under pressure in the aerosol can is [4];

Bulk (Liquid surfactant system): 96.00 % w/w

Hydrocarbon propellant: 4.00 % w/w

The aerosol system is a sealed system, so both the bulk and the propellant are liquid

and mix under pressure to form a homogeneous liquid system. Only a very small

amount of propellant, residing in the head space of the can, is in vapor form and

helps to expel the product out when the actuator is pressed [4].

2.2.2 Microscopic and Viscosity Study

The shaving foam used in this research work has a density of 60 kg/m3

as measured

using a pycnometer. Microscopic study of the shaving foam was performed using

Olympus microscope. The foam sample was dropped on the slide and studied at

magnification 100X. The foam produces finely dispersed bubbles with an average

initial size of 15 m. The microscopic study of conventional aqueous foams (Gillette

regular and DENIM original) was carried out at different time intervals to observe

the foam stability, bubble size and coalescence. Foam stability is related to its

drainage rate (i.e. the volume of liquid that drains out of expanded foam over time).

Foams were examined in 30 minute intervals for a total time of two hours Initially, a

rapid increase in average bubble size is observed as depicted in Figure 2-1, Figure

2-2 and Figure 2-3. The coarsening due to coalescence of bubbles slowed down with

time. The bubble size increased to 120 m in 2 hours. The aqueous foams stability

deteriorated with time but the DENIM foam was found to be in better condition even

after 24 hours.

a b

Figure 2-1 : Denim foam-average bubble size (a) 15 µm at 0 hrs (b) 85 µm at 1 hrs

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The graphical representation of bubbles coarsening of both commercially available

shaving foams is shown in Figure 2-4.

c d

Figure 2-2: Denim foam-average bubble size (c) 120 µm at 2 hrs (d) at 24 hrs

c d

a b

Figure 2-3: Gillette foam-average bubble size (a) 20 µm at 0 hrs (b) 105 µm

at 1 hrs (c) 155 µm at 2 hrs (d) at 24 hrs

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The viscosity of DENIM shaving foam was measured with DV2T viscometer at 24

0C using RV06 spindle for torque ranging from 17.4% to 45%. A rapid drop in

viscosity was observed at low shear rates. The decreasing viscosity trend at higher

shear rates is shown in Figure 2-5 and indicates a shear thinning behavior of the two-

phase medium.

2.2.3 Sound Speed Measurement

Sound speed was measured both in air and in shaving foam at a temperature of 240C.

A motor bike horn was used as the sound source. Two terminal condenser mics,

connected with an RC circuit and a 5V DC power supply, were used to record sound

signals on an oscilloscope. Perspex channel measuring 225 x 75 x 75 mm3 was used

to house the two mics and foam. Mics were fixed at a separation of 84 mm. The

testing setups are shown in Figure 2-6 and Figure 2-7 for sound speed measurement

in air and shaving foam respectively.

Figure 2-4: The graphical representation of bubbles coarsening of conventional

aqueous foams (a) Denim (b) Gillette

Figure 2-5: Shear rate vs viscosity plot for shaving foam

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The waveforms of sound signals were recorded on mic-1 and mic-2 and displayed on

two channels of oscilloscope. The time interval (T) between the two peaks was

recorded. Sound speed was calculated using the simple expression given in eq. (2.1).

𝐶0 =

𝑺

∆𝑻

(2.1)

Where, S is the distance between two mics and T is time interval obtained from

oscilloscope. The average sound speed measured in air at 240C was 345.8 m/s. The

sound speed is proportional to square root of the absolute temperature. From

literature, the sound speed in air at 240C is 343.0 m/s [5]. The relative error in

measured value with this setup was less than 1.0 %.

The Perspex channel and the complete path including the sound source, horn, was

then filled with shaving foam as shown in Figure 2-7 and T are measured to

compute the sound speed in foam. The recorded waveforms are shown in Figure 2-8.

The sound speed measured in shaving foam was 65.98±3 m/s. A significant reduction

in sound speed was observed in this two-phase medium compared to sound speed in

air and water.

Mic-1 Mic-2 Horn

Perspex channel

Figure 2-6: Setup for measuring sound speed in air

Horn

Foam in Perspex channel

Figure 2-7: Setup for measuring sound speed in shaving foam

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The two-phase mixture density and sound speed can be computed by Wood’s law

(also known as mixture law) given in eqs. (2.2) and (2.3) [6, 7].

𝜌𝑓 = 𝛼𝑊𝜌𝑊 + (1 − 𝛼𝑊)𝜌𝑎 (2.2)

1

𝜌𝑓 𝐶2=

𝛼𝑊

𝜌𝑊𝐶𝑊2 +

𝛼𝑎

𝜌𝑎𝐶𝑎2

(2.3)

Where W and a are volume fractions of water and air. The subscripts f, w and a

represents foam, water and air respectively. For a liquid volume fraction of 6.0% in

foam the density and sound speed computed from this relation are 61.15 kg/m3 and

52.69 m/s respectively. The measured values for density and sound speed are in close

agreement to the calculated values.

2.3 C4 Explosive

C4 or Composition C4 is RDX based explosive. The heat of detonation of C4 is 5.3

MJ/kg [8, 9]. The prevalent formulation is;

RDX 91.0%,

Di(2-ethylhexyl) Sebacate 5.3%,

Polyisobutylene (PIB) 2.1 %

20-weight motor oil 1.6%

A similar British formulation is known as PE-4 that comprises 88 % RDX and 12 %

plasticizer. An important characteristic of C4 is that it can easily be molded into any

desired shape. It can only be initiated by a shock wave [10]. A cylindrical geometry

was used in the present work. The velocity of detonation and C-J pressure of C4 used

a b

Figure 2-8: Waveforms (a) in air (b) in shaving foam

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in present work (at C4 density=1.46 g/cm3) were 7300 m/s and 19.98 GPa

respectively [8, 11].

2.4 Diagnostic Tools

2.4.1 High-Speed Photography

High-speed photography is used for recording transient phenomenon. The advances

in high-speed camera technology have enabled researchers to see dynamic events

taking place in microsecond time domain. The events may include gaseous discharge,

detonation, explosion of wires under high current and blast wave propagation. High-

speed camera was employed in present work for visual study of the blast wave

propagation and in particular for fireball measurement. The high-speed Phantom

camera was operated at frame rates of 8000 -54000 fps during these tests.

2.4.2 Pressure Transducers

Transducer is a device that converts one form of energy into another. Piezo-electric

(PE) gauges have been used to measure pressure time, P(t), history in a variety of

applications including- blast waves in air, propellant pressure in gun chamber and

combustion chamber pressure in rocket motors. Many different crystals generate

piezo-electric charge when strained. For pressure gauge application quartz has been

used as active material in most transducers because of its desirable electrical and

mechanical properties [12] .

The transducer comprises a stainless steel (SS) case with a coaxial electrical

connector at one end. A SS diaphragm closes the other end while covering the cavity

that contains the sensing element. The sensing elements are stacked quartz plates.

The applied pressure on the diaphragm compresses the quartz stack and produces

proportional charge output. The piezoelectric crystal generates a very small charge

which is amplified by a charge amplifier. If the charge amplifier is an external device

it is referred as charge output or PE sensor. If the electronic circuit is integrated in to

the sensor housing, it is referred as voltage output or IEPE sensor [12]. The

transducer and its orientation for measuring incident pressure (Ps) and reflected

pressure (Pr) are shown in Figure 2-9(a). Sensitivity of the transducer is expressed in

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milli-volts per psi (mV/psi). The coaxial cable simultaneously carries operating

power to the transducer and transmits the signal from it.

Kistler-PIEZOTRON 211B series pressure transducers (211B2, 211B3 and 211B5)

were used with the multi-channel coupler as a power source and amplifier for

transducer output. The Data Acquisition (DAQ) system comprises National

Instruments 16-bit, 1.25 MS/s hardware, which was coupled with eight-channel

noise, minimized differential signaling acquisition software to receive transducer

data. The data stored in the PC was plotted for P(t) history and impulse calculations.

The DAQ system may be operated in the frequency range of 100 kHz–1000 kHz. The

components of DAQ are shown in Figure 2-9(b).

Figure 2-9: (a) Transducers orientation for Pr and Ps measurement (b) Components of data

acquisition (DAQ) system

b

Transducer Multi Channel

Coupler

8-Channel Data Acquisistion

Systerm-(16-bit, 1.25MS/sec),

100-1000 kHz

Storage/Display Device

a

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2.4.3 Arrival Time Sensors

To augment the diagnostic equipment, cylindrical sensor/probe as shown in Figure

2-10 was developed and employed to measure the time of arrival (Ta) of blast waves.

The sensor comprised an aluminum cylinder, an axial pin electrically insulated from

the cylinder and a Brass foil of diameter 20 mm fixed at one end. The Brass foil and

pin were separated by a very small distance. The cylindrical casing and the pin were

connected through a cable to a recording device like an oscilloscope or a transient

recorder. The blast wave impact at the thin foil pushed the foil towards the axial pin.

The electrical path is completed with the contact of foil and the pin and a signal is

registered on the oscilloscope or the transient recorder. The sensors were placed in

parallel to the pressure transducers. The arrival time measured, for 82 grams C4

detonation, with the sensor was in close agreement with that of the pressure

transducer measurements, as shown in Figure 2-11. These sensors are quite

inexpensive.

a c b

Pin

Figure 2-10: (a) Arrival time sensor (b) section view (c) mounted in the fixture

Figure 2-11: Comparison of Time of arrival with pressure

transducer and arrival time probe

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2.5 Experimental Work

2.5.1 Blast Mitigation with Shaving Foam

Four Experiments were performed to evaluate the fireball suppression and blast

attenuation capabilities of shaving foam. All experiments were performed using C4

explosive. TNT equivalent of C4 is taken as 1.27 [13]. Cylindrical geometry of

explosive was used in the present work. Experiments were conducted with bare

charges as well as covered in shaving foam. The blast wave measurement and

recording equipment (DAQ system) are schematized in Figure 2-9(b). High-speed

photography was employed for visual study in particular, fireball measurement. A 2D

view of the experimental layout is shown in Figure 2-12.

C4 was placed on polystyrene (PS) foam of radius 21 mm and height 25 mm above a

4 mm thick plywood sheet as shown in Figure 2-13. The charge was initiated from

the top side with a Tetryl booster pellet and a detonator. The pressure sensors fitted

inside steel pipe measure incident pressure (Ps) whereas the sensor flush mounted

and facing the charge as shown in Figure 2-13(c) measures reflected pressure

(Pr).The blast wave parameters (Ps, Pr and Ta) were measured for bare 82 g C4

charge and covered in shaving foam of radius 0.2 m having volume 0.0168 m3

(weighing 1.0 kg). This shaving/aqueous foam has relatively lesser liquid volume

fraction (0.6). An increased liquid volume fraction enhances the mitigation as

reported by Kan et al [14, 15]. Therefore, 100 ml water was sprayed uniformly with

Figure 2-12: 2D view of Experimental Layout for blast

parameters measurement

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31

the foam. The transducers were placed 230 mm above the C4 stand to avoid the

recording of a reflected blast from the plywood stand.

The fireball formation and expansion with and without shaving foam are shown in

Figure 2-14 and Figure 2-15. The blast wave undergoes reflection when the forward

moving air molecules are brought to rest and further compressed upon meeting an

obstacle, thus forming a reflected overpressure. The reflected overpressure time

history Pr(t) and impulse at 0.8 m is presented in Figure 2-16. Testing setup and blast

wave parameters for the bare and foam-covered 82 g C4 at 0.85 m distance is shown

in Figure 2-17 and Figure 2-18 respectively.

Figure 2-14: High-speed images, 82g bare C4 detonation in air and propagation of

fireball

Figure 2-13: Test setup for measuring blast parameters for (a) bare charge (b) immersed in

shaving foam(c) Transducer orientation for measuring reflected pressure

a b c

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Figure 2-15: A sequence of events after detonation of charge immersed

in shaving foam

Figure 2-16: (a) Reflected overpressure (b) Impulse plots for 82g C4 blast

at 0.8 m for bare charge and covered in shaving foam

a

b

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Figure 2-17: Test setup for measuring 82g C4 blast parameters for (a) bare

charge (b) covered in shaving foam at 0.85 m

b a

Figure 2-18: (a) Incident overpressure and (b) Impulse profiles for 82g C4 bare

and covered in shaving foam at 0.85 m

a

b

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Another experiment was performed using 250 grams C4 charge. The charge was

immersed in 0.038 m3 volume (weighing 2.28 kg) of shaving foam without water

spray. Incident overpressure time history Ps(t) and positive impulse at 1.0 m distance

was measured and shown in Figure 2-19. Peak incident overpressure of 81 psi (558.4

kPa) and 32 psi (220.6 kPa) was recorded at 1.0 m distance for C4 detonation in air

and covered in shaving foam respectively. The corresponding blast wave arrival time

was 0.63 ms and 1.17 ms respectively.

Results for bare and foam-covered charges at different distances are presented in

Table 2-1. Arrival time (Ta) delay of 61%, peak pressure reduction of 72 and impulse

reduction of 61% were observed with shaving foam confinement. Since data was

clipped at 1.0 ms for sensor at 1.1 m distance, the impulse value for the shaving foam

should be higher than recorded. An extrapolated value of positive impulse is

tabulated at this distance.

Figure 2-19: (a) Pressure and (b) Impulse plots for bare 250g C4 blast at 1.0 m and

submerged in shaving foam

b

a

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Table 2-1 : Blast parameters for bare charges and covered in shaving foam

C4 Dist. Blast Parameters

Bare C4 charge With shaving foam

(g) (m) Ta(ms) Ps(psi) Pr(psi) Impulse

(psi-ms)

Foam

(grams)

Ta(ms) Ps(psi) Pr(psi) Impulse

(psi-ms)

82

0.50 0.23 143 7.93 1000 0.39 43 2.72

0.70 0.45 62 4.91 0.67 18 2.20

0.80 0.57 185 18.87 0.90 51 6.11

0.85 0.72 47.6 4.1 1.20 17 2.9

1.10 0.99 55

250

0.8 0.42 133 602 6.5 2280 0.74 42 141 3.51

1.0 0.62 81 6.2 1.17 32 4.86

250 0.8 0.42 133 6.5 2700 0.72 36 3.44

2.5.2 Effects of Foam Volume and Liquid Content on Mitigation

The test was repeated with an increased volume of shaving foam having a radius 0.28 m

and volume of 0.045 m3 (weighing 2.7 kg). Moreover, 300 ml water was uniformly

sprayed with the foam. The setup is shown in Figure 2-20. The pressure plot with

shaving foam is shown in Figure 2-21. About 76% overpressure reduction is observed in

this case. The increased volume of shaving foam around the charge and the liquid

volume fraction increased the attenuation level. Further experimental results are

presented in section 2.7.2.

--0.56m-

--0.76m-

250 g C4

Figure 2-20: Test setup for measuring 250g C4 blast parameters for bare

charge and covered in 0.05 m3 shaving foam

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2.5.3 Blast Parameters at Z < 1.0 m/kg1/3

Overpressure measurements were made within the shaving foam at scaled distances

(Z) less than 1.0 m/kg1/3

. The testing setup is schematized in Figure 2-22and Figure

2-23. The pressure transducers were fixed within the shaving foam at close distances

from the charge. The transducers and data cables were sealed and fitted in safety

jackets to avoid damage from fireball at such close distances. The charges weighing

150, 200 and 250 grams were detonated within the Perspex channels measuring

(1000 x 200 x 200) mm3 filled with shaving foam. The foam thickness behind C4

cylinder was 150 mm. The high-speed images for the blast mitigation within shaving

foam, shown in Figure 2-24, depict the rapid blast propagation in air (left side in each

image) and its attenuation inside the foam (right side in each image).

Figure 2-21: Peak incident pressure for 250g Bare C4 and covered in

shaving foam at 0.8m

a b

Figure 2-22: (a) Perspex channel filled with foam (b) Testing setup

within shaving foam

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Since the blast wave parameters for an open air HE detonation could not be measured

at such proximity due to fireball effects, therefore, numerical simulations were

performed to acquire blast parameters for bare charges at 0.20 – 0.50 m standoff

distances. Experimental and simulated results are shown in Figure 2-25 and Figure

2-26. Peak pressure of 731 psi (5040 kPa) measured at 0.25 m was reduced to 244 psi

(1682 kPa) at 0.3 m for 200 g C4 within shaving foam. The corresponding impulse

values were reduced from 74 psi-ms to 40 psi-ms.

b a c

Figure 2-24: High-speed images of 200g C4 detonation inside Perspex channel (a)

just after detonation (b) fireball expansion (c) product gasses expansion

a b

c

Figure 2-23: Experimental setup for measuring blast parameters for Z < 1 (m/kg1/3

) (a)

sensors fixed inside empty Perspex channel (b & c) shaving foam filled inside channel

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Figure 2-25 : Pressure and scaled distance plots for HE detonation in shaving foam for Z<1

The pressure-time history measured at 0.25 m and 0.30 m are shown in Figure

2-26(a). The impulse at these distances is also shown in Figure 2-26(b). Average

a

b

Figure 2-26: (a) Pressure and (b) Impulse plots for 200g C4 charge

detonated inside shaving foam at 0.25 and 0.30m from charge face

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peak pressure attenuation of 73% within the shaving foam is observed for Z<1. The

dry aqueous foam significantly reduced the peak pressure and positive impulse.

2.6 Numerical Modeling and Simulation

ANSYS AUTODYN [16] was used to develop models and simulate the blast wave

parameters for bare C4 detonation. Multi-material (MM) Euler solver was used to

simulate C4 detonation and expansion in air in axial-symmetric form.

2.6.1 Material Modeling

JWL (Jones-Wilkins-Lee) Equation of state (EOS) [17] was used for C4 detonation

and product expansion. The JWL EOS is given in equation (2.4).

𝑃 = 𝐴 (1 −𝜔

𝑅1𝑉) 𝑒−𝑅1𝑉 + 𝐵 (1 −

𝜔

𝑅2𝑉) 𝑒−𝑅2𝑉 +

𝜔𝐸

𝑉 (2.4)

Where E is the detonation energy per unit volume, V is the ratio of the detonation

product volume with the original volume of the explosive, and A, B, R1, R2 and ω are

empirical fitting parameters. Ideal gas EOS shown in equation (2.5) was used for air

surrounding the shell.

𝑃 = 𝜌𝑎(𝛾 − 1)𝑒 (2.5)

Where P is the pressure, is specific heats ratio (=1.4 for air), e is specific internal

energy and a is air density. The JWL parameters for C4, as shown in Table 2-2,

were calculated by EXPLO5 code [8]. The difference from the standard published

data was due to relatively lesser density of C4 used in the present study. The

parameters for Ideal gas EOS used for air were obtained from ANSYS AUTODYN

material library. The space surrounding the charge was filled with air for an initial

pressure of 101 kPa (14.7 psi) by assigning specific internal energy of 2.068e+5

kJ/kg. Flow out boundary condition was used at the boundaries. Material data for

polystyrene (PS) foam was taken from AUTODYN library. Material model for balsa

wood [18], as given in Table 2-2, was used for simulating the plywood sheet as data

for plywood was not available.

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Table 2-2: JWL parameters of C4, EOS data for Balsa wood and air

2.6.2 Blast Wave Parameters

The numerical simulation results of detonation events greatly depend on the mesh

size. An optimal mesh size that speeds up the calculations and give adequate results

is important [19]. The errors due to mesh discretization can be fixed by evaluating

the quality and adequacy of the mesh [20]. The discretization error in present

simulation work was minimized by optimizing the grid size. Simulation was run as

per experimental setup for bare 82 g C4 with different grid sizes and results are

presented in Table 2-3. Simulation with grid size of 1 x 1 mm2 reasonably well

reproduced the experimental results.

Table 2-3: Effect of grid size and discretization error in AUTODYN Simulation

The expansion of detonation product gases after the detonation of C4 in air and

subsequent formation of blast wave is schematized in Figure 2-27 and Figure 2-28

Simulations were run for bare 82 and 250 g C4.

JWL parameters for C4 Balsa wood

Equation of State JWL EOS Shock

Density (g/cm3) 1.46 Density (g/cm

3) 0.123

A 3.13640E+08 (kPa ) 1.415

B 6.39000E+06 (kPa ) C (m/s) 61

R1 4.0600 S 1.31

R2 9.80000E-01 Air

W 3.50000E-01 EOS Ideal gas

Detonation velocity 7.301E+03 (m/s ) Density (g/cm3) 0.00123

C-J-Energy/unit

volume

7.40E+06 (kJ/m3 ) 1.4

C-J Pressure 1.990E+07 (kPa ) e 2.068e5 kJ/kg

Stand

–off

Dist.

(m)

AUTODYN Simulation at different grid size Experimental

Results Grid

(mm2)

No. of

elements

Grid

(mm2)

No. of

elements

Grid

(mm2)

No. of

elements

4 x 4 41,250 3 x 3 80,000 1 x 1 353,000

Ta(ms) P(psi) Ta(ms) P(psi) Ta(ms) P(psi) Ta(ms) P(psi)

0.5 0.28 179.34 0.27 134.505 0.25 138.18 0.23 143

0.7 0.45 101.43 0.47 57.036 0.46 60.858 0.45 62

0.8 0.56 72.03 0.63 44.688 0.6 42.63 0.57 47.3

1.1 1.00 32.046 1.14 23.226 1.11 22.785 0.99 18.8

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A comparison of experimental and simulated results for overpressure and impulse

values is depicted in Figure 2-29 and Figure 2-30 respectively. The simulated results

for peak overpressures and arrival time were in close agreement to experimental

results; however, a discrepancy in impulse is observed.

a b

Figure 2-27: (a) ANSYS AUTODYN model (b) expansion of

detonation product gases after detonation of 250g C4

Figure 2-28: (a) Formation of blast wave and (b) propagation in air

a b

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2.7 Results and Discussion

The microscopic study of shaving foam revealed evenly distributed bubbles with an

average initial size of 15 m. The coarsening due to coalescence of bubbles slowed

down with time. The bubble size increased to 120 m in 2 hours showing good

stability. The viscosity of shaving foam measured at shear rate of 24.4 S-1

was 11650

Figure 2-30: Experimental and simulation results for 82g C4

bare blast, incident overpressure at 0.65 m and 0.85 m

Figure 2-29: Experimental and simulation results for 82g C4 bare blast, (a)

Incident overpressure (b) Impulse at 0.5m and 0.7m from charge center

a

b

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cP. The two-phase medium exhibited a decreasing viscosity trend at higher shear

rates. The density and average sound speed measured in shaving foam at temperature

of 240C was 60.0 kg/m

3 and 65.98±3 m/s respectively. The measured values were in

good agreement to the values calculated using mixture law or Wood’s formula [6].

Several experiments were performed with bare C4 charges and covered in shaving

foam. A computer program written in Python was used to plot the pressure-time

history of the transducer’s data. Impulse was computed by integrating the pressure-

time plot for positive phase duration. The blast wave parameters obtained for bare

charges were compared with Kingery-Bulmash (KB) blast parameter calculator [21,

22]. Results are presented in Table 2-4.

Table 2-4: Comparison of bare charge tests with Kingrey-Bulmash (KB) results

A discrepancy in measured peak pressure and impulse values with the KB

calculations was observed. The reason for this deviation is the geometry of the

charges and the relatively lower density (1.46 g/cm3 in contrary to 1.6 g/cm

3) of C4

explosive used. Cylindrical shape (L/D1) of C4 was used in the present work

contrary to the hemi-spherical shape assumed for KB calculations. Moreover, tests

were conducted by placing the explosive on a 4.0 mm thick plywood sheet that was

770 mm above the ground level. This setup has not provided the same magnitude of

reflection as obtained for hemi-spherical surface burst charges. The higher pressures

generated in surface burst charges lead to higher values of positive phase duration

and consequently the higher impulse values.

C4

mass

Dist. Blast Parameters for bare charges

Present Experimental work Kingrey-Bulmash (KB)

(g) (m) Ta(ms) Ps(psi) Pr(psi) Impulse

(psi-ms)

Ta(ms) Ps(psi) Impulse

(psi-ms)

82 0.50 0.23±0.01 143±4 -- 7.93±0.2 0.25 173.4 15.4

0.70 0.47±0.02 61±1.5 -- 4.71±0.12 0.46 81.73 11.8

0.80 0.57±0.03 -- 185±9 18.87±0.45 0.60 58.8 10.4

0.85 0.73±0.03 46.6±1.3 -- 4.1±0.11 0.67 51.45 9.9

1.1 0.98±0.04 -- 56±2.8 -- 1.08 28.95 7.7

250

0.8 0.41±0.02 133±3.6 -- 6.5±0.16 0.43 141 21.5

0.9 0.56±0.02 95±2.7 -- 4.76±0.12 0.53 108 19.7

1.0 0.62±0.03 81±2.1 -- 6.2±0.15 0.65 85 17.8

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2.7.1 Fireball and Afterburning Suppression

The suppression of fireball and the attenuation of highly pressurized product gases is

important for mitigation purposes. The dry aqueous foam, when placed on charge,

appears to serve this purpose [23]. Generally, a fireball is related to hot products

which emit light when sufficiently hot [8]. C4 (C3.86H7.57N5.22O5.32) has an oxygen

balance of −46.6%. The detonation products contain a lot of C(solid), CO, H2 etc.

During expansion some products are further oxidized (e.g. C and CO to CO2, H2 to

H2O, etc.) producing additional heat. This process is called afterburning reactions.

Total heat of combustion is, thus, the sum of detonation heat and afterburning heat.

For C4 the heat of detonation is only 44% of the total combustion heat [9]. EXPLO5

calculations for C4, assuming all combustible products (Cs, CO, H2…) are fully

oxidized, yielded the following results [8];

Heat of detonation 5.137 MJ/kg

Afterburning heat 6.145 MJ/k

Total heat of combustion 11.282 MJ/kg

The experimentally measured value of heat of detonation for C4 is 5.1±0.2 MJ/kg

[9]. It is worth mentioning here that the latent heat of vaporization for water is 2.25

MJ/kg and its specific heat capacity at constant pressure is 4.187 kJ/kg-K. That is

why water is able to absorb the energy of detonation (and combustion) of high-

energy explosives, provided it is aerosolized [24]. The even distribution of thin liquid

films covering micron sized gas bubbles in shaving foam readily evaporate under C4

detonation conditions and reduced the temperature to a level that suppressed fireball

and the afterburning reaction.

Fireball was measured with the help of high-speed images and is shown in Figure

2-31 - Figure 2-33. The detonation of bare 82 g C4 produced an initial fireball radius

of 0.8 m as shown in Figure 2-31(a, b). The afterburning in this fireball resulted in

formation of the secondary fireball with radius 1.1 m. The sequence of events with

increasing time is shown in Figure 2-31(c - f).

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For C4 covered in shaving foam, the fireball appeared below the stand as shown in

Figure 2-32(a), while mainly suppressed by the shaving foam above the plywood

stand. The expansion of carbonaceous soot is more pronounced in Figure 2-32(b, c).

Fireball for bare 250 g C4 could not be measured accurately as it exceeded the

window diameter of 2.0 m as evident from Figure 2-33(b, c). The actual radius

was greater than 1.0 m. The fireball measurement and suppression for 250 g C4

covered in shaving foam is shown in Figure 2-33(d, e, f). The emergence of fireball

and partial suppression indicates that the volume of shaving foam for this charge was

insufficient.

a b c

f d e

Figure 2-31: Fireball for bare 82 g C4 (a, b) and formation of secondary fireball (c, d, e, f)

b

c

a

-0.25m

-0.76m

Figure 2-32: (a) Fireball formation and (b, c) quenching for 82 g C4 covered

in shaving foam

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The presence of much higher concentration of carbonaceous soot (C) in high-speed

images shown in Figure 2-32(a, b, c) is an evidence of the suppression of

afterburning reaction and, hence, the reduction of the fireball radius. Almost 80%

reduction in fireball was observed with this shaving foam. The measured data is also

presented in Table 2-5.

Table 2-5: Fireball radius for C4 detonation in air and with shaving foam

C4 (g) Fireball Radius (m)

In air With shaving foam

82 1.1±0.01m 0.125±0.01m

250 >1m 0.265±0.01m

2.7.2 Peak Pressure and Impulse Reduction

The shaving foam confinement slows down the shock propagation due to high

compressibility of gas bubbles in aqueous foam. The bubbles readily accommodate the

change in volume caused by the pressure [23]. This deformation of gas bubbles and the

final bursting of the thin liquid films dissipate energy and cause blast wave mitigation.

The reduction in pressure is also attributed to lower sound speed of this two-phase

medium. The presence of air between the transducers and shaving foam, as shown in the

experimental setups, also plays a role in mitigation. An impedance mismatch at air-

shaving foam interface attenuates the overpressure and impulse [25]. The impedance is

the resistance offered by a material to transmission of shock and is the product of initial

density (0) and shock velocity (Us) [26]. Stated simply, the shock impedance is

-= 2.0m-

a

-=2.0m-

b

-= 2.0m-

c

d

--0.53m-

f

--0.53m-

e

Figure 2-33: Fireball for 250 g C4 (a, b, c) bare C4 and (d, e, f) covered in shaving foam

Page 74: EXPERIMENTAL AND NUMERICAL STUDIES OF BLAST, …

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analogous to acoustic impedance. The numerical values of acoustic impedances (C00)

of shaving foam and air are 3904 and 419 respectively, showing a difference of an order

of magnitude at the interface.

The overpressure and impulse reduction for 82 g C4 charge at a distance of 0.5 m is

depicted in Figure 2-34. Peak pressure reduction of 68 – 74 % is recorded for 82g C4

tests at 0.5, 0.7 and 0.8 m distances. An average impulse reduction of 63% is recorded,

corresponding to these overpressure values. The 250 g C4 produces stronger effects and

requires more shaving foam confinement (foam radius> 0.28 m). A shaving foam

confinement of radius 0.28 m with uniform water spray of 300 ml was used for 250 g

C4. The incident overpressure-time history for this charge is shown in Figure 2-35.

Figure 2-34: Incident pressure and Impulse plots for 82g C4 blast at 0.5 m-

for bare charge and submerged in shaving foam

Figure 2-35: (a) Peak incident pressure and (b) impulse plots for 250 g Bare C4

and covered in shaving foam at 0.9 m

a

b

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48

The Figure 2-35 indicates a pressure reduction of 80% for the above stated setup. The

test was then repeated without external water spray with shaving foam and blast

parameters were measured at 0.8 m distance. The incident and reflected peak

pressure plot and the corresponding impulse plot are shown in Figure 2-36. The

reflected pressure plots are overlapping the incident overpressure plots. Peak

reflected pressure reduced by 74% whereas the reduction in peak incident pressure

was 68%. Impulse reduction of 60% was observed. The additional water or higher

liquid content available in confinement slightly enhanced the blast mitigation. That is

why wet aqueous foams provide better attenuation against blast waves. Figure 2-37

depicts the variation of peak pressure with distance for bare and shaving foam-

covered C4.

Figure 2-36: Incident and reflected pressure plot (left) and impulse

plot (right) for 250g C4 at 0.8m

a

b

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Figure 2-37: Peak pressure and distance plots with and without shaving

foam for (a) 82 g C4 (b) 250 g C4

a

b

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investigation of various water-induced explosion mitigation

mechanisms(2007).

[25] A. Britan, H. Shapiro, M. Liverts, G. Ben-Dor, A. Chinnayya, A. Hadjadj,

Shock Waves. 23(2013) 5.

[26] X. Kong, W. Wu, J. Li, F. Liu, P. Chen, Y. Li, Materials & Design. 51(2013)

729.

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52

Characterization of Shell Chapter 3

Fragmentation

3.1 Introduction

The detonation of an explosive device results in the formation of a blast wave in air.

When an explosive is encased, the detonation energy and momentum are partitioned

into formation of fragments and the blast wave [1]. Fragmentation is the breaking of

shell body into a number of pieces. It is a complex phenomenon where the

fragmenting material fractures under intense shock wave loading produced by the

detonation of high explosive. The fragmentation process starts with the radial

expansion of the casing material. The outer surface fractures develop into cracks and

grow to the inner casing surface. The highly pressurized explosive product gases

begin to flow through the cracks, causing massive venting. The casing expands to 50-

60 % of the initial diameter [1]. Once the metal casing starts to break, the highly

pressurized product gases escape, resulting in the formation of a blast wave [2]. The

blast wave propagates outwards and leads the fragments. The neighboring objects are

first hit by this blast wave followed by the high velocity fragments, causing severe

damage. The highly accelerated fragments have sufficient energy to penetrate hard

targets and damage vulnerable components. The understanding of the fragmentation

phenomenon is important to devise protective measures against the damaging effects

[2, 3]. The fragment velocity, shape and mass distribution are important parameters

in the characterization of the fragmentation process [2]. Mott and Linfoot [4],

presented the relationship for fragment mass distribution given in eq. (3.1);

𝑁(> 𝑚) = 𝑁0exp [−(𝑚 𝛽)⁄ ] (3.1)

Where m is the fragment mass, N(>m) is the number of fragments with mass higher

than m, No is total number of fragments and is fragment size variable [1]. The

fragment mass distribution and velocity vectors are important to the assessment of

the lethal radius of a munition. The lethal radius is evaluated based on the velocity of

fragments and average fragment mass [5]. Gurney [6] proposed a relation for

estimating initial fragment velocity for cylindrical casing exploded under energetic

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53

filling. The relation, given in eq. (3.2), is used for the computation of the fragment

velocity of a cylindrical shell.

𝑉 = √2𝐸 √

𝐶𝑀

1 + 0.5 𝐶𝑀

(3.2)

Where C and M are explosive and metal mass per unit length and √2𝐸 is the Gurney

constant for the explosive in km/s. This constant can also be approximated as;

√2𝐸 = 0.338𝐷, where D is the detonation velocity [7]. Huang et al [8] proposed a

relationship for initial fragment velocity calculations along the axis of cylindrical

casing by incorporating the influence of rarefaction waves at the ends. The velocity

relation shown in eq. (3.3) is given by;

𝑉 = (1 − 0.361𝑒1.111𝑥 𝑑⁄ )(1 − 0.192𝑒3.03(𝐿−𝑥) 𝑑⁄ ). √2𝐸 √𝐶

𝑀

1+0.5 𝐶

𝑀

(3.3)

Where x is the distance to the detonation end along the axis of cylindrical casing, d is

the explosive diameter and L is length of the casing.

3.1.1 Effects of Fragmentation

Fragmentation is the most lethal among cased explosive detonation effects because

fragments can fly large distances and cause serious injuries to humans [9]. Injuries to

personnel due to fragment impact can be classified into primary fragment and

secondary fragment injuries. Primary fragments are usually small, having high-

velocities that cause injury by penetration and perforation of vital organs of the body.

Secondary fragments are usually larger and have less velocity. Upon impact these

can cause non-penetrating blunt force trauma. Therefore, it is very difficult to

effectively deal with this mechanism. It necessitates a higher mass solution or an

expensive lightweight ballistic protection technique [3, 10].

3.2 Characterization

The fragment initial velocity, shape and mass distribution are important parameters

in the characterization of the fragmentation process. For this purpose, a scaled down

artillery shell (155mm) was considered. The field testing and required data

acquisition for a standard shell is a difficult task and requires significant resources.

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Therefore, a geometrically scaled down (1:4) model of this shell was selected to

investigate its blast and fragmentation effects on the surrounding. The shell, as

shown in Figure 3-1, comprised a hollow steel casing filled with 104 grams of Comp-

B explosive. The Comp-B filling is illustrated in the cut-view of Figure 3-1(b). The

other parameters of shell along with parameters of a standard 155 mm shell are

presented in Table 3-1.

Table 3-1: Material and dimensions of scaled down and standard 155mm shell

Mass

(g)

Length

(mm)

Cyl.

OD(mm)

ID (mm)

Scaled down

shell

Steel casing 450 140 37 28

Comp-B 104 127 28 --

Standard

155mm Shell

Steel casing 35700 630 154 132

Comp-B 6800 535 133 --

3.2.1 Experimental Work

Three experiments were conducted with this scaled down (1:4) model to study the

blast and fragmentation effects. Pressure transducers were used with Data

Acquisition (DAQ) system to measure peak overpressure (Ps) and arrival time (Ta) of

the blast wave at different distances from the shell center. The experimental layout is

shown in Figure 3-2.

Figure 3-1: (a) scaled down shells (b) its cut-view (c) standard 155mm shell

b c a

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The destructive potential of fragments is a function of their kinetic energy distribution.

Therefore, the initial velocity and mass distribution of the fragments need to be

determined [9]. Fiberglass and plywood sheets were employed to witness the fragment

impact. Flat Brass probes were used to measure the fragment velocities. The following

sections describe the characterization of the shell fragmentation.

Flat Brass timing probes, shown in Figure 3-3, were used to measure the fragment’s

velocity and arrival time at predefined distances. The probe comprised two Brass

foils, measuring 125 x 125 and thickness 0.1 mm, separated by a 0.1 mm thick Mylar

sheet. The Mylar sheet has enough strength to provide sufficient insulation. A cable

was used to connect the two Brass foils with a recording device like an oscilloscope

or a transient recorder. A magnified section view of probes is shown in Figure 3-3(c).

Upon impact and penetration by a metallic fragment, the electrical path was

completed momentarily and the event was registered by a recording device. Two

such probes, when placed in parallel and separated by fixed distance (S), as shown

in Figure 3-3(d), can record the fragment’s impact time. The fragment’s velocity was

computed with the help of the measured time interval and known separation distance

of the probes. The probes were fixed rigidly to avoid any disturbance by the

approaching blast wave.

Timing Probes

Fiberglass

Plywood sheets

Tran

sdu

cers

Shell

Figure 3-2: Layout for blast and fragmentation tests of scaled

down shell

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Fragment velocities from different locations of the shell were measured using these

timing probes. The brass probes were also placed just below the shell base to find the

fragments velocity and number of fragments from this part of the shell. The setup is

shown in Figure 3-4.

The spatial distribution of the fragments was determined with the help of holes in

fiberglass and plywood witness plates penetrated and perforated by fragments. Two

fiberglass sheets measuring 457 x 457 x 10 mm3 and spanning 25.8

0 both in azimuth

and in elevation were placed one meter apart from the center of the scaled shell for

test 1. The testing setup is shown in Figure 3-5(a). For the other two experiments,

plywood sheets measuring 600 x 600 x 8 mm3 as shown in Figure 3-5(b) were placed

at 700 mm from the shell. The plywood sheets spanned 46o in azimuth and 44

o in

elevation. A layout of the experimental setup is shown in Figure 3-6.

a b

Brass

Insulator

Brass

c

S

d

Figure 3-3: (a) Flat Brass probe (b) 3-D view(c) section view (d) Two probes setup

a b

Figure 3-4: Flat probes arrangement for fragment velocity

measurement (a) test-1 (b) test-2

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57

F/G

Sheets

Timing

Probe

s

Shell

a

Plywood

Sheet

b

Figure 3-5: Testing setup with (a) fiberglass (F/G) sheets and timing

probes (b) plywood sheet

Figure 3-7 and Figure 3-8 show the impact and perforation of fragments through

fiberglass and plywood witness sheets which were used to estimate the total number

of fragments and their spatial distribution.

Plywood

sheets

Shell

Brass sheet

a b

Figure 3-6: Setup for fragments impact and spatial

distribution (a) Test-2 and (b) Test-3

a b c

Figure 3-7: Fiberglass witness sheets (a, b) before and (c) after fragments impacts

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The majority of the fragments, especially small ones, could not be recovered. A few

of the recovered fragments are shown in Figure 3-9. The fragments’ mass, size and

velocity distribution is presented in the results and discussion section.

3.3 Numerical Simulation

ANSYS AUTODYN [11] was used to simulate the fragmentation phenomenon of the

scaled down shell. Smoothed Particle Hydrodynamics (SPH) solver was used to

simulate explosively driven fragmentation. Being a mesh-free method, SPH can

handle nonlinear problems with large deformation without mesh degeneration or

tangling. Unlike Lagrange solver non-physical numerical erosion model is not

required [12]. Euler Multi-Material (MM) solver coupled with ALE was used to

simulate the blast phenomenon of the exploded shell in air.

a b

Figure 3-8: Plywood witness sheets (a) before and (b) after the fragments impact

Figure 3-9: Fragments recovered in the tests

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3.3.1 Material Modeling

JWL (Jones-Wilkins-Lee) [13] equation of state (EOS) was used for expansion of

Comp-B product gases. The JWL parameters for Comp-B were used from ANSYS

AUTODYN material library. Ideal gas EOS was used for air surrounding the shell.

Steel AISI-1006 was used as the casing material. The Shock EOS (Mie-Grüneisen

form) [14] was used as the equation of state model for Steel-1006. This EOS, shown

in equation (3.4), is widely used for materials under shock loading.

𝑃 = 𝑃𝐻 + 𝜌(𝐸 − 𝐸𝐻) (3.4)

The Johnson–Cook strength model [15] was used to simulate the behavior of the steel

(AISI-1006) shell under high strain rate loading of explosive detonation. The model

presented in equation (3.5) reproduce very well the strain hardening, strain rate and

thermal softening effects of steel casing subjected to such high strain rate loading.

𝜎𝑦 = [𝐴 + 𝐵𝜀𝑝𝑛][1 + 𝐶 𝑙𝑛 𝜀𝑝

∗][1 − 𝑇𝐻𝑚] (3.5)

Where A, B, C, n and m are constants for each material and TH is homologous

temperature. The material model parameters for steel, Comp-B and air were used

from ANSYS AUTODYN library. The Johnson-Cook failure model [16] shown in

equation (3.6) was used along with the strength model for casing material (AISI-

1006).

𝜀𝑓 = [𝐷1 + 𝐷2 𝑒𝐷3𝜎∗ ][1 + 𝐷4 𝑙𝑛|𝜀∗|][1 + 𝐷5𝑇𝐻] (3.6)

The values of constants D1 to D5 for steel 1006 are presented in Table 3-2.

Table 3-2: Johnson Cook damage parameters for Steel-1006 [17]

D1 D2 D3 D4 D5

-0.8 2.1 0.5 0.0002 0.61

3.3.2 Fragmentation of Shell

The computational grid influences the accuracy and reliability of the numerical

prediction results [18]. A particle size of 1 was used for packing after optimizing the

size for SPH solver [3, 19]. Quarter geometry of the shell was modeled with 28820

nodal points to reduce the computational time. The shell model and gauge points

defined on steel casing are shown in Figure 3-10.

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60

ANSYS AUTODYN generates fragment analysis when material status plot option is

activated or checked in during the simulation. When fragmentation option is checked,

it can output fragment analysis in HTML format. The analysis comprised number of

fragments alongside mass, kinetic energy, momentum, length, origin, coordinates and

velocity of each fragment. The fragmentation of shell casing at different time and the

venting of pressurized detonation product gasses are shown in Figure 3-11and Figure

3-12. The escape of product gases leads to the formation of the blast wave which

surpasses the fragments.

Figure 3-10: SPH Model of scaled down shell with gauge points

b a c

Product Gases

Steel Fragmenting

Figure 3-11: Fragmentation process (a) at 27 s (b) at 48 s (c) venting of

product gases

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The number of fragments and their mass distribution is schematized in Figure 3-13.

Fragments with mass ranging from tens of milligrams to a few grams were produced.

The fragments’ velocity profile is shown in Figure 3-14. The fragment mass

distribution and velocity are important to evaluate the hit density and lethal radius

calculations [5].

0

25

50

75

100

125

150

175

200

No

. of

Frag

men

ts

Mass (g)

No. and mass distribution of fragments scaled down shell)

Figure 3-13: Number of fragments and mass distribution

Figure 3-12: Fragmentation process and radial expansion with time (a) at 57 s (b) at

80 s and (c) 150s (d) at 200 s (e) at 250 s

a b c

d e

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The velocity distribution with the number of fragments is shown in Figure 3-15. The

majority of the fragments exhibited velocities ranging from 1000 - 1400 m/s. Only a

few fragments have velocities below 800 m/s.

3.3.3 Blast Parameters for Shell Detonation

Simulation for blast parameters was performed using coupled ALE-Euler Multi-

Material (MM) approach in ANSYS AUTODYN. The hollow steel shell was

modeled in ALE whereas Comp-B filling and surrounding air were modelled in Euler

MM solver. The ALE mesh was embedded inside the Euler MM fixed mesh. The

interaction between the two solvers was controlled by an automatic coupling option

available in ANSYS AUTODYN. An optimized grid size of 1x1 mm2 was used for

both solvers [3, 19].

a b

Figure 3-14: Fragment velocities of gauge points defined on shell

casing (a) with ALE solver (b) with SPH

Figure 3-15: Number of fragments and their velocity distribution

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63

The air surrounding the shell was filled for ambient pressure of 101 kPa (14.7 psi) by

assigning specific internal energy of 2.068e+5 kJ/kg. Flow out boundary condition

was used at the Euler subgrid boundaries. The numerical model of the shell,

detonation propagation and expansion were shown in Figure 3-16. The Comp-B

filling was completely detonated in 15.8 s. The expansion and fracturing of the

casing material lead to initial escape of product gases and the subsequent formation

of a blast wave in air. The venting of product gasses at 40 s, subsequent blast wave

formation and its propagation in surrounding air is depicted in Figure 3-17. The

radial propagation of blast wave with time is shown in Figure 3-18.

a b c

Figure 3-16: (a) AUTODYN model of shell (b) detonation

wave propagation inside shell (c) Expansion of shell at 20 s

Gas

es v

enti

ng

a b c

Figure 3-17: (a) Venting of pressurized gases in air at t= 40 s and

expansion (b) at t= 61 s (c) at 90 s

a b c

Figure 3-18: (a) Blast wave propagation in air at t=0.150ms, (b) at t= 0.604ms

and (c) at t= 0.88ms

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64

The pressure-time history at gauge points was integrated for positive phase duration

to obtain positive impulse. The peak incident pressure and positive impulse at

distances of 0.60 m and 0.76 m for simulated and experimental results are shown in

Figure 3-19. The blast arrival time and peak pressure values were in close agreement

with the experimental findings. However, a discrepancy in impulse was observed at

0.60 m distance.

3.4 Experimental Results

Three tests were conducted with a geometrically scaled down (1:4) model of the 155

mm artillery shell to study the blast and fragmentation characteristics. A simple

experimental approach was employed to measure the fragments’ velocity. The testing

setup with the timing probe for fragments’ velocity measurement is shown in Figure

3-20(a, b).

a

b

Figure 3-19: Simulated and experimental (a) peak Pressure and (b) Impulse plots

for scaled down shell

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The fragments’ impacts on the timing probe can also be witnessed in Figure 3-20(c).

The impact time (t1) of the fragment on front probe was registered by an oscilloscope

and transient recorder. When this fragment perforated the second probe (placed

behind the front one), time (t2) was recorded. Fragment velocity was computed by

dividing the distance between the two probes (S) as shown in Figure 3-21(a) by the

time interval t. The penetration time through Brass probe is much smaller compared

to the total flight time of fragment and is therefore ignored for velocity calculations.

The fragment impact and arrival time at timing probes placed at 430 mm and 710

mm from shell center is shown in Figure 3-21(b) and Figure 3-21(c) respectively.

The impact time of the fragments produced from different locations of the shell

(base, cylindrical, conical etc.), as shown in Figure 3-22, was recorded with the help

of oscilloscope and transient recorder. The velocities were calculated from the known

distances (S) and recorded time intervals (t).

Timing

probes

a b c

Figure 3-20: (a, b) Fragment's velocity measurement from different parts of

the shell (c) timing probe after fragment impact

b c

t1

t2

a

s

Figure 3-21: : (a) Two probes setup (b) Fragment’s impact on

timing probe and (c) arrival time for velocity calculations

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66

Fragment velocities ranging from 960 to 1555 m/s were measured for different parts

of the shell. Fragments from the cylindrical portion of the shell were found flying

with maximum velocities of 1346 to 1555 m/s due to the highest C/M ratio.

Fragments with relatively lesser velocities were produced from conical region on

account of a smaller C/M ratio. However, the minimum velocity of 960 m/s was

recorded for fragments produced from the base region of the shell as this was the

thickest metal portion. The fragments from this part of the shell were most likely to

be relatively massive. The fragment velocities were also computed from Gurney

relation [6] given in eq. (3.2 and Huang modification [8] shown in eq. (3.3). A

comparison is presented in Table 3-3.

Table 3-3: Comparison of experimental, numerical and analytical fragments velocities

The measured fragments velocities were found closer to Huang modified

formulation; however, Gurney relation predictions were also in close agreement with

other methods for the cylindrical part of the shell. The fragment velocities simulated

by ANSYS AUTODYN were in close agreement with the experimentally measured

Position Fragment velocity (m/s)

Frag. Velocities measured Experimentally Autodyn Gurney Huang

S1 mm

t1 ms

S2 mm

t2 ms

S t V=S/t m/s m/s m/s

mm ms m/s

Cylindrical 430 0.276 710 0.456 280 0.180 1555 1510 1340 1349

Cylindrical 500 0.379 675 0.509 175 0.130 1346 1350 1340 1349

Base 370 0.307 550 0.484 170 0.177 960 910 -- --

Conical 500 0.520 -- 500 0.520 961 1025 1123 948

Base

Cone Cylinder

1 2 3 5 6 7

11

Figure 3-22: Different positions of shell for fragment velocity calculations

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67

values. The proposed method provides a fairly economical and simple approach to

measure fragment velocities accurately.

The total number of fragments produced could not be collected as the fragments

dispersed over a large area. Two fiberglass sheets each measuring 457 x 457 mm2

and spanning 25.80 both in azimuth and in elevation placed at a distance of 1.0 m

from the shell witnessed the fragment impact for test-1 as shown in Figure 3-23.

Plywood sheets measuring 600 x 600 x 8 mm3 and spanning 46

0 in azimuth and

elevation were used to witness the impact and penetration/perforation for the second

and third experiments. Fragments weighing tens of milligrams to a maximum of 6.3 g

were observed to impact the fiberglass/plywood sheets, as can be seen from Figure

3-24. Most of the small-sized fragments could not be recovered. A few of the

fragments recovered are shown in Figure 3-9 of the experimental work section. The

mass and size of recovered fragments are presented in Table 3-4. ANSYS

AUTODYN results are also tabulated for the corresponding recovered fragments.

a b c

Figure 3-24: (a, b) Plywood witness sheets (c) Timing probe

placed below the shell base

Figure 3-23: Fragment impacts and perforation through Fiberglass witness sheets

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Table 3-4: Measured mass and size of the recovered fragments- comparison with simulation

results

Measured

Mass

(g)

Measured ANSYS AUTODYN

Length

(mm)

Width (mm) Length

(mm)

Mass (g)

3.9±0.1 29.8±0.7 9.4±0.2 46 4.07

3.69±0.1 48±1.2 6±0.1 40.52 4.10

3.0±0.1 37.8±0.9 5.4±0.1 31 2.63

1.5±0.05 21.9±0.5 6.7±0.1 15.35 1.46

0.9±0.04 10±0.2 8±0.2 11.94 0.35

0.9±0.04 12.6±0.3 4.5±0.1 12 0.52

0.6±0.03 10.5±0.2 4.8±0.1 14.7 0.56

0.3±0.02 13.8±0.3 5.4±0.1 9.96 0.30

0.2±0.01 7.3±0.2 4.9±0.1 8.8 0.31

0.4±0.02 7.8±0.2 4.2±0.1 10.33 0.33

Considering the shell geometry and assuming a symmetrical fragment distribution in

radial direction, as witnessed from the fiberglass and plywood sheets shown in Figure

3-23 and Figure 3-24, the total number of fragments was grouped into the following

three categories.

Small (< 0.04g)

Medium (0.04 - 0.4g)

Large (0.41 – 6.5g)

0

200

400

600

Small Medium Large

No

. of

Frag

me

nts

No. of Fragments and Mass Distribution

Experimental

Simulation

Figure 3-25: Number of fragments and their mass distribution for

scaled shell

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69

A comparison of the number of fragments and their mass distribution is presented in

Figure 3-25. Most of the fragments have mass less than 0.5 g. The SPH simulation

results shown in Figure 3-25 provided a good agreement with the experimental

findings. A few of the recovered fragments of masses ranging between 0.2 – 3.9 g

were in fair agreement with the simulation results.

The peak overpressures (Ps) at 0.55, 0.59, 0.60, 0.65, 0.675 and 0.76 meter distances

were recorded. The pressure time history for experimental and simulated data at four

of the above stated distances are shown in Figure 3-26. Peak overpressure values of

44.2 psi (304.7 kPa) at 0.55 m and 23.38 psi (161.2 kPa) at 0.675 m were measured.

The corresponding time of arrival (Ta) was 0.505 ms and 0.733 ms respectively.

Incident impulse of 3.3 and 1.8 psi-ms were computed corresponding to these peak

overpressure values.

A summary of the experimental and simulated results is presented in Table 3-5. A

good agreement between simulated and experimental results for the blast parameters

was obtained for the scaled down model of 155 mm artillery shell. Therefore, one

a

b

Figure 3-26: : Experimental and simulated peak incident pressure plots at

(a) 0.55m & 0.65m (b) 0.59m & 0.675m

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70

can utilize the simulation techniques to predict the blast and fragmentation effects of

such munitions and hence minimize the cost and time spent on full scale testing.

Table 3-5: Summary of the experimental & simulation Pressure-time values

Distance Experimental Results Simulation Results

R(mm) Ta(ms) Ps(psi) Ta(ms) P

s(psi)

550 0.505 44.2±1.1 0.507 43.08

590 0.573 36.54±0.9 0.57 36.22

600 0.603 35.5±0.9 0.59 34.87

650 0.668 26.5±0.6 0.675 28.85

675 0.733 23.38±0.5 0.720 26.43

760 0.882 16.79±0.4 0.887 18.94

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71

References

[1] R.M. Lloyd, Reston, VA: American Institute of Aeronautics and

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[3] K. Ahmed, A.Q. Malik, A. Hussain, I.R. Ahmad, I. Ahmad, AIP Advances.

10(2020) 095221.

[4] N. Mott, E. Linfoot, HA theory of fragmentation(1943).

[5] G. Tanapornraweekit, W. Kulsirikasem, International Journal of Mechanical

and Mechatronics Engineering. 6(2012) 1070.

[6] R.W. Gurney, The initial velocities of fragments from bombs, shell and

grenades(1943).

[7] B. Zecevic, J. Terzic, A. Catovic, S. Serdarevic-Kadic. Influencing

parameters on HE projectiles with natural fragmentation. in International

Conference on New Trends in Research of Energetic Materials. 2006.

[8] G.-y. Huang, W. Li, S.-s. Feng, International Journal of Impact Engineering.

76(2015) 20.

[9] E. Lozano, Design and analysis of a personnel blast shield for different

explosives applications(2016).

[10] K.J. Sharpe, J. Waddell, J.F. Gordon, Explosive effect mitigated containers

and enclosing devices(2008).

[11] U. ANSYS Inc., Century Dynamics. Release 14.0 documentation for ANSYS

AUTODYN.(2011).

[12] M.A. Abdalla. Fragmentation Analysis of OG-7 Warhead Using AUTODYN

SPH Solver. in Advanced Materials Research. 2012. Trans Tech Publ.

[13] E. Lee, H. Hornig, J. Kury, California: University of California, (1968).

[14] M.A. Meyers, Dynamic behavior of materials. (1994.

[15] G.R.a.C. Johnson, W.H. A Constitutive Model and Data for Metals Subjected

to Large Strains, High Strain Rates, and High Temperatures. in Proceedings

7th International Symposium on Ballistics. 1983. Hague.

[16] G.R. Johnson, T.J. Holmquist. An improved computational constitutive

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[17] B. Adams, M. Geers, v. Dommelen, A. Huizinga, Simulation of ballistic

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73

Protective Configurations against Chapter 4

Fragments

4.1 Protective Mechanisms

Protective systems are usually comprised of high strength steel, ceramics, and

composite materials etc. to defeat impacting fragments/projectiles [1]. But armor

steel becomes too heavy while Ceramics are inherently brittle and may cause

secondary fragmentation unless treated properly. The development of a protective

system depends on the type of threats to be defeated. However, several lightweight

materials are available for use in a protective configuration. Ceramics, fibre-

reinforced polymers (FRP) and porous materials are a few that were selected for this

study. These materials offer high strength at much lower densities. In present study,

the protective mechanism was configured to undermine the momentum of incoming

threat (projectile/fragment) and subsequent dispersion and absorption of the energy

produced in the form of shock waves.

4.1.1 Momentum Disruption

The explosively driven fragments/projectiles (bullets etc.) can move at very high

velocities. However, unlike bullets, fragments do not have regular shapes required

for deep penetration/perforation of hard targets. The momentum of these fragments

can be disrupted using a high strength material capable of resisting penetration from

compressive forces and spreading the momentum before it damages the target [2].

Ceramics like silicon carbide (SiC), alumina (Al2O3), boron carbide (B4C), etc. have

been used for the containment of blast and fragment penetration due to their high

hardness and erosion properties. These are highly brittle and are usually backed by

metal plates. The backup metal delays the initiation of tensile failure in the ceramic at

the ceramic-backing plate interface and thus allowing more projectile erosion. The

blunting of nose and projectile erosion are the dominant factors in the reduction of

projectile penetration. The fracturing and pulverization of ceramics are also effective

ways to dissipate a part of the kinetic energy generated by the impacting projectile.

The response of a brittle ceramic tile (Al2O3) to bullet impact is shown in Figure 4-1.

The plastic flow of the hard ceramic fragments around the projectile erodes the tip or

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even the entire length of the projectile, which further dissipating energy and

increasing the impact area [3]. Alumina tiles measuring 170 x 170 mm2, shown in

Figure 4-2, having hardness greater than 75 HRC were used in present study. The

tiles were fabricated by iso-statically pressing the alumina powder and sintering at

1600oC.

4.1.2 Shock Wave Spreading

Orthotropic materials offer anisotropy in materials along different directions.

Therefore, sound speed along the length of fibers is found to be several times higher

than its value in other directions. This property was used to spread the impacting

shock laterally, thereby reducing the shock strength along the impact direction [4].

After the early-stage disruption by the momentum disruption mechanism of the

ceramic tile, the shock wave transmitted into the protective material was further

attenuated by dispersion in the lateral direction. This layer of fabric can also capture

the secondary fragmentation of the brittle ceramic. In present work, laminated GFRP

and the high-strength aramid fabric Kevlar were used for this purpose.

Figure 4-1: (a) 7.62 mm bullet impact. (b) Pulverization of alumina disk. (c) Fragmentation

and scattering of alumina

Figure 4-2 : Alumina tiles used in present work

17

0 m

m

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4.1.3 Shock Energy Absorption

After disrupting the fragment momentum and dispering the major portion of the

transmitted shock in the lateral direction, a third layer of a porous material is

introduced in some of the configurations. The remaining shock wave energy can be

absorbed by porous materials like polystyrene (PS) and polyurethane PU) foams. The

porous materials (PE, PU, Al foams etc.) convert shock energy into heat or work

done, thus attenuating the shock energy. These materials absorb the energy through

the pore collapse mechanism [5]. A stress-strain curve of a porous material, as shown

in Figure 4-3, illustrates the energy absorption mechanism [6]. PU/PS foams were

used in present work.

Figure 4-3 : Stress-strain relation of porous material [6]

4.2 Protection against Fragments Impact

Fragmentation is the most lethal effect of EM detonation because fragments can

travel to large distances and cause serious injuries to humans. It is also one of the

dominant threats to vulnerable components, light structures and even hard targets.

IEDs and cased charges are often used to generate this damaging effect. It is

imperative to describe the threat level for which a protective configuration is

developed and tested.

A combination of lightweight materials can be employed for protection against both

blast and fragment impact. Present work deals with the design, development and

testing of various lightweight protective configurations against blast and

fragmentation. To evaluate fragmentation loading and protection against

fragmentation, scaled down artillery shell was used in present work. Details of the

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blast parameters and fragmentation characterization of this shell has been presented

in Chapter 3. The protective configurations were tested against reflected overpressure

of 235 psi (1620 kPa) and fragments weighing up to 4.3 g impacting with velocities

ranging from 961 to 1555 m/s. A steel plate measuring 250 x 250 x 6 mm3 was

placed at a distance of 0.60 m from the shell. The fragments’ impact, penetration and

perforation through the steel plate are evident from Figure 4-4. The protective

configurations were exposed to such extreme loading conditions.

4.2.1 Protective Configurations

Numerous lightweight materials have been used in a protective configuration. Kevlar

fabric has shown excellent ballistics impact resistance [7]. Kevlar woven fabric, 110

GSM (grams per square meter), was used with epoxy resin to maximize its

mechanical properties. Combinations of Kevlar fabrics, laminated GFRP, PU foam

and alumina tile were selected on the basis of their inherent properties of shock

dispersion, absorption and momentum disruption. In the present work the material’s

combination, order and dimensions were optimized using AUTODYN simulations

and their performance was then validated with experimental work. Two novel

compositions containing PU-alumina and PU-silica were also investigated. The seven

configurations were designated as C-1, C-2, C-3, C-4, C-5, C-6 and C-7. The

dimensions and constituent materials for each configuration are summarized in Table

4-1. Configuration and its protective capability against the blast and fragments

impact are briefly described in the following section of experimental work.

a b

Figure 4-4: Fragments penetration and perforation (a) Front side

(b) back sides of the 6 mm thick steel plate

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Table 4-1: Constituent materials and dimensions of protective configurations

Sr. # Alumina tile GFRP PU Foam Kev-epoxy Size (mm) Mass (g)

C-1 --- 5mm thick, 6mm thick, 12 layers 470 GSM

285x210x24 1123

C-2 --- 5mm thick, 6mm thick, 12 layers 110 GSM

240x150x17 435

C-3 --- 5mm thick, 6mm thick, 12 layers 110 GSM

220x220x18 626

C-4 9mm thick, Al back-1mm

5mm thick,

---

6 layers 470 GSM

165x165x21 1500

C-5 10mm thick, Al back-1mm

5mm thick,

5mm thick,

Size- 7˝ x 7˝ 12 layers 110 GSM

165x165x26 --

C-6 Multi-layers- 85% PU (4-layers) with 15% sand (3-layers) -212, 22 762

C-7 Mixture of 85% PU and 15% sand - Mixture of 85% PU and 15% Alumina powder

-212, 27 698

MS Plate 225x225x6 2396

4.2.2 Experimental Work

Two experiments were conducted with the scaled down shell (155 mm) to study the

blast and fragmentation effects on the protective configurations listed in Table 4-1.

The experimental setup for testing these configurations against the fragmentation of

this shell is shown in Figure 4-5.

C-1

Shell Flat probesss

Figure 4-5: Experimental setup for testing protective configurations against

fragments impact

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C-1 comprised Kevlar woven fabric (470 GSM) wrapped on laminated GFRP and

PU foam sheets. The configuration weighed 1123 grams with areal density of 1.87

g/cm2. The assembled view of the specimen is shown in Figure 4-6.

A closer view of the testing setup for C-1 and C-3 is also shown in Figure 4-7. Both

configurations were placed at 0.65 m away from the shell. Out of 15 fragments that

impacted C-1, only 5 perforated the configuration. The majority of the high velocity

fragments were captured within the configuration.

The configuration was tested again with a second shell detonation under the same

conditions. The impact spots of the first test were marked with circles to distinguish

them from the fresh impacts. The test setup and post-test impact on the configuration

is shown in Figure 4-8. Eleven fragments impacted the configuration and only three

could perforate C-1.

a b

Figure 4-6: (a) Front side (b) back side of C-1

b c C-1 C-3

a

Figure 4-7: (a) Setup for testing C-1 and C-3. (b) Front (c) back sides of C-1

after fragment’s impact

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C-2 comprised Kevlar woven fabric (110 GSM) wrapped on 5 mm thick laminated

GFRP and PU foam sheets. The configuration weighed 435 grams with an areal

density of 1.2 g/cm2. The assembled view of C-2 is shown in Figure 4-9.

C-2 and its testing setup are shown in Figure 4-10. Flat Brass probes are also visible

in Figure 4-10(a) for fragment velocity measurement. The Figure 4-11depicts the

post-test view of both sides of the configuration. A view of the laminated GFRP and

PU foam is also shown in this figure. Nine fragments impacted the configuration and

six were able to perforate the configuration. Being the lightest configurations, it

could not offer sufficient strength to capture most of the impacted fragments. As

expected the Kevlar-470 GSM has offered more resistance to fragments penetration

than equal number of layers of Kevlar-110 GSM.

a b c d

Figure 4-8: (a, b) Test-2 setup and C-2 view after (c) impacted and (d)

perforated fragments

a b

Figure 4-9: Assembled view of C-2, (a) front and (b) back sides

a b c

Figure 4-10: (a, b) C-2 testing setup (c) C-2 along with 6 mm thick MS plate

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C-3 comprised a combination of Kevlar fabric (110 GSM) wrapped on 5 mm thick

laminated GFRP and PU foam. It weighed 626 g with an areal density of 1.29 g/cm2.

A view of C-3 before test is shown in Figure 4-12.

The assembled view of C-3 after testing is shown in Figure 4-13. The relatively

wider configuration placed at the nearest location of 0.50 m from the shell received

16 fragments out of which 8 perforated C-3. The second test of C-3 was conducted

by placing it at a distance of 0.80 m from the shell. The net fragments that perforated

C-3 in first and second test were 14. Figure 4-14 schematizes the tests results of C-3.

The configuration was able to capture almost 60% of the impacted fragments.

b a c d

Figure 4-11: C-2 (a) front (b) back sides (c) laminated GFRP (d) PU foam

after fragments impact

a b

Figure 4-12: (a) Front and (b) back sides of C-3

Figure 4-13: C-3 front and back sides after fragments impact- first test

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C-4 comprised a combination of Kevlar fabric (470 GSM) wrapped on an alumina

tile and laminated GFRP sheet. The configuration weighed 1500 grams. The

assembled view and testing setup are shown in Figure 4-15. The Kevlar-470 GSM

was wrapped on alumina tile and laminated GFRP sheets. The configuration was

placed at 0.80 m from the shell. Being relatively farther and having relatively smaller

frontal area, only 4 fragments impacted and none of these could perforate the

configuration as evident from the back-side view of C-4 shown in Figure 4-16.

C-5 comprised a combination of alumina tile (10 mm) backed by laminated GFRP (5

mm) and PU foam (6 mm), all wrapped in 12 layers of Kevlar-epoxy. The front and

back side views of C-5 are shown in Figure 4-17. This configuration was also tested

a b c d

Figure 4-14: C-3 Second test (a) Front (b) back sides, (c, d) laminated GFRP

a b c

Figure 4-15: (a, b) Assembled view of C-4 and (c) testing setup for C-4 and C-5

a b c d

Figure 4-16: (a, b) C-4 front and (c, d) back sides after the test

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against 7.62 mm bullet impact. The bullet impact is evident on front side of

configuration without a significant backface signature [8].

C-5 was located 0.725 m from the shell. Seven (7) fragments impacted the

configuration, as shown in Figure 4-18(a), and none of these could perforate this

configuration as seen from the back side view of the configuration shown in Figure

4-18(b). The Kev-epoxy covering was observed to contain the secondary

fragmentation of brittle alumina and retained the integrity of the configuration

against severe impacts of fragments.

C-6 comprised a multi-layered combination of 85% Polyurethane and 15% silica.

Three layers of silica were sandwiched in four layers of polyurethane. The 22 mm

thick sample weighed 762 grams and is shown in Figure 4-19(a, b).

C-7 comprised a combination of two composites. The first one was prepared by

mixing 15% (by weight) alumina powder in 85% Polyurethane. The 10 mm thick

sample disc weighed 321 grams. The second sample was prepared by mixing 15%

(by weight) silica with 85% polyurethane. The 17 mm thick sample weighed 367

grams. Both these samples are shown in Figure 4-19(c, d) and joined together with an

adhesive and cotton tap to test against fragments impact.

a b

Figure 4-17: C-5 (a) Front side (b) back side

b a

Figure 4-18: (a) Front and (b) back sides of C-5 after fragment's impact

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The testing setup for C-6, C-7 and other samples is shown in Figure 4-20. C-1, C-4

and MS witness plate are also visible in this figure. C-6 was located at a stand-off

distance of 0.60 m. The post-test scenario is shown in Figure 4-21. Eleven (11) out of

eighteen (18) impacted fragments perforated C-7 as shown in Figure 4-21(c, d). The

composition did not offer significant resistance to impacting fragments. However,

these two configurations have shown good blast and thermal effects resistance

against the nearby detonation of the scaled shell. Scabbing from rear side is also

witnessed from this Figure 4-21(b, d). Flat timing probes were placed behind C-7 to

measure the exit velocity of the fragments. Fragments with velocity ranging between

1349–1555 m/s were supposed to impact the configuration due to its position. The

fragment’s exit velocity measured with flat Brass probes was 1038 m/s.

a b c d

Figure 4-19: (a, b) A view of C-6 and (c, d) C-7 configurations

Figure 4-20: Testing setup for C-6 and C-7

Figure 4-21: (a, b) front and back sides of C-6 after test, (c, d) front

and back sides of C-7 after test

a b c d

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4.3 Protection against Bullet Impact

The protective configuration (C-5) consisting of alumina (Al2O3) tile, followed by

laminated GFRP and PU foam, and covered with 9 layers of Kev-epoxy was tested

against 7.62 × 39 mm (MSC) mild steel-core bullet impact. This bullet is fired from

popular AK-47 Kalashnikov assault rifle [9]. The details of the configurations are

also presented in Table 4-2. The bullet shape and its material properties play a vital

role in penetration. The bullet, weighing 7.77 grams, was cut into two sections and its

constituent materials (mild steel core, copper-coated steel jacket and lead filler), as

shown in

Figure 4-22, were inspected, weighed and measured. The measured values are

summarized in Table 4-3[8].

Table 4-2: Protective configuration for bullet impact tests [8]

Sr. # Alumina GFRP PU Foam Cladding Thickness

1 10 mm thick,

Size- 7˝ x 7˝

6mm thick,

Size- 7˝ x 7˝

6mm thick,

Size- 7˝ x 7˝

Kev-

epoxy 26 mm

2 Blunt Force Trauma test - depth of depression = 10 mm

Figure 4-22 : Different parts of 7.62x39 mm bullet, (left) steel core, lead filler, and copper

coated steel jacket. (Right) cut sections of bullet [8]

Table 4-3: Measured values of 7.62x39 mm MSC bullet

Material Mass (g) Hardness (HRC)

Mild steel-core (MSC) 3.87 17

Copper-coated steel jacket 1.82 16

Lead filler 2.08 --

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The impact velocity measured using high-speed photography was 715 m/s. The bullet

was stopped and captured by the configuration. The target configuration retained its

integrity without any escape of secondary fragmentation from brittle alumina. The

Kevlar-epoxy resin provided enough strength and support to the target constituent

materials. Figure 4-23 illustrates the bullet impacting the target configuration C-5.

The ceramic tile stopped the bullet penetration through erosion and blunting of the

nose. No evidence of bullet penetration behind the ceramic tile was observed. The

recovered mushroom-shape bullet is shown in Figure 4-24.

4.3.1 Blunt Force Trauma Test

Soft body armor comprising higher molecular weight polyethylene (HMWPE) or

high strength fabrics like Kevlar are prone to back face signature (blunt force

trauma). Despite the soft body armor vest’s protection, the possibility exists of blunt

injury resulting from the impact [10]. Body armor is supposed to stop the projectile

and provide protection from internal injury resulting from the impact energy. Blunt

force trauma or backface signature is the result of the energy transferred from the

impacting projectile to the human body (shielded by a bullet resistant vest) without

penetrating the skin. The severity of such an injury may result in ruptured organs,

Figure 4-24: 7.62 x 39 mm MSC original and plastically deformed recovered bullet

Figure 4-23: High speed images of bullet impacting the target configuration

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internal bleeding and ultimate death. This effect can be minimized by spreading the

impact of the projectile over a wide area of the torso.

The backface signatures (blunt force trauma) test of this configuration was performed

using Plastilina clay [11] as backing material in a wooden frame. Any external cover

or fabric was not used during this test. The configuration was placed inside this

frame, as shown in Figure 4-25, and tested against 7.62 x 39 mm MSC bullet impact

at a distance of four meters. High-speed photographic images of this test are shown

in Figure 4-26.

The bullet penetrated the configuration and was captured inside as seen from Figure

4-27(b). Any bulging effect was not observed on the backside of the Kevlar-epoxy

covered configuration, as shown in Figure 4-27(c). The impact of the bullet was

a b c d

Figure 4-27: (a) Testing setup (b) 7.62mm bullet impact (c), Rear side

of C-5 (d) and impact on Plastilina clay

Figure 4-25: The testing configuration, including Plastilina clay as backing medium

Figure 4-26: High speed photographic images of blunt force trauma test at

three different times

b c a

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observed on the clay, as shown in Figure 4-27(d). The impact was spread out,

indicating the dispersion of the shock wave over a wide area, thus decreasing the

intensity as desired. The maximum depth of depression measured was 10 mm. This

was well within the European, German and British standards for backface signatures

which allow 20 to 25 mm ‘Backface Signature’ [8, 11].

It was observed that the front ceramic tile was able to completely defeat the

penetration of the bullet owing to its high hardness and eroding effects. The shock

energy transferred from the ceramic tile was well distributed by the laminated GFRP

in lateral directions. Finally, the porous layer of PU foam was able to absorb the rest

of the shock energy, as evident from the blunt force trauma test. The initial

momentum disruption with transmitted shock dispersion and absorption methodology

was found effective to counter a bullet/fragment impact threat. The fiber reinforced

cladding of Kevlar-epoxy was able to prevent the disintegration of the brittle alumina

tile, maintaining the integrity of the configuration.

4.4 Numerical Simulation

ANSYS AUTODYN [12] was used to simulate the fragmentation phenomenon of

scaled down artillery shell (155 mm). In a Lagrangian solver the grid moves with the

material and undergoes distortion causing inaccuracies in solution. This solver is

ideal for simulating materials undergoing low distortion. An erosion model is used

with this solver to avoid mesh tangling. Smoothed Particle Hydrodynamics (SPH)

solver was used to simulate explosively driven fragmentation of shell and the

response of protective configurations to impacting fragments. SPH being a meshfree

method can handle nonlinear problems with large deformation without mesh

degeneration or tangling unlike the Lagrange solver. The non-physical, numerical

erosion model is not required for SPH [13]. A coupled Euler-ALE approach was used

to simulate the blast effects. A coupled SPH-ALE approach was also used to simulate

the fragments impact on protective configurations.

4.4.1 Material Modeling

JWL (Jones-Wilkins-Lee) equation of state [14] was used for expansion of Comp-B

product gases. Shell body was modelled with (AISI-1006) steel. Ideal gas EOS was

used for air. Material models for these materials were used from ANSYS

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AUTODYN material library which has already been discussed under the section on

material modeling in Chapter 3. Material properties for Alumina, GRFP laminate and

Kev-epoxy used for simulating protective configurations are presented in Table 4-4.

Alumina and Kev-epoxy were retrieved from AUTODYN library. Material

properties for GFRP, PU foam and Kevlar were used from [15], [2] and [16]

respectively.

Table 4-4: Material properties used in simulation

Al2O3-99.5 GFRP laminate [15] Kev-Epoxy

Density – 3.89 g/cm3 Density – 1.80 g/cm

3 Density – 1.29 g/cm

3

EOS - Polynomial EOS - Orthotropic EOS - Puff

A1 = 231 GPa E 11 (kPa) = 6.0e+6 Stiffness Matrix (kpa)

A2 = -160.0 GPa E 22 (kPa) = 1.97e+7 C11=3.42e+6,C22= 1.35e+7,

C33= 1.35e+7, C12=1.14e+6

C23=1.20e+6, C31=1.14e+6

A3 = 2774 GPa

B0=B1=0

E 33 (kPa) = 1.97e+7

T1= 231 Gpa Poisson ratio 12 = 0.15 Shear Modulus(Gpa)

G12=G23=G31=1.0

T2 = 0 Poisson ratio 23 = 0.13 Volum. response-Polynomial

A1=4.15Gpa, A2=40Gpa

,T1=4.15Gpa

T (Ref) = 0 Poisson ratio 13 =0.15

Strength – JH2 Strength – Elastic Strength – Elastic

G(Gpa) = 152 G(kpa) = 1.79e+6 G(kpa) = 1.0e+6

HEL=6.57GPa, A = 0.88, N

= 0.64, C= 0.007, B = 0.28,

M = 0.6

Max frac. Ratio =1.0

Failure-JH2 Failure-Stress/strain Failure-Mat Stress/strain

D1= 0.01, D2=0.7, β = 1

Hyd. Tensile limit =-2.620e-

1 Gpa

Ten fail stress 22(kpa)

4.318e+5

Max. shear stress 23 (kpa)

8.0e+4

Ten fail strain 11 = 0.009

Ten fail strain 22 = 0.02

Ten fail strain 33 = 0.02

Ten fail strain 11 = 0.01

Ten fail strain 22 = 0.08

Ten fail strain 33 = 0.08

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4.4.2 Shell Fragmentation and Impact on Protective Configurations

SPH solver in ANSYS AUTODYN was used to model the scaled down shell for

fragmentation studies. Particle size of 1 was used for packing. The quarter symmetry

of the shell was modeled with 28,820 nodal points. The shell model, number of

fragments, fragments mass and velocity distribution have already been discussed in

the section on simulation in Chapter 3. The gauge points defined in the model and the

fragments velocity distribution will be discussed frequently in this section, therefore,

the FE model of the shell with gauge points and their velocity plot is shown in Figure

4-28. Present work is focused on the simulation of the behavior of various protective

configurations against fragment impact and the study of blast wave loading on these

configurations. The protective capability of the configurations is presented in this

section.

Figure 4-28: (a, b) FE model with gauge points defined and Fragment velocities of

gauge points defined on shell casing (c) with ALE solver (d) with SPH

c d

a b

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4.4.3 Coupled SPH-ALE Simulation

The fragmentation phenomenon was modeled and simulated in SPH solver. A

coupled SPH-ALE approach was used to simulate the impact of explosively driven

fragments on protective configurations. ALE solver combines the best features of

both Lagrange and Euler methods. Due to symmetry on two axes, quarter symmetry

of the shell was modeled in SPH and the simulation was run until the fragments

traveled a radial distance of 560 mm. Protective configurations C-1 and C-5 were

then modeled using ALE solver. Kevlar 470 GSM layers were modeled with a

macro-homogeneous model that considers the whole layers as homogenous in

geometry with orthotropic mechanical properties [16].

A grid size of 50 x 25 x 3 was used for Kevlar 470 GSM layer measuring 200 x 100

x 4 mm3. A ratio of 4:1 between SPH particle and ALE cell size best defines the

interaction between the two solvers [17].

Figure 4-29 depicts the FE models of C-1(a, b)) and C-5 (c, d) using ALE solver.

Both grid and material plots of the configurations are shown in this figure.

Figure 4-29: FE models of (a, b) C-1 and (c, d) C-5

a b

c d

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The fragments approaching both configurations located perpendicular to Y and Z-

axes are shown in Figure 4-30. Gauge points defined on steel casing approaching the

protective configurations are also visible in this figure. The fragments traveling in

radial direction and their interaction with C-1 and C-5 are also shown in Figure 4-31.

Both C-1 and C-5 were placed at a position where fragments from the cylindrical part

of the shell body were most likely to impact, as can be seen from Figure 4-30. The

alumina tile in C-5 offers high resistance to high velocity fragments. The laminated

GFRP backing provides strength to alumina by absorbing the shock energy and

further causing a delay in fracturing of the brittle alumina tile. The combination of

Kevlar-470 GSM and GFRP in C-1 resists the fragments penetration. The Kevlar

fabric undergoes deformation and absorbs the impacting energy. The fabric

deformation at the rear end of the configuration can be seen in Figure 4-31(a, b). The

results are consistent with the experimental testing of C-1 and C-3 discussed in

experimental section. C-5 captures all the impacting fragments; however, a bulge on

the rear side of the configuration is seen in the simulated results of Figure 4-31.

Figure 4-30: Isometric view of shell fragmentation with C-1 and C-5,

fragments impacting C-1 & C-5

C-1

C-5C-1

C-5

a b

c

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The velocity profile of fragments defined on the cylindrical portion of the shell is

shown in Figure 4-32. The fragments impacting C-5 are captured within the

configuration. An abrupt drop in velocity profile can be seen as the gauge points hit

the protective configurations. Velocity plot of these gauge points is shown in Figure

4-32(a) for configuration C-5. The velocity profile of gauge points impacted on C-1

is shown in Figure 4-32(b). The velocity of gauge points 11 and 12 is approaching

200 m/s while gauge point 10 still has a velocity 400 m/s showing a potential to

perforate the remaining part of the configuration.

Figure 4-31: (a) Fragments penetration through C-1 (b) deformation of Kevlar woven

fabric and (c) Fragments impact on C-5 and bulge on back side of C-5

a b

c

Figure 4-32: (a) Velocity profile of gauge points before and after impacting

C-5 (b) before and after impacting C-1

a b

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The fragment impact on a 6 mm thick MS (mild steel) plate was also simulated. The

simulation setup is shown in Figure 4-33. Most of the fragments were stopped by the

MS plate as also observed in experimental work shown in Figure 4-4. Fragments

penetration and perforation through MS plate is shown in Figure 4-34.

The simulation setup for C-4 and C-2 is shown in Figure 4-35. SPH model of the

shell with gauge points defined on shell casing are visible in this figure. The

fragment expansion in the radial direction along with the moving gauge point is also

shown in Figure 4-35.

Figure 4-34: Penetration and perforation through (a) MS plate.

(b) Close view of MS plate

a b

Figure 4-33: (a) Fragments impacting on MS plate (b) isometric view

a b

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The protective model for C-4 in ALE is shown in Figure 4-36. An enlarged view of

the configuration and the approaching fragments can be seen from this figure. As

most of the high velocity fragments hit the central region of the configuration, a

graded zoning was employed in the central part of the layered protective

construction. The graded zoning is visible in the grid plots of Figure 4-36 for C-4.

Figure 4-35: (a) Shell model in SPH (b) radial expansion of fragments

and (c) moving gauges are visible

a

b c

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Figure 4-36: (a) ALE model of C-4 (b, c) Fragments approaching the configurations

a b

c

Figure 4-37: Fragments impact on C-4, (a) front side view, (b, c) back side view

a b

c

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The impact of fragments on C-4 is shown in Figure 4-37. Soon after impacting the

configuration, the fragments lost most of their kinetic energy on meeting the hard

alumina tile. The backing laminated GFRP and Kevlar fabric also offered penetration

resistance alongside providing structural support to the brittle alumina against its

inherent shattering. The abrupt drop in velocity to below 200 m/s is an indication of

the protective capability of the configuration. Contrary to the experimental results, a

slight bulge on rear side of C-4 is visible in Figure 4-37. The velocity profile of the

gauge points just before and after impacting C-4 is shown in Figure 4-38.

The ALE model of C-2 is shown in Figure 4-39 to simulate the behavior against

fragment impact. The grid and material plots are shown in Figure 4-39(a) and Figure

4-39(b) respectively.

An isometric view of fragment impact on C-2 and C-4 is shown in Figure 4-40. The

fragments penetrating configuration C-2 and the gauge points are also shown in this

figure. An enlarged view of C-2 shows that fragments have almost penetrated the

configuration.

Figure 4-38: Velocity plot of gauge points (a) before and (b) after impacting C-4

a b

Figure 4-39: ALE model of C-2. (a) Grid plot and (b) material plot

a b

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A 3D view of the fragmentation and protective configurations C-2 and C-4 is shown

in Figure 4-41. The Kevlar fabric (110 GSM) and GFRP laminate exert a resisting

force to fragments, reducing their velocity. At the same time, the fabric is deformed

Figure 4-40: (a) Isometric view of C-2 and C-4, (b) Fragments perforation

through C-2. (c) Gauge points defined on C-2

a b

c

Figure 4-41: (a) Fragments penetration through C-2 (b, c) combined view of

C-2 and C-4

a

b c

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and accelerated, thereby dissipating the energy. Several fragments were captured

within the configuration. A few of them were able to perforate. The velocity profile

of the gauge points before impact and after penetrating C-2 is shown in Figure 4-42.

A sudden drop in velocity of the gauge points is observed. However, two of the

gauge points still show a residual velocity of 500 m/s, indicating their capability of

perforation through C-2 as shown in Figure 4-42(b).

Both C-1 and C-2 were having equal number of layers of two different Kevlar

fabrics. From the simulated and experimental results, it was evident that Kevlar

fabric-110 GSM has presented a relatively lesser resistive force to the impacting

fragments as compared to the Kevlar-450 GSM fabric used in configuration C-1.

4.4.4 Blast Loading on Protective Configurations

Simulation for blast parameters was performed using coupled ALE-Euler multi-

material approach in ANSYS AUTODYN. The hollow steel shell was modeled in

ALE, whereas Comp-B filling and surrounding air were modeled in the Euler solver.

An optimized grid size of 1x1 mm was used for both solvers [18]. Configuration C-2

was selected for simulating the blast loading as this was the lightest among C-1 to C-

5 configurations. The numerical model and shell detonation are shown in Figure

4-43. Upon detonation, the shell casing starts expanding under pressurized detonation

product gases as shown in Figure 4-43. The escape of detonation products in air and

subsequent formation of a blast wave and its propagation is already shown in Figure

3-11 of Chapter 3. The formation of blast wave and its outward propagation is shown

in Figure 4-44.

Figure 4-42: Velocity profiles of gauge points (a) before and (b) after impacting C-2

a

C2

b

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The blast wave arrival, impact and loading on C-2 are depicted in Figure 4-45. The

figure also illustrates the configuration before and after the blast impact and confirms

the integrity of this most vulnerable configuration in present study.

Figure 4-43: (a) AUTODYN model of shell (b) detonation wave

propagation inside shell (c) Expansion of shell at 20 s

a b c

Figure 4-44: (a) Expansion of shell at 40 s (b) at 61 s and (c) at t= 90 s

a b

c

Figure 4-45: (a) Blast wave approaching C-2 (b) impacted on C-2 and (c) C-2 before

and (d) after blast impact

a b

c d

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The blast wave undergoes reflection when the forward moving air molecules are

brought to rest and further compressed upon meeting the front surface of C-2,

forming a reflected wave with pressure designated by Pr. The reflected blast wave on

the face of C-2 delivers a compressive shock wave from Kev-epoxy layers to PU

foam and laminated GFRP. The shock wave energy is absorbed and dispersed by PU

foam and GFRP layers respectively.

The gauge point 2 was defined 10 mm ahead of C-2 and gauge point 3 was defined

on the back side of C-2 for peak pressure measurement, as shown in Figure 4-45(a).

Peak incident (Ps) and reflected (Pr) pressures of 57 psi (393 kPa)and 261 psi (1799

kPa) respectively were observed at the front of configuration. The pressure-time

history P(t) at gauge point 2 was integrated for the positive phase duration to obtain

reflected impulse. The pressure and impulse plot are shown in Figure 4-46(a) and

Figure 4-46(b) respectively. IS and IR represents incident and reflected impulse

respectively.

The 10 mm gap differentiates the incident and reflected pressure rise time as well as

the impulse shown in Figure 4-46. A peak pressure value of 2.3 psi (15.85 kPa) for

gauge point 3 was obtained in simulation, as shown in Figure 4-47(a). The gauge

Figure 4-46: For gauge point 2 (a) Incident and

reflected overpressure (b) Impulse plots

a

b

IS

IR

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point 7 was defined to face the blast impact on PU foam whereas the gauge point 8

was located 4.0 mm behind point 7. The shock wave transmitted into the PU foam

and its absorption and shock mitigation in terms of specific internal energy is shown

in Figure 4-47(b). The figure demonstrates that the pore collapse mechanism in PU

foam absorbs substantial energy.

4.5 Experimental Results

Two tests were conducted with a scaled down model of 155 mm artillery shell to study

the fragmentation and blast phenomenon and their loading effects on seven protective

configurations. The fragmentation phenomenon involves the detonation of the explosive

filling in the shell producing a very high pressure which is imparted to the metal casing

within a time scale of microseconds. The detonation wave exerts high pressure on

successive cross-sections of the shell body until it fractures and disintegrates into high

velocity fragments.

Figure 4-47: (a) Pressure at gauge point 3, (b) Change in

Specific internal energy in PU foam for gauge points 7 and 8

b

a

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The protective configuration C-1 located at 0.65 m from the shell was impacted by

15 fragments and only 5 were able to perforate. In the second test, 3 fragments could

perforate out of 11 those impacted the configuration. The Kevlar fabric exerted a

resisting force to impacting fragments and reduced their velocity. The high strength

Kevlar fabric (470 GSM) and laminated GFRP combination was able to contain the

majority (70%) of the high velocity fragments. The perforation of few of the

fragments and a closer view of the fragments captured in Kevlar and laminated

GFRP are shown in Figure 4-48.

Unlike C-1, both C-2 and C-3 employed Kevlar fabric-110 GSM with the same

number of layers as that of C-1. Configuration C-2 captured only 3 of the 9

fragments impacted on it, whereas C-3 captured 8 out of a total 16. The fragment

impact and perforation through C-2 and C-3 is shown in Figure 4-49 and Figure 4-50

respectively. While resisting the fragment impact, the Kevlar fabric was elongated.

The post impact view on laminated GFRP and PU form (of C-2) is also shown in

Figure 4-50(b, c).

Figure 4-48: Fragments perforation and captured in (a, b) Kevlar and (c, d) GFRP

a b c d

Figure 4-49: (a) C-2, (b) laminated GFRP and (c) PU foam after

fragments impact

a b c

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The total number of fragments that perforated C-3 in both tests was 14. The

configuration was able to capture almost 60% of the impacted fragments. The Kevlar

fabric-470 GSM and laminated GFRP have offered significant resistance to high

velocity fragments owing to their higher modulus values compared to Kevlar fabric-

110 GSM. From the simulated and experimental results, it was evident that Kevlar

fabric-110 GSM offered less resistive force to impacting fragments compared to 450

GSM fabric used in configurations C-1 and C-4.

C-4 was relatively distant, located 0.80 m away, it was impacted by only 4 fragments

and none of these could perforate the configuration. This was also evident from the

back-side view of C-4 shown in Figure 4-51(a). The front and back sides of

laminated GFRP, shown in Figure 4-51(b & c) did not show any evidence of

fragment impact. Moreover, no bulging effect was noticed on backside of the Kevlar

covered configuration, as evident from Figure 4-51(a). However, the simulation

results show a slight bulge on back side of the configuration.

Configuration C-5, located 0.725 m from shell, was impacted by 7 fragments but no

perforation or backface signature was observed, as shown in Figure 4-52(b).

Figure 4-50: (a) Front and (b) back sides of C-3 (c) laminated GFRP after second test.

a b c

Figure 4-51: (a) Back side of C-4 (b, c) front and back sides of laminated GFRP

placed behind the ceramic tile

a b c

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The alumina tiles in C-4 and C-5, with hardness greater than 75 HRC, offered very

high resistance to impacting fragments. The backing laminated GFRP sheet further

dispersed the shock energy transmitted through the ceramic tile in lateral directions.

After the test, a few outer layers of Kev-epoxy, as shown in Figure 4-52(a, b) were

removed. A fragment weighing 3.69 g and measuring 48 x 5 mm2 was recovered. A

previously captured bullet was also recovered. The configuration was previously

tested against 7.62 mm bullet at an impact velocity of 715 m/s. The configuration

stopped the bullet without a significant backface signature [8]. The recovered bullet

and fragment are also shown in the Figure 4-52(c). The figure did not show any

evidence of fragment perforation through this configuration. The front alumina tile

completely disrupted the impacting fragment as well as the impacted bullet because

of its high hardness. The shock transmitted from alumina was dispersed in lateral

directions by the backing GFRP, and finally absorbed by the pore collapse

mechanism in the PU foam. The Kev-epoxy covering also served to contain the

secondary fragmentation of brittle alumina and retained the integrity of the

configuration against multiple fragment’s impact.

The configurations C-4 and C-5 employing a ceramic (alumina tile) were able to

completely capture the high velocity fragments, thus providing 100% protection

against fragments weighing up to 4.5 g and moving with velocities up to 1555 m/s.

The backface signatures (also known as blunt force trauma) test of C-5 was

performed and maximum depth of depression of 10 mm was measured [8] , which

was well within the US, European, German and British standards for backface

signatures [11, 19]. The test and the results are evident from the Figure 4-27.

Figure 4-52: (a) Front (b) back sides of C-5 after fragment's

impact, (c) recovered fragment & bullet

a b c

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C-6 comprised a multi-layered composition of PU-silica of density 1.1 g/cm3. C-6

was located at a stand-off distance of 0.60 m. A total of 14 fragments impacted this

configuration, of those 9 were able to perforate. Another low-density configuration

comprising mixtures of PU, silica and alumina powder was tested at a distance of

0.57 m. Eleven (11) fragments perforated from a counted eighteen (18) impacted on

C-7. A fragment velocity of 1038 m/s at the free surface was calculated by means of

flat timing probes placed behind this configuration. Both C-6 and C-7, being lightest

and most thermally resistant of all configurations, did not offer significant resistance

to the impacting fragments. The post- test view of C-6 and C-7 is shown in Figure

4-53.

A summary of the experimental and simulated results is presented in Table 4-5.

Although all of the configurations withstood the blast wave loading when fixed

rigidly, only C-4 and C-5 provided full protection against both threats of blast wave

and high velocity fragment loading.

a b

c d

Figure 4-53: (a, b) Front and back sides of C-6 (c, d) C-7, after

fragments impact

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Table 4-5: Summary of the experimental and simulated results

Confi

gura

tions

Thickness

(mm)

Results Protection

Blast/Fragments

Experimental Simulation

Fragments

Impacted

Fragments

Perforated

C-1 24 26 8 perforation Full/Partial

C-2 17 9 6 perforation Full/Partial

C-3 18 18 8 perforation Full/Partial

C-4 21 8 0 Slight bulge Full /Full

C-5 26 7 0 Slight bulge Full/Full

C-6 22 14 9 perforation Full/Partial

C-7 27 18 11 perforation Full/Partial

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References

[1] P. Qiao, M. Yang, F. Bobaru, Journal of Aerospace Engineering. 21(2008)

235.

[2] C.W. Poh, Investigation of new materials and methods of construction of

personnel armor, M.Sc(2008).

[3] W.W. Chen, ", Journal of the American Ceramic Society. 4(2007).

[4] J.S. I. M. Ward, An Introduction to the Mechanical Properties of Solid

Polymers, 2nd Edition. (2004), 394.

[5] B.C. Wai, Investigation of Shock Wave Attenuation in Porous Media,

M.Sc(2009).

[6] L.J. Gibson, M.F. Ashby, Cellular solids: structure and properties. (1999.

[7] Y. Ma, Ballistic strength of multi-layer fabrics against fragment simulating

projectiles(2017).

[8] K. Ahmed, A.Q. Malik, I.R. Ahmad, International Journal of Protective

Structures. 10(2019) 289.

[9] L. Carbajal, J. Jovicic, H. Kuhlmann, Assault riffle bullet-experimental

characterization and computer (FE) modeling, in Experimental and Applied

Mechanics, Volume 6. 2011, Springer.651.

[10] A.C. Merkle, E.E. Ward, J.V. O'Connor, J.C. Roberts, Journal of Trauma and

Acute Care Surgery. 64(2008) 1555.

[11] R. Kaiser. Understanding Blunt Force Trauma/ Backface Signature. Available

from: https://www.ppss-group.com/blog/understanding-blunt-force-trauma-

backface-signature/.

[12] U. ANSYS Inc., Century Dynamics. Release 14.0 documentation for ANSYS

AUTODYN.(2011).

[13] M.A. Abdalla. Fragmentation Analysis of OG-7 Warhead Using AUTODYN

SPH Solver. in Advanced Materials Research. 2012. Trans Tech Publ.

[14] E. Lee, H. Hornig, J. Kury, California: University of California, (1968).

[15] M.M. Ansari, A. Chakrabarti, M.A. Iqbal, Procedia engineering. 173(2017)

153.

[16] A.M. Soydan, B. Tunaboylu, A.G. Elsabagh, A.K. Sarı, R. Akdeniz,

Advances in Materials Science and Engineering. 2018(2018).

[17] R. Messahel, M. Souli, CMES: Computer Modeling in Engineering &

Sciences. 96(2013) 435.

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[18] K. Ahmed, A.Q. Malik, AIP Advances. 10(2020) 065130.

[19] N.L. Enforcement, C.T. Center, U.S.o. America, O.o.L.E. Standards, (2001).

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Containment for Blast, Fragmentation Chapter 5

and Thermal Effects

5.1 Introduction

The detonation of a cased energetic material or an IED is manifested by blast

overpressure, fragmentation and thermal effects. Human beings are sensitive to

overpressure and their air filled organs like, ears, lungs and the gastrointestinal track

are the most susceptible to damage [1]. Thermal effect is a potential injury

mechanism and is associated with the burning due to heat and fireball [2, 3]. A

rapidly propagating fire hazard is also probable if any hydrocarbon fuel is present in

the close vicinity. Fragmentation is the most lethal effect because fragments can

travel to large distances and cause serious injuries to humans. In recent years, nails,

screws, ball bearings and other metallic parts have been used in IEDs to enhance this

injury mechanism. Blast wave mitigation and on-spot quenching of the fireball are

imperative to avoid loss of invaluable lives and infrastructure. Efforts have been

made in the past by individuals and organizations to reduce such life threatening and

infrastructure damaging effects associated with EM detonation. The present work

deals with the experimental and numerical investigation of the on-spot quenching of

fireball, blast wave attenuation and containment of primary and secondary fragments

using lightweight composite materials discussed in previous chapters. The open area

energetic material detonation effects were compared with the detonation inside this

containment system.

5.2 Materials and Experimental Work

5.2.1 Scaled down Container

To limit the devastating effects of a cased EM or an IED detonation, a heterogeneous

cylindrical container of diameter 250 mm and height 525 mm, comprising 2 mm

thick steel liner (height-250 mm) wrapped in laminated GFRP and Kevlar fabric was

developed and studied. Shaving foam was used as filling material in this container as

shown in Figure 5-1. Kevlar woven fabric 470 GSM (grams per square meter) and

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laminated GFRP were wrapped on 2 mm thick steel liner to provide sufficient

strength against highly repulsive detonation product gases. A combination of

composites, including Bakelite, PU-silica and EPS foam was employed at the base of

the container. The PU-silica composite has density of 1.1 g/cm3 and compressive

strength of 232 MPa. The material has shown good thermal resistance and shock

absorbance at extreme conditions [4]. C4 charge weighing 104 grams was tested in

open area as a surface burst to measure the blast wave parameters.

C4 weighing 104 grams was placed in contact with the base of the container, as

shown in Figure 5-1(b). The container was then filled with shaving foam shown in

Figure 5-1(c). Pressure transducers (S1 – S4) were employed at radial distances of

280 - 620 mm and different heights to measure the pressure-time history of the blast

wave. Transducers were sealed in steel pipes for protection against fragment impact.

The blast wave data was obtained through the transducers with a data acquisition

(DAQ) system. High-speed photography was used for visual studies of the fast events

at 54000 fps. A sketch of testing setup for C4 surface burst and inside composite

container is shown in Figure 5-2.

a b

Figure 5-2: A sketch of testing setup for (a) surface burst (b) detonation

inside cylindrical container

Figure 5-1: (a) Empty container (b) C4 placed at the bottom (c) filled with shaving foam

a b c

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The experimental setups for surface burst and inside composite container are shown

in Figure 5-3 and Figure 5-4 respectively. For bare C4 test, the charge was placed on

25 mm thick expanded polystryne (EPS) foam which was placed on 60 mm thick

steel disc. The EPS foam was employed to avoid a fragment or debris flight and their

impact on sensors and recording instruments. The EPS foam has absorbed a part of

explosive energy before reflection of blast wave from the steel disc. A part of the

energry may also be wasted in crater formation if placed directly on ground.

5.3 Numerical Simulation

5.3.1 C4 Surface Burst Parameters

Simulation for blast parameters was performed using coupled ALE-Euler approach in

ANSYS AUTODYN [5]. C4 explosive filling and surrounding air were modelled in

Figure 5-4 (a) Experimental setup for C4 detonation inside container (b) C4 and

foam filled in container

b

S1

S2

S3

S4

a

Figure 5-3: Experimental setup for bare C4 charge test (a) close view

(b) complete setup

C4

a

S1 S2

S3

S4

C4

b

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Euler solver whereas the steel reflecting surfaces with the transducers were modeled

in ALE. JWL (Jones-Wilkins-Lee) equation of state [6] was used for expansion of C4

product gases and ideal gas EOS was used for modeling air. An optimized grid size

of 1x1 mm2 was used for both solvers [2, 4, 7]. The numerical model, product gases

expansion and blast wave propagation are shown in Figure 5-5 and Figure 5-6. C4

charge was placed on 25 mm thick EPS foam and a 60 mm thick steel disc as shown

in Figure 5-3(a). A Steel reflecting medium measuring 10 x 5 mm2 was modeled in

ALE close to gauge points 2, 3 and 4. These points give reflected overpressure (Pr)

whereas the gauge point 1 represents incident overpressure (Ps).

The simulation results for the surface burst are presented in Table 5-1. Here, X

represents the radial distance from the center of cylindrical charge and Y is the height

from ground level. The blast wave arrival time is indicated by Ta.

c d

Figure 5-6: (c) Blast wave formation and (d) propagation in air towards gauge points

a b

Figure 5-5: (a) AUTODYN model (b) product gases expansion

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Table 5-1: Simulation results for 104g bare C4 surface blast

Gauge Nos. Position Overpressure (psi) Ta (ms)

X Y Ps/Pr

1 280 990 26.6 (Ps) 0.905

2 620 810 58 (Pr) 0.83

3 390 790 75.3 (Pr) 0.671

4 370 550 203 (Pr) 0.381

The pressure-time history at gauge points 1 to 4, defined for positions of pressure

transducers, is shown in Figure 5-7. Only radial distances (X), rather than slant

heights, are shown in pressure-time plot. The blast arrival time and peak pressure

values are in close agreement with the experimental findings.

The exact material model for shaving foam was not available. Two-phase EOS for

water was used for the foam filling inside container. This EOS incorporates the effect

of evaporation. The simulation inside container filled with shaving foam was only

performed to have an idea of the wave propagation pattern and reflection from the

bottom and walls of the container. The AUTODYN model and C4 detonation inside

the container is shown in Figure 5-8. The blast wave reflection from the base of the

container and walls are shown in Figure 5-8(b). The nearest part of the container with

the C4 charge has undergone deformation as seen from Figure 5-8(c). However, any

escape of the blast pressure in lateral directions is not observed in the simulation.

Figure 5-7: Simulated P(t) history of gauge points for 104g bare C4

surface blast

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5.3.2 Fragments Impact on Scaled down Container

The response of the container to fragment impact was investigated using coupled

SPH-ALE approach. The scaled down shell and its fragmentation was modeled and

simulated using SPH solver. The container was modeled in ALE. Quarter symmetric

FE model of shell and container is shown in Figure 5-9. The height of the container

was adjusted to simulate only the impact of the highest velocity fragments from the

cylindrical part of the shell. That is why the fragments from the base of the shell were

deleted at 76.0 s after detonation just to reduce the computational time and efforts.

Figure 5-9: FE model for shell and container

a b c

Figure 5-8: (a) AUTODYN Model (b) blast wave reflection from base and walls (c) blast

wave loading on container walls

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Fragments weighing tens of milligrams to 6.5 grams were produced. The fragments’

mass, spatial distribution and velocity distribution has already been presented in

Figure 3-13. The shell fragmentation at 63.93 s after detonation and the velocity

plot are shown in Figure 5-11. The fastest fragments traversed a radial distance of 86

mm as shown in this figure. The detonation product gases were deleted to study the

impact of only fragments with the container. An isometric view of the fragments with

the container wall at 78.8 s is shown in Figure 5-12.

Figure 5-11: Isometric view of the fragments, radial dispersion and container

Figure 5-10: (a) Shell fragmentation at 63.93 s and (b) velocity plot of the gauge points

a b

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The fragments impact and penetration is shown in Figure 5-12(a). The steel liner

deformation and perforation by few of the fragments through this lining material at

131 s is visible in Figure 5-12(b). The composite layers of laminated GFRP and

Kevlar fabric has offered a good resistance to impacting fragments leading to a drop

in fragments velocity. Fragments perforated the steel liner were captured within the

composite layers. The fragments lost most of their kinetic energy due to high

resistance offered by the composite materials combination. The velocity plot of the

gauge points after impacting the container walls is shown in Figure 5-13.

Although the container was not tested experimentally against the fragments, the

tested configurations against the shell fragmentation presented in Chapter 4 validate

the simulated results.

Figure 5-13: Fragments velocity after impacting the container walls

Figure 5-12: Fragments penetration into steel liner and its deformation

a b

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5.4 Experimental Results

5.4.1 Scaled down Container Test

The small-sized bubbles (15 – 100 m) in shaving foam were found to be stable over

time. The measured sound speed in the two-phase medium, 65.98±3 m/s, was far

below the sound speed in air and water. This significant difference in the acoustic

property played an important role in peak pressure attenuation. Two experiments

were performed with 104 grams C4 charge as surface burst and inside the cylindrical

container filled with shaving foam. The appearance of fireball is the most immediate

event upon detonation of an energetic material. For bare C4 detonation, the entrapped

oxygen within the fireball assists in afterburning reactions and enhances the total

energy. The total heat of combustion is the sum of heat of detonation and the

afterburning heat [2]. The measured fireball radius from high-speed images was 1.1

m. The resulting high pressure and temperature trigger the formation of a blast wave

in air. Consequently, the blast wave begins to propagate outwards in air. The

sequence of events is shown in Figure 5-14, Figure 5-15 and Figure 5-16. The high-

speed Phantom camera was operated at frame rate of 54000 fps for these tests.

Figure 5-15: High speed images (c) t= 0.320 ms and (d) t= 0.725 ms

d c

Figure 5-14: High speed images of bare C4 (a) detonator fired (b) t= 0.22 ms

after detonation

a b

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The high-speed images of 104 grams C4 detonation inside the cylindrical container

filled with shaving foam are shown in Figure 5-17, Figure 5-18 and Figure 5-19. The

shaving foam has completely suppressed the fireball owing to a rapid heat and

momentum transfer mechanisms. This transfer mechanism is enhanced by the

presence of finely distributed small-sized bubbles. The suppression of fireball also

seized the afterburning reactions due to a reduction in temperature [2, 8]. The

quenching of fireball also diminishes the thermal affects. The reduction in pressure is

also attributed to the much lower sound speed in foam compared to sound speed in

air and water.

The emergence of carbonaceous soot is also an indication of the fireball suppression

and quenching of afterburning reactions. The carbonaceous soot with the product

gases emerged from the open top of the container, along with the product gases, at

about 0.80 ms after the detonation, as seen from Figure 5-17(b). The high-speed

images shown in Figure 5-18 and Figure 5-19 further illustrate the relatively slower

movement compared to an open area detonation. The product gases did not reach the

transducer located above the container, 0.99 m above ground, until 1.8 ms, as shown

in Figure 5-19(e).

Figure 5-16: High speed images of bare C4 detonation

f e

a b

Figure 5-17: high speed images at (a) t=0.075ms (b) t = 0.800 ms

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The protective container also restricted the escape of product gases in lateral

directions. The combination of high strength Kevlar fabric 470 GSM and laminated

GFRP provided sufficient resistance to the expansion of product gases. The

laminated GFRP retained its integrity against the loading whereas a slight

deformation (elongation) was observed in Kevlar fabric. Adhesive debonding under

shock effect was observed in the outer layer of Kevlar fabric.

The container base was the most vulnerable place due to in contact detonation of C4.

The combination of EPS foam, Bakelite and PU-silica composite layers provided

protection against the extreme loading conditions of C4 detonation. Therefore, the

platform or object holding the container at the base (vehicle, ship and other

vulnerable objects or structures) will remain protected against the damaging effects

of energetic material detonation. The severity of the contact detonation can be seen

from Figure 5-20 where 30 grams C4 was detonated on top of a 5 mm thick steel

plate stand. A complete perforation of the steel plate was observed [2]. The novel

combination for the base proposed in present work has provided good protection

against any perforation, even with a higher charge.

c d

Figure 5-18: High speed images at (c) t=1.075ms and (d) t=1.475ms

Figure 5-19: C4 charge detonation inside container at (e) 1.80ms

and (f) t= 2.675ms

e f

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The pressure-time histories at the four transducers placed around the charge, in open

-air and inside container, are shown in Figure 5-21(a & b) respectively. Transducer

S1 has recorded side-on (incident) overpressure whereas transducers S2, S3 & S4

have experienced some levels of pressure reflection due to their orientation and

location with respect to the charge as shown in the experimental setups of Figure 5-3.

Figure 5-20: Contact detonation of 30 g C4 (a) test setup (b) post-test view

a b

a

b

Figure 5-21: Pressure plots for 104g C4 detonated (a) Surface

burst (b) inside container

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The P(t) plot for 104g bare C4 surface burst is shown in Figure 5-21(a). A reflected

overpressure of 203 psi (1399.6 kPa) was measured at transducer S4 located 0.55 m

above ground at a radial distance of 0.370 m from cylindrical axis (X). The

corresponding arrival time (Ta) was 0.38 ms. A reflected overpressure of 70.5 psi

(486 kPa) was measured at S2 located 0.81 m above ground at the radial distance(X)

of 0.61 m.

In case of the detonation inside container, the blast wave undergoes several

reflections from the bottom and the walls of the container, as evident from the shape

of the P(t) plot in Figure 5-21(b). The pressure transducer S4 placed at the height of

0.550 m and radial distance of 0.470 m recorded a reflected overpressure of 8.4 psi

(57.9 kPa) with an arrival time of 1.75 ms. The maximum pressure measured was

18.3 psi (126 kPa) at transducer S1 placed on top and 80 mm away from the outer

walls of the container. The arrival time for the peak value was 1.83 ms.

A pressure reduction of more than 80% is obtained with the arrangement. The

shaving foam also caused a significant delay in the upward flow of the product gases,

as evident from high-speed images in Figure 5-17(a-b) and pressure plot in Figure

5-21(b). The layered combination of laminated GFRP and Kevlar fabric provided

sufficient strength to contain the rest of the detonation product gases and the blast

wave. The post-test sights of the container and PU-silica composite are shown in

Figure 5-22

Although the effect of fragmentation was not studied experimentally, a simulation

was performed to study the fragment impact on the container. The fragment’s

velocities were immediately reduced to below 200 m/s on meeting the walls of the

container, showing evidence that the container would also provide protection against

c a b

Figure 5-22: Post-test sights of (a & b) PU-sand composite top and side (c) container

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fragments. The investigation has produced a reliable approach towards on-spot

fireball suppression leading to thermal effects diminution, blast wave mitigation and

ultimate containment against fragments. A good agreement between simulated and

experimental results for bare blast parameters was obtained.

5.4.2 Container Test with 1.0 kg TNT Equivalent Charge

The scaled down container for 104 grams C4 charge was scaled up to contain the

detonation effects of 1.0 kg bare or 0.6 kg steel cased TNT equivalent charge (pipe

bomb). The full scale container comprised an inner and an outer cylindrical

container. The inner layer was made of 3 mm thick mild steel (MS) cylinder with an

inner diameter (ID) 500 mm and height of 350 mm. A 5 mm thick MS disc was

welded at the bottom of the cylinder. Three steel fixtures of tubular configuration 40

mm high were welded 120o apart to the bottom plate. Four layers of Kevlar woven

fabric 470 GSM were wrapped on the MS cylinder. The weight of the inner cylinder

shown in Figure 5-23 was 24.4 kg.

EPS Foam 50 mm thick and of diameter 490 mm was positioned on MS bottom

plate. Bakelite sheet measuring 380 x 295 x 20 mm3 and weighing 3.2 kg was then

placed on top of EPS foam. PU-Silica disc prepared with 6 alternate layers of PU and

silica was placed on the Bakelite sheet. Another sheet of EPS foam with thickness of

50 mm and diameter of 200 mm was then placed on the PU-silica composite. The

PU-silica, EPS foam and Bakelite sheets are shown in Figure 5-24.

a b

Figure 5-23: (a) MS cylinder (b) Inner container

Figure 5-24: (a, b) PU-silica disc (c) EPS foam and Bakelite sheet c a b

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The outer cylinder was made of 8 mm thick laminated GFRP sheets with inner

diameter 550 mm and height 800 mm. A single layer of Kevlar fabric 110 GSM was

employed at the inner surface of the GFRP cylinder with silicon sealant. Eight layers

of Kevlar fabric 470 GSM were then wrapped on the outer surface of the GFRP

cylinder shown in Figure 5-25. The top and bottom of the outer cylinder were left

open. The outer container shown in Figure 5-25 weighed 34 kg.

The inner cylinder was then placed inside the outer composite cylinder. The net

weight of the combined container was 67 kg. C4 charge weighing 800 grams (1.0

kg TNT equivalent) was placed at the center of the container as shown in Figure

5-26(a). Shaving foam was filled around the charge and inside the inner container as

shown in Figure 5-26(b). The charge was initiated at the top end.

b c a

Figure 5-25: (a) GFRP cylinder (b) inner view of composite container (c) outer

composite container

a b

Figure 5-26: (a) C4 placed inside container (b) shaving foam filled

around C4

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The testing setup is shown in Figure 5-27. Three pressure transducers were placed

0.9 m above ground level at radial distances of 0.8, 0.9 and 1.0 meter from center of

charge. The transducers were positioned to measure the reflected overpressures (Pr).

The shaving foam completely suppressed the fireball and the container restricted the

movement of product gases in lateral directions. The high-speed images of the event

at different time steps are shown in Figure 5-28(a – e). The product gases appeared

from the open top after 0.482 ms of C4 detonation. The expansion of carbonaceous

soot with product gases is shown in the high-speed images. The outer layer of the

Kevlar fabric was detached due to debonding of adhesive. Figure 5-28(f) shows the

post experiment view of the container.

Figure 5-27: Experimental setup for 800 g C4 detonation inside container

(a) at t= 0 (b) at t= 0.482ms (c) at t= 1.50ms

(d) at t= 2.0 ms (e) at t= 4.2ms (f)

Figure 5-28: High-speed images of 800g C4 detonation inside container

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There was a 40 mm gap between the base of the inner cylinder and ground level to

allow for the expansion of MS base plate. However, the intense pressure detached the

welded base plate from the MS cylinder. Some leakage of the gases at the bottom

side was observed at a later stage. These gases were less pressurized and reached the

1.5 m radial distance after 35.0 ms of detonation.

The measured reflected overpressure and arrival time data is shown in Figure 5-29. A

reflected overpressure peak of 25.5 psi (175.8 kPa) was recorded at 0.9 m from the

charge center. A maximum reflected overpressure of 12.4 psi (85.5 kPa) was

recorded at 1.0 m distance from the center of the container.

5.4.3 Container Test with Steel Cased Charge (Pipe-bomb)

The second experiment of the container was performed to study its protective

capability against combined blast, fragmentation and thermal effects. A steel cased

charge (pipe-bomb), shown in Figure 5-30, was considered. This cased explosive

also simulates the effects of a lighter IED. The details of the steel cased charge are

given in Table 5-2.

Figure 5-30: Steel cased charge (Pipe-bomb)

Figure 5-29: Reflected overpressure-time history for

800g C4 detonation inside container

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Table 5-2: Material and dimensions of pipe-bomb for blast and fragmentation study

Material Mass (g) Length(mm) OD(mm) ID (mm)

MS Casing 1275 173 61 50

Comp-B filling 565 170 50 --

The blast wave parameters and fragmentation characteristics of this steel cased

charge were not studied experimentally. However, numerical simulations were

performed to have an estimate of these parameters. The SPH simulations of the

fragmentation within the MS cylinder are shown in Figure 5-31 and Figure 5-32.

A total of 732 fragments were produced. These fragments were grouped in to four

categories based on their mass in grams (g);

a b c

Figure 5-31: (a) SPH- ALE model for steel cased charge and inner container (b) at 15

s of detonation (c) fragmentation at 40 s

a b

Figure 5-32: (a) Gauge points location at 58s, (b) radial flight at 105 s

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Very small < 0.1 g

Small 0.1 – 1.0 g

Medium 1.0 – 5.5 g

Large > 5.5 g

The number of fragments and their mass distribution is shown in Figure 5-33(a)

while the velocity of the gauge points defined on the casing is shown in Figure

5-33(b). Most of the fragments have velocities around 1550 m/s. The fragment

velocities were comparable to that of the scaled down shell described in Chapter 3.

However, the mass distribution is on the higher side.

The overall strength of the container was already weakened by the explosive loading

during the first experiment of 1.0 kg TNT equivalent charge. An additional layer of

GFRP was laid inside the MS cylinder for this test. The container filled with shaving

foam and the testing setup is shown in Figure 5-34(a, b).

a b

Figure 5-33: (a) No. of fragments and mass distribution (b) fragments velocity plot

a b

Figure 5-34: (a) Shaving foam filled around steel cased charge (b) experimental setup

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The amount of shaving foam filled for this test was relatively less as shown in Figure

5-34(a). That is why the fire ball was partially suppressed as can be seen from the

high-speed images in Figure 5-35(b – c). However, the container still provided

significant protection against overpressure. The appearance of a partially quenched

fireball and the product gases containing carbonaceous soot from the open top are

evident in Figure 5-35(b – f).

Although, the container collapsed during this test, there was no evidence of any

debris flight beyond 1.5 m from the blast. The additional layer of GFRP inside the

MS cylinder was able to offer considerable resistance against high velocity

fragments. Majority of the fragments lost their kinetic energy while perforating this

layer. A view of the fragments impact and perforation through inner and outer layers

of GFRP is shown in Figure 5-36(a) and Figure 5-36 (b) respectively.

(a) t=0 (b) t=0.407ms (c) t= 0.648ms

(d) t=1.222ms (e) t=2.500ms (f) t=6.055ms

Figure 5-35: High-speed images of steel cased 565g Comp-B detonation inside container

a b

Figure 5-36: Fragments impact and perforation (a) inner layer (b) outer layer of GFRP

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The outer composite container was able to contain the majority of the fragments.

Only 13 fragments were able to perforate the outer layer of Kevlar fabric as shown in

Figure 5-37(a, b). The bottom MS disc is shown in Figure 5-37(c). A combination of

lightweight materials (EPS foam, Bakelite and PU-silica) at the bottom of the

container and in contact with the charge was able to mitigate the extreme loading.

Although the MS disc at the bottom of the container was deformed, no signs of a

fragment penetration were observed, as visible in Figure 5-37(c).

The maximum reflected overpressure measured at 0.85 m was 6.8 psi (46.88 kPa)

with an arrival time of 1.21 ms. The first peak value at 0.9 m distance was 5.8 psi (40

kPa) with arrival time of 1.41 ms. The multiple reflections from the ground and the

walls of the container yielded a reflected overpressure of 11.79 psi (81 kPa) at the

distance of 0.9 m. The reflected overpressure-time history is shown in Figure 5-38.

Figure 5-37: (a, b) Fragments perforation through outer layer of Kevlar fabric

(c) bottom MS disc after second test

b

c

a

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Table 5-3 presents comparison of the present studies with Conwep results. A hemi-

spherical surface burst was considered for Conwep calculations. As the charge was

positioned 166 mm above the ground level, the slant heights for Conwep calculations

[9] corresponding to given radial distances of 1.0 and 0.9 meter were 1.2 and 1.1

meter respectively. The transducers were 0.9 m above the ground level.

Table 5-3: Comparison of experimental results with Conwep calculations

W (TNT

eq.)

Conwep Results- Surface Burst With Container Reduction

R(m) Ta(ms) Ps(psi) Pr(psi) Ta(ms) Pr(psi) Ps(psi) %

1.0 kg

1.0 0.65 133 705 1.73 12.8 3.3 97

0.9 0.55 163 940 1.48 25.5 5.5 98

0.6 kg

Steel

Cased

0.9 0.64 109 570 1.41 11.79 3.1 97

As seen from the observed results the container was able to limit the devastating

blast, fragmentation and thermal effects of 1.0 kg TNT equivalent EM detonation.

Besides, for bare charge, the container also provides protection against cased charges

up to 0.6 kg TNT equivalent, pipe-bomb and lighter IEDs. The two layers container

provides safety against blast, fragmentation and thermal effects produced by higher

Figure 5-38: Reflected overpressure -time history for steel cased

565 g Comp-B charge inside container

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explosive mass compared to existing trash receptacles, BCRs etc. cited in references

[10-15] at reduced cost, size and weight.

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References

[1] B. Rutter, (2019).

[2] K. Ahmed, A.Q. Malik, AIP Advances. 10(2020) 065130.

[3] P. Peters, Military Medicine. 176(2011) 110.

[4] K. Ahmed, A.Q. Malik, A. Hussain, I.R. Ahmad, I. Ahmad, AIP Advances.

10(2020) 095221.

[5] U. ANSYS Inc., Century Dynamics. Release 14.0 documentation for ANSYS

AUTODYN.(2011).

[6] E. Lee, H. Hornig, J. Kury, Adiabatic expansion of high explosive detonation

products(1968).

[7] H. Draganić, D. Varevac, Shock and Vibration. 2018(2018).

[8] L.S. Lebel, P. Brousseau, L. Erhardt, W.S. Andrews, Combustion and flame.

161(2014) 1038.

[9] D. Hyde, US Army Engineer Waterways Experiment Station, USA. 2(1991).

[10] M. Silnikov, A. Sadyrin, A. Mikhaylin, A. Orlov, Materials Physics &

Mechanics. 20(2014).

[11] Blastguard Trash Receptacles. Available from:

http://blastgardtech.com/blastwrap#blastgard-mtr.

[12] Blast Containment Tank. Available from:

https://www.tmi2001.com/products/blast-containment-tank/.

[13] A. Resnyansky, T. Delaney, Experimental study of blast mitigation in a water

mist(2006).

[14] J. Polak, R. Romek, A. Wiśniewski, Problemy Techniki Uzbrojenia.

37(2008).

[15] G. Greenfield, P.R. Gefken, J.D. Colton, Container for explosive

device(2006).

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Conclusions and Recommendations Chapter 6

6.1 Conclusions

This PhD thesis focused on mitigating the damaging effects of bare and cased

energetic materials detonation, including lighter IEDs. A number of experimental and

numerical simulation studies were conducted to optimize the performance of

lightweight material combinations against combined blast, fragmentation and thermal

effects of cased EM detonation.

Commercially available Denim shaving foam was characterized. It was found that

the coarsening due to coalescence of bubbles slowed down with time. The bubble

size increased from an initial value of 15 m to 120 m in 2 hours showing good

stability. The viscosity of shaving foam measured at shear rate of 24.4 S-1

was 11650

cP. The two-phase medium exhibited a decreasing viscosity trend at higher shear

rates. The density and average sound speed measured in shaving foam at temperature

of 240C was 60.0 kg/m

3 and 65.98±3 m/s respectively. A significant reduction in

sound velocity is observed in shaving foam compared to its value in air. The

measured values were in good agreement to the values calculated using mixture law

or Wood’s formula.

The mitigation properties of foam were analyzed. Blast wave parameters, generated

by the C4 explosive detonation in air and covered in shaving foam, were measured

for scaled distances ranging from 0.39 – 1.80 m/kg1/3

. The shaving foam confinement

reduced the explosive fireball radius up to 80% and eliminated the afterburning

reactions. The suppression of fireball and quenching of afterburning reactions

diminished the thermal effects. An average blast overpressure reduction of 70% with

a corresponding 62% in impulse reduction was observed. This attenuation to blast

wave parameters is due to a number of factors including fast heat and momentum

transfer. The deformation of foam bubbles and the ultimate bursting of thin liquid

films dissipate energy. The evaporation of the liquid content contributes to decrease

the high pressure and temperature.

The fragmentation effect was studied by considering a scaled down (1:4) model of an

artillery shell. The shell fragmentation was characterized by measuring the fragments

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initial velocity, mass and spatial distributions. Fragments weighing from tens of

milligram(s) to 6.4 grams were produced with velocities ranging from 960 to 1555

m/s. The majority of the fragments produced were weighing below 1.0 gram. The

cylindrical part of the shell has larger contribution among high velocity fragments

1369-1555m/s than the conical and rear parts due to higher charge to mass (C/M)

ratio. The shell fragmentation was numerically characterized by SPH solver in

ANSYS UTODYN. The SPH simulations reproduced fragment mass, size and initial

velocity distribution reasonably well.

Lightweight protective configurations were tested against the combined blast and

fragmentation effects of a cased EM detonation. The protective capabilities were

tested against peak reflected overpressure of 235 psi (1620 kPa) and fragments

weighing up to 4.3 grams with velocities ranging from 961 - 1555 m/s. The

multilayer combinations of Kevlar woven fabrics, laminated GFRP and PU foam

demonstrated significant absorption and attenuation of impacting fragments. The

number of layers of Kevlar woven fabric has a profound effect on fragments

absorption. The configuration C-1 was able to capture 70% of the impacted

fragments. However, the Configurations employing Ceramic (alumina) tile were able

to withstand 7.62 x 39 mm MSC bullet impact, as well as blast and high velocity

fragments impact, without any significant backface signatures. The maximum depth

of depression measured for this configuration was 10 mm. This was well within the

European, German and British standards for backface signatures. The fiber

reinforced cladding of Kevlar-epoxy successfully prevented the disintegration of the

brittle alumina tile, maintaining the integrity of the configuration against multiple

fragments’ impact. The PU-silica composite having density of 1.1 g/cm3 and

compressive strength of 232 MPa has shown ductile behavior and good toughness.

The composite was not able to resist majority of the fragments penetration, however,

it was effective against severe blast loading.

Coupled SPH (Smoothed Particle Hydrodynamics)-ALE (Arbitrary Lagrangian-

Eulerian) approach was used to simulate the interaction of fragments with protective

configurations. A coupled Euler-ALE approach was employed for blast wave loading

on protective configurations. The blast wave parameters determined using coupled

ALE-Euler approaches were in good agreement with experimental results. These

approaches can be used to predict the blast and fragmentation effects produced by a

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cased EM detonation and hence minimize the cost and time consumption on full

scale testing.

A scaled down container weighing 13.5 kg and comprising 2 mm thick steel liner

layered by GFRP strips and nine layers of Kevlar woven fabric (470 GSM) was

tested with 104 grams of C4 after filling with shaving foam. The arrangement has

completely suppressed the fireball and hence diminished the thermal effects. It also

provided more than 80 % peak overpressure reduction.

A model container weighing 67 kg was developed and tested against detonation of

1.0 kg bare and 0.6 kg steel cased (pipe-bomb) TNT equivalent charges. This two

layers container completely quenched the thermal effects, provided 97%

overpressure reduction as well as contained the high velocity fragments. The novel

combination of lightweight materials (EPS foam, Bakelite and PU-silica) provided

protection against in contact explosive detonation at the base of the container. The

upshot of this research work, besides being of academic significance, is that it

provides ample data for the development of a blast mitigation system to combat

terrorism against lighter time bomb/IEDs placed at public places, high profile

meeting venues and transportation systems (land, air etc.).

6.2 Recommendations

The work presented in this thesis pertained to the studies for the development of

protective configurations using commercially available lightweight materials to

counter the effects of energetic material detonation.

The work can be extended to devise container that can withstand higher amounts of

charge. The development of a material model for shaving foam will be helpful in

simulating the response of this two-phase medium under extreme loading conditions.