Department of CERTIFICATE OF CALIBRATION Issued to: … · run #2 i run #3 mean i std. dev. n a hinp 8 trnirin ati~li i ~nyuc vcniribn i iuiy position guide range #l range #2 range

,

S O U T H W E S T R E S E A R C H I N S T I T U T E

Department of Quality Assurance Calibration Laboratory

CERTIFICATE OF CALIBRATION

Device No: 2028 Issued to: DIV20 B57 NARASI SRIDHAR

Manufacturer: METTLER Model: UMT2

Nomenclature: ELECTRONIC BALANCE

Serial Number: 211001-142 SwRI No: NONE Cal interval 6 Mo.

Remarks

Accuracy: MFGR SPECS Procedure: SWRI

ENVIRONMENT Temperature: 0 Humidity: 0 Location: SWRI DIV20 B57

CONCLUSION Tolerance/Remarks: Received into the system, introduced or reactivated

LIMITED CALIBRATION ; to +/- -030 milli grams. CALIBRATED TO +/- 30 micro grams.

Calibration was in accord with requirements of MIL-STD-45662A. Measurements are traceable to the National Institute of Standards and Technology. Inspection and test data are on

Signed

Calibr

Cal interval: 6 Months

Record Number: 00010556 Next Calibration Due: 10/29/93



Device Serial No: 211001-142

STANDARDS --------- Standard No: 1704 Manufacturer: RICE LAKE Nomenclature: WEIGHT STANDARD Serial No: C859 Cal.Due: 07/08/93

Standard No: 1706 Manufacturer: RICE LAKE Nomenclature: WEIGHT STANDARD Serial No: C861 Cal.Due: 07/08/93

Standard No: 1720 Manufacturer: RICE LAKE Nomenclature: WEIGHT STANDARDS Serial No: C858 Cal.Due: 07/08/93

Calibration Date: 04/29/93

Model: 1 GRAM

Cal.Rec.No: 00000000

Model: 2 GRAM


Model: 1 - 500 MG


b

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W

2 0

E.c tn 0

PI

z 4 a W

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S O U T H W E S T F l E S E A R C H I N S T I T U T E



Issued to: DIV20 B57 NARASI SRIDHAR


Nomenclature: ELECTRONIC BALANCE

Serial Number: 211001-142 SwRI No: NONE

Remarks

Accuracy: MFGR SPECS

Device No: 2028

Cal interval 6 Mo.

Procedure: SWRI

ENVIRONMENT Temperature: 70 Humidity: 40 Location: SWRI DIV20 BLDG. 57

CONCLUSION Tolerance/Remarks: Received in tolerance, no adjustments made

LIMITED CALIBRATION- +/- .030mg

Calibration was in accord with requirements of MIL-STD-45662A. Measurements are traceable to the Nation Inspection and test data are on fi available f o r inspection,



S O U T H W E S T It E S E A R C H I N S T I T U T E


Device Serial No: 211001-142 Calibration Date: 10/22/93

STANDARDS ---------

Standard No: 1704 Manufacturer: RICE LAKE Model: 1 GRAM Nomenclature: WEIGHT STANDARD Serial No: C859 Cal.Due: 06/30/94 Cal.Rec.No: 00011756


Standard No: 1720 Manufacturer: RICE LAKE Model: 1 - 500 MG Nomenclature: WEIGHT STANDARDS Serial No: C858 Cal.Due: 06/30/94 Cal.Rec.No: 00011772

I BALANCE CAUBRATION VERIFICATION FORM

MFGR: &?k772dk/W MODEL:

SER. NO.Z//@ RANGE: <, CALIBRATION DATES /

I TEMPERATURE: 96 HUMIDITY: yb

I BALANCE TOLERANCES

// BALANCE CAL #: LINE. TOL.: REP. TOL.: I

I DATA PTS.

RUN #1

RUN #2

RUN #3

I MEAN

I STD. DEV.

n A h i n p 8 trnirin A T I ~ L I I ~ N Y U C v c n i r i b n I IUIY

POSITION GUIDE RANGE #l RANGE #2 RANGE #3

CALIBRATION POINTS I CALIBRATION POINTS I CALIBRATION POINTS I rn 1 1 2

COMMENTS: l / M f l k p SHIFT VERIFICATION

,03&5pZacrr SELF CALIBRATION Y/N INTERNAL: 1 EXTERNAL -

WEIGHT PAN POSITION VALUE

/

1 2 3 i SIGNATURE: - -- SWRI FORM QA-153-0

S O U T H W E S T F l E S E A R C H I N S T I T U T E



Device No: 2028 Issued to: DIV20 B57 NARASI SRIDHAR


Nomenclature: ELECTRONIC BALANCES

Serial Number: 211001-142 SwRI No: NONE Cal interval 6 Mo.

Remarks

Accuracy: MFGR SPECS Procedure: SWRI

Temperature: ENVIRONMENT

Humidity : Location: SWRI DIV20 BLDG. 57

CONCLUSION Tolerance/Remarks: Received in tolerance, no adjustments made

Limited Calibration- +/-0.030mg

Calibration was in accord with requirements of MIL-STD-45662A. Measurements are traceable to the National Institute of Standards and Technology. Inspection and test data are on file available for inspection.





Device Serial No: 211001-142 Calibration Date: 04/26/94

STANDARDS --------- Standard No: 1704 Manufacturer: RICE LAKE Model: 1 GRAM Nomenclature: WEIGHT STANDARD Serial No: C859 Cal.Due: 06/30/94 Cal.Rec.No: 00011756


Standard No: 1720 Manufacturer: RICE LAKE Model: 1 - 500 MG Nomenclature: WEIGHT STANDARDS Serial No: C858 Cal.Due: 06/30/94 Cal.Rec.No: 00011772

I BALANCE CALIBRATION VERIFICATION FORM

&L/TLt/e MODEL: &m/cz MFGR:

SER. NO. 2 // 00 @/qZ RANGE: 9 CALIBRATION DATES - 6

HUM I DlTY: I TEMPERATURE:

I CALIBRATED BY: /o b !& BALANCE TOLERANCES d/e ,~d>

BALANCE CAL #: /3J5-z I RANGE VERIFICATION

I RANGE #1 I RANGE #2 I RANGE #3

I CALIBRATION POINTS 1 CALIBRATION POINTS I CALIBRATION POINTS

MEAN

STD. DEV.

I I I I I I I I.

POSITION GUIDE

1 COMMENTS: SHIFT VERIFICATION

SELF CALIBRATION Y/N INTERNAL: EXTERNAL

WEIGHT PAN POSITION

1 2 3 4 VALUE

SWRI FORM QA-153-0

SOUTHWEST RESEARCH INSTITUTE


CERTIFICATE OF CALIBRATION ll/Ol/94

Issued to: NARASI SRIDHAR DIW2O ,B57 Manufacturer: METTL Nomenclature: ELECTRONIC BALANCE Serial Number: 211001-142

Asset Number: 002028 Model Number: UMT2

SwRI Capital Number: NONE

ENVIRONMENTAL CONDITIONS

Temperature: 69.OF Relative Humidity: 51 %

CALIBRATION INFORMATION

Location: B57 Procedure Number: SWRI Remarks : LIMITED TO +/-0.030 MIL GRAMS.

Technician: 7213 Accuracy: MFGR SPECS Received IN Tolerance

Calibration was in accordance with requirements of MIL-STD-45662A. Measurements are traceable to the National Institute of Standards and Tech- nology. Inspection and test data are on file and available for inspection.

STANDARDS USED FOR CERTIFICATION

001720 C858 R I C E 1 - 500 BIG WEIGHT STANDARDS

001704 C859 R I C E 1 GRAM WEIGHT STANDARD

001705 C 8 6 0 R I C E 2 GRAM WEIGHT STANDARD

07/20/94 12 07/20/95 07/20/94 12 07/20/95 07/20/94 12 07/20/95

Work Order: 15529 Chibration Date: 10/27/94 Interval: 6 months Next Calibration Due: 04/27/95

37 r TEMPERATURE: 69 HUM I DITY: I

t RANGE .vERiF[cATioN I

0 -c. .430-9n& I COMMENTS: // mw2-P 7 SHIFT VERIFICATION

SELF CALIBRATION Y/N INTERNAL: EXTERNAL

WEIGHT PAN POSITION VALUE

~

SWRI FORM QA-153-0

4

SOUTHWEST RESEARCH INSTITUTE


CERTIFICATE OF CALIBRATION os/os/9s

Issued to : DARRELL DUNN D IV2 0 I B57 Manufacturer: METTL Nomenclature: ELECTRONIC BALANCE Serial Number: 211001-142

Asset Number: 002028 Model Number: UMT2

SwRI/Div. I.D. #: NONE


Temperature: 70.OF Relative Humidity: 56%

CALI BRAT I ON INFORMATION

Procedure Number: SWRI Remarks : LIMITED TO +/-O0O3C) MIL GRAMS

Accuracy: MFGR SPECS Received IN Tolerance

Calibration was in accordance with requirements of MIL-STD-45662A. Measurements are traceable to the National Institute of Standards and Tech- nology. Inspection and test data are on file and available for inspection.

STANDAFLDS USED FOR CERTIFICATION

Asset # Serial # Mfg Model # Nomenc 1 a ture Cal Date Int. Cal Due

001720 C858 RICE 1 - 500 MG WEIGHT STANDARDS 07/20/94 12 07/20/95 001704 C859 R I C E 1 GRAM WEIGHT STANDARD 07/20/94 12 07/20/95 001705 C860 R I C E 2 GRAM WEIGHT STANDARD 07/20/94 12 07/20/95

. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

A Certified by :

/

Certificate#: 17215 I / Calibration Date: 05/05/95

Interval: 6 months Next Calibration Due: 11/05/95

-- - -~

M C E CAU8RATION VERIFICATION FORM

SER. NO. z / /m - /Yz RANGE: z c CALIBRATION DATES /

TEMPERATURE: 7 d b HUMIDITY:

1

BALANCE CAL #:

BALANCE TOLERANCES C/.S ,TG LINE. TOL.: REP. TOL.:

RANGE VERIFICATION

1 I I RANGE #1 RANGE #2 RANGE #3 POSITION GUIDE

- - ~ -~ ~

I

COMMENTS: d24,7&B /'a ,030 a y SHIFT VERIFICATION

SELF CALIBRATION Y/N INTERNAL EXTERNAL - WEIGHT

4

A

SWRI FORM QA-153-0

SOUTHWEST RESEARCH INSTITUTE .

Department of Quality ASSUranc8 Calibration Laboratory

CER!PIFICATE OF CALIBRATION 11/03/95

Issued to: DARRELL DUNN D IV2 0 I B57 Manufacturer/Model: METTL/UMT2 Nomenclature: ELECTRONIC BALANCE Serial Number: 211001-142 Asset Number: 002028 Notes:


Temperature: 75.OF Relative Humidity: 66%

CALIBRATION INFORMATION

Procedure Number: WI-9-30-WT01 Remarks : LIMITED TO +/-0.03 MGRAMS

Accuracy: MFGR SPECS Received IN Tolerance

Calibration was in accordance with requirements of MIL-STD-45662A. Measurements are traceable to the National Institute of Standards and Tech- nology. Inspection and test: data are on file and available for inspection.

STANDARDS USED FOR CERTIFICATION

Certif icateX: 19168 Calibration Date : 11/02 /95 Interval: 6 months Next Calibration Due: 05/02/96

CALIBRATION DAES

REP. TOL: UNE. Tm: f

1

3

'1 4 i

.

Southwest Research Institute 6220 Culebra Road

San Antonio, TX 78238 IDepartment of Quality Assurance Calibration Laboratory

Total Pages Printed: 1

Certificate of Calibration 3 May 1996

Issued to: DARRELL DUNN DIV20 B57 Man ufact u rer/M ode I : MElrTL UMT2 Description: ELECTRONIC BALANCE Serial Number: Asset Number: 002028

21 1001 -1 42

[E n v i ro n menta I C o n d it i o n s I Tem pe rat u re : 78.0 Humidity: 59%

[Calibration Information I Calibration was in accordance with requirements of MIL-STD-45662A and ANSVNCSL 2540-1 -1 994. Measurements are traceable to tlhe National Institute of Standards and Technology (NIST). This report may not be reproduced except in full without written approval of the originator. Inspection and test data are on file and available for inspection.

Calibration Date: 2 May 96 Calibration Procedure: WI-9-30-WTO 1

Interval: 6 months Accuracy: MFGR SPECS

Next Calibration Due: 2 Nov 96 Received: In Tolerance

Remarks: LIMITED TO +\- 0.03 MILLIGRAMS

Certificate ## 21114

EI I

\ c

\4


San Antonio, TX 78238 Department of Quality Assurance Calibration Laboratory

Certificate of Calibration 11 November 1996

Issued to: DARRELL DUNN DIV20 B57 Manufacturer/Model: METTL UMT2 Description: ELECTRONIC BALANCE Serial Number: 211001-142 Asset Number: 002028

c ~~~ rr- nvironmental ~~ - Conditions

Temperature: 71 .O Deg. F Humidity: 55%

ICalibration Information LI

Calibration was in accordance with requirements of MIL-STD-45662A and ANSVNCSL 2540-1 -1 994. Measurements are traceable to the National Institute of Standards and Technology (NIST). This report may not be reproduced except in full without written approval of the originator. Inspection and test data are on file and available for inspection.

Calibration Date: 1 Nov 96 Cali brat ion Proced u re : CLC P-WB-00 1


Next Calibration Due: 1 May 97 Received: In Tolerance

Remarks: LIMITED TO +/-0.03 MILLIGRAMS

Certificate # 23192

/ ’ LAST PAGE OF REPORT Total Pages Printed: 1



1

Total Pages Printed: 1


Issued to: DARRELL DUNN DIV20 857 Manufacturer/Model: ME'TTL UMT2 Description: ELECTRONIC BALANCE Serial Number: Asset Number: 002028

21 1001 -1 4P!

I Environmental Conditions C

Temperature: 80.0 Deg. F Humidity: 57%

ICalibration Information C

Calibration was in accordance wiith requirements of MIL-STD-45662A and ANSVNCSL 2540-1 -1 994. Measurements are traceable to the National Institute of Standards and Technology (NIST). This report may not be reproduced except in full without written approval of the originator. Inspection and test data are on file and available for inspection.

Calibration Date: 1 May 97 Cali brat ion Procedure: C LC P-WB-00 1



Remarks: MEASURED UNCElRTAINTY OF BALANCE IS +/- 0.034MG AT 80 DEG. F.

Standards Used I Asset MFR Model Description Serial No. Due Cal 001704 RICE 1 GRAM WEIGHT STANDARD C859 19 Jul97 001706 RICE 2 GRAM WEIGHT STANDARD C86 1 19 Jul97 001720 RICE 1 - 500 MG WEIGHT STANDARDS C858 19 Jul97

Certificate # 25285



Certnficate of Calibration 4 November 1997

Issued to: DARRELL DUNN DIV20 857 Manufacturer/Model: METTLER UMT2 Description: ELECTRONIC BALANCE Serial Number: Asset Number: 002028

21 1001 -1 42

!Environmental Conditions b ~ ~

Temperature: 72.00 Deg. F Humidity: 33 % RH

1 Cali brat ion Information c Calibration was in accordance with requirements of MIL-STD-45662A and ANSVNCSL 2540-1 -1 994. Measurements are traceable to the National Institute of Standards and Technology (NIST). This report may not be reproduced except in full without written approval of the originator. Inspection and test data are on file and available for inspection.

The uncertainty of the calibration was sufficient to determine that the instrument met the manufacturer% specifications.

Calibration Date: 3 Nov 97 Cali bration Procedure: CLCP-WT-001

Interval: 6 months

Next Calibration Due: 3 Nlay 98 Received: In Tolerance

Remarks:

!Standards Used -LI

Asset MFR Model Description

001704 RICELAKE 1G WEIGHT STANDARD 001705 RICELAKE 2G WEIGHT STANDARD 001 720 RICE LAKE 1 MG-500 MG WEIGHT SET

Serial No. Due Cal

C859 C860 C858

n

21 Jul98 21 Jut98 21 Jul98

LAST PAGE OF REPORT Total Pages Printed: 1

Certificate # 27411

Soil t li wes t Resea 1-c h I rist i t ii te 6220 Cri1ebi.a Road

Saii Antonio, TX 78238

C a 1 i b ration L 21 bo 1-23 to r y Del) it rt me 11 t of Qu ;I I i t y Assu I - i l IICC


Issued to: DARRELL DUNN DIV20 Manufacture r/M ode I : ME'TTLER UMT2 Description: ELECTRONIC BALANCE Serial Number: 21 1001 -142 Asset Number: 002028

B57

v ACCREDITED

c ~- ~

IEnvironmental Conditions

Temperature: 73.00 Deg. F Humidity: 62 O/O RH

Calibration was in accordance with requirements of MIL-STD-45662A and ANSVNCSL 2540-1 -1 994. Measurements are traceable to the National Institute of Standards and Technology (NET). This report may not be reproduced except in full without written approval of the originator. Inspection and test data are on file and available for inspection.

The uncertainty of the calibration was sufficient to determine that the instrument met the manufacturer's speci fi cations.

Calibration Date: 4 May 98 Ca I i brat i o n P roced u re : CLCP-WT-001

Interval: 6 months


Remarks: UNCERTAINTY OF +/-0.034 MIL GRAMS

IStandards Used c Asset MFR Model Description Serial No. Due Cal

001706 RICE LAKE 2G WEIGHT STANDARD 001 720 RICE LAKE 1 MG-500 MG WEIGHT SET

LAST PAGE OF REPORT Total Pages Printed 1

C861 C858

21 Jul98 21 Jul 98

Certificate # 29572

\

Iss ed to



ACCREDITED - Certificate #

09 72-0 1

Certificate of Calibration 27 October 1998

DARRELL DUNN Manufacturer/Model: METTLER UMT2 Description: ELECTRONIC BALANCE Serial Number: 21 1001-142 Asset Number: 002028

DIV20 B57

kalibration Information I

Calibration was in accordance with requirements of MIL-STD-45662A and ANSVNCSL 2540-1 -1 994. Measurements are traceable to the National Institute of Standards and Technology (NIST). This report may not be reproduced except in full without written approval of the originator. Inspection and test data are on file and available for inspection.

This laboratory is accredited by the American Association for Laboratory Accreditation (A2LA) and the results shown in this calibration certificate have been determined in accordance with the laboratory's terms of accreditation unless stated otherwise in the report. The uncertainty of the calibration was sufficient to determine that the instrument met the manufacturer's specifications.

Temperature: 70.0 Deg. F Humidity: 65 % RH

Calibration Date: 27 Oct 98 Calibration Procedure: CLCP-WT-001

Interval: 6 months Received: IN TOLERANCE

Next Calibration Due: 27 Apr 99

Remarks:

lSGnd&ds Used b

Asset MFR Model Description Serial No. Due Cal

00170p RICE LAKE 1G WEIGHT STANDARD RICE LAKE 2G WEIGHT STANDARD RICE LAKE 1 MG-500 IblG WEIGHT SET

C859 25 Jun 99 C861 25 Jun 99 C858 25 Jun 99

n

LAST PAGE OF REPORT Total Pages Printed: 1

Certificate # 31805

Southwest Research Institue 6220 Culebra Road

San Antonio, TX 78238

Department of Quality Assurance (210) 522-5215

Calibration Laboratory

Certificate of Calibration 7 April 1999

Accredited

Certificate ## 0972-01

Issued to: DARRELLDU" DIV20 B57 ManufacturerModel: ME"LER UMT2 Description: ELECTRONIC BALANCE

Asset Number: 002028 Serial Number: 211001-142

This certifies the above item was calibrated in compliance with MIL-STD-45662A and ANSVNCSL 2540-1-1994. Standards used in this calibration, described in the referenced calibration procedure with associated uncertainties or tolerances, ame traceable to the National Institute of Standards and Technology (NIST). Supporting documentation relative to traceatility is on file and is available for examination upon request. This certificate is not to be reproduced, except in firll, without the written approval of the Southwest Research Institute Department of Quality Assurance Calibration Laboratory.

This laboratory is accredited by the American Association for Laboratory Accreditation (A2LA) and the results of this calibration certificate were: determined in accordance with the terms of accreditation unless stated o thedse below.

The uncertainty of the calibration was sufficient to determine that the item met the manufacturer's published specifications unless stated otherwise below.

Ambient Conditions: Temperature: 67.0 Degrees Fahrenheit Humidity: 68 'YO RH

Calibration Date: 3 1 Mar 99 Calibration Procedure: CLCP-WT-001 AUG 97

Condition as Received: IN TOLERANCE

Condition as Released: IN TOLERANCE, ADJUSTED

Remarks: MEASURING UNCERTAINTY IS +/-0.034 MILLIGRAMS.

Approved by: _ _

: Jim Patterson, Supervisor or Walt Hill, :Metrologist

Certificate ## 33828 m:\a2la.rpt Rev date 10 Mar 99

I I / Page 1 of 1

Southwest Research Institue 6220 Culebra Road

San Antonio, TX 78238

Department of Quality Assurance (210) 522-5215

Calibration Laboratory

Accredited m

Certificate # 0972-0 1

Certificate of Calibration 30 September 1999

Issued to: DARRELLDUNN DIV20 B57 ManufacturerRModel: METTLER lJMT2 Description: ELECTRONIC BALANCE

Asset Number: 002028 Serial Number: 211001-142

This certifies the above item was calibrated in compliance with MIL-STD-45662A and ANSI/NCSL 2540-1-1994. Standards used in this calibration, described in the referenced calibration procedure with associated uncertainties or tolerances, are traceable to the National Institute of Standards and Technology 0. Supporting documentation relative to traceability is on file and is available for examination upon request. This certificate is not to be reproduced, except in full, without the written approval of the Southwest Research Institute Department of Quality Assurance Calibration Laboratory.

This laboratory is accredited by the American Association for Laboratory Accreditation (A2LA) and the results of t h i s calibration certificate were determined in accordance with the terms of accreditation unless stated otherwise below.

The uncertainty of the calibration was siflicient to determine that the item met the manufacturer's published specifications unless stated otherwise below.

Ambient Conditions: Temperature: 78.0 Degrees Fahrenheit Humidity: 37 % RH

Calibration Date: 30 Sep 99 Calibration Procedure CLCP-WT-001 AUG 97

Condition as Received: IN TOLERANCE

Condition as Released: IN TOLERANCE

Remarks:

n Approved by: d

Jim Patterson, S u w Certificate # 36118 m:Wlrrpt Rev date 10 Mar 99

Page 1 of 1

SOUTHWEST RESEARCH INSTITUTE CALIBRATION LABORATORY

6220 CULEBRA ROAD POST OFflCE DRAWER 28510 SAN ANTONIO, TEXAS 78228-0510 TEL (210) 522-5215 FAX (210) 5223692

Receipt for Work Order 40566 Date Received 9/14/00 ................................... ............................................

Asset No. 002028 Manufacturer METTLER Model UMT2 ........................................................... ............................. ............................................ ....................................

Description ELECTRONIC BALANCE Serial Number 21 1 001 -1 42 ......................................................................................................................................................................................................................... ........................................................

Accessory Received/Required NONE ........................................................................................................................................................................................

Div/CC ID NONE Accessory to Asset No NIA Accuracy MFG SPECS ............................................................................................. ....................................................................................... .........................................................................................................

Custodian DARRELL DUNN Tel. 6090 ................................................... ........................................................... ...................... B57 ............................................. Div/CC DIV20 Location

Char g e/P ro j ec t N 0. 2 0.0 0 7 5 1 . 0 0 6 P ro p r i e t a ry /Co n f i de n ta I ..... N.. ... Date R eq u i red R 0 U TI N E .................................................................................................. ..................................

Work Requested CALIBRATION ONSlTEf ................................................................................................................................................................................................................................................................��

Rece i vi n g I ns pect i o n

Delivered By N/A ....................................................................................................................................................................................................................................................... Tel. 6090

CUSTOMER COMMENTS REQUESTED The Calibration Laboratory staff is committed to good laboratory practice and providing our customers quality calibration services. Please rate how well we are meeting our goal and provide us with your recommendations for im prov em en t .

Quality of service provided Turn-around time Certificates Calibration labels Recall notification Condition of returned equipment Overall service

Rating Scale 4 = Excellent

2 = Acceptable 1 = Needs improvement

3 = Good

Please check all that apply: Equipment user Delivery person Cus tod ian

IF WE PLEASE YOU, TELL OTHERS; IF NOT, TELL US.

COMMENTS:

Name Tel.

workreq.rpt Rev 30 Jan 00

Y

SOUTHW EST RESEARCH INS' 6 2 2 0 C u l e b r a R o a d , P.O. D r a w e r 2 8 5 1 0

Ins t i tu te Q u a l i t y S y s t e m s Ins t i tu te Cal ibra t ion L a b o r a t o r y

P h o n e : 2 1 0 - 5 2 2 - 5 2 1 5 F a x 2 1 0 - 5 2 2 - 3 6 9 2

Certificate of Calibration

ITU T E T M

Submitted By: D I V 2 0 Address: B57 Contact: D A R R E L L D U N N

Manufacturer Model: M E T T L E R U M T 2 Description: BALANCE

Serial No: 2 1 1 0 0 1 - 142 Asset No: 002028

Procedure: CLCP-WT-00 1, 12/99

Work Order: 444049935 Date Issued: 8/20/2002

Calibration Date: Aug 1 9 , 2 0 0 2 ""Calibration Due: F e b 1 9 , 2 0 0 3

Calibration Location: B57 L113 Environment: Temp. 70.O"F Hum. 62 %RH

*As Found: LIMITED CALIBRATION *As Left: LIMITED CALIBRATION

This certificate documents traceability to the National Institute of Standards and Technology (NIST) and the International System of Units (SI). The Laboratory quality system conforms to ISO/IEC 17025, 1999 and ANSI/NCSL 2540-1-1994 which are equivalent to relevant requirements of the IS0 9000-1994 series of standards. This certificate may not be reproduced, except in full, without the written approval of the Southwest Research Institute Calibration Laboratory. The results of this calibration relate only to the individual instrument described above. This certificate shall not be used to claim product endorsement by the American Association for Laboratory Accreditation (A2LA) or any agency of the U. S. Government.

Uncertainty evaluation includes the item under test and is calculated in accordance with the IS0 "Guide to the Expression of Uncertainty in Measurement" (GUM). The uncertainty represents an expanded uncertainty using a coverage factor of k=2 to approximate a 95% confidence level. The calibration process provides a Test Uncertainty Ratio (TUR) of less than or equal to 25% (4: 1) of the test limit unless otherwise stated in remarks or an attachment.

*The client has sole responsibility for determination of inlout olf tolerance or compliancehoncompliance. An in/out of tolerance opinion is provided for your convenience based only on the Test Instrument (TI) reading(s) and limits as reported. The reported uncertainty relates only to the results at the time of calibration and does not imply any short or long term stability of the TI.

**Calibration interval is determined by the client and does not assure the instrument will remain within tolerance until this date. Any number of factors may cause the instrument to be out of tolerance before the next calibration date.

Remarks: U S E R STATED A C C U R A C Y IS +/-0.034. MILLIGRAMS.

Standards Used Asset Manufacturer Model Description Cal Due

00 1705 RICE LAKE 2G WEIGHT, CLASS 2 Jun 14 ,03 00 1704 RICE LAKE 1G WEIGHT, CLASS 1 Jun 14,03 001720 RICE LAKE 1MG-500 MG WEIGHT SET, CLASS 1 Jun 14,03

Approved by: Walt Hill Metrology Group Leader m:Wona2lal.rpt Rev date 15, August 02

Metrology Technician Page 1 of 1

Southwest Research lnst it u te Calibration Laboratory Calibration Data Sheet

Location: Bldg. 57/ Lab 113 I IAmbient Conditions: 70 F 62 %RH 14.18 PSlA

Operational Check: Limits +/- : 0.0000340 g Uncertainty: 0.0000746 g

STD Mass As Found Instrument Load I n d ica t ion Error

Post Calibration Check:

STD Mass Post calibration Instrument

Repeatability Check: Mass Load: 1.0000000 g

1 2 3 4 5 , Std Dwiation Tolerance

0.0000074 g 0.0000340 g I : k: Mass Load: 1 .OOOOOOO g Uncertainty: 0.0000746 g

Instrument I n d i cat io n Error +/- Limits Resu Its

1 2 3 4

I I

Non-Linearity Check: Fta ng e : 2.0000000 g Uncertainty: 0.0000746 g

STD Mass Instrument Load In d icat i o n Error +/- Limits Results

Datasheets, Mettler.xls 20 August 2002, Rev. 01 Page 1 of 1

L

SOUTHW EST RESEARCH INS' 622:O C u l e b r a Road, P.O. Drawer 285 10

Ins t i t u t e Qual i ty S y s t e m s Ins t i t u t e C a l i b r a t i o n L a b o r a t o r y

Phone: 210-522-5215 F a x 210-522-3692 Certificate of Calibration

TITU TETM

Submitted By: DIV20 Address: B57 Contact: DARRELL DUNN

Manufacturer Model: METTLER UMT2 Description: BALANCE

Serial No: 21 1001-142 Asset No: 002028

Procedure: CLCP-WT-001, 12/99

Work Order: 444052194 Date Issued: Jan 30,2003

Calibration Date: Jan 29, 2003 **Calibration Due: Jul29, 2003

Calibration Location: B57 LAB 113 Environment: Temp. 72.O"F Hum. 53 %RH

*As Found: SEE ATTACHED DATA *As Left: SEE ATTACHED DATA

This certificate documents traceability to the National Institute of Standards and Technology (NIST) and the International System of Units (SI). The Laboratory quality system conforms to ISO/IEC 17025, 1999 and ANSI/NCSL 2540-1-1994 which are equivalent to relevant requirements of the IS0 900G1994 series ofstandards. This certificate may not be reproduced, except in full, without the written approwl ofthe Southwest Research Institute Calibration Laboratory. The results of this calibration relate only to the individual instrument described above. This certificate shall not be used to claim product endorsement by the American Association for Laboratory Accredtation (A2LA) or any agency ofthe U. S. Government

Uncertainty evaluation includes the item under test and is calculated in accordance with the IS0 "Guide to the Expression of Uncertainty in Measurement" (GUM). The uncertainty represents an expanded uncertainty using a coverage factor ofk=2 to approximate a 95% confidence level. The calihation process provides aTest Uncertainty Ratio (TUR) of less than or equal to 25% (4: 1) ofthe test limit unless otherwise stated in remarks or an attachment

*The client has sole responsibility for determination of in/out oftolerance or compliance/noncompliance. An in/out of tolerance opinion is povided for your convenience based on@ on the Test Instrument (TI) reading(s) and limits as reported. The reported uncertainty relates only to the results a t the time ofcalibration and does not imply any short or long term stability ofthe TI.

**Calibration interval is determined by the client and does not assure the instrument will remain within tolerance until this date. Any number of factors may cause the instrument to be out of tolerance before the next calibration date. Remarks: None

Standards Used Asset Manufacturer Model Description Cal Uue

007 102 TROEMNER 1MGTO lOOG WEIGHT SET, CLASS El Jun 13,03

Approved by: Walt Hill Metrology Group Leader n:\Nona2lal.rpt Revdate 15, August 02

Metrology Technician 1 of 1

So ut hwest Research Institute Calibration La bora tory Calibration Data Sheet

. Work Order 444052194 Mfr. Mettler Technician Mark A. Romero Asset No. 002028 Model UMT2 Procedure CLCP-WT-001. 12/99

Location: Bldg. 57/ Lab 113 I IAm bient Conditions: 72 F 53 %RH 14.21 PSlA

Limits +/- : 14.3 ug Uncertainty: 20.4 ug

Nominal Conventional Weight Value Value (Di'sola v) Deviation

Post Calibration Check:

Nominal Conventional Weight Value Adjustment Value Mass De via tion

Repeatability Check: Mass Load: 2000000.0 ug

1 2 3 4 5

Std Deviation Tolerance 0.8 ug 0.5 ug I

I Off -Centerline Check: Mass Load: 1000000.0 ug Uncertainty:

In strum en t Indication Error +/- Limits

1 2 3 4

20.4 ug

2000000.0 ug Uncertainty: 20.4 ug

Nominal Conventional Weight Value

Datasheets, Mettler 20 January 2003, Rev. 01 Page 1 of 1

, J

S O U T H W E S T R E S E A R C H INSTITUTETM 6220 C u l e b r a R o a d , P . O . D r a w e r 28510

Ins t i t u t e Q u a l i t y S y s t e m s Inst i tute Cal ibra t ion L a b o r a t o r y

P h o n e : 210-522-5215 F a x 210-522-3692

0972-01 Certificate of Calibration



Serial No: 2 1 100 1 - 142 Asset No: 002028

Procedure: CLCP-WT-00 1, DEC/99

Work Order: 444055472 Date Issued: Oct 2,2003

Calibration Date: Oct 2, 2003 **Calibration Due: Apr 2, 2004

Calibration Location: B57 Environment: Temp. 73.O"F Hum. 48 %RH


This certificate documents traceability to the National Institute of Stimdards and Technology (NIST) and the International System of Units (SI). The Laboratory quality system conforms to ISO/IEC 17025, 1999 and ANSWCSL 2540-1-1994 which areequivalent to relevant requirements of the IS0 900@ 1994 series ofstandards. This certificate may not be reprodwed, except in full, without the written approml ofthe Southwest Research Institute Calibration Laboratory. The results of this calibration relate only to the individual instrument described above. This certificate shall not be used to claim poduct endorsement by the American Association for Laboratory Accreditation (A2LA) or any agency ofthe U. S. Government

Uncertainty evaluation includes the item under test and is calculated in accordance with the IS0 "Guide to the Expession of Uncertainty in Measurement" (GUM). The uncertainty represents an expanded uncertainty using a coverage factor ofk=2 to approximate a 95% confidence level. The calikation process provides aTest Uncertainty Ratio (TUR) of less than or equal to 25% (4: 1) of the test limit unless otherwise stated in remarks or an attachment

*The client has sole responsibility for determination of idout oftolerance or compliance/noncompliance. An in/out of tolerance opinion is povided for your convenience tased only on the Test Instrument (TI) reading(s) ard limits as reported. The reported uncertainty relates only to the results at the time of calibration and does not imply any short or long term stability ofthe TI.

**Calibration interval is determined bj the client and does not a s w e the instrument will remain within tolerance until this date. Any number of factors may cause the instrument to be cut of tolerance before the next calibration date. Remarks: None


007 102 TROEMNER 1MG TO lOOG WEIGHT SET, CLASS E l Aug 29,04

Approved by: Walt Hill Metrology Group Leader m:\dlal.rpt Rev date 15, August 02 1 of 1

c . L.

Southwest Research Institute Calibration La bora tory Calibration Data Sheet

IAmbient Conditions: 73 F 48 %RH 14.35 PSlA

Operational Check: Limits +/- : 14.3 ug Uncertainty: 20.4 ug

Nominal Conventional Weight Value Value (Display) De via tion

2000000.0 1999995.6 u 2000399.2 ug 403.6 ug I Post Calibration Check:

Nominal Conventional Weight Value Adjustment Value (Disda Y ) De via tion

Re peata bi I ity Check: Mass Load: 2000000.0 ug

1 2 3 4 5

Std Deviation To le ra n ce I 19.1 uq 0.5 uq I

Off-Centerline Check: Mass Load: 1000000.0 ug Uncertainty: 20.4 ug

lnstrumen t Indication Error +/- Limits

I 2 3

Rang e : 2000000.0 ug Uncertainty: 20.4 ug

m 4 Non-Linearity Check:

Conventional Weight Value Mass (Dimla v) De via tion +/- Limits

1500000.0 500002.2 ug 499991.1 ug -1.5 ug 2.0 2000000.0 499994.6 ug 499992.3 ug -0.3 ug 2.0

__-____ Remarks: * Data is provided without regard to ‘pass” or “fail“. The end user is responsible ____ in determining __ whether the results meet

their - . requirements. _. - - - . . - _ _ . _.

Readability is 0. lug. Standard used 7702. __________

Datasheets, Mettler.xls 20 January 2003, Rev. 01 Page 1 of 1

&

S O U T H W E S T R E S E A R C H INSTITUTETM 6 2 2 0 C u l e b r a R o a d , P . O . D r a w e r 2 8 5 1 0

Ins t i tu te Qua l i ty S y s t e m s Ins t i tu te C: a l ibra t ion Labora to ry

P h o n e : 2 1 0 - 5 2 2 - 5 2 1 5 F a x 210-522-3692

Certificate of Calibration 0972-01




Procedure: CLCP-WT-00 1 , DEC/99

Work Order: 444058 18 1 Date Issued: Apr 6,2004

Calibration Date: Apr 2, 2004 **Calibration Due: Oct 2, 2004



This certificate documents traceability to the National Institute of Standards and Technology (NIST) and the International System of Units (SI). The Laboratory quality system conforms to ISO/IEC 17025, 1999 and ANSL'NCSL 2540-1-1994 which areequivalent to relevant requirements of the IS0 900@ 1994 series ofstandards. This certificate may not be reproduced, except in full, without the written approml of the Southwest Research Institute Calibration Laboratory. The results of this calibration relate only to the individual instrument described above. This certificate shall not be used to claim pcduct endorsement by the American Association for Laboratory Accreditation (A2LA) or any agency ofthe U. S. Government

Uncertainty evaluation includes the item under test and is calculated in accordance with the IS0 "Guide to the Expession of Uncertainty in Measurement" (GUM). The uncertainty represents an expanded uncertainty using a coverage factor ofk=2 to approximate a 95% confidence level. The calibration process provides aTest Uncertainty Ratio (TUR) of less than or equal to 25?? (4: 1) of the test limit unless otherwise stated in, remarks or an attachment

*Theclient has sole responsibility for determination of idout of tolerance or compliance/noncompliance. An in/out of tolerance opinion is provided for ycur convenience based only on the Test Instrument (TI) reading@) a d limits as reported. The reported uncertainty relates only to the results at the time ofcalibration and does not imply any short or long term stability oftheTI.

**Calibration interval is determined by the client and does not assure the instrument will remain within tolerance until this date. Any number of factors may cause the instrument to be cut of tolerance before the next calibration date. Remarks: None


00 1705 RICE LAKE 001704 RICE LAKE 001720 RICE LAKE

2G 1G 1MG-500 MG

WEIGHT, CLASS 2 WEIGHT, CLASS 1 WEIGHT SET, CLASS 1

Jun 23 ,04 Jun 23 ,04 Jun 20,04

f

Approved by: Walt Hill Metrology Group Leader m:\a2lal .rpt Rev date 15, August 02 W 1 of 1

Southwest Research Institute Calibration Laboratory Calibration Data Sheet

Found / Left

Location: Bldg. 571 Lab L105 I IAmbient Conditions: F %RH PSlA

Operational Check: Limits +/- : 14.3 ug Uncertainty: 20.4 ug

I Nominal Conventional Weight Value

Repeatability Check: Mass Load: 2000000.0 ug

I 2 3 4 5

Std Deviation Tolerance 0.5 ug I I 3.8 ug

Mass Load: 1000000.0 ug Uncertainty: 20.4 ug

lnstrumen t Indication Error +/- Limits

Non-Linearity Check: I Fta n g e: 2000000.0 ug Uncertainty: 20.4 ug

Nominal Conventional Weighlt Value

Page 1 of 1 Datasheets, Mettler.xls 20 January 2003, Rev. 01

~ ~~ ~ ~~~~~~~ ~

SOUTHWEST RESEARCH INSTITUTETM 6220 C u l e b r a R o a d , P . O . Drawer 285 1 0

Ins t i tu te Q u a l i t y Systems Ins t i tu t e C a l i bra ti on Lab o r a t o r y

P h o n e : 2 10-522-52 1 5 Fax 2 1 0 - 5 2 2 - 3 6 9 2 Certificate of Calibration



Serial No: 2 1 1001-142 Asset No: 002028

Procedure: CLCP-WT-00 1, DEC/99

Work Order: 444061018 Date Issued: Oct 1, 2004

Calibration Date: Oct 1, 2004 **Calibration Due: Apr 1,2005



This certificate documents traceability to the National Institute of Standards and Technology (NIST) and the International System of Units (SI). The Laboratory quality system conforms to ISO/IEC 17025, 1999 and ANSI/NCSL 2540-1-1994 which are equivalent to relevant requirements of the I S 0 900@ 1994 series ofstandards. This certificate may not be reproduced, except in full, without the written approval ofthe Southwest Research Institute Calibration Laboratory. The results of this calibration relate only to the individual instrument described above. This certificate shall not be used to claim poduct endorsement by the American Association for Laboratory Accreditation (A2LA) or any agency ofthe U. S. Government

Uncertainty evaluation includes the item under test and is calculated in accordance with the IS0 "Guide to the Expession of Uncertainty in Measurement" (GUM). The uncertainty represents an expanded uncertainty using a coverage factor ofk=2 to approximate a 95% confidence level. See Remarks a attached Calibration Report with thesame Work Order number for calilxation data

*The client has sole responsibility for determination of idout ofto1ei:ance or compliancehoncompliance. An in/out of tolerance opinion is povided for your convenience bsed only on the Test Instrument (TI) reading(s) and limits as reported. The reported uncertainty relates only to the results at the time ofcalibration and does not imply any short or long term stability of the TI.

**Calibration interval is determined by the client and does not assure the instrument will remain within tolerance until this date. Any number of factors may cause the instrument to be out of tolerance before the next calibration date. Remark: Readings are without pass or fail indication. Customer must determine if measurements meet their needs.

Standards Used Asset Manufacturer Model Descrip tion Cal Due

005566 007290 001 704 001705 001720

MERIAN VAISALA RICE LAKE RICE LAKE RICE LAKE

A0030P HM34F 1G 2G 1MG-500 MG

Approved by: Walt Hill Metrology Group Leader n:\Nona2lal. rpt Rev date 1 1, May 04

PRESSURE GAUGE, ABSOLUTE Oct 15,04 HUMIDTY/ TEMPERATURE METER Apr 07 ,05 WEIGHT, CLASS 1 Jun 23,05 WEIGHT, CLASS 2 Jun 23 ,05 WEIGHT SET, CLASS 1 Jun 23,05

Measurements by: Scott Kester Metrology Technician

1 of 1

Southwest Research Institute Calibration Laboratory Measurement Report

Work Order: 444061018 Mfr. Mettler Asset No. 002028 Model UMT2

Technician SRK

Serial No. 21 1001-142 ITyple. Balance (Cat Date. 0 1 -0ct-04 Remarks: Readings are without pass or fail indications. Customer must determine if measurements meet their needs. Ambient Conditions 74 deg F 73 % RH 14.22 PSlA

FunctionIRange Test Point TI Reading Difference +/-Limit +/-Uncertainty

Repeatability Check ug ug ug ug ug 1 2000000.0 200001 3.2 2 2000000.0 2000014.7 3 2000000.0 2000002.6 4 2000000.0 200001 1.6 5 2000000.0 1999998.3 6 2000000.0 2000007.9 7 2000000.0 2000006.2 8 2000000.0 2000031 .O 9 2000000.0 2000004.7 10 2000000.0 1999996.9

Std Deviation 9.8

Front 1000000.0 1000014.6 14.6

Rear 1000000.0 1000014.4 14.4 Left 1000000.0 1000008.6 8.6

Offcenter Check

Right 1000000.0 100001 1.1 11.1

Non I i neari ty Check 0 0.0 0.0 0.0

500000 499996.3 :500005.1 8.8

1500000 499983.2 50001 5.9 32.7 2000000 500012.0 500036.5 24.5

End of Report

1000000 499986.9 1499968.2 -1 8.7

0.5

2.0 2.0 2.0 2.0

2.0 2.0 2.0 2.0 2.0

3.0 3.0 3.0 3.0

2.4 2.5 3.0 3.1 2.8

Rev, OcVO4 Page 1 of 1 Mettler U MT2.xls

S O U T H W E S T R E S E A R C H INS' 6220 Culebra Road , P . O . Drawer 2 8 5 1 0

Institute Quality Sys t ems Institute Calibration Laboratory

Phone : 210-522-5215 Fax 210-522-3692

Certificate of Calibration

TIT U T E T M

Certificate #

0972-01

Submitted By: DIV20 Address: B57 Contact: DARRELL D U "



Procedure: BALANCES & SCALES, DEC/04

Work Order: 303063529 Date Issued: Apr 4,2005

Calibration Date: Apr 1 , 2005

Calibration Location: B57 **Calibration Due: Sep 30, 2005

Environment: Temp. 73.O"F Hum. 22 %RH *As Found: SEE ATTACHED DATA

*As Left: SEE ATTACHED DATA

This certificate documents traceability to the National Institute of Standards and Technology (NIST) and the International System of Units (SI). The Laboratory quality system conforms to ISO/IEC 17025, 1999 and ANSIOJCSL 2540-1-1994 which are equivalent to relevant requirements of the IS0 9000-1994 series of standards. This certificate may not be reproduced, except in full, without the written approval of the Southwest Research Institute Calibration Laboratory. The results of this calibration relate only to the individual instrument described above. This certificate shall not be used to claim product endorsement by the American Association for Laboratory Accreditation (A2LA) or any agency of the U. S. Government.

Uncertainty evaluation includes the item under test and is calculated in accordance with the IS0 "Guide to the Expression of Uncertainty in Measurement" (GUM). The uncertainty represents an expanded uncertainty using a coverage factor of k=2 to approximate a 95% confidence level. See Remarks or attached Calibration Report with the same Work Order number for calibration data.

T h e client has sole responsibility for determination of inlout of tolerance or compliance/noncompliance. An idout of tolerance opinion is provided for your :onvenience based only on the Test Instrument (TI) reading(s) and limits as reported. The reported uncertainty relates only to the results at the time of calibration md does not imply any short or long term stability of the TI.

"Calibration interval is determined by the client and does not assure the instrument will remain within tolerance until this date. Any number of factors may cause h e instrument to be out of tolerance before the next calibration date.

Remarks: None

standards Used Manufacturer Model Description Cal Due Asset

007290 00 1704 00 1705 001720 005566

VAISALA RICE LAKE RICE LAKE RICE LAKE MERIAN

HM34F 1G 2G 1MG-500 MG A0030P

4pproved by: Walt Hill vletrology Group Leader n:\a2lal .rpt Rev date 1 1, May 04

HUMIDTY/ TEMPERATURE METER Apr 07,05 WEIGHT, CLASS 1 Jun 23,05 WEIGHT, CLASS 2 Jun 23,05 WEIGHT SET, CLASS 1 Jun 23,05 PRESSURE GAUGE, ABSOLUTE Apr 14,05

I

Measurements by: Scott Kester Metrology Technician

Page 1 of 1

k

Work Order: 303063529 Asset No. 002028

Southwest Research Institute Cali bration Laboratory Measurement Report

Mfr. Mettler Technician SRK Model UMT2

Serial No. 21 1001-142 IType. Balance lCal Date. 01 -Apr-05 Remarks: Readings are witholut pass or fail indications. Customer must determine if measurements meet their needs. Ambient Conditions 73 O F 22 % RH 14.44 PSlA

Function/Range Test Point TI Reading Difference +/-Limit +/-U ncertai n ty

Repeatability ug ug ug ug ug 1 1000000.0 !399977.7 2 1000000.0 !3 9 9 9 82.4 3 1000000.0 !39 998 3.0 4 1000000.0 99 99 80.4 5 1000000.0 999983.1 6 1000000.0 99 99 80.6 7 1000000.0 13 99 96 8.8 8 1000000.0 $399981.6 9 1000000.0 $399984.3 10 1000000.0 $399970.5

Std Deviation 5.39 0.50 Nonlinearity Check

0 ug 0.0 0.0 0.0 2.0 8.9 200000 ug 199999.8 II 99999.8 0.0 2.0 8.9 400000 ug 399994.0 3 99999.4 5.4 2.0 8.9 600000 ug 599999.0 600007.8 8.8 2.0 8.9 800000 ug 799998.8 €!00004.1 5.3 2.0 8.9 1000000 ug 999986.9 99 9986.8 -0.1 2.0 8.9 1200000 ug 1 199986.7 1 199986.7 0.0 2.0 8.9 1400000 ug 1399980.9 1$399986.3 5.4 2.0 8.9 1600000 ug 1599985.9 11599981.5 -4.4 2.0 8.9 1800000 ug 1799985.7 1'799997.4 11.7 2.0 8.9 2000000 ug 2000012.0 200001 8.0 6.0 2.0 8.9

End of Report

Rev, OW04 Page 1 of 1 Mettler UMT2.xls

Documents

Department of CERTIFICATE OF CALIBRATION Issued to: … · run #2 i run #3 mean i std. dev. n a hinp 8 trnirin ati~li i ~nyuc vcniribn i iuiy position guide range #l range #2 range