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F E N V I R O N M E N T A L S E R V I C E S
June 141996
Town of Marblehead by and through its Water amp Sewer Commission and Electric Light Commission Attn Mr Dana E Snow amp Mr Robert Jolly Superintendent Water amp Sewer Commission PO Box 1108 Marblehead Massachusetts 01945
Project Name Lafayette Street Former Railroad Right-of-Way Marblehead MA MA DEP Release Tracking Number 3-12695 Project 9508132
Introduction
On May 2 1996 MyKroWaters personnel United States Environmental Protection Agency (USEPA) personnel and representatives from the Town of Marblehead conducted a site walkover at the former railroad right-of-way located on Lafayette Street in Marblehead (the Property) The following work has been completed by MyKro Waters for the Town of Marblehead in order to comply with the USEPA to further evaluate the extent of soil contamination
1 Additional soil sampling was conducted in areas located to the east of the Property along the bike path and from the eroded areas of the embankment adjacent to the bike path
2 Soil samples were submitted to IEA Laboratories Inc of Billerica MA for Total Lead analysis
The following report summarizes field activities and laboratory analytical results including data tables and a site plan
Subsurface Investigation
On May 16 1996 MyKro Waters collected twenty soil samples from zero to six inches below grade for Total Lead analysis Soil sampling locations and soil lead concentrations are plotted on Maps 1 and 2 Soil samples were sent to IEA Laboratories of Billerica MA with original laboratory data sheets located in the Appendix
Cf-
The Property was previously mapped and divided into 100 foot (length) grids lettered A through I outlined in MyKro Waters report dated November 16 1995 (see Sample
PO Box 1088 bull Concord Massachusetts 01742 bull Telephone 1-800-588-8680
Town of MarbleheadFonner Railroad Right-of-Way June 14 1996 File (2)marblehe5081321tdoc 2
Location Map Figure 1) The same grid identification scheme was used for this sampling round In addition a new block J was added to the grid Block T extends eastward approximately 360 feet from the eastern border of the Property to the nearest residential property visible from the path Samples were collected from eroded areas of the embankment adjacent to the bike path on the Property and from the middle of the bike path Samples are identified as B3S B4S CSS C6S C7S CSS IMS D5S D6S D7S G3S G4S H4S H5S H6S H7S J1S J2S J3S and J4S and are plotted on Maps 1 and 2
Soil Sampling amp Analytical Results
Soil samples were collected using a small hand auger All sampling equipment was decontaminated between sampling locations utilizing methanol and distilled water Soils were placed into new soil jars with screw-on caps Brief sample descriptions are outlined in the following table
Soil Matrix Description Town of MarbleheadFonner Railroad Right-of-Way
May 161996
Sample Sample Description ID
B3S Lt brown coarse sand with occasional granules and pebbles poorly sorted B4S Brown medium sand with roots granules and pebbles poorly sorted CSS Lt graybrown coarse sand with abundant pebbles and cobbles very poorly sorted C6S Black medium sand with some granules and pebbles poorly sorted C7S Dk brown medium sand with some granules and pebbles poorly sorted CSS Lt graybrown coarse sand with abundant pebbles and cobbles very poorly sorted D4S Lt graybrown coarse sand with abundant pebbles and cobbles very poorly sorted D5S Lt brown medium coarse sand with some pebbles and cobbles poorly sorted D6S Lt graybrown medium sand with abundant pebbles and cobbles very poorly sorted D7S Lt graybrown medium sand with abundant pebbles and cobbles very poorly sorted G3S Lt graybrown medium sand with some pebbles and cobbles very poorly sorted G4S Dk brown medium sandy soil with some pebbles roots H4S Lt graybrown medium sand with some pebbles and cobbles very poorly sorted H5S Dk brown medium sandy soil with some pebbles roots H6S Dk brown medium sandy soil with some pebbles roots H7S Lt graybrown medium sand with some pebbles and cobbles very poorly sorted J1S Lt graybrown coarse sand with some pebbles and cobbles very poorly sorted J2S Lt graybrown medium sand with some pebbles and cobbles very poorly sorted J3S Lt graybrown medium sand with some pebbles and cobbles very poorly sorted J4S Lt graybrown medium sand with some pebbles and cobbles very poorly sorted
Analytical results from Total Lead analysis are tabulated in Table 1 The Massachusetts Contingency Plan (MCP) Reportable Concentrations (RC) for lead is 300 mgkg for SI soils Five soil samples (C7S D4S D5S G3S and G4S) were over MCP RC SI standards These samples were located on paths adjacent to the bike path and on eroded
E N V I R O N M E N T A L S E R V I C E S
Town of MarbleheadFormer Railroad Right-of-Way June 141996 File (2)marblehe5081321tdoc 3
areas along the path The samples collected east of the property on the bike path (H7S J1S J2S J3S and J4S) had total lead concentrations below MCP RC SI standards
Table 1 Laboratory Analysis of Soil for Total Lead Concentrations
Town of MarbleheadFormer Railroad Right-of-Way May 161996
(concentrations in mgkg(dry)) Sample ID Date Results B3S 52196 10 B4S 52196 123 CSS 52196 44 C6S 52196 286 C7S 52196 385 CSS 52196 175 D4S 52196 598 D5S 52196 733 D6S 52196 260 D7S 52196 17 G3S 52196 7330 G4S 52196 1270 H4S 52196 89 H5S 52196 36 H6S 52196 60 H7S 52196 126 J1S 52196 53 J2S 52196 58 J3S 52196 68 J4S 52196 63 MCPRC 300
Notes 1 MCP RC Indicates the Massachusetts Contingency Plan Reportable Concentrations
2 Bold amp italicized results above lead MCP RCfor SI soils
E N V I R O N M E N T A L S E R V I C E S
Town of MarbleheadFormer Railroad Right-of-Way June 14 1996 File(2)marblehc5081321tdoc 4
Summary
MyKroWaters collected soil samples at twenty sampling locations at the former railroad right-of-way to further assess environmental conditions Soil samples were collected from the path east of the property as well as from eroded areas of the embankment adjacent to the bike path Soil samples were analyzed for Total Lead Five soil samples located on paths adjacent to the bike path and on eroded areas along the path were over MCP RC S1 standards for soil (300 mgkg) The samples collected east of the property on the path contained Total Lead concentrations below MCP RC SI standards
Based on the additional data it does not appear that geotextile cover will need to be extended further along the bike path than originally proposed in the Bid Specification for Pathway Restoration prepared for the Town of Marblehead However areas along the sides of the path were found to contain concentrations over 300 mgkg Exposure to these areas should be restricted as proposed If you have any questions or concerns please call me at 800-588-8680
Sincerely
Deborah R Farnsworth
cc Ted Bazenas US EPA Richard Chalpin MA DEP Mary Ellen Walsh-Rogalski Esq Town of Marblehead Stephen Anderson Esq Anderson amp Kreiger City of Salem Board of Health Board of Health Marblehead
f N V IR ON M f N I A L S E R V I C E S
APPENDIX
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IEA Inc 149 Rangeway Road Phone 508-667-1400 North Billerica MA 01862 Fax 508 667-7871 IEA
An Aquarion Company
Ms D Farnsworth Mykrowaters 97 Lowell Road Concord MA 01742
May 30 1996
Dear Ms Famsworth
Please find enclosed the analytical results of the sample(s) received at our laboratory on May 16 1996contains sections addressing the following information at a minimum
This report
sample ID correspondence table analytical methodology analytical results
bull chain-of-custody (if applicable) bull definitions of data qualifiers and terminology
state certifications
Client Project 9508132 Client Project Name MARBLEHEAD
EEA Report Ml 33-030 Purchase Order NA
Copies of this analytical report and supporting data are maintained in our files for a minimum of 3 years unless special arrangements are made Unless specifically indicated all analytical testing was performed at the lEA-Massachusetts laboratory
We appreciate your selection of our services and welcome any questions or suggestions you may have relative to this report Please contact your customer service representative at (508) 667-1400 for any additional information Thank you for utilizing our services and we hope you will consider us for your future analytical needs
I have reviewed and approved the enclosed data for final release
Sincerely
Michael F Wheeler PhD Laboratory Director lEA-Massachusetts
MWsmb
hrcportsformsdconwinrproOlOOma 53096 4 32 pm
Monroe Schaumtxjrg Whippany Gary Connecticut Illinois New Jersey North Carolina
203 261 4458 708 7050740 201 428 8181 919677 009C
1
V An Aquarion Company
Sample ID Correspondence Table
Client Sample ED
G3S
G4S
H4S
H5S
H6S
H7S
J1S
J2S
J3S
J4S
B4S
B3S
CSS
C6S
C7S
CSS
D4S
D5S
D6S
DBA Sample ID
M133-030-01
Ml 33-030-02
M133-030-03
Ml 33-030-04
Ml 33-030-05
M 133-030-06
Ml 33-030-07
Ml 33-030-08
Ml 33 -030-09
M133-030-10
M133-030-11
M133-030-12
M133-030-13
M133-030-14
M133-030-15
M133-030-16
M133-030-17
M133-030-18
Ml 33-030- 19
h rcporuformsidconwinrpC00100 ma 53096 4 32pm
IEA n Aquarion Company
D7S M133-030-20
h reporuformsdconwinrpf00100 ma 53096 4 32 pm
An Aquanon Company
Client Project Report Date
IEA Client ID
Xl G3S
G4S ^
H4S ^
4 H5S
H6S
16 H7S
7 J1S
8 J2S
9 J3S
lo J4S
fl B4S
12 B3S
^3 CSS
bull C6S
j15 C7S
Mykrowaters 9508 132 MA RBLEHEAD 053096
Parameter
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
IEA Laboratory Results
IEA ID M133-030 Received 051696
Date Results Units PQL Analyzed Analyst Method
7330 mgkg (dry) 10 052196 JB 6010
1270 mgkg (dry) 10 052196 JB 6010
89 mgkg (dry) 10 052196 JB 6010
36 mgkg (dry) 10 052196 JB 6010
60 mgkg (dry) 10 052196 JB 6010
126 mgkg (dry) 10 052196 JB 6010
53 mgkg (dry) 10 052196 JB 6010
58 mgkg (dry) 10 052196 JB 6010
68 mgkg (dry) 10 052196 JB 6010
63 mgkg (dry) 10 052196 JB 6010
^
123 mgkg (dry) 10 052196 JB 6010
10 mgkg (dry) 10 052196 JB 6010
44 mgkg (dry) 10 052196 JB 6010
286 mgkg (dry) 10 052196 JB 6010
385 mgkg (dry) 10 052196 JB 6010
h eportsforrnsdconwinrpf 10000ma Page 1 of 2 r - 053096 162 ]
ajIEAAn Aquanon Company
Client Mykrowaters Project 9508132 MARBLEHEAD Report Date 053096
IEA Client ID Parameter
TOTAL METALS 16 CSS Lead
TOTAL METALS D4S Lead
TOTAL METALS D5S Lead
TOTAL METALS
x 9 D6S Lead
TOTAL METALS D7S Lead
IEA Laboratory Results
Results Units
175 mgkg(dry)
598 mgkg(dry)
733 mgkg(dry)
260 mgkg(dry)
17 mgkg(dry)
Date PQL Analyzed
10 052196
10 052196
10 052196
10 052196
10 052196
IEA ID M133-030 Received 051696
Analyst Method
JB 6010
JB 6010
JB 6010
JB 6010
JB 6010
Comments PQL = Practical quantitation limit BQL = Below quantitation l imi t
reponsforms^dconwmrpf 10000 ma Page 2 of 2 053090 16 23
UJ
05
UJ
IEA An Aquanon Company
Definitions of Data Qualifiers and Terminology
A number of data qualifiers are widely used within the environmental testing industry and may be utilized in our data reports The following definitions of these qualifiers are included as a service to our clientele The majority of the qualifiers have evolved from the EPA contract laboratory program (CLP)
B - This flag is used when the analyte is found in the associated blank as well as in the sample It indicates possibleprobable blank contamination and warns the data user to use caution when applying the results of this analyte
BQL - Below Quantitation Limit indicates the compound was not detected in the sample above the practical quanmation limit
D - Indicates the compound was diluted below the calibration range
E - Indicates that the concentration of the specific compound exceeded the calibration range of the instrument for that particular analysis
J - Indicates an estimated value The compound is determined to be present in the sample based on GCMS criteria but the amount is less than the sample quantitation limit IEA - MA GCMS reports do not typically report J - marked results If requested J - marked results are provided and the report flagged to verify that the data was appropriately reviewed
MDL - The method detection limit is defined as the minimum concentration of a substance that can be measured and reported with 99 confidence that the analyte concentration is greater than zero
NA - Not applicable or not available
ND - Indicates the compound or analyte was not detected in the sample above the method detection limit or the practical quantitanon limit for the particular analysis
PQL - The practical quantitation limit is the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine operating conditions
h reportstorms d^
PIEA An Aquarion Company
Analytical Methodology
IEA utilizes approved environmental methodologies whenever possible and appropriate Due to the varying nature of sample matrices submitted to our laboratories we utilize a wide variety of analytical methodologies and quality assurance protocols Analytical results and Quality Assurance protocols employed by our network laboratories are based on guidelines specified in the following documents
(1) Methods of Organic Chemical Analysis of Municipal and Industrial Wastewater Federal Register Vol 49 No 209 October 26 1984
(2) Test Methods for Evaluating Solid Waste SW-846 Third Edition September 1986 USEPA
(3) Standard Methods for the Examination of Water and Wastewater 1985 14th15th and 16lh Edition
(4) Methods for Chemical Analysis of Water and Wastes March 1983 EMSL EPA
(5) Manual of Analytical Methods for the Analysis of Pesticides in Humans and Environmental Samples EPA 6008-80-038 June 1980
(6) Organic Analysis Multi-media Multi-Concentration-IFB-CLP January 1991 Document Number OLMO1 2 (plus revisions)
(7) Inorganic Analysis Multi-media Multi-Concentration-IFB-CLP Document Number ILM01 0
(8) Handbook for Analytical Quality Control in Water and Wastewater Laboratories EPA-6004-79-019 March 1979
(9) National Enforcement Investigation Center Policies and Procedures Manual EPA-330978001-R Revised May 1986
(10) Manual for the Certification of Laboratories Analyzing Drinking Water April 1990 EPA5709-90008
(11) NIOSH Manual of Analytical Methods August 1994 4th Edition
h reportsformsckcmwinrpro0202 ma
bullailEA AAnn AquanoAquanon CompanyI I n Cor
State Certifications
In some instances it may be necessary for environmental data to be reported to a regulatory authority with reference to a certified laboratory For your convenience the laboratory identification numbers for the lEA-Massachusetts laboratory are provided in the following table Many states certify laboratories for specific parameters or tests within a category (eg EPA method 624 for wastewater) The information in the following table indicates the lab is certified in a general category of testing such as drinking water or wastewater analysis The laboratory should be contacted directly if parameter specific certification information is required
lEA-Massachusetts Certification Summary as of November 1993
L
State Responsible Agency Area of Certification Lab Number
Connecticut Department of Health Services General Environmental 0646
Maine Department of Human Services Drinking Water MA038
Massachusetts Department of Environmental Drinking Water MA038 Protection Wastewater
New Hampshire Department of Environmental Drinking Water C300 Services Wastewater
New York Department of Public Health Wastewater 10838
North Carolina Department of Natural Wastewater 333 Resources
Rhode Island Department of Health Chemistry A58
Virginia Department of General Services Drinking Water 00157
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SKETCH A-1
TYPICAL PATHWAY PLAN VIEW (see Sketch A-2 for detail)
LOAMCOMPOST BERM
STONE DUST AND SOIL AGGREGATE SUB-BASE OVER GEOTEXTILE FABRIC
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Town of MarbleheadFonner Railroad Right-of-Way June 14 1996 File (2)marblehe5081321tdoc 2
Location Map Figure 1) The same grid identification scheme was used for this sampling round In addition a new block J was added to the grid Block T extends eastward approximately 360 feet from the eastern border of the Property to the nearest residential property visible from the path Samples were collected from eroded areas of the embankment adjacent to the bike path on the Property and from the middle of the bike path Samples are identified as B3S B4S CSS C6S C7S CSS IMS D5S D6S D7S G3S G4S H4S H5S H6S H7S J1S J2S J3S and J4S and are plotted on Maps 1 and 2
Soil Sampling amp Analytical Results
Soil samples were collected using a small hand auger All sampling equipment was decontaminated between sampling locations utilizing methanol and distilled water Soils were placed into new soil jars with screw-on caps Brief sample descriptions are outlined in the following table
Soil Matrix Description Town of MarbleheadFonner Railroad Right-of-Way
May 161996
Sample Sample Description ID
B3S Lt brown coarse sand with occasional granules and pebbles poorly sorted B4S Brown medium sand with roots granules and pebbles poorly sorted CSS Lt graybrown coarse sand with abundant pebbles and cobbles very poorly sorted C6S Black medium sand with some granules and pebbles poorly sorted C7S Dk brown medium sand with some granules and pebbles poorly sorted CSS Lt graybrown coarse sand with abundant pebbles and cobbles very poorly sorted D4S Lt graybrown coarse sand with abundant pebbles and cobbles very poorly sorted D5S Lt brown medium coarse sand with some pebbles and cobbles poorly sorted D6S Lt graybrown medium sand with abundant pebbles and cobbles very poorly sorted D7S Lt graybrown medium sand with abundant pebbles and cobbles very poorly sorted G3S Lt graybrown medium sand with some pebbles and cobbles very poorly sorted G4S Dk brown medium sandy soil with some pebbles roots H4S Lt graybrown medium sand with some pebbles and cobbles very poorly sorted H5S Dk brown medium sandy soil with some pebbles roots H6S Dk brown medium sandy soil with some pebbles roots H7S Lt graybrown medium sand with some pebbles and cobbles very poorly sorted J1S Lt graybrown coarse sand with some pebbles and cobbles very poorly sorted J2S Lt graybrown medium sand with some pebbles and cobbles very poorly sorted J3S Lt graybrown medium sand with some pebbles and cobbles very poorly sorted J4S Lt graybrown medium sand with some pebbles and cobbles very poorly sorted
Analytical results from Total Lead analysis are tabulated in Table 1 The Massachusetts Contingency Plan (MCP) Reportable Concentrations (RC) for lead is 300 mgkg for SI soils Five soil samples (C7S D4S D5S G3S and G4S) were over MCP RC SI standards These samples were located on paths adjacent to the bike path and on eroded
E N V I R O N M E N T A L S E R V I C E S
Town of MarbleheadFormer Railroad Right-of-Way June 141996 File (2)marblehe5081321tdoc 3
areas along the path The samples collected east of the property on the bike path (H7S J1S J2S J3S and J4S) had total lead concentrations below MCP RC SI standards
Table 1 Laboratory Analysis of Soil for Total Lead Concentrations
Town of MarbleheadFormer Railroad Right-of-Way May 161996
(concentrations in mgkg(dry)) Sample ID Date Results B3S 52196 10 B4S 52196 123 CSS 52196 44 C6S 52196 286 C7S 52196 385 CSS 52196 175 D4S 52196 598 D5S 52196 733 D6S 52196 260 D7S 52196 17 G3S 52196 7330 G4S 52196 1270 H4S 52196 89 H5S 52196 36 H6S 52196 60 H7S 52196 126 J1S 52196 53 J2S 52196 58 J3S 52196 68 J4S 52196 63 MCPRC 300
Notes 1 MCP RC Indicates the Massachusetts Contingency Plan Reportable Concentrations
2 Bold amp italicized results above lead MCP RCfor SI soils
E N V I R O N M E N T A L S E R V I C E S
Town of MarbleheadFormer Railroad Right-of-Way June 14 1996 File(2)marblehc5081321tdoc 4
Summary
MyKroWaters collected soil samples at twenty sampling locations at the former railroad right-of-way to further assess environmental conditions Soil samples were collected from the path east of the property as well as from eroded areas of the embankment adjacent to the bike path Soil samples were analyzed for Total Lead Five soil samples located on paths adjacent to the bike path and on eroded areas along the path were over MCP RC S1 standards for soil (300 mgkg) The samples collected east of the property on the path contained Total Lead concentrations below MCP RC SI standards
Based on the additional data it does not appear that geotextile cover will need to be extended further along the bike path than originally proposed in the Bid Specification for Pathway Restoration prepared for the Town of Marblehead However areas along the sides of the path were found to contain concentrations over 300 mgkg Exposure to these areas should be restricted as proposed If you have any questions or concerns please call me at 800-588-8680
Sincerely
Deborah R Farnsworth
cc Ted Bazenas US EPA Richard Chalpin MA DEP Mary Ellen Walsh-Rogalski Esq Town of Marblehead Stephen Anderson Esq Anderson amp Kreiger City of Salem Board of Health Board of Health Marblehead
f N V IR ON M f N I A L S E R V I C E S
APPENDIX
WHH3RHBB ( HV I R O N M E N I A t S E R V I C E S
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bull5 bullpound shyS2 8 rt O
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pound 2-S bullsin _pound E gt fth 5 O
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IEA Inc 149 Rangeway Road Phone 508-667-1400 North Billerica MA 01862 Fax 508 667-7871 IEA
An Aquarion Company
Ms D Farnsworth Mykrowaters 97 Lowell Road Concord MA 01742
May 30 1996
Dear Ms Famsworth
Please find enclosed the analytical results of the sample(s) received at our laboratory on May 16 1996contains sections addressing the following information at a minimum
This report
sample ID correspondence table analytical methodology analytical results
bull chain-of-custody (if applicable) bull definitions of data qualifiers and terminology
state certifications
Client Project 9508132 Client Project Name MARBLEHEAD
EEA Report Ml 33-030 Purchase Order NA
Copies of this analytical report and supporting data are maintained in our files for a minimum of 3 years unless special arrangements are made Unless specifically indicated all analytical testing was performed at the lEA-Massachusetts laboratory
We appreciate your selection of our services and welcome any questions or suggestions you may have relative to this report Please contact your customer service representative at (508) 667-1400 for any additional information Thank you for utilizing our services and we hope you will consider us for your future analytical needs
I have reviewed and approved the enclosed data for final release
Sincerely
Michael F Wheeler PhD Laboratory Director lEA-Massachusetts
MWsmb
hrcportsformsdconwinrproOlOOma 53096 4 32 pm
Monroe Schaumtxjrg Whippany Gary Connecticut Illinois New Jersey North Carolina
203 261 4458 708 7050740 201 428 8181 919677 009C
1
V An Aquarion Company
Sample ID Correspondence Table
Client Sample ED
G3S
G4S
H4S
H5S
H6S
H7S
J1S
J2S
J3S
J4S
B4S
B3S
CSS
C6S
C7S
CSS
D4S
D5S
D6S
DBA Sample ID
M133-030-01
Ml 33-030-02
M133-030-03
Ml 33-030-04
Ml 33-030-05
M 133-030-06
Ml 33-030-07
Ml 33-030-08
Ml 33 -030-09
M133-030-10
M133-030-11
M133-030-12
M133-030-13
M133-030-14
M133-030-15
M133-030-16
M133-030-17
M133-030-18
Ml 33-030- 19
h rcporuformsidconwinrpC00100 ma 53096 4 32pm
IEA n Aquarion Company
D7S M133-030-20
h reporuformsdconwinrpf00100 ma 53096 4 32 pm
An Aquanon Company
Client Project Report Date
IEA Client ID
Xl G3S
G4S ^
H4S ^
4 H5S
H6S
16 H7S
7 J1S
8 J2S
9 J3S
lo J4S
fl B4S
12 B3S
^3 CSS
bull C6S
j15 C7S
Mykrowaters 9508 132 MA RBLEHEAD 053096
Parameter
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
IEA Laboratory Results
IEA ID M133-030 Received 051696
Date Results Units PQL Analyzed Analyst Method
7330 mgkg (dry) 10 052196 JB 6010
1270 mgkg (dry) 10 052196 JB 6010
89 mgkg (dry) 10 052196 JB 6010
36 mgkg (dry) 10 052196 JB 6010
60 mgkg (dry) 10 052196 JB 6010
126 mgkg (dry) 10 052196 JB 6010
53 mgkg (dry) 10 052196 JB 6010
58 mgkg (dry) 10 052196 JB 6010
68 mgkg (dry) 10 052196 JB 6010
63 mgkg (dry) 10 052196 JB 6010
^
123 mgkg (dry) 10 052196 JB 6010
10 mgkg (dry) 10 052196 JB 6010
44 mgkg (dry) 10 052196 JB 6010
286 mgkg (dry) 10 052196 JB 6010
385 mgkg (dry) 10 052196 JB 6010
h eportsforrnsdconwinrpf 10000ma Page 1 of 2 r - 053096 162 ]
ajIEAAn Aquanon Company
Client Mykrowaters Project 9508132 MARBLEHEAD Report Date 053096
IEA Client ID Parameter
TOTAL METALS 16 CSS Lead
TOTAL METALS D4S Lead
TOTAL METALS D5S Lead
TOTAL METALS
x 9 D6S Lead
TOTAL METALS D7S Lead
IEA Laboratory Results
Results Units
175 mgkg(dry)
598 mgkg(dry)
733 mgkg(dry)
260 mgkg(dry)
17 mgkg(dry)
Date PQL Analyzed
10 052196
10 052196
10 052196
10 052196
10 052196
IEA ID M133-030 Received 051696
Analyst Method
JB 6010
JB 6010
JB 6010
JB 6010
JB 6010
Comments PQL = Practical quantitation limit BQL = Below quantitation l imi t
reponsforms^dconwmrpf 10000 ma Page 2 of 2 053090 16 23
UJ
05
UJ
IEA An Aquanon Company
Definitions of Data Qualifiers and Terminology
A number of data qualifiers are widely used within the environmental testing industry and may be utilized in our data reports The following definitions of these qualifiers are included as a service to our clientele The majority of the qualifiers have evolved from the EPA contract laboratory program (CLP)
B - This flag is used when the analyte is found in the associated blank as well as in the sample It indicates possibleprobable blank contamination and warns the data user to use caution when applying the results of this analyte
BQL - Below Quantitation Limit indicates the compound was not detected in the sample above the practical quanmation limit
D - Indicates the compound was diluted below the calibration range
E - Indicates that the concentration of the specific compound exceeded the calibration range of the instrument for that particular analysis
J - Indicates an estimated value The compound is determined to be present in the sample based on GCMS criteria but the amount is less than the sample quantitation limit IEA - MA GCMS reports do not typically report J - marked results If requested J - marked results are provided and the report flagged to verify that the data was appropriately reviewed
MDL - The method detection limit is defined as the minimum concentration of a substance that can be measured and reported with 99 confidence that the analyte concentration is greater than zero
NA - Not applicable or not available
ND - Indicates the compound or analyte was not detected in the sample above the method detection limit or the practical quantitanon limit for the particular analysis
PQL - The practical quantitation limit is the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine operating conditions
h reportstorms d^
PIEA An Aquarion Company
Analytical Methodology
IEA utilizes approved environmental methodologies whenever possible and appropriate Due to the varying nature of sample matrices submitted to our laboratories we utilize a wide variety of analytical methodologies and quality assurance protocols Analytical results and Quality Assurance protocols employed by our network laboratories are based on guidelines specified in the following documents
(1) Methods of Organic Chemical Analysis of Municipal and Industrial Wastewater Federal Register Vol 49 No 209 October 26 1984
(2) Test Methods for Evaluating Solid Waste SW-846 Third Edition September 1986 USEPA
(3) Standard Methods for the Examination of Water and Wastewater 1985 14th15th and 16lh Edition
(4) Methods for Chemical Analysis of Water and Wastes March 1983 EMSL EPA
(5) Manual of Analytical Methods for the Analysis of Pesticides in Humans and Environmental Samples EPA 6008-80-038 June 1980
(6) Organic Analysis Multi-media Multi-Concentration-IFB-CLP January 1991 Document Number OLMO1 2 (plus revisions)
(7) Inorganic Analysis Multi-media Multi-Concentration-IFB-CLP Document Number ILM01 0
(8) Handbook for Analytical Quality Control in Water and Wastewater Laboratories EPA-6004-79-019 March 1979
(9) National Enforcement Investigation Center Policies and Procedures Manual EPA-330978001-R Revised May 1986
(10) Manual for the Certification of Laboratories Analyzing Drinking Water April 1990 EPA5709-90008
(11) NIOSH Manual of Analytical Methods August 1994 4th Edition
h reportsformsckcmwinrpro0202 ma
bullailEA AAnn AquanoAquanon CompanyI I n Cor
State Certifications
In some instances it may be necessary for environmental data to be reported to a regulatory authority with reference to a certified laboratory For your convenience the laboratory identification numbers for the lEA-Massachusetts laboratory are provided in the following table Many states certify laboratories for specific parameters or tests within a category (eg EPA method 624 for wastewater) The information in the following table indicates the lab is certified in a general category of testing such as drinking water or wastewater analysis The laboratory should be contacted directly if parameter specific certification information is required
lEA-Massachusetts Certification Summary as of November 1993
L
State Responsible Agency Area of Certification Lab Number
Connecticut Department of Health Services General Environmental 0646
Maine Department of Human Services Drinking Water MA038
Massachusetts Department of Environmental Drinking Water MA038 Protection Wastewater
New Hampshire Department of Environmental Drinking Water C300 Services Wastewater
New York Department of Public Health Wastewater 10838
North Carolina Department of Natural Wastewater 333 Resources
Rhode Island Department of Health Chemistry A58
Virginia Department of General Services Drinking Water 00157
h reponsformsdconwmrpf00202 ma
SKETCH A-1
TYPICAL PATHWAY PLAN VIEW (see Sketch A-2 for detail)
LOAMCOMPOST BERM
STONE DUST AND SOIL AGGREGATE SUB-BASE OVER GEOTEXTILE FABRIC
bull15
m co O
CD gt o
O m O m
m -n gt CD
o
p
OO TJ O CO
co O
CD CD co m CD
73
co CD
co m
o o -o o CO
33 O
O o o co CO CO m o
O
co 7s m o
gt
2
cc LU CD
O CL
CO I
O
LU
O)
05 O O ID
O Cpound o o
O
Q_
O Q_
_ O LU CD Q LU
co
V
Town of MarbleheadFormer Railroad Right-of-Way June 141996 File (2)marblehe5081321tdoc 3
areas along the path The samples collected east of the property on the bike path (H7S J1S J2S J3S and J4S) had total lead concentrations below MCP RC SI standards
Table 1 Laboratory Analysis of Soil for Total Lead Concentrations
Town of MarbleheadFormer Railroad Right-of-Way May 161996
(concentrations in mgkg(dry)) Sample ID Date Results B3S 52196 10 B4S 52196 123 CSS 52196 44 C6S 52196 286 C7S 52196 385 CSS 52196 175 D4S 52196 598 D5S 52196 733 D6S 52196 260 D7S 52196 17 G3S 52196 7330 G4S 52196 1270 H4S 52196 89 H5S 52196 36 H6S 52196 60 H7S 52196 126 J1S 52196 53 J2S 52196 58 J3S 52196 68 J4S 52196 63 MCPRC 300
Notes 1 MCP RC Indicates the Massachusetts Contingency Plan Reportable Concentrations
2 Bold amp italicized results above lead MCP RCfor SI soils
E N V I R O N M E N T A L S E R V I C E S
Town of MarbleheadFormer Railroad Right-of-Way June 14 1996 File(2)marblehc5081321tdoc 4
Summary
MyKroWaters collected soil samples at twenty sampling locations at the former railroad right-of-way to further assess environmental conditions Soil samples were collected from the path east of the property as well as from eroded areas of the embankment adjacent to the bike path Soil samples were analyzed for Total Lead Five soil samples located on paths adjacent to the bike path and on eroded areas along the path were over MCP RC S1 standards for soil (300 mgkg) The samples collected east of the property on the path contained Total Lead concentrations below MCP RC SI standards
Based on the additional data it does not appear that geotextile cover will need to be extended further along the bike path than originally proposed in the Bid Specification for Pathway Restoration prepared for the Town of Marblehead However areas along the sides of the path were found to contain concentrations over 300 mgkg Exposure to these areas should be restricted as proposed If you have any questions or concerns please call me at 800-588-8680
Sincerely
Deborah R Farnsworth
cc Ted Bazenas US EPA Richard Chalpin MA DEP Mary Ellen Walsh-Rogalski Esq Town of Marblehead Stephen Anderson Esq Anderson amp Kreiger City of Salem Board of Health Board of Health Marblehead
f N V IR ON M f N I A L S E R V I C E S
APPENDIX
WHH3RHBB ( HV I R O N M E N I A t S E R V I C E S
Q
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^ o SP H o
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IEA Inc 149 Rangeway Road Phone 508-667-1400 North Billerica MA 01862 Fax 508 667-7871 IEA
An Aquarion Company
Ms D Farnsworth Mykrowaters 97 Lowell Road Concord MA 01742
May 30 1996
Dear Ms Famsworth
Please find enclosed the analytical results of the sample(s) received at our laboratory on May 16 1996contains sections addressing the following information at a minimum
This report
sample ID correspondence table analytical methodology analytical results
bull chain-of-custody (if applicable) bull definitions of data qualifiers and terminology
state certifications
Client Project 9508132 Client Project Name MARBLEHEAD
EEA Report Ml 33-030 Purchase Order NA
Copies of this analytical report and supporting data are maintained in our files for a minimum of 3 years unless special arrangements are made Unless specifically indicated all analytical testing was performed at the lEA-Massachusetts laboratory
We appreciate your selection of our services and welcome any questions or suggestions you may have relative to this report Please contact your customer service representative at (508) 667-1400 for any additional information Thank you for utilizing our services and we hope you will consider us for your future analytical needs
I have reviewed and approved the enclosed data for final release
Sincerely
Michael F Wheeler PhD Laboratory Director lEA-Massachusetts
MWsmb
hrcportsformsdconwinrproOlOOma 53096 4 32 pm
Monroe Schaumtxjrg Whippany Gary Connecticut Illinois New Jersey North Carolina
203 261 4458 708 7050740 201 428 8181 919677 009C
1
V An Aquarion Company
Sample ID Correspondence Table
Client Sample ED
G3S
G4S
H4S
H5S
H6S
H7S
J1S
J2S
J3S
J4S
B4S
B3S
CSS
C6S
C7S
CSS
D4S
D5S
D6S
DBA Sample ID
M133-030-01
Ml 33-030-02
M133-030-03
Ml 33-030-04
Ml 33-030-05
M 133-030-06
Ml 33-030-07
Ml 33-030-08
Ml 33 -030-09
M133-030-10
M133-030-11
M133-030-12
M133-030-13
M133-030-14
M133-030-15
M133-030-16
M133-030-17
M133-030-18
Ml 33-030- 19
h rcporuformsidconwinrpC00100 ma 53096 4 32pm
IEA n Aquarion Company
D7S M133-030-20
h reporuformsdconwinrpf00100 ma 53096 4 32 pm
An Aquanon Company
Client Project Report Date
IEA Client ID
Xl G3S
G4S ^
H4S ^
4 H5S
H6S
16 H7S
7 J1S
8 J2S
9 J3S
lo J4S
fl B4S
12 B3S
^3 CSS
bull C6S
j15 C7S
Mykrowaters 9508 132 MA RBLEHEAD 053096
Parameter
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
IEA Laboratory Results
IEA ID M133-030 Received 051696
Date Results Units PQL Analyzed Analyst Method
7330 mgkg (dry) 10 052196 JB 6010
1270 mgkg (dry) 10 052196 JB 6010
89 mgkg (dry) 10 052196 JB 6010
36 mgkg (dry) 10 052196 JB 6010
60 mgkg (dry) 10 052196 JB 6010
126 mgkg (dry) 10 052196 JB 6010
53 mgkg (dry) 10 052196 JB 6010
58 mgkg (dry) 10 052196 JB 6010
68 mgkg (dry) 10 052196 JB 6010
63 mgkg (dry) 10 052196 JB 6010
^
123 mgkg (dry) 10 052196 JB 6010
10 mgkg (dry) 10 052196 JB 6010
44 mgkg (dry) 10 052196 JB 6010
286 mgkg (dry) 10 052196 JB 6010
385 mgkg (dry) 10 052196 JB 6010
h eportsforrnsdconwinrpf 10000ma Page 1 of 2 r - 053096 162 ]
ajIEAAn Aquanon Company
Client Mykrowaters Project 9508132 MARBLEHEAD Report Date 053096
IEA Client ID Parameter
TOTAL METALS 16 CSS Lead
TOTAL METALS D4S Lead
TOTAL METALS D5S Lead
TOTAL METALS
x 9 D6S Lead
TOTAL METALS D7S Lead
IEA Laboratory Results
Results Units
175 mgkg(dry)
598 mgkg(dry)
733 mgkg(dry)
260 mgkg(dry)
17 mgkg(dry)
Date PQL Analyzed
10 052196
10 052196
10 052196
10 052196
10 052196
IEA ID M133-030 Received 051696
Analyst Method
JB 6010
JB 6010
JB 6010
JB 6010
JB 6010
Comments PQL = Practical quantitation limit BQL = Below quantitation l imi t
reponsforms^dconwmrpf 10000 ma Page 2 of 2 053090 16 23
UJ
05
UJ
IEA An Aquanon Company
Definitions of Data Qualifiers and Terminology
A number of data qualifiers are widely used within the environmental testing industry and may be utilized in our data reports The following definitions of these qualifiers are included as a service to our clientele The majority of the qualifiers have evolved from the EPA contract laboratory program (CLP)
B - This flag is used when the analyte is found in the associated blank as well as in the sample It indicates possibleprobable blank contamination and warns the data user to use caution when applying the results of this analyte
BQL - Below Quantitation Limit indicates the compound was not detected in the sample above the practical quanmation limit
D - Indicates the compound was diluted below the calibration range
E - Indicates that the concentration of the specific compound exceeded the calibration range of the instrument for that particular analysis
J - Indicates an estimated value The compound is determined to be present in the sample based on GCMS criteria but the amount is less than the sample quantitation limit IEA - MA GCMS reports do not typically report J - marked results If requested J - marked results are provided and the report flagged to verify that the data was appropriately reviewed
MDL - The method detection limit is defined as the minimum concentration of a substance that can be measured and reported with 99 confidence that the analyte concentration is greater than zero
NA - Not applicable or not available
ND - Indicates the compound or analyte was not detected in the sample above the method detection limit or the practical quantitanon limit for the particular analysis
PQL - The practical quantitation limit is the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine operating conditions
h reportstorms d^
PIEA An Aquarion Company
Analytical Methodology
IEA utilizes approved environmental methodologies whenever possible and appropriate Due to the varying nature of sample matrices submitted to our laboratories we utilize a wide variety of analytical methodologies and quality assurance protocols Analytical results and Quality Assurance protocols employed by our network laboratories are based on guidelines specified in the following documents
(1) Methods of Organic Chemical Analysis of Municipal and Industrial Wastewater Federal Register Vol 49 No 209 October 26 1984
(2) Test Methods for Evaluating Solid Waste SW-846 Third Edition September 1986 USEPA
(3) Standard Methods for the Examination of Water and Wastewater 1985 14th15th and 16lh Edition
(4) Methods for Chemical Analysis of Water and Wastes March 1983 EMSL EPA
(5) Manual of Analytical Methods for the Analysis of Pesticides in Humans and Environmental Samples EPA 6008-80-038 June 1980
(6) Organic Analysis Multi-media Multi-Concentration-IFB-CLP January 1991 Document Number OLMO1 2 (plus revisions)
(7) Inorganic Analysis Multi-media Multi-Concentration-IFB-CLP Document Number ILM01 0
(8) Handbook for Analytical Quality Control in Water and Wastewater Laboratories EPA-6004-79-019 March 1979
(9) National Enforcement Investigation Center Policies and Procedures Manual EPA-330978001-R Revised May 1986
(10) Manual for the Certification of Laboratories Analyzing Drinking Water April 1990 EPA5709-90008
(11) NIOSH Manual of Analytical Methods August 1994 4th Edition
h reportsformsckcmwinrpro0202 ma
bullailEA AAnn AquanoAquanon CompanyI I n Cor
State Certifications
In some instances it may be necessary for environmental data to be reported to a regulatory authority with reference to a certified laboratory For your convenience the laboratory identification numbers for the lEA-Massachusetts laboratory are provided in the following table Many states certify laboratories for specific parameters or tests within a category (eg EPA method 624 for wastewater) The information in the following table indicates the lab is certified in a general category of testing such as drinking water or wastewater analysis The laboratory should be contacted directly if parameter specific certification information is required
lEA-Massachusetts Certification Summary as of November 1993
L
State Responsible Agency Area of Certification Lab Number
Connecticut Department of Health Services General Environmental 0646
Maine Department of Human Services Drinking Water MA038
Massachusetts Department of Environmental Drinking Water MA038 Protection Wastewater
New Hampshire Department of Environmental Drinking Water C300 Services Wastewater
New York Department of Public Health Wastewater 10838
North Carolina Department of Natural Wastewater 333 Resources
Rhode Island Department of Health Chemistry A58
Virginia Department of General Services Drinking Water 00157
h reponsformsdconwmrpf00202 ma
SKETCH A-1
TYPICAL PATHWAY PLAN VIEW (see Sketch A-2 for detail)
LOAMCOMPOST BERM
STONE DUST AND SOIL AGGREGATE SUB-BASE OVER GEOTEXTILE FABRIC
bull15
m co O
CD gt o
O m O m
m -n gt CD
o
p
OO TJ O CO
co O
CD CD co m CD
73
co CD
co m
o o -o o CO
33 O
O o o co CO CO m o
O
co 7s m o
gt
2
cc LU CD
O CL
CO I
O
LU
O)
05 O O ID
O Cpound o o
O
Q_
O Q_
_ O LU CD Q LU
co
V
Town of MarbleheadFormer Railroad Right-of-Way June 14 1996 File(2)marblehc5081321tdoc 4
Summary
MyKroWaters collected soil samples at twenty sampling locations at the former railroad right-of-way to further assess environmental conditions Soil samples were collected from the path east of the property as well as from eroded areas of the embankment adjacent to the bike path Soil samples were analyzed for Total Lead Five soil samples located on paths adjacent to the bike path and on eroded areas along the path were over MCP RC S1 standards for soil (300 mgkg) The samples collected east of the property on the path contained Total Lead concentrations below MCP RC SI standards
Based on the additional data it does not appear that geotextile cover will need to be extended further along the bike path than originally proposed in the Bid Specification for Pathway Restoration prepared for the Town of Marblehead However areas along the sides of the path were found to contain concentrations over 300 mgkg Exposure to these areas should be restricted as proposed If you have any questions or concerns please call me at 800-588-8680
Sincerely
Deborah R Farnsworth
cc Ted Bazenas US EPA Richard Chalpin MA DEP Mary Ellen Walsh-Rogalski Esq Town of Marblehead Stephen Anderson Esq Anderson amp Kreiger City of Salem Board of Health Board of Health Marblehead
f N V IR ON M f N I A L S E R V I C E S
APPENDIX
WHH3RHBB ( HV I R O N M E N I A t S E R V I C E S
Q
clO
O s~ N _laquo
^ o SP H o
bull5 bullpound shyS2 8 rt O
^ C3
O
Q mdash
C3 on
o poundgtN
pound 2-S bullsin _pound E gt fth 5 O
a bullsect c mdash
111J2 o
Q
eS 00
IEA Inc 149 Rangeway Road Phone 508-667-1400 North Billerica MA 01862 Fax 508 667-7871 IEA
An Aquarion Company
Ms D Farnsworth Mykrowaters 97 Lowell Road Concord MA 01742
May 30 1996
Dear Ms Famsworth
Please find enclosed the analytical results of the sample(s) received at our laboratory on May 16 1996contains sections addressing the following information at a minimum
This report
sample ID correspondence table analytical methodology analytical results
bull chain-of-custody (if applicable) bull definitions of data qualifiers and terminology
state certifications
Client Project 9508132 Client Project Name MARBLEHEAD
EEA Report Ml 33-030 Purchase Order NA
Copies of this analytical report and supporting data are maintained in our files for a minimum of 3 years unless special arrangements are made Unless specifically indicated all analytical testing was performed at the lEA-Massachusetts laboratory
We appreciate your selection of our services and welcome any questions or suggestions you may have relative to this report Please contact your customer service representative at (508) 667-1400 for any additional information Thank you for utilizing our services and we hope you will consider us for your future analytical needs
I have reviewed and approved the enclosed data for final release
Sincerely
Michael F Wheeler PhD Laboratory Director lEA-Massachusetts
MWsmb
hrcportsformsdconwinrproOlOOma 53096 4 32 pm
Monroe Schaumtxjrg Whippany Gary Connecticut Illinois New Jersey North Carolina
203 261 4458 708 7050740 201 428 8181 919677 009C
1
V An Aquarion Company
Sample ID Correspondence Table
Client Sample ED
G3S
G4S
H4S
H5S
H6S
H7S
J1S
J2S
J3S
J4S
B4S
B3S
CSS
C6S
C7S
CSS
D4S
D5S
D6S
DBA Sample ID
M133-030-01
Ml 33-030-02
M133-030-03
Ml 33-030-04
Ml 33-030-05
M 133-030-06
Ml 33-030-07
Ml 33-030-08
Ml 33 -030-09
M133-030-10
M133-030-11
M133-030-12
M133-030-13
M133-030-14
M133-030-15
M133-030-16
M133-030-17
M133-030-18
Ml 33-030- 19
h rcporuformsidconwinrpC00100 ma 53096 4 32pm
IEA n Aquarion Company
D7S M133-030-20
h reporuformsdconwinrpf00100 ma 53096 4 32 pm
An Aquanon Company
Client Project Report Date
IEA Client ID
Xl G3S
G4S ^
H4S ^
4 H5S
H6S
16 H7S
7 J1S
8 J2S
9 J3S
lo J4S
fl B4S
12 B3S
^3 CSS
bull C6S
j15 C7S
Mykrowaters 9508 132 MA RBLEHEAD 053096
Parameter
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
IEA Laboratory Results
IEA ID M133-030 Received 051696
Date Results Units PQL Analyzed Analyst Method
7330 mgkg (dry) 10 052196 JB 6010
1270 mgkg (dry) 10 052196 JB 6010
89 mgkg (dry) 10 052196 JB 6010
36 mgkg (dry) 10 052196 JB 6010
60 mgkg (dry) 10 052196 JB 6010
126 mgkg (dry) 10 052196 JB 6010
53 mgkg (dry) 10 052196 JB 6010
58 mgkg (dry) 10 052196 JB 6010
68 mgkg (dry) 10 052196 JB 6010
63 mgkg (dry) 10 052196 JB 6010
^
123 mgkg (dry) 10 052196 JB 6010
10 mgkg (dry) 10 052196 JB 6010
44 mgkg (dry) 10 052196 JB 6010
286 mgkg (dry) 10 052196 JB 6010
385 mgkg (dry) 10 052196 JB 6010
h eportsforrnsdconwinrpf 10000ma Page 1 of 2 r - 053096 162 ]
ajIEAAn Aquanon Company
Client Mykrowaters Project 9508132 MARBLEHEAD Report Date 053096
IEA Client ID Parameter
TOTAL METALS 16 CSS Lead
TOTAL METALS D4S Lead
TOTAL METALS D5S Lead
TOTAL METALS
x 9 D6S Lead
TOTAL METALS D7S Lead
IEA Laboratory Results
Results Units
175 mgkg(dry)
598 mgkg(dry)
733 mgkg(dry)
260 mgkg(dry)
17 mgkg(dry)
Date PQL Analyzed
10 052196
10 052196
10 052196
10 052196
10 052196
IEA ID M133-030 Received 051696
Analyst Method
JB 6010
JB 6010
JB 6010
JB 6010
JB 6010
Comments PQL = Practical quantitation limit BQL = Below quantitation l imi t
reponsforms^dconwmrpf 10000 ma Page 2 of 2 053090 16 23
UJ
05
UJ
IEA An Aquanon Company
Definitions of Data Qualifiers and Terminology
A number of data qualifiers are widely used within the environmental testing industry and may be utilized in our data reports The following definitions of these qualifiers are included as a service to our clientele The majority of the qualifiers have evolved from the EPA contract laboratory program (CLP)
B - This flag is used when the analyte is found in the associated blank as well as in the sample It indicates possibleprobable blank contamination and warns the data user to use caution when applying the results of this analyte
BQL - Below Quantitation Limit indicates the compound was not detected in the sample above the practical quanmation limit
D - Indicates the compound was diluted below the calibration range
E - Indicates that the concentration of the specific compound exceeded the calibration range of the instrument for that particular analysis
J - Indicates an estimated value The compound is determined to be present in the sample based on GCMS criteria but the amount is less than the sample quantitation limit IEA - MA GCMS reports do not typically report J - marked results If requested J - marked results are provided and the report flagged to verify that the data was appropriately reviewed
MDL - The method detection limit is defined as the minimum concentration of a substance that can be measured and reported with 99 confidence that the analyte concentration is greater than zero
NA - Not applicable or not available
ND - Indicates the compound or analyte was not detected in the sample above the method detection limit or the practical quantitanon limit for the particular analysis
PQL - The practical quantitation limit is the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine operating conditions
h reportstorms d^
PIEA An Aquarion Company
Analytical Methodology
IEA utilizes approved environmental methodologies whenever possible and appropriate Due to the varying nature of sample matrices submitted to our laboratories we utilize a wide variety of analytical methodologies and quality assurance protocols Analytical results and Quality Assurance protocols employed by our network laboratories are based on guidelines specified in the following documents
(1) Methods of Organic Chemical Analysis of Municipal and Industrial Wastewater Federal Register Vol 49 No 209 October 26 1984
(2) Test Methods for Evaluating Solid Waste SW-846 Third Edition September 1986 USEPA
(3) Standard Methods for the Examination of Water and Wastewater 1985 14th15th and 16lh Edition
(4) Methods for Chemical Analysis of Water and Wastes March 1983 EMSL EPA
(5) Manual of Analytical Methods for the Analysis of Pesticides in Humans and Environmental Samples EPA 6008-80-038 June 1980
(6) Organic Analysis Multi-media Multi-Concentration-IFB-CLP January 1991 Document Number OLMO1 2 (plus revisions)
(7) Inorganic Analysis Multi-media Multi-Concentration-IFB-CLP Document Number ILM01 0
(8) Handbook for Analytical Quality Control in Water and Wastewater Laboratories EPA-6004-79-019 March 1979
(9) National Enforcement Investigation Center Policies and Procedures Manual EPA-330978001-R Revised May 1986
(10) Manual for the Certification of Laboratories Analyzing Drinking Water April 1990 EPA5709-90008
(11) NIOSH Manual of Analytical Methods August 1994 4th Edition
h reportsformsckcmwinrpro0202 ma
bullailEA AAnn AquanoAquanon CompanyI I n Cor
State Certifications
In some instances it may be necessary for environmental data to be reported to a regulatory authority with reference to a certified laboratory For your convenience the laboratory identification numbers for the lEA-Massachusetts laboratory are provided in the following table Many states certify laboratories for specific parameters or tests within a category (eg EPA method 624 for wastewater) The information in the following table indicates the lab is certified in a general category of testing such as drinking water or wastewater analysis The laboratory should be contacted directly if parameter specific certification information is required
lEA-Massachusetts Certification Summary as of November 1993
L
State Responsible Agency Area of Certification Lab Number
Connecticut Department of Health Services General Environmental 0646
Maine Department of Human Services Drinking Water MA038
Massachusetts Department of Environmental Drinking Water MA038 Protection Wastewater
New Hampshire Department of Environmental Drinking Water C300 Services Wastewater
New York Department of Public Health Wastewater 10838
North Carolina Department of Natural Wastewater 333 Resources
Rhode Island Department of Health Chemistry A58
Virginia Department of General Services Drinking Water 00157
h reponsformsdconwmrpf00202 ma
SKETCH A-1
TYPICAL PATHWAY PLAN VIEW (see Sketch A-2 for detail)
LOAMCOMPOST BERM
STONE DUST AND SOIL AGGREGATE SUB-BASE OVER GEOTEXTILE FABRIC
bull15
m co O
CD gt o
O m O m
m -n gt CD
o
p
OO TJ O CO
co O
CD CD co m CD
73
co CD
co m
o o -o o CO
33 O
O o o co CO CO m o
O
co 7s m o
gt
2
cc LU CD
O CL
CO I
O
LU
O)
05 O O ID
O Cpound o o
O
Q_
O Q_
_ O LU CD Q LU
co
V
APPENDIX
WHH3RHBB ( HV I R O N M E N I A t S E R V I C E S
Q
clO
O s~ N _laquo
^ o SP H o
bull5 bullpound shyS2 8 rt O
^ C3
O
Q mdash
C3 on
o poundgtN
pound 2-S bullsin _pound E gt fth 5 O
a bullsect c mdash
111J2 o
Q
eS 00
IEA Inc 149 Rangeway Road Phone 508-667-1400 North Billerica MA 01862 Fax 508 667-7871 IEA
An Aquarion Company
Ms D Farnsworth Mykrowaters 97 Lowell Road Concord MA 01742
May 30 1996
Dear Ms Famsworth
Please find enclosed the analytical results of the sample(s) received at our laboratory on May 16 1996contains sections addressing the following information at a minimum
This report
sample ID correspondence table analytical methodology analytical results
bull chain-of-custody (if applicable) bull definitions of data qualifiers and terminology
state certifications
Client Project 9508132 Client Project Name MARBLEHEAD
EEA Report Ml 33-030 Purchase Order NA
Copies of this analytical report and supporting data are maintained in our files for a minimum of 3 years unless special arrangements are made Unless specifically indicated all analytical testing was performed at the lEA-Massachusetts laboratory
We appreciate your selection of our services and welcome any questions or suggestions you may have relative to this report Please contact your customer service representative at (508) 667-1400 for any additional information Thank you for utilizing our services and we hope you will consider us for your future analytical needs
I have reviewed and approved the enclosed data for final release
Sincerely
Michael F Wheeler PhD Laboratory Director lEA-Massachusetts
MWsmb
hrcportsformsdconwinrproOlOOma 53096 4 32 pm
Monroe Schaumtxjrg Whippany Gary Connecticut Illinois New Jersey North Carolina
203 261 4458 708 7050740 201 428 8181 919677 009C
1
V An Aquarion Company
Sample ID Correspondence Table
Client Sample ED
G3S
G4S
H4S
H5S
H6S
H7S
J1S
J2S
J3S
J4S
B4S
B3S
CSS
C6S
C7S
CSS
D4S
D5S
D6S
DBA Sample ID
M133-030-01
Ml 33-030-02
M133-030-03
Ml 33-030-04
Ml 33-030-05
M 133-030-06
Ml 33-030-07
Ml 33-030-08
Ml 33 -030-09
M133-030-10
M133-030-11
M133-030-12
M133-030-13
M133-030-14
M133-030-15
M133-030-16
M133-030-17
M133-030-18
Ml 33-030- 19
h rcporuformsidconwinrpC00100 ma 53096 4 32pm
IEA n Aquarion Company
D7S M133-030-20
h reporuformsdconwinrpf00100 ma 53096 4 32 pm
An Aquanon Company
Client Project Report Date
IEA Client ID
Xl G3S
G4S ^
H4S ^
4 H5S
H6S
16 H7S
7 J1S
8 J2S
9 J3S
lo J4S
fl B4S
12 B3S
^3 CSS
bull C6S
j15 C7S
Mykrowaters 9508 132 MA RBLEHEAD 053096
Parameter
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
IEA Laboratory Results
IEA ID M133-030 Received 051696
Date Results Units PQL Analyzed Analyst Method
7330 mgkg (dry) 10 052196 JB 6010
1270 mgkg (dry) 10 052196 JB 6010
89 mgkg (dry) 10 052196 JB 6010
36 mgkg (dry) 10 052196 JB 6010
60 mgkg (dry) 10 052196 JB 6010
126 mgkg (dry) 10 052196 JB 6010
53 mgkg (dry) 10 052196 JB 6010
58 mgkg (dry) 10 052196 JB 6010
68 mgkg (dry) 10 052196 JB 6010
63 mgkg (dry) 10 052196 JB 6010
^
123 mgkg (dry) 10 052196 JB 6010
10 mgkg (dry) 10 052196 JB 6010
44 mgkg (dry) 10 052196 JB 6010
286 mgkg (dry) 10 052196 JB 6010
385 mgkg (dry) 10 052196 JB 6010
h eportsforrnsdconwinrpf 10000ma Page 1 of 2 r - 053096 162 ]
ajIEAAn Aquanon Company
Client Mykrowaters Project 9508132 MARBLEHEAD Report Date 053096
IEA Client ID Parameter
TOTAL METALS 16 CSS Lead
TOTAL METALS D4S Lead
TOTAL METALS D5S Lead
TOTAL METALS
x 9 D6S Lead
TOTAL METALS D7S Lead
IEA Laboratory Results
Results Units
175 mgkg(dry)
598 mgkg(dry)
733 mgkg(dry)
260 mgkg(dry)
17 mgkg(dry)
Date PQL Analyzed
10 052196
10 052196
10 052196
10 052196
10 052196
IEA ID M133-030 Received 051696
Analyst Method
JB 6010
JB 6010
JB 6010
JB 6010
JB 6010
Comments PQL = Practical quantitation limit BQL = Below quantitation l imi t
reponsforms^dconwmrpf 10000 ma Page 2 of 2 053090 16 23
UJ
05
UJ
IEA An Aquanon Company
Definitions of Data Qualifiers and Terminology
A number of data qualifiers are widely used within the environmental testing industry and may be utilized in our data reports The following definitions of these qualifiers are included as a service to our clientele The majority of the qualifiers have evolved from the EPA contract laboratory program (CLP)
B - This flag is used when the analyte is found in the associated blank as well as in the sample It indicates possibleprobable blank contamination and warns the data user to use caution when applying the results of this analyte
BQL - Below Quantitation Limit indicates the compound was not detected in the sample above the practical quanmation limit
D - Indicates the compound was diluted below the calibration range
E - Indicates that the concentration of the specific compound exceeded the calibration range of the instrument for that particular analysis
J - Indicates an estimated value The compound is determined to be present in the sample based on GCMS criteria but the amount is less than the sample quantitation limit IEA - MA GCMS reports do not typically report J - marked results If requested J - marked results are provided and the report flagged to verify that the data was appropriately reviewed
MDL - The method detection limit is defined as the minimum concentration of a substance that can be measured and reported with 99 confidence that the analyte concentration is greater than zero
NA - Not applicable or not available
ND - Indicates the compound or analyte was not detected in the sample above the method detection limit or the practical quantitanon limit for the particular analysis
PQL - The practical quantitation limit is the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine operating conditions
h reportstorms d^
PIEA An Aquarion Company
Analytical Methodology
IEA utilizes approved environmental methodologies whenever possible and appropriate Due to the varying nature of sample matrices submitted to our laboratories we utilize a wide variety of analytical methodologies and quality assurance protocols Analytical results and Quality Assurance protocols employed by our network laboratories are based on guidelines specified in the following documents
(1) Methods of Organic Chemical Analysis of Municipal and Industrial Wastewater Federal Register Vol 49 No 209 October 26 1984
(2) Test Methods for Evaluating Solid Waste SW-846 Third Edition September 1986 USEPA
(3) Standard Methods for the Examination of Water and Wastewater 1985 14th15th and 16lh Edition
(4) Methods for Chemical Analysis of Water and Wastes March 1983 EMSL EPA
(5) Manual of Analytical Methods for the Analysis of Pesticides in Humans and Environmental Samples EPA 6008-80-038 June 1980
(6) Organic Analysis Multi-media Multi-Concentration-IFB-CLP January 1991 Document Number OLMO1 2 (plus revisions)
(7) Inorganic Analysis Multi-media Multi-Concentration-IFB-CLP Document Number ILM01 0
(8) Handbook for Analytical Quality Control in Water and Wastewater Laboratories EPA-6004-79-019 March 1979
(9) National Enforcement Investigation Center Policies and Procedures Manual EPA-330978001-R Revised May 1986
(10) Manual for the Certification of Laboratories Analyzing Drinking Water April 1990 EPA5709-90008
(11) NIOSH Manual of Analytical Methods August 1994 4th Edition
h reportsformsckcmwinrpro0202 ma
bullailEA AAnn AquanoAquanon CompanyI I n Cor
State Certifications
In some instances it may be necessary for environmental data to be reported to a regulatory authority with reference to a certified laboratory For your convenience the laboratory identification numbers for the lEA-Massachusetts laboratory are provided in the following table Many states certify laboratories for specific parameters or tests within a category (eg EPA method 624 for wastewater) The information in the following table indicates the lab is certified in a general category of testing such as drinking water or wastewater analysis The laboratory should be contacted directly if parameter specific certification information is required
lEA-Massachusetts Certification Summary as of November 1993
L
State Responsible Agency Area of Certification Lab Number
Connecticut Department of Health Services General Environmental 0646
Maine Department of Human Services Drinking Water MA038
Massachusetts Department of Environmental Drinking Water MA038 Protection Wastewater
New Hampshire Department of Environmental Drinking Water C300 Services Wastewater
New York Department of Public Health Wastewater 10838
North Carolina Department of Natural Wastewater 333 Resources
Rhode Island Department of Health Chemistry A58
Virginia Department of General Services Drinking Water 00157
h reponsformsdconwmrpf00202 ma
SKETCH A-1
TYPICAL PATHWAY PLAN VIEW (see Sketch A-2 for detail)
LOAMCOMPOST BERM
STONE DUST AND SOIL AGGREGATE SUB-BASE OVER GEOTEXTILE FABRIC
bull15
m co O
CD gt o
O m O m
m -n gt CD
o
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co O
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73
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33 O
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O
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O CL
CO I
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O
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V
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O s~ N _laquo
^ o SP H o
bull5 bullpound shyS2 8 rt O
^ C3
O
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C3 on
o poundgtN
pound 2-S bullsin _pound E gt fth 5 O
a bullsect c mdash
111J2 o
Q
eS 00
IEA Inc 149 Rangeway Road Phone 508-667-1400 North Billerica MA 01862 Fax 508 667-7871 IEA
An Aquarion Company
Ms D Farnsworth Mykrowaters 97 Lowell Road Concord MA 01742
May 30 1996
Dear Ms Famsworth
Please find enclosed the analytical results of the sample(s) received at our laboratory on May 16 1996contains sections addressing the following information at a minimum
This report
sample ID correspondence table analytical methodology analytical results
bull chain-of-custody (if applicable) bull definitions of data qualifiers and terminology
state certifications
Client Project 9508132 Client Project Name MARBLEHEAD
EEA Report Ml 33-030 Purchase Order NA
Copies of this analytical report and supporting data are maintained in our files for a minimum of 3 years unless special arrangements are made Unless specifically indicated all analytical testing was performed at the lEA-Massachusetts laboratory
We appreciate your selection of our services and welcome any questions or suggestions you may have relative to this report Please contact your customer service representative at (508) 667-1400 for any additional information Thank you for utilizing our services and we hope you will consider us for your future analytical needs
I have reviewed and approved the enclosed data for final release
Sincerely
Michael F Wheeler PhD Laboratory Director lEA-Massachusetts
MWsmb
hrcportsformsdconwinrproOlOOma 53096 4 32 pm
Monroe Schaumtxjrg Whippany Gary Connecticut Illinois New Jersey North Carolina
203 261 4458 708 7050740 201 428 8181 919677 009C
1
V An Aquarion Company
Sample ID Correspondence Table
Client Sample ED
G3S
G4S
H4S
H5S
H6S
H7S
J1S
J2S
J3S
J4S
B4S
B3S
CSS
C6S
C7S
CSS
D4S
D5S
D6S
DBA Sample ID
M133-030-01
Ml 33-030-02
M133-030-03
Ml 33-030-04
Ml 33-030-05
M 133-030-06
Ml 33-030-07
Ml 33-030-08
Ml 33 -030-09
M133-030-10
M133-030-11
M133-030-12
M133-030-13
M133-030-14
M133-030-15
M133-030-16
M133-030-17
M133-030-18
Ml 33-030- 19
h rcporuformsidconwinrpC00100 ma 53096 4 32pm
IEA n Aquarion Company
D7S M133-030-20
h reporuformsdconwinrpf00100 ma 53096 4 32 pm
An Aquanon Company
Client Project Report Date
IEA Client ID
Xl G3S
G4S ^
H4S ^
4 H5S
H6S
16 H7S
7 J1S
8 J2S
9 J3S
lo J4S
fl B4S
12 B3S
^3 CSS
bull C6S
j15 C7S
Mykrowaters 9508 132 MA RBLEHEAD 053096
Parameter
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
IEA Laboratory Results
IEA ID M133-030 Received 051696
Date Results Units PQL Analyzed Analyst Method
7330 mgkg (dry) 10 052196 JB 6010
1270 mgkg (dry) 10 052196 JB 6010
89 mgkg (dry) 10 052196 JB 6010
36 mgkg (dry) 10 052196 JB 6010
60 mgkg (dry) 10 052196 JB 6010
126 mgkg (dry) 10 052196 JB 6010
53 mgkg (dry) 10 052196 JB 6010
58 mgkg (dry) 10 052196 JB 6010
68 mgkg (dry) 10 052196 JB 6010
63 mgkg (dry) 10 052196 JB 6010
^
123 mgkg (dry) 10 052196 JB 6010
10 mgkg (dry) 10 052196 JB 6010
44 mgkg (dry) 10 052196 JB 6010
286 mgkg (dry) 10 052196 JB 6010
385 mgkg (dry) 10 052196 JB 6010
h eportsforrnsdconwinrpf 10000ma Page 1 of 2 r - 053096 162 ]
ajIEAAn Aquanon Company
Client Mykrowaters Project 9508132 MARBLEHEAD Report Date 053096
IEA Client ID Parameter
TOTAL METALS 16 CSS Lead
TOTAL METALS D4S Lead
TOTAL METALS D5S Lead
TOTAL METALS
x 9 D6S Lead
TOTAL METALS D7S Lead
IEA Laboratory Results
Results Units
175 mgkg(dry)
598 mgkg(dry)
733 mgkg(dry)
260 mgkg(dry)
17 mgkg(dry)
Date PQL Analyzed
10 052196
10 052196
10 052196
10 052196
10 052196
IEA ID M133-030 Received 051696
Analyst Method
JB 6010
JB 6010
JB 6010
JB 6010
JB 6010
Comments PQL = Practical quantitation limit BQL = Below quantitation l imi t
reponsforms^dconwmrpf 10000 ma Page 2 of 2 053090 16 23
UJ
05
UJ
IEA An Aquanon Company
Definitions of Data Qualifiers and Terminology
A number of data qualifiers are widely used within the environmental testing industry and may be utilized in our data reports The following definitions of these qualifiers are included as a service to our clientele The majority of the qualifiers have evolved from the EPA contract laboratory program (CLP)
B - This flag is used when the analyte is found in the associated blank as well as in the sample It indicates possibleprobable blank contamination and warns the data user to use caution when applying the results of this analyte
BQL - Below Quantitation Limit indicates the compound was not detected in the sample above the practical quanmation limit
D - Indicates the compound was diluted below the calibration range
E - Indicates that the concentration of the specific compound exceeded the calibration range of the instrument for that particular analysis
J - Indicates an estimated value The compound is determined to be present in the sample based on GCMS criteria but the amount is less than the sample quantitation limit IEA - MA GCMS reports do not typically report J - marked results If requested J - marked results are provided and the report flagged to verify that the data was appropriately reviewed
MDL - The method detection limit is defined as the minimum concentration of a substance that can be measured and reported with 99 confidence that the analyte concentration is greater than zero
NA - Not applicable or not available
ND - Indicates the compound or analyte was not detected in the sample above the method detection limit or the practical quantitanon limit for the particular analysis
PQL - The practical quantitation limit is the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine operating conditions
h reportstorms d^
PIEA An Aquarion Company
Analytical Methodology
IEA utilizes approved environmental methodologies whenever possible and appropriate Due to the varying nature of sample matrices submitted to our laboratories we utilize a wide variety of analytical methodologies and quality assurance protocols Analytical results and Quality Assurance protocols employed by our network laboratories are based on guidelines specified in the following documents
(1) Methods of Organic Chemical Analysis of Municipal and Industrial Wastewater Federal Register Vol 49 No 209 October 26 1984
(2) Test Methods for Evaluating Solid Waste SW-846 Third Edition September 1986 USEPA
(3) Standard Methods for the Examination of Water and Wastewater 1985 14th15th and 16lh Edition
(4) Methods for Chemical Analysis of Water and Wastes March 1983 EMSL EPA
(5) Manual of Analytical Methods for the Analysis of Pesticides in Humans and Environmental Samples EPA 6008-80-038 June 1980
(6) Organic Analysis Multi-media Multi-Concentration-IFB-CLP January 1991 Document Number OLMO1 2 (plus revisions)
(7) Inorganic Analysis Multi-media Multi-Concentration-IFB-CLP Document Number ILM01 0
(8) Handbook for Analytical Quality Control in Water and Wastewater Laboratories EPA-6004-79-019 March 1979
(9) National Enforcement Investigation Center Policies and Procedures Manual EPA-330978001-R Revised May 1986
(10) Manual for the Certification of Laboratories Analyzing Drinking Water April 1990 EPA5709-90008
(11) NIOSH Manual of Analytical Methods August 1994 4th Edition
h reportsformsckcmwinrpro0202 ma
bullailEA AAnn AquanoAquanon CompanyI I n Cor
State Certifications
In some instances it may be necessary for environmental data to be reported to a regulatory authority with reference to a certified laboratory For your convenience the laboratory identification numbers for the lEA-Massachusetts laboratory are provided in the following table Many states certify laboratories for specific parameters or tests within a category (eg EPA method 624 for wastewater) The information in the following table indicates the lab is certified in a general category of testing such as drinking water or wastewater analysis The laboratory should be contacted directly if parameter specific certification information is required
lEA-Massachusetts Certification Summary as of November 1993
L
State Responsible Agency Area of Certification Lab Number
Connecticut Department of Health Services General Environmental 0646
Maine Department of Human Services Drinking Water MA038
Massachusetts Department of Environmental Drinking Water MA038 Protection Wastewater
New Hampshire Department of Environmental Drinking Water C300 Services Wastewater
New York Department of Public Health Wastewater 10838
North Carolina Department of Natural Wastewater 333 Resources
Rhode Island Department of Health Chemistry A58
Virginia Department of General Services Drinking Water 00157
h reponsformsdconwmrpf00202 ma
SKETCH A-1
TYPICAL PATHWAY PLAN VIEW (see Sketch A-2 for detail)
LOAMCOMPOST BERM
STONE DUST AND SOIL AGGREGATE SUB-BASE OVER GEOTEXTILE FABRIC
bull15
m co O
CD gt o
O m O m
m -n gt CD
o
p
OO TJ O CO
co O
CD CD co m CD
73
co CD
co m
o o -o o CO
33 O
O o o co CO CO m o
O
co 7s m o
gt
2
cc LU CD
O CL
CO I
O
LU
O)
05 O O ID
O Cpound o o
O
Q_
O Q_
_ O LU CD Q LU
co
V
o poundgtN
pound 2-S bullsin _pound E gt fth 5 O
a bullsect c mdash
111J2 o
Q
eS 00
IEA Inc 149 Rangeway Road Phone 508-667-1400 North Billerica MA 01862 Fax 508 667-7871 IEA
An Aquarion Company
Ms D Farnsworth Mykrowaters 97 Lowell Road Concord MA 01742
May 30 1996
Dear Ms Famsworth
Please find enclosed the analytical results of the sample(s) received at our laboratory on May 16 1996contains sections addressing the following information at a minimum
This report
sample ID correspondence table analytical methodology analytical results
bull chain-of-custody (if applicable) bull definitions of data qualifiers and terminology
state certifications
Client Project 9508132 Client Project Name MARBLEHEAD
EEA Report Ml 33-030 Purchase Order NA
Copies of this analytical report and supporting data are maintained in our files for a minimum of 3 years unless special arrangements are made Unless specifically indicated all analytical testing was performed at the lEA-Massachusetts laboratory
We appreciate your selection of our services and welcome any questions or suggestions you may have relative to this report Please contact your customer service representative at (508) 667-1400 for any additional information Thank you for utilizing our services and we hope you will consider us for your future analytical needs
I have reviewed and approved the enclosed data for final release
Sincerely
Michael F Wheeler PhD Laboratory Director lEA-Massachusetts
MWsmb
hrcportsformsdconwinrproOlOOma 53096 4 32 pm
Monroe Schaumtxjrg Whippany Gary Connecticut Illinois New Jersey North Carolina
203 261 4458 708 7050740 201 428 8181 919677 009C
1
V An Aquarion Company
Sample ID Correspondence Table
Client Sample ED
G3S
G4S
H4S
H5S
H6S
H7S
J1S
J2S
J3S
J4S
B4S
B3S
CSS
C6S
C7S
CSS
D4S
D5S
D6S
DBA Sample ID
M133-030-01
Ml 33-030-02
M133-030-03
Ml 33-030-04
Ml 33-030-05
M 133-030-06
Ml 33-030-07
Ml 33-030-08
Ml 33 -030-09
M133-030-10
M133-030-11
M133-030-12
M133-030-13
M133-030-14
M133-030-15
M133-030-16
M133-030-17
M133-030-18
Ml 33-030- 19
h rcporuformsidconwinrpC00100 ma 53096 4 32pm
IEA n Aquarion Company
D7S M133-030-20
h reporuformsdconwinrpf00100 ma 53096 4 32 pm
An Aquanon Company
Client Project Report Date
IEA Client ID
Xl G3S
G4S ^
H4S ^
4 H5S
H6S
16 H7S
7 J1S
8 J2S
9 J3S
lo J4S
fl B4S
12 B3S
^3 CSS
bull C6S
j15 C7S
Mykrowaters 9508 132 MA RBLEHEAD 053096
Parameter
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
IEA Laboratory Results
IEA ID M133-030 Received 051696
Date Results Units PQL Analyzed Analyst Method
7330 mgkg (dry) 10 052196 JB 6010
1270 mgkg (dry) 10 052196 JB 6010
89 mgkg (dry) 10 052196 JB 6010
36 mgkg (dry) 10 052196 JB 6010
60 mgkg (dry) 10 052196 JB 6010
126 mgkg (dry) 10 052196 JB 6010
53 mgkg (dry) 10 052196 JB 6010
58 mgkg (dry) 10 052196 JB 6010
68 mgkg (dry) 10 052196 JB 6010
63 mgkg (dry) 10 052196 JB 6010
^
123 mgkg (dry) 10 052196 JB 6010
10 mgkg (dry) 10 052196 JB 6010
44 mgkg (dry) 10 052196 JB 6010
286 mgkg (dry) 10 052196 JB 6010
385 mgkg (dry) 10 052196 JB 6010
h eportsforrnsdconwinrpf 10000ma Page 1 of 2 r - 053096 162 ]
ajIEAAn Aquanon Company
Client Mykrowaters Project 9508132 MARBLEHEAD Report Date 053096
IEA Client ID Parameter
TOTAL METALS 16 CSS Lead
TOTAL METALS D4S Lead
TOTAL METALS D5S Lead
TOTAL METALS
x 9 D6S Lead
TOTAL METALS D7S Lead
IEA Laboratory Results
Results Units
175 mgkg(dry)
598 mgkg(dry)
733 mgkg(dry)
260 mgkg(dry)
17 mgkg(dry)
Date PQL Analyzed
10 052196
10 052196
10 052196
10 052196
10 052196
IEA ID M133-030 Received 051696
Analyst Method
JB 6010
JB 6010
JB 6010
JB 6010
JB 6010
Comments PQL = Practical quantitation limit BQL = Below quantitation l imi t
reponsforms^dconwmrpf 10000 ma Page 2 of 2 053090 16 23
UJ
05
UJ
IEA An Aquanon Company
Definitions of Data Qualifiers and Terminology
A number of data qualifiers are widely used within the environmental testing industry and may be utilized in our data reports The following definitions of these qualifiers are included as a service to our clientele The majority of the qualifiers have evolved from the EPA contract laboratory program (CLP)
B - This flag is used when the analyte is found in the associated blank as well as in the sample It indicates possibleprobable blank contamination and warns the data user to use caution when applying the results of this analyte
BQL - Below Quantitation Limit indicates the compound was not detected in the sample above the practical quanmation limit
D - Indicates the compound was diluted below the calibration range
E - Indicates that the concentration of the specific compound exceeded the calibration range of the instrument for that particular analysis
J - Indicates an estimated value The compound is determined to be present in the sample based on GCMS criteria but the amount is less than the sample quantitation limit IEA - MA GCMS reports do not typically report J - marked results If requested J - marked results are provided and the report flagged to verify that the data was appropriately reviewed
MDL - The method detection limit is defined as the minimum concentration of a substance that can be measured and reported with 99 confidence that the analyte concentration is greater than zero
NA - Not applicable or not available
ND - Indicates the compound or analyte was not detected in the sample above the method detection limit or the practical quantitanon limit for the particular analysis
PQL - The practical quantitation limit is the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine operating conditions
h reportstorms d^
PIEA An Aquarion Company
Analytical Methodology
IEA utilizes approved environmental methodologies whenever possible and appropriate Due to the varying nature of sample matrices submitted to our laboratories we utilize a wide variety of analytical methodologies and quality assurance protocols Analytical results and Quality Assurance protocols employed by our network laboratories are based on guidelines specified in the following documents
(1) Methods of Organic Chemical Analysis of Municipal and Industrial Wastewater Federal Register Vol 49 No 209 October 26 1984
(2) Test Methods for Evaluating Solid Waste SW-846 Third Edition September 1986 USEPA
(3) Standard Methods for the Examination of Water and Wastewater 1985 14th15th and 16lh Edition
(4) Methods for Chemical Analysis of Water and Wastes March 1983 EMSL EPA
(5) Manual of Analytical Methods for the Analysis of Pesticides in Humans and Environmental Samples EPA 6008-80-038 June 1980
(6) Organic Analysis Multi-media Multi-Concentration-IFB-CLP January 1991 Document Number OLMO1 2 (plus revisions)
(7) Inorganic Analysis Multi-media Multi-Concentration-IFB-CLP Document Number ILM01 0
(8) Handbook for Analytical Quality Control in Water and Wastewater Laboratories EPA-6004-79-019 March 1979
(9) National Enforcement Investigation Center Policies and Procedures Manual EPA-330978001-R Revised May 1986
(10) Manual for the Certification of Laboratories Analyzing Drinking Water April 1990 EPA5709-90008
(11) NIOSH Manual of Analytical Methods August 1994 4th Edition
h reportsformsckcmwinrpro0202 ma
bullailEA AAnn AquanoAquanon CompanyI I n Cor
State Certifications
In some instances it may be necessary for environmental data to be reported to a regulatory authority with reference to a certified laboratory For your convenience the laboratory identification numbers for the lEA-Massachusetts laboratory are provided in the following table Many states certify laboratories for specific parameters or tests within a category (eg EPA method 624 for wastewater) The information in the following table indicates the lab is certified in a general category of testing such as drinking water or wastewater analysis The laboratory should be contacted directly if parameter specific certification information is required
lEA-Massachusetts Certification Summary as of November 1993
L
State Responsible Agency Area of Certification Lab Number
Connecticut Department of Health Services General Environmental 0646
Maine Department of Human Services Drinking Water MA038
Massachusetts Department of Environmental Drinking Water MA038 Protection Wastewater
New Hampshire Department of Environmental Drinking Water C300 Services Wastewater
New York Department of Public Health Wastewater 10838
North Carolina Department of Natural Wastewater 333 Resources
Rhode Island Department of Health Chemistry A58
Virginia Department of General Services Drinking Water 00157
h reponsformsdconwmrpf00202 ma
SKETCH A-1
TYPICAL PATHWAY PLAN VIEW (see Sketch A-2 for detail)
LOAMCOMPOST BERM
STONE DUST AND SOIL AGGREGATE SUB-BASE OVER GEOTEXTILE FABRIC
bull15
m co O
CD gt o
O m O m
m -n gt CD
o
p
OO TJ O CO
co O
CD CD co m CD
73
co CD
co m
o o -o o CO
33 O
O o o co CO CO m o
O
co 7s m o
gt
2
cc LU CD
O CL
CO I
O
LU
O)
05 O O ID
O Cpound o o
O
Q_
O Q_
_ O LU CD Q LU
co
V
IEA Inc 149 Rangeway Road Phone 508-667-1400 North Billerica MA 01862 Fax 508 667-7871 IEA
An Aquarion Company
Ms D Farnsworth Mykrowaters 97 Lowell Road Concord MA 01742
May 30 1996
Dear Ms Famsworth
Please find enclosed the analytical results of the sample(s) received at our laboratory on May 16 1996contains sections addressing the following information at a minimum
This report
sample ID correspondence table analytical methodology analytical results
bull chain-of-custody (if applicable) bull definitions of data qualifiers and terminology
state certifications
Client Project 9508132 Client Project Name MARBLEHEAD
EEA Report Ml 33-030 Purchase Order NA
Copies of this analytical report and supporting data are maintained in our files for a minimum of 3 years unless special arrangements are made Unless specifically indicated all analytical testing was performed at the lEA-Massachusetts laboratory
We appreciate your selection of our services and welcome any questions or suggestions you may have relative to this report Please contact your customer service representative at (508) 667-1400 for any additional information Thank you for utilizing our services and we hope you will consider us for your future analytical needs
I have reviewed and approved the enclosed data for final release
Sincerely
Michael F Wheeler PhD Laboratory Director lEA-Massachusetts
MWsmb
hrcportsformsdconwinrproOlOOma 53096 4 32 pm
Monroe Schaumtxjrg Whippany Gary Connecticut Illinois New Jersey North Carolina
203 261 4458 708 7050740 201 428 8181 919677 009C
1
V An Aquarion Company
Sample ID Correspondence Table
Client Sample ED
G3S
G4S
H4S
H5S
H6S
H7S
J1S
J2S
J3S
J4S
B4S
B3S
CSS
C6S
C7S
CSS
D4S
D5S
D6S
DBA Sample ID
M133-030-01
Ml 33-030-02
M133-030-03
Ml 33-030-04
Ml 33-030-05
M 133-030-06
Ml 33-030-07
Ml 33-030-08
Ml 33 -030-09
M133-030-10
M133-030-11
M133-030-12
M133-030-13
M133-030-14
M133-030-15
M133-030-16
M133-030-17
M133-030-18
Ml 33-030- 19
h rcporuformsidconwinrpC00100 ma 53096 4 32pm
IEA n Aquarion Company
D7S M133-030-20
h reporuformsdconwinrpf00100 ma 53096 4 32 pm
An Aquanon Company
Client Project Report Date
IEA Client ID
Xl G3S
G4S ^
H4S ^
4 H5S
H6S
16 H7S
7 J1S
8 J2S
9 J3S
lo J4S
fl B4S
12 B3S
^3 CSS
bull C6S
j15 C7S
Mykrowaters 9508 132 MA RBLEHEAD 053096
Parameter
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
IEA Laboratory Results
IEA ID M133-030 Received 051696
Date Results Units PQL Analyzed Analyst Method
7330 mgkg (dry) 10 052196 JB 6010
1270 mgkg (dry) 10 052196 JB 6010
89 mgkg (dry) 10 052196 JB 6010
36 mgkg (dry) 10 052196 JB 6010
60 mgkg (dry) 10 052196 JB 6010
126 mgkg (dry) 10 052196 JB 6010
53 mgkg (dry) 10 052196 JB 6010
58 mgkg (dry) 10 052196 JB 6010
68 mgkg (dry) 10 052196 JB 6010
63 mgkg (dry) 10 052196 JB 6010
^
123 mgkg (dry) 10 052196 JB 6010
10 mgkg (dry) 10 052196 JB 6010
44 mgkg (dry) 10 052196 JB 6010
286 mgkg (dry) 10 052196 JB 6010
385 mgkg (dry) 10 052196 JB 6010
h eportsforrnsdconwinrpf 10000ma Page 1 of 2 r - 053096 162 ]
ajIEAAn Aquanon Company
Client Mykrowaters Project 9508132 MARBLEHEAD Report Date 053096
IEA Client ID Parameter
TOTAL METALS 16 CSS Lead
TOTAL METALS D4S Lead
TOTAL METALS D5S Lead
TOTAL METALS
x 9 D6S Lead
TOTAL METALS D7S Lead
IEA Laboratory Results
Results Units
175 mgkg(dry)
598 mgkg(dry)
733 mgkg(dry)
260 mgkg(dry)
17 mgkg(dry)
Date PQL Analyzed
10 052196
10 052196
10 052196
10 052196
10 052196
IEA ID M133-030 Received 051696
Analyst Method
JB 6010
JB 6010
JB 6010
JB 6010
JB 6010
Comments PQL = Practical quantitation limit BQL = Below quantitation l imi t
reponsforms^dconwmrpf 10000 ma Page 2 of 2 053090 16 23
UJ
05
UJ
IEA An Aquanon Company
Definitions of Data Qualifiers and Terminology
A number of data qualifiers are widely used within the environmental testing industry and may be utilized in our data reports The following definitions of these qualifiers are included as a service to our clientele The majority of the qualifiers have evolved from the EPA contract laboratory program (CLP)
B - This flag is used when the analyte is found in the associated blank as well as in the sample It indicates possibleprobable blank contamination and warns the data user to use caution when applying the results of this analyte
BQL - Below Quantitation Limit indicates the compound was not detected in the sample above the practical quanmation limit
D - Indicates the compound was diluted below the calibration range
E - Indicates that the concentration of the specific compound exceeded the calibration range of the instrument for that particular analysis
J - Indicates an estimated value The compound is determined to be present in the sample based on GCMS criteria but the amount is less than the sample quantitation limit IEA - MA GCMS reports do not typically report J - marked results If requested J - marked results are provided and the report flagged to verify that the data was appropriately reviewed
MDL - The method detection limit is defined as the minimum concentration of a substance that can be measured and reported with 99 confidence that the analyte concentration is greater than zero
NA - Not applicable or not available
ND - Indicates the compound or analyte was not detected in the sample above the method detection limit or the practical quantitanon limit for the particular analysis
PQL - The practical quantitation limit is the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine operating conditions
h reportstorms d^
PIEA An Aquarion Company
Analytical Methodology
IEA utilizes approved environmental methodologies whenever possible and appropriate Due to the varying nature of sample matrices submitted to our laboratories we utilize a wide variety of analytical methodologies and quality assurance protocols Analytical results and Quality Assurance protocols employed by our network laboratories are based on guidelines specified in the following documents
(1) Methods of Organic Chemical Analysis of Municipal and Industrial Wastewater Federal Register Vol 49 No 209 October 26 1984
(2) Test Methods for Evaluating Solid Waste SW-846 Third Edition September 1986 USEPA
(3) Standard Methods for the Examination of Water and Wastewater 1985 14th15th and 16lh Edition
(4) Methods for Chemical Analysis of Water and Wastes March 1983 EMSL EPA
(5) Manual of Analytical Methods for the Analysis of Pesticides in Humans and Environmental Samples EPA 6008-80-038 June 1980
(6) Organic Analysis Multi-media Multi-Concentration-IFB-CLP January 1991 Document Number OLMO1 2 (plus revisions)
(7) Inorganic Analysis Multi-media Multi-Concentration-IFB-CLP Document Number ILM01 0
(8) Handbook for Analytical Quality Control in Water and Wastewater Laboratories EPA-6004-79-019 March 1979
(9) National Enforcement Investigation Center Policies and Procedures Manual EPA-330978001-R Revised May 1986
(10) Manual for the Certification of Laboratories Analyzing Drinking Water April 1990 EPA5709-90008
(11) NIOSH Manual of Analytical Methods August 1994 4th Edition
h reportsformsckcmwinrpro0202 ma
bullailEA AAnn AquanoAquanon CompanyI I n Cor
State Certifications
In some instances it may be necessary for environmental data to be reported to a regulatory authority with reference to a certified laboratory For your convenience the laboratory identification numbers for the lEA-Massachusetts laboratory are provided in the following table Many states certify laboratories for specific parameters or tests within a category (eg EPA method 624 for wastewater) The information in the following table indicates the lab is certified in a general category of testing such as drinking water or wastewater analysis The laboratory should be contacted directly if parameter specific certification information is required
lEA-Massachusetts Certification Summary as of November 1993
L
State Responsible Agency Area of Certification Lab Number
Connecticut Department of Health Services General Environmental 0646
Maine Department of Human Services Drinking Water MA038
Massachusetts Department of Environmental Drinking Water MA038 Protection Wastewater
New Hampshire Department of Environmental Drinking Water C300 Services Wastewater
New York Department of Public Health Wastewater 10838
North Carolina Department of Natural Wastewater 333 Resources
Rhode Island Department of Health Chemistry A58
Virginia Department of General Services Drinking Water 00157
h reponsformsdconwmrpf00202 ma
SKETCH A-1
TYPICAL PATHWAY PLAN VIEW (see Sketch A-2 for detail)
LOAMCOMPOST BERM
STONE DUST AND SOIL AGGREGATE SUB-BASE OVER GEOTEXTILE FABRIC
bull15
m co O
CD gt o
O m O m
m -n gt CD
o
p
OO TJ O CO
co O
CD CD co m CD
73
co CD
co m
o o -o o CO
33 O
O o o co CO CO m o
O
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gt
2
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O CL
CO I
O
LU
O)
05 O O ID
O Cpound o o
O
Q_
O Q_
_ O LU CD Q LU
co
V
V An Aquarion Company
Sample ID Correspondence Table
Client Sample ED
G3S
G4S
H4S
H5S
H6S
H7S
J1S
J2S
J3S
J4S
B4S
B3S
CSS
C6S
C7S
CSS
D4S
D5S
D6S
DBA Sample ID
M133-030-01
Ml 33-030-02
M133-030-03
Ml 33-030-04
Ml 33-030-05
M 133-030-06
Ml 33-030-07
Ml 33-030-08
Ml 33 -030-09
M133-030-10
M133-030-11
M133-030-12
M133-030-13
M133-030-14
M133-030-15
M133-030-16
M133-030-17
M133-030-18
Ml 33-030- 19
h rcporuformsidconwinrpC00100 ma 53096 4 32pm
IEA n Aquarion Company
D7S M133-030-20
h reporuformsdconwinrpf00100 ma 53096 4 32 pm
An Aquanon Company
Client Project Report Date
IEA Client ID
Xl G3S
G4S ^
H4S ^
4 H5S
H6S
16 H7S
7 J1S
8 J2S
9 J3S
lo J4S
fl B4S
12 B3S
^3 CSS
bull C6S
j15 C7S
Mykrowaters 9508 132 MA RBLEHEAD 053096
Parameter
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
IEA Laboratory Results
IEA ID M133-030 Received 051696
Date Results Units PQL Analyzed Analyst Method
7330 mgkg (dry) 10 052196 JB 6010
1270 mgkg (dry) 10 052196 JB 6010
89 mgkg (dry) 10 052196 JB 6010
36 mgkg (dry) 10 052196 JB 6010
60 mgkg (dry) 10 052196 JB 6010
126 mgkg (dry) 10 052196 JB 6010
53 mgkg (dry) 10 052196 JB 6010
58 mgkg (dry) 10 052196 JB 6010
68 mgkg (dry) 10 052196 JB 6010
63 mgkg (dry) 10 052196 JB 6010
^
123 mgkg (dry) 10 052196 JB 6010
10 mgkg (dry) 10 052196 JB 6010
44 mgkg (dry) 10 052196 JB 6010
286 mgkg (dry) 10 052196 JB 6010
385 mgkg (dry) 10 052196 JB 6010
h eportsforrnsdconwinrpf 10000ma Page 1 of 2 r - 053096 162 ]
ajIEAAn Aquanon Company
Client Mykrowaters Project 9508132 MARBLEHEAD Report Date 053096
IEA Client ID Parameter
TOTAL METALS 16 CSS Lead
TOTAL METALS D4S Lead
TOTAL METALS D5S Lead
TOTAL METALS
x 9 D6S Lead
TOTAL METALS D7S Lead
IEA Laboratory Results
Results Units
175 mgkg(dry)
598 mgkg(dry)
733 mgkg(dry)
260 mgkg(dry)
17 mgkg(dry)
Date PQL Analyzed
10 052196
10 052196
10 052196
10 052196
10 052196
IEA ID M133-030 Received 051696
Analyst Method
JB 6010
JB 6010
JB 6010
JB 6010
JB 6010
Comments PQL = Practical quantitation limit BQL = Below quantitation l imi t
reponsforms^dconwmrpf 10000 ma Page 2 of 2 053090 16 23
UJ
05
UJ
IEA An Aquanon Company
Definitions of Data Qualifiers and Terminology
A number of data qualifiers are widely used within the environmental testing industry and may be utilized in our data reports The following definitions of these qualifiers are included as a service to our clientele The majority of the qualifiers have evolved from the EPA contract laboratory program (CLP)
B - This flag is used when the analyte is found in the associated blank as well as in the sample It indicates possibleprobable blank contamination and warns the data user to use caution when applying the results of this analyte
BQL - Below Quantitation Limit indicates the compound was not detected in the sample above the practical quanmation limit
D - Indicates the compound was diluted below the calibration range
E - Indicates that the concentration of the specific compound exceeded the calibration range of the instrument for that particular analysis
J - Indicates an estimated value The compound is determined to be present in the sample based on GCMS criteria but the amount is less than the sample quantitation limit IEA - MA GCMS reports do not typically report J - marked results If requested J - marked results are provided and the report flagged to verify that the data was appropriately reviewed
MDL - The method detection limit is defined as the minimum concentration of a substance that can be measured and reported with 99 confidence that the analyte concentration is greater than zero
NA - Not applicable or not available
ND - Indicates the compound or analyte was not detected in the sample above the method detection limit or the practical quantitanon limit for the particular analysis
PQL - The practical quantitation limit is the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine operating conditions
h reportstorms d^
PIEA An Aquarion Company
Analytical Methodology
IEA utilizes approved environmental methodologies whenever possible and appropriate Due to the varying nature of sample matrices submitted to our laboratories we utilize a wide variety of analytical methodologies and quality assurance protocols Analytical results and Quality Assurance protocols employed by our network laboratories are based on guidelines specified in the following documents
(1) Methods of Organic Chemical Analysis of Municipal and Industrial Wastewater Federal Register Vol 49 No 209 October 26 1984
(2) Test Methods for Evaluating Solid Waste SW-846 Third Edition September 1986 USEPA
(3) Standard Methods for the Examination of Water and Wastewater 1985 14th15th and 16lh Edition
(4) Methods for Chemical Analysis of Water and Wastes March 1983 EMSL EPA
(5) Manual of Analytical Methods for the Analysis of Pesticides in Humans and Environmental Samples EPA 6008-80-038 June 1980
(6) Organic Analysis Multi-media Multi-Concentration-IFB-CLP January 1991 Document Number OLMO1 2 (plus revisions)
(7) Inorganic Analysis Multi-media Multi-Concentration-IFB-CLP Document Number ILM01 0
(8) Handbook for Analytical Quality Control in Water and Wastewater Laboratories EPA-6004-79-019 March 1979
(9) National Enforcement Investigation Center Policies and Procedures Manual EPA-330978001-R Revised May 1986
(10) Manual for the Certification of Laboratories Analyzing Drinking Water April 1990 EPA5709-90008
(11) NIOSH Manual of Analytical Methods August 1994 4th Edition
h reportsformsckcmwinrpro0202 ma
bullailEA AAnn AquanoAquanon CompanyI I n Cor
State Certifications
In some instances it may be necessary for environmental data to be reported to a regulatory authority with reference to a certified laboratory For your convenience the laboratory identification numbers for the lEA-Massachusetts laboratory are provided in the following table Many states certify laboratories for specific parameters or tests within a category (eg EPA method 624 for wastewater) The information in the following table indicates the lab is certified in a general category of testing such as drinking water or wastewater analysis The laboratory should be contacted directly if parameter specific certification information is required
lEA-Massachusetts Certification Summary as of November 1993
L
State Responsible Agency Area of Certification Lab Number
Connecticut Department of Health Services General Environmental 0646
Maine Department of Human Services Drinking Water MA038
Massachusetts Department of Environmental Drinking Water MA038 Protection Wastewater
New Hampshire Department of Environmental Drinking Water C300 Services Wastewater
New York Department of Public Health Wastewater 10838
North Carolina Department of Natural Wastewater 333 Resources
Rhode Island Department of Health Chemistry A58
Virginia Department of General Services Drinking Water 00157
h reponsformsdconwmrpf00202 ma
SKETCH A-1
TYPICAL PATHWAY PLAN VIEW (see Sketch A-2 for detail)
LOAMCOMPOST BERM
STONE DUST AND SOIL AGGREGATE SUB-BASE OVER GEOTEXTILE FABRIC
bull15
m co O
CD gt o
O m O m
m -n gt CD
o
p
OO TJ O CO
co O
CD CD co m CD
73
co CD
co m
o o -o o CO
33 O
O o o co CO CO m o
O
co 7s m o
gt
2
cc LU CD
O CL
CO I
O
LU
O)
05 O O ID
O Cpound o o
O
Q_
O Q_
_ O LU CD Q LU
co
V
IEA n Aquarion Company
D7S M133-030-20
h reporuformsdconwinrpf00100 ma 53096 4 32 pm
An Aquanon Company
Client Project Report Date
IEA Client ID
Xl G3S
G4S ^
H4S ^
4 H5S
H6S
16 H7S
7 J1S
8 J2S
9 J3S
lo J4S
fl B4S
12 B3S
^3 CSS
bull C6S
j15 C7S
Mykrowaters 9508 132 MA RBLEHEAD 053096
Parameter
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
IEA Laboratory Results
IEA ID M133-030 Received 051696
Date Results Units PQL Analyzed Analyst Method
7330 mgkg (dry) 10 052196 JB 6010
1270 mgkg (dry) 10 052196 JB 6010
89 mgkg (dry) 10 052196 JB 6010
36 mgkg (dry) 10 052196 JB 6010
60 mgkg (dry) 10 052196 JB 6010
126 mgkg (dry) 10 052196 JB 6010
53 mgkg (dry) 10 052196 JB 6010
58 mgkg (dry) 10 052196 JB 6010
68 mgkg (dry) 10 052196 JB 6010
63 mgkg (dry) 10 052196 JB 6010
^
123 mgkg (dry) 10 052196 JB 6010
10 mgkg (dry) 10 052196 JB 6010
44 mgkg (dry) 10 052196 JB 6010
286 mgkg (dry) 10 052196 JB 6010
385 mgkg (dry) 10 052196 JB 6010
h eportsforrnsdconwinrpf 10000ma Page 1 of 2 r - 053096 162 ]
ajIEAAn Aquanon Company
Client Mykrowaters Project 9508132 MARBLEHEAD Report Date 053096
IEA Client ID Parameter
TOTAL METALS 16 CSS Lead
TOTAL METALS D4S Lead
TOTAL METALS D5S Lead
TOTAL METALS
x 9 D6S Lead
TOTAL METALS D7S Lead
IEA Laboratory Results
Results Units
175 mgkg(dry)
598 mgkg(dry)
733 mgkg(dry)
260 mgkg(dry)
17 mgkg(dry)
Date PQL Analyzed
10 052196
10 052196
10 052196
10 052196
10 052196
IEA ID M133-030 Received 051696
Analyst Method
JB 6010
JB 6010
JB 6010
JB 6010
JB 6010
Comments PQL = Practical quantitation limit BQL = Below quantitation l imi t
reponsforms^dconwmrpf 10000 ma Page 2 of 2 053090 16 23
UJ
05
UJ
IEA An Aquanon Company
Definitions of Data Qualifiers and Terminology
A number of data qualifiers are widely used within the environmental testing industry and may be utilized in our data reports The following definitions of these qualifiers are included as a service to our clientele The majority of the qualifiers have evolved from the EPA contract laboratory program (CLP)
B - This flag is used when the analyte is found in the associated blank as well as in the sample It indicates possibleprobable blank contamination and warns the data user to use caution when applying the results of this analyte
BQL - Below Quantitation Limit indicates the compound was not detected in the sample above the practical quanmation limit
D - Indicates the compound was diluted below the calibration range
E - Indicates that the concentration of the specific compound exceeded the calibration range of the instrument for that particular analysis
J - Indicates an estimated value The compound is determined to be present in the sample based on GCMS criteria but the amount is less than the sample quantitation limit IEA - MA GCMS reports do not typically report J - marked results If requested J - marked results are provided and the report flagged to verify that the data was appropriately reviewed
MDL - The method detection limit is defined as the minimum concentration of a substance that can be measured and reported with 99 confidence that the analyte concentration is greater than zero
NA - Not applicable or not available
ND - Indicates the compound or analyte was not detected in the sample above the method detection limit or the practical quantitanon limit for the particular analysis
PQL - The practical quantitation limit is the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine operating conditions
h reportstorms d^
PIEA An Aquarion Company
Analytical Methodology
IEA utilizes approved environmental methodologies whenever possible and appropriate Due to the varying nature of sample matrices submitted to our laboratories we utilize a wide variety of analytical methodologies and quality assurance protocols Analytical results and Quality Assurance protocols employed by our network laboratories are based on guidelines specified in the following documents
(1) Methods of Organic Chemical Analysis of Municipal and Industrial Wastewater Federal Register Vol 49 No 209 October 26 1984
(2) Test Methods for Evaluating Solid Waste SW-846 Third Edition September 1986 USEPA
(3) Standard Methods for the Examination of Water and Wastewater 1985 14th15th and 16lh Edition
(4) Methods for Chemical Analysis of Water and Wastes March 1983 EMSL EPA
(5) Manual of Analytical Methods for the Analysis of Pesticides in Humans and Environmental Samples EPA 6008-80-038 June 1980
(6) Organic Analysis Multi-media Multi-Concentration-IFB-CLP January 1991 Document Number OLMO1 2 (plus revisions)
(7) Inorganic Analysis Multi-media Multi-Concentration-IFB-CLP Document Number ILM01 0
(8) Handbook for Analytical Quality Control in Water and Wastewater Laboratories EPA-6004-79-019 March 1979
(9) National Enforcement Investigation Center Policies and Procedures Manual EPA-330978001-R Revised May 1986
(10) Manual for the Certification of Laboratories Analyzing Drinking Water April 1990 EPA5709-90008
(11) NIOSH Manual of Analytical Methods August 1994 4th Edition
h reportsformsckcmwinrpro0202 ma
bullailEA AAnn AquanoAquanon CompanyI I n Cor
State Certifications
In some instances it may be necessary for environmental data to be reported to a regulatory authority with reference to a certified laboratory For your convenience the laboratory identification numbers for the lEA-Massachusetts laboratory are provided in the following table Many states certify laboratories for specific parameters or tests within a category (eg EPA method 624 for wastewater) The information in the following table indicates the lab is certified in a general category of testing such as drinking water or wastewater analysis The laboratory should be contacted directly if parameter specific certification information is required
lEA-Massachusetts Certification Summary as of November 1993
L
State Responsible Agency Area of Certification Lab Number
Connecticut Department of Health Services General Environmental 0646
Maine Department of Human Services Drinking Water MA038
Massachusetts Department of Environmental Drinking Water MA038 Protection Wastewater
New Hampshire Department of Environmental Drinking Water C300 Services Wastewater
New York Department of Public Health Wastewater 10838
North Carolina Department of Natural Wastewater 333 Resources
Rhode Island Department of Health Chemistry A58
Virginia Department of General Services Drinking Water 00157
h reponsformsdconwmrpf00202 ma
SKETCH A-1
TYPICAL PATHWAY PLAN VIEW (see Sketch A-2 for detail)
LOAMCOMPOST BERM
STONE DUST AND SOIL AGGREGATE SUB-BASE OVER GEOTEXTILE FABRIC
bull15
m co O
CD gt o
O m O m
m -n gt CD
o
p
OO TJ O CO
co O
CD CD co m CD
73
co CD
co m
o o -o o CO
33 O
O o o co CO CO m o
O
co 7s m o
gt
2
cc LU CD
O CL
CO I
O
LU
O)
05 O O ID
O Cpound o o
O
Q_
O Q_
_ O LU CD Q LU
co
V
An Aquanon Company
Client Project Report Date
IEA Client ID
Xl G3S
G4S ^
H4S ^
4 H5S
H6S
16 H7S
7 J1S
8 J2S
9 J3S
lo J4S
fl B4S
12 B3S
^3 CSS
bull C6S
j15 C7S
Mykrowaters 9508 132 MA RBLEHEAD 053096
Parameter
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
TOTAL METALS Lead
IEA Laboratory Results
IEA ID M133-030 Received 051696
Date Results Units PQL Analyzed Analyst Method
7330 mgkg (dry) 10 052196 JB 6010
1270 mgkg (dry) 10 052196 JB 6010
89 mgkg (dry) 10 052196 JB 6010
36 mgkg (dry) 10 052196 JB 6010
60 mgkg (dry) 10 052196 JB 6010
126 mgkg (dry) 10 052196 JB 6010
53 mgkg (dry) 10 052196 JB 6010
58 mgkg (dry) 10 052196 JB 6010
68 mgkg (dry) 10 052196 JB 6010
63 mgkg (dry) 10 052196 JB 6010
^
123 mgkg (dry) 10 052196 JB 6010
10 mgkg (dry) 10 052196 JB 6010
44 mgkg (dry) 10 052196 JB 6010
286 mgkg (dry) 10 052196 JB 6010
385 mgkg (dry) 10 052196 JB 6010
h eportsforrnsdconwinrpf 10000ma Page 1 of 2 r - 053096 162 ]
ajIEAAn Aquanon Company
Client Mykrowaters Project 9508132 MARBLEHEAD Report Date 053096
IEA Client ID Parameter
TOTAL METALS 16 CSS Lead
TOTAL METALS D4S Lead
TOTAL METALS D5S Lead
TOTAL METALS
x 9 D6S Lead
TOTAL METALS D7S Lead
IEA Laboratory Results
Results Units
175 mgkg(dry)
598 mgkg(dry)
733 mgkg(dry)
260 mgkg(dry)
17 mgkg(dry)
Date PQL Analyzed
10 052196
10 052196
10 052196
10 052196
10 052196
IEA ID M133-030 Received 051696
Analyst Method
JB 6010
JB 6010
JB 6010
JB 6010
JB 6010
Comments PQL = Practical quantitation limit BQL = Below quantitation l imi t
reponsforms^dconwmrpf 10000 ma Page 2 of 2 053090 16 23
UJ
05
UJ
IEA An Aquanon Company
Definitions of Data Qualifiers and Terminology
A number of data qualifiers are widely used within the environmental testing industry and may be utilized in our data reports The following definitions of these qualifiers are included as a service to our clientele The majority of the qualifiers have evolved from the EPA contract laboratory program (CLP)
B - This flag is used when the analyte is found in the associated blank as well as in the sample It indicates possibleprobable blank contamination and warns the data user to use caution when applying the results of this analyte
BQL - Below Quantitation Limit indicates the compound was not detected in the sample above the practical quanmation limit
D - Indicates the compound was diluted below the calibration range
E - Indicates that the concentration of the specific compound exceeded the calibration range of the instrument for that particular analysis
J - Indicates an estimated value The compound is determined to be present in the sample based on GCMS criteria but the amount is less than the sample quantitation limit IEA - MA GCMS reports do not typically report J - marked results If requested J - marked results are provided and the report flagged to verify that the data was appropriately reviewed
MDL - The method detection limit is defined as the minimum concentration of a substance that can be measured and reported with 99 confidence that the analyte concentration is greater than zero
NA - Not applicable or not available
ND - Indicates the compound or analyte was not detected in the sample above the method detection limit or the practical quantitanon limit for the particular analysis
PQL - The practical quantitation limit is the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine operating conditions
h reportstorms d^
PIEA An Aquarion Company
Analytical Methodology
IEA utilizes approved environmental methodologies whenever possible and appropriate Due to the varying nature of sample matrices submitted to our laboratories we utilize a wide variety of analytical methodologies and quality assurance protocols Analytical results and Quality Assurance protocols employed by our network laboratories are based on guidelines specified in the following documents
(1) Methods of Organic Chemical Analysis of Municipal and Industrial Wastewater Federal Register Vol 49 No 209 October 26 1984
(2) Test Methods for Evaluating Solid Waste SW-846 Third Edition September 1986 USEPA
(3) Standard Methods for the Examination of Water and Wastewater 1985 14th15th and 16lh Edition
(4) Methods for Chemical Analysis of Water and Wastes March 1983 EMSL EPA
(5) Manual of Analytical Methods for the Analysis of Pesticides in Humans and Environmental Samples EPA 6008-80-038 June 1980
(6) Organic Analysis Multi-media Multi-Concentration-IFB-CLP January 1991 Document Number OLMO1 2 (plus revisions)
(7) Inorganic Analysis Multi-media Multi-Concentration-IFB-CLP Document Number ILM01 0
(8) Handbook for Analytical Quality Control in Water and Wastewater Laboratories EPA-6004-79-019 March 1979
(9) National Enforcement Investigation Center Policies and Procedures Manual EPA-330978001-R Revised May 1986
(10) Manual for the Certification of Laboratories Analyzing Drinking Water April 1990 EPA5709-90008
(11) NIOSH Manual of Analytical Methods August 1994 4th Edition
h reportsformsckcmwinrpro0202 ma
bullailEA AAnn AquanoAquanon CompanyI I n Cor
State Certifications
In some instances it may be necessary for environmental data to be reported to a regulatory authority with reference to a certified laboratory For your convenience the laboratory identification numbers for the lEA-Massachusetts laboratory are provided in the following table Many states certify laboratories for specific parameters or tests within a category (eg EPA method 624 for wastewater) The information in the following table indicates the lab is certified in a general category of testing such as drinking water or wastewater analysis The laboratory should be contacted directly if parameter specific certification information is required
lEA-Massachusetts Certification Summary as of November 1993
L
State Responsible Agency Area of Certification Lab Number
Connecticut Department of Health Services General Environmental 0646
Maine Department of Human Services Drinking Water MA038
Massachusetts Department of Environmental Drinking Water MA038 Protection Wastewater
New Hampshire Department of Environmental Drinking Water C300 Services Wastewater
New York Department of Public Health Wastewater 10838
North Carolina Department of Natural Wastewater 333 Resources
Rhode Island Department of Health Chemistry A58
Virginia Department of General Services Drinking Water 00157
h reponsformsdconwmrpf00202 ma
SKETCH A-1
TYPICAL PATHWAY PLAN VIEW (see Sketch A-2 for detail)
LOAMCOMPOST BERM
STONE DUST AND SOIL AGGREGATE SUB-BASE OVER GEOTEXTILE FABRIC
bull15
m co O
CD gt o
O m O m
m -n gt CD
o
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co O
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73
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ajIEAAn Aquanon Company
Client Mykrowaters Project 9508132 MARBLEHEAD Report Date 053096
IEA Client ID Parameter
TOTAL METALS 16 CSS Lead
TOTAL METALS D4S Lead
TOTAL METALS D5S Lead
TOTAL METALS
x 9 D6S Lead
TOTAL METALS D7S Lead
IEA Laboratory Results
Results Units
175 mgkg(dry)
598 mgkg(dry)
733 mgkg(dry)
260 mgkg(dry)
17 mgkg(dry)
Date PQL Analyzed
10 052196
10 052196
10 052196
10 052196
10 052196
IEA ID M133-030 Received 051696
Analyst Method
JB 6010
JB 6010
JB 6010
JB 6010
JB 6010
Comments PQL = Practical quantitation limit BQL = Below quantitation l imi t
reponsforms^dconwmrpf 10000 ma Page 2 of 2 053090 16 23
UJ
05
UJ
IEA An Aquanon Company
Definitions of Data Qualifiers and Terminology
A number of data qualifiers are widely used within the environmental testing industry and may be utilized in our data reports The following definitions of these qualifiers are included as a service to our clientele The majority of the qualifiers have evolved from the EPA contract laboratory program (CLP)
B - This flag is used when the analyte is found in the associated blank as well as in the sample It indicates possibleprobable blank contamination and warns the data user to use caution when applying the results of this analyte
BQL - Below Quantitation Limit indicates the compound was not detected in the sample above the practical quanmation limit
D - Indicates the compound was diluted below the calibration range
E - Indicates that the concentration of the specific compound exceeded the calibration range of the instrument for that particular analysis
J - Indicates an estimated value The compound is determined to be present in the sample based on GCMS criteria but the amount is less than the sample quantitation limit IEA - MA GCMS reports do not typically report J - marked results If requested J - marked results are provided and the report flagged to verify that the data was appropriately reviewed
MDL - The method detection limit is defined as the minimum concentration of a substance that can be measured and reported with 99 confidence that the analyte concentration is greater than zero
NA - Not applicable or not available
ND - Indicates the compound or analyte was not detected in the sample above the method detection limit or the practical quantitanon limit for the particular analysis
PQL - The practical quantitation limit is the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine operating conditions
h reportstorms d^
PIEA An Aquarion Company
Analytical Methodology
IEA utilizes approved environmental methodologies whenever possible and appropriate Due to the varying nature of sample matrices submitted to our laboratories we utilize a wide variety of analytical methodologies and quality assurance protocols Analytical results and Quality Assurance protocols employed by our network laboratories are based on guidelines specified in the following documents
(1) Methods of Organic Chemical Analysis of Municipal and Industrial Wastewater Federal Register Vol 49 No 209 October 26 1984
(2) Test Methods for Evaluating Solid Waste SW-846 Third Edition September 1986 USEPA
(3) Standard Methods for the Examination of Water and Wastewater 1985 14th15th and 16lh Edition
(4) Methods for Chemical Analysis of Water and Wastes March 1983 EMSL EPA
(5) Manual of Analytical Methods for the Analysis of Pesticides in Humans and Environmental Samples EPA 6008-80-038 June 1980
(6) Organic Analysis Multi-media Multi-Concentration-IFB-CLP January 1991 Document Number OLMO1 2 (plus revisions)
(7) Inorganic Analysis Multi-media Multi-Concentration-IFB-CLP Document Number ILM01 0
(8) Handbook for Analytical Quality Control in Water and Wastewater Laboratories EPA-6004-79-019 March 1979
(9) National Enforcement Investigation Center Policies and Procedures Manual EPA-330978001-R Revised May 1986
(10) Manual for the Certification of Laboratories Analyzing Drinking Water April 1990 EPA5709-90008
(11) NIOSH Manual of Analytical Methods August 1994 4th Edition
h reportsformsckcmwinrpro0202 ma
bullailEA AAnn AquanoAquanon CompanyI I n Cor
State Certifications
In some instances it may be necessary for environmental data to be reported to a regulatory authority with reference to a certified laboratory For your convenience the laboratory identification numbers for the lEA-Massachusetts laboratory are provided in the following table Many states certify laboratories for specific parameters or tests within a category (eg EPA method 624 for wastewater) The information in the following table indicates the lab is certified in a general category of testing such as drinking water or wastewater analysis The laboratory should be contacted directly if parameter specific certification information is required
lEA-Massachusetts Certification Summary as of November 1993
L
State Responsible Agency Area of Certification Lab Number
Connecticut Department of Health Services General Environmental 0646
Maine Department of Human Services Drinking Water MA038
Massachusetts Department of Environmental Drinking Water MA038 Protection Wastewater
New Hampshire Department of Environmental Drinking Water C300 Services Wastewater
New York Department of Public Health Wastewater 10838
North Carolina Department of Natural Wastewater 333 Resources
Rhode Island Department of Health Chemistry A58
Virginia Department of General Services Drinking Water 00157
h reponsformsdconwmrpf00202 ma
SKETCH A-1
TYPICAL PATHWAY PLAN VIEW (see Sketch A-2 for detail)
LOAMCOMPOST BERM
STONE DUST AND SOIL AGGREGATE SUB-BASE OVER GEOTEXTILE FABRIC
bull15
m co O
CD gt o
O m O m
m -n gt CD
o
p
OO TJ O CO
co O
CD CD co m CD
73
co CD
co m
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33 O
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O CL
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LU
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05 O O ID
O Cpound o o
O
Q_
O Q_
_ O LU CD Q LU
co
V
UJ
05
UJ
IEA An Aquanon Company
Definitions of Data Qualifiers and Terminology
A number of data qualifiers are widely used within the environmental testing industry and may be utilized in our data reports The following definitions of these qualifiers are included as a service to our clientele The majority of the qualifiers have evolved from the EPA contract laboratory program (CLP)
B - This flag is used when the analyte is found in the associated blank as well as in the sample It indicates possibleprobable blank contamination and warns the data user to use caution when applying the results of this analyte
BQL - Below Quantitation Limit indicates the compound was not detected in the sample above the practical quanmation limit
D - Indicates the compound was diluted below the calibration range
E - Indicates that the concentration of the specific compound exceeded the calibration range of the instrument for that particular analysis
J - Indicates an estimated value The compound is determined to be present in the sample based on GCMS criteria but the amount is less than the sample quantitation limit IEA - MA GCMS reports do not typically report J - marked results If requested J - marked results are provided and the report flagged to verify that the data was appropriately reviewed
MDL - The method detection limit is defined as the minimum concentration of a substance that can be measured and reported with 99 confidence that the analyte concentration is greater than zero
NA - Not applicable or not available
ND - Indicates the compound or analyte was not detected in the sample above the method detection limit or the practical quantitanon limit for the particular analysis
PQL - The practical quantitation limit is the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine operating conditions
h reportstorms d^
PIEA An Aquarion Company
Analytical Methodology
IEA utilizes approved environmental methodologies whenever possible and appropriate Due to the varying nature of sample matrices submitted to our laboratories we utilize a wide variety of analytical methodologies and quality assurance protocols Analytical results and Quality Assurance protocols employed by our network laboratories are based on guidelines specified in the following documents
(1) Methods of Organic Chemical Analysis of Municipal and Industrial Wastewater Federal Register Vol 49 No 209 October 26 1984
(2) Test Methods for Evaluating Solid Waste SW-846 Third Edition September 1986 USEPA
(3) Standard Methods for the Examination of Water and Wastewater 1985 14th15th and 16lh Edition
(4) Methods for Chemical Analysis of Water and Wastes March 1983 EMSL EPA
(5) Manual of Analytical Methods for the Analysis of Pesticides in Humans and Environmental Samples EPA 6008-80-038 June 1980
(6) Organic Analysis Multi-media Multi-Concentration-IFB-CLP January 1991 Document Number OLMO1 2 (plus revisions)
(7) Inorganic Analysis Multi-media Multi-Concentration-IFB-CLP Document Number ILM01 0
(8) Handbook for Analytical Quality Control in Water and Wastewater Laboratories EPA-6004-79-019 March 1979
(9) National Enforcement Investigation Center Policies and Procedures Manual EPA-330978001-R Revised May 1986
(10) Manual for the Certification of Laboratories Analyzing Drinking Water April 1990 EPA5709-90008
(11) NIOSH Manual of Analytical Methods August 1994 4th Edition
h reportsformsckcmwinrpro0202 ma
bullailEA AAnn AquanoAquanon CompanyI I n Cor
State Certifications
In some instances it may be necessary for environmental data to be reported to a regulatory authority with reference to a certified laboratory For your convenience the laboratory identification numbers for the lEA-Massachusetts laboratory are provided in the following table Many states certify laboratories for specific parameters or tests within a category (eg EPA method 624 for wastewater) The information in the following table indicates the lab is certified in a general category of testing such as drinking water or wastewater analysis The laboratory should be contacted directly if parameter specific certification information is required
lEA-Massachusetts Certification Summary as of November 1993
L
State Responsible Agency Area of Certification Lab Number
Connecticut Department of Health Services General Environmental 0646
Maine Department of Human Services Drinking Water MA038
Massachusetts Department of Environmental Drinking Water MA038 Protection Wastewater
New Hampshire Department of Environmental Drinking Water C300 Services Wastewater
New York Department of Public Health Wastewater 10838
North Carolina Department of Natural Wastewater 333 Resources
Rhode Island Department of Health Chemistry A58
Virginia Department of General Services Drinking Water 00157
h reponsformsdconwmrpf00202 ma
SKETCH A-1
TYPICAL PATHWAY PLAN VIEW (see Sketch A-2 for detail)
LOAMCOMPOST BERM
STONE DUST AND SOIL AGGREGATE SUB-BASE OVER GEOTEXTILE FABRIC
bull15
m co O
CD gt o
O m O m
m -n gt CD
o
p
OO TJ O CO
co O
CD CD co m CD
73
co CD
co m
o o -o o CO
33 O
O o o co CO CO m o
O
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O CL
CO I
O
LU
O)
05 O O ID
O Cpound o o
O
Q_
O Q_
_ O LU CD Q LU
co
V
IEA An Aquanon Company
Definitions of Data Qualifiers and Terminology
A number of data qualifiers are widely used within the environmental testing industry and may be utilized in our data reports The following definitions of these qualifiers are included as a service to our clientele The majority of the qualifiers have evolved from the EPA contract laboratory program (CLP)
B - This flag is used when the analyte is found in the associated blank as well as in the sample It indicates possibleprobable blank contamination and warns the data user to use caution when applying the results of this analyte
BQL - Below Quantitation Limit indicates the compound was not detected in the sample above the practical quanmation limit
D - Indicates the compound was diluted below the calibration range
E - Indicates that the concentration of the specific compound exceeded the calibration range of the instrument for that particular analysis
J - Indicates an estimated value The compound is determined to be present in the sample based on GCMS criteria but the amount is less than the sample quantitation limit IEA - MA GCMS reports do not typically report J - marked results If requested J - marked results are provided and the report flagged to verify that the data was appropriately reviewed
MDL - The method detection limit is defined as the minimum concentration of a substance that can be measured and reported with 99 confidence that the analyte concentration is greater than zero
NA - Not applicable or not available
ND - Indicates the compound or analyte was not detected in the sample above the method detection limit or the practical quantitanon limit for the particular analysis
PQL - The practical quantitation limit is the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine operating conditions
h reportstorms d^
PIEA An Aquarion Company
Analytical Methodology
IEA utilizes approved environmental methodologies whenever possible and appropriate Due to the varying nature of sample matrices submitted to our laboratories we utilize a wide variety of analytical methodologies and quality assurance protocols Analytical results and Quality Assurance protocols employed by our network laboratories are based on guidelines specified in the following documents
(1) Methods of Organic Chemical Analysis of Municipal and Industrial Wastewater Federal Register Vol 49 No 209 October 26 1984
(2) Test Methods for Evaluating Solid Waste SW-846 Third Edition September 1986 USEPA
(3) Standard Methods for the Examination of Water and Wastewater 1985 14th15th and 16lh Edition
(4) Methods for Chemical Analysis of Water and Wastes March 1983 EMSL EPA
(5) Manual of Analytical Methods for the Analysis of Pesticides in Humans and Environmental Samples EPA 6008-80-038 June 1980
(6) Organic Analysis Multi-media Multi-Concentration-IFB-CLP January 1991 Document Number OLMO1 2 (plus revisions)
(7) Inorganic Analysis Multi-media Multi-Concentration-IFB-CLP Document Number ILM01 0
(8) Handbook for Analytical Quality Control in Water and Wastewater Laboratories EPA-6004-79-019 March 1979
(9) National Enforcement Investigation Center Policies and Procedures Manual EPA-330978001-R Revised May 1986
(10) Manual for the Certification of Laboratories Analyzing Drinking Water April 1990 EPA5709-90008
(11) NIOSH Manual of Analytical Methods August 1994 4th Edition
h reportsformsckcmwinrpro0202 ma
bullailEA AAnn AquanoAquanon CompanyI I n Cor
State Certifications
In some instances it may be necessary for environmental data to be reported to a regulatory authority with reference to a certified laboratory For your convenience the laboratory identification numbers for the lEA-Massachusetts laboratory are provided in the following table Many states certify laboratories for specific parameters or tests within a category (eg EPA method 624 for wastewater) The information in the following table indicates the lab is certified in a general category of testing such as drinking water or wastewater analysis The laboratory should be contacted directly if parameter specific certification information is required
lEA-Massachusetts Certification Summary as of November 1993
L
State Responsible Agency Area of Certification Lab Number
Connecticut Department of Health Services General Environmental 0646
Maine Department of Human Services Drinking Water MA038
Massachusetts Department of Environmental Drinking Water MA038 Protection Wastewater
New Hampshire Department of Environmental Drinking Water C300 Services Wastewater
New York Department of Public Health Wastewater 10838
North Carolina Department of Natural Wastewater 333 Resources
Rhode Island Department of Health Chemistry A58
Virginia Department of General Services Drinking Water 00157
h reponsformsdconwmrpf00202 ma
SKETCH A-1
TYPICAL PATHWAY PLAN VIEW (see Sketch A-2 for detail)
LOAMCOMPOST BERM
STONE DUST AND SOIL AGGREGATE SUB-BASE OVER GEOTEXTILE FABRIC
bull15
m co O
CD gt o
O m O m
m -n gt CD
o
p
OO TJ O CO
co O
CD CD co m CD
73
co CD
co m
o o -o o CO
33 O
O o o co CO CO m o
O
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O CL
CO I
O
LU
O)
05 O O ID
O Cpound o o
O
Q_
O Q_
_ O LU CD Q LU
co
V
PIEA An Aquarion Company
Analytical Methodology
IEA utilizes approved environmental methodologies whenever possible and appropriate Due to the varying nature of sample matrices submitted to our laboratories we utilize a wide variety of analytical methodologies and quality assurance protocols Analytical results and Quality Assurance protocols employed by our network laboratories are based on guidelines specified in the following documents
(1) Methods of Organic Chemical Analysis of Municipal and Industrial Wastewater Federal Register Vol 49 No 209 October 26 1984
(2) Test Methods for Evaluating Solid Waste SW-846 Third Edition September 1986 USEPA
(3) Standard Methods for the Examination of Water and Wastewater 1985 14th15th and 16lh Edition
(4) Methods for Chemical Analysis of Water and Wastes March 1983 EMSL EPA
(5) Manual of Analytical Methods for the Analysis of Pesticides in Humans and Environmental Samples EPA 6008-80-038 June 1980
(6) Organic Analysis Multi-media Multi-Concentration-IFB-CLP January 1991 Document Number OLMO1 2 (plus revisions)
(7) Inorganic Analysis Multi-media Multi-Concentration-IFB-CLP Document Number ILM01 0
(8) Handbook for Analytical Quality Control in Water and Wastewater Laboratories EPA-6004-79-019 March 1979
(9) National Enforcement Investigation Center Policies and Procedures Manual EPA-330978001-R Revised May 1986
(10) Manual for the Certification of Laboratories Analyzing Drinking Water April 1990 EPA5709-90008
(11) NIOSH Manual of Analytical Methods August 1994 4th Edition
h reportsformsckcmwinrpro0202 ma
bullailEA AAnn AquanoAquanon CompanyI I n Cor
State Certifications
In some instances it may be necessary for environmental data to be reported to a regulatory authority with reference to a certified laboratory For your convenience the laboratory identification numbers for the lEA-Massachusetts laboratory are provided in the following table Many states certify laboratories for specific parameters or tests within a category (eg EPA method 624 for wastewater) The information in the following table indicates the lab is certified in a general category of testing such as drinking water or wastewater analysis The laboratory should be contacted directly if parameter specific certification information is required
lEA-Massachusetts Certification Summary as of November 1993
L
State Responsible Agency Area of Certification Lab Number
Connecticut Department of Health Services General Environmental 0646
Maine Department of Human Services Drinking Water MA038
Massachusetts Department of Environmental Drinking Water MA038 Protection Wastewater
New Hampshire Department of Environmental Drinking Water C300 Services Wastewater
New York Department of Public Health Wastewater 10838
North Carolina Department of Natural Wastewater 333 Resources
Rhode Island Department of Health Chemistry A58
Virginia Department of General Services Drinking Water 00157
h reponsformsdconwmrpf00202 ma
SKETCH A-1
TYPICAL PATHWAY PLAN VIEW (see Sketch A-2 for detail)
LOAMCOMPOST BERM
STONE DUST AND SOIL AGGREGATE SUB-BASE OVER GEOTEXTILE FABRIC
bull15
m co O
CD gt o
O m O m
m -n gt CD
o
p
OO TJ O CO
co O
CD CD co m CD
73
co CD
co m
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33 O
O o o co CO CO m o
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LU
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05 O O ID
O Cpound o o
O
Q_
O Q_
_ O LU CD Q LU
co
V
bullailEA AAnn AquanoAquanon CompanyI I n Cor
State Certifications
In some instances it may be necessary for environmental data to be reported to a regulatory authority with reference to a certified laboratory For your convenience the laboratory identification numbers for the lEA-Massachusetts laboratory are provided in the following table Many states certify laboratories for specific parameters or tests within a category (eg EPA method 624 for wastewater) The information in the following table indicates the lab is certified in a general category of testing such as drinking water or wastewater analysis The laboratory should be contacted directly if parameter specific certification information is required
lEA-Massachusetts Certification Summary as of November 1993
L
State Responsible Agency Area of Certification Lab Number
Connecticut Department of Health Services General Environmental 0646
Maine Department of Human Services Drinking Water MA038
Massachusetts Department of Environmental Drinking Water MA038 Protection Wastewater
New Hampshire Department of Environmental Drinking Water C300 Services Wastewater
New York Department of Public Health Wastewater 10838
North Carolina Department of Natural Wastewater 333 Resources
Rhode Island Department of Health Chemistry A58
Virginia Department of General Services Drinking Water 00157
h reponsformsdconwmrpf00202 ma
SKETCH A-1
TYPICAL PATHWAY PLAN VIEW (see Sketch A-2 for detail)
LOAMCOMPOST BERM
STONE DUST AND SOIL AGGREGATE SUB-BASE OVER GEOTEXTILE FABRIC
bull15
m co O
CD gt o
O m O m
m -n gt CD
o
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CD CD co m CD
73
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SKETCH A-1
TYPICAL PATHWAY PLAN VIEW (see Sketch A-2 for detail)
LOAMCOMPOST BERM
STONE DUST AND SOIL AGGREGATE SUB-BASE OVER GEOTEXTILE FABRIC
bull15
m co O
CD gt o
O m O m
m -n gt CD
o
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73
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