51
Suitable for use with: Standard SAC Alloys Engineering Manual LOCTITE GC 10 T4 Solder Paste GC 10 The Game Changer

Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

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Page 1: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

Suitable for use with: Standard SAC Alloys

Engineering ManualLOCTITE GC 10 T4 Solder Paste

GC 10 – The Game Changer

Page 2: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste2

1. Performance Summary

2. Introduction: Properties, Features & Benefits

3. Operating Parameters

• Printing: Process Window

• Printing: Continuous and Abandon Time Testing

• Slump Testing

• Tack-Life Force

• Reflow Process Window

• Reflow Performance Testing

• Voiding Data

4. Reliability and Specification Testing

5. Operating Parameters: Storage

• Printing & Reflow Performance

6. Product Summary

Contents

Page 3: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste3

1. Performance Summary

2. Introduction: Properties, Features & Benefits

3. Operating Parameters

• Printing: Process Window

• Printing: Continuous and Abandon Time Testing

• Slump Testing

• Tack-Life Force

• Reflow Process Window

• Reflow Performance Testing

• Voiding Data

4. Reliability and Specification Testing

5. Operating Parameters: Storage

• Printing & Reflow Performance

6. Product Summary

Contents

Page 4: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste4

GC 10: Performance Summary

Flux

• Halogen-free flux: passes IC with pretreatment IPC-TM-650

2.3.34/EN14582

• Halogen-free flux classification: ANSI/J-STD-004 Rev. B for

a type ROL0 classification

Paste

• Suitable for fine pitch, high speed printing up to 125mm/s (5”/s)

• Optimized for long hot soak reflow profiles

• Excellent fine pitch coalescence in air & nitrogen atmosphere

• Excellent humidity resistance

• Excellent solderability on challenging surface finishes,

including CuNiZn

• Colorless residues for easy post-reflow inspection

• Long 12month shelf-life when stored below 26.5C

Page 5: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste5

1. Performance Summary

2. Introduction: Properties, Features & Benefits

3. Operating Parameters

• Printing: Process Window

• Printing: Continuous and Abandon Time Testing

• Slump Testing

• Tack-Life Force

• Reflow Process Window

• Reflow Performance Testing

• Voiding Data

4. Reliability and Specification Testing

5. Operating Parameters: Storage

• Printing & Reflow Performance

6. Product Summary

Contents

Page 6: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

IntroductionBasic Solder Paste Properties

Flux Description GC 10

Alloy SAC305

Henkel Powder Size Type 4

Powder Size range, m 38-20

Metal Content, % 88.5

Malcom Viscosity, 10rpm Pa.s 190

TI 0.50

IPC slump @182C (0.33mm x 2.03mm)

first space no bridge

0.20

IPC Solder Balling preferred

October 23, 2015 Engineering Manual GC 10 Solder Paste6

Page 7: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste7

IntroductionGC 10 Features & Benefits

Product Attribute Process Benefit

Halogen Free • No added halogen

• Measured <900ppm chlorine and bromine and <1,500ppm total by

oxygen (O2) bomb test

Halide Free • Flux classification ROL0 in accordance to J-STD-004B

Application • Designed for printing and pin-in-paste

• Excellent wetting to a broad range of metallisations, even through

long hot soak profiles in an air atmosphere

• Compatible with existing halogen free solutions

• Suitable for medium to large board assemblies

• Designed for long 12 month shelf-life stability without impact to

printing or reflow

Page 8: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste8

IntroductionGC 10 Features & Benefits

Product Attribute Process Benefit

Technology Printing

Advantages

• Wide process window for printing and minimal slump

• Fine pitch abandon time of up to 2 hours; work life > 16 hours

• Fine pitch capability and reduction in solder bridging

• Suited for high throughput production, where yield consistency on print

deposits is key

• Improved paste transfer efficiency

• Allows on line paste utilisation protocols to be re-written

Technology Reflow

Advantages

• Optimised for long hot soak reflow processes

• Very shiny Pb-free solder joints over wide range of reflow

• Excellent fine pitch coalescence

• Excellent humidity resistance

• Excellent solderability on challenging surface finishes (ENIG, Copper OSP,

CuNiZn and Imm Ag)

Low Voiding • Low void levels increases solder joint reliability

• New chemistries allow pursuit of class 3 void levels in accordance to IPC7095B

on industry surface finishes: ENIG, Copper OSP, CuNiZn and Imm Ag

• Low voiding in CSP

Residues • Clear, transparent and colourless

• Pin testable after 5x reflows

Page 9: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste9

1. Performance Summary

2. Introduction: Properties, Features & Benefits

3. Operating Parameters

• Printing: Process Window

• Printing: Continuous and Abandon Time Testing

• Slump Testing

• Tack-Life Force

• Reflow Process Window

• Reflow Performance Testing

• Voiding Data

4. Reliability and Specification Testing

5. Operating Parameters: Storage

• Printing & Reflow Performance

6. Product Summary

Contents

Page 10: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste10

Operating ParametersPrint Process Window (LOCTITE GC 10 SAC305 T4 885V)

Speed mm/s

Pre

ssu

re

kg

/m

m

120100806040

0.04

0.03

0.02

>

< 1.33

1.33 1.67

1.67 2.00

2.00

Cpk0.8mmBGA

Speed mm/s

Pre

ssu

re

kg

/m

m

120100806040

0.04

0.03

0.02

>

< 1.33

1.33 1.67

1.67 2.00

2.00

Cpk0.4mmCSP56

Speed mm/s

Pre

ssu

re

kg

/m

m

120100806040

0.04

0.03

0.02

>

< 1.33

1.33 1.67

1.67 2.00

2.00

Cpk0.5mmBGA

Speed mm/s

Pre

ssu

re

kg

/m

m

120100806040

0.04

0.03

0.02

>

< 1.33

1.33 1.67

1.67 2.00

2.00

0201 Cpk

Contour Plot of 0.5mmBGA (266um aperture) Cpk

Contour Plot of 0.4mmCSP56 (300um aperture) Cpk

Contour Plot of 0201 Cpk

Contour Plot of 0.8mmBGA Cpk• Excellent printing in the

range 25 – 125mm/s

0.8mm, 0.5mm & 0.4mm round apertures, 0201 (100µm stencil)

Page 11: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste11

Operating ParametersPrint Process Window (LOCTITE GC 10 SAC305 T4 885V)

Speed mm/s

Pre

ssu

re

kg

/m

m

120100806040

0.04

0.03

0.02

>

< 1.33

1.33 1.67

1.67 2.00

2.00

diam Cpk0.22mm

Speed mm/s

Pre

ssu

re

kg

/m

m

120100806040

0.04

0.03

0.02

>

< 1.33

1.33 1.67

1.67 2.00

2.00

diam Cpk0.20mm

Speed mm/s

Pre

ssu

re

kg

/m

m

120100806040

0.04

0.03

0.02

>

< 1.33

1.33 1.67

1.67 2.00

2.00

diam Cpk0.18mm

Speed mm/s

Pre

ssu

re

kg

/m

m

120100806040

0.04

0.03

0.02

>

< 1.33

1.33 1.67

1.67 2.00

2.00

diam Cpk0.15mm

Contour Plot of 0.22mm diam Cpk

Contour Plot of 0.18mm diam Cpk Contour Plot of 0.15mm diam Cpk

Contour Plot of 0.20mm diam Cpk• Excellent printing in the

range 25 – 125mm/s, 0.18-0.22mm round apertures

0.22mm – 0.15mm round apertures, (100µm stencil)

Page 12: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste12

Operating Parameters – Separation SpeedPrint Process Window (LOCTITE GC 10 SAC305 T4 885V)

0.15

mm diam

0.18

mm d

iam

0.20

mm diam

0.22

mm diam

0.5B

GA (0.26

6mm ap)

0.4m

mCSP5

6 (0

.30m

m ap)

0.8B

GA

5

4

3

2

1

0

Component_Cpk

Cp

k

1.33 ref1.67 ref

Fast

Medium

Slow

Variable

Separation Speed, CpkLoctite GC10 T4

• Excellent printing in the range down to 0.18mm round apertures.

• Fast separation speed is preferable.

0.8mm BGA – 0.15mm round apertures, (100µm stencil) 100m stencil thickness,

60mm/s

Page 13: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

Operating Parameters Continuous Print and Abandon Stability Assessment

Paste

added to stencil

Paste

kneaded

Dry under

stencil wipe

1hr pausePrint 5 PCBsPrint 5 PCBs

• Printing

• DEK Europa

• Stainless steel, laser cut

• 100m thickness

• Vacuum tooling

• 250mm, 60 squeegee

• 60mm/s squeegee speed

• 20mm/s separation speed

• Conditions Typical, 22C, 40% RH

• Koh Young KY-8020T volume measurement

Print 15 PCBs,

dry wipe every 5

2hr pause

Volumes

Measured

Blank stencil

1000 or 2000

cycles

Print 15 PCBs,

dry wipe every 5

Volumes

Measured

October 23, 2015 Engineering Manual GC 10 Solder Paste13

Henkel Board 0.8mm BGA to 0.15mm diameter circles Process flow for Henkel print test as shown below

Page 14: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

Operating ParametersPrinting

October 23, 2015 Engineering Manual GC 10 Solder Paste14

• GC 10 solder pastes show exceptional print quality

• On 0.18mm diameter fine pitch devices only one knead stroke is required after 2hour machine down times

• On coarser pitch deposits it is expected that the first print after abandon can in normal circumstances be

perfectly acceptable for production quality

0402 0201 01005

0.4mm TQFP120 0.5mm CSP56 0.4mm BGA432

Page 15: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste15

0.15

mm diam

0.18

mm diam

0.20

mm diam

0.22

mm diam

0.5B

GA (0

.266

mm ap)

0.4m

mCS

P56 (0.30m

m ap)

0.8B

GA

5

4

3

2

1

0

Cp

k

1.33 ref1.67 ref

initial

1hr

2hr

2hr + 1 knead

Variable

Abandon Time 1hr, 2hr, 2hr +1 kneadGC10 T4

Operating Parameters – Abandon Stability 22C/40%RH Print Process Window (LOCTITE GC 10 SAC305 T4 885V)

• Excellent printing in the range down to 0.18mm round apertures

• Single knead cycle required after 2hr abandon at 0.18mm round apertures

0.8mm BGA – 0.15mm round apertures, (100µm stencil)

100m stencil thickness, 60mm/s, Fast separation, 250mm squeegee, 8kg

Page 16: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste16

Operating Parameters – Abandon Stability 30C/50%RH Print Process Window (LOCTITE GC 10 SAC305 T4 885V)

0.15

mm diam

0.18

mm diam

0.20

mm diam

0.22

mm diam

0.5B

GA (0

.266

mm ap)

0.4m

mCS

P56 (0

.30m

m ap)

0.8B

GA

5

4

3

2

1

0

Cp

k

1.33 ref1.67 ref

initial

1hr

2hr

2hr + 1 knead

Variable

GC10 T4 30C/50%RH

Abandon Time 1hr, 2hr, 2hr + 1 knead

• Excellent abandon time resistance

• No knead cycle required after 2hrs abandon down to 0.20mm round apertures.

• Single knead stroke required after 2hr abandon at 0.18mm round apertures

0.8mm BGA – 0.15mm round apertures, (100µm stencil)

100m stencil thickness,60mm/s, Fast separation, 250mm squeegee, 8kg

Page 17: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste17

Operating Parameters – Continuous Print Stability Print Process Window (LOCTITE GC 10 SAC305 T4 885V)

0.15

mm diam

0.18

mm diam

0.20

mm diam

0.22

mm diam

0.5B

GA (0

.266

mm ap)

0.4m

mCS

P56 (0.30m

m ap)

0.8B

GA

5

4

3

2

1

0

Cp

k

1.33 ref1.67 ref

initial

1000 cycles

2000 cycles

Variable

GC10 T4

Continuous Print Stability 1000 cycles, 2000 cycles

• No impact on print performance after 4 hours (1000 cycles) and 8 hours (2000 cycles) printing

0.8mm BGA – 0.15mm round apertures, (100µm stencil)

100m stencil thickness, 60mm/s, Fast separation, 250mm squeegee, 8kg

Page 18: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

200010000

0.38

0.36

0.34

0.32

0.30

0.28

Cycles

Min

imu

m G

ap

no

t B

rid

ge

d (

mm

)

22°C, 30%RH

30°C, 40-50%RH

Conditions

IPC Slump @ 182C After Continuous Printing0.63mm x 2.03mm, 200um stencil thickness

Operating ParametersPaste Properties After Continuous Printing

200010000

300

250

200

150

100

50

0

Cycles

10

rpm

(P

a.s

)

22°C, 30%RH

30°C, 40-50%RH

Conditions

Viscosity after Continuous Print

200010000

1.0

0.8

0.6

0.4

0.2

0.0

Cycles

TI

22°C, 30%RH

30°C, 40-50%RH

Conditions

TI Change After Continuous Print

October 23, 2015 Engineering Manual GC 10 Solder Paste18

200010000

0.4

0.3

0.2

0.1

0.0

Cycles

Min

imu

m G

ap

no

t B

rid

ge

d (

mm

)

22°C, 30%RH

30°C, 40-50%RH

Conditions

0.33mm x 2.03mm, 200um stencil thickness

IPC Slump @ 182C After Continuous Printing

Page 19: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste19

Operating ParametersSlump

• Slump evaluation was performed in accordance with J-STD-005A, IPC-TM-650 2.4.35

• First spacing with no bridge recorded after 10 minutes at 182C (35C below melting point 217C)

Stencil

Design/

thickness

A 21

200m

A 20

100m

Aperture 0.63 x

2.03mm

0.33 x

2.03mm

0.33 x

2.03mm

0.20 x

2.03mm

Pass

mark0.63mm 0.30mm 0.30mm 0.25mm

GC 10

25C0.33mm 0.10mm 0.08mm 0.075mm

GC 10

182C0.33mm 0.20mm 0.15mm 0.125mm

A21

200m

A20

100m

Page 20: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

Operating ParametersTack Force

Preload 300g

Preload time 5 secs

Retraction Speed 2.5mm/sec

Deposit diameter 5.1mm

Deposit height 0.25mm

October 23, 2015 Engineering Manual GC 10 Solder Paste20

• Slump Tackiness evaluation was performed in accordance with

J-STD-005A, IPC-TM-650 2.4.44

• GC 10 tack-life >48hours

Malcom TK1 Tackiness Tester

Page 21: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste21

Operating ParametersSolder Balling

Initial

Preferred Pass

• Solder balling performance as been assessed in accordance with

an extended version of IPC-TM-650 2.4.4.3

• Clear and colourless residues observed post-reflow

24hrs 25C 50% RH

Preferred Pass

Page 22: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste22

Operating ParametersReflow Process Window (Air)

Profile 1 2 3 4

Peak Temp (°C) 244 254 260 255

Time to Peak (min) 3.3 4.5 5.1 6.0

Soak Time (150-200°C) (min)

(No

Soak)

1.0

2.35 2.80 3.44

Time above Liquidus (min) 0.62 1.46 1.75 1.45

Time above Liquidus (sec) 37.2 87.6 105.0 87.0

• LOCTITE GC 10 solder paste offers halogen containing reflow performance in a

truly halogen free formulation

• GC 10 shows excellent coalescence onto a range of PCB and component finishes

especially during long-hot profiles

• There is no single profile that works for all applications and each process should be

assessed individually, under laboratory conditions the following profiles have been

found to give good results

• These process window guidelines are suitable for Type 4 SAC powder

76543210

300

250

200

150

100

50

0

Time (minutes)

Te

mpe

r at u

r e( °

C) 217°C

Profile 1

Profile 2

Profile 3

Profile 4

Reflow Profiles

Page 23: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

Operating Parameters (Reflow)

October 23, 2015 Engineering Manual GC 10 Solder Paste23

1 2 3 4

0.5

mm

CS

P5

60

20

10

40

2

Reflow Profile

76543210

300

250

200

150

100

50

0

Time (minutes)

Te

mp

er

atu

re

C)

217°C

Profile 1

Profile 2

Profile 3

Profile 4

Reflow Profiles

Page 24: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

Operating Parameters (Reflow)

October 23, 2015 Engineering Manual GC 10 Solder Paste24

1 2 3 4

Overp

rinte

d0.4

mm

TQ

FP

120

0.4

mm

TQ

FP

120

Reflow Profile

76543210

300

250

200

150

100

50

0

Time (minutes)

Te

mp

er

atu

re

C)

217°C

Profile 1

Profile 2

Profile 3

Profile 4

Reflow Profiles

Page 25: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

Operating Parameters (Reflow)

October 23, 2015 Engineering Manual GC 10 Solder Paste25

1 2 3 4

0.5

mm

CS

P56

0.4

mm

TQ

FP

120

0.4

mm

TQ

FP

120

Reflow Profile

76543210

300

250

200

150

100

50

0

Time (minutes)

Te

mp

er

atu

re

C)

217°C

Profile 1

Profile 2

Profile 3

Profile 4

Reflow Profiles

Page 26: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

Operating Parameters (Reflow)

October 23, 2015 Engineering Manual GC 10 Solder Paste26

1 2 3 4

01005

Capacitors

01005 R

esis

tors

Reflow Profile

76543210

300

250

200

150

100

50

0

Time (minutes)

Te

mp

er

atu

re

C)

217°C

Profile 1

Profile 2

Profile 3

Profile 4

Reflow Profiles

Page 27: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

6543210

300

250

200

150

100

50

0

Time (min)

Te

mp

era

ture

(°C

) 217°C

Profile 2

• No change to reflow performance after 8hours

printing (2000 print cycles)

October 23, 2015 Engineering Manual GC 10 Solder Paste27

Operating Parameters (Reflow)Paste Properties After Continuous Printing

1,000 cycles

22°C, 30%RH

2,000 cycles

22°C, 30%RH

1,000 cycles

30°C, 40-50%RH

0.5

mm

CS

P6.5

mm

Overp

rint

Page 28: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste28

Operating Parameters (Reflow – GC10)

Reflow Profile

1 2

01005 R

esis

tors

01005 R

esis

tors

0.5

mm

CS

P &

0.4

mm

QF

P

6543210

250

200

150

100

50

Time (minutes)

Te

mp

era

tu

re

C)

217°C

Profile 1

Profile 2

Reflow Profiles

Page 29: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

Operating ParametersVoiding

GC 10 meets IPC7095B class 3

Profile 4Profile 3Profile 2Profile 1

20

15

10

5

0

IPC

Vo

idin

g %

Class 2

Class 1

Class 3

Boxplot of IPC Voiding Percentage

Profile 4Profile 3Profile 2Profile 1

0.50

0.45

0.40

0.35

0.30A

ve

rag

e D

iam

ete

r (m

m)

Boxplot of Void Size

October 23, 2015 Engineering Manual GC 10 Solder Paste29

• Void performance assessed using 4 different reflow profiles

• GC 10 shows low levels of voiding over a range of profiles

• Void Percentage analysed in accordance with IPC7095B

76543210

300

250

200

150

100

50

0

Time (minutes)

Te

mp

era

tu

re

C)

217°C

Profile 1

Profile 2

Profile 3

Profile 4

Reflow Profiles

Page 30: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

76543210

300

250

200

150

100

50

0

Time (minutes)

Te

mp

er

atu

re

C)

217°C

Profile 1

Profile 2

Profile 3

Profile 4

Reflow Profiles

Board

Stencil 100m

Pads 500 pads per board, 2 boards tested

Probe 0.9mm 4 point plain crown light spring probe 100g spring force

Profiles 4 reflow profiles

No. of reflow 1, 2, 3 & 4 passes through oven

Atmosphere Air & 1000ppm O2

Time after reflow 1 day, 1 week

October 23, 2015 Engineering Manual GC 10 Solder Paste30

Before

Test

Operating ParametersPin Testing

After

Test

Page 31: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

76543210

300

250

200

150

100

50

0

Time (minutes)

Te

mp

er

atu

re

C)

217°C

Profile 1

Profile 2

Profile 3

Profile 4

Reflow Profiles

October 23, 2015 Engineering Manual GC 10 Solder Paste31

1 2 3 4

1 r

eflow

2 r

eflow

s3

reflow

s

Reflow Profile (% after 1000 tests)

Operating ParametersPin Testing

4 r

eflow

s

100% 100% 100% 99.5%

100%

99.9%

99.9%

100%

100%

100% 100%

100%

99.6% 99.9%

98.9%

98.5%

Page 32: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

76543210

300

250

200

150

100

50

0

Time (minutes)

Te

mp

er

atu

re

C)

217°C

Profile 1

Profile 2

Profile 3

Profile 4

Reflow Profiles

Operating ParametersPin Testing

October 23, 2015 Engineering Manual GC 10 Solder Paste32

Reflow

ed in N

21 d

ay

aft

er

reflow

1 w

eek a

fter

reflow

1 2 3 4

Reflow Profile (% after 1000 tests)

100%

99.6%99.3%99.8%

99.6%99.8%99.9%

100% 100% 100%

100%

100%

Page 33: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

Operating ParametersSurface Finish

October 23, 2015 Engineering Manual GC 10 Solder Paste33

OS

P F

inis

hS

ilver

Fin

ish

Tin

Fin

ish

1 2 3 4

Reflow Profile (0.5mm CSP56)

76543210

300

250

200

150

100

50

0

Time (minutes)

Te

mp

er

atu

re

C)

217°C

Profile 1

Profile 2

Profile 3

Profile 4

Reflow Profiles

Page 34: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste34

Operating ParametersSurface Finish

OS

P F

inis

hS

ilver

Fin

ish

Tin

Fin

ish

1 2 3 4

Reflow Profile (0201)

76543210

300

250

200

150

100

50

0

Time (minutes)

Te

mp

er

atu

re

C)

217°C

Profile 1

Profile 2

Profile 3

Profile 4

Reflow Profiles

Page 35: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste35

Operating ParametersSurface Finish

OS

P F

inis

hS

ilver

Fin

ish

Tin

Fin

ish

1 2 3 4

Reflow Profile (0402)

76543210

300

250

200

150

100

50

0

Time (minutes)

Te

mp

er

atu

re

C)

217°C

Profile 1

Profile 2

Profile 3

Profile 4

Reflow Profiles

Page 36: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste36

Operating ParametersSurface Finish

OS

P F

inis

hS

ilver

Fin

ish

Tin

Fin

ish

1 2 3 4

Reflow Profile (6.5mm overprint)

76543210

300

250

200

150

100

50

0

Time (minutes)

Te

mp

er

atu

re

C)

217°C

Profile 1

Profile 2

Profile 3

Profile 4

Reflow Profiles

Page 37: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

GC 10 meets IPC7095B class 3

Operating ParametersVoiding Different Surface Finishes 0.5mm CSP56

October 23, 2015 Engineering Manual GC 10 Solder Paste37

• Void performance on OSP Cu and Immersion Sn surface finishes assessed using 4

different reflow profiles

Finish

Profile

OSP CuImm Sn

Profile 4Profile 3Profile 2Profile 1Profile 4Profile 3Profile 2Profile 1

20

15

10

5

0

IPC

Vo

idin

g %

Class 3

Class 2

Class 1

Boxplot of IPC Voiding Percentage

Finish

Profile

OSP CuImm Sn

Profile 4Profile 3Profile 2Profile 1Profile 4Profile 3Profile 2Profile 1

0.50

0.45

0.40

0.35

0.30A

ve

rag

e D

iam

ete

r (m

m)

Boxplot of Void Size

76543210

300

250

200

150

100

50

0

Time (minutes)

Te

mp

er

atu

re

C)

217°C

Profile 1

Profile 2

Profile 3

Profile 4

Reflow Profiles

Page 38: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste38

1. Performance Summary

2. Introduction: Properties, Features & Benefits

3. Operating Parameters

• Printing: Process Window

• Printing: Continuous and Abandon Time Testing

• Slump Testing

• Tack-Life Force

• Reflow Process Window

• Reflow Performance Testing

• Voiding Data

4. Reliability and Specification Testing

5. Operating Parameters: Storage

• Printing & Reflow Performance

6. Product Summary

Contents

Page 39: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

Reliability and Specification TestingHead- in Pillow Test

Copper plate

Solder paste

Solder sphere

250+/-5˚C

Place a solder

sphere onto

printed paste

refere

nce pa

ste G

refere

nce pa

ste F

refere

nce pa

ste E

refere

nce pa

ste D

refere

nce pa

ste C

referenc

e pa

ste B

refere

nce pa

ste A

GC10

1mth 40°

C

GC10

Initial

18

16

14

12

10

8

6

4

2

0

Paste

Av

era

ge

Tim

e (

s)

Head In PillowTime to First Defect

October 23, 2015 Engineering Manual GC 10 Solder Paste39

First

250+/-5˚C

…..Initial 10sec 20sec…..1st sphere 2nd sphere 3rd sphere Defect

• Print solder paste on a Cu plate, 0402 pad, stencil thickness 125 m.

• When the solder paste starts to melt, place a solder sphere (SAC305,

0.76mm diameter) on the printed solder paste

• Place another sphere after 3sec, 6 sec, 9sec… until the solder sphere

no-longer coalesces

Page 40: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

Standard Test Result

ANSI/

J-STD-004B

Cu CorrosionPass

Cu MirrorPass

Halogen Pass (no added halogen)

Surface Insulation Resistance Pass6.0x1011 Ohms after 7days

Electromigration Pass 5.0x1010 Ohms after 21days

GC 10 Control

October 23, 2015 Engineering Manual GC 10 Solder Paste40

GC 10 J-STD-004B classification ROL0

Reliability and Specification TestingHead- in Pillow Test

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October 23, 2015 Engineering Manual GC 10 Solder Paste41

Reliability and Specification Testing3rd Party Testing

• SGS report for GC 10

• Sample reflowed flux residue

• Reference EN14582/IC Analysis

• To meet halogen free requirements

• Br<900ppm, Cl <900ppm, and combined <1500ppm

• Halogen – Fluorine - ND

• Halogen – Chorine - ND

• Halogen – Bromine – ND

• Halogen – Iodine – ND

GC 10 has no detectable halogen and is designated as halogen free

Page 42: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

Reliability and Specification TestingIPC J-STD 004B

October 23, 2015 Engineering Manual GC 10 Solder Paste42

6543210

250

200

150

100

50

Time (minutes)

Tem

p er a

tur e

( °C)

217°C

Profile 1

Profile 2

Reflow Profiles

12

11.5

11

10.5

10

9.5

9

Lo

g S

IR L

og

Oh

ms

GC10 Emig IPC-TM-650 2.6.14.1

Profile 1 Profile 2 Blank Control

Reflow profile

4 days 21 days Passmark (decrease by a factor of 10)

GC10 SIR IPC-TM-650 2.6.3.7

Lo

g S

IR L

og

Oh

ms

12.5

12.5

11.5

11

10.5

10

9.5

9

8.5

8

7.5

0 1 2 3 4 5 6 7

Time days

Profile 1 nitrogen

Profile 2 nitrogen

Blank control

Profile 1 Air

Profile 2 air

Pass

Page 43: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste43

1. Performance Summary

2. Introduction: Properties, Features & Benefits

3. Operating Parameters

• Printing: Process Window

• Printing: Continuous and Abandon Time Testing

• Slump Testing

• Tack-Life Force

• Reflow Process Window

• Reflow Performance Testing

• Voiding Data

4. Reliability and Specification Testing

5. Operating Parameters: Storage

• Printing & Reflow Performance

6. Product Summary

Contents

Page 44: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste44

Operating Parameters: StoragePrinting After Storage 1month 40C

ContinuousAbandon Time

5

4

3

2

1

0

Test

Cp

k

1.33 ref

1.67 ref

initial

1000 cycles

1hr abandon

2hr abandon

Variable

Continuous Print & Abandon Time After StorageGC10 T4 1 month 40C

• Excellent print capability after storage for 1 month @ 40C

• No knead cycle required after 2hrs abandon down to 0.20mm round apertures

0.4mm BGA ,100m stencil thickness, 60mm/s, Fast separation,

250mm squeegee, 8kg

Page 45: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

ContinuousAbandon Time

5

4

3

2

1

0

Test

Cp

k

1.33 ref

1.67 ref

initial

1000 cycles

1hr abandon

2hr abandon

Variable

Continuous Print & Abandon Time After StorageGC10 T4 6 month 25C

October 23, 2015 Engineering Manual GC 10 Solder Paste45

Operating Parameters: StoragePrinting After Storage 6months 25C

• Excellent print capability after storage for 6 months @ 25C

• No knead cycle required after 2hrs abandon down to 0.20mm round apertures

0.4mm BGA ,100m stencil thickness, 60mm/s, Fast separation,

250mm squeegee, 8kg

Page 46: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

ContinuousAbandon Time

5

4

3

2

1

0

Test

Cp

k

1.33 ref

1.67 ref

initial

1000 cycles

1hr abandon

2hr abandon

Variable

Continuous Print & Abandon Time After StorageGC10 T4 12 month 25C

October 23, 2015 Engineering Manual GC 10 Solder Paste46

Operating Parameters: StoragePrinting After Storage 12months 25C

• Excellent print capability after storage for 12 months @ 25C

• No knead cycle required after 2hrs abandon down to 0.20mm round apertures

0.4mm BGA ,100m stencil thickness, 60mm/s, Fast separation,

250mm squeegee, 8kg

Page 47: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

Operating Parameters: Storage

6543210

300

250

200

150

100

50

0

Time (min)

Te

mp

era

ture

(°C

) 217°C

Profile 2

October 23, 2015 Engineering Manual GC 10 Solder Paste47

Initial 1m 40°C 6m 25°C

0.5

mm

CS

P0

20

10

40

2

After Paste storage

Page 48: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

Operating Parameters: StorageAfter storage and 2nd side/pre-reflow

October 23, 2015 Engineering Manual GC 10 Solder Paste48

Initial 1 Month 40°C Initial 1 Month 40°C

Fre

sh P

CB

Pre

-reflow

ed P

CB

0.5mmCSP 0201

6543210

300

250

200

150

100

50

0

Time (min)

Te

mp

er

atu

re

C)

217°C

Profile 3

Page 49: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste49

1. Performance Summary

2. Introduction: Properties, Features & Benefits

3. Operating Parameters

• Printing: Process Window

• Printing: Continuous and Abandon Time Testing

• Slump Testing

• Tack-Life Force

• Reflow Process Window

• Reflow Performance Testing

• Voiding Data

4. Reliability and Specification Testing

5. Operating Parameters: Storage

• Printing & Reflow Performance

6. Product Summary

Contents

Page 50: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

October 23, 2015 Engineering Manual GC 10 Solder Paste50

GC 10: Performance Summary

Flux

• Halogen-free flux: passes IC with pretreatment IPC-TM-650

2.3.34/EN14582

• Halogen-free flux classification: ANSI/J-STD-004 Rev. B for

a type ROL0 classification

Paste

• Suitable for fine pitch, high speed printing up to 125mm/s (5”/s)

• Optimized for long hot soak reflow profiles

• Excellent fine pitch coalescence in air & nitrogen atmosphere

• Excellent humidity resistance

• Excellent solderability on challenging surface finishes,

including CuNiZn

• Colorless residues for easy post-reflow inspection

• Long 12month shelf-life when stored below 26.5C

Page 51: Engineering Manual HF212 Solder Paste - OEM …media.oem.se/.../pdf/henkel_ae_gc10_engineering_manual.pdf · Engineering Manual LOCTITE GC 10 T4 Solder Paste ... Operating Parameters

Thank you!