Condition: Bi annual Leachate Monitoring Report 2020

Document Title:

Leachate Report Round 1

Document Ref: RP 5.1.5

Responsibility: Facility Manager / Environmental Manager

Licence Condition:

Author: Patrick Rogers

Version: 001 Version Date: 12th June 2020

Integrated Materials Solutions Partnership Limited W0129‐02

Page 1 of 12

ROUND 1 2020

Integrated Materials Solutions Licence No. W0129-02

Bi‐annual Leachate Monitoring Report 2020

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Table of Contents 1.0 Introduction .............................................................................................................................. 3

1.1 Background ................................................................................................................................ 3

1.2 Sampling Locations .................................................................................................................... 3

Table 1: Leachate Monitoring Locations .......................................................................................... 3

1.3 Sampling & Analysis .................................................................................................................. 4

1.3.1 Sampling Personnel ................................................................................................................ 4

1.3.2 Sampling Methodology ........................................................................................................... 4

1.3.3 Laboratory details ................................................................................................................... 4

1.3.4 Interpretation of Results .......................................................................................................... 4

2.0 Results .................................................................................................................................... 5

2.1 Leachate Analysis ...................................................................................................................... 5

Table 2.1: Leachate Monitoring Results for LC1 (Lab Cert No.20/7108) ............................................ 5

Table 2.2: Leachate Monitoring Results for LC3 (Lab Cert No.20/7109) ........................................ 6




Table 2.6: Leachate Monitoring Results for LC7 (Lab Cert No.20/7120) ...................................... 10

3.0 Discussion ................................................................................................................................... 11

4.0 Conclusion ................................................................................................................................... 11

Appendix 1 ............................................................................................................................................ 12

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1.0 Introduction

1.1 Background Integrated Materials Solutions Limited Partnership (IMS) operates a landfill for inert waste at its site at Hollywood Great, Nag’s Head, Naul, Co. Dublin. The site is a former shale and limestone quarry. Restoration of the site will return it to pre‐quarrying conditions and blend it into the surrounding landscape As part of the requirements set out in EPA Waste License No. W0129‐02, Integrated Materials Solutions (IMS) are required to monitor Leachate Bi‐annually (see Schedule D of License) at several locations across site. Sampling was carried out by Patrick Rogers (BSc (Hons), & Jason Mc Guirk (BSc (Hons), of IMS on the 4th of June 2020 and the samples taken were appropriately stored prior to being transported to a certified laboratory for analysis.

1.2 Sampling Locations

Table 1: Leachate Monitoring Locations

Name/Ref Location Co‐ordinates

LC1 Leachate monitoring borehole within Cell 1

53.560372, ‐6.256196

LC3 Leachate monitoring borehole within Cell 3 extension

53.559572, ‐6.255890


53.560015, ‐6.256963


53.560132, ‐6.253507


53.560525, ‐6.253122


53.561465, ‐6.252693

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1.3 Sampling & Analysis

1.3.1 Sampling Personnel Sampling was carried out by Patrick Rogers (BSc (Hons), and Jason Mc Guirk (BSc (Hons), of IMS Ltd. on the 4th of June 2020.

1.3.2 Sampling Methodology Samples were extracted from monitoring boreholes using bailers and filled into the corresponding sampling bottles. Temperature was not recorded due to meter being inoperable at the time. All samples were estimated to be <15˚C prior to chilling. The samples were labelled, place in a cooler box and appropriately stored at 4˚C according to standard sampling techniques. The samples were sent via courier to Element Materials Technology Laboratories for chemical analysis.

1.3.3 Laboratory details Analysis of the surface water samples were conducted by Element Materials Technology. Element Materials Technology is UKAS and MCERTS accredited. Certified laboratory results are included as Appendix 1.

1.3.4 Interpretation of Results Results were received on the 12th of June 2020 (See Appendix 1.) These results were tabulated and compared against Waste Acceptance Criteria values listed in Table A.4.1 of EPA Licence W0129‐02 and the EPA Parameters of Water Quality – Interpretation and Standards (2001). If results exceeded limits prescribed in legislation or trigger levels, these would be highlighted in the report and possible causes described.

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2.0 Results 2.1 Leachate Analysis

2.1.1 Laboratory results for Q2, 2020 are attached in Appendix 1.

2.1.2 The results of analysis of Leachate for Q2, 2020, as well as historic monitoring results, are given in Tables 2.1 – 2.6.

2.1.3 If results were in excess of limits prescribed in legislation, these would be

highlighted in the tables and possible causes would be investigated and discussed.

2.1.4 Only parameters which are found to be in excess of the limit value concentrations and/or EPA trigger levels for the site and which are directly attributable to site operations, are reported to The Agency as “Incidents”.

Table 2.1: Leachate Monitoring Results for LC1 (Lab Cert No.20/7108)

Parameter Units WAC W0129‐ 02 Table A.4.1

Q2, 2020 Q4, 2019 Q2, 2019 Q2, 2018

Ammoniacal Nitrogen mg/l NH4‐N

‐ 3.0 9.74 1.56 0.36

Chloride mg/l 800 26.7 103.3 77.4 78.4

COD mg/l ‐ 8 36 27 28

Colour N/A ‐ Clear Clear Clear Clear

Conductivity mS/cm ‐ 0.62 1.7 1.3 1.6

Leachate Level m aOD Malin

‐ 122.98 121.90 122.58 121.49

List I & II Substances mg/l ‐ N/A <0.0001 <0.00003 N/A

Odour N/A ‐ None None None Sulphurous

Organic Carbon, Dissolved

500

<2 13 6 6

Organic Carbon, Total mg/l ‐ 6 11 8 6

pH mg/l ‐ 7.47 7.3 7.0 7.4

Potassium pH ‐ 30.1 44.7 30.4 35.2

Sodium mg/l ‐ 93.7 124.2 78.1 96.6

Sulphate mg/l 1000 154.2 665.6 976.6 914.9

Total Oxidised Nitrogen

mg/l ‐ 2.0 4.3 <0.2 0.9

Total Phenols mg/l ‐ <0.15 <0.2 <0.2 <0.2

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Q2, 2020 Q4, 2019 Q2, 2019 Q2, 2018


‐ 0.40 0.05 <0.03 0.05

Chloride mg/l 800 109 83.1 81.6 157.6

COD mg/l ‐ 27 27 25 27

Colour N/A ‐ Clear Clear Clear Black precipitate



‐ 112.93 113.54 119.20 115.10


Odour N/A ‐ None None None None


500

9 11

6

10

Organic Carbon, Total mg/l ‐ 8 8 16 9

pH mg/l ‐ 7.69 7.4 7.5 7.8

Potassium pH ‐ 31.8 35.4 32.8 35.7

Sodium mg/l ‐ 98.7 117.7 106.8 141.3

Sulphate mg/l 1000 841 633.5 711.9 908.5


mg/l ‐ <0.2 1.0 0.7 <0.2


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Q2, 2020 Q4, 2019 Q2, 2019 Q2, 2018


‐ 0.14

Insufficient sample volume

0.21 1.20

Chloride mg/l 800 364.9 222 315.7

COD mg/l ‐ 263 140 305

Colour N/A ‐ Yellow Tinge Black SS Black

Conductivity mS/cm ‐ 2.7 1.5 1.9


‐ 107.3 107.33 107.39

List I & II Substances mg/l ‐ N/A <0.00003 N/A

Odour N/A ‐ None None Sulphurous


500

96 49

103

Organic Carbon, Total mg/l ‐ 95 50 106

pH mg/l ‐ 7.91 7.3 8.0

Potassium pH ‐ 62 49.1 68.6

Sodium mg/l ‐ 318.5 180.2 245.6

Sulphate mg/l 1000 655.6 976.5 662.3


mg/l ‐ 5.6 5.3 2.0

Total Phenols mg/l ‐ <0.15 <0.2 <0.2

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Q2, 2020 Q4, 2019 Q2, 2019 Q2, 2018


‐ 7.14 8.6 1.8 11.4

Chloride mg/l 800 333.1 402.9 145.7 932.6

COD mg/l ‐ 92 108 39 75

Colour N/A ‐ Clear Green tinge Green tinge Green tinge



‐ 109.61 117.78 108.27 106.52


Odour N/A ‐ None Sulphurous Sulphurous Sulphurous


500

32 38

16

39

Organic Carbon, Total mg/l ‐ 32 38

14

41

pH mg/l ‐ 10.54 11.2 8.7 11.3

Potassium pH ‐ 46.1 32.8 43.3 35.7

Sodium mg/l ‐ 340.1 370.2 185.9 558.2

Sulphate mg/l 1000 661.2 435.2 808.4 236.6


mg/l ‐ <0.2 8.6

7.2

<0.2

Total Phenols mg/l ‐ <0.15 <0.2 <0.2 0.5

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Q2, 2020 Q4, 2019 Q2, 2019 Q2, 2018


‐ 8.90 7.95 3.82 2.63

Chloride mg/l 800 285.5 233.5 149.9 291.8

COD mg/l ‐ 88 82 78 52

Colour N/A ‐ Clear Brown Tinge Clear Clear



‐ 110.25 109.55 109.10 106.92


Odour N/A ‐ None None None None


500

29 28

20

15


23

15

pH mg/l ‐ 10.83 10.6 9.7 8.7

Potassium pH ‐ 38.8 43.4 34.1 34.8

Sodium mg/l ‐ 190.6 181.0 127.0 279.2

Sulphate mg/l 1000 502.9 545.8 753.1 1125.8


mg/l ‐ 0.4 0.5 2.4 0.9


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Q2, 2020 Q4, 2019 Q2, 2019 Q2, 2018


‐ 8.02

No Access

12.57 10.72

Chloride mg/l 800 314.5 413.4 204.7

COD mg/l ‐ 74 100 84

Colour N/A ‐ Yellow Tinge Clear Clear

Conductivity mS/cm ‐ 2.5 1.2 1.9


‐ 110.54 110.27 107.38

List I & II Substances mg/l ‐ N/A <0.0003 N/A

Odour N/A ‐ Slight Odour Sharp Smell None


500

21 29

26


26

pH mg/l ‐ 11.72 10.6 12.2

Potassium pH ‐ 67.8 108.8 90.9

Sodium mg/l ‐ 317.0 354.6 265.6

Sulphate mg/l 1000 270.6 190.1 245.4


mg/l ‐ <0.2 0.6

1.3

Total Phenols mg/l ‐ <0.15 <0.2 0.3

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Appendix 1

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Element Materials Technology P: +44 (0) 1244 833780

Unit 3 Deeside Point F: +44 (0) 1244 833781

Zone 3

Deeside Industrial Park W: www.element.com

Deeside

CH5 2UA

IMS Integrated Material Solutions Limited Partnership

Attention :

Date :

Your reference :

Our reference :

Location :

Date samples received :

Status :

Issue :

Please include all sections of this report if it is reproduced

Nags Head

Hollywood

Naul

Co Dublin

Ireland

Jason McGuirk

12th June, 2020

Leachate Testing No.1

Test Report 20/7108 Batch 1

Hollywood

5th June, 2020

Final report

Senior Project Manager

1

One sample was received for analysis on 5th June, 2020 of which one was scheduled for analysis. Please find attached our Test Report which

should be read with notes at the end of the report and should include all sections if reproduced. Interpretations and opinions are outside the scope of

any accreditation, and all results relate only to samples supplied.

All analysis is carried out on as received samples and reported on a dry weight basis unless stated otherwise. Results are not surrogate corrected.

Authorised By:

Phil Sommerton BSc

Element Materials Technology Environmental UK Limited

Registered in England and Wales

Registered Office: 10 Lower Grosvenor Place, London, SW1W 0EN

Company Registration No: 11371415 1 of 11

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Client Name: Report : Liquid

Reference:

Location:

Contact: Liquids/products: V=40ml vial, G=glass bottle, P=plastic bottle

EMT Job No: 20/7108 H=H2SO4, Z=ZnAc, N=NaOH, HN=HN03

EMT Sample No. 1-8

Sample IDIMS

LEACHATE

NO.1

Depth

COC No / misc

Containers V H HN P G

Sample Date 04/06/2020 09:00

Sample Type Ground Water

Batch Number 1

Date of Receipt 05/06/2020

Odour Absent None TM129/PM0

Odour Type none None TM129/PM0

Dissolved Potassium # 30.1 <0.1 mg/l TM30/PM14

Dissolved Sodium # 93.7 <0.1 mg/l TM30/PM14

Pesticides

Organochlorine Pesticides

Aldrin <0.01 <0.01 ug/l TM149/PM30

Alpha-HCH (BHC) <0.01 <0.01 ug/l TM149/PM30

Beta-HCH (BHC) <0.01 <0.01 ug/l TM149/PM30

Delta-HCH (BHC) <0.01 <0.01 ug/l TM149/PM30

Dieldrin <0.01 <0.01 ug/l TM149/PM30

Endosulphan I <0.01 <0.01 ug/l TM149/PM30

Endosulphan II <0.01 <0.01 ug/l TM149/PM30

Endosulphan sulphate <0.01 <0.01 ug/l TM149/PM30

Endrin <0.01 <0.01 ug/l TM149/PM30

Gamma-HCH (BHC) <0.01 <0.01 ug/l TM149/PM30

Heptachlor <0.01 <0.01 ug/l TM149/PM30

Heptachlor Epoxide <0.01 <0.01 ug/l TM149/PM30

o,p'-Methoxychlor <0.01 <0.01 ug/l TM149/PM30

p,p'-DDE <0.01 <0.01 ug/l TM149/PM30

p,p'-DDT <0.01 <0.01 ug/l TM149/PM30

p,p'-Methoxychlor <0.01 <0.01 ug/l TM149/PM30

p,p'-TDE <0.01 <0.01 ug/l TM149/PM30

Organophosphorus Pesticides

Azinphos methyl <0.01 <0.01 ug/l TM149/PM30

Diazinon <0.01 <0.01 ug/l TM149/PM30

Dichlorvos <0.01 <0.01 ug/l TM149/PM30

Disulfoton <0.01 <0.01 ug/l TM149/PM30

Ethion <0.01 <0.01 ug/l TM149/PM30

Ethyl Parathion (Parathion) <0.01 <0.01 ug/l TM149/PM30

Fenitrothion <0.01 <0.01 ug/l TM149/PM30

Malathion <0.01 <0.01 ug/l TM149/PM30

Methyl Parathion <0.01 <0.01 ug/l TM149/PM30

Mevinphos <0.01 <0.01 ug/l TM149/PM30

Total Phenols HPLC <0.15 <0.15 mg/l TM26/PM0

Sulphate as SO4 # 154.2 <0.5 mg/l TM38/PM0

Chloride # 26.7 <0.3 mg/l TM38/PM0

Total Oxidised Nitrogen as N # 2.0 <0.2 mg/l TM38/PM0

Ammoniacal Nitrogen as N # 3.00 <0.03 mg/l TM38/PM0

Hollywood

Jason McGuirk

Please see attached notes for all

abbreviations and acronyms

LOD/LOR UnitsMethod

No.

Element Materials Technology



QF-PM 3.1.2 v11Please include all sections of this report if it is reproduced

All solid results are expressed on a dry weight basis unless stated otherwise. 2 of 11

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Location:



EMT Sample No. 1-8

Sample IDIMS

LEACHATE

NO.1

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1


COD (Settled) # 8 <7 mg/l TM57/PM0

Dissolved Organic Carbon # <2 <2 mg/l TM60/PM0

Electrical Conductivity @25C # 620 <2 uS/cm TM76/PM0

pH # 7.47 <0.01 pH units TM73/PM0

Total Organic Carbon # 6 <2 mg/l TM60/PM0

True Colour <15 <15 PCU TM35/PM0

LOD/LOR UnitsMethod

No.




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Client Name: SVOC Report : Liquid

Reference:

Location:

Contact:

EMT Job No: 20/7108

EMT Sample No. 1-8

Sample IDIMS

LEACHATE

NO.1

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1


SVOC MS

Phenols

2-Chlorophenol # <1 <1 ug/l TM16/PM30

2-Methylphenol # <0.5 <0.5 ug/l TM16/PM30

2-Nitrophenol <0.5 <0.5 ug/l TM16/PM30

2,4-Dichlorophenol # <0.5 <0.5 ug/l TM16/PM30

2,4-Dimethylphenol <1 <1 ug/l TM16/PM30

2,4,5-Trichlorophenol # <0.5 <0.5 ug/l TM16/PM30

2,4,6-Trichlorophenol <1 <1 ug/l TM16/PM30

4-Chloro-3-methylphenol # <0.5 <0.5 ug/l TM16/PM30

4-Methylphenol <1 <1 ug/l TM16/PM30

4-Nitrophenol <10 <10 ug/l TM16/PM30

Pentachlorophenol <1 <1 ug/l TM16/PM30

Phenol <1 <1 ug/l TM16/PM30

PAHs

2-Chloronaphthalene # <1 <1 ug/l TM16/PM30

2-Methylnaphthalene # <1 <1 ug/l TM16/PM30

Naphthalene # <1 <1 ug/l TM16/PM30

Acenaphthylene # <0.5 <0.5 ug/l TM16/PM30

Acenaphthene # <1 <1 ug/l TM16/PM30

Fluorene # <0.5 <0.5 ug/l TM16/PM30

Phenanthrene # <0.5 <0.5 ug/l TM16/PM30

Anthracene # <0.5 <0.5 ug/l TM16/PM30

Fluoranthene # <0.5 <0.5 ug/l TM16/PM30

Pyrene # <0.5 <0.5 ug/l TM16/PM30

Benzo(a)anthracene # <0.5 <0.5 ug/l TM16/PM30

Chrysene # <0.5 <0.5 ug/l TM16/PM30

Benzo(bk)fluoranthene # <1 <1 ug/l TM16/PM30

Benzo(a)pyrene <1 <1 ug/l TM16/PM30

Indeno(123cd)pyrene <1 <1 ug/l TM16/PM30

Dibenzo(ah)anthracene # <0.5 <0.5 ug/l TM16/PM30

Benzo(ghi)perylene # <0.5 <0.5 ug/l TM16/PM30

Phthalates

Bis(2-ethylhexyl) phthalate <5 <5 ug/l TM16/PM30

Butylbenzyl phthalate <1 <1 ug/l TM16/PM30

Di-n-butyl phthalate # <1.5 <1.5 ug/l TM16/PM30

Di-n-Octyl phthalate <1 <1 ug/l TM16/PM30

Diethyl phthalate # <1 <1 ug/l TM16/PM30

Dimethyl phthalate <1 <1 ug/l TM16/PM30

Hollywood

Jason McGuirk



LOD/LOR UnitsMethod

No.






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Reference:

Location:

Contact:

EMT Job No: 20/7108

EMT Sample No. 1-8

Sample IDIMS

LEACHATE

NO.1

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1


SVOC MS

Other SVOCs

1,2-Dichlorobenzene # <1 <1 ug/l TM16/PM30

1,2,4-Trichlorobenzene # <1 <1 ug/l TM16/PM30



2-Nitroaniline <1 <1 ug/l TM16/PM30

2,4-Dinitrotoluene # <0.5 <0.5 ug/l TM16/PM30

2,6-Dinitrotoluene <1 <1 ug/l TM16/PM30


4-Bromophenylphenylether # <1 <1 ug/l TM16/PM30

4-Chloroaniline <1 <1 ug/l TM16/PM30

4-Chlorophenylphenylether # <1 <1 ug/l TM16/PM30

4-Nitroaniline <0.5 <0.5 ug/l TM16/PM30

Azobenzene # <0.5 <0.5 ug/l TM16/PM30

Bis(2-chloroethoxy)methane # <0.5 <0.5 ug/l TM16/PM30

Bis(2-chloroethyl)ether # <1 <1 ug/l TM16/PM30

Carbazole # <0.5 <0.5 ug/l TM16/PM30

Dibenzofuran # <0.5 <0.5 ug/l TM16/PM30

Hexachlorobenzene # <1 <1 ug/l TM16/PM30

Hexachlorobutadiene # <1 <1 ug/l TM16/PM30

Hexachlorocyclopentadiene <1 <1 ug/l TM16/PM30

Hexachloroethane # <1 <1 ug/l TM16/PM30

Isophorone # <0.5 <0.5 ug/l TM16/PM30

N-nitrosodi-n-propylamine # <0.5 <0.5 ug/l TM16/PM30

Nitrobenzene # <1 <1 ug/l TM16/PM30

Surrogate Recovery 2-Fluorobiphenyl 90 <0 % TM16/PM30

Surrogate Recovery p-Terphenyl-d14 119 <0 % TM16/PM30

LOD/LOR UnitsMethod

No.




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EPA Export 22-02-2021:06:51:36

Client Name: VOC Report : Liquid

Reference:

Location:

Contact:

EMT Job No: 20/7108

EMT Sample No. 1-8

Sample IDIMS

LEACHATE

NO.1

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1


VOC MS

Dichlorodifluoromethane <2 <2 ug/l TM15/PM10

Methyl Tertiary Butyl Ether # 7.3 <0.1 ug/l TM15/PM10

Chloromethane # <3 <3 ug/l TM15/PM10

Vinyl Chloride # <0.1 <0.1 ug/l TM15/PM10

Bromomethane <1 <1 ug/l TM15/PM10

Chloroethane # <3 <3 ug/l TM15/PM10

Trichlorofluoromethane # <3 <3 ug/l TM15/PM10

1,1-Dichloroethene (1,1 DCE) # <3 <3 ug/l TM15/PM10

Dichloromethane (DCM) # <5 <5 ug/l TM15/PM10

trans-1-2-Dichloroethene # <3 <3 ug/l TM15/PM10

1,1-Dichloroethane # <3 <3 ug/l TM15/PM10

cis-1-2-Dichloroethene # <3 <3 ug/l TM15/PM10

2,2-Dichloropropane <1 <1 ug/l TM15/PM10

Bromochloromethane # <2 <2 ug/l TM15/PM10

Chloroform # <2 <2 ug/l TM15/PM10

1,1,1-Trichloroethane # <2 <2 ug/l TM15/PM10

1,1-Dichloropropene # <3 <3 ug/l TM15/PM10

Carbon tetrachloride # <2 <2 ug/l TM15/PM10


Benzene # <0.5 <0.5 ug/l TM15/PM10

Trichloroethene (TCE) # <3 <3 ug/l TM15/PM10

1,2-Dichloropropane # <2 <2 ug/l TM15/PM10

Dibromomethane # <3 <3 ug/l TM15/PM10

Bromodichloromethane # <2 <2 ug/l TM15/PM10

cis-1-3-Dichloropropene <2 <2 ug/l TM15/PM10

Toluene # <5 <5 ug/l TM15/PM10

trans-1-3-Dichloropropene <2 <2 ug/l TM15/PM10


Tetrachloroethene (PCE) # <3 <3 ug/l TM15/PM10


Dibromochloromethane # <2 <2 ug/l TM15/PM10

1,2-Dibromoethane # <2 <2 ug/l TM15/PM10

Chlorobenzene # <2 <2 ug/l TM15/PM10

1,1,1,2-Tetrachloroethane # <2 <2 ug/l TM15/PM10

Ethylbenzene # <1 <1 ug/l TM15/PM10

m/p-Xylene # <2 <2 ug/l TM15/PM10

o-Xylene # <1 <1 ug/l TM15/PM10

Styrene <2 <2 ug/l TM15/PM10

Bromoform # <2 <2 ug/l TM15/PM10

Isopropylbenzene # <3 <3 ug/l TM15/PM10

1,1,2,2-Tetrachloroethane <4 <4 ug/l TM15/PM10

Bromobenzene # <2 <2 ug/l TM15/PM10

1,2,3-Trichloropropane # <3 <3 ug/l TM15/PM10

Propylbenzene # <3 <3 ug/l TM15/PM10

2-Chlorotoluene # <3 <3 ug/l TM15/PM10

1,3,5-Trimethylbenzene # <3 <3 ug/l TM15/PM10


tert-Butylbenzene # <3 <3 ug/l TM15/PM10


sec-Butylbenzene # <3 <3 ug/l TM15/PM10

4-Isopropyltoluene # <3 <3 ug/l TM15/PM10



n-Butylbenzene # <3 <3 ug/l TM15/PM10


1,2-Dibromo-3-chloropropane <2 <2 ug/l TM15/PM10

1,2,4-Trichlorobenzene <3 <3 ug/l TM15/PM10

Hexachlorobutadiene <3 <3 ug/l TM15/PM10


Surrogate Recovery Toluene D8 102 <0 % TM15/PM10

Surrogate Recovery 4-Bromofluorobenzene 107 <0 % TM15/PM10

Hollywood

Jason McGuirk



LOD/LOR UnitsMethod

No.






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EPA Export 22-02-2021:06:51:36

Notification of Deviating Samples

EMT

Job

No.

Batch Depth

EMT

Sample

No.

Analysis Reason

Please note that only samples that are deviating are mentioned in this report. If no samples are listed it is because none were deviating.

Only analyses which are accredited are recorded as deviating if set criteria are not met.

Contact:

Sample ID

Client Name: IMS Integrated Material Solutions Limited Partnership

Reference:

Location:

No deviating sample report results for job 20/7108



Hollywood

Jason McGuirk

QF-PM 3.1.11 v3 Please include all sections of this report if it is reproduced 7 of 11

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EPA Export 22-02-2021:06:51:36

EMT Job No.:

SOILS

DEVIATING SAMPLES

SURROGATES

DILUTIONS

BLANKS

NOTE

Data is only reported if the laboratory is confident that the data is a true reflection of the samples analysed. Data is only reported as accredited when

all the requirements of our Quality System have been met. In certain circumstances where all the requirements of the Quality System have not been

met, for instance if the associated AQC has failed, the reason is fully investigated and documented. The sample data is then evaluated alongside

the other quality control checks performed during analysis to determine its suitability. Following this evaluation, provided the sample results have not

been effected, the data is reported but accreditation is removed. It is a UKAS requirement for data not reported as accredited to be considered

indicative only, but this does not mean the data is not valid.

Where possible, and if requested, samples will be re-extracted and a revised report issued with accredited results. Please do not hesitate to contact

the laboratory if further details are required of the circumstances which have led to the removal of accreditation.

As surface waters require different sample preparation to groundwaters the laboratory must be informed of the water type when submitting samples.

Where Mineral Oil or Fats, Oils and Grease is quoted, this refers to Total Aliphatics C10-C40.

All samples should be submitted to the laboratory in suitable containers with sufficient ice packs to sustain an appropriate temperature for the

requested analysis. The temperature of sample receipt is recorded on the confirmation schedules in order that the client can make an informed

decision as to whether testing should still be undertaken.

Surrogate compounds are added during the preparation process to monitor recovery of analytes. However low recovery in soils is often due to peat,

clay or other organic rich matrices. For waters this can be due to oxidants, surfactants, organic rich sediments or remediation fluids. Acceptable

limits for most organic methods are 70 - 130% and for VOCs are 50 - 150%. When surrogate recoveries are outside the performance criteria but

the associated AQC passes this is assumed to be due to matrix effect. Results are not surrogate corrected.

A dilution suffix indicates a dilution has been performed and the reported result takes this into account. No further calculation is required.

Where analytes have been found in the blank, the sample will be treated in accordance with our laboratory procedure for dealing with contaminated

blanks.

Sufficient amount of sample must be received to carry out the testing specified. Where an insufficient amount of sample has been received the

testing may not meet the requirements of our accredited methods, as such accreditation may be removed.

Negative Neutralization Potential (NP) values are obtained when the volume of NaOH (0.1N) titrated (pH 8.3) is greater than the volume of HCl (1N)

to reduce the pH of the sample to 2.0 - 2.5. Any negative NP values are corrected to 0.

The calculation of Pyrite content assumes that all oxidisable sulphides present in the sample are pyrite. This may not be the case. The calculation

may be an overesitimate when other sulphides such as Barite (Barium Sulphate) are present.

WATERS

Please note we are not a UK Drinking Water Inspectorate (DWI) Approved Laboratory .

ISO17025 accreditation applies to surface water and groundwater and usually one other matrix which is analysis specific, any other liquids are

outside our scope of accreditation.

If you have not already done so, please send us a purchase order if this is required by your company.

Where appropriate please make sure that our detection limits are suitable for your needs, if they are not, please notify us immediately.

All analysis is reported on a dry weight basis unless stated otherwise. Limits of detection for analyses carried out on as received samples are not

moisture content corrected. Results are not surrogate corrected. Samples are dried at 35°C ±5°C unless otherwise stated. Moisture content for

CEN Leachate tests are dried at 105°C ±5°C.


Where a CEN 10:1 ZERO Headspace VOC test has been carried out, a 10:1 ratio of water to wet (as received) soil has been used.

% Asbestos in Asbestos Containing Materials (ACMs) is determined by reference to HSG 264 The Survey Guide - Appendix 2 : ACMs in buildings

listed in order of ease of fibre release.

NOTES TO ACCOMPANY ALL SCHEDULES AND REPORTS

20/7108

Please note we are only MCERTS accredited (UK soils only) for sand, loam and clay and any other matrix is outside our scope of accreditation.

Where an MCERTS report has been requested, you will be notified within 48 hours of any samples that have been identified as being outside our

MCERTS scope. As validation has been performed on clay, sand and loam, only samples that are predominantly these matrices, or combinations

of them will be within our MCERTS scope. If samples are not one of a combination of the above matrices they will not be marked as MCERTS

accredited.

It is assumed that you have taken representative samples on site and require analysis on a representative subsample. Stones will generally be

included unless we are requested to remove them.

All samples will be discarded one month after the date of reporting, unless we are instructed to the contrary.



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EPA Export 22-02-2021:06:51:36

EMT Job No.:

Measurement Uncertainty

#

SA

B

DR

M

NA

NAD

ND

NDP

SS

SV

W

+

>>

*

AD

CO

LOD/LOR

ME

NFD

BS

LB

N

TB

OC Outside Calibration Range

Matrix Effect

No Fibres Detected

AQC Sample

Blank Sample

Client Sample

Trip Blank Sample

AQC failure, accreditation has been removed from this result, if appropriate, see 'Note' on previous page.

Results above calibration range, the result should be considered the minimum value. The actual result could be significantly

higher, this result is not accredited.

Analysis subcontracted to an Element Materials Technology approved laboratory.

Samples are dried at 35°C ±5°C

Suspected carry over

Limit of Detection (Limit of Reporting) in line with ISO 17025 and MCERTS

No Asbestos Detected.

None Detected (usually refers to VOC and/SVOC TICs).

No Determination Possible

Calibrated against a single substance

Surrogate recovery outside performance criteria. This may be due to a matrix effect.

Results expressed on as received basis.

ISO17025 (UKAS Ref No. 4225) accredited - UK.

ISO17025 (SANAS Ref No.T0729) accredited - South Africa

Indicates analyte found in associated method blank.

Dilution required.

MCERTS accredited.

Not applicable

20/7108

REPORTS FROM THE SOUTH AFRICA LABORATORY

Any method number not prefixed with SA has been undertaken in our UK laboratory unless reported as subcontracted.

Measurement uncertainty defines the range of values that could reasonably be attributed to the measured quantity. This range of values has not

been included within the reported results. Uncertainty expressed as a percentage can be provided upon request.

ABBREVIATIONS and ACRONYMS USED



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EPA Export 22-02-2021:06:51:36

EMT Job No: 20/7108

Test Method No. Description

Prep Method

No. (if

appropriate)

Description

ISO

17025

(UKAS/S

ANAS)

MCERTS

(UK soils

only)

Analysis done

on As Received

(AR) or Dried

(AD)

Reported on

dry weight

basis

TM15Modified USEPA 8260B v2:1996. Quantitative Determination of Volatile Organic

Compounds (VOCs) by Headspace GC-MS.PM10

Modified US EPA method 5021A v2:2014. Preparation of solid and liquid samples for GC

headspace analysis.




headspace analysis. Yes

TM16Modified USEPA 8270D v5:2014. Quantitative determination of Semi-Volatile Organic

compounds (SVOCs) by GC-MS. PM30 Water samples are extracted with solvent using a magnetic stirrer to create a vortex.


compounds (SVOCs) by GC-MS. PM30 Water samples are extracted with solvent using a magnetic stirrer to create a vortex. Yes

TM26Determination of phenols by Reversed Phased High Performance Liquid

Chromatography and Electro-Chemical Detection.PM0 No preparation is required.

TM30

Determination of Trace Metals by ICP-OES (Inductively Coupled Plasma – Optical

Emission Spectrometry): WATERS by Modified USEPA Method 200.7, Rev. 4.4, 1994;

Modified EPA Method 6010B, Rev.2, Dec 1996; Modified BS EN ISO 11885:2009:

SOILS by Modified USEP

PM14Preparation of waters and leachates for metals by ICP OES/ICP MS. Samples are filtered

for Dissolved metals, and remain unfiltered for Total metals then acidifiedYes

TM35

True and apparent colour by Hach Lange DR3800 spectrophotometer. Apparent colour

includes dissolved and suspended matter. True colour is determinined after filtration of

the sample.

PM0 No preparation is required.

TM38

Soluble Ion analysis using Discrete Analyser. Modified US EPA methods: Chloride 325.2

(1978), Sulphate 375.4 (Rev.2 1993), o-Phosphate 365.2 (Rev.2 1993), TON 353.1

(Rev.2 1993), Nitrite 354.1 (1971), Hex Cr 7196A (1992), NH4+ 350.1 (Rev.2 1993

(comparabl

PM0 No preparation is required. Yes

TM57

Modified US EPA Method 410.4. (Rev. 2.0 1993) Comparable with ISO 15705:2002.

Chemical Oxygen Demand is determined by hot digestion with Potassium Dichromate

and measured spectrophotometerically.


TM60

TC/TOC analysis of Waters by High Temperature Combustion followed by NDIR

detection. Based on the following modified standard methods: USEPA 9060A (2002),

APHA SMEWW 5310B:1999 22nd Edition, ASTM D 7573, and USEPA 415.1.


Element Materials Technology Method Code Appendix


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EPA Export 22-02-2021:06:51:36

EMT Job No: 20/7108


Prep Method

No. (if

appropriate)

Description

ISO

17025

(UKAS/S

ANAS)

MCERTS

(UK soils

only)

Analysis done

on As Received

(AR) or Dried

(AD)

Reported on

dry weight

basis

TM73Modified US EPA methods 150.1 (1982) and 9045D Rev. 4 - 2004) and BS1377-

3:1990. Determination of pH by Metrohm automated probe analyser.PM0 No preparation is required. Yes

TM76Modified US EPA method 120.1 (1982). Determination of Specific Conductance by

Metrohm automated probe analyser.PM0 No preparation is required. Yes

TM129 Odour of samples PM0 No preparation is required. AR

TM149Determination of Pesticides by Large Volume Injection on GC Triple Quad MS, based

upon USEPA method 8270D v5:2014PM30 Water samples are extracted with solvent using a magnetic stirrer to create a vortex.



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EPA Export 22-02-2021:06:51:36



Zone 3


Deeside

CH5 2UA


Attention :

Date :

Your reference :

Our reference :

Location :


Status :

Issue :


Nags Head

Hollywood

Naul

Co Dublin

Ireland

Jason McGuirk

11th June, 2020



Hollywood

5th June, 2020

Final report

Project Manager

1





Authorised By:

Bruce Leslie





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EPA Export 22-02-2021:06:51:36


Reference:

Location:



EMT Sample No. 1-8

Sample IDIMS/LEACHAT

E NO.3

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1






Pesticides


Aldrin <0.01 <0.01 ug/l TM149/PM30








Endrin <0.01 <0.01 ug/l TM149/PM30





p,p'-DDE <0.01 <0.01 ug/l TM149/PM30

p,p'-DDT <0.01 <0.01 ug/l TM149/PM30


p,p'-TDE <0.01 <0.01 ug/l TM149/PM30






Ethion <0.01 <0.01 ug/l TM149/PM30









Total Oxidised Nitrogen as N # <0.2 <0.2 mg/l TM38/PM0


Hollywood

Jason McGuirk



LOD/LOR UnitsMethod

No.






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EPA Export 22-02-2021:06:51:36


Reference:

Location:



EMT Sample No. 1-8


E NO.3

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1



Dissolved Organic Carbon # 9 <2 mg/l TM60/PM0


pH # 7.69 <0.01 pH units TM73/PM0


True Colour <15 <15 PCU TM35/PM0

LOD/LOR UnitsMethod

No.




Hollywood

Jason McGuirk





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EPA Export 22-02-2021:06:51:36


Reference:

Location:

Contact:

EMT Job No: 20/7109

EMT Sample No. 1-8


E NO.3

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1


SVOC MS

Phenols













PAHs










Pyrene # <0.5 <0.5 ug/l TM16/PM30








Phthalates







Hollywood

Jason McGuirk



LOD/LOR UnitsMethod

No.






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EPA Export 22-02-2021:06:51:36


Reference:

Location:

Contact:

EMT Job No: 20/7109

EMT Sample No. 1-8


E NO.3

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1


SVOC MS

Other SVOCs



























LOD/LOR UnitsMethod

No.




Hollywood

Jason McGuirk





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EPA Export 22-02-2021:06:51:36


Reference:

Location:

Contact:

EMT Job No: 20/7109

EMT Sample No. 1-8


E NO.3

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1


VOC MS


Methyl Tertiary Butyl Ether # <0.1 <0.1 ug/l TM15/PM10

























































Naphthalene <2 <2 ug/l TM15/PM10




Hollywood

Jason McGuirk



LOD/LOR UnitsMethod

No.






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EPA Export 22-02-2021:06:51:36


EMT

Job

No.

Batch Depth

EMT

Sample

No.

Analysis Reason



Contact:

Sample ID


Reference:

Location:




Hollywood

Jason McGuirk


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EPA Export 22-02-2021:06:51:36

EMT Job No.:

SOILS

DEVIATING SAMPLES

SURROGATES

DILUTIONS

BLANKS

NOTE




















blanks.







WATERS














20/7109





accredited.






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EPA Export 22-02-2021:06:51:36

EMT Job No.:


#

SA

B

DR

M

NA

NAD

ND

NDP

SS

SV

W

+

>>

*

AD

CO

LOD/LOR

ME

NFD

BS

LB

N

TB

OC Outside Calibration Range

Matrix Effect

No Fibres Detected

AQC Sample

Blank Sample

Client Sample

Trip Blank Sample

















Dilution required.

MCERTS accredited.

Not applicable

20/7109








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EPA Export 22-02-2021:06:51:36

EMT Job No: 20/7109


Prep Method

No. (if

appropriate)

Description

ISO

17025

(UKAS/S

ANAS)

MCERTS

(UK soils

only)

Analysis done

on As Received

(AR) or Dried

(AD)

Reported on

dry weight

basis




headspace analysis.











TM30







TM35



the sample.


TM38




(comparabl


TM57





TM60







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EPA Export 22-02-2021:06:51:36

EMT Job No: 20/7109


Prep Method

No. (if

appropriate)

Description

ISO

17025

(UKAS/S

ANAS)

MCERTS

(UK soils

only)

Analysis done

on As Received

(AR) or Dried

(AD)

Reported on

dry weight

basis










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EPA Export 22-02-2021:06:51:36



Zone 3


Deeside

CH5 2UA


Attention :

Date :

Your reference :

Our reference :

Location :


Status :

Issue :


Nags Head

Hollywood

Naul

Co Dublin

Ireland

Jason McGuirk

12th June, 2020



Hollywood

4th June, 2020

Final report


1





Authorised By:

Phil Sommerton BSc





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EPA Export 22-02-2021:06:51:36


Reference:

Location:



EMT Sample No. 1-8


E NO.4

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1





Dissolved Sodium # 318.5AA <0.1 mg/l TM30/PM14

Pesticides


Aldrin <0.01 <0.01 ug/l TM149/PM30








Endrin <0.01 <0.01 ug/l TM149/PM30





p,p'-DDE <0.01 <0.01 ug/l TM149/PM30

p,p'-DDT <0.01 <0.01 ug/l TM149/PM30


p,p'-TDE <0.01 <0.01 ug/l TM149/PM30






Ethion <0.01 <0.01 ug/l TM149/PM30











Hollywood

Jason McGuirk



LOD/LOR UnitsMethod

No.






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EPA Export 22-02-2021:06:51:36


Reference:

Location:



EMT Sample No. 1-8


E NO.4

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1





pH # 7.91 <0.01 pH units TM73/PM0


True Colour 107 <15 PCU TM35/PM0

LOD/LOR UnitsMethod

No.




Hollywood

Jason McGuirk





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EPA Export 22-02-2021:06:51:36


Reference:

Location:

Contact:

EMT Job No: 20/7111

EMT Sample No. 1-8


E NO.4

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1


SVOC MS

Phenols













PAHs










Pyrene # <0.5 <0.5 ug/l TM16/PM30








Phthalates

Bis(2-ethylhexyl) phthalate 23 <5 ug/l TM16/PM30






Hollywood

Jason McGuirk



LOD/LOR UnitsMethod

No.






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EPA Export 22-02-2021:06:51:36


Reference:

Location:

Contact:

EMT Job No: 20/7111

EMT Sample No. 1-8


E NO.4

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1


SVOC MS

Other SVOCs



























LOD/LOR UnitsMethod

No.




Hollywood

Jason McGuirk





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EPA Export 22-02-2021:06:51:36


Reference:

Location:

Contact:

EMT Job No: 20/7111

EMT Sample No. 1-8


E NO.4

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1


VOC MS






























































Hollywood

Jason McGuirk



LOD/LOR UnitsMethod

No.






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EPA Export 22-02-2021:06:51:36


EMT

Job

No.

Batch Depth

EMT

Sample

No.

Analysis Reason



Contact:

Sample ID


Reference:

Location:




Hollywood

Jason McGuirk


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EPA Export 22-02-2021:06:51:36

EMT Job No.:

SOILS

DEVIATING SAMPLES

SURROGATES

DILUTIONS

BLANKS

NOTE




















blanks.







WATERS














20/7111





accredited.






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se.

EPA Export 22-02-2021:06:51:36

EMT Job No.:


#

SA

B

DR

M

NA

NAD

ND

NDP

SS

SV

W

+

>>

*

AD

CO

LOD/LOR

ME

NFD

BS

LB

N

TB

OC

AA x5 Dilution

Outside Calibration Range

Matrix Effect

No Fibres Detected

AQC Sample

Blank Sample

Client Sample

Trip Blank Sample

















Dilution required.

MCERTS accredited.

Not applicable

20/7111








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ectio

n pur

pose

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EPA Export 22-02-2021:06:51:36

EMT Job No: 20/7111


Prep Method

No. (if

appropriate)

Description

ISO

17025

(UKAS/S

ANAS)

MCERTS

(UK soils

only)

Analysis done

on As Received

(AR) or Dried

(AD)

Reported on

dry weight

basis




headspace analysis.











TM30







TM35



the sample.


TM38




(comparabl


TM57





TM60







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ectio

n pur

pose

s only

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EPA Export 22-02-2021:06:51:36

EMT Job No: 20/7111


Prep Method

No. (if

appropriate)

Description

ISO

17025

(UKAS/S

ANAS)

MCERTS

(UK soils

only)

Analysis done

on As Received

(AR) or Dried

(AD)

Reported on

dry weight

basis










For

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ectio

n pur

pose

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EPA Export 22-02-2021:06:51:36



Zone 3


Deeside

CH5 2UA


Attention :

Date :

Your reference :

Our reference :

Location :


Status :

Issue :


Nags Head

Hollywood

Naul

Co Dublin

Ireland

Jason McGuirk

11th June, 2020



Hollywood

5th June, 2020

Final report

Project Manager

1





Authorised By:

Bruce Leslie





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EPA Export 22-02-2021:06:51:36


Reference:

Location:



EMT Sample No. 1-8

Sample IDLEACHATE

TESTING

NO.5

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1






Pesticides


Aldrin <0.01 <0.01 ug/l TM149/PM30








Endrin <0.01 <0.01 ug/l TM149/PM30





p,p'-DDE <0.01 <0.01 ug/l TM149/PM30

p,p'-DDT <0.01 <0.01 ug/l TM149/PM30


p,p'-TDE <0.01 <0.01 ug/l TM149/PM30






Ethion <0.01 <0.01 ug/l TM149/PM30











Hollywood

Jason McGuirk



LOD/LOR UnitsMethod

No.






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EPA Export 22-02-2021:06:51:36


Reference:

Location:



EMT Sample No. 1-8

Sample IDLEACHATE

TESTING

NO.5

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1





pH # 10.54 <0.01 pH units TM73/PM0



LOD/LOR UnitsMethod

No.




Hollywood

Jason McGuirk





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EPA Export 22-02-2021:06:51:36


Reference:

Location:

Contact:

EMT Job No: 20/7118

EMT Sample No. 1-8

Sample IDLEACHATE

TESTING

NO.5

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1


SVOC MS

Phenols













PAHs










Pyrene # <0.5 <0.5 ug/l TM16/PM30








Phthalates







Hollywood

Jason McGuirk



LOD/LOR UnitsMethod

No.






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EPA Export 22-02-2021:06:51:37


Reference:

Location:

Contact:

EMT Job No: 20/7118

EMT Sample No. 1-8

Sample IDLEACHATE

TESTING

NO.5

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1


SVOC MS

Other SVOCs



























LOD/LOR UnitsMethod

No.




Hollywood

Jason McGuirk





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EPA Export 22-02-2021:06:51:37


Reference:

Location:

Contact:

EMT Job No: 20/7118

EMT Sample No. 1-8

Sample IDLEACHATE

TESTING

NO.5

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1


VOC MS































































Hollywood

Jason McGuirk



LOD/LOR UnitsMethod

No.






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EPA Export 22-02-2021:06:51:37


EMT

Job

No.

Batch Depth

EMT

Sample

No.

Analysis Reason



Contact:

Sample ID


Reference:

Location:




Hollywood

Jason McGuirk


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EPA Export 22-02-2021:06:51:37

EMT Job No.:

SOILS

DEVIATING SAMPLES

SURROGATES

DILUTIONS

BLANKS

NOTE




















blanks.







WATERS














20/7118





accredited.






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EPA Export 22-02-2021:06:51:37

EMT Job No.:


#

SA

B

DR

M

NA

NAD

ND

NDP

SS

SV

W

+

>>

*

AD

CO

LOD/LOR

ME

NFD

BS

LB

N

TB

OC

AA x5 Dilution


Matrix Effect

No Fibres Detected

AQC Sample

Blank Sample

Client Sample

Trip Blank Sample

















Dilution required.

MCERTS accredited.

Not applicable

20/7118








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ectio

n pur

pose

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EPA Export 22-02-2021:06:51:37

EMT Job No: 20/7118


Prep Method

No. (if

appropriate)

Description

ISO

17025

(UKAS/S

ANAS)

MCERTS

(UK soils

only)

Analysis done

on As Received

(AR) or Dried

(AD)

Reported on

dry weight

basis




headspace analysis.











TM30







TM35



the sample.


TM38




(comparabl


TM57





TM60







For

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ectio

n pur

pose

s only

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EPA Export 22-02-2021:06:51:37

EMT Job No: 20/7118


Prep Method

No. (if

appropriate)

Description

ISO

17025

(UKAS/S

ANAS)

MCERTS

(UK soils

only)

Analysis done

on As Received

(AR) or Dried

(AD)

Reported on

dry weight

basis










For

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ectio

n pur

pose

s only

.

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r req

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se.

EPA Export 22-02-2021:06:51:37



Zone 3


Deeside

CH5 2UA


Attention :

Date :

Your reference :

Our reference :

Location :


Status :

Issue :

Phil Sommerton BSc


Nags Head

Hollywood

Naul

Co Dublin

Ireland

Jason McGuirk

12th June, 2020



Hollywood

5th June, 2020

Final report


1

One sample was received for analysis on 5th June, 2020 of which one were scheduled for analysis. Please find attached our Test Report which




Authorised By:





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EPA Export 22-02-2021:06:51:37


Reference:

Location:



EMT Sample No. 1-8

Sample IDIMS

LEACHATE

N0.6

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1






Pesticides


Aldrin <0.01 <0.01 ug/l TM149/PM30








Endrin <0.01 <0.01 ug/l TM149/PM30





p,p'-DDE <0.01 <0.01 ug/l TM149/PM30

p,p'-DDT <0.01 <0.01 ug/l TM149/PM30


p,p'-TDE <0.01 <0.01 ug/l TM149/PM30






Ethion <0.01 <0.01 ug/l TM149/PM30














Hollywood

Jason McGuirk



LOD/LOR UnitsMethod

No.



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ectio

n pur

pose

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EPA Export 22-02-2021:06:51:37


Reference:

Location:



EMT Sample No. 1-8

Sample IDIMS

LEACHATE

N0.6

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1





pH # 10.83 <0.01 pH units TM73/PM0



LOD/LOR UnitsMethod

No.




Hollywood

Jason McGuirk





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EPA Export 22-02-2021:06:51:37


Reference:

Location:

Contact:

EMT Job No: 20/7119

EMT Sample No. 1-8

Sample IDIMS

LEACHATE

N0.6

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1


SVOC MS

Phenols













PAHs



Naphthalene # 1 <1 ug/l TM16/PM30







Pyrene # <0.5 <0.5 ug/l TM16/PM30








Phthalates










Hollywood

Jason McGuirk



LOD/LOR UnitsMethod

No.



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n pur

pose

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EPA Export 22-02-2021:06:51:37


Reference:

Location:

Contact:

EMT Job No: 20/7119

EMT Sample No. 1-8

Sample IDIMS

LEACHATE

N0.6

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1


SVOC MS

Other SVOCs



























LOD/LOR UnitsMethod

No.




Hollywood

Jason McGuirk





For

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ectio

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pose

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EPA Export 22-02-2021:06:51:37


Reference:

Location:

Contact:

EMT Job No: 20/7119

EMT Sample No. 1-8

Sample IDIMS

LEACHATE

N0.6

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1


VOC MS

































































Hollywood

Jason McGuirk



LOD/LOR UnitsMethod

No.



For

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ectio

n pur

pose

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EPA Export 22-02-2021:06:51:37


EMT

Job

No.

Batch Depth

EMT

Sample

No.

Analysis Reason





Hollywood

Jason McGuirkContact:

Sample ID


Reference:

Location:



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EPA Export 22-02-2021:06:51:37

EMT Job No.:

SOILS

DEVIATING SAMPLES

SURROGATES

DILUTIONS

BLANKS

NOTE




20/7119





accredited.












blanks.







WATERS
























For

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ectio

n pur

pose

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EPA Export 22-02-2021:06:51:37

EMT Job No.:


#

SA

B

DR

M

NA

NAD

ND

NDP

SS

SV

W

+

>>

*

AD

CO

LOD/LOR

ME

NFD

BS

LB

N

TB

OC

Not applicable

20/7119









Dilution required.

MCERTS accredited.















Matrix Effect

No Fibres Detected

AQC Sample

Blank Sample

Client Sample

Trip Blank Sample



For

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ectio

n pur

pose

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EPA Export 22-02-2021:06:51:37

EMT Job No: 20/7119


Prep Method

No. (if

appropriate)

Description

ISO

17025

(UKAS/S

ANAS)

MCERTS

(UK soils

only)

Analysis done

on As Received

(AR) or Dried

(AD)

Reported on

dry weight

basis




headspace analysis.











TM30







TM35



the sample.


TM38




(comparabl


TM57





TM60







For

insp

ectio

n pur

pose

s only

.

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nt of

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EPA Export 22-02-2021:06:51:37

EMT Job No: 20/7119


Prep Method

No. (if

appropriate)

Description

ISO

17025

(UKAS/S

ANAS)

MCERTS

(UK soils

only)

Analysis done

on As Received

(AR) or Dried

(AD)

Reported on

dry weight

basis










For

insp

ectio

n pur

pose

s only

.

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nt of

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r req

uired

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ny ot

her u

se.

EPA Export 22-02-2021:06:51:37



Zone 3


Deeside

CH5 2UA


Attention :

Date :

Your reference :

Our reference :

Location :


Status :

Issue :


Nags Head

Hollywood

Naul

Co Dublin

Ireland

Jason McGuirk

12th June, 2020



Hollywood

5th June, 2020

Final report

Project Manager

1

Two samples were received for analysis on 5th June, 2020 of which one was scheduled for analysis. Please find attached our Test Report which




Authorised By:

Bruce Leslie





For

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ectio

n pur

pose

s only

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EPA Export 22-02-2021:06:51:37


Reference:

Location:



EMT Sample No. 1-7

Sample IDLEACHATE

TESTING

NO.7

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1






Pesticides


Aldrin <0.01 <0.01 ug/l TM149/PM30








Endrin <0.01 <0.01 ug/l TM149/PM30





p,p'-DDE <0.01 <0.01 ug/l TM149/PM30

p,p'-DDT <0.01 <0.01 ug/l TM149/PM30


p,p'-TDE <0.01 <0.01 ug/l TM149/PM30






Ethion <0.01 <0.01 ug/l TM149/PM30











Hollywood

Jason McGuirk



LOD/LOR UnitsMethod

No.






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ectio

n pur

pose

s only

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EPA Export 22-02-2021:06:51:37


Reference:

Location:



EMT Sample No. 1-7

Sample IDLEACHATE

TESTING

NO.7

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1





pH # 11.72 <0.01 pH units TM73/PM0



LOD/LOR UnitsMethod

No.




Hollywood

Jason McGuirk





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EPA Export 22-02-2021:06:51:37


Reference:

Location:

Contact:

EMT Job No: 20/7120

EMT Sample No. 1-7

Sample IDLEACHATE

TESTING

NO.7

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1


SVOC MS

Phenols













PAHs



Naphthalene # 1 <1 ug/l TM16/PM30







Pyrene # <0.5 <0.5 ug/l TM16/PM30








Phthalates







Hollywood

Jason McGuirk



LOD/LOR UnitsMethod

No.






For

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pose

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EPA Export 22-02-2021:06:51:37


Reference:

Location:

Contact:

EMT Job No: 20/7120

EMT Sample No. 1-7

Sample IDLEACHATE

TESTING

NO.7

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1


SVOC MS

Other SVOCs



























LOD/LOR UnitsMethod

No.




Hollywood

Jason McGuirk





For

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EPA Export 22-02-2021:06:51:37


Reference:

Location:

Contact:

EMT Job No: 20/7120

EMT Sample No. 1-7

Sample IDLEACHATE

TESTING

NO.7

Depth

COC No / misc


Sample Date 04/06/2020 09:00


Batch Number 1


VOC MS































































Hollywood

Jason McGuirk



LOD/LOR UnitsMethod

No.






For

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EPA Export 22-02-2021:06:51:37


EMT

Job

No.

Batch Depth

EMT

Sample

No.

Analysis Reason



Contact:

Sample ID


Reference:

Location:




Hollywood

Jason McGuirk


For

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EPA Export 22-02-2021:06:51:37

EMT Job No.:

SOILS

DEVIATING SAMPLES

SURROGATES

DILUTIONS

BLANKS

NOTE




















blanks.







WATERS














20/7120





accredited.






For

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pose

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EPA Export 22-02-2021:06:51:37

EMT Job No.:


#

SA

B

DR

M

NA

NAD

ND

NDP

SS

SV

W

+

>>

*

AD

CO

LOD/LOR

ME

NFD

BS

LB

N

TB

OC

AA x5 Dilution


Matrix Effect

No Fibres Detected

AQC Sample

Blank Sample

Client Sample

Trip Blank Sample

















Dilution required.

MCERTS accredited.

Not applicable

20/7120








For

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ectio

n pur

pose

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EPA Export 22-02-2021:06:51:37

EMT Job No: 20/7120


Prep Method

No. (if

appropriate)

Description

ISO

17025

(UKAS/S

ANAS)

MCERTS

(UK soils

only)

Analysis done

on As Received

(AR) or Dried

(AD)

Reported on

dry weight

basis




headspace analysis.











TM30







TM35



the sample.


TM38




(comparabl


TM57





TM60







For

insp

ectio

n pur

pose

s only

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nt of

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EPA Export 22-02-2021:06:51:37

EMT Job No: 20/7120


Prep Method

No. (if

appropriate)

Description

ISO

17025

(UKAS/S

ANAS)

MCERTS

(UK soils

only)

Analysis done

on As Received

(AR) or Dried

(AD)

Reported on

dry weight

basis










For

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ectio

n pur

pose

s only

.

Conse

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EPA Export 22-02-2021:06:51:37

For

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EPA Export 22-02-2021:06:51:37

Documents

Condition: Bi annual Leachate Monitoring Report 2020