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ACCESSORIES CATALOG ELECTROCHEMISTRY CORROSION CELL ANALYTICAL CELL GLASSWARE ELECTRODES ROTATING RING-DISK ELECTRODE SPECTROELECTROCHEMISTRY QUARTZ CRYSTAL MICROBALANCE BATTERY HOLDERS FARADAY CAGE MEMBRANE FOR FUEL CELL CONNECTION ACCESSORIES

ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

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Page 1: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

ACCESSORIES CATALOGELECTROCHEMISTRY

CORROSION CELL

ANALYTICAL CELL

GLASSWARE

ELECTRODES

ROTATING RING-DISK ELECTRODE

SPECTROELECTROCHEMISTRY

QUARTZ CRYSTAL MICROBALANCE

BATTERY HOLDERS

FARADAY CAGE

MEMBRANE FOR FUEL CELL

CONNECTION ACCESSORIES

Page 2: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

Bio-Logic SAS (founded in 1983)

is located near Grenoble in the French Alps.

We design and manufacture high performance, research

laboratory instruments for electrochemistry and

fuel cell testing. Bio-Logic’s product range

is based on a modular and flexible design.

We offer potentiostat workstations from single channel

up to 16 channel systems, integrating EIS capability and

high current boosters.

ELECTROCHEMISTRY ACCESSORIES2

CONTENTS

Page 3: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

Analytical cell kit Small volume cells 4 Large volume cells 6 Flow cells 7 Interdigitated array (IDA) electrodes 8 Ring disk type electrodes 8 Screen printed electrodes 9

Corrosion cell kit Standard corrosion cells 10 Avesta cell 11 Flat cells, 1 to 10 cm² sample area 12 Galvanic cells, 1 to 10 cm² sample area 13 Plate material evaluating cell, up to 1 cm² sample area 13

Glassware Small volume cell vials, 1 to 100 mL 14 Big volume cell vials, 100 to 2.000 mL 14 Small size bridge tubes 16 Bridge tubes for corrosion cells 16 Purge tubes for corrosion cells 16 Bridge tubes for analytical cells 17 Purge tubes for analytical cells 17 Bridge tubes with ceramic junction 17

Electrodes Working electrodes 18 Reference electrodes 20 Counter electrodes 24

Rotating ring disk electrode Rotating ring disk electrode RRDE-3A 26 Working electrode tips 27

Spectroelectrochemistry Three utilization modes & two spectrometers 28 Static experiment 30 Flow experiment 31

Quartz Crystal Analyzer EQCM 32 biosensor QCM 34

Battery accessories Battery holder 36 Coin cell holder 36 Sense adapter module SAM-50 36

Faraday cages 37

Fuel cell Membrane electrode assemblies (MEA) 38 Semi-automatic filling kit 39 Educational kit 39

Connection accessories Multi-electrode investigations cables 40 Specific cables 41 Test boxes 42 External device connection 42 Connectors 43 Miscellaneous 43

Softcurrent

modularpotentio

statsgalvano

BioLogic

3

CONTENTS

Page 4: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

Each voltammetry cell is designed for a specific application (specific working electrode, volume of solution, oxygen free condition...). For example, for voltammetry investigations using standard working electrode with an outer diameter (OD) of 6 mm the fixed configuration of SVC-3 kit is recommended.For application requiring other working electrode shape, SVC-2 is more suitable.If only a small amount of the electroactive compound is available, SVC-2 in the microvolume mode is recommended.

Small volume cells

ANALYTICAL CELL KIT

ELECTROCHEMISTRY ACCESSORIES4

For electrode with OD of 10 mm

Small amount of solution (200 μL in the sample holder)

oxygen free modeSVC-2 modularity: microvolume mode

For electrode with OD of 6 mm

For microelectrode with OD of 4 mm

AnalyticalAnalytical

Platinum cyclic voltammetry

Page 5: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

Note that a complete analytical special kit SK-2 (A-012763) is also proposed, but the reference electrode has to be purchased separately.This kit includes:

SVC-3 kit (A-012669), PK-3 polishing kit (A-011975), one glassy carbon electrode, OD 6.0 mm, ID 3.0 mm (A-002012), one platinum electrode, OD 6.0 mm, ID 1.6 mm (A-002013).

5

Catalog No. Catalog No. Catalog No. Catalog No.A-012668 A-012669 A-011224 A-001197

ContentsSample vial A-001056 20 mL, qty 7 A-001056 20 mL, qty 7 A-011504 5 mL, qty 7 A-012632 100 mL, qty 1Counter electrode A-002222 5.7 cm A-002233 5 cm A-002222 5.7 cm A-002234 23 cmTeflon cap A-012670 A-012671 A-011226 A-012551Purge tube (ETFE), 1 m A-010537 A-010537 A-010537 A-010537Additional items adapter 10 to 6 A-011227 cell holder A-010530 porous carbon electrode

A-001198 Lid for CEA-001196 chamber for CEA-001236 O-ringA-009131 port plugA-000178 stirrer bar

OptionalSample holder A-012177 9.0 mm, qty 2 A-012176 6.0 mm, qty 2Cell holder A-001209 for 20 mLWorking electrode see page 18 see page 18 see page 18Reference electrode see page 20 see page 20 see page 20 see page 20Teflon cap 10.2 mm

1.6 mm

6.2 mm

1.65 mm

6.3 mm

1.6 mm

6.2 mm

1.6 mm

The geometry of the cell should be optimized to reduce the ohmic drop. Working and reference electrodes have to be close to each other. The surface area of the counter electrode has to be higher than the surface area of the working electrode.

Cell geometry

SVC-2 Modular

SVC-3 For a volume of 5 to 20 mL, only for working electrode with OD of 6 mm.

Bulk electrolysis cellFor a volume of 100 mL.

VC-4For a volume of 1 to 3 mL, only for working electrode with OD of 6 mm.

cell kit

OD: outer diameter ID: inner diameter

Page 6: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

EL-A-012

EL-A-009

EL-A-008

EL-A-005

EL-A-003

EL-A-004EL-A-002

ANALYTICAL CELL KIT

ELECTROCHEMISTRY ACCESSORIES6

This analytical cell with volumes from 50-200 mL is well adapted for macro electrochemistry applications. Two packages are offered:

the standard analytical cell kit the complete analytical cell kit (which allows temperature control and gas purging).

Other volumes are available on request.

Large volume cells

Catalog No.Standard analytical cell kit (80 mL) EL-ELECTRO-1

Complete analytical cell kit (80 mL) EL-ELECTRO-2

Glass cell 80 mL EL-A-001Double jacketed glass cell 80 mL EL-A-002Teflon cap 5 holes EL-A-003Teflon ring (silicon encapsulated, OD 10.2 cm) EL-A-004Cell collar with clamp EL-A-005Double purge tube EL-A-006Bridge tube for reference electrode with OD of 6 mm EL-A-008Pt counter electrode EL-A-009Purge tube EL-A-016Reference electrode A-002056Double nut 25 mm and 12 mm diameter EL-A-011Telescopic cell stand EL-A-012

OptionsElectrode bridge extension for electroanalytical cell EL-A-022Bridge tube for reference electrode of OD 8 mm EL-A-017PT100 probe (indicate connector type) EL-C-014Magnetic stirrer & heater, without PT100 probe

220 V EL-C-015A110 V EL-C-015B

Aluminum base holder for magnetic stirrer EL-C-018

AnalyticalAnalytical

EL-A-022

Page 7: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

7

Flow cells

Catalog No. Item DescriptionCross flow A-001000 glassy carbon electrode Ø 3 mm x 2 (dual type), size 25 x 25 mm

A-001002 gold electrode Ø 3 mm x 2 (dual type), size 25 x 25 mmA-001012 platinum electrode Ø 3 mm x 2 (dual type), size 25 x 25 mmA-001008 silver electrode Ø 3 mm x 2 (dual type), size 25 x 25 mmA-001004 carbon paste electrode Ø 3 mm x 2 (dual type), size 25 x 25 mmA-001009 nickel electrode Ø 3 mm x 2 (dual type), size 25 x 25 mmA-001006 glassy carbon/gold electrode Ø 3 mm x 2 (dual type), size 25 x 25 mmA-012583 glassy carbon/platinum electrode Ø 3 mm x 2 (dual type), size 25 x 25 mmA-001046 TG-2M teflon gasket (4 pieces) film thickness 12 μmA-001047 TG-5M teflon gasket (4 pieces) film thickness 25 μmA-001048 TG-6M teflon gasket (4 pieces) film thickness 50 μmA-001049 TG-8M teflon gasket (4 pieces) film thickness 100 μmA-001092 TG-11M silicon gasket (4 pieces) film thickness 500 μmA-001093 TG-12M silicon gasket (4 pieces) film thickness 1 000 μmA-001032 cross flow cell block material PEEK

Radial flow A-001016 glassy carbon electrode Ø 6 mm (single type), size 25 x 25 mmA-012124 glassy carbon electrode Ø 3 mm (single type), size 25 x 25 mmA-009908 platinum electrode Ø 3 mm (single type), size 25 x 25 mmA-011155 gold electrode Ø 3 mm (single type), size 25 x 25 mmA-000999 PFCE carbon electrode Ø 3 mm (single type), size 25 x 25 mmA-010251 carbon paste electrode Ø 3 mm (single type), size 25 x 25 mmA-001146 TG-2MR teflon gasket (4 pieces) film thickness 12 μmA-001147 TG-5MR teflon gasket (4 pieces) film thickness 25 μmA-001148 TG-6MR teflon gasket (4 pieces) film thickness 50 μmA-012802 TG-8MR teflon gasket (4 pieces) film thickness 100 μmA-001192 TG-11MR teflon gasket (4 pieces) film thickness 500 μmA-001193 TG-12MR teflon gasket (4 pieces) film thickness 1 000 μmA-001031 radial flow cell block material PEEK

Cross/radial A-012169 RE-3V Ag/AgCl reference electrode screw type size Ø 10 x 48 mmA-001531 1/16" PEEK tube ID 0.25 mm, length 3.0 mA-004130 dynaseal PEEK fingertight (10 pieces) screw for pipe connecting integrated 1/16"

Catalog No.Cross flow cell A-012798Gasket, working and reference electrodes are sold separately

Catalog No.Radial flow cell A-012799Gasket, working and reference electrodes are sold separately

Single/radial flow

Dual, series/cross flow

Dual, parallel/cross flow

Cross flow cell Radial flow cell

INLET OUTLET

gasket detector gasket detector

INLETOUTLET

OUTLETflow channel

Schematic diagram Schematic diagram

cell kit

Page 8: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

ANALYTICAL CELL KIT

ELECTROCHEMISTRY ACCESSORIES8

AnalyticalAnalytical

Catalog No. Width Interval Length Number of feet Film thicknessIDA electrode Au A-012257 2 μm 2 μm 2 mm 65 pairs 90 nm

Pt A-012258 2 μm 2 μm 2 mm 65 pairs 90 nmAu without passivation membrane A-012261 2 μm 2 μm 2 mm 65 pairs 90 nmPt without passivation membrane A-012264 2 μm 2 μm 2 mm 65 pairs 90 nmAu A-012129 3 μm 3 μm 2 mm 65 pairs 90 nmPt A-012130 3 μm 3 μm 2 mm 65 pairs 90 nmAu without passivation membrane A-012260 3 μm 3 μm 2 mm 65 pairs 90 nmPt without passivation membrane A-012263 3 μm 3 μm 2 mm 65 pairs 90 nmAu A-012125 10 μm 5 μm 2 mm 65 pairs 90 nmPt A-012126 10 μm 5 μm 2 mm 65 pairs 90 nmITO A-012128 10 μm 5 μm 2 mm 65 pairs 100 ± 20 nmcarbon A-012127 10 μm 5 μm 2 mm 65 pairs 1200 ± 100 nmAu without passivation membrane A-012259 10 μm 5 μm 2 mm 65 pairs 90 nmPt without passivation membrane A-012262 10 μm 5 μm 2 mm 65 pairs 90 nmITO without passivation membrane A-012265 10 μm 5 μm 2 mm 65 pairs 100 ± 200 nmcarbon without passivation membrane A-012266 10 μm 5 μm 2 mm 65 pairs 1200 ± 100 nm

OptionsCable kit for IDA electrode A-011066Ag/AgCl ink for reference electrode (2.0 mL) A-011464

Interdigitated array (IDA) electrodes

Ring disk type electrodes

3 μm

10 μm

Catalog No. Ring OD Ring ID DiskGold ring disk electrode (3 pieces) A-002081 6 mm 4 mm 3 mmPlatinum ring disk electrode (3 pieces) A-002082 6 mm 4 mm 3 mmCarbon ring disk electrode (3 pieces) A-002083 6 mm 4 mm 3 mm

20

Counter electrode

Passivation membrane

Reference electrode

Working electrode #1

Working electrode #2

Quartz plate, thickness = 0.5 mm 12

2

Page 9: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

9

cell kit

Screen Printed Electrodes

Dimensions in mm

Screen Printed Electrode (SPE) are low cost and disposable. They include one reference electrode, one counter electrode and one or several working electrodes according to the design needed.The working electrode can be made of glassy carbon, platinum, gold…The SPE allows user to work with a small amount of solution (25-100 μL).A two–electrodes set-up is used for multi working electrode SPE with one shared reference electrode and one shared counter electrode.

Note with BioLogic’s multichannel potentiostats, it is possible to run simultaneously investigation on each working electrode of the array (up to 16).

Catalog No. Working electrode Counter electrode Reference electrode Substrat3-electrode Ø of WE: 2 mm

size of RE: 0.5 x 1 mmratio CE/WE surface area: 4/1overall dimension: 50 x 10 mm 100 pieces

G-GGA graphite graphite Ag/AgCl aluminaG-GGP graphite graphite Ag/AgCl PVCG-PTGA Pt graphite Ag/AgCl aluminaG-PTGP Pt graphite Ag/AgCl PVCG-AUGA Au graphite Ag/AgCl aluminaG-AUGP Au graphite Ag/AgCl PVC

Array of 16 WE Ø of WE: 0.8 mmsize of pseudo-RE: 20 x 1 mmoverall dimension: 45 x 19 mm10 pieces

G-A-GA graphite Ag/AgCl aluminaG-A-GP graphite Ag/AgCl PVCG-A-PTA Pt Ag/AgCl aluminaG-A-PTP Pt Ag/AgCl PVCG-A-AUA Au Ag/AgCl aluminaG-A-AUP Au Ag/AgCl PVC

Counter electrode

Reference electrode

Working electrode

Three-electrode sensor Array of 16 working electrodes

Page 10: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

For corrosion applications, two packages for large volume i.e. ~1 L are available:

basic corrosion cell kit, complete corrosion cell kit (allows temperature control and includes sample holder and cell stand).

Catalog No. Basic corrosion cell kit EL-CORR-1

Complete corrosion cell kit EL-CORR-2

Glass cell 1L EL-C-001Double jacketed glass cell 1L EL-C-002Teflon cap EL-C-003Teflon ring (silicon encapsulated), OD 10.2 cm EL-C-004Cell Collar with clamp EL-C-005Double purge tube EL-C-006Graphite counter electrode rod (2 pieces) EL-C-009Double nut 25 mm and 12 mm diameter EL-C-011Telescopic cell stand EL-C-012Sample holder 1 cm2, maximum thickness of sample 10 mm,diameter included between 11.3 mm to 15.4 mm

092-C-013

Purge tube EL-C-016Bridge tube for 8 mm diameter reference electrode EL-C-017Calomel reference electrode length 80 mm, OD 8 mm screw cap

R-XR110

Cable connection for screw cap 10 cm, 2 mm banana plug R-A94L11112 mm OD conical rings for reference electrode of 8 mm R-X31M012

OptionsBridge tube for 6 mm diameter reference electrode EL-C-008PT100 probe (indicate connector type) EL-C-014Magnetic stirrer & heater, without PT100 probe EL-C-015A (220 V)

EL-C-015B (110 V)Aluminum base holder for magnetic stirrer EL-C-018

CORROSION CELL KIT

ELECTROCHEMISTRY ACCESSORIES10

Standard corrosion cells

Corrosion

EL-C-005

EL-C-003

EL-C-004EL-C-002

EL-C-017

EL-C-013

EL-C-009

Corrosion

Other volumes are available on request.

Page 11: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

Internal gasket

External gasketFilter paper ring

SampleCopper connector

INLET

Avesta cell is an electrochemical cell developed for pitting corrosion testing (ASTM G150). It is designed to avoid microcrevice corrosion formed between the working electrode and the gasket at the bottom aperture of the cell. A filter paper ring placed between the sample and the gasket is flooded by distilled water in order to eliminate crevice corrosion.The water flow is controlled by a peristaltic pump (EL-AV-008) which delivers 0.5 to 5 mL/h.

Catalog No.Avesta cell kit EL-AV-001

ContentsDouble jacketed cell glass 250 mL EL-AV-002Teflon cap 5 holes EL-AV-003O-ring PTFE silcone encapsulated El-AV-004Cell collar with clamp EL-C-005Double purge tube EL-AV-006Filter paper ring (100 units) EL-AV-007Graphite counter electrode rods (2 pieces) EL-C-009Bridge tube for RE 6 mm EL-C-010Double nut EL-C-011Telescopic cell stand EL-AV-012Skeleton EL-AV-015

OptionsPeristaltic pump for low flow EL-AV-008Bridge tube for reference electrode with OD of 8 mm

EL-AV-013

Single purge tube EL-AV-014Temperature probe PT 100 EL-C-014

11

Avesta cell

cell kit

Principle of Avesta cell

Page 12: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

This cell with a volume of 250 mL is adapted to perform AC or DC experiments on flat specimen of 1 cm2 or 10 cm2 area. This cell has a double jacket for temperature control and three holes for reference electrode, purge tube and temperature probe with inner diameter of 17.6 mm and the 2 others of 8.3 mm. Thanks to its design, any sample with a thickness inferior to 1 cm fits in the holder. Catalog No. Flat cell 1 cm2

EL-FLATFlat cell 10 cm2 EL-FLAT-2

Complete cell for flat sample 1 cm2 EL-FLAT-3Complete cell for flat sample 10 cm2 EL-FLAT-4Bridge tube EL-F-004Platinum gauze counter electrode A-702439SCE reference electrode A-002056

CORROSION CELL KIT

ELECTROCHEMISTRY ACCESSORIES12

Flat cells, 1 to 10 cm² sample area

CorrosionCorrosion

If the experiment is performed in more agressive medias such as fluorhydric acid media, it is possible to get a body of the flat cell in PVDF instead of glass.

Investigation in agressive medias

Fluorhydric acid 48%

Sulfuric acid 98%

Phosphoric acid 85%

Hydrochloric acid 35%

Nitric acid 70%

Perchlorique acid

Sodium hydroxide 50%

Potassium hydroxide concentred

Temperature 20° C 50° C 20° C 50° C 20° C 50° C 20° C 50° C 20° C 50° C 20° C 50° C 20° C 50° C 20° C 50° CTeflonPVDF*Borosilicated glass

excellent good not recommended not compatible

Catalog No.

PVDF* body EL-F-PVDFEPDM O-ring kit for 1 cm2 EL-SEAL-1

for 10 cm2 EL-SEAL-10Teflon O-ring kit for 1 cm2 EL-SEAL-T1

for 10 cm2 EL-SEAL-T10The O-ring kits include 4 O-rings for the glassware side and 10 O-rings for the sample side* Polyvinylidenefluoride

Page 13: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

Thanks to the modular design of the flat cell, it is possible to set two different materials at each end of the cell.The surface area may be 1 or 10 cm2.

Catalog No.Galvanic cell 1 cm2 EL-FLAT-3 + 092-FLAT/1

10 cm2 EL-FLAT-4 + 092-FLAT/10

Catalog No.Plate material evaluating cell A-011951

Contents: teflon cell [body &base] - O-ring - screw 20 mm - purging tube, 1 m -Pt counter electrode A-002222

13

Galvanic cells, 1 to 10 cm² sample area

This quite handy cell was developed to evaluate a plate material such as a metal, semi-conducting plate... The sample plate is sandwiched between the two cell blocks.

Plate material evaluating cell, up to 1 cm² sample area

cell kit

092-FLAT/10

Page 14: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

ELECTROCHEMISTRY ACCESSORIES14

To complete a kit, the cell vials are also offered separately. Note that other volumes are available on request.

Catalog No. Volume OD ID Height Qty PurposeSmall volume cell vials

sample vial A-011504 5 mL 18 mm 15.6 mm 30 mm 10 VC-4A-001056 20 mL 28 mm 25.6 mm 50 mm 10 SVC-2, SVC-3A-012632 100 mL 50 mm 46.4 mm 50 mm 1 RRDE-3A, bulk electrolysis

water jacketed-glass vial A-012672 5 mL 40 mm 15.6 mm 40 mm 1 VC-4A-001051 20 mL 55 mm 25.6 mm 50 mm 1 SVC-2, SVC-3A-012652 100 mL 70 mm 46.4 mm 80 mm 1 RRDE-3A, bulk electrolysis

cell holder for 20 mL vial A-001209 1 SVC-2, SVC-3Big volume cell vials

sample vial EL-A-001 80 mL 90 mm 62 mm 80 mm 1 EL-ELECTRO-1EL-C-001 1 000 mL 120 mm 90 mm 175 mm 1 EL-CORR-1

Water jacketed-glass vial EL-A-002 80 mL 90 mm 62 mm 85 mm 1 EL-ELECTRO-2EL-C-002 1 000 mL 120 mm 90 mm 200 mm 1 EL-CORR-2

cell holder for king size vial (1 L) EL-C-019 1 EL-CORR-1

GLASSWARE

Small volume cell vials, 1 to 100 mL ID 15.6

A-011504

18

30

GlasswareGlassware

EL-A-001

6290

80

EL-A-002

6290

85

Big volume cell vials, 100 to 2,000 mL

A-001209cell holder for A-011506

ID 25.6A-011506

28

50

Page 15: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

15

28

72

ID 46.4 A-012632

cell vials

A-001051

25.655

50

A-012672

40

40

15,6

A-012652

4570

EL-C-002

90120

200

175

90120

Dimensions in mm

EL-C-001

EL-C-019, cell holder for EL-C-001

Page 16: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

The tolerance of each dimension is approximately +/- 0.5 mm. The inner diameter is the size at the top side.

GLASSWARE

ELECTROCHEMISTRY ACCESSORIES16

Bridge tubes Tubes

A-012177

9

65

A-012176

6

65

Small size bridge tubes

Purge tubes for corrosion cells

EL-C-016

10

200

EL-C-006

10

100

220

Bridge tubes for corrosion cells

10 10

EL-F-004B

60

120

10

EL-C-008 EL-C-017 EL-F-004

10

60

140

250

Page 17: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

17

purge tubes

EL-A-017 EL-A-008

165

10

10

Bridge tubes for analytical cells

Bridge tubes with ceramic junction

Dimensions in mm

R-AL100 R-AL110 R-AL120

138

250

70

Purge tubes for analytical cells

EL-A-006

100

10

200

160

10

EL-A-016

Ref. electrode Catalog No. OD Height Qty PurposeSmall size bridge tube

Ø 6 mm A-012176 6 mm 68 mm 2, 22 for A-012306 SVC-2, SVC-3Ø 9 mm A-012177 9 mm 68 mm 2, 22 for A-012307 SVC-2

Bridge tube for corrosion cells

Ø 6 mm EL-C-008 10 mm 250 mm 1 EL-CORRØ 8 mm EL-C-017 10 mm 250 mm 1 EL-CORR

EL-F-004 10 mm 120 mm 1 EL-FLATEL-F-004B 10 mm 140 mm 1 EL-FLAT

Bridge tube for analytical cells

Ø 8 mm EL-A-017 10 mm 165 mm 1 EL-ELECTROØ 6 mm EL-A-008 10 mm 155 mm 1 EL-ELECTRO

Purge tube for analytical cells

single EL-A-016 10 mm 200 mm 1 EL-ELECTROdouble EL-A-006 10 mm 220 mm 1 EL-ELECTRO

Purge tube for corrosion cells

single EL-C-016 10 mm 160 mm 1 EL-CORRdouble EL-C-006 10 mm 200 mm 1 EL-CORR

Bridge tube with ceramic junction

short R-AL100 12 mm 70 mm 1standard R-AL110 8 mm 250 mm 1with reverse sleeve (non aqueous) R-AL210 8 mm 138 mm 1standard R-AL120 8 mm 138 mm 1

Option: repair kit for vycor-based bridge tubes is also offered (A-012796).

Page 18: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

ELECTRODES

ELECTROCHEMISTRY ACCESSORIES18

WorkingElectrodes

To address every application, a wide range of working electrodes (WE) is offered with a diameter going from 7 μm up to 6 mm and built with different materials.

Standard type

55

15

6

15

Long type

110

6

Small type

55

15

3

Micro type

70

4

Gauze type

23

25

10

35

To refresh the surface of the electrode we recommend to polish the electrode after each measurement.

Working electrodes maintenance Catalog No.PK-3 electrode polishing kit A-011975

Contents0.05 μm polishing alumina (20 mL) A-0010501 μm polishing diamond (10 mL) A-002054Glass plate (1 piece) A-002249Alumina polishing pad (10 pieces)Diamond polishing pad (10 pieces)

Replacement itemAlumina polishing pad (20 pieces) A-001040Diamond polishing pad (20 pieces) A-001041Emery paper UF800 (20 pieces) A-012611Coarse polishing pad (20 pieces) A-001042

Working electrode maintenance

Working electrodes

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19

Dimensions in mm

electrodespH =0Pt

pH = 7pH = 14

TBAP/DMF

1 M HCIO4C0.1 M KCI

TBAP/ACN

-2-3 -1 0 1 2 3

V vs SCE

Electroactivity window of the working electrodes in different media

Catalog No. Isolation Type OD Electrode sizeCarbon LGCE glassy carbon electrode A-012744 PEEK long 6 mm 3 mm

GCE glassy carbon electrode A-002417 PEEK standard 10 mm 5 mmA-002012 PEEK standard 6 mm 3 mmA-012297 PEEK standard 6 mm 1.6 mmA-002411 PEEK standard 6 mm 1 mm

SGCE glassy carbon electrode A-012298 PEEK small 3 mm 1.6 mmA-002412 PEEK small 3 mm 1 mm

MCE micro carbon fiber electrode A-002002 glass micro 4 mm 33 μm A-002007 glass micro 4 mm 7 μm

Pyrolytic graphite electrode Basal Plane A-002252 PEEK standard 6 mm 3 mm

Edge Plane A-002253 PEEK standard 6 mm 3 mm

PFCE carbon electrode A-002408 PEEK standard 6 mm 3 mmA-002409 PEEK standard 6 mm 1 mm

SPFCE carbon electrode A-011854 PEEK small 3 mm 1 mm

Platinum Platinum gauze electrode A-002250 PEEK gauze 80 mesh 25 x 35 mmLPTE platinum electrode A-012745 PEEK long 6 mm 3 mm

PTE platinum electrode A-002420 PEEK standard 10 mm 5 mmA-002422 PEEK standard 6 mm 3 mmA-002013 PEEK standard 6 mm 1.6 mm

SPTE platinum electrode A-002313 PEEK small 3 mm 1.6 mm

MPTE micro Platinum electrode A-002009 glass micro 4 mm 100 μmA-002003 glass micro 4 mm 25 μmA-002015 glass micro 4 mm 15 μmA-002005 glass micro 4 mm 10 μm

Gold Gold gauze electrode A-002251 PEEK gauze 100 mesh 25 x 35 mmLAUE gold electrode A-012746 PEEK long 6 mm 3 mm

AUE gold electrode A-002418 PEEK standard 10 mm 5 mmA-002421 PEEK standard 6 mm 3 mmA-002014 PEEK standard 6 mm 1.6 mm

SAUE gold electrode A-002314 PEEK small 3 mm 1.6 mm

MAUE micro gold electrode A-002010 glass micro 4 mm 100 μmA-002004 glass micro 4 mm 25 μmA-002006 glass micro 4 mm 10 μm

Silver AGE silver electrode A-002416 PEEK standard 10 mm 5 mmA-002419 PEEK standard 6 mm 3 mmA-002011 PEEK standard 6 mm 1.6 mm

SAGE silver electrode A-002315 PEEK small 3 mm 1.6 mm

Palladium PDE palladium electrode A-002019 PEEK standard 6 mm 1.6 mm

SPDE palladium electrode A-002319 PEEK small 3 mm 1.6 mm

Nickel NIE nickel electrode A-002016 PEEK standard 6 mm 1.5 mm

MNIE micro nickel electrode A-002273 glass micro 4 mm 100 μm

Copper CUE copper electrode A-002017 PEEK standard 6 mm 1.6 mm

CUE copper electrode A-012584 PEEK standard 6 mm 3 mm

MCUE copper electrode A-002271 glass micro 4 mm 25 μm

Iron FEE iron electrode A-002018 PEEK standard 6 mm 1.5 mm

FEE iron electrode A-012585 PEEK standard 6 mm 3 mm

Carbon paste CPE carbon paste electrode hole depth 4 mm A-002210 PEEK standard 6 mm 3 mm

SCPE carbon paste electrode hole depth 4 mm A-002223 PEEK small 3 mm 1.6 mm

CPO carbon paste oil base 1 g A-001010

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Reference electrodes are divided into two groups according to the media in which the electrode is immersed (aqueous or organic media).

ELECTROCHEMISTRY ACCESSORIES20

For aqueous media (Ag/AgCl, Hg)

Catalog No. Junction Electrolyte PurposeRE-1B silver, silver chloride reference electrode A-012167 vycor glass 3 M NaCl SVC-2, SVC-3, VC-4, bulk electrolysis,

RRDE-3A, flat cellRE-1S silver, silver chloride reference electrode A-012168 vycor glass 3 M NaCl SECMRE-1C silver, silver chloride reference electrode A-002058 ceramic saturated KCl SVC-2, SVC-3, VC-4, bulk electrolysis,

RRDE-3A, flat cellRE-3V silver, silver chloride reference electrode screw type, poly acetal resin

A-012169 vycor glass 3 M NaCl for flow cell spectroelectrochemcial cell SEC-3F

RE-3VP Ag/AgCl screw type electrode, PEEK resin

A-012170 vycor glass 3 M NaCl for flow cell spectroelectrochemcial cell SEC-3F

Ag/AgCl ink, 2 mL A-011464 surface resistance: 0.2 Ω/sq/25.4 μm viscosity: 50,000 ±10,000 CP @21.1 °C flash point: 82 °C

for micro CV cell, IDA measurment

RE-2B calomel reference electrode A-002056 ceramic saturated KCl SVC-2, SVC-3, VC-4, bulk electrolysis, RRDE-3A, flat cell

RE-2C Hg2SO4 reference electrode, free from chloride

A-002057 ceramic saturated K2SO4

RE-6H Hg/HgO reference electrode kit available in alkaline solution (mercury solution is not included)

A-011503 ceramic 1M NaOH for alkaline media

ELECTRODES ReferenceElectrodes

RE-1C RE-2BReference electrodes RE-1B

80

RE-1S

50

RE-3V

40,5

11

RE-6H

65

60

RE-2C

45

45

Ag/AgCl ink

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To avoid electrolyte leakage or concentration due to evaporation during storage or transport, the electrolyte is separated from the body. This gives the possibility to fill it regularly.

21

For non aqueous media (Ag/Ag+)

Catalog No. Junction Electrolyte PurposeRE-7 non aqueous reference electrode (Ag/Ag+) A-012171 vycor glass Ag/Ag+/ACN*/TBAP** CVRE-7S non aqueous reference electrode (Ag/Ag+) A-012172 vycor glass Ag/Ag+/ACN*/TBAP** SECMRE-7V non aqueous reference electrode (Ag/Ag+) screw type, poly acetal resin A-012173 vycor glass Ag/Ag+/ACN*/TBAP** flow cellRE-7VP non aqueous reference electrode (Ag/Ag+) screw type, PEEK resin A-012174 vycor glass Ag/Ag+/ACN*/TBAP** flow cell

* Acetonitrile** Tetra Butyl Ammonium Perchlorate

electrodes

RE-7S

1020

23

RE-7VP

5,5

11

3035

RE-7V

5,5

11

3035

RE-7

68

1020

44

RE-7 - Electrolyte solution (3 mL)

RE-7 - Electrolyte solution (3 mL)

RE-7 - Electrolyte solution (3 mL)

RE-7 - Electrolyte solution (3 mL)

Dimensions in mm

0.930 V Hg/HgO/ NaOH (0.1 M)

0.650 V Hg/Hg2SO4 / K2SO4 (sat)

0.624 V Fc/Fc+ TBAP (0.1M) ACN

0.542 V Ag/Ag+ TBAP (0.1M) ACN

0.241 V Hg/Hg2Cl2 KCl (sat)

0.236 V Hg/Hg2Cl2 NaCl (sat)

0.205 V Ag/AgCl/ KCl (3.5 M)

0.197 V Ag/AgCl/ KCl (sat)

0.194 V Ag/AgCl/ NaCl( sat)

0.000 V NHE Normal Hydrogen ElectrodeE/V vs NHE at 25°C

Potentials of reference electrodes

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ELECTROCHEMISTRY ACCESSORIES22

ReferenceElectrodes

Store your reference electrode immersed in the electrolyteWhen it is not in use, the recommended way to maintain the reference electrode capability and lifetime, is to keep it in a sealed preservative vial with a solution. This storage solution should be identical to the filling solution of the reference electrode.

Replace the vycor when needed Yellowish discoloration indicates contamination. This is caused by the adsorption of organic compounds into their pores.

Maintenance of Vycor-based reference electrode

Catalog No.RE-PV preservative vial for reference electrode, 10 mL A- 012108

ContentsTeflon cap for RE-PV -Screw vial 10 mL -

OptionRE-7 electrolyte solution 10 mL A-012549

Catalog No.Repair kit for bridge tube: - vycor glass rod, Ø 2.85 x 4.0 mm (10 pieces), - heat shrink teflon tubing, 150 mm, (1 piece)

A-012796

Heat shrink teflon tubing, 100 mm (1 piece) A-012183

Prevent contaminationTo prevent contamination of the reference electrode, a sample holder can be used.

Catalog No.Bridge tube Ø 9.0 mm (2 pieces) A-012177Bridge tube Ø 9.0 mm (22 pieces) A-012307

A-012177

9

65

ELECTRODES

Reference electrodes

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23

electrodes

Dimensions in mm

Catalog No. Junction Electrolyte PurposeAg/AgCl reference electrode length 120 mm, OD 8 mm R-XR300 ceramic sat KCl CV

length 160 mm, OD 8 mm R-XR820 ceramic sat KCl EISCalomel reference electrode length 103 mm, OD 7,5 mm R-REF921 ceramic LiCl general

(non aqueous)length 80 mm, OD 8 mm R-XR110 ceramic Sat KCl CV

Hg/Hg2SO4 reference electrode length 103 mm, OD 8 mm R-REF621 ceramic sat K2SO4 chloride freelength 120 mm, OD 8 mm R-XR200 ceramic sat K2SO4 CV

Hg/HgO reference electrode length 120 mm, OD 8 mm R-XR400 ceramic 0,1M KOH CV

OptionsShort connection cable for screw cap electrode length 10 cm with 2 mm male banana plug R-A94L111*Long connection cable for screw cap electrode length 1 m with 4 mm banana plug R-C123A*12 mm OD conical rings for 8 mm OD electrodes (4 pieces) R-X31M012Bridge tube with ceramic junction length: 70 mm, OD 12 mm R-AL100

length: 250 mm, OD 8 mm R-AL110with reverse sleeve (non aqueous) length: 138 mm, OD 8 mm R-AL210length: 138 mm, OD 8 mm R-AL120

* R-A94L111 or R-C123A connectors are strongly recommended to connect these reference electrodes to the potentiostat

R-XR820R-XR300 R-REF921 R-XR110 R-REF621 R-XR200 R-XR400

120 120

160

103 103

80

King size electrodes

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Catalog No. Length Wire Ø Surf. area PurposePt A-002222 5.7 cm 0.5 mm ~ 0.7 cm2 SVC-2, VC-4, plate material evaluating cell

A-002233 5 cm 0.5 mm ~ 0.7 cm2 SVC-3A-002234 23 cm 0.5 mm ~ 3.6 cm2 RRDE-3A, bulk electrolysis, SVC-3

Au A-012638 23 cm 0.5 mm ~ 3.6 cm2 RRDE-3A, bulk electrolysis, SVC-3Ni A-012639 23 cm 0.5 mm ~ 3.6 cm2 RRDE-3A, bulk electrolysis, SVC-3Stainless steel A-012198 5 cm 1.5 mm ~ 2.35 cm2 for flow cellPlatinum gauze electrode, PEEK 80 mesh A-002250 25 x 35 mm 0.08 mm ~ 1 cm2

Gold gauze electrode, PEEK 100 mesh A-002251 25 x 35 mm 0.07 mm ~ 1 cm2

55 mesh A-002254 40 x 50 mm 0.12 mm ~ 5.1 cm2

Counter electrodes

ELECTROCHEMISTRY ACCESSORIES24

CounterElectrodes

The counter should not be the limiting factor for the electron transfer, so the surface area of the counter electrode should be higher than the surface area of the working electrode.

Counter electrode selection

A-002233 A-002234 A-012638 A-012639 A-012198A-002222

ELECTRODES

Small size

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Catalog No. Length OD Wire dimensionPlatinum electrode for Voltammetry R-XM110 80 mm 8 mm diameter of 1 mm

R-XM120 120 mm 8 mm plate 5 x 5 mmR-XM140 120 mm 8 mm plate 8 x 8 mmR-XM150 120 mm 12 mm disk of 10 mm

Glassy electrode for Voltammetry R-M291C 103 mm 8 mm rod diameter of 3 mm

OptionsShort connection cable for screw cap electrode length 10 cm with 2 mm male banana plug

R-A94L111*

Long connection cable for screw cap electrode length 1 m with 4 mm banana plug

R-C123A*

12 mm OD conical rings for 8 mm OD electrodes (4 pieces) R-X31M012* R-A94L111 or R-C123A connectors are strongly recommended to connect these counter electrodes to the potentiostat

25

electrodes

R-XM120R-XM110 R-XM140 R-XM150

120

A-002250

23

25

10

35

A-002254

100

Dimensions in mm

King size

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Catalog No.RRDE-3A rotating ring disk electrode apparatus A-012180

ContentsRRDE-3A glass cell vial 100 mL A-012632Spin coating adapter A-012064Nipple for purge valve A-012065TYGON tubing, OD1/4 x ID1/8 (1.3 m) A-010058Teflon cap for RRDE-3A A-012631Instruction manual -Power cable -

AccessoryWater-jacketed glass cell (100 mL, OD 70 mm, ID 46.4 mm, H 80 mm) A-012652DB9 cable to control RRDE-3A 092-22/11Bipotentiostat cable for two standard channels 092-22/12

Working electrodes (page 27), reference electrodes (page 20) and counter electrodes (page 24) have to be purchased separately.

Rotating ring disk electrode RRDE-3A

ELECTROCHEMISTRY ACCESSORIES26

ROTATING RING DISK ELECTRODE Rotating

Ring disk electrode

RDE investigations at different rotation speed

SpecificationsRotational range 100 - 8,000 rpmSetting resolution 1 rpmAccuracy ‹ 0.1%Rotation control type PLL (phase-locked loop) Bandwidth 60 Hz at 3,500 rpm

base and 1,000 rpm peak-to-peak modulation

Inlet gas pressure 5 PSITemperature 10-50 deg CPower 100-240 VAC, 50/60 HzSize (W x D x H) 185 x (base: 230,

body: 120) x 400 mmWeight 6 kg

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Working electrode tips

27

ring disk electrode

Catalog No. Tips length Tips OD Ring ID Ring OD Disk ØRRDE Pt ring/Pt disk A-011172 25 mm 12 mm 5.0 mm 7.0 mm 4.0 mm

Pt ring/GC disk A-011162 25 mm 12 mm 5.0 mm 7.0 mm 4.0 mmAu ring/GC disk A-011163 25 mm 12 mm 5.0 mm 7.0 mm 4.0 mmPt ring/Au disk A-011164 25 mm 12 mm 5.0 mm 7.0 mm 4.0 mmAu ring/Pt disk A-012617 25 mm 12 mm 5.0 mm 7.0 mm 4.0 mmGC ring/GC disk A-012618 25 mm 12 mm 5.0 mm 7.0 mm 4.0 mm

RDE GCE glassy carbon disk A-011169 25 mm 12 mm - - 3.0 mmPTE platinum disk A-011170 25 mm 12 mm - - 3.0 mmAUE gold disk A-011171 25 mm 12 mm - - 3.0 mmALE aluminum disk A-011966 25 mm 12 mm - - 3.0 mmAGE silver disk A-011967 25 mm 12 mm - - 3.0 mmCUE copper disk A-011968 25 mm 12 mm - - 3.0 mmNIE nickel disk A-011969 25 mm 12 mm - - 3.0 mmTAE tantalum disk A-011970 25 mm 12 mm - - 3.0 mmTIE titanium disk A-011971 25 mm 12 mm - - 3.0 mmWE tungsten disk A-011972 25 mm 12 mm - - 3.0 mmCPE carbon paste disk hole depth 4 mm A-011973 25 mm 12 mm - - 3.0 mm

OptionsPK-3 polishing kit A-011975

A-012614 A-012613 A-012616 A-012615 A-011170 A-011171 A-011169

Disk electrode Ø 4 mmRing electrode Ø 7 mmRRDE Ø 12 mm

Disk electrode Ø 3 mmRDE Ø 12 mm

To refresh the surface of the electrode we recommend to polish the electrode after each measurement.

Working electrode maintenanceWorking electrodes maintenance Catalog No.PK-3 electrode polishing kit A-011975

Contents0.05 μm polishing alumina (20 mL) A-0010501 μm polishing diamond (10 mL) A-002054Glass plate (1 piece) A-002249Alumina polishing pad (10 pieces)Diamond polishing pad (10 pieces)

Replacement itemAlumina polishing pad (20 pieces) A-001040Diamond polishing pad (20 pieces) A-001041Emery paper UF800 (20 pieces) A-012611Coarse polishing pad (20 pieces) A-001042

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SPECTRO- ELECTROCHEMISTRY

ELECTROCHEMISTRY ACCESSORIES28

Three utilization modes & two spectrometers

SpectroSpectro

Transmittance Fluorescence Irradiance

Spectroelectrochemistry (SEC) can be useful to elucidate electrochemical reaction mechanisms. The spectroelectrochemical kit is composed of three parts (spectrometer, light source and cuvette holder).

Catalog No. Catalog No.Spectrometer combo kit type A-012196 SEC2000-UV/VIS A-012598 SEC2000-VIS/NIR

ComponentsSpectrometer A-012191 SEC2000-UV/VIS A-012565 SEC2000-VIS/NIRLight source A-012193 SEC2000-DH UV A-012194 SEC2000-TH VisibleCuvette holder A-012195 SEC2000-CUV A-012244 SEC2000-CUV

with diffusion plate

SEC2000-UV/VIS combo kit

SEC2000-VIS/NIR combo kit

Wavelenght (nm)

Abso

rban

ce

Absorbance changes for the oxidation of the potassium ferrocyanide.

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29

electrochemistry

SEC2000-UV/VIS combo kit SEC2000-VIS/NIR combo kit

Detector 2048 pixels CCD arrayWave length range 220 - 800 nm 500 - 1000 nmGrating blazed at 400 nm blazed at 750 nmResolution 1.8 ± 0.2 nm: slit 50 μm x 1000 μm (standard) (1)

Accuracy < 1% at a AbsDark noise < 2 mAbsA/D resolution 14 bitOptical entrance SMA905Interface USB 2.0Operating system WindowsTM XPDimension (W x D x H) 98 x 118 x 35 mmCatalog No. A-012191 A-012565* 1. Slit could be selected from: 10, 25, 100, 200 μm.

SEC2000-DH Light source (deuterium & tungsten halogen)

SEC2000-TH Light source (tungsten halogen)

Spectral range (Halogen + D2) 200 - 1100 nm 360 - 2000 nmD2 lamp spectral range 200 - 400 nm -

power consumption (240 nm) < 5 x 10-8 W/nmsr -stability 1 x 10-3 AU -drift < 0.25%/h -bulb life (2) < 1000 h -

Halogen lamp bulb life > 2000 h 1,500 hConnector SMA905 included SMA905 not includedDimension (W x D x H) 98 x 118 x 35 mm 98 x 118 x 35 mmCatalog No. A-012193 A-012194* 2. Value for less than 50% power consumption of 240 nm.

SEC2000-UV/VIS combo kit SEC2000-VIS/NIR combo kitCuvette holder A-012195 A-012244

Spectrometer

Light source

Cuvette holder

Page 30: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

Platinum kit Gold kit

Quartz glass spectroelectrochemical cell kit Catalog No. Catalog No.

0.5 mm kit A-012604 A-012605

Componentsgrid metal - Pt - AuPt counter electrode A-012609 A-012609 thin layer quartz glass cell A-012608 A-012608teflon cap A-011501 A-011501purging tube A-010537 A-010537gauze working electrode A-012606 80 mesh, height 6 mm A-012607 100 mesh, height 6 mm

1 mm kit A-011240 A-012186

Componentsgrid metal - Pt - AuPt counter electrode A-011499 A-011499thin layer quartz glass cell A-011500 A-011500teflon cap A-011501 A-011501purging tube A-010537 A-010537gauze working electrode A-011498 80 mesh, height 5 mm A-012017 100 mesh, height 5 mm

Optional itemsRE-1B Ag/AgCl reference electrode A-012167RE-7 non aqueous reference electrode A-012171

Static experiment

SPECTRO- ELECTROCHEMISTRY

ELECTROCHEMISTRY ACCESSORIES30

SpectroSpectro

42

13

10039

5,5 mm0,5 mm

5 mm

6,5 mm1 mm

6 mm

40

6

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A-012656

Flow experiment

31

electrochemistry

Working electrodeSilicone gasket 500 μmCounter electrodeCollimating Lens Reference electrode

Inlet

Outlet

Catalog No. QtySEC-2F spectroelectrochemical flow cell A-012660

ContentsSEC-2F flow cell base - 1

cover - 1block A - 1block B - 1

SEC-2F S500 silicone gasket A-012661 2Stainless tube OD 1/16" (50 mm) A-012198 1Needle adaptor - 1Dynaseal PEEK fingertight - 2Silicon tube (30 cm) - 1Teflon tube (1 m) - 1

OptionalReference electrode screw type

Ø 10 x 55 mm RE-3V aqueous A-012169RE-3VP aqueous (PEEK) A-012170RE-7V non aqueous A-012173RE-7VP non aqueous (PEEK) A-012174

Working grid electrode for flow cell

8 x 27 x 1 mm Pt grid electrode (1 piece) A-012655Au grid electrode (1 piece) A-012656carbon grid electrode (1 piece) A-012657ITO electrode (4 pieces) A-012658

8 x 27 x 0,5 mm ITO electrode (12 pieces) A-01146510 x 20 x 0,5 mm ITO electrode (10 pieces) A-01088710 x 10 x 0,5 mm ITO electrode (30 pieces) A-011233Ø 4 inch x 0,5 mm ITO electrode (1 piece) A-011827

Gasket silicone S500, 500 μmt (4 pieces) A-012661S250, 250 μmt (4 pieces) A-012662S100, 100 μmt (4 pieces) A-012663

teflon T500, 500 μmt (4 pieces) A-012664T250, 250 μmt (4 pieces) A-012665T100, 100 μmt (4 pieces) A-012666

Fiber and lens 400 μm optical fiber SR, 25 cm A-012667400 μm optical fiber SR, 2 m A-011522UV/VIS collimating lens, 200-2000 nm A-012234

Dimensions in mm

Page 32: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

QUARTZ CRYSTAL ANALYZER

ELECTROCHEMISTRY ACCESSORIES32

Quartz crystalQuartz Crystal

The instrument monitors both the resonant frequency and the resonant resistance which are also reflected on the two analog outputs. It is possible to connect the Quartz Crystal Analyzer (QCA922) to a Biologic potentiostat using a small optional DB9-8BNC cable (ref: 092-22/1).

Catalog No.Quartz crystal microbalance 9 MHz kit SE-QCA922B

ContentsEQCM 9 MHz (or 5 MHz) main unit SE-QCA922-00Adapter cable SE-QCA922-10Male BNC/BNC cable (2 pieces, length 1 m) COR28100

OptionsHolder is needed to get a full QCM or EQCM set-up

static and flow QCA cell 092-QCA-FCdip cell SE-CL3well cell SE-CL4transparent well cell SE-CL5flow cell (90 μL) SE-CL7 is transparent SE-CL6/SE-CL7

Connector from QCA to potentiostat 092-22/1Low flow peristaltic pump EL-AV-008

SpecificationsFrequency range 1 MHz-10 MHz,

resolution 0.1 HzResonant resistance range

10-16 Ω, resolution 0.1 Ω

∆F Output full scale: ± 10 V (12 bit) ± 200 Hz / ± 2 kHz / ± 20 kHz / ± 200 kHz

Resistance Output full scale: 0-10 V (11 bit) 1 / 2 / 4 / 8 / 16 kΩ

Gate time variable (0.1, 1.0, 10.0 s)Display 40 Digits x 2 rowsInterface IEEE-488, RS-232CSize 260 x 88 x 230 mmWeight 3.3 kgTemperature 0 - 40 °CPower consumption 100-120 V AC,

230-240 V AC, 50-60 Hz, (15 W)

EQCM

Frequency and resistance measurements

Electropolymerization by voltage scan of pyrrol to polypyrrol

092-QCA-FC SE-CL3

Page 33: ELECTROCHEMISTRY ACCESSORIES CATALOG - ec-lab · electrochemistry accessories catalog corrosion cell analytical cell glassware electrodes rotating ring-disk electrode spectroelectrochemistry

Catalog No.Resonators 5 MHzf0 = 5 MHz (calibration at 5 MHz at factory with no charge when purchased)

gold electrode (25 pieces) SE- 5AUgold electrode separated lead wire (25 pieces) SE- 5AU-Sgold electrode mirror finish (25 pieces) SE- 5AU-Mgold electrode mirror finish separated lead wire (25 pieces) SE- 5AU-MS

Resonators 9 MHzf0 = 9 MHz

etching finish gold electrode (30 pieces) SE- 9AU-E/1gold electrode (100 pieces) SE- 9AU-E/3

polish finish gold electrode (30 pieces) SE- 9AU-P/1gold electrode (100 pieces) SE- 9AU-P/3

standard finish resonator and lead wire

silver electrode (25 pieces) SE- 9AGaluminum electrode (25 pieces) SE- 9ALgold electrode (25 pieces) SE- 9AUgraphite electrode (25 pieces) SE- 9Ccupper electrode (25 pieces) SE- 9CUmolybdenum electrode (25 pieces) SE- 9MOnickel electrode (25 pieces) SE- 9NIplatinum electrode (25 pieces) SE- 9PTsilicium oxide electrode (25 pieces) SE- 9SOstainless steel (SUS304) electrode (25 pieces) SE- 9SStitanium electrode (25 pieces) SE- 9TI

separated lead wire

silver electrode (25 pieces) SE- 9AG-Saluminum electrode (25 pieces) SE- 9AL-Sgold electrode (25 pieces) SE- 9AU-Sgraphite electrode (25 pieces) SE- 9C-Scopper electrode (25 pieces) SE- 9CU-Smolybdenum electrode (25 pieces) SE- 9MO-Snickel electrode (25 pieces) SE- 9NI-Splatinum electrode (25 pieces) SE- 9PT-Ssilicium electrode (25 pieces) SE- 9SI-Ssilicium oxide electrode (25 pieces) SE- 9SO-Sstainless steel (SUS304) electrode (25 pieces) SE- 9SS-Stitanium electrode (25 pieces) SE- 9TI-S

mirror finish resonator and lead wire

silver electrode (25 pieces) SE- 9AG-Maluminum electrode (25 pieces) SE- 9AL-Mgold electrode (25 pieces) SE- 9AU-Mgraphite electrode (25 pieces) SE- 9C-Mcopper electrode (25 pieces) SE- 9CU-MITO electrode (25 pieces) SE- 9IT-Mmolybdenum electrode (25 pieces) SE- 9MO-Mnickel electrode (25 pieces) SE- 9NI-Mplatinum electrode (25 pieces) SE- 9PT-Msilicium electrode (25 pieces) SE- 9SI-Msilicium oxide electrode (25 pieces) SE- 9SO-Mstainless steel (SUS304) electrode (25 pieces) SE- 9SS-Mtitanium electrode (25 pieces) SE- 9TI-M

separated lead wire

silver electrode (25 pieces) SE- 9AG-MSaluminum electrode (25 pieces) SE- 9AL-MSgold electrode (25 pieces) SE- 9AU-MSgraphite electrode (25 pieces) SE- 9C-MScopper electrode (25 pieces) SE- 9CU-MSITO electrode (25 pieces) SE- 9IT-MSmolybdenum electrode (25 pieces) SE- 9MO-MSnickel electrode (25 pieces) SE- 9NI-MSplatinum electrode (25 pieces) SE- 9PT-MSsilicium electrode (25 pieces) SE- 9SI-MSsilicium oxide electrode (25 pieces) SE- 9SO-MSstainless steel electrode (25 pieces) SE- 9SS-MStitanium electrode (25 pieces) SE- 9TI-MS

OthersResonators lead wire no sputter (50 pieces) SE- LEAD/2Resonators 9 MHz, no sputter no lead wire (50 pieces) SE- 9Q/2

mirror finish no lead wire (50 pieces) SE- 9Q-M/2

33

analyzer

Surface finishingRoughness/µm Electrode materials deposition

Standard finish 0.6 μm sputteredEtching finish 0.6 μm vacuum depositionMirror finish 0.06 μm sputteredPolish finish 0.06 μm vacuum deposition

Gold electrode

stainless steelelectrode

Platinum electrode

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Biosensor QCM

The specification (27 MHz) of the Quartz Crystal Microbalance (QCM934) allows user to measure a small mass change. So QCM934 is especially suitable in the bio-sensing field.

Excellent sensitivity and resolution. Specially designed oscillation circuit for added stability. Simultaneous measurement of resonant frequency, resonant resistance and temperature.

Expandable up to 4 channels. Works with flows cell, well cell, dip cell. Computer control and data collection via USB interface.

Resonators of 9 MHz are compatible with QCM934 and the cell.

QUARTZ CRYSTAL ANALYZER

ELECTROCHEMISTRY ACCESSORIES34

Quartz crystalQuartz Crystal

Four configurations are available

Temp.Status

Osc.Status

Oscillator & TemperatureControl Module

QCM934Quartz Crystal Microbalance

Power

"Flow cell-based system of QCM934", "perista pump" and "notebook computer"

Temp.Status

Osc.Status

Oscillator & TemperatureControl Module

QCM934Quartz Crystal Microbalance

Power Transparent Well CellQA -CL5

Dip CellQA - CL3

"Batch cell-based system of QCM934", "transparent well / dip cell" and "notebook computer"

Temp.Status

Osc.Status

Oscillator & TemperatureControl Module

QCM934Quartz Crystal Microbalance

Power

"Micro flow cell-based system of QCM934", "perista pump" and "notebook computer"

Temp.Status

Osc.Status

Oscillator & TemperatureControl Module

QCM934Quartz Crystal Microbalance

Power

PotentiostatWith Analog Out

"EQCM-based system of QCM934" and "notebook computer"

SpecificationsFrequency range 25 MHz-27 MHz,

resolution 0.01 HzResonant resistance range

2 Ω, resolution 0.1 Ω

Max channel 4Gate time variable (0.1, 1.0, 10.0 s)Display 20 Digits x 2 rowsInterface USB 2.0Size 320 x 280 x 133 mmWeight 5.5 kgTemperature 10 - 40 °CPower consumption 100-120 V AC, 230-240 V

AC, 50-60 Hz, (60 W)

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35

microbalance

Catalog No. Catalog No. Catalog No.Product SE-QCM934-F SE-QCM934-MF SE-QCM934-BMain unit SE-QCM934-000WinQCM software SE-WQCMOscillator & temperature control module SE-QCM934-200Cable for oscillator & temperature control module SE-QCM934-200AMeasurement chamber SE-QCM934-500Cable for OSC module connection SE-QCM934-300Flow cell (90 μL) SE-QCM934-510Micro flow cell (1 μlL) SE-QCM934-600Additional channel SE-QCM934-1CHF SE-QCM934-1CHMF SE-QCM934-1CHB

OptionLow flow peristaltic pump EL-AV-008

Flow cell Micro flow cell Batch cell

Measurement chamber Oscillation circuit Flow cell (90 μL) Micro flow cell (1 μL)

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4-point measurement 4 A maximum current Adaptable to a wide variety of battery sizes (coin cells, 18 650 or 26 650 cells)

Ability to link together many battery holders

To be added to a multichannel system to perform stack measurements up to 50 V for 5 channel boards and 10 elements measurement.

The coin cell holder is directly plugged to the potentiostat connectors. No cable is required. 4 coin cells can be investigated simultaneously.

Battery holder

Coin cell holder

BATTERY ACCESSORIES

ELECTROCHEMISTRY ACCESSORIES36

Sense adapter module SAM-50

Battery accessoriesBattery

Catalog No.Coin cell holder, 62 x 82 x 83 mm 092-22/14

Catalog No.Battery holder 092-22/10

Catalog No.Sense adaptor module SAM-50 092-26

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FARADAY CAGES

37

Faraday cages

Standard Faraday cage

Advanced Faraday cage

Inside the cage

Panel open

Rear panel

SpecificationsTemperature 0 - 50 °CPower supply 100 VAC-240 VAC, 50/60 HzFuse 1 AGas pressure ‹ 34 kPa max.Size (W x D x H) 286 x 230 x 320 mmInterface IEEE-488, RS-232CWeight 3.8 kg

Catalog No. Dimensions

Standard Faraday cage for standard channel N-FAR600 600 x 400 x 200 mm for low current channel NS-FAR600 600 x 400 x 200 mm

Advanced Faraday cage A-012033 286 x 230 x 320 mm

To avoid any external perturbations, specially for low current application, we recommend to use the Faraday cage. Please note that to activate this protection, Faraday cage has to be connected to the ground of the instrument (green plug on the rear panel of the instrument).

External disturbance

NS-FAR600

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FUEL CELL

ELECTROCHEMISTRY ACCESSORIES38

FuelFuel cell

Membrane electrode assemblies (MEA)

These MEAs are based on a 50 μm-thick perfluoronated membrane, and a platinum loading of 0.5 mg/cm² (± 0.05), obtained with the standard catalyst concentration, 70% Pt/C.

3 layers MEA corresponds to a catalyst covered membrane (CCM): the proton exchanged membrane is covered with an ink containing the catalyst on the electroactive area. Platinum and Platinum-Ruthenium alloys are available for hydrogen and reformate operations respectively.

5 layers MEA corresponds to a CCM with gas diffusion layers (GDL) completing the electrodes on the electroactive area on both sides of the membrane.

7 layers MEA corresponds to a 5-layer MEA with a flat gasket (fiberglass reinforced silicon) around both electrodes.A subgasket, protecting the membrane and the edges of the active layer can be added to 5 and 7-layer MEAs.

Catalog No.Single cell fixture (without MEA's)

5 cm² 095- 08/116 cm² 095- 08/225 cm² 095- 0750 cm² 095- 08100 cm² 095- 08/3

Membrane Electrode Assemblies

MEA S5, 5 cm² 3 layers 095-09/135 layers 095-09/147 layers 095-09/15

MEA S16, 16 cm² 3 layers 095-09/165 layers 095-09/177 layers 095-09/18

MEA S25, 25 cm² 3 layers 095-09/15 layers 095-09/27 layers 095-09/3

MEA S50, 50 cm² 3 layers 095-09/45 layers 095-09/57 layers 095-09/6

MEA S100, 100 cm² 3 layers 095-09/75 layers 095-09/87 layers 095-09/9

MEA S225, 225 cm² 3 layers 095-09/105 layers 095-09/117 layers 095-09/12

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39

cell

Semi-automatic filling kit

An external kit (Semi Automatic Water Filling Kit) can be added to an existing FCT. This kit consists of two separate pumps that can be easily added to the front panel of a FCT. Using this external tool, researchers can manually fill the humidifier (anodic and cathodic side separately) without switching off the instrument or disrupting the experiment in progress.

Catalog No.Single cell fixture (without MEA's)

5 cm² 095- 08/116 cm² 095- 08/225 cm² 095- 0750 cm² 095- 08100 cm² 095- 08/3

Membrane Electrode Assemblies

MEA S5, 5 cm² 3 layers 095-09/135 layers 095-09/147 layers 095-09/15

MEA S16, 16 cm² 3 layers 095-09/165 layers 095-09/177 layers 095-09/18

MEA S25, 25 cm² 3 layers 095-09/15 layers 095-09/27 layers 095-09/3

MEA S50, 50 cm² 3 layers 095-09/45 layers 095-09/57 layers 095-09/6

MEA S100, 100 cm² 3 layers 095-09/75 layers 095-09/87 layers 095-09/9

MEA S225, 225 cm² 3 layers 095-09/105 layers 095-09/117 layers 095-09/12

Catalog No.Educational kit (fuel cell / electrolyzer)

110 V 095-20/A220 V 095-20/B

ContentsKit PAC#1: 25cm² air-breathing cells (MEA S25-7L N50-Pt/C 70%), no possibility to dismantle the cell 095-20/1

PAC#2: 25cm² air-breathing cells (MEA S25-7L N125-Pt/C 70%), no possibility to dismantle the cell 095-20/2PAC#3: 25cm² air-breathing cells (MEA S25-7L N212-Pt/C 40%), no possibility to dismantle the cell 095-20/3

Electrolyzer kit (including gas line) 095-20/4Variable resistance 095-20/5Data acquisition (including connection, data logger, software) 095-20/7Power supply 220 V 095-20/9110 V/220 V adapter for 110 V configuration 095-20/10

Optional products25 cm² air-breathing cell (no MEA) 095-20/6Power supply by two photovoltaic cells 095-20/8

Educational kitThe educational fuel cell kit is very simple and easy to use: just plug the hydrogen tank into the cell and let the fuel cell use the oxygen in the surrounding air to produce electricity.

1 plastic electrolyser cell (25 cm²) containing a 7-layer membrane electrode assembly. At the anode side of the electrolyser cell there is a water reservoir, the hydrogen gas produced comes out of the cell via one of the gas exits on the top and bottom side of the cell. A plastic screw is included for closing the unused gas exit.

1 plastic air-breathing fuel cell (25cm²). The cell has one hydrogen gas input and one exit. A porous material is placed inside the kit for the homogeneous diffusion of hydrogen over the whole surface area of the membrane electrode assembly.

Catalog No.Semi-automatic filling kit 095-16

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Multi- electrode investigationscables

Bipot cable: Dedicated to RRDE applications.

CONNECTION ACCESSORIES

ELECTROCHEMISTRY ACCESSORIES40

ConnectionConnection

Low current Nstat box

Connection to the cell

Nstat box (8 channels).

Channel Number of channels Length Catalog No.Bipot cable (for VSP, BiStat, VMP3)

standard 2 1.5 m 092-22/122 3 m 092-22/12A2 4 m 092-22/12B

Nstat box (for VSP, VMP3)

standard 4 1.5 m 092-168 1.5 m 092-22/3

low current 8 1.5 m 092-22/4

OptionExternal power supply for the Nstat box (this option is needed if more than one Nstat box is connected to VMP3 or if the user uses VSP)

092-16/1

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Specific cables

By default, the potentiostat and the booster are provided with a cell cable of 1.5 m long. The cable connected from the booster to the potentiostat is 80 cm long.For some applications, the user may need cables with different length. That's why, longer cable are offered.Moreover for applications performed in glove box, hermetic cell cables are also offered.

Please contact us for other cable length.

41

accessories

Available length Catalog No.SP-50, SP-150, VSP, VMP3, MPG2 2.5 m 092-23/2

3 m 092-23/75 m 092-23/310 m 092-23/4

Booster 2 A, 4 A, 5 A 2.5 m 092-33/113 m 092-33/125 m 092-33/13

Booster 8 A, 10 A, 20 A 2.5 m 092-33/213 m 092-33/225 m 092-33/23

Catalog No.SP-50, SP-150, BiStat, VSP, VMP3, MPG2 092-23/5SP-200, SP-300 094-101/8

Bad connection could induce some effects on the measurement (effect on the stability of the potentiostat, artifact...). We recommend the user to optimize his set-up by using the accessories offered in this section.

Set-up connection

Longer cable

Available length Catalog No.All boosters 3 m 092-33/5

5 m 092-33/6

Connection cable from booster to potentiostat

Hermetic cell cable for glove box

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CONNECTION ACCESSORIES

ELECTROCHEMISTRY ACCESSORIES42

Connectionaccessories

External device connection

Test boxes

Catalog No.BNC-DB9 connector for auxiliary I/O 092-22/1

Catalog No. Contents PurposeTest-Box 1 092-22/5 16 R/C circuits standard check

2 092-22/6 several circuits with high precision resistors calibration and validation3 092-22/7 3 circuits: linear, exponential, non-linear for teaching and demonstration4 092-22/9 2 R/C circuits standard check

Dummy cell 094-111/1 1 R/C circuit standard checkfor booster 2 to 5 A 092-32/2 1 power resistor, 50 mOhm standard checkfor booster 8 to 20 A 092-32/1 1 power resistor, 5 mOhm standard check

5 - I monitor4 - Trigger out3 - Open in2 - Analog out1 - Analog inl

E monitor - 9Trigger in - 8

Ground - 7Analog in 2 - 6

Catalog No.PT100 temperature probe 092-22/13To be connected to the auxiliary I/O

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43

Colour Catalog No.Alligator clips with female connector of 2 mm (pack of 10) black 092-1001/1

red 092-1001/2white 092-1001/22blue 092-1001/26

Alligator clips with female connector of 4 mm (pack of 5) black 092-1001/13red 092-1001/14blue 092-1001/23

Sockets 2 mm female (pack of 10) black 092-1001/5red 092-1001/6blue 092-1001/7white 092-1001/8

Sockets 4 mm female (pack of 10) black 092-1001/25red 092-1001/4blue 092-1001/3

Banana plugs 2 mm (pack of 10) black 092-1001/9red 092-1001/10blue 092-1001/11white 092-1001/12

Banana stackable plugs 4 mm (pack of 5) blue 092-1001/15red 092-1001/16yellow 092-1001/17white 092-1001/24

Banana adapter 2 mm female socket to 4 mm male plug (pack of 5) black 092-1001/18red 092-1001/19blue 092-1001/20white 092-1001/21

Adapter for banana 2 mm female socket to 4 mm male plug (pack of 5) 092-1001/27

Connectors

Miscellaneous Catalog No.SP-200 suitcase care 094-082

accessories

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w w w . b i o - l o g i c . i n f o

USA Customers Bio-Logic USA, LLCP.O.Box 30009Knoxville TN 37930 - USATel.: +1 865 769 3800 Fax: +1 865 769 3801www.bio-logic.us

Corporate OfficeBio-Logic, SAS

1, rue de l’Europe38640 CLAIX - FranceTel.: +33 476 98 68 31 Fax: +33 476 98 69 09

www.bio-logic.info

Broc

hure

rele

ased

on

May

201

0 -

1001

003

DISTRIBUTION

France: Bio-Logic SAS (Corporate Office)USA: Bio-Logic USA LLC (Affiliate Office)India: Bio-Logic India PVT. Ltd. (Affiliate Office)Japan: Hokuto Denko Corp.South Korea: Neoscience Co. Ltd.Germany: Gamec AnalysenTechnikChina: Dalian Huayang Scientific Instruments Co. Ltd.Spain: Trallero & SchleeTaiwan: Beam Associates Co. Ltd.UK & Ireland: EC-Lab Ltd.Canada: Gamble Technologies Ltd.Israel: New Road Agencies

Bio-Logic Science Instruments is present in most countries through an extensive distribution network

Romania: Sc Remed Prodimpex SrlSingapore/Malaysia: Alpha Analytical Ltd.Bosnia/Croatia/Slovenia/Serbia: Inspirion d.o.o.Turkey: Entek Electronik Ltd. Sti.South America/Australia : Bio-Logic USA LLCRest of the world: contact us