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Determination of Lead in Drinking Water

Determination of Lead in Drinking Water. What Is Lead? Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant

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Page 1: Determination of Lead in Drinking Water. What Is Lead? Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant

Determination of Lead in Drinking Water

Page 2: Determination of Lead in Drinking Water. What Is Lead? Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant

What Is Lead?

• Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant for non-infectious diseases, those illnesses associated with toxic chemical pollution.

Page 3: Determination of Lead in Drinking Water. What Is Lead? Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant

Where Is Lead Found?

• Lead can be found in natural deposit, and is commonly used in household plumbing and water service lines. Lead enters tap water through corrosion of plumbing materials.

Page 4: Determination of Lead in Drinking Water. What Is Lead? Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant

What Is the Limited Concentration of Lead in

Potable Water?

• The amount of lead concentration limited in drinking water is 15 ppb (parts per billion) or 15 g/l of water.

Page 5: Determination of Lead in Drinking Water. What Is Lead? Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant

Who Regulates the Concentration Limits?

• Safe Drinking Water Act (SDWA)– through the Environmental Protection

Agency (EPA)

Page 6: Determination of Lead in Drinking Water. What Is Lead? Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant

Experimental Apparatus

Page 7: Determination of Lead in Drinking Water. What Is Lead? Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant

Graphite Furnace Atomic Absorption

Spectrophotometer•

Page 8: Determination of Lead in Drinking Water. What Is Lead? Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant

Hallow Cathode Lamp

Page 9: Determination of Lead in Drinking Water. What Is Lead? Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant

Pyrocoated Graphite Furnace (Tube)

                            

Page 10: Determination of Lead in Drinking Water. What Is Lead? Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant

Sample Carousel

Page 11: Determination of Lead in Drinking Water. What Is Lead? Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant

Motor Driven Sampling Arm

Page 12: Determination of Lead in Drinking Water. What Is Lead? Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant

The Instrument Is Computer-controlled and Provides Automation

to Most Steps of the Analysis.

Page 13: Determination of Lead in Drinking Water. What Is Lead? Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant

The method to identify the experiment is called 239_2_pbA_100 and is the standard method used for the GFAAS. This method is approved

by the EPA and regulated by the

SDWA.

Page 14: Determination of Lead in Drinking Water. What Is Lead? Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant

Method and Procedure Data Book

Page 15: Determination of Lead in Drinking Water. What Is Lead? Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant

Water Samples&

Calibrated Standards

Page 16: Determination of Lead in Drinking Water. What Is Lead? Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant

Absorbance vs Time = ppb Concentration (peak area)

Page 17: Determination of Lead in Drinking Water. What Is Lead? Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant

Water Samples Lead Concentration

1st Draw = 12.0 ppb Mean = 11.7 ppb or g/L

11.4 ppb

2nd Draw = 0.119 ppb Mean = 0.265ppb or g/L

0.412 ppb

Page 18: Determination of Lead in Drinking Water. What Is Lead? Lead is one of the heavy metals that puts enormous risk to human health and is a major determinant

The end