Environmental - Schneider Laboratories Global, Inc...SCHNEIDER LABORATORIES GLOBAL, INCORPORATED 2512 W. Cary Street, Richmond, VA 23220-5117 Tel: 804-353-6778 Toll Free: 800-785-LABS

SCHNEIDER LABORATORIES GLOBAL, INCORPORATED 2512 W. Cary Street, Richmond, VA 23220-5117

Tel: 804-353-6778 Toll Free: 800-785-LABS (5227) FAX: 804-359-1475 www.slabinc.com [email protected]

Desk Reference Guide

Environmental

2018

Methods (media and testing) subject to change Call Customer Services for Pricing

mailto:[email protected]

Table of Contents

Letter from the President

Statement of Qualifications

Overall Scope of Services

Testing Policies

Quality, Convenience and Service

Abbreviations

Desk Reference Guide

Metals Analyses

Hazardous Waste Characterization

Drinking Water Profiles

Environmental Tests by Analyte

Holding Times

Sampling Media

Appendices

Semi Volatile Parameters A

Volatile Parameters B

PCB, Pesticide & Herbicide Parameters C

Regulatory Limits D

Customer Information Forms and Credit Application E

COC’s, Sample Acceptance Policy & Supply Request Form F

Accreditations G

Test Kits H


Tel: 804-353-6778 Toll Free: 800-785-LABS (5227) FAX: 804-359-1475 www.slabinc.com [email protected]

From the President Dear Valued Customer: Thank you for allowing us to provide you with our Desk Reference Guide. Schneider Laboratories Global, Inc. (SLGi) is immensely pleased to inform you of the testing capabilities we offer to service your industrial hygiene and environmental needs. SLGi is nationally and internationally recognized through many accrediting agencies. National accreditations held by SLGi are the American Industrial Hygiene Association (AIHA), the National Voluntary Laboratory Accreditation Program (NVLAP) and the National Environmental Laboratory Accreditation Program through Virginia (VELAP). SLGi also holds several state accreditations such as California, Kansas, New York, New Jersey, North Carolina, South Carolina, Pennsylvania and many other states. Schneider Laboratories Global, Inc. specializes in the analysis of organic compounds, asbestos, mold, Total Coliform and E.coli bacteria, lead and other metals in various matrices such as air, paint, soil, wipes, building materials, hazardous wastes, wastewater, drinking water and product testing. SLGi is dedicated to serving the testing needs of occupational environmental health and safety professionals worldwide. The hallmark of SLGi’s success has been the ability to create partnerships with our customers to provide accurate laboratory analysis at competitive prices, with no extra charge for weekend analysis. With continuous growth and expansions in our services, we are confident to say that we have the knowledge, skill and ability to meet the needs of our current and future customers. If you have any questions, please do not hesitate to call us at 1-800-785-5227. Thank you, again! Sincerely,

Najwa Abouzaki President/CEO


Statement of Qualifications

Schneider Laboratories Global, Inc. specializes in the analyses of metals, organic compounds, asbestos and mold in various matrices including air, paint, soil, wipes, building materials, wastewater, drinking water and hazardous wastes. SLGi is an independent, AIHA (ISO-17025)/ NVLAP /VELAP accredited commercial analytical testing laboratory located in Richmond, VA. The laboratory is dedicated to serving the testing needs of occupational/environmental health and safety professionals worldwide. The hallmark of SLGi's success has been our ability to create partnerships with customers to provide accurate laboratory analysis at competitive prices. SLGi provides the security, instrumentation and storage to efficiently and reliably perform all analyses. SLGi utilizes a 20,000 square feet facility which is continually evaluated and renovated as needed to accommodate required analytical/safety requirements. Since its inception in 1987, SLGi has experienced tremendous growth in all analytical areas including Industrial Hygiene, Environmental, Lead, Asbestos and Mold and is recognized as a leader in laboratory testing. Quality Control/Quality Assurance: Schneider Laboratories Global has stringent quality control and quality assurance policies in compliance with ISO 17025, NELAC and EPA standards. SLGi has developed a comprehensive quality assurance/quality control (QA/QC) program that includes internal and external evaluations to ensure the integrity of analyses and guarantees the accuracy of analytical results. Schneider Laboratories Global employs a quality assurance and quality control director and quality control officers who maintain and implement an internal QA/QC program designed to monitor employee capabilities, reagent and standard quality and instrument performance. Internationally: SLGi assists industrial professionals, engineers, consultants and government agencies worldwide to meet the ongoing and ever changing needs for industrial hygiene, environmental, lead and asbestos testing. Nationally: SLGi was the first laboratory in the nation to receive accreditation for the analysis of lead based paint chips, soil and dust wipes through AIHA's ELLAP Program. Schneider Laboratories Global is listed in the first group of laboratories in the United States to receive NELAC accreditation. Regionally: SLGi was the first laboratory in Virginia to be licensed for asbestos analysis. Our reputation for courteous and responsive interaction with our customers is widespread.

Our documentation process is exact and complete.

Our distinction as an "AUTHORITY" in asbestos and lead testing has become globally recognized.

Overall Scope of Services

Since its inception in 1987, SLGI has experienced tremendous growth in all analytical areas including Industrial Hygiene, Environmental, Lead, Asbestos and Mold. Below is a list of the wide array of analytical testing services offered at SLGI. Asbestos Testing–

Bulk Asbestos analysis performed by Polarized Light Microscopy (PLM) using EPA Methods 600/R-93/116 and 600/M4-82-020 and New York ELAP 198.1 and/or 198.6. Airborne Asbestos analysis is performed by Phase Contrast Microscopy (PCM) using NIOSH Method 7400.

Environmental Lead Testing–

Lead in Paint, Dust and Soil by EPA 6000 and 7000 series analysis methods, Lead in surface coatings analysis by CPSC-CH-E1003-9.1 and Lead in Air by NIOSH 7082, NIOSH 7300, and NIOSH 7105 and 40 CFR 50 Appendix G methods.

Multi- Metal Testing–

Metals in Solid, Bulk and Soil Samples by EPA 3000 Series digestion Methods and by 6000 and 7000 series analysis methods; Metals in Water by both EPA 6000 Series and EPA 200 Series Methods and Metals in Air by NIOSH 7082, NIOSH 7300, and other NIOSH methods as well as OSHA ID 121. Metals testing using TCLP preparation by EPA 1311, SPLP preparation by EPA 1312 and California Waste Extraction Test (WET) Method followed by the appropriate analysis methods.

Gravimetric Testing–

Total Suspended Particulate by 40 CFR 50 Appendix B method, Total Nuisance Dust by NIOSH 0500, Total Respirable Dust by NIOSH 0600, and Carbon Black by NIOSH 5000.

Silica Testing–

Samples are analyzed by FTIR using NIOSH 7602 Method.

Mold Testing –

Air, Bulk, Tape and Swab samples are analyzed using AIHA approved In-house methods. Testing includes the identification and quantification of mold spores.

Microbiology Testing –

Drinking water samples are analyzed using NELAC approved methods. Testing includes the identification and quantification of Total Coliform and E.coli Bacteria.

Industrial Hygiene Testing-

Air Samples are analyzed by using NIOSH, OSHA and EPA Methods. Air samples can be tested for Acids, Benzene, Toluene, Xylenes, Formaldehyde, Isocyanates, Hydrogen Sulfide, Ammonia, Sulfur Dioxide, Total Petroleum Hydrocarbons as Hexane, Organic Solvent Profile and many other analytes.

Environmental Testing-

Samples are analyzed by using EPA 300 Series, EPA 600 Series, EPA 3000 Series, EPA 8000 Series Methods and Standard Methods depending on the matrix. Samples can be tested for PCBs, Volatile and Semi-Volatile Organic Compounds, Herbicides, Pesticides, Chlordane, Toxaphene, BTEX and other analytes.

Exact Methods can be found in the ‘Test by Analyte’ Section of this fee schedule

Testing Policies

Turnaround Time (TAT): Same day, 1-day, 2-day, 3-day and 5-day turn-around times are available for most analyses. Standard turn around time on most analyses is 5 business days with weekend analysis available upon advanced notification at NO additional charge. A 2-hr TAT is available for some analyses. Examples of rate increases for faster TATs are as follows:

Priority 1-Day : 100% additional charge

Priority 2-Day : 75% additional charge

Reports are available online or transmitted via fax, email, electronic deliverable (EDD)

The Full TCLP test and certain metals profiles by Graphite Furnace Atomic Absorption have a standard 10 day TAT but may be completed sooner. Any samples received after 3 PM ET are entered into the data entry system as if they were received on the next day business day. All results are reported by the end of the business day which is 6:00 pm.

Weekends: Schneider Laboratories Global offers same day turn-around on Saturday and Sunday testing (except TEMS and send-out/referral tests). Advance notice of sample arrival and are required by Friday at 3 PM ET in order to receive Saturday and Sunday results. Rush turn-around-time requests remain the same for weekends and weekdays. Turnaround time on send-out/referral tests is based on the customer needs. Call your Project Manager to get available turnaround times.

Chain of Custody (COC): Chain of custody forms are provided at no additional charge and are also available online at http://www.slabinc.com/content/resources/. Chain of custody forms should be legible and complete. Include the following information when submitting samples to the laboratory. SLGI will pre-print your COC upon request at no charge.

1. Customer name and address (if not using pre-printed form) 2. Telephone number and fax number 3. Project name/number 4. Date, time and state of sample collection 5. Certification Requirements 6. Number and types of samples 7. Type of analysis requested on each sample 8. Sample identification, including time, flow rates, volumes and areas 9. Purchase order information 10. Signature of person submitting samples 11. Sample identification numbers must be clearly marked on each sample submitted

and are necessary for cross-referencing and sample tracking throughout the laboratory. The number chosen to identify your samples should also be written on the chain of custody form submitted with the samples.

12. Indicate any special instructions

Providing this information will help eliminate delays.

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Duplicates: Enough sample quantity must be sent to the laboratory so that the laboratory can perform a duplicate sample analysis for solid and water matrices. If enough sample is received the laboratory will also perform a sample spike analysis. Blanks: Blanks act as a control for analysis by accounting for contamination that can occur during handling, storage, or shipment of samples. A field blank is opened and handled in the same manner as a sample, except in the case of industrial hygiene samples no air should be drawn. Since blanks are analyzed as any other sample in the laboratory, they are priced the same as the analysis requested. Sample Collection Media: A nominal fee will be charged for collection media. Sampling media are routinely shipped by ground delivery FedEx. If air express shipping is requested, the customer will be billed for this service. Billing: Invoicing is by sample group and payment is net 30 days. International customers are prepaid by credit card only. A line of credit can be established upon review of a customer’s credit application. Credit Cards: For your convenience, VISA, MasterCard, Discover and American Express are accepted. Warranty: All sample results are strictly confidential and will not be released to anyone other than the sample submitter without the permission of the customer. Schneider Laboratories Global cannot be responsible for loss of samples, and reserves the right to refuse samples that are not collected on the appropriate sampling medium. Schneider Laboratories Global will employ qualified personnel to analyze samples and, where possible, will use established and recognized analytical testing procedures. Schneider Laboratories Global makes no other warranties expressed or implied. QA/QC Data Packages: For your convenience the laboratory is able to supply the necessary QC package as listed below. The customer has the responsibility to notify the laboratory about the desired QC package prior to or at the time of sample receipt. Level 2 Data Package – additional 25% of the invoice total Basic QC Data:

LCS, LCSD, MS, MSD, DUP and MB

Level 3 Data Package – additional 50% of the invoice total

Calibration Data plus Basic QC data: LCS, LCSD, MS, MSD, MB, RB, ICV, CCV, CCB, Internal Standard and Retention Time Summary

Level 4 Data Package – additional 100% of the invoice total

Analytical Raw Data and Summary plus Calibration and Basic QC data:

LCS, LCSD, MS, MSD, MB, ICV, CCV, CCB, Internal Standard Summary, Retention Time Summary, Pesticide Breakdown Check and all chromatograms, daily instrument checks, sample prep and standard prep logs plus a written summary of analytical results

Quality, Convenience and Service

Quality • American Industrial Hygiene Association (AIHA) accreditation – ELLAP,

IHLAP and EMLAP

• National Institute of Standards and Technology, National Voluntary Laboratory Accreditation Program (NVLAP) accredited for bulk asbestos fiber analysis

• National Lead Laboratory Accreditation Program (NLLAP)/EPA recognized for lead in paint chips, soil, and dust wipes

• National Environmental Laboratory Approval Program through Virginia (VELAP) – accredited for environmental testing in drinking water, wastewater and solid and hazardous waste

• Comprehensive quality assurance/quality control program

• Defensible data provided

Service • Standard turn-around time for testing is 5 business days from receipt of sample

• Quality control data included on chemistry reports (Upon Request)

• Toll free customer service number

• Results available online at www.slabinc.com, by email, fax, and/or EDD

• Final reports signed by approved signatories that are immediately available on our website, emailed and/or faxed to customer

• Invoice mailed with hard copy report or “Go Green” emailed

• Hard copy report mailed with original chain of custody or “Go Green” emailed or available online

• Calculated TWA’s

• NO Charge Pump and Cyclone Loan Program

No Hidden Charges • No minimum sample billing

• Chain of custody forms provided by print or email

• Printable Chain of custody forms available online at www.slabinc.com

No Conflict of Interest • Laboratory testing only . . . no field or consulting services

Payment Options • Credit Cards accepted

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Abbreviations

AG Silver Membrane Treated Filter HPLC High Performance Liquid

Chromatography

CF Cellulose Filter IC Ion Chromatography

CHROM Chromosorb Tube ICP Inductively Coupled Plasma Atomic Emission Spectrometry

COLOR Colorimetric IMP Impinger CP Cellulose Pad ISE Ion Selective Electrode CT Charcoal Tube MCE Mixed Cellulose Ester Filter CV Cold Vapor Atomic Absorption LG CT Large Charcoal Tube DNPH Dinitrophenylhydrazine LG Large

DT Drying Tube LG SGT Large Silica Gel Tube

ECD Electron Capture Detector OVS OSHA Versatile Sampler

ETOM Ethylene Oxide Passive Monitor PCM Phase Contrast Microscopy

FBT Firebrick Tube PET CT Petroleum Charcoal Tube

FID Flame Ionization Detector POVM Passive Organic Vapor Monitor

FAA Flame Atomic Absorption PLM Polarized Light Microscopy FL Flourescense PVC Polyvinyl Chloride Filter

FLR Florisil Tube P&T Purge and Trap

FPM Formaldehyde Passive Monitor PTFE Teflon Filter FPD Flame Photometric Detector SGT Silica Gel Tube

FTIR Fourier Transform Infrared Spectrophotometry SKC PM SKC Passive Monitor

GC Gas Chromatography Sp Special

GCMS Gas Chromatography Mass

Spectometry SSS Stainless Steel Screen

GFAA Graphite Furnace Atomic Absorption TEM Transmission Electron Microscopy

GFF Glass Fiber Filter TITR Titrimetric GRAV Gravimetric TR Treated GWS Glass Wool Separator UV Ultraviolet Detector

HG Hydride Generation UV/VIS Ultraviolet Visible Spectrophotometry

Method6010/200.7

7470/7471/245.1

6010/200.7

7010/200.9

7470/7471/245.1

6010/200.7

7470/7471/245.1

6010/200.7

7470/7471/245.1

6010/200.7

7470/7471/245.1

6010/7196

Individual Metal by ICP

6010/200.7 7470/7471/245.1

200.7/200.9

Metals Analyses

(As, Be, Cd, Cr, Pb, V)

6010/200.7

7000/7082 (Air)

200.7/200.9/245.1

6010/200.7 7470/7471/245.1

200.7/200.9Secondary Drinking Water

(Ag, Al, Ca, Fe, Mn, Na, Zn)

(Soil, Paint Chips, Air, Final Wipe Clearance)

Individual Metal by GFAA

Full ICP Metals 26

(Ag, Al, As, B, Ba, Be, Ca, Cd, Co, Cr, Cu, Fe, K, Mg,

Mn, Mo, Na, Ni, Pb, Sb, Se, Sn, Ti, Tl, V, Zn)

Lead (Total Concentration by FAA)

Chromium III (Based on Total Cr & CrVI calculation)

Mercury by CVAA

Primary Drinking Water

(As, Ba, Be, Cd, Cr, Cu, Hg, Ni, Pb, Sb, Se, Tl)

Priority Pollutant Metals

(Ag, As, Be, Cd, Cr, Cu, Hg, Ni, Pb, Sb, Se, Tl, Zn)

RCRA Metals (Total Concentration)

Reed Minerals 30

TAL Metals 23

(Al, Sb, As, Ba, Be, Cd, Ca, Cr, Co, Cu, Fe, Pb,

Parameter

Welding Fumes Metals

(Al, Be, Cd, Co, Cr, Cu, Fe, Mn, Mo, Ni, Pb, Sb, Ti, V, Zn)

California-17

(Ag, As, Ba, Be, Cd, Co, Cr, Cu, Hg, Mo, Ni, Pb, Sb, Se, Ti, V, Zn)

(Ag, As, Ba, Cd, Cr, Hg, Pb, Se)

Mg, Mn, Hg, Ni, K, Se, Ag, Na, Tl, V, Zn)

Toxic Metals 6 - Drinking Water

(Ag, Al, As, Ba, Be, Ca, Cd, Co, Cr, Fe, Hg, K, Mg, Mn,

Mo, Na, Ni, Pb, Rh, Sb, Se, Ta, Te, Ti, Tl, U, V, Y, Zn, Zr)

Analysis for SPLP

Analysis for TTLC

Full TCLP extraction & analysis (10 day TAT)

TCLP extraction for metals/semivolatiles/volatiles (ZHE)

PCBs

Analysis for lead only

Analysis for semivolatile compounds

Analysis for pesticides

Analysis for herbicides

Analysis for volatile compounds

Analysis for STLC

Corrosivity as pH

Subcontracted Hazardous Waste ParametersReactivity

Other Hazardous Waste Parameters

Free Liquids Test

Ignitability/Flashpoint

Hazardous Waste Characterization

Toxicity Characteristic Leaching Procedure (TCLP)Individual Tests

(See alphabetical listing for sample requirements.)

Waste may be categorized as hazardous or non-hazardous by listing of the waste type in the Federal Registeror by testing for the four characteristics of hazardous waste given below. The four characteristics of hazardouswaste are reactivity, corrosivity, ignitability, and toxicity. The toxicity characteristic is tested using the toxicitycharacteristic leaching procedure or TCLP. There are other tests that also aid in hazardous waste investigationswhich are given below.

* Includes extraction

Parameter

Extraction Procedures

TCLP Analysis *(See TCLP PARAMETERS AND REGULATORY LIMITS for a list of compounds)

Analysis for RCRA metals

30 Hour Holding Time

E. Coli Total Coliform

Collection media: 100mL Sodium Thiosulfate preserved bottle

48 Hour Holding Time

Nitrates + Nitrites

Collection media:

Arsenic Barium Beryllium CadmiumChromium Copper Mercury NickelLead Antimony Selenium Thallium

Collection media: 1L Plastic, 1:1HNO3 preserved

Silver Aluminum Calcium IronManganese Sodium Zinc


Arsenic Beryllium Cadmium ChromiumLead Vanadium


General Drinking Water Profiles

Bacteria

Toxic Metals 6 Profile

Metals - Primary Drinking Water Profile

Nitrate + Nitrites

125 ml Plastic

Metals - Secondary Drinking Water Profile

Test Name Matrix MethodAnalytical

Technique

Collection

Media

Minimum

AmountPreservative Notes

Aluminum Soil/Bulk 6010 ICP G/T 5 grams 4ºC See Metals Analyses Section.

Aluminum Water 200.7/6010 ICP P/G 125 ml HNO3 See Metals Analyses Section.

Anion Scan Soil/Bulk EPA 9056 IC P/G 50 grams 4ºCBromide, Chloride, Fluoride, Nitrate,

Nitrite, Phosphate, Sulfate

Anion Scan Water 300.0 IC P/G 125ml 4ºCBromide, Chloride, Fluoride, Nitrate,

Nitrite, Phosphate, Sulfate

Antimony Soil/Bulk 6010/7010 ICP/GFAA G/T 5 grams 4ºC

Antimony Water 6010/7010 ICP/GFAA P/G 125 ml HNO3

Asbestos BulkEPA 600/M4-82-020

EPA 600/R-93-116 PLM P 2 x 2 inch None

See Microscopy & Microbiology Fee

Schedule

Asbestos TEM Chatfield Bulk Chatfield Method TEM P 2 x 2 inch NoneSee Microscopy & Microbiology Fee

Schedule

Asbestos - Verm Vermiculite

Modified Cincinatti

Method

EPA 600/M4-82-020

PLM PSmall Ziploc

BagNone

See Microscopy & Microbiology Fee

Schedule

Arsenic Soil/Bulk 6010/7010 ICP/GFAA G/T 5 grams 4ºC

Arsenic Water200.7/200.9 or

6010/7010ICP/GFAA P/G 125 ml HNO3

Barium Soil/Bulk 6010/7010 ICP/GFAA G/T 50 grams 4ºC

Environmental Sampling Guide


Technique

Collection

Media

Minimum


Barium Water200.7/200.9 or


Beryllium Soil/Bulk 6010/7010 ICP/GFAA G/T 5 grams 4ºC

Beryllium Water200.7/200.9 or


Boron Soil/Bulk 6010 ICP G/T 5 grams 4ºC

Boron Water 200.7/6010 ICP P/G 125 ml HNO3

Bromide Soil/Bulk EPA 9056 IC P/G 50 grams None

Bromide Water 300.0 IC P/G 125 ml None

BTEX (Benzene, Toluene,

Ethylbenzene, Xylene)Soil/Bulk 8021/624/8260 GCPID/GCMS G/T 50 grams 4ºC Minimum Headspace

BTEX (Benzene, Toluene,

Ethylbenzene, Xylene)Water 8021/624/8260 GCPID/GCMS G/T 3x40 ml

HCl, 4ºC, no residual

chlorineNo Headspace In Sample Container.

BTEX And MTBE

(Methyl T-Butyl Ether)Soil/Bulk 8021/624/8260 GCPID/GCMS G/T 50 grams 4ºC Minimum Headspace

BTEX And MTBE

(Methyl T-Butyl Ether)Water 8021/624/8260 GCPID/GCMS G/T 3x40 ml


chlorineNo Headspace In Sample Container.

Cadmium Soil/Bulk 6010/7010 ICP/GFAA G/T 5 grams 4ºC

Cadmium Water200.7/200.9 or


California 17 Profile Soil/Bulk 6010/7471 ICP/CVAA G/T 5 grams 4ºC See Metals Analyses Section.

California 17 Profile Water200.7/245.1 or

6010/7470ICP/CVAA P/G 1 Liter HNO3 See Metals Analyses Section.

Calcium Soil/Bulk 6010 ICP G/T 5 grams 4ºC

Calcium Water 200.7/6010 ICP P/G 125 ml HNO3


Technique

Collection

Media

Minimum


Chloride Soil/Bulk EPA 9056 IC P/G 50 grams None

Chloride Water 300.0 IC P/G 125ml None

Chromium Soil/Bulk 6010/7010 ICP/GFAA G/T 5 grams 4ºC

Chromium Water200.7/200.9 or


Chrome III Soil/Bulk 6010 and 7196 ICP & UV/VIS

Chrome III Water 6010/200.7 and 7196 ICP & UV/VIS

Chrome IIIDrinking

Water200.9 and 7196 GFAA & UV/VIS

Chromium, Hexavalent

(Chrome VI, Cr+6)Soil/Bulk 7196 UV/VIS P/G 100 grams 4ºC

Chromium, Hexavalent

(Chrome VI, Cr+6)Water 7196 UV/VIS P/G 250 ml 4ºC

Conductance, Specific

(Conductivity)Water 120.1

Conductivity

MeterP/G 125 ml 4ºC

Copper Soil/Bulk 6010/7010 ICP/GFAA G/T 5 grams 4ºC

Copper Water200.7/200.9 or


Corrosivity (pH) Soil/Bulk 9045 pH METER P/G 50 grams 4ºC

Corrosivity (pH) Water 9045 pH METER P/G 50 ml 4ºC

Fluoride Soil/Bulk EPA 9056 IC P/G 50 grams None

Fluoride Water 300.0 IC P/G 125ml None

Free Liquids Test Soil/Bulk 9095 P/G 200 grams 4ºC

(Calculation based on anaysis of Total Cr & CrVI)




Technique

Collection

Media

Minimum


Full ICP Metals 26 Profile Soil/Bulk 6010 ICP/CVAA G/T 5 grams 4ºC See Metals Analyses Section.

Full ICP Metals 26 Profile Water 200.7 or 6010 ICP/CVAA P/G 1 Liter HNO3 See Metals Analyses Section.

Herbicides, Chlorinated Soil/Bulk 8151 GC/ECD G/T 100 grams 4ºCSee Appendix C for

list of analytes.

Herbicides, Chlorinated Water 8151 GC/ECD G/T 2x1000 ml 4ºCSee Appendix C for

list of analytes.

Iron Soil/Bulk 6010 ICP G/T 5 grams 4ºC

Iron Water 200.7/6010 ICP P/G 125 ml HNO3

Jet Fuel JP-4 Soil/Bulk 8015 GC/FID G/T 100 grams 4ºC

Jet Fuel JP-4 Water 8015 GC/FID G/T 2x1000 ml HCl optional, 4ºC

Lead Based Paint Paint 7000/6010 FAA/ICP G/T 1 gram None

Lead Soil/Bulk 7000/6010 FAA/ICP G/T 5 grams 4ºC

Lead Water 7000 or 200.7/6010 FAA/ICP P/G 125 ml HNO3

Lead (Drinking Water) Water 200.9 GFAA P 125 ml HNO3

Lead Wipe 7000 or 6010 FAA/ICP P/G -

Lithium Soil/Bulk 6010 ICP G/T 5 grams 4ºC

Lithium Water 200.7/6010 ICP P/G 125 ml HNO3

Magnesium Soil/Bulk 6010 ICP G/T 5 grams 4ºC


Technique

Collection

Media

Minimum


Magnesium Water 200.7/6010 ICP P/G 125 ml HNO3

Manganese Soil/Bulk 6010/7010 ICP/GFAA G/T 5 grams 4ºC

Manganese Water200.7/200.9 or


Mercury Soil/Bulk 7471 CVAA P/G 5 grams 4ºC

Mercury Water 245.2/7470 CVAA P/G 125 ml HNO3

Molybdenum Soil/Bulk 6010 ICP G/T 5 grams 4ºC

Molybdenum Water 200.7/6010 ICP P/G 125 ml HNO3

Naphthalene Soil/Bulk 8021/8260 GCPID/GCMS G/T 50 grams

Nickel Soil/Bulk 6010/7010 ICP/GFAA G/T 5 grams 4ºC

Nickel Water200.7/200.9 or


Nitrate Soil/Bulk EPA 9056 IC P/G 50 grams 4ºC

Nitrate Water 300.0 IC P/G 125ml 4ºC

Nitrite Soil/Bulk EPA 9056 IC P/G 50 grams 4ºC

Nitrite Water 300.0 IC P/G 125ml 4ºC

PAHs (Polynuclear Aromatic

Hydrocarbons)Soil/Bulk 8270 GCMS G/T 100 grams 4ºC

See Appendix A for

list of analytes.

PAHs (Polynuclear Aromatic

Hydrocarbons)Water 625/8270 GCMS G/T 2x1000 ml 4ºC

See Appendix A for

list of analytes.

Paint Filter Liquids Test Soil/Bulk 9095 - P/G 200 grams 4ºC


Technique

Collection

Media

Minimum


Paint Filter Liquids Test Water 9095 - P/G 250 ml 4ºC

PCBs Oil 8082 GC/ECD G/T 50 grams 4ºC

PCBs Soil/Bulk 8082 GC/ECD G/T 50 grams 4ºC

PCBs Water 608/8082 GC/ECD G/T 2x1000ml 4ºC Na2S2O3

PCBs Wipe 8082 GC/ECD G/T - 4ºC

Pesticides, Organochlorine Soil/Bulk 8081 GC/ECD G/T 100g 4ºCSee Appendix C for

list of analytes.

Pesticides, Organochlorine Water 608/8081 GC/ECD G/T 2x1000ml 4ºCSee Appendix C for

list of analytes.

Pesticides, Organochlorine Wipe 8081 GC/ECD G/T - 4ºCSee Appendix C for

list of analytes.

pH Soil/Bulk 9045 pH METER P/G 20 grams 4ºC

pH Water 9040 pH METER P/G 125 ml 4ºC

Phenols Soil/Bulk 8270 GCMS G/T 100 grams 4ºC

Phenols Water 625/8270 GCMS G/T 2x1000ml 4ºC

Phosphate Soil/Bulk EPA 9056 IC P/G 50 grams None

Phosphate Water 300.0 IC P/G 125ml None

Potassium Soil/Bulk 6010 ICP G/T 5 grams 4ºC

Potassium Water 200.7/6010 ICP P/G 125 ml HNO3

Primary Drinking Water ProfileDrinking

Water200.7/200.9 ICP/GFAA P/G 1 Liter HNO3 See Metals Analyses Section.


Technique

Collection

Media

Minimum


Priority Pollutant Metals Profile Soil/Bulk 6010 ICP G/T 5 grams 4ºC See Metals Analyses Section.

Priority Pollutant Metals Profile Water 200.7/6010 ICP P/G 1 Liter HNO3 See Metals Analyses Section.

Priority Pollutant Metals ProfileDrinking


RCRA Metals Profile Soil/Bulk 6010 ICP G/T 5 grams 4ºC See Metals Analyses Section.

RCRA Metals Profile Water 200.7/6010 ICP P/G 1 Liter HNO3 See Metals Analyses Section.

Reed Minerals 30 Profile Soil/Bulk 6010/7471 ICP/CVAA G/T 5 grams 4ºC See Metals Analyses Section.

Reed Minerals 30 Profile Water200.7/245.1 or

6010/7470ICP/CVAA P/G 1 Liter HNO3 See Metals Analyses Section.

Resistivity Soil/Bulk EPA 120.1MConductivity

MeterG/T 100 grams 4ºC

Secondary Drinking Water

Profile

Drinking


Selenium Soil/Bulk 6010/7010 ICP/GFAA G/T 5 grams 4ºC

Selenium Water200.7/200.9 or


Silica Soil/Bulk NIOSH 7602M FTIR G/T 5 grams 4ºC

Silver Soil/Bulk 6010/7010 ICP/GFAA G/T 5 grams 4ºC

Silver Water200.7/200.9 or


Sodium Soil/Bulk 6010 ICP G/T 5 grams 4ºC

Sodium Water 200.7/6010 ICP P/G 125 ml HNO3

Strontium Soil/Bulk 6010 ICP G/T 5 grams 4ºC


Technique

Collection

Media

Minimum


Strontium Water 200.7/6010 ICP P/G 125 ml HNO3

Sulfate Soil/Bulk EPA 9056 IC P/G 50 grams None

Sulfate Water 300.0 IC P/G 125ml None

SVOCS (Semi-volatile Organic

Compounds)Soil/Bulk 8270 GCMS G/T 50 grams 4ºC

See Appendix A for

list of analytes.

SVOCS (Semi-volatile Organic

Compounds)Water 625/8270 GCMS G/T 2x1000 ml 4ºC

See Appendix A for

list of analytes.

TAL Metals Profile Soil/Bulk 6010/7471 ICP G/T 5 grams 4ºC See Metals Analyses Section.

TAL Metals Profile Water6010/7470 or

200.7/245.1ICP P/G 1 Liter HNO3 See Metals Analyses Section.

TCLP (Toxicity Characteristic

Leaching Procedure) - Full ProfileSoil/Bulk 1311 VARIOUS G/T 250 grams 4ºC

See Appendix D for

list of analytes.

TCLP (Toxicity Characteristic

Leaching Procedure) - Full ProfileWater 1311 VARIOUS G/T 2x1000 ml 4ºC

See Appendix D for

list of analytes.

TCLP Herbicide Analysis Soil/Bulk 1311/8151 GC/ECD G/T 100 grams 4ºCSee Appendix D for

list of analytes.

TCLP Herbicide Analysis Water 1311/8151 GC/ECD G/T 2x1000 ml 4ºCSee Appendix D for

list of analytes.

TCLP Lead only Analysis (includes

extraction)Soil/Bulk 1311/7000 FAA P 100 grams 4ºC

TCLP Lead only Analysis (includes

extraction)Water 1311/7000 FAA P 250 ml 4ºC

TCLP Metals (RCRA) Analysis

(includes extraction)Soil/Bulk 1311/6010/ 7471 ICP/CVAA P/G 100 grams 4ºC

See Appendix D for

list of analytes.

TCLP Metals (RCRA) Analysis

(includes extraction)Water

1311/200.7/6010

245.2/7470ICP/CVAA P/G 500 ml 4ºC

See Appendix D for

list of analytes.


Technique

Collection

Media

Minimum


TCLP Pesticide Analysis Soil/Bulk 1311/8082 GC/ECD G/T 100 grams 4ºCSee Appendix D for

list of analytes.

TCLP Pesticide Analysis Water 1311/608/8081 GC/ECD G/T 2x1000 ml 4ºCSee Appendix D for

list of analytes.

TCLP Semi-Volatiles Analysis Soil/Bulk 1311/8270 GCMS G/T 100 grams 4ºCSee Appendix D for

list of analytes.

TCLP Semi-Volatiles Analysis Water 1311/625/8270 GCMS G/T 2x1000 ml 4ºCSee Appendix D for

list of analytes.

TCLP Volatiles Analysis Soil/Bulk 1311/8260 GCMS G/T 100 grams 4ºCSee Appendix D for

list of analytes.

TCLP Volatiles Analysis Water 1311/624/8260 GCMS G/T 2x1000 ml 4ºCSee Appendix D for list of analytes.

No Headspace

TDS (Total Dissolved Solids) Water SM2450 C Balance P/G 2x1000 ml 4ºC

Thallium Soil/Bulk 6010/7010 ICP/GFAA G/T 5 grams 4ºC

Thallium Water200.7/200.9 or


Titanium Soil/Bulk 6010 ICP G/T 5 grams 4ºC

Titanium Water 200.7/6010 ICP P/G 125 ml HNO3

Toxic Metals 6 - Drinking WaterDrinking


TPH (Total Recoverable

Petroleum Hydrocarbons)Soil/Bulk 418.1 FTIR G/T 100 grams 4ºC

TPH (Total Recoverable

Petroleum Hydrocarbons)Water 418.1 FTIR G/T 2x1000 ml HCl, 4ºC

TPH-DRO (Total Petroleum

Hydrocarbons, Diesel Range

Organics)

Soil/Bulk 8015 GC G/T 100 g 4ºC


Technique

Collection

Media

Minimum


TPH-DRO (Total Petroleum

Hydrocarbons, Diesel Range

Organics)

Water 8015 GC G/T 2x1000 ml 4ºC

TPH-GRO (Total Petroleum

Hydrocarbons, Gasoline Range

Organics)

Soil/Bulk 8015 P&T/GC G/T 50 grams 4ºC Minimum Headspace

TPH-GRO (Total Petroleum

Hydrocarbons, Gasoline Range

Organics)

Water 8015 P&T/GC G/T 3x40 ml HCl, 4ºC No Headspace In Sample Container.

TPH ERO (Extended Range

Organics)Soil/Bulk 8015 P&T/GC G/T 50 grams 4ºC Minimum Headspace

TPH ERO (Extended Range

Organics)Water 8015 P&T/GC G/T 3x40 ml HCl, 4ºC No Headspace In Sample Container.

TSS (Total Suspended Solids) Water SM2540 D Balance P/G 2x1000 ml 4ºC

Tungsten Soil/Bulk 6010 ICP G/T 5 grams 4ºC

Tungsten Water 200.7/6010 ICP P/G 125 ml HNO3

Turbidity Water 180.1 TURB. P/G 125 ml 4ºC

Vanadium Soil/Bulk 6010 ICP G/T 5 grams 4ºC

Vanadium Water 200.7/6010 ICP P/G 125 ml HNO3

VOCS (Volatile Organic

Compounds)Soil/Bulk 8260 P&T/GCMS G/T 50 grams 4ºC

Minimum Headspace, See Appendix

B for list of analytes.


Technique

Collection

Media

Minimum


VOCS (Volatile Organic

Compounds)Water 624/8260 P&T/GCMS G/T 3x40 ml


chlorine

No Headspace, See Appendix B for

list of analytes.

Welding Fume Metals Profile Soil/Bulk 6010 ICP G/T 5 grams 4ºC See Metals Analyses Section.

Welding Fume Metals Profile Water 200.7/6010 ICP P/G 1 Liter HNO3 See Metals Analyses Section.

Zinc Soil/Bulk 6010 ICP G/T 5 grams 4ºC

Zinc Water 200.7/6010 ICP P/G 125 ml HNO3

Inorganic Tests Methods Holding Time

Alkalinity SM 2320B 14 Days

Ammonia as Nitrogen EPA 300.0 (M) 28 Days

Bacteria, E-coli & Coliform - Drinking Water SM 9223B 30 Hours

Bacteria, E-coli & Coliform - Non-Potable Water SM 9223B 6 Hours

Bromide EPA 300.0 28 Days

Calcium Hardness SM 2340C 6 Months

Chloride EPA 300.0 28 Days

Conductivity SM 2510B 28 Days

Corrosivity as pH EPA 9040 Immediate

Fluoride EPA 300.0 28 Days

Hexavalent Chromium (CrVI) EPA 7196 24 hours

Lead by FLAA EPA 7000 6 months

Mercury EPA 7471 28 days

Metals (except CrVI and Mercury) ICP EPA 6010, EPA 200.7 6 Months

Metals (except CrVI and Mercury) GFAA EPA 200.8 6 Months

Nitrate (NO3) EPA 300.0 48 Hours

Nitrate + Nitrite EPA 300.0 48 Hours

Nitrite (NO2) EPA 300.0 48 Hours

Orthophosphate EPA 300.0 48 Hours

pH by Electrode EPA 9040 Immediate

Sulfate EPA 300.0 28 Days

Total Dissolved Solids SM 2540C 7 Days

Total Suspended Solids SM 2540D 7 Days

Turbidity SM 2130B 48 Hours

Organic Tests Methods Holding Time*

Herbicides, Chlorinated EPA 8151 7 Days

PCBs EPA 8082, EPA 608 7 Days

Pesticides, Organochlorine EPA 8081, EPA 608 7 Days

SVOCs (BNAs) EPA 8270, EPA 625 7 Days

DRO EPA 8015 7 Days

GRO/BTEX/MTBE EPA 8021 14 Days

VOCs EPA 8260, EPA 624 14 Days

Holding Times for Water/Aqueous Samples

* days for extraction; 40 days after extraction for analysis.

Inorganic Tests Mehods Holding Time

Alkalinity SM 2320B 14 Days

Ammonia as Nitrogen EPA 300.0 (M) 28 Days

Bromide EPA 300.0 (M) 28 Days

Chloride EPA 300.0 (M) 28 Days

Corrosivity as pH EPA 9045 24 Hours

Fluoride EPA 300.0 28 Days

Hexavalent Chromium (CrVI) EPA 7196 30 Days

Lead by FLAA EPA 7000 6 months

Mercury EPA 7471 28 days

Metals (except CrVI and Mercury) ICP EPA 6010 6 Months

Nitrate (NO3) EPA 300.0 (M) 7 Days

Nitrite (NO2) EPA 300.0 (M) 7 Days

Orthophosphate EPA 300.0 (M) 7 Days

pH by Electrode EPA 9045 24 Hours

Sulfate EPA 300.0 (M) 28 Days

Organic Tests Methods Holding Time*

Herbicides, Chlorinated EPA 8151 14 Days

Oil & Grease EPA 413 28 Days

PCBs EPA 8082 14 Days

Pesticides, Organochlorine EPA 8081 14 Days

SVOCs (BNAs) EPA 8270 14 Days

DRO EPA 8015 14 Days

GRO EPA 8015 14 Days

GRO/BTEX/MTBE EPA 8021 14 Days

VOCs EPA 8260 14 Days

Holding Times for Solid Samples

* days for extraction; 40 days after extraction for analysis.

Media Media

Media ID # Description Index

Cassettes / Metals

37mm MCEF Lead / Metals

37mm MW Matched Weighed

37mm UNW Unweighed PVC

37mm PW PVC Pre-Weighed PVC 2pc

37mm PW PVC Pre-Weighed Plc. 3pc

Cassettes / Asbestos

25mm MCEF PCM Asbestos

25mm MCEF TEM Asbestos

Cassettes

37mm GFF 225-7 Coal Tar Pitch

37mm MCE Tr (sodium carbonate) 225-9001

37mm GFF Tr (1-2pyrdl(peperazine) 225-9002 Isocyanates a

37mm GFF Tr(2,4,dinitrophenylhydrazine)) 225-9003 Gluderaldehye a

37mm FGG Tr(Sulfuric Acid) 225-9004

37mm MCE Tr (sodium carbonate) 225-9005 MDA

37mm Teflon 225-9006 Chlorine

37mm GFF Tr (mercuric acetate) 225-9007 Mercaptan a

37mm GFF (nitrate impregnated) 225-9014 Ozone

Stainless Steel Back Up Pad 225-26 Carbon Black

Swinex 225-32+226-39Fl. Tube PCB kit

37mm 2ug PTFE Filter 225-17-07

37mm 1.0ug PTFE Filter 225-17-01

25mm PTFE Washed Filter 225-1708+225-3-25

Mold

Air-o-Cell Cassette Zefon AOC010 Mold

Bio-Tape Zefon BT0025 Mold

Filters

TSP Filters

TSPW Filters (weighed)

PM 10 Filters

PW Whattman Filters

Sampling Media

Media Media


Badges

Passive Sampler 500-100 UMEX Formaldehyde

3M 3500 3M 3500 Badge

3M 3520 3M 3520 Badge

3M 3551 (ethylene Oxide) 3M 3551 Badge

Mercury Badge Holder Mercury Badge Holder

Mercury Badge Mercury Badge

OVM Badge OVM Badge (charcoal)

OVM Badge OVM Badge (Anasorb 747)

Tubes

Small Charcoal Tube 226-01

Lg. Charcoal Tube 226-09

Silica Gel Tube (75/150) 226-10

Silica Gel Tube specially clean 226-10-03

Silica Gel Tube (150/300) 226-10-04

Silica Gel Tube (sulfuric acid0 226-10-06 b

Silica Gel Tube (260/520) 226-15

Sorbent Tube 226-17-1A For Mercury

XAD (2-hydroxymethylpiperidine) 226-27 b

Soda lime Tube 226-28

Anasorb 747 (sulfuric acid) 226-29 b

XAD-2 Tube (40-80) 226-30

XAD-2 Tube (set of 2) 226-30-02

XAD-2 Tube (50/100) 226-30-04

XAD-2 Tube (p-anisidine) 226-30-07

Anasorb 708 226-30-08

XAD-2 Tube/GFF (OVS) 226-30-16 b

XAD-2 Tube 226-30-18 (naphthylisothiocyanate) b

Tenax Tube (10/20) 226-35-01 b

Charcoal Tub, JXC 226-36

Anasorb CSC, Charcoal Tube 226-37 set of 2

Treated Charcoal Tube 226-38-03 a

Florisil Tube 226-39

NO/NO2 Tubes (set of 30) 226-40

front tube NO2 nitrogen dioxide, middle tube

molecular sieve, back tube NO nitric oxide a

NO2 Tubes Only 226-40-02 NO2 Tube b

Gas Chrom-R Tube (sulfuric acid) 226-42-02 Gas Chrom-R b

Media Media


TUBES Cont.

Drying Tube 226-44 Drying Tube

Silica Gel Tube (50/100) 226-51 Silica Gel

XAD-2 Tube (2 hydroxymethyl 226-54 XAD-2 b

Tenax Tub / GFF (OVS) 226-56 Tenax / GFF (OVS) b

XAD-7/GFF (OVS) 226-57 XAD-7/GFF (OVS) b

XAD-2/Quartz Filter (OVS) 226-58 XAD-2/Quartz Filter(OVS) b

Coconut CT (potassium hydroxide) 226-67 Coconut CT b

Coconut CT (t-butylcatechol) 226-73 Coconut CT b

Anasorb 747 (potassium hydroxide) 226-80 Anasorb 747 b

Anasorb 747 (70/140) 226-81A Anasorb 747

Anasorb 747 (200/400) 226-83 Anasorb 747

XAD-7 (50/100) 226-95 XAD-7 (50/100)

XAD-7 (chloride) 226-96 XAD-7 b

XAD-7 (1) specially cleaned (2) regular (set of 3

tubes) 226-97 XAD-7

XAD-7 (phosphoric acid) 226-98 XAD-7 b

Chromasorb-102 226-107 Chromasorb-102

Chromosorb 106 226-111A Chromasorb-106

Porapak-Q 226-115 Porapak-Q

XAD-2 (2-hydroxymethylpiperidine) 226-117 XAD-2 Lg. b

XAD-2 (2-hydroxymethylpiperidine) 226-118 XAD-2 Sm. b

Silica Gel (2,4 dintrophenlhydrazine) 226-119 Silica Gel a

Anasorb (75/150) 226-121 Anasorb (75/150)

Orbo 34 20211 Orbo 34

Orbo 43 20258 Orbo 43

Orbo 49P 20350 Orbo 49P

Orbo 53 20365 Orbo 53

Orbo 90 20358 Orbo 90

Orbo 92 20362 Orbo 92

BAGS

Tedlar Bags 233-01B Tedlar Bags

3x5 3x5 sample bag (Qty 100)

4x6 4x6 sample bag (Qty 100)

12x12 12x12 sample bag(Qty 100)

Wipes

ASTM Ghost Wipes ASTM Ghost Wipes

Whattman Filters Whattman Filters

Spike Wipes Spike Wipes (200 mic.)

PCB Wipe Kit In House Watt. Filter/Hex. Scint. Via

Media Media


Glassware

Plastic Bottle 125ml




Amber Liter 1L

Clear wm jar 4oz

Clear wm jar 8oz

Scintillation Vials Scintillation Vials

50ml Centrifuge Tubes Lead Centrifuge tubes

40 ml Amber VOA Unpr. 40ml Unpreserved

40ml Amber VOA Pres. 40ml HCL Preserved

40ml Clear Voa unpr. 40ml Unpreserved

40ml Clear Voa Pres. 40ml Preserved

Gloves

S. Powder Free Gloves SM (100 ea. Box)

Lg. Powder Free Gloves Lg (100 ea. Box)

XL Powder Free Gloves XL (100 ea. Box)

A

B

C

Key

Appendix

A

A

8270 625 PPL1 PAHs2 A3 B/N4

Acenaphthene X X X X XAcenaphthylene X X X X XAniline X X XAnthracene X X X X XBenzidine X X X XBenzo(a)anthracene X X X X XBenzo(a)pyrene X X X X XBenzo(b)fluoranthene X X X X XBenzo(g,h,i)perylene X X X X XBenzo(k)fluoranthene X X X X XBenzoic acid X X XBenzyl alcohol X XBis (2-chloroethoxy) methane X X X XBis (2-chloroethyl) ether X X X X2,2'-Oxybis(1-Chloropropane) X X X XBis (2-ethylhexyl) phthalate X X X X

4- Bromophenyl phenyl ether X X X XButylbenzyl phthalate X X X XCarbazol X X X

4- Chloro-3-methylphenol X X X X4- Chloroaniline X X2- Chloronaphthalene X X X X2- Chlorophenol X X X X4- Chlorophenyl phenyl ether X X X X

Chrysene X X X X XDibenz(a,h)anthracene X X X X XDibenzofuran X XDibutyl phthalate X X X X

1,2- Dichlorobenzene X X1,3- Dichlorobenzene X X1,4- Dichlorobenzene X X3,3'- Dichlorobenzidine X X X X2,4- Dichlorophenol X X X X

Diethyl phthalate X X X XDimethyl phthalate X X X X

2.4- Dimethylphenol X X X X4,6- Dinitro-2-methylphenol X X X X

SEMI-VOLATILE ANALYTES

ANALYTE

BY MASS SPECTROMETRY(Compounds reported in a standard profile)

A

8270 625 PPL1 PAHs2 A3 B/N4ANALYTE

2,4- Dinitrophenol X X X X2,4- Dinitrotoluene X X X X2,6- Dinitrotoluene X X X X

Di-n-octyl phthalate X X X XFluoranthene X X X X XFluorene X X X X XHexachlorobenzene X X X XHexachlorobutadiene X X X XHexachlorocyclopentadiene X X X XHexachloroethane X X X XIndeno(1,2,3-cd)pyrene X X X X XIsophorone X X X X

2- Methyl phenol X X X3- and 4- Methyl phenol X X

2- Methylnaphthalene X XNaphthalene X X X X X

2- Nitroaniline X X3- Nitroaniline X X4- Nitroaniline X X

Nitrobenzene X X X X2- Nitrophenol X X X X4- Nitrophenol X X X XN- Nitrosodimethylamine X X X XN- Nitroso-di-n-propylamine X X X XN- Nitrosodiphenylamine X X X X

Pentachlorophenol X X X XPhenanthrene X X X X XPhenol X X X XPyrene X X X X XPyridine X X X

1,2,4- Trichlorobenzene X X X X2,4,5- Trichlorophenol X X2,4,6- Trichlorophenol X X X X

1. PPL - Priority Pollutant List2. PAHs - Polyaromatic Hydrocarbons3. A - Acid Semi-volatile fraction4. B/N - Base/Neutral Semi-volatile fraction

Appendix

B

B

ANALYTE 8021 8260 624Acetone X X

Benzene X X X

Bromobenzene X

Bromochloromethane X

Bromodichloromethane X X

Bromoform X X

Bromomethane X X

n- Butylbenzene X

sec- Butylbenzene X

tert- Butylbenzene X

Carbon disulfide X

Carbon tetrachloride X X

Chlorobenzene X X

Chloroethane X X

2- Chloroethylvinyl ether X X

Chloroform X X

Chloromethane X X

2- Chlorotoluene X

4- Chlorotoluene X

1,2- Dibromo-3-chloropropane X

Dibromochloromethane X X

1,2- Dibromoethane X X

Dibromofluoromethane X X

Dibromomethane X

1,2- Dichlorobenzene X X



Dichlorodifluoromethane X X

1,1- Dichloroethane X X

1,2- Dichloroethane X X

1,1- Dichloroethene X X

cis-1,2- Dichloroethene X X

trans-1,2- Dichloroethene X X

1,2- Dichloropropane X X

1,3- Dichloropropane X

VOLATILE ANALYTES(Compounds reported in a standard profile)

B

ANALYTE 8021 8260 624

2,2- Dichloropropane X

1,1- Dichloropropene X

cis-1,3- Dichloropropene X X

trans-1,3- Dichloropropene X X

Ethylbenzene X X X

Hexachlorobutadiene X

2- Hexanone X

Isopropylbenzene X

p- Isopropyltoluene X

Methyl ethyl ketone X X

Methyl isobutyl ketone X X

Methyl t-butyl ether (MTBE) X X X

4- Methyl-2-pentanone X X

Methylene Chloride X X

Naphthalene X

n- Propylbenzene X

Styrene X

1,1,1,2- Tetrachloroethane X

1,1,2,2- Tetrachloroethane X X

Tetrachloroethene X X

Toluene X X X

1,2,3- Trichlorobenzene X

1,2,4- Trichlorobenzene X

1,1,1- Trichloroethane X X

1,1,2- Trichloroethane X X

Trichloroethene X X

Trichlorofluoromethane X X

1,2,3- Trichloropropane X

1,2,4- Trimethylbenzene X

1,3,5- Trimethylbenzene X

Vinyl acetate X

Vinyl chloride X X

m-,p- Xylene X X X

o- Xylene X X X

p- Xylene X X X

Appendix

C

C

Pesticides Pesticides Herbicides PCBsANALYTE 608* 8081 8151 8082

Aldrin X Xalpha-BHC X Xbeta-BHC X Xdelta-BHC X Xgamma-BHC (Lindane) X X

α- Chlordane Xg- Chlordane X

Chlordane X X4,4’- DDD X X4,4’- DDE X X4,4’- DDT X X

Dieldrin X XEndosulfan I X XEndosulfan II X XEndosulfan sulfate X XEndrin X XEndrin aldehyde X XEndrin ketone XHeptachlor X XHeptachlor epoxide X XMethoxychlor X

2-4-D X2,4,5-T X2,4,5-TP X

Toxaphene X X

Aroclor – 1016 X XAroclor – 1221 X XAroclor – 1232 X XAroclor – 1242 X XAroclor – 1248 X XAroclor – 1254 X XAroclor – 1260 X X

PCB / PESTICIDEAND HERBICIDE ANALYTES

(Compounds reported in a standard profile)

Appendix

D

D

PARAMETER REGULATORY LIMITS (mg/L)

Metals Arsenic 5.0Barium 100Cadmium 1.0Chromium 5.0Lead 5.0Mercury 0.2Selenium 1.0Silver 5.0

Volatiles Benzene 0.5Carbon Tetrachloride 0.5Chlorobenzene 100Chloroform 6.0

1,4- Dichlorobenzene 7.51,2- Dichloroethane 0.51,1- Dichloroethene 0.7

2- Butanone (MEK) 200Tetrachloroethene 0.7Trichloroethene 0.5Vinyl Chrloride 0.2

Semi-Volatiles 2,4- Dinitrotoluene 0.13Hexachlorobenzene 0.13Hexachlorobutadiene 0.5Hexachloroethane 3.0

2- Methylphenol 2003-,4- Methylphenol 400

Nitrobenzene 2.0Pentachlorophenol 100Pyridine 5.0

2,4,5- Trichlorophenol 4002,4,6- Trichlorophenol 2.0

Pesticides Chlordane 0.03Endrin 0.02Heptachlor 0.008Heptachlor Epoxide 0.008Lindane 0.4Methoxychlor 10.0Toxaphene 0.5

Herbicides 2,4- D 102,4,5- TP (Silvex) 1.0

TCLP PARAMETERSAND REGULATORY LIMITS

D

Substance STLC Level (mg/L)

TTLC Level (mg/kg)

Antimony 15 500.0Arsenic 5 50Barium 100 10000.0Beryllium 0.75 75.0Cadmium 1 100.0Chromium VI compounds 5 500.0Chromium 5 2500.0Cobalt 80 8000Copper 25 2500Lead 5 1000.0Mercury 0.2 20Molybdenum 350 3500Nickel 20 2000Selenium 1 100Silver 5 500Thallium 7 700Vanadium 24 2400Zinc 250 5000

Source is California Code of Regulations, Title 22, Chapter 11, Article 3.

STLC/TTLC REGULATORY LIMITSFor Inorganic Substances

D

Substance STLC Level (mg/L)

TTLC Level (mg/kg - Wet Weight)

Aldrin 0.14 1.4Chlrodane 0.25 2.5DDT, DDE, DDD 0.1 1.02,4-Dichlorophenoxyacetic acid 10 100.0Dieldrin 0.8 8.0Dioxin (2,3,7,8-TCDD) 0.001 0.0Endrin 0.02 0.2Heptachlor 0.47 4.7Kepone 2.1 21Lead compounds, organic - 13Lindane (gamma-BHC) 0.4 4Methoxychlor 10 100.0Mirex 2.1 21Pentachlorophenol 1.7 17PCBs (Polychlorinated Biphenyls) 5 50Toxaphene 0.5 5Trichloroethylene 204 2040

2,4- Trichlorophenoxypropionic acid 1 10

Source is California Code of Regulations, Title 22, Chapter 11, Article 3.

STLC/TTLC REGULATORY LIMITSFor Organic Substances

Appendix

E

Date

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PAYMENT INFORMATION VISA MASTERCARD AMERICAN EXPRESS DISCOVER

2512 W. Cary Street, Richmond, VA 23220Phone 804-353-6778 Fax 804-254-9586Email [email protected]

Customer Name

Special Instruction

Address

City State Zip

Phone Email

Credit Card Type

Credit Card Number Exp Auth #

Cardholder Name

Cardholder Signature Date

SCHNEIDER LABORATORIES GLOBAL, INCORPORATED

CREDIT CARD INFORMATION

VISA MASTERCARD AMERICAN EXPRESS DISCOVER

I authorize SLGI to charge our current invoices to my credit card. I understand that I am responsible for communicating any credit card changes directly to SLGI. Furthermore, I understand that I must provide a new card number in the event that this

card becomes expired or I change credit card providers

CREDIT CARD AUTHORIZATION

"Confidential"


2512 W. Cary Street, Richmond, VA 23220

To Whom It May Concern,

This is to inform you about Schneider Laboratories Global sample disposal policy. The bottom right hand

side of our COC has a box in which the sender can choose how they want the laboratory to dispose of their

samples. If this box is not checked then the laboratory will dispose of the samples within the appropriate

time frame.

The Sample Disposal box shown above also has a statement which says that a fee of $50 will be charged

for samples with an excessive weight. This is due to the high cost of disposing hazardous waste.

This process bases an excessive weight on the actual amount of sample needed for the analysis. This

disposal fee affects the analysis of soils, paints and bulk samples.

Test Excessive Amount

TCLP > 150 grams or 1/4 pound

Metals except Chromium VI > 5 grams (1/8 cup or 2 Tbsp.)

Chromium VI > 10 grams (1/4 cup or 4 Tbsp.)

Bulk Asbestos > small ziplock bag (Fits in hand)

Vermiculite (float method) > quart size ziplock bag

We thank you for understanding the need for this process. Lowering our hazardous waste disposal costs

will ensure we can keep offering the lowest prices. If you have any questions or concerns, please do not

hesitate to contact us.

Please sign and return the form,

_______________________________________ Printed Name _______________________________________ ________________________ Signature Date

Appendix

F

Sample Disposal Return to Sender (shipping fees) Disposal by Lab ($50 fee for excessive weight)

SCHNEIDER LABORATORIES GLOBAL, INC.

2512 West Cary Street, Richmond, Virginia 23220-5117 804-353-6778 • 800-785-LABS (5227) • Fax 804-359-1475

www.slabinc.com e-mail: [email protected]

Submitting Co. Lab WO# Phone

Acct # Fax / Email

**State of Collection

**Cert. Required Yes No

Project Name:

Project Location:

Project Number:

PO Number:

Turn Around Time (TAT) Matrix / Sample Type (Select ONE) Tests / Analytes (Select ALL that Apply)

2 hours* All samples on form should be of SAME Asbestos in Air Asbestos in Bulk Metals-Total

Same day* †matrix type. Use additional forms as needed.

PCM (NIOSH 7400) PLM Lead

1 business day* † Air Solid TEM (AHERA) PLM (Point Count) RCRA Metals

2 business days* † Aqueous Waste TEM (EPA Level II) PLM (Qualitative only) TCLP

3 business days* † Bulk Wastewater Miscellaneous Tests NYELAP TCLP / Lead

5 business days* † Hi-Vol Filter (PM10) Water,Drinking Total Dust (NIOSH 0500) CAELAP (Point Count) TCLP / RCRA Metals

* Not available for all tests Hi-Vol Filter (TSP) Compliance Resp. Dust (NIOSH 0600) TEM (Chatfield) TCLP / Full (w/ organics) 10 day

A job received past 3PM Oil Wipe Silica - FTIR (NIOSH 7602) ______________________ Microbiology † will begin its TAT the next business day Paint Wipe, Composite Silica - XRD (NIOSH 7500) FOR ASBESTOS AIR: BACT (MPN & P/A)

Schedule rush organics, multi- Sludge _________________ Other TYPE OF RESPIRATOR Mold Direct Exammetals & weekend tests in

advance. Soil _________________ ______________________ USED: ___________________ _______________________

Sample #Date

Sampled**Time

Sampled**Sample Identification

(Employee, SSN, Bldg, Material, Type1)Wiped

Area (ft2)pH /

Temp * Start Stop Start StopTotal4

Air

1Type: A=Area B=Blank P=Personal E=Excursion 2Beginning/End of Sample Period 3Pump Calibration in Liters/Minute 4Volume in Liters [time in min × flow in L/min]

Relinquished to lab by NAME ________________________________ SIGNATURE ___________________________ DATE / TIME ___________________________

WO Label

Time2 Flow Rate3

Sampled by NAME ________________________________ SIGNATURE ___________________________ DATE / TIME ___________________________

Special Instructions [include requests for special reporting or data packages]

For Lab Use:

Chain-of-Custody documentation continued internally within lab.Terms and conditions page 2.* Temperature taken with IR Gun A. **Required.

All soil and aqueous samples must be sent in adequate quantity for duplicate analysis to be performed per EPA requirements. Failure to perform a sample duplicate analysis, due to a lack of sample quantity, will lead to a disclaimer on the report. All problem jobs without customer response held over 30 days will be voided and disposed of.

SCHNEIDER LABORATORIES GLOBAL, INC. TERMS AND CONDITIONS

Schneider Laboratories Global, Inc. (“Schneider”, which includes all of Schneider’s officers, directors, employees, agents, and all other representatives and/or agents of any kind [collectively, Schneider]) hereby expressly disclaims any and all liability for both any and all indirect and consequential damages which might be asserted or alleged by any person or entity – including but not limited to the person or entity submitting samples for testing its customer(s), agents, representatives or third parties [collectively, the Submitting Company] – arising from or in any way relating to Schneider’s performance of any and all services – including but not limited to analysis, testing and reporting regarding samples provided by Submitting Company – performed in connection with, or in any way relating to, this Chain-of-Custody form, the samples referenced herein, the Purchase Order referenced herein.

Schneider’s liability is hereby expressly limited to the direct cost of correcting any error or omission in the performance of its services (which shall be strictly limited to the direct out-of-pocket cost of correctly performing the specific analyses or tests referenced herein, or the direct out-of-pocket cost of correctly reporting any result of Schneider’s work).

(1) the person submitting, signing, or initialing this form represents and warrants that he is authorized by the Submitting Company, all customers of the Submitting Company, and all other persons or entities who may be affected, to execute this form and all related forms and agreements and to bind all such persons/entities to all terms and conditions set forth herein; and (2) the Submitting Company hereby represents and warrants that it is authorized by all customers of the Submitting Company, and all other persons or entities who may be affected, to execute this form and all related forms and agreements and to bind all such persons/entities to all terms and conditions set forth herein; and

(3) on behalf of all such customers persons and entities, the Submitting Company hereby agrees to all terms and conditions set forth herein and expressly waives and releases any and all claims, whether past or future, for indirect or consequential damages as described herein.

By submitting, signing, or initialing this form,

Sample Disposal Return to Sender (shipping fees) Disposal by Lab ($50 fee for excessive weight)

Project Name:

Project Location:

Project Number:

Purchase Order # TAT Requested

(Business Day) 1 2 3 4 5 10 All jobs received past 3PM will begin its TAT the next business day

Lab Use Matrix

Sample #**Date

Sampled

# C

onta

iner

s

Chl

orin

e (C

l)

Tem

p *

pH

Oil

or A

ir

Drin

king

Wat

er

Was

te W

ater

Gro

und

Wat

er

**Time Sampled

Wip

e

Soil

/ Slu

dge

Bulk

Analysis Request Other

SCHNEIDER LABORATORIES GLOBAL, INC.2512 West Cary Street, Richmond, Virginia 23220-5117

804-353-6778 • 800-785-LABS (5227) • Fax 804-359-1475 www.slabinc.com e-mail: [email protected]

Submitting Co. Lab WO# Phone

Acct # Fax \ Email

**State of Collection

**Cert. Required Yes No

WO Label

Relinquished to lab by NAME ________________________________ SIGNATURE ___________________________ DATE / TIME ___________________________

For Lab Use: Sampled by NAME ________________________________ SIGNATURE ___________________________ DATE / TIME ___________________________

BTEX

M

TBE

N

apht

hale

ne

Purg

eabl

e Ar

omat

ics

8021

Petro

l Hyd

roca

rbon

s G

C 8

015M

Die

sel

8015

M G

as

TPH

418

.1

Cor

rosi

vity

Rea

ctiv

ity

F

lash

poin

t, C

lose

d C

up

Vola

tile

Org

anic

s 62

4

82

60

Sem

ivol

atile

Org

anic

s 62

5

82

70

PAH

s 61

0

82

70

8

310

By H

PLC

TCLP

Sem

i-Vol

s

BN

As

P

est

H

erb

VOAs

Full

Pest

icid

es 6

08

8

081

Her

bici

des

8151

PC

B's

8082

Chain-of-Custody documentation continued internally within lab.Terms and conditions page 2.

Special Instructions [include requests for special reporting or data packages]

* Temperature taken with IR Gun A. **Required.

All soil and aqueous samples must be sent in adequate quantity for duplicate analysis to be performed per EPA requirements. Failure to perform a sample duplicate analysis, due to a lack of sample quantity, will lead to a disclaimer on the report. All problem jobs without customer response held over 30 days will be voided and disposed of.

SCHNEIDER LABORATORIES GLOBAL, INC. TERMS AND CONDITIONS

Schneider Laboratories Global, Inc. (“Schneider”, which includes all of Schneider’s officers, directors, employees, agents, and all other representatives and/or agents of any kind [collectively, Schneider]) hereby expressly disclaims any and all liability for both any and all indirect and consequential damages which might be asserted or alleged by any person or entity – including but not limited to the person or entity submitting samples for testing its customer(s), agents, representatives or third parties [collectively, the Submitting Company] – arising from or in any way relating to Schneider’s performance of any and all services – including but not limited to analysis, testing and reporting regarding samples provided by Submitting Company – performed in connection with, or in any way relating to, this Chain-of-Custody form, the samples referenced herein, the Purchase Order referenced herein.

Schneider’s liability is hereby expressly limited to the direct cost of correcting any error or omission in the performance of its services (which shall be strictly limited to the direct out-of-pocket cost of correctly performing the specific analyses or tests referenced herein, or the direct out-of-pocket cost of correctly reporting any result of Schneider’s work).

(1) the person submitting, signing, or initialing this form represents and warrants that he is authorized by the Submitting Company, all customers of the Submitting Company, and all other persons or entities who may be affected, to execute this form and all related forms and agreements and to bind all such persons/entities to all terms and conditions set forth herein; and (2) the Submitting Company hereby represents and warrants that it is authorized by all customers of the Submitting Company, and all other persons or entities who may be affected, to execute this form and all related forms and agreements and to bind all such persons/entities to all terms and conditions set forth herein; and

(3) on behalf of all such customers, persons and entities, the Submitting Company hereby agrees to all terms and conditions set forth herein and expressly waives and releases any and all claims, whether past or future, for indirect or consequential damages as described herein.

By submitting, signing, or initialing this form,

Acceptance Policy

BASIC REQUIREMENTS

• Samples must be submitted with a SLGi Submittal form or equivalent, with full instructions including tests requested, turnaround time desired, certification needs, submitter and customer information.

• It is the customer’s responsibility to communicate specific methods or detection limits required.

• Samples must be appropriately sealed to prevent leakage or cross-contamination.

• Samples must be clearly labeled.

• Samples should be collected on the appropriate media for the test and/or submitted in the appropriate vessel type. (See Sampling Guide for information per test.)

• Samples should be shipped in a manner to preserve the sample’s safety, quality, and integrity.

• It is the customer’s responsibility to ship the samples to the lab at the appropriate temperature for sample preservation.

• Sample temperature will be monitored upon receipt for temperature-sensitive samples. The receipt temperature for organics environmental samples is displayed on the final report. Customers may be notified of the receipt temperature upon request.

LABORATORY RESPONSE TO UNSUITABLE SAMPLES

• When testing requests, sample labeling, or other associated information is unclear, the laboratory will contact the customer for clarification.

• The laboratory retains the right to reject, or request re-collection and re-submission of any sample believed to be unsuitable for testing.

• The laboratory will provide report comments regarding any samples with questionable suitability.

LABORATORY RESPONSIBILTY & SAMPLER’S / CUSTOMER’S RESPONSIBILTY

• The laboratory does not provide sampling services for its customers.

• All samples are tested as received, and all laboratory analysis results relate only to the portion tested.

• It is the sampler’s responsibility to provide a sample that is representative of the material being investigated.


804-353-6778 Toll Free - 800-785-LABS (5227) FAX - 804-359-1475 www.slabinc.com [email protected]

Supply Request Form Shipping and handling charges will be applied.

Requested by:

Account Number: ________________ Date/Time: __________________________

CompanyName:________________________________________________________________

Requester’sName:___________________________________Phone#______________________

Requester'sSignature:____________________________________________________________

Ship To:

Company/SiteName:_____________________________________________________________

ShipAttention:__________________________________________________________________

Address:______________________________________________________________________

City: ________________________________________ State: ______Zip: ______________

DateNeeded:__________________________ShipVia: _________________________________

Qty Supply Items Qty Supply Items Qty Supply Items Ghost Wipes Plastic Bottles - 125ml w/HNO3 Asbestos/Soil Bag - 3 x 5

Gloves, Latex - 100 count box Plastic Bottles - 500ml w/HNO3 Asbestos/Soil Bag - 4 x 6

Centrifuge Tubes Plastic Bottles - 1L w/HNO3 Sample Bag - 12 x 12

Cassettes - 25mm Asbestos VOA’s w/HCL Waybills - Fed Ex

Cassettes - 37mm Metals Amber Jars - 1L w/preservative Waybills - UPS

Cassettes - 37mm PW (2 pc) Jars - 4oz. COC - Standard COC

Cassettes - 37mm PW (3 pc) Jars - 8oz. COC - Organic COC

Qty Additional Items Qty Additional Items Qty Additional Items

Order Taken By: ______________________________ Date/Time Shipped: _________________________


Appendix

G

Schneider Laboratories Inc. Accreditations, Certifications, Licenses

CERTIFICATION/LICENSE/APPROVAL

Bulk Asbestos Fiber Analysis Polarized Light Microscopy

Industrial Hygiene Laboratory Accreditation Program (IHLAP):

Metals, Asbestos PCM, Organic Solvents, Silica, Asbestos PCM, Diffusive Samples;

Environmental Lead Laboratory Accreditation Program (ELLAP/NLLAP):

Paint Chips, Dust Wipes, Air, Soil Environmental Microbiology Laboratory

Accreditation Program (EMLAP): Mold

VELAP - NELAC Drinking Water - Metals, E-Coli, Total Coliform Non-Potable Water - Anions, Metals, Organics

Solid/Hazardous Waste - TCLP, Metals, Organics Polarized Light Microscopy (PLM) - Bulk

National Environmental Laboratory Accreditation Conference (NELAC)

U. S. Dept. of Commerce,National Institute of Standards and Technology (NIST)

National Voluntary Laboratory Accreditation Program (NVLAP)

FOR STATE AND MUNICIPALITIES Check Website - www.slabinc.com or call laboratory for information

NATIONAL ACCREDITATION

DEPT./AGENCY

American Industrial Hygiene Association(AIHA)

Appendix

H

Is there a strange odor in your house? Is the paint peeling where your child plays? Do you see mold? Does your water taste or smell odd? If you are concerned with any of these questions, don’t wait another minute to see if your family is exposed to a potential health hazard. With one of our Lead Test Kits, Mold Test Kits, Asbestos Test Kits, or other easy to use and inexpensive home test kits, you can reach the peace of mind you need. Overwhelming media attention and newly enacted legislation regarding life threatening home and office pollutants has heightened consumer awareness. This awareness has in turn created the demand for professional-grade environmental home safety test kits. SLGI Certified Test Kits © are the first of their kind available nationally and globally. What we have to offer you is sure to satisfy any need you have to identify dangerous contaminants polluting the environments that surround you. The analytical cost is included in the cost of the kit so there are no hidden laboratory fees. Test Kits are available online from various vendors but can also be found at Schneider Laboratories Global Website: www.slabinc.com If you are submitting a kit with multiple samples (eg 5 Pack or 10 Pack), your samples must be submitted in one shipment only.


Documents

Environmental - Schneider Laboratories Global, Inc...SCHNEIDER LABORATORIES GLOBAL, INCORPORATED 2512 W. Cary Street, Richmond, VA 23220-5117 Tel: 804-353-6778 Toll Free: 800-785-LABS