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有有害害化化学学物物質質含含有有実実態態調調査査
結結果果デデーータタ集集
（（平平成成 1155～～ 2222 年年度度））
②（白）13-01-276_本文_MK.indd B13-01-276_本文_MK.indd B 2013/01/24 21:16:472013/01/24 21:16:47
①13-01-276_本文_MK.indd A13-01-276_本文_MK.indd A 2013/01/24 21:16:472013/01/24 21:16:47
18 22 1
17
22
PAHs
4
20 12
1 http://www.maff.go.jp/j/syouan/seisaku/risk_analysis/survei/middle_chem_h18.html 2 DON 3-
3-Ac-DON 15- 15-Ac-DON NIV4- 4-Ac-NIV A
11
i
13-01-276_本文_MK.indd i13-01-276_本文_MK.indd i 2013/01/24 21:16:472013/01/24 21:16:47
3- 15-4-
1 20.4
mg/kg 0.4 mg/kg
11 3 30
3 1,664
3 p PCDD
PCDF PCB Co-PCB
ii
13-01-276_本文_MK.indd ii13-01-276_本文_MK.indd ii 2013/01/24 21:16:482013/01/24 21:16:48
31 11,549 297
1 2
7
1,001 1,371
2,169
iii
13-01-276_本文_MK.indd iii13-01-276_本文_MK.indd iii 2013/01/24 21:16:482013/01/24 21:16:48
914
3- -1,2-3-MCPD
20 6
3-MCPD 21
3-MCPD
PAHs17 19 PAHs
PAHs100 1,600
PAHs
PAHs
536
iv
13-01-276_本文_MK.indd iv13-01-276_本文_MK.indd iv 2013/01/24 21:16:482013/01/24 21:16:48
760
v
13-01-276_本文_MK.indd v13-01-276_本文_MK.indd v 2013/01/24 21:16:482013/01/24 21:16:48
vi（白）13-01-276_本文_MK.indd vi13-01-276_本文_MK.indd vi 2013/01/24 21:16:482013/01/24 21:16:48
............................................................................................ vii
............................................................................ xii
2.1. ............................................................................ 2
2.2. .................................................................... 2
2.3. ........................................................ 13
3.1. ................................................................................. 17
3.1.1. ........................................................................................... 17 3.1.1.1. .............................................................................................. 17 3.1.1.2. ........................................................................................... 26 3.1.1.3. ........................................................................................... 30 3.1.1.4. ............................................................................ 33 3.1.2. ........................................................................................... 34 3.1.3. ....................................................................................... 38 3.1.3.1. ................................................................................ 38 3.1.3.2. .................................................................................... 43 3.1.3.3. .................................................................................... 44 3.1.3.4. .................................................................................... 46
vii
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3.1.3.5. .................................................................................... 47 3.1.3.6. .................................................................................... 52 3.1.3.7. ....................................................................................... 57 3.1.3.8. .................................................................................... 58 3.1.3.9. .................................................................................... 63 3.1.3.10. .................................................................................... 68 3.1.3.11. ............................................................................. 70 3.1.3.12. ....................................................................................... 71 3.1.3.13. .................................................................................... 73 3.1.3.14. ............................................................................. 74 3.1.3.15. ................................................................................ 79 3.1.3.16. ....................................................................................... 81 3.1.3.17. ............................................................................. 86 3.1.3.18. ........................................................................................... 89 3.1.3.19. ........................................................................................... 91 3.1.3.20. .................................................................................... 92 3.1.3.21. ....................................................................................... 93 3.1.3.22. .................................................................................... 94 3.1.3.23. ....................................................................................... 95 3.1.3.24. ............................................................................. 96 3.1.3.25. .................................................................................... 97 3.1.3.26. .................................................................................. 103 3.1.3.27. .................................................................................. 107 3.1.3.28. ......................................................................................... 111 3.1.3.29. ..................................................................................... 112 3.1.3.30. .................................................................................. 117 3.1.3.31. ..................................................................................... 122 3.1.3.32. ........................................................................... 123 3.1.3.33. .................................................................................. 126 3.1.3.34. ..................................................................................... 130 3.1.4. ......................................................................................... 133 3.1.4.1. ..................................................................................... 133 3.1.4.2. .............................................................................. 138 3.1.4.3. ......................................................................................... 139 3.1.4.4. ..................................................................................... 143 3.1.4.5. ......................................................................................... 147
viii
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3.1.4.6. ......................................................................................... 148 3.1.4.7. ......................................................................................... 151 3.1.4.8. ..................................................................................... 156 3.1.4.9. ....................................................................... 161 3.1.5. ....................................................................... 162 3.1.5.1. ............................................................................................ 162 3.1.5.2. .................................................................................. 165
3.2. ............................................................................... 166
3.3. ............................................................................... 167
3.3.1. ..................................................................................... 167 3.3.2. ..................................................................................... 168
3.4. ........................................................................... 172
3.4.1. .............................................................................. 172 3.4.1.1. ..................................................................................... 172 3.4.1.2. ..................................................................................... 173 3.4.1.3. .................................................................................. 174 3.4.1.4. .............................................................................. 175 3.4.1.5. .......................................................................... 176 3.4.1.6. .................................................................................. 177 3.4.1.7. .......................................................................... 178 3.4.2. ................................................................ 179 3.4.2.1. ....................................................................... 179 3.4.2.2. ......................................................................................... 180 3.4.2.3. ....................................................................... 181 3.4.2.4. ......................................................................................... 182 3.4.3. .................................................................................. 183 3.4.4. .............................................................................. 185 3.4.4.1. ..................... 185 3.4.4.2. .......................................................................... 187 3.4.4.3. ................................................................ 188 3.4.5. ..................................................................................... 193 3.4.5.1. .......................................................................... 193 3.4.5.2. .......................................................................... 194
ix
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3.4.5.3. ................................................................ 196 3.4.5.4. ....................................................................... 197 3.4.5.5. .................................................................................. 198 3.4.6. ......................................................................................... 199 3.4.6.1. ....................................................................... 199 3.4.6.2. ......................................................................................... 200 3.4.6.3. .................................................................................. 202 3.4.6.4. ........................................................................... 203 3.4.6.5. .................................................................................. 204 3.4.6.6. ....................................................................... 206 3.4.6.7. ......................................................................................... 207 3.4.6.8. .................................................................................. 208 3.4.7. ..................................................................................... 209 3.4.7.1. ................................ 209 3.4.7.2. ......................................................................................... 214 3.4.7.3. ....................................... 216 3.4.7.4. .................................................. 217 3.4.7.5. ................................................................... 218 3.4.8. ................................................................... 219 3.4.8.1. ....................................................................... 219 3.4.8.2. ..................... 221 3.4.8.3. ........................................................................... 223
4.1. ............................................................................... 224
4.2. .................................................................... 226
4.2.1. .............................................................................. 226 4.2.2. ............................ 228 4.2.3. .............................................. 230
4.3. ................................................................ 232
4.4. ................................................................ 236
x
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4.5. ...................................................... 245
4.5.1. 3- -1,2- 3-MCPD ......................... 245 4.5.2. 1,3- -2- 1,3-DCP ............................. 247
4.6. PAHS ..................................... 248
4.7. ........................................................................ 252
4.8. ............................................................................... 253
4.9. ........................................................................... 255
5.1. ........................................................................... 256
5.2. .................................................................................. 262
xi
13-01-276_本文_MK.indd xi13-01-276_本文_MK.indd xi 2013/01/24 21:16:482013/01/24 21:16:48
1
DON
26 30
172 173 174 175
176 177 193 199200 209 214
3- - 3-Ac-DON
26 30
15- - 15-Ac-DON
26 30
NIV
26 30
172 173 174 175
176 177 193 199200 209 214
xii
13-01-276_本文_MK.indd xii13-01-276_本文_MK.indd xii 2013/01/24 21:16:492013/01/24 21:16:49
4- 4-Ac-NIV
26 30
A
17 26
33
26 30
206
2
17 26
34
38 43 44 4752
58 63 74 8186
91 92
xiii
13-01-276_本文_MK.indd xiii13-01-276_本文_MK.indd xiii 2013/01/24 21:16:492013/01/24 21:16:49
97 103 111 112117
123 130 133 138 143 147 148
151 156 161 165
17 26
34
38 43 44 4752
58 63 74 8186
91 92 97 103 111 112
117 123
130 133 138 143 147 148
151 156 161 165
168
xiv
13-01-276_本文_MK.indd xiv13-01-276_本文_MK.indd xiv 2013/01/24 21:16:492013/01/24 21:16:49
169
18
38 43 44 4647 52 57
58 63 79 86 91 92 94 95
96 97 111 112 122
169
17 26
34
38 43 44 4752
58 63 74 8186
91 92 97 103 111 112
117 123
130
xv
13-01-276_本文_MK.indd xv13-01-276_本文_MK.indd xv 2013/01/24 21:16:492013/01/24 21:16:49
133 138 143 147 148151 156 161
165
167
17
167
19 27 31
34
43 45 58 63 68 70
71 73 74 7981 87
91 93 97 103 107
143 147 148 156 162
166
170
xvi
13-01-276_本文_MK.indd xvi13-01-276_本文_MK.indd xvi 2013/01/24 21:16:492013/01/24 21:16:49
3
173 176 178
179
183
193 194 196197 198
201 202 204 208
210 214 216
221
210
PAHs
189 190 191
185 192219
xvii
13-01-276_本文_MK.indd xvii13-01-276_本文_MK.indd xvii 2013/01/24 21:16:492013/01/24 21:16:49
180 181 182
186187
201 202 203 205
206 207
213 215217 218
220 222 223
4
20 28 31
35
39 48 53 59 64 68 72
75 80 82 87 89
98 104 107 112117
123 126 130 134 139 144 149 151
157 162
xviii
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15 7
1
2
3
15 22
1 http://www.fsc.go.jp/hourei/kihonhou_saishin.pdf 2 http://www.maff.go.jp/j/syouan/kijun/codex/standard_list/pdf/cac_gl62.pdf 3 http://www.maff.go.jp/j/syouan/seisaku/risk_analysis/sop/index.html
1
13-01-276_本文_MK.indd 113-01-276_本文_MK.indd 1 2013/01/24 21:16:492013/01/24 21:16:49
2.1.
2.2
2.2.
18
4
PCBDON
NIV A 4 http://www.maff.go.jp/j/syouan/seisaku/risk_analysis/priority/chemical_h18.html
2
13-01-276_本文_MK.indd 213-01-276_本文_MK.indd 2 2013/01/24 21:16:492013/01/24 21:16:49
PAH 3-MCPD, 1,3-DCP
PBDE T-2
HT-2
1822
5
DON NIV A
PBDET-2
HT-2 PAH
18 6
5 http://www.maff.go.jp/j/syouan/seisaku/risk_analysis/survei/middle_chem_h18.html 6 http://www.maff.go.jp/j/syouan/seisaku/risk_manage/index_old.html
3
13-01-276_本文_MK.indd 313-01-276_本文_MK.indd 3 2013/01/24 21:16:492013/01/24 21:16:49
18 22
18 19 20 21 22
DON, NIV
100 100 120 120 120
10 10 100 100 100
50
15 50
15 60
30
20
20
10
20
( ) 20
20
20
20
3-Ac-DON 100 120 120 120
10 100 100 100
15-Ac-DON 100 120 120 120
10 100 100 100
4-Ac-NIV 100 120 120 120
10 100 100 100
A
100 100 100 100
100 100 100 101
20
10
20
10
10
4
13-01-276_本文_MK.indd 413-01-276_本文_MK.indd 4 2013/01/24 21:16:502013/01/24 21:16:50
18 19 20 21 22
A 10
100 100 120 120 120
100 100
300
300
300
300
300
299
201
107
100
32
30
36
30
31
30
40
40
40
30
40
39
32
50
31
33
30
53
30
30
20
5
13-01-276_本文_MK.indd 513-01-276_本文_MK.indd 5 2013/01/24 21:16:502013/01/24 21:16:50
18 19 20 21 22
35
20
50
40
50
50
40
100 20
60 30 30
90 15 15
105 15
60 25 35
20 50 50
53 37 30
10 50 60
60 60
83 37
60 60
84 36
90 30
60 60
60 60
100 20
60 30 30
90 15 15
105 15
60 25 35
20 50 50
53 37 30
10 50 60
60 60
6
13-01-276_本文_MK.indd 613-01-276_本文_MK.indd 6 2013/01/24 21:16:502013/01/24 21:16:50
18 19 20 21 22
83 37
60 60
84 36
90 30
60 60
60 60
1000 1000
120 120
120 120
300 300
120 120
120 120
300 300
300 300
120 120
120 120
120 120
300 300
300 300
300 300
120 120
120
120 120
120 120
120 120
120 120
119 120
600
900
300
201
107
7
13-01-276_本文_MK.indd 713-01-276_本文_MK.indd 7 2013/01/24 21:16:502013/01/24 21:16:50
18 19 20 21 22
100
32
30
36
30
31
30
40
40
40
30
40
39
32
50
31
33
30
53
30
20
35
20
50
40
50
50
40
30
100 150 120
50 50 100
8
13-01-276_本文_MK.indd 813-01-276_本文_MK.indd 8 2013/01/24 21:16:502013/01/24 21:16:50
18 19 20 21 22
50 50
50 50
100 150 120
50 50
50 50
50 50
20
5
5
11
3
1
8
10
2 6
1
1
1
1
1
4
2 17
1 5
1
2
1
4
3
4
7
2
3 1
30 30 25
9
13-01-276_本文_MK.indd 913-01-276_本文_MK.indd 9 2013/01/24 21:16:502013/01/24 21:16:50
18 19 20 21 22
30 30
40 40 25
20
30 30 30
30 30 25
30 30 25
30
30
12 4 30
12 5 30
14 4 30 30
15 5 30 30
12 4 30 30
14 2 30
3 10 30
3 10 30
10 30
3 10 30
2 10 30
30
180
50
149
180 361 59
143
200
30
121
30
10
13-01-276_本文_MK.indd 1013-01-276_本文_MK.indd 10 2013/01/24 21:16:502013/01/24 21:16:50
18 19 20 21 22
50
50
100
100
54 55
81 48
PAH
50
16
34
92
332
112
30
30
10
40
20
10
10
30
80 30
30
10
50
30 30
10
11
13-01-276_本文_MK.indd 1113-01-276_本文_MK.indd 11 2013/01/24 21:16:502013/01/24 21:16:50
18 19 20 21 22
20
60 30
100
100
103 102 50 49 50
90 90 44 46 46
2 6 3 4
102 102 49 49 51
88
99 97 50
92 49 50
105 101 49 48 49
104 100 49 49
97 96 100
132
48
90 95 99
98 98 51 49 51
103 149 99 97 99
92 102 99 100
97 150 100 100 99
102 148 100 99 99
131 100 98 98
94 96 94
98 50 50 50
106 100 100 100 100
103 100
101 99 50 50 50
94
96 49 49 50
100 49 51 50
12
13-01-276_本文_MK.indd 1213-01-276_本文_MK.indd 12 2013/01/24 21:16:512013/01/24 21:16:51
2.3.
7
7
13
13-01-276_本文_MK.indd 1313-01-276_本文_MK.indd 13 2013/01/24 21:16:512013/01/24 21:16:51
18 2217
DON 3-Ac-DON 3- 15-Ac-DON 15- NIV 4-Ac-NIV 4-
PAH PAH 134 188
GEMS/Food
14
13-01-276_本文_MK.indd 1413-01-276_本文_MK.indd 14 2013/01/24 21:16:512013/01/24 21:16:51
60%
60%
1/2
50%
2
8 19
2,3,7,8-TCDD 1 TEQ
TEQpg-TEQ/g TEQ WHO 2005
9
8 http://www.maff.go.jp/j/syouan/seisaku/risk_analysis/survei/result.html 9 http://www.who.int/foodsafety/chem/tef_update/en/index.html
15
13-01-276_本文_MK.indd 1513-01-276_本文_MK.indd 15 2013/01/24 21:16:512013/01/24 21:16:51
16 17
3.1.1.1.
16
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3.1.
3.1.1.
3.1.1.1.
A15 21 1,098 2,898
1 A
21
Codex 0.2 mg/kg
9
1
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg) (mg/kg)
A 498 0.00030 498 - - 0.000072 -
600 0.02 580 < 0.02 0.04 0.011 -
600 0.01 0 0.04 0.43 0.17 0.16
600 0.01 0 0.04 0.37 0.15 0.15
600 0.001 46 < 0.001 0.013 0.003 0.002
17
13-01-276_本文_MK.indd 1713-01-276_本文_MK.indd 17 2013/01/24 21:16:512013/01/24 21:16:51
15 22 10,360 2
0.4 mg/kg 0.4 mg/kg95 23 2
0.4 mg/kg 0.4 mg/kg
2
(mg/kg)
10
(mg/kg)
(mg/kg)
11
1,201
0.04
347
0.4
1,141 0.08
12
9,159 4,080 9,124 0.04
21 22 2,000 3
0.4 mg/kg
10 1.0 ppm Codex
23 2 28 0.4 mg/kg0.4 mg/kg
0.4 mg/kg 11 0.4 mg/kg
3 0.4 mg/kg
12
18
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3
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
2,000 0.04 1,149 < 0.04 0.4 0.05 < 0.04
1517 19 83 4
4 pg-TEQ/g
83 0.000021 0.012 0.0014
1622 151 2,942 199,587
5 199,215
99.8 %XMC 17 1
0.4 mg/kg
19
13-01-276_本文_MK.indd 1913-01-276_本文_MK.indd 19 2013/01/24 21:16:512013/01/24 21:16:51
5
(mg/kg)
(ppm)
2,4-D (2,4-PA) 33 0.01 33 0.1 33
BHC 2,588 0.02 2,588 0.2 2,588
EPN 2,589 0.02 2,588 0.1 2,589
EPTC 2,588 0.02 2,588 0.1 2,588
MCPA 39 0.002 39 0.1 39
MCPB 61 0.01 61 0.1 61
XMC 2,588 0.02 2,583 0.2 2,587
-S-
10 0.01 10 0.1 10
35 0.01 35 0.1 35
95 0.1 95 0.2 95
17 0.01 17 0.05 17
2,588 0.07 2,583 0.2 2,588
MIPC 2,588 0.1 2,588 0.5 2,588
2,588 0.2 2,579 2 2,588
25 0.005 25 0.05 25
3 0.05 3 3 3
IBP 2,589 0.01 2,579 0.2 2,589
66 0.01 66 0.1 66
127 0.04 127 1 127
26 0.02 26 0.05 26
2,601 0.02 2,601 0.05 2,601
P
2,588 0.01 2,588 0.1 2,588
2,607 0.01 2,607 0.02 2,607
EDDP
2599 0.05 2589 0.2 2599
19 0.01 19 0.1 19
20
13-01-276_本文_MK.indd 2013-01-276_本文_MK.indd 20 2013/01/24 21:16:512013/01/24 21:16:51
(mg/kg)
(ppm)
2,691 0.02 2,671 0.5 2,691
2,588 0.005 2,588 0.005 2,588
20 0.01 20 0.1 20
2,588 0.01 2,588 0.1 2,588
1 0.01 1 0.1 1
182 0.05 182 0.05 182
66 0.05 66 0.5 66
138 0.01 138 0.1 138
122 0.05 122 0.1 122
NAC 2,588 0.1 2,588 1 2,588
2,600 0.1 2,600 1 2,600
2,593 0.05 2,593 0.2 2,593
ACN 44 0.003 44 0.03 44
7 0.05 7 5 7
27 0.02 27 0.1 27
49 0.01 49 0.1 49
28 0.05 28 0.50 28
62 0.05 62 0.7 62
7 0.02 7 0.2 7
123 0.02 123 0.1 123
2,588 0.01 2,588 0.1 2,588
2,588 0.01 2,588 0.01 2,588
CVP 2,588 0.02 2,588 0.05 2,588
TPN 55 0.01 55 0.1 55
DCMU 10 0.01 10 0.05 10
63 0.05 63 0.5 63
42 0.01 42 0.1 42
21
13-01-276_本文_MK.indd 2113-01-276_本文_MK.indd 21 2013/01/24 21:16:522013/01/24 21:16:52
(mg/kg)
(ppm)
41 0.01 41 0.1 41
DBN 2 0.01 2 0.05 2
37 0.02 37 2 37
2,588 0.01 2,588 0.07 2,588
2 0.01 2 0.1 2
55 0.2 55 2 55
2,641 0.05 2,641 0.1 2,641
2,588 0.01 2,588 0.1 2,588
2,634 0.01 2,634 0.1 2,634
2,588 0.04 2,587 0.1 2,588
2,588 0.05 2,588 1 2,588
2,607 0.01 2,607 0.05 2,607
2,588 0.05 2,588 0.3 2,588
2,588 0.01 2,588 0.1 2,588
17 0.01 17 0.1 17
2,588 0.01 2,587 0.1 2,588
725 0.03 725 0.1 725
26 0.01 26 0.1 26
13 0.1 13 1 13
28 0.01 28 0.1 28
6 0.01 6 0.1 6
14 0.2 14 2 14
2,599 0.05 2,599 0.2 2,599
2,588 0.01 2,588 0.02 2,588
2,603 0.02 2,597 0.5 2,603
28 0.01 28 0.2 28
2,590 0.01 2,590 0.1 2,590
22
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(mg/kg)
(ppm)
2,588 0.05 2,588 0.05 2,588
54 0.05 54 0.5 54
2,588 0.005 2,588 0.005 2,588
DEP 4 0.01 4 0.20 4
2,679 0.05 2,612 3 2,679
5 0.05 5 5 5
2,588 0.01 2,588 0.05 2,588
30 0.05 30 0.5 30
2,589 0.01 2,589 0.1 2,589
18 0.01 18 0.1 18
2,588 0.02 2,588 1 2,588
11 0.02 11 0.1 11
20 0.01 20 0.1 20
2,588 0.05 2,588 0.1 2,588
196 0.05 196 0.5 196
6 0.01 6 0.1 6
35 0.01 35 0.1 35
134 0.02 134 0.1 134
57 0.02 57 0.1 57
2,588 0.02 2,588 0.1 2,588
2,588 0.05 2,587 0.05 2,588
2,601 0.01 2,600 0.03 2,601
23
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(mg/kg)
(ppm)
2,644 0.02 2,644 0.1 2,644
2,588 0.01 2,588 0.2 2,588
2,651 0.02 2,648 0.2 2,651
2,588 0.01 2,588 0.01 2,588
MEP
2,684 0.05 2,675 0.2 2,684
37 0.1 37 1 37
BPMC
2,614 0.02 2,540 1.0 2,614
150 0.1 143 1 150
MPP 2,598 0.01 2,598 0.05 2,598
PAP 2,595 0.01 2,591 0.05 2,595
69 0.01 69 0.1 69
2,714 0.1 2,709 1 2,714
2,617 0.05 2,617 0.1 2,617
2,588 0.01 2,588 0.05 2,588
81 0.05 81 0.5 81
10 0.01 10 0.1 10
49 0.1 49 1 49
2,588 0.01 2,587 0.02 2,588
2,611 0.03 2,545 2.0 2,611
2,666 0.01 2,666 0.03 2,666
DCPA 2,589 0.01 2,589 0.1 2,589
2,588 0.01 2,588 0.05 2,588
2,588 0.02 2,588 0.1 2,588
27 0.02 27 0.2 27
179 0.05 179 0.5 179
PHC 2,588 0.1 2,588 1 2,588
24
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(mg/kg)
(ppm)
2,588 0.01 2,588 0.05 2,588
2,693 0.1 2,689 0.7 2,693
49 0.01 49 0.05 49
4 0.02 4 2.0 4
2,588 0.1 2,587 0.5 2,588
14 0.01 14 0.1 14
26 0.02 26 0.2 26
56 0.02 56 0.1 56
49 0.01 49 0.1 49
2,588 0.005 2,588 0.02 2,588
65 0.02 65 0.2 65
2,588 0.01 2,588 0.2 2,588
100 0.01 100 0.1 100
76 0.02 76 0.2 76
2,601 0.02 2,601 0.05 2,601
2,588 0.01 2,588 0.1 2,588
150 0.01 150 0.1 150
9 0.01 9 0.1 9
2,588 0.5 2,588 5 2,588
2,588 0.01 2,588 0.1 2,588
2,588 0.01 2,588 0.05 2,588
2,615 0.03 2,615 0.05 2,615
2,595 0.02 2,534 2.0 2,595
38 0.02 38 0.1 38
25
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3.1.1.2.
15 225,921 6
DON NIV DON 13
DON NIV
DON NIV
DON NIV A 95%
DON NIV
A
21
Codex 0.2 mg/kg
8 9
6
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
DON 1,199 0.05 884 < 0.05 0.93 0.059 -
3-Ac-DON 460 0.016 446 < 0.016 0.034 0.004 -
15-Ac-DON 460 0.009 457 < 0.009 0.017 0.002 -
NIV 1,199 0.05 996 < 0.05 1.0 0.037 -
13 1.1 ppm 1.1 mg/kg
26
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3.1.1.2.
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
4-Ac-NIV 460 0.012 460 - - 0.002 -
680 0.012 649 < 0.012 0.44 0.005 -
A 500 0.0002 499 < 0.0002 0.00071 0.00007 -
300 0.02 238 < 0.02 0.05 0.02 -
363 0.01 312 < 0.01 0.04 0.009 -
300 0.001 298 < 0.001 0.001 0.0006 -
1517 19 20 7
7 pg-TEQ/g
20 0.00082 0.014 0.0045
27
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1722 38 598 7,408
8
8
(mg/kg)
(ppm)
MCPA 13 0.002 13 0.1 13
12 0.01 12 0.1 12
29 0.1 29 0.5 29
3 0.02 3 0.05 3
15 0.02 15 0.1 15
282 0.1 282 1 282
289 0.1 289 0.5 289
4 0.05 4 0.1 4
2 0.05 2 0.2 2
404 0.05 403 0.1 404
IPC
287 0.03 287 0.05 287
DDVP 282 0.03 282 0.2 282
394 0.05 394 0.1 394
282 0.005 282 0.2 282
323 0.01 323 0.5 323
284 0.1 284 0.2 284
47 0.1 44 1 47
319 0.05 319 0.05 319
28
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(mg/kg)
(ppm)
25 0.03 25 0.1 25
307 0.05 307 2 307
2 0.05 2 0.5 2
3 0.03 3 0.1 3
302 0.05 302 1.0 302
194 0.02 194 0.1 194
318 0.05 318 0.1 318
285 0.05 285 0.1 285
282 0.05 282 0.1 282
MEP 348 0.1 347 10 348
BPMC 296 0.15 296 0.3 296
PAP 57 0.02 56 0.4 57
282 0.1 282 2 282
463 0.1 461 1.0 463
PHC 1 0.02 1 0.5 1
6 0.005 6 0.05 6
358 0.03 358 0.2 358
282 0.1 282 8 282
301 0.1 301 2 301
25 0.02 25 0.2 25
29
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3.1.1.3.
15 222,090 9
DON NIV
DON NIV
DON NIV DON NIV 8
9
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
DON 480 0.05 335 < 0.05 3.7 0.11 -
3-Ac-DON 310 0.01 251 < 0.01 0.15 0.009 -
15-Ac-DON 310 0.01 305 < 0.01 0.023 0.003 -
NIV 480 0.05 308 < 0.05 3.0 0.09 -
4-Ac-NIV 310 0.008 272 < 0.008 0.22 0.006 -
200 0.0021 171 < 0.0021 0.041 0.002 -
1517 19 20 10
30
13-01-276_本文_MK.indd 3013-01-276_本文_MK.indd 30 2013/01/24 21:16:532013/01/24 21:16:53
3.1.1.3.
10 pg-TEQ/g
20 0.0028 0.016 0.0074
1722 30 83 1,505
11
11
(mg/kg)
(ppm)
7 0.01 7 0.1 7
1 0.04 1 0.3 1
68 0.1 68 1 68
68 0.1 68 0.5 68
2 0.05 2 0.1 2
68 0.05 67 5.0 68
IPC 68 0.02 68 0.05 68
DBN 1 0.005 1 0.05 1
DDVP 68 0.03 68 0.2 68
68 0.05 68 0.1 68
68 0.02 68 0.1 68
68 0.01 68 2 68
31
13-01-276_本文_MK.indd 3113-01-276_本文_MK.indd 31 2013/01/24 21:16:532013/01/24 21:16:53
(mg/kg)
(ppm)
68 0.1 68 0.5 68
13 0.1 9 1 13
71 0.05 71 0.05 71
10 0.01 10 0.1 10
68 0.03 68 0.05 68
72 0.05 72 1.0 72
17 0.02 17 0.1 17
68 0.05 68 0.1 68
68 0.05 68 0.1 68
68 0.05 68 0.1 68
MEP 68 0.1 68 5 68
BPMC 68 0.05 68 0.3 68
74 0.1 72 1.0 74
3 0.005 3 0.05 3
73 0.03 73 0.2 73
68 0.1 68 2 68
68 0.1 68 2 68
5 0.01 5 0.1 5
3.1.1.4.
32
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3.1.1.4.
A20 80 12
12 A
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
20 0.00009 20 - - 0.00004 -
10 0.0003 10 - - 0.0001 -
20 0.00023 20 - - 0.00009 -
10 0.00011 10 - - 0.00004 -
10 0.00013 10 - - 0.00005 -
10 0.00013 10 - - 0.00005 -
33
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3.1.2.
1518 900 13
9
13
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
300 0.02 265 < 0.02 0.06 0.02 -
300 0.01 278 < 0.01 0.04 0.008 -
300 0.001 274 < 0.001 0.002 0.0008 -
1517 19 44 14
14 pg-TEQ/g
44 0.000015 0.0088 0.0012
34
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1822 62 353 1,672
15 1,631 97.5 %
18 1 0.08 mg/kg
19 7
15
(mg/kg)
(ppm)
10 0.02 10 0.5 10
47 0.05 47 0.5 47
32 0.03 32 0.2 32
9 0.01 6 0.05 8
1 0.05 1 0.2 1
20 0.01 20 0.1 20
30 0.02 30 0.03 30
12 0.01 11 0.5 12
11 0.05 11 5 11
147 0.02 147 0.2 147
3 0.01 3 5 3
8 0.01 8 0.3 8
5 0.1 5 10 5
6 0.03 6 0.1 6
3 0.02 3 0.5 3
1 0.01 1 0.3 1
6 0.05 6 1.0 6
35
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(mg/kg)
(ppm)
IPC 2 0.03 2 0.20 2
TPN 2 0.01 2 0.2 2
3 0.02 3 0.3 3
CYAP 11 0.02 11 0.1 11
5 0.03 5 0.1 5
ECP
31 0.01 31 0.03 31
22 0.02 22 0.2 22
56 0.05 50 3 56
7 0.01 7 0.1 7
24 0.1 24 0.5 24
8 0.05 8 0.05 8
3 0.01 3 0.2 3
87 0.02 87 0.05 87
5 0.02 5 0.1 5
11 0.05 11 0.1 11
8 0.02 8 0.1 8
80 0.01 80 0.02 80
121 0.3 121 3 121
10 0.01 10 0.2 10
46 0.01 41 1 46
64 0.05 64 0.02 64
5 0.05 5 0.5 5
39 0.02 39 0.1 39
52 0.01 52 0.15 52
3 0.02 3 0.2 3
MEP
141 0.02 141 0.2 141
36
13-01-276_本文_MK.indd 3613-01-276_本文_MK.indd 36 2013/01/24 21:16:532013/01/24 21:16:53
(mg/kg)
(ppm)
MPP 22 0.01 22 0.02 22
PAP 16 0.02 16 0.05 16
19 0.05 19 0.20 19
2 0.1 1 1 2
14 0.02 14 0.10 14
26 0.05 1 2 26
34 0.02 34 0.05 34
22 0.02 22 0.1 22
2 0.01 2 1 2
2 0.01 2 0.05 2
42 0.02 42 0.05 42
54 0.01 54 0.2 54
2 0.05 2 0.5 2
20 0.3 20 3 20
2 0.05 2 0.2 2
4 0.01 4 0.05 4
1 0.02 1 0.05 1
11 0.02 11 0.2 11
180 0.05 180 0.5 180
37
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3.1.3.
3.1.3.1.
1518 300
21 22 240 16
1
8
16
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
100 0.04 99 < 0.04 0.04 0.01 -
100 0.01 100 - - 0.004 -
100 0.001 99 < 0.001 0.006 0.0006 -
240 0.01 47 < 0.01 0.08 0.02 0.02
1718 92 90 343
17
38
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3.1.3.1.
17
(mg/kg)
(ppm)
BHC 2 0.02 2 0.2 2
DDT 2 0.01 2 0.2 2
29 0.01 27 1.0 29
2 0.01 2 0.05 2
2 0.02 2 0.06 2
2 0.01 2 0.01 2
2 0.07 2 0.05 2
2 0.03 2 0.5 2
4 0.02 4 0.1 4
2 0.01 2 0.02 2
2 0.01 2 0.1 2
2 0.03 2 0.3 2
6 0.01 5 1 6
4 0.01 4 0.10 4
2 0.01 2 0.03 2
NAC 8 0.02 8 0.1 8
2 0.01 2 0.05 2
2 0.01 2 0.1 2
2 0.01 2 0.05 2
2 0.01 2 0.05 2
CVP
2 0.02 2 0.1 2
2 0.02 2 0.1 2
IPC
2 0.03 2 50 2
2 0.02 2 0.02 2
TPN 3 0.01 3 0.2 3
DDVP
7 0.01 7 0.1 7
39
13-01-276_本文_MK.indd 3913-01-276_本文_MK.indd 39 2013/01/24 21:16:542013/01/24 21:16:54
(mg/kg)
(ppm)
2 0.02 2 3 2
5 0.01 5 0.5 5
3 0.02 3 0.04 3
2 0.02 2 0.1 2
2 0.05 2 0.1 2
2 0.03 2 0.05 2
10 0.05 10 0.05 10
10 0.1 10 1.0 10
1 0.01 1 0.1 1
33 0.02 33 2 33
10 0.01 10 0.1 10
6 0.04 6 0.3 6
2 0.05 2 0.02 2
2 0.02 2 0.1 2
2 0.01 2 0.1 2
2 0.02 2 0.1 2
2 0.01 2 0.005 2
2 0.03 2 0.1 2
2 0.02 2 0.1 2
DEP 2 0.01 2 0.50 2
2 0.04 2 0.05 2
5 0.01 5 0.15 5
4 0.02 4 1.0 4
2 0.02 2 0.1 2
2 0.01 2 0.05 2
3 0.01 3 0.05 3
2 0.02 2 0.1 2
2 0.01 2 0.1 2
2 0.01 2 0.05 2
40
13-01-276_本文_MK.indd 4013-01-276_本文_MK.indd 40 2013/01/24 21:16:542013/01/24 21:16:54
(mg/kg)
(ppm)
2 0.01 2 0.05 2
2 0.03 2 1 2
2 0.02 2 0.02 2
MEP
4 0.01 4 0.05 4
2 0.05 2 0.1 2
2 0.02 2 0.1 2
MPP 2 0.01 2 0.05 2
PAP 5 0.01 5 0.05 5
10 0.03 10 0.05 10
2 0.02 2 0.02 2
2 0.02 2 1 2
2 0.01 2 0.2 2
3 0.03 3 0.05 3
2 0.025 2 0.2 2
3 0.01 3 0.01 3
2 0.01 2 0.5 2
2 0.01 2 0.05 2
DCPA
2 0.02 2 0.1 2
2 0.02 2 0.05 2
10 0.01 10 0.05 10
PHC
2 0.02 2 0.5 2
2 0.02 2 0.02 2
2 0.02 2 0.2 2
2 0.02 2 0.03 2
2 0.02 2 0.05 2
2 0.01 2 0.05 2
3 0.05 3 0.2 3
10 0.02 10 0.1 10
1 0.02 1 0.03 1
41
13-01-276_本文_MK.indd 4113-01-276_本文_MK.indd 41 2013/01/24 21:16:542013/01/24 21:16:54
(mg/kg)
(ppm)
2 0.02 2 0.2 2
3 0.01 3 0.5 3
10 0.03 10 0.3 10
2 0.01 2 0.25 2
3 0.01 3 0.3 3
DMTP
2 0.01 2 0.02 2
6 0.02 6 1.0 6
1 0.02 1 0.1 1
3.1.3.2.
42
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3.1.3.2.
1518 300
21 22 240 18
9
5
18
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
100 0.04 99 < 0.04 0.04 0.02 -
100 0.01 94 < 0.01 0.01 0.004 -
100 0.001 100 - - 0.0005 -
240 0.01 123 < 0.01 0.02 0.01 -
1517 19 15 19
19 pg-TEQ/g
15 0.00019 0.087 0.014
43
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3.1.3.3.
1518 20 596
8821 22 600 20 21
7 8
9
20
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
400 0.04 364 < 0.04 0.36 0.03 -
98 0.01 59 < 0.01 0.04 0.01 -
98 0.001 72 < 0.001 0.004 0.001 -
600 0.01 71 < 0.01 0.42 0.04 0.03
21
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
30 0.04 30 - - 0.02 -
29 0.01 29 - - 0.006 -
29 0.001 24 < 0.001 0.001 0.001 -
44
13-01-276_本文_MK.indd 4413-01-276_本文_MK.indd 44 2013/01/24 21:16:542013/01/24 21:16:54
3.1.3.3.
1517 19 7 22
22 pg-TEQ/g
7 0.00037 0.0042 0.0019
45
13-01-276_本文_MK.indd 4513-01-276_本文_MK.indd 45 2013/01/24 21:16:542013/01/24 21:16:54
3.1.3.4.
2122 240 23
5
23
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
240 0.01 131 < 0.01 0.08 0.01 -
3.1.3.5.
46
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3.1.3.4.
3.1.3.5.
1518 300
21 22 240 24
1
8
24
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
100 0.04 100 - - 0.01 -
100 0.01 100 - - 0.004 -
100 0.001 99 < 0.001 0.001 0.0004 -
240 0.01 194 < 0.01 0.05 0.01 -
1720 99 415 13,027
25
47
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25
(mg/kg)
(ppm)
BHC 156 0.02 156 0.2 156
DDT 156 0.01 156 0.2 156
7 0.01 7 0.5 7
207 0.01 195 1.0 207
177 0.01 176 0.5 177
156 0.02 156 0.02 156
166 0.01 166 0.01 166
171 0.07 171 0.1 171
157 0.05 157 5.0 157
3 0.02 3 0.1 3
156 0.01 156 0.3 156
184 0.02 184 2 184
156 0.01 156 0.1 156
156 0.01 156 0.005 156
160 0.03 160 0.50 160
156 0.01 155 5 156
12 0.01 12 0.50 12
8 0.01 8 0.2 8
165 0.01 165 0.05 165
NAC 157 0.02 156 1.0 157
156 0.01 156 0.05 156
3 0.01 3 5 3
156 0.01 156 0.3 156
162 0.01 162 0.5 162
157 0.01 157 0.1 157
170 0.01 169 0.1 170
CVP 156 0.02 156 0.1 156
168 0.05 168 2.0 168
IPC
156 0.03 156 0.05 156
48
13-01-276_本文_MK.indd 4813-01-276_本文_MK.indd 48 2013/01/24 21:16:552013/01/24 21:16:55
(mg/kg)
(ppm)
156 0.02 156 0.02 156
TPN 9 0.01 9 0.1 9
13 0.03 13 0.05 13
CYAP 17 0.02 17 0.05 17
156 0.02 156 5.0 156
ECP 3 0.01 3 0.03 3
DDVP 41 0.01 41 0.1 41
156 0.02 156 3 156
27 0.01 27 0.2 27
4 0.01 2 0.5 4
156 0.02 156 0.5 156
156 0.05 156 0.5 156
156 0.03 156 0.5 156
162 0.05 162 0.05 162
164 0.1 164 1 164
156 0.02 156 0.05 156
3 0.01 3 0.2 3
220 0.02 220 0.1 220
162 0.04 162 0.5 162
156 0.005 156 0.02 156
294 0.02 294 0.1 294
166 0.03 166 0.1 166
156 0.01 156 0.005 156
156 0.03 156 0.1 156
156 0.02 156 0.1 156
156 0.04 156 1.0 156
DEP 4 0.01 3 0.20 4
164 0.01 164 0.05 164
169 0.02 169 2.0 169
49
13-01-276_本文_MK.indd 4913-01-276_本文_MK.indd 49 2013/01/24 21:16:552013/01/24 21:16:55
(mg/kg)
(ppm)
10 0.01 10 0.2 10
156 0.01 156 0.3 156
156 0.02 156 1.0 156
156 0.01 156 0.05 156
157 0.01 157 0.1 157
8 0.05 8 0.1 8
2 0.02 2 0.1 2
156 0.01 156 0.10 156
156 0.01 156 1.0 156
156 0.03 156 1 156
156 0.02 156 0.5 156
MEP 156 0.01 156 0.2 156
156 0.05 156 0.1 156
BPMC 156 0.01 156 0.3 156
PAP 214 0.02 213 0.1 214
166 0.1 166 0.50 166
156 0.02 156 0.02 156
156 0.01 156 0.05 156
156 0.03 156 0.05 156
158 0.01 158 0.05 158
161 0.02 161 0.1 161
2 0.01 2 0.03 2
156 0.01 156 0.5 156
DCPA 156 0.02 156 0.1 156
156 0.02 156 0.05 156
PHC 156 0.02 156 2 156
156 0.02 156 0.02 156
156 0.02 156 0.03 156
156 0.02 156 0.1 156
156 0.05 156 0.05 156
50
13-01-276_本文_MK.indd 5013-01-276_本文_MK.indd 50 2013/01/24 21:16:552013/01/24 21:16:55
(mg/kg)
(ppm)
156 0.02 156 0.5 156
32 0.02 25 0.2 32
156 0.02 156 0.3 156
161 0.03 161 0.5 161
219 0.03 218 0.5 219
191 0.01 184 0.5 191
167 0.02 167 2 167
DMTP 156 0.01 156 0.05 156
1 0.02 1 0.1 1
188 0.02 188 1.0 188
2 0.02 2 0.05 2
51
13-01-276_本文_MK.indd 5113-01-276_本文_MK.indd 51 2013/01/24 21:16:552013/01/24 21:16:55
3.1.3.5.
1518 300
21 22 600 26
1
7
26
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
100 0.04 100 - - 0.02 -
100 0.01 100 - - 0.004 -
100 0.001 99 < 0.001 0.001 0.0008 -
600 0.01 157 < 0.01 0.14 0.02 0.02
1718 21 22 86 193
659 27
52
3.1.3.63.1.3.6
13-01-276_本文_MK.indd 5213-01-276_本文_MK.indd 52 2013/01/24 21:16:552013/01/24 21:16:55
3.1.3.5.
27
(mg/kg)
(ppm)
DDT 2 0.01 2 0.2 2
4 0.01 4 1 4
2 0.02 2 0.02 2
2 0.01 2 0.01 2
5 0.07 5 0.1 5
33 0.05 31 5.0 33
1 0.02 1 0.4 1
2 0.01 2 0.3 2
2 0.02 2 0.5 2
2 0.01 2 0.005 2
2 0.01 2 0.2 2
2 0.03 2 0.2 2
2 0.005 2 0.01 2
2 0.01 2 5 2
7 0.01 7 0.20 7
NAC 2 0.02 2 0.5 2
2 0.01 2 0.05 2
34 0.02 34 0.3 34
2 0.01 2 0.5 2
2 0.01 2 0.03 2
CVP
2 0.02 2 0.4 2
2 0.02 2 2.0 2
IPC
2 0.03 2 0.05 2
2 0.02 2 0.02 2
TPN 6 0.01 6 1 6
2 0.02 2 5.0 2
DDVP
42 0.01 42 0.1 42
53
13-01-276_本文_MK.indd 5313-01-276_本文_MK.indd 53 2013/01/24 21:16:552013/01/24 21:16:55
(mg/kg)
(ppm)
2 0.02 2 3 2
1 0.01 0 0.7 1
2 0.02 2 0.5 2
2 0.02 2 0.2 2
2 0.05 2 0.1 2
2 0.03 2 0.5 2
4 0.05 4 0.05 4
8 0.1 8 1 8
2 0.02 2 0.05 2
3 0.02 3 0.2 3
45 0.02 45 0.5 45
30 0.04 30 0.5 30
3 0.05 3 0.02 3
2 0.005 2 0.1 2
31 0.02 31 0.1 31
2 0.02 2 0.1 2
2 0.01 2 0.005 2
2 0.03 2 0.1 2
2 0.02 2 0.1 2
DEP 3 0.01 3 0.5 3
3 0.05 3 1.0 3
15 0.01 13 1 15
4 0.02 4 2.0 4
2 0.01 2 0.3 2
2 0.02 2 1.0 2
2 0.01 2 0.05 2
2 0.01 2 0.50 2
2 0.01 2 1.0 2
2 0.03 2 1 2
2 0.02 2 0.5 2
54
13-01-276_本文_MK.indd 5413-01-276_本文_MK.indd 54 2013/01/24 21:16:562013/01/24 21:16:56
(mg/kg)
(ppm)
MEP
2 0.01 2 0.2 2
2 0.05 2 0.1 2
BPMC
2 0.01 2 0.3 2
PAP 31 0.02 29 0.1 31
2 0.03 2 0.50 2
2 0.02 2 0.02 2
20 0.01 20 0.05 20
2 0.03 2 0.05 2
2 0.01 2 0.02 2
2 0.01 2 0.5 2
DCPA 2 0.02 2 0.1 2
2 0.02 2 0.05 2
PHC 2 0.02 2 2 2
2 0.02 2 0.02 2
2 0.02 2 0.1 2
5 0.02 5 0.1 5
75 0.05 75 0.2 75
2 0.02 2 0.5 2
2 0.01 2 0.7 2
41 0.02 38 0.2 41
2 0.02 2 0.3 2
13 0.03 13 0.5 13
42 0.03 42 0.5 42
2 0.01 2 0.01 2
4 0.02 4 0.05 4
DMTP
2 0.01 2 0.1 2
1 0.02 1 0.1 1
55
13-01-276_本文_MK.indd 5513-01-276_本文_MK.indd 55 2013/01/24 21:16:562013/01/24 21:16:56
(mg/kg)
(ppm)
2 0.02 2 2 2
33 0.02 29 1 33
3.1.3.6.
56
13-01-276_本文_MK.indd 5613-01-276_本文_MK.indd 56 2013/01/24 21:16:562013/01/24 21:16:56
3.1.3.6.
2122 600 28
9
28
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
600 0.01 37 < 0.01 0.21 0.03 0.03
57
3.1.3.73.1.3.7
13-01-276_本文_MK.indd 5713-01-276_本文_MK.indd 57 2013/01/24 21:16:562013/01/24 21:16:56
3.1.3.7.
1518 301
21 22 240 29
6
29
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
101 0.05 101 - - 0.02 -
100 0.01 100 - - 0.003 -
100 0.001 100 - - 0.0004 -
240 0.01 141 < 0.01 0.04 0.01 -
228 30
30 pg-TEQ/g
8 0 0.00056 0.00011
58
3.1.3.83.1.3.8
13-01-276_本文_MK.indd 5813-01-276_本文_MK.indd 58 2013/01/24 21:16:562013/01/24 21:16:56
3.1.3.7.
17 22 98 421 6,908
31
31
(mg/kg)
ppm
BHC 65 0.02 65 0.2 65
DDT 65 0.01 65 0.2 65
16 0.02 15 5 16
209 0.01 185 5.0 209
116 0.01 115 3.0 116
65 0.02 65 0.02 65
65 0.01 65 0.01 65
66 0.07 66 0.1 66
155 0.05 144 5.0 155
62 0.02 57 0.5 62
65 0.01 65 0.3 65
107 0.02 106 5 107
65 0.01 65 0.005 65
65 0.01 65 0.1 65
66 0.03 66 0.5 66
78 0.05 76 5 78
51 0.01 38 2 51
NAC 75 0.05 75 1.0 75
65 0.01 65 0.05 65
7 0.01 7 5 7
113 0.02 106 2 113
65 0.01 65 1.0 65
75 0.02 75 0.1 75
59
13-01-276_本文_MK.indd 5913-01-276_本文_MK.indd 59 2013/01/24 21:16:562013/01/24 21:16:56
(mg/kg)
ppm
137 0.02 129 1 137
CVP 65 0.02 65 0.1 65
78 0.05 78 2.0 78
IPC
65 0.03 65 0.05 65
65 0.02 65 0.02 65
TPN 70 0.01 52 2 70
52 0.03 52 2 52
CYAP 3 0.02 3 0.05 3
65 0.02 65 5.0 65
DDVP
51 0.01 51 0.1 51
65 0.02 65 3 65
2 0.01 2 0.5 2
13 0.01 9 1.4 13
66 0.02 66 1.0 66
65 0.02 65 0.2 65
67 0.05 67 2.0 67
65 0.03 65 1.0 65
77 0.05 77 5.0 77
84 0.1 84 1 84
79 0.02 79 0.2 79
25 0.02 24 8 25
83 0.02 83 0.1 83
23 0.02 21 2 23
92 0.04 92 2 92
65 0.005 65 0.02 65
65 0.02 65 10 65
79 0.02 79 0.1 79
92 0.03 91 0.5 92
60
13-01-276_本文_MK.indd 6013-01-276_本文_MK.indd 60 2013/01/24 21:16:562013/01/24 21:16:56
(mg/kg)
ppm
65 0.01 65 0.005 65
3 0.01 2 0.5 3
65 0.03 65 0.1 65
65 0.02 65 0.1 65
65 0.04 65 1.0 65
79 0.01 79 0.05 79
67 0.02 67 2.0 67
7 0.01 6 0.5 7
65 0.01 65 0.3 65
65 0.02 65 1.0 65
65 0.01 65 0.05 65
69 0.01 69 0.5 69
42 0.02 35 1 42
65 0.01 65 2.0 65
65 0.01 65 1.0 65
65 0.03 65 1 65
65 0.02 65 0.5 65
MEP
65 0.01 65 0.5 65
65 0.05 65 0.1 65
BPMC
65 0.01 65 0.3 65
PAP 90 0.02 90 0.1 90
177 0.1 174 3.0 177
65 0.02 65 0.02 65
65 0.02 65 3 65
65 0.01 65 0.05 65
66 0.03 66 0.50 66
73 0.01 69 1.0 73
82 0.02 81 0.5 82
57 0.01 39 5 57
65 0.01 65 0.5 65
61
13-01-276_本文_MK.indd 6113-01-276_本文_MK.indd 61 2013/01/24 21:16:562013/01/24 21:16:56
(mg/kg)
ppm
65 0.01 65 0.1 65
DCPA 65 0.02 65 0.1 65
65 0.02 65 0.05 65
PHC 65 0.02 65 2 65
65 0.02 65 0.02 65
65 0.02 65 0.03 65
77 0.02 77 5.0 77
68 0.05 68 0.2 68
65 0.02 65 0.5 65
65 0.02 65 0.3 65
171 0.03 171 2.0 171
188 0.03 177 2 188
178 0.01 145 2 178
102 0.02 101 0.3 102
DMTP
65 0.01 65 0.1 65
8 0.02 8 7.0 8
10 0.05 10 1 10
3.1.3.8.
62
13-01-276_本文_MK.indd 6213-01-276_本文_MK.indd 62 2013/01/24 21:16:562013/01/24 21:16:56
3.1.3.8.
1518 300
21 22 240 32
6
32
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
100 0.05 100 - - 0.02 -
100 0.01 100 - - 0.003 -
100 0.001 100 - - 0.0004 -
240 0.01 234 < 0.01 0.02 0.01 -
2210 33
33 pg-TEQ/g
10 0 0.00061 0.00011
63
3.1.3.93.1.3.9
13-01-276_本文_MK.indd 6313-01-276_本文_MK.indd 63 2013/01/24 21:16:572013/01/24 21:16:57
1721 109 441 12,424
34
34
(mg/kg)
(ppm)
BHC 133 0.02 133 0.2 133
DDT 133 0.01 133 0.2 133
EPN 146 0.03 146 0.1 146
9 0.01 9 5 9
229 0.01 197 5.0 229
144 0.01 144 3.0 144
133 0.02 133 0.02 133
139 0.01 139 0.01 139
137 0.07 137 0.1 137
179 0.05 178 5.0 179
17 0.02 17 0.5 17
133 0.01 133 0.3 133
168 0.02 168 2 168
133 0.01 133 0.02 133
133 0.01 133 0.1 133
134 0.03 134 2 134
135 0.01 133 5 135
10 0.01 9 2 10
133 0.01 133 0.01 133
NAC 136 0.05 136 1.0 136
133 0.01 133 0.05 133
3 0.01 3 5 3
133 0.01 133 2 133
64
13-01-276_本文_MK.indd 6413-01-276_本文_MK.indd 64 2013/01/24 21:16:572013/01/24 21:16:57
(mg/kg)
(ppm)
4 0.005 4 0.7 4
133 0.01 133 0.05 133
135 0.02 135 0.1 135
199 0.01 195 0.7 199
CVP
133 0.02 133 0.2 133
154 0.05 154 2.0 154
IPC
133 0.03 133 0.05 133
133 0.02 133 0.02 133
TPN 20 0.01 20 2 20
5 0.03 5 0.05 5
133 0.01 133 0.05 133
CYAP 1 0.02 1 0.05 1
133 0.02 133 5.0 133
DDVP
42 0.01 42 0.1 42
133 0.02 133 3 133
13 0.01 12 0.5 13
3 0.01 2 2 3
140 0.05 140 0.4 140
133 0.02 133 0.2 133
133 0.05 133 2.0 133
133 0.03 133 1.0 133
140 0.05 140 1.0 140
18 0.01 18 0.1 18
143 0.1 143 1 143
1 0.01 1 2 1
133 0.02 133 0.2 133
16 0.01 16 2 16
170 0.02 170 0.1 170
65
13-01-276_本文_MK.indd 6513-01-276_本文_MK.indd 65 2013/01/24 21:16:572013/01/24 21:16:57
(mg/kg)
(ppm)
19 0.02 19 1 19
169 0.04 168 5 169
133 0.005 133 0.02 133
133 0.02 133 5 133
142 0.02 142 0.1 142
172 0.03 172 0.5 172
133 0.01 133 0.05 133
1 0.01 1 0.5 1
133 0.03 133 1 133
133 0.02 133 0.1 133
DEP 2 0.01 1 0.50 2
133 0.04 133 1.0 133
143 0.01 143 0.1 143
165 0.02 165 2.0 165
8 0.01 8 0.3 8
133 0.01 133 0.3 133
133 0.02 133 0.2 133
133 0.01 133 0.05 133
135 0.01 135 2 135
27 0.02 27 0.2 27
133 0.01 133 1.0 133
133 0.01 133 1.0 133
133 0.03 133 1.0 133
133 0.02 133 0.5 133
MEP
133 0.01 133 0.5 133
133 0.05 133 0.1 133
BPMC
133 0.01 133 0.3 133
PAP 177 0.02 177 0.1 177
180 0.1 180 3.0 180
133 0.02 133 0.02 133
66
13-01-276_本文_MK.indd 6613-01-276_本文_MK.indd 66 2013/01/24 21:16:572013/01/24 21:16:57
(mg/kg)
(ppm)
133 0.02 133 0.4 133
134 0.01 134 0.05 134
4 0.005 4 2 4
138 0.03 138 0.50 138
162 0.03 162 2.0 162
136 0.01 136 0.5 136
163 0.02 163 0.5 163
53 0.01 52 3 53
159 0.03 156 2 159
140 0.02 139 0.2 140
DCPA 133 0.02 133 0.1 133
133 0.02 133 0.05 133
PHC 133 0.02 133 0.05 133
133 0.02 133 0.02 133
133 0.02 133 0.03 133
144 0.02 144 5.0 144
136 0.05 136 0.2 136
134 0.02 134 0.5 134
7 0.01 6 3.0 7
133 0.02 133 2.0 133
178 0.03 178 2.0 178
252 0.03 250 5 252
194 0.01 166 1.0 194
146 0.02 146 0.5 146
DMTP
133 0.01 133 0.1 133
7 0.02 7 7 7
4 0.02 4 1 4
18 0.02 18 1 18
67
13-01-276_本文_MK.indd 6713-01-276_本文_MK.indd 67 2013/01/24 21:16:572013/01/24 21:16:57
3.1.3.9.
1517 19 22 14
35
35 pg-TEQ/g
14 0.0011 0.035 0.014
20 22 21 293 642
36
36
(mg/kg)
(ppm)
82 0.02 51 5 82
7 0.01 7 5.0 7
2 0.01 2 15 2
6 0.005 6 0.01 6
16 0.02 16 5 16
1 0.01 1 5 1
68
3.1.3.10.3.1.3.10.3.1.3.9.
13-01-276_本文_MK.indd 6813-01-276_本文_MK.indd 68 2013/01/24 21:16:572013/01/24 21:16:57
3.1.3.9.
(mg/kg)
(ppm)
22 0.02 13 5 22
55 0.03 26 15 55
59 0.01 10 5 59
67 0.05 38 5.0 67
69 0.02 65 5 69
47 0.02 45 0.1 47
4 0.02 2 5 4
69 0.02 64 0.5 69
4 0.01 3 0.05 4
19 0.01 13 1.0 19
50 0.02 28 10 50
18 0.02 15 2 18
7 0.01 7 0.7 7
37 0.02 31 1 37
1 0.02 1 0.01 1
69
13-01-276_本文_MK.indd 6913-01-276_本文_MK.indd 69 2013/01/24 21:16:572013/01/24 21:16:57
3.1.3.10.
22 1 37
37
pg-TEQ/g
1 - - 0.016
3.1.3.11.
70
3.1.3.11.3.1.3.11.
13-01-276_本文_MK.indd 7013-01-276_本文_MK.indd 70 2013/01/24 21:16:572013/01/24 21:16:57
3.1.3.10.
3.1.3.11.
1517 19 4 38
38 pg-TEQ/g
4 0.015 0.038 0.025
1916 132 174
39 144 82.8 %
1 0.09 mg/kg
71
3.1.3.12.3.1.3.12.
13-01-276_本文_MK.indd 7113-01-276_本文_MK.indd 71 2013/01/24 21:16:582013/01/24 21:16:58
39
(mg/kg)
(ppm)
9 0.01 4 5 9
3 0.01 3 5 3
1 0.005 1 0.01 1
4 0.02 3 5 4
4 0.03 3 10 4
DDVP 9 0.01 9 0.1 9
9 0.01 6 5.0 9
4 0.01 3 5 4
36 0.02 35 0.1 36
39 0.02 38 0.5 39
9 0.01 8 0.05 8
6 0.01 5 1.0 6
27 0.02 14 10 27
10 0.02 8 3.0 10
3 0.01 3 2 3
1 0.02 1 2 1
3.1.3.12.
72
13-01-276_本文_MK.indd 7213-01-276_本文_MK.indd 72 2013/01/24 21:16:582013/01/24 21:16:58
3.1.3.12.
1517 19 4 40
40 pg-TEQ/g
4 0.0055 0.012 0.0087
73
3.1.3.13.3.1.3.13.
13-01-276_本文_MK.indd 7313-01-276_本文_MK.indd 73 2013/01/24 21:16:582013/01/24 21:16:58
3.1.3.13.
15 18 300 41
1
41
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
100 0.05 100 - - 0.02 -
100 0.01 99 < 0.01 0.01 0.003 -
100 0.001 99 < 0.001 0.001 0.0007 -
22 1 42
42
pg-TEQ/g
1 - - 0.00042
74
3.1.3.14.3.1.3.14.
13-01-276_本文_MK.indd 7413-01-276_本文_MK.indd 74 2013/01/24 21:16:582013/01/24 21:16:58
3.1.3.13.
17 22 94 76 1,829 43
43
(mg/kg)
(ppm)
BHC 21 0.02 21 0.2 21
DDT 21 0.01 21 0.2 21
EPN 26 0.03 26 0.1 26
2 0.02 2 2 2
38 0.01 38 5.0 38
21 0.01 21 3.0 21
21 0.02 21 0.02 21
21 0.01 21 0.01 21
22 0.07 22 0.1 22
22 0.05 22 25 22
1 0.02 1 5 1
21 0.01 21 0.3 21
21 0.02 21 2 21
21 0.01 21 0.005 21
21 0.01 21 0.2 21
21 0.03 21 0.5 21
21 0.01 21 5 21
6 0.01 4 0.2 6
NAC 21 0.02 21 6 21
21 0.01 21 0.05 21
1 0.01 1 5 1
21 0.01 21 30 21
2 0.005 2 1 2
75
13-01-276_本文_MK.indd 7513-01-276_本文_MK.indd 75 2013/01/24 21:16:582013/01/24 21:16:58
(mg/kg)
(ppm)
21 0.01 21 1 21
21 0.01 21 0.03 21
35 0.02 33 1 35
CVP
21 0.02 21 0.05 21
27 0.05 27 2.0 27
21 0.02 21 0.02 21
TPN 2 0.01 1 5 2
1 0.03 1 1 1
21 0.02 21 5.0 21
DDVP
4 0.01 4 0.1 4
21 0.02 21 3 21
4 0.01 4 2 4
21 0.02 21 0.5 21
21 0.02 21 0.2 21
21 0.05 21 2.0 21
21 0.03 21 1 21
21 0.05 21 1.0 21
21 0.1 21 1 21
21 0.02 21 0.05 21
14 0.02 14 2 14
23 0.02 23 0.1 23
4 0.02 4 2 4
21 0.04 21 2 21
21 0.02 21 0.5 21
24 0.02 24 0.5 24
29 0.03 29 1 29
21 0.01 21 0.05 21
21 0.03 21 1 21
21 0.02 21 0.1 21
21 0.04 21 1.0 21
76
13-01-276_本文_MK.indd 7613-01-276_本文_MK.indd 76 2013/01/24 21:16:582013/01/24 21:16:58
(mg/kg)
(ppm)
22 0.01 22 0.05 22
22 0.02 22 2.0 22
5 0.01 4 1 5
21 0.01 21 0.3 21
21 0.02 21 0.2 21
21 0.01 21 0.05 21
21 0.01 21 0.1 21
10 0.02 10 2 10
21 0.01 21 1.0 21
21 0.01 21 1.0 21
21 0.03 21 1 21
1 0.01 1 0.05 1
21 0.02 21 0.5 21
MEP
21 0.01 21 0.5 21
21 0.05 21 0.1 21
BPMC
21 0.01 21 0.3 21
PAP 27 0.02 27 0.1 27
23 0.1 23 2.0 23
21 0.02 21 0.02 21
21 0.02 21 3 21
21 0.01 21 0.05 21
21 0.03 21 0.20 21
24 0.02 24 5 24
21 0.01 21 5 21
21 0.01 21 0.2 21
DCPA 21 0.02 21 0.1 21
21 0.02 21 0.05 21
PHC 21 0.02 21 2 21
21 0.02 21 0.02 21
21 0.02 21 0.5 21
77
13-01-276_本文_MK.indd 7713-01-276_本文_MK.indd 77 2013/01/24 21:16:582013/01/24 21:16:58
(mg/kg)
(ppm)
21 0.02 21 0.03 21
27 0.02 27 2.0 27
21 0.05 21 0.05 21
21 0.02 21 0.5 21
21 0.02 21 0.3 21
24 0.03 24 5.0 24
28 0.03 28 2 28
38 0.01 38 1.0 38
27 0.02 27 0.5 27
DMTP
21 0.01 21 0.1 21
4 0.02 4 5 4
3.1.3.14.
78
13-01-276_本文_MK.indd 7813-01-276_本文_MK.indd 78 2013/01/24 21:16:592013/01/24 21:16:59
3.1.3.14.
2122 240 44
8
44
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
240 0.01 45 < 0.01 0.4 0.03 0.02
221 45
45 pg-TEQ/g
1 - - 0.044
79
3.1.3.15.3.1.3.15.
13-01-276_本文_MK.indd 7913-01-276_本文_MK.indd 79 2013/01/24 21:16:592013/01/24 21:16:59
2022 13 284 369
46
46
(mg/kg)
(ppm)
44 0.02 27 5 44
4 0.01 0 30 4
33 0.03 32 0.1 33
1 0.02 1 2.5 1
1 0.01 1 5 1
54 0.02 30 30 54
65 0.01 16 20 65
3 0.05 3 5 3
2 0.01 2 0.2 2
1 0.025 1 5 1
150 0.02 75 10 150
8 0.5 4 100 8
3 0.02 1 3.0 3
3.1.3.15.
80
13-01-276_本文_MK.indd 8013-01-276_本文_MK.indd 80 2013/01/24 21:16:592013/01/24 21:16:59
3.1.3.15.
1518 298 47
1
47
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
100 0.05 100 - - 0.02 -
99 0.01 99 - - 0.003 -
99 0.001 98 < 0.001 0.001 0.0004 -
224 48
48 pg-TEQ/g
4 0.000003 0.00019 0.000081
81
3.1.3.16.3.1.3.16.
13-01-276_本文_MK.indd 8113-01-276_本文_MK.indd 81 2013/01/24 21:16:592013/01/24 21:16:59
1722 97 358 2,334
49
49
(mg/kg)
(ppm)
BHC 11 0.02 11 0.2 11
DDT 11 0.01 11 0.2 11
9 0.02 8 5 9
111 0.01 94 5.0 111
69 0.01 63 30 69
11 0.02 11 0.02 11
11 0.01 11 0.01 11
19 0.07 19 0.1 19
85 0.05 79 10 85
34 0.02 31 2.5 34
11 0.01 11 2 11
37 0.02 36 2 37
11 0.01 11 0.02 11
11 0.01 11 0.2 11
11 0.03 11 1 11
14 0.01 12 5 14
1 0.01 0 0.50 1
37 0.01 34 0.7 37
NAC 11 0.02 11 10 11
11 0.01 11 0.05 11
11 0.01 11 30 11
14 0.005 11 20 14
11 0.01 11 0.1 11
82
13-01-276_本文_MK.indd 8213-01-276_本文_MK.indd 82 2013/01/24 21:16:592013/01/24 21:16:59
(mg/kg)
(ppm)
11 0.01 11 0.1 11
84 0.02 71 20 84
CVP
11 0.02 11 0.1 11
14 0.05 14 2.0 14
IPC
12 0.03 12 0.05 12
11 0.02 11 0.02 11
TPN 34 0.01 31 1 34
9 0.03 7 10 9
55 0.05 55 5.0 55
DDVP
49 0.01 49 0.1 49
11 0.02 11 3 11
18 0.01 15 5 18
18 0.05 18 2.0 18
11 0.05 11 2.0 11
11 0.03 11 1 11
27 0.05 26 2.0 27
11 0.1 11 2 11
11 0.02 11 2 11
20 0.02 19 8 20
43 0.02 43 0.1 43
36 0.02 32 3 36
46 0.04 46 5 46
11 0.05 11 0.2 11
11 0.02 11 10 11
21 0.02 21 0.5 21
45 0.03 44 1 45
11 0.01 11 0.005 11
11 0.03 11 0.1 11
83
13-01-276_本文_MK.indd 8313-01-276_本文_MK.indd 83 2013/01/24 21:16:592013/01/24 21:16:59
(mg/kg)
(ppm)
11 0.02 11 0.1 11
11 0.04 11 1.0 11
15 0.01 15 0.1 15
46 0.02 41 2.0 46
28 0.01 24 10 28
11 0.01 11 0.3 11
11 0.02 11 1.0 11
11 0.01 11 0.05 11
11 0.01 11 3.0 11
16 0.02 16 5 16
11 0.01 11 0.01 11
11 0.01 11 0.01 11
11 0.03 11 0.03 11
11 0.02 11 0.02 11
MEP
11 0.01 11 0.2 11
11 0.05 11 0.1 11
BPMC
11 0.01 11 0.3 11
PAP 20 0.02 20 0.1 20
97 0.1 93 2.0 97
11 0.02 11 0.02 11
13 0.01 13 0.05 13
11 0.01 11 13 11
11 0.03 11 0.05 11
16 0.03 16 3.0 16
23 0.01 18 3.0 23
41 0.02 41 10 41
65 0.01 50 15 65
70 0.03 42 5 70
DCPA 11 0.02 11 0.1 11
11 0.02 11 0.05 11
84
13-01-276_本文_MK.indd 8413-01-276_本文_MK.indd 84 2013/01/24 21:16:592013/01/24 21:16:59
(mg/kg)
(ppm)
PHC 11 0.02 11 2 11
11 0.02 11 0.02 11
11 0.02 11 0.5 11
11 0.02 11 0.03 11
26 0.02 23 3.0 26
13 0.05 13 0.2 13
11 0.02 11 0.5 11
5 0.02 2 20 5
11 0.02 11 0.3 11
101 0.03 101 2.0 101
122 0.03 116 5 122
87 0.01 82 1.0 87
11 0.01 11 2 11
DMTP
11 0.01 11 0.1 11
8 0.02 7 30 8
11 0.02 11 1.0 11
85
13-01-276_本文_MK.indd 8513-01-276_本文_MK.indd 85 2013/01/24 21:16:592013/01/24 21:16:59
3.1.3.16.
15 18 20 66121 22 600
50 9 8
6
10
50
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
401 0.05 364 < 0.05 0.34 0.04 -
160 0.01 126 < 0.01 0.12 0.01 -
100 0.001 34 < 0.001 0.006 0.001 0.001
600 0.01 10 < 0.01 0.59 0.06 0.05
15 17 19 22 25 51
86
3.1.3.17.3.1.3.17.
13-01-276_本文_MK.indd 8613-01-276_本文_MK.indd 86 2013/01/24 21:17:002013/01/24 21:17:00
3.1.3.16.
51 pg-TEQ/g
25 0.0059 0.081 0.033
18 22 29 547 1,069 52
2222 10 2.5 mg/kg 1 4.7 mg/kg
15 mg/kg
52
(mg/kg)
(ppm)
9 0.02 8 3 9
50 0.01 50 0.01 50
9 0.07 9 0.1 9
54 0.02 42 2.5 53
2 0.05 2 5 2
5 0.01 5 0.1 5
34 0.01 34 5 34
62 0.03 29 25 62
87
13-01-276_本文_MK.indd 8713-01-276_本文_MK.indd 87 2013/01/24 21:17:002013/01/24 21:17:00
(mg/kg)
(ppm)
DDVP
143 0.01 143 0.1 143
1 0.01 1 0.5 1
8 0.01 3 15 8
158 0.05 111 2.0 158
1 0.1 0 1 1
3 0.02 3 8 3
165 0.02 163 0.1 165
4 0.02 4 10 4
1 0.02 1 0.5 1
24 0.03 17 5 24
2 0.02 2 2.0 2
MEP
4 0.01 3 0.2 4
PAP 20 0.02 19 0.1 20
8 0.02 7 0.5 8
95 0.02 31 10 95
25 0.02 21 2.0 25
5 0.03 5 2.0 5
87 0.02 80 5 87
50 0.02 49 2 50
7 0.02 7 1.0 7
33 0.05 33 0.3 33
3.1.3.17.
88
13-01-276_本文_MK.indd 8813-01-276_本文_MK.indd 88 2013/01/24 21:17:002013/01/24 21:17:00
3.1.3.17.
1922 22 393 1,273
53 19
1 1.0 mg/kg21
1 0.6 mg/kg
22 10
221 54 mg/kg
53
(mg/kg)
(ppm)
114 0.02 65 5 114
126 0.01 59 5 126
6 0.02 5 1 6
240 0.02 57 30 239
74 0.01 19 15 74
192 0.05 119 6.0 192
127 0.1 120 1 127
43 0.02 35 5 43
11 0.02 11 0.1 11
14 0.02 8 2 14
55 0.03 35 0.5 53
89
3.1.3.18.3.1.3.18.
13-01-276_本文_MK.indd 8913-01-276_本文_MK.indd 89 2013/01/24 21:17:002013/01/24 21:17:00
(mg/kg)
(ppm)
55 0.02 52 0.1 55
23 0.05 21 5.0 23
31 0.05 30 0.5 31
MEP
1 0.01 1 0.2 1
1 0.02 1 0.02 1
19 0.01 19 0.05 19
53 0.03 22 10 53
20 0.02 20 0.1 20
8 0.01 8 0.05 8
DMTP
46 0.02 46 0.1 46
14 0.02 12 0.2 14
3.1.3.18.
90
13-01-276_本文_MK.indd 9013-01-276_本文_MK.indd 90 2013/01/24 21:17:002013/01/24 21:17:00
3.1.3.18.
1518 300 21
22 600 54
1
7
54
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
100 0.04 99 < 0.04 0.05 0.01 -
100 0.01 99 < 0.01 0.02 0.005 -
100 0.001 100 - - 0.0005 -
600 0.01 427 < 0.01 0.05 0.01 -
1517 19 22 9 55
55 pg-TEQ/g
9 0.00004 0.027 0.0057
91
3.1.3.19.3.1.3.19.
13-01-276_本文_MK.indd 9113-01-276_本文_MK.indd 91 2013/01/24 21:17:002013/01/24 21:17:00
3.1.3.19.
1518 300
21 22 600 56
6
56
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
100 0.04 100 - - 0.01 -
100 0.01 100 - - 0.005 -
100 0.001 100 - - 0.0004 -
600 0.01 249 < 0.01 0.12 0.01 0.01
3.1.3.20.
92
3.1.3.20.3.1.3.20.
13-01-276_本文_MK.indd 9213-01-276_本文_MK.indd 92 2013/01/24 21:17:002013/01/24 21:17:00
3.1.3.19.
3.1.3.20.
1517 19 8 57
57 pg-TEQ/g
8 0.0030 0.069 0.023
93
3.1.3.21.3.1.3.21.
13-01-276_本文_MK.indd 9313-01-276_本文_MK.indd 93 2013/01/24 21:17:002013/01/24 21:17:00
3.1.3.21.
2122 240 58
8
58
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
240 0.01 50 < 0.01 0.18 0.02 0.02
3.1.3.22.
94
3.1.3.22.3.1.3.22.
13-01-276_本文_MK.indd 9413-01-276_本文_MK.indd 94 2013/01/24 21:17:012013/01/24 21:17:01
3.1.3.21.
3.1.3.22.
21120 59
59
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
120 0.01 0 0.02 0.43 0.12 0.11
95
3.1.3.23.3.1.3.23.
13-01-276_本文_MK.indd 9513-01-276_本文_MK.indd 95 2013/01/24 21:17:012013/01/24 21:17:01
3.1.3.23.
2122 240 60
60
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
240 0.01 154 < 0.01 0.05 0.01 -
3.1.3.24.
96
3.1.3.24.3.1.3.24.
13-01-276_本文_MK.indd 9613-01-276_本文_MK.indd 96 2013/01/24 21:17:012013/01/24 21:17:01
3.1.3.23.
3.1.3.24.
1518 302
21 22 240 61
3 9
61
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
100 0.04 100 - - 0.01 -
101 0.01 98 < 0.01 0.02 0.006 -
101 0.001 101 - - 0.0005 -
240 0.01 231 < 0.01 0.01 0.01 -
1517 19 8 62
62 pg-TEQ/g
8 0.00070 0.075 0.015
97
3.1.3.25.3.1.3.25.
13-01-276_本文_MK.indd 9713-01-276_本文_MK.indd 97 2013/01/24 21:17:012013/01/24 21:17:01
1722 114 566 4,757
63
63
(mg/kg)
(ppm)
BHC 20 0.02 20 0.2 20
DDT 20 0.01 20 0.2 20
EPN 20 0.03 20 0.1 20
17 0.01 17 0.5 17
107 0.02 92 2 107
30 0.01 30 5.0 30
144 0.01 119 1 144
20 0.02 20 0.02 20
23 0.07 23 0.1 23
40 0.05 33 5.0 40
114 0.02 104 1 114
20 0.01 20 0.3 20
12 0.03 12 0.3 12
90 0.02 90 2 90
20 0.01 20 0.02 20
20 0.01 20 0.1 20
22 0.03 21 0.5 22
26 0.01 23 5 26
6 0.01 6 2.0 6
29 0.01 29 0.05 29
NAC 20 0.02 20 3 20
20 0.01 20 0.05 20
60 0.01 54 5.0 60
98
13-01-276_本文_MK.indd 9813-01-276_本文_MK.indd 98 2013/01/24 21:17:012013/01/24 21:17:01
(mg/kg)
(ppm)
77 0.02 73 0.5 77
53 0.005 40 2 53
20 0.01 20 0.05 20
20 0.01 20 0.03 20
188 0.02 121 1 188
CVP
20 0.02 20 0.2 20
21 0.02 21 2.0 21
IPC
20 0.03 20 0.05 20
20 0.02 20 0.02 20
TPN
230 0.01 169 5 230
102 0.03 93 0.7 102
CYP
20 0.01 20 0.05 20
223 0.05 223 5.0 223
DDVP
22 0.01 22 0.2 22
20 0.02 20 2.0 20
2 0.01 2 0.5 2
104 0.01 52 2 104
21 0.05 21 0.5 21
23 0.02 23 1 23
20 0.05 20 2.0 20
77 0.05 77 0.5 77
20 0.03 20 1.0 20
79 0.05 78 0.5 79
20 0.1 20 1 20
1 0.01 1 0.7 1
131 0.02 130 2 131
99
13-01-276_本文_MK.indd 9913-01-276_本文_MK.indd 99 2013/01/24 21:17:012013/01/24 21:17:01
(mg/kg)
(ppm)
57 0.02 55 0.5 57
31 0.02 31 0.1 31
3 0.03 2 1 3
72 0.02 64 0.5 72
20 0.04 20 0.2 20
20 0.005 20 0.02 20
7 0.02 5 0.5 7
49 0.01 49 0.5 49
20 0.02 20 0.2 20
20 0.01 20 0.005 20
1 0.01 1 0.5 1
42 0.03 41 0.5 42
46 0.02 44 0.1 46
DEP
6 0.01 4 1.0 6
293 0.05 284 1.0 293
20 0.01 20 1.0 20
30 0.02 30 2.0 30
24 0.01 23 1 24
20 0.01 20 0.3 20
20 0.02 20 0.2 20
25 0.01 25 0.5 25
22 0.01 22 0.5 22
1 0.05 1 0.1 1
48 0.03 44 1.0 48
9 0.02 9 0.5 9
2 0.02 2 0.2 2
20 0.01 20 2.0 20
20 0.01 20 2.0 20
20 0.03 20 1 20
31 0.1 31 0.5 31
100
13-01-276_本文_MK.indd 10013-01-276_本文_MK.indd 100 2013/01/24 21:17:012013/01/24 21:17:01
(mg/kg)
(ppm)
MEP
55 0.01 54 0.2 55
20 0.05 20 0.1 20
BPMC
27 0.01 27 1.5 27
MPP
20 0.01 20 3 20
PAP
20 0.01 20 0.1 20
20 0.03 20 0.20 20
35 0.02 35 0.5 35
25 0.02 25 2 25
20 0.01 20 1 20
38 0.05 36 1 38
27 0.03 21 2 27
20 0.03 20 1.0 20
20 0.025 20 0.05 20
23 0.01 23 1.0 23
137 0.02 133 2 137
1 0.01 0 0.7 1
194 0.03 53 5 194
DCPA 20 0.02 20 0.1 20
20 0.02 20 0.05 20
PHC
20 0.02 20 2 20
20 0.02 20 0.02 20
24 0.02 24 1 24
20 0.02 20 0.03 20
36 0.02 36 0.5 36
21 0.03 21 0.5 21
16 0.02 10 5 16
142 0.02 136 0.2 142
101
13-01-276_本文_MK.indd 10113-01-276_本文_MK.indd 101 2013/01/24 21:17:022013/01/24 21:17:02
(mg/kg)
(ppm)
20 0.02 20 0.3 20
46 0.03 46 0.5 46
1 0.02 1 1.0 1
20 0.03 20 0.2 20
28 0.01 28 1.0 28
107 0.02 76 1 107
DMTP
20 0.01 20 0.05 20
21 0.02 21 1.0 21
3.1.3.25.
102
13-01-276_本文_MK.indd 10213-01-276_本文_MK.indd 102 2013/01/24 21:17:022013/01/24 21:17:02
3.1.3.25.
1618 300 64
1
64
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
100 0.02 99 < 0.02 0.02 0.01 -
100 0.01 100 - - 0.003 -
100 0.001 100 - - 0.0006 -
1517 19 4 65
65 pg-TEQ/g
4 0.00031 0.0018 0.00098
103
3.1.3.26.3.1.3.26.
13-01-276_本文_MK.indd 10313-01-276_本文_MK.indd 103 2013/01/24 21:17:022013/01/24 21:17:02
1778 3 234
66
66
(mg/kg)
(ppm)
BHC 3 0.02 3 1 3
DDT 3 0.01 3 0.5 3
3 0.01 3 1 3
3 0.01 3 1 3
3 0.02 3 0.02 3
3 0.07 3 0.1 3
3 0.03 3 5.0 3
3 0.01 3 0.3 3
3 0.02 3 2 3
3 0.01 3 0.2 3
3 0.01 3 0.005 3
3 0.03 3 0.5 3
3 0.005 3 0.05 3
3 0.01 3 5 3
NAC 3 0.02 3 3 3
3 0.01 3 0.05 3
3 0.01 3 0.5 3
3 0.01 3 0.05 3
3 0.01 3 0.03 3
3 0.01 3 0.5 3
3 0.02 3 2.0 3
3 0.02 3 5.0 3
104
13-01-276_本文_MK.indd 10413-01-276_本文_MK.indd 104 2013/01/24 21:17:022013/01/24 21:17:02
(mg/kg)
(ppm)
3 0.02 3 1 3
3 0.02 3 0.5 3
3 0.02 3 0.3 3
3 0.05 3 2.0 3
3 0.03 3 1 3
3 0.05 3 5.0 3
3 0.1 3 1 3
3 0.02 3 0.5 3
3 0.01 3 0.1 3
3 0.04 3 0.5 3
3 0.005 3 0.1 3
3 0.01 3 0.5 3
3 0.02 3 0.2 3
3 0.01 3 0.005 3
3 0.03 3 2 3
3 0.02 3 0.1 3
3 0.04 3 1.0 3
3 0.01 3 0.05 3
3 0.02 3 2.0 3
3 0.01 3 0.3 3
3 0.02 3 1.0 3
3 0.01 3 0.5 3
3 0.01 3 0.4 3
3 0.01 3 1.0 3
3 0.01 3 0.50 3
3 0.01 3 1.0 3
3 0.03 3 1 3
3 0.02 3 0.5 3
MEP
3 0.01 3 0.2 3
3 0.05 3 0.1 3
105
13-01-276_本文_MK.indd 10513-01-276_本文_MK.indd 105 2013/01/24 21:17:022013/01/24 21:17:02
(mg/kg)
(ppm)
BPMC
3 0.01 3 0.3 3
MPP 3 0.01 3 3 3
PAP
3 0.01 3 0.1 3
3 0.03 3 0.50 3
3 0.02 3 0.02 3
3 0.02 3 2 3
3 0.01 3 0.05 3
3 0.01 3 0.5 3
3 0.03 3 0.05 3
3 0.01 3 0.1 3
3 0.02 3 0.2 3
3 0.01 3 2 3
DCPA 3 0.02 3 0.1 3
3 0.02 3 0.05 3
PHC
3 0.02 3 2 3
3 0.02 3 0.02 3
3 0.02 3 1 3
3 0.02 3 0.03 3
3 0.02 3 0.5 3
3 0.02 3 0.5 3
3 0.02 3 0.3 3
3 0.01 3 8.0 3
3 0.03 3 0.5 3
3 0.01 3 0.1 3
3 0.01 3 2 3
DMTP
3 0.01 3 0.1 3
3.1.3.26.
106
13-01-276_本文_MK.indd 10613-01-276_本文_MK.indd 106 2013/01/24 21:17:022013/01/24 21:17:02
3.1.3.26.
1517 3 67
67 pg-TEQ/g
3 0.0048 0.010 0.0073
1780 1 80
68
68
(mg/kg)
(ppm)
DDT 1 0.01 1 0.5 1
1 0.01 1 0.5 1
1 0.01 1 1 1
1 0.02 1 0.02 1
1 0.07 1 0.1 1
1 0.03 1 5.0 1
1 0.01 1 2 1
107
3.1.3.27.3.1.3.27.
13-01-276_本文_MK.indd 10713-01-276_本文_MK.indd 107 2013/01/24 21:17:022013/01/24 21:17:02
(mg/kg)
(ppm)
1 0.02 1 2 1
1 0.01 1 0.005 1
1 0.01 1 0.2 1
1 0.03 1 0.5 1
1 0.005 1 0.05 1
1 0.01 1 5 1
NAC 1 0.02 1 10 1
1 0.01 1 0.05 1
1 0.01 1 3 1
1 0.01 1 0.01 1
1 0.01 1 0.03 1
1 0.01 1 1 1
1 0.02 1 2.0 1
1 0.02 1 0.02 1
1 0.01 1 0.05 1
1 0.02 1 5.0 1
1 0.02 1 3 1
1 0.02 1 0.5 1
1 0.05 1 2.0 1
1 0.03 1 1 1
1 0.05 1 0.05 1
1 0.1 1 1 1
1 0.02 1 0.5 1
MCC 1 0.01 1 0.5 1
1 0.01 1 0.1 1
1 0.04 1 0.5 1
1 0.005 1 0.1 1
1 0.02 1 10 1
1 0.01 1 0.5 1
1 0.02 1 0.2 1
1 0.01 1 0.005 1
108
13-01-276_本文_MK.indd 10813-01-276_本文_MK.indd 108 2013/01/24 21:17:022013/01/24 21:17:02
(mg/kg)
(ppm)
1 0.03 1 2 1
1 0.02 1 1 1
1 0.04 1 1.0 1
1 0.01 1 0.05 1
1 0.02 1 2.0 1
1 0.01 1 0.05 1
1 0.02 1 1.0 1
1 0.01 1 0.5 1
1 0.01 1 0.4 1
1 0.01 1 2.0 1
1 0.01 1 2 1
1 0.01 1 1.0 1
1 0.03 1 1 1
1 0.02 1 0.5 1
MEP
1 0.01 1 0.2 1
1 0.05 1 0.1 1
BPMC
1 0.01 1 0.3 1
MPP 1 0.01 1 3 1
PAP 1 0.01 1 0.1 1
1 0.03 1 0.50 1
1 0.02 1 0.5 1
1 0.02 1 2 1
1 0.01 1 0.05 1
1 0.01 1 0.5 1
1 0.03 1 0.50 1
1 0.02 1 0.5 1
1 0.01 1 1 1
DCPA 1 0.02 1 0.1 1
1 0.02 1 0.05 1
PHC 1 0.02 1 2 1
109
13-01-276_本文_MK.indd 10913-01-276_本文_MK.indd 109 2013/01/24 21:17:032013/01/24 21:17:03
(mg/kg)
(ppm)
1 0.02 1 0.02 1
1 0.02 1 1 1
1 0.02 1 0.03 1
1 0.02 1 3.0 1
1 0.05 1 0.05 1
1 0.02 1 0.5 1
1 0.02 1 0.3 1
1 0.01 1 2.0 1
1 0.03 1 0.5 1
1 0.01 1 0.5 1
1 0.01 1 2 1
DMTP
1 0.01 1 0.1 1
3.1.3.27.
110
13-01-276_本文_MK.indd 11013-01-276_本文_MK.indd 110 2013/01/24 21:17:032013/01/24 21:17:03
3.1.3.27.
1518 300 21
22 240 69 3
7
69
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
100 0.04 100 - - 0.01 -
100 0.01 97 < 0.01 0.01 0.006 -
100 0.001 100 - - 0.0004 -
240 0.01 167 < 0.01 0.08 0.01 -
111
3.1.3.28.3.1.3.28.
13-01-276_本文_MK.indd 11113-01-276_本文_MK.indd 111 2013/01/24 21:17:032013/01/24 21:17:03
3.1.3.28.
1518 300
21 22 240 70
6
70
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
100 0.04 100 - - 0.01 -
100 0.01 100 - - 0.004 -
100 0.001 100 - - 0.0004 -
240 0.01 141 < 0.01 0.03 0.01 -
1722 112 549 2,620
71
71
(mg/kg)
(ppm)
BHC 1 0.02 1 0.2 1
112
3.1.3.29.3.1.3.29.
13-01-276_本文_MK.indd 11213-01-276_本文_MK.indd 112 2013/01/24 21:17:032013/01/24 21:17:03
3.1.3.28.
(mg/kg)
(ppm)
DDT 1 0.01 1 0.2 1
EPN 1 0.03 1 0.1 1
4 0.01 4 0.5 4
119 0.02 104 2 119
57 0.01 48 5.0 57
99 0.01 64 3 99
1 0.02 1 0.02 1
1 0.07 1 0.1 1
64 0.05 35 5.0 64
47 0.02 43 2 47
1 0.01 1 0.3 1
33 0.02 27 2 33
1 0.01 1 0.02 1
1 0.01 1 0.2 1
1 0.03 1 0.5 1
9 0.05 9 5 9
2 0.01 2 2.0 2
3 0.01 3 0.01 3
NAC 1 0.02 1 5 1
1 0.01 1 0.05 1
15 0.01 13 5.0 15
1 0.01 1 3 1
25 0.005 14 3 25
1 0.01 1 0.5 1
1 0.01 1 0.5 1
58 0.02 50 1.0 58
CVP 1 0.02 1 0.1 1
4 0.05 4 2.0 4
IPC
1 0.03 1 0.05 1
1 0.02 1 0.02 1
113
13-01-276_本文_MK.indd 11313-01-276_本文_MK.indd 113 2013/01/24 21:17:032013/01/24 21:17:03
(mg/kg)
(ppm)
TPN 187 0.01 137 5 187
55 0.03 47 2 55
187 0.05 181 5.0 187
DDVP 11 0.01 11 0.1 11
1 0.02 1 1 1
4 0.01 4 0.5 4
144 0.01 93 2 144
5 0.05 5 0.5 5
8 0.02 5 0.5 8
1 0.05 1 2.0 1
3 0.05 3 0.5 3
1 0.03 1 1.0 1
29 0.05 27 2.0 29
2 0.1 2 1.0 2
83 0.02 81 2 83
55 0.02 55 0.5 55
7 0.02 7 0.1 7
55 0.03 46 1 55
18 0.02 17 2 18
1 0.04 1 0.5 1
1 0.005 1 0.02 1
11 0.02 7 1 11
1 0.02 1 1 1
1 0.01 1 0.5 1
46 0.03 45 0.5 46
1 0.01 1 0.005 1
1 0.03 1 0.5 1
1 0.02 1 0.3 1
154 0.05 150 2.0 154
114
13-01-276_本文_MK.indd 11413-01-276_本文_MK.indd 114 2013/01/24 21:17:032013/01/24 21:17:03
(mg/kg)
(ppm)
1 0.01 1 0.1 1
2 0.02 2 2.0 2
37 0.01 26 2 37
1 0.01 1 0.3 1
1 0.02 1 0.2 1
1 0.01 1 3 1
2 0.01 2 0.5 2
164 0.03 144 1.0 164
45 0.02 29 5 45
22 0.02 22 1 22
1 0.01 1 1.0 1
1 0.01 1 2.0 1
1 0.03 1 1 1
18 0.1 18 0.5 18
MEP 6 0.01 6 0.2 6
1 0.05 1 0.1 1
BPMC 1 0.01 1 1.0 1
1 0.02 1 0.1 1
MPP 1 0.01 1 5 1
PAP 1 0.01 1 0.1 1
1 0.03 1 1.0 1
42 0.02 30 0.5 42
8 0.02 8 2 8
3 0.01 3 0.05 3
91 0.05 80 1 91
69 0.03 59 2 69
1 0.03 1 0.20 1
1 0.025 1 0.05 1
14 0.01 13 0.5 14
115
13-01-276_本文_MK.indd 11513-01-276_本文_MK.indd 115 2013/01/24 21:17:032013/01/24 21:17:03
(mg/kg)
(ppm)
101 0.02 87 0.5 101
24 0.01 18 0.7 24
34 0.03 19 5 34
DCPA 1 0.02 1 0.1 1
1 0.02 1 0.05 1
PHC 1 0.02 1 2 1
1 0.02 1 0.02 1
1 0.02 1 0.1 1
1 0.02 1 0.02 1
12 0.02 9 1.0 12
1 0.05 1 0.05 1
1 0.02 1 0.5 1
59 0.02 18 5 59
41 0.02 41 0.2 41
1 0.02 1 0.3 1
3 0.03 3 0.5 3
1 0.02 1 1.0 1
1 0.03 1 0.5 1
39 0.01 31 2.0 39
73 0.02 68 2 73
DMTP 1 0.01 1 0.1 1
1 0.02 1 1.0 1
53 0.05 52 0.5 53
3.1.3.29.
116
13-01-276_本文_MK.indd 11613-01-276_本文_MK.indd 116 2013/01/24 21:17:032013/01/24 21:17:03
3.1.3.29.
1518 300 72
72
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
100 0.04 100 - - 0.01 -
100 0.01 100 - - 0.004 -
100 0.001 100 - - 0.0004 -
1719 22 102 443 2,535
73
73
(mg/kg)
(ppm)
BHC 8 0.02 8 0.2 8
DDT 8 0.01 8 0.2 8
EPN 9 0.03 8 0.1 9
27 0.01 22 1 27
91 0.02 67 1 91
30 0.01 29 5.0 30
117
3.1.3.30.3.1.3.30.
13-01-276_本文_MK.indd 11713-01-276_本文_MK.indd 117 2013/01/24 21:17:032013/01/24 21:17:03
(mg/kg)
(ppm)
42 0.01 29 3 42
8 0.07 8 0.1 8
109 0.05 85 10 109
116 0.02 103 3 116
8 0.01 8 0.3 8
33 0.02 29 5 33
8 0.01 8 0.02 8
8 0.01 8 0.2 8
8 0.03 8 0.5 8
8 0.01 8 5 8
9 0.01 9 0.01 9
NAC 8 0.02 8 5 8
8 0.01 8 0.05 8
7 0.01 7 5 7
55 0.02 40 2 55
12 0.005 2 3 12
8 0.01 8 0.5 8
8 0.01 8 0.5 8
178 0.02 121 1 178
CVP 8 0.02 8 0.1 8
28 0.05 26 2.0 28
IPC
8 0.03 8 0.05 8
8 0.02 8 0.02 8
TPN
128 0.01 96 7 128
38 0.03 35 1 38
8 0.02 8 5.0 8
DDVP
43 0.01 43 0.1 43
118
13-01-276_本文_MK.indd 11813-01-276_本文_MK.indd 118 2013/01/24 21:17:042013/01/24 21:17:04
(mg/kg)
(ppm)
8 0.02 8 1 8
75 0.01 37 3 75
8 0.02 8 1.0 8
8 0.05 8 5.0 8
27 0.05 27 1 27
8 0.03 8 1 8
54 0.05 50 2.0 54
10 0.1 10 1 10
8 0.02 8 0.2 8
60 0.02 56 2 60
52 0.02 52 0.1 52
9 0.03 7 5 9
51 0.02 46 1 51
8 0.04 8 0.7 8
8 0.005 8 0.02 8
8 0.02 8 1 8
8 0.01 8 0.5 8
8 0.02 8 0.5 8
8 0.01 8 0.005 8
23 0.03 16 1 23
23 0.02 23 0.3 23
81 0.05 79 5.0 81
8 0.01 8 0.1 8
10 0.02 10 2.0 10
4 0.01 1 3 4
8 0.01 8 0.3 8
8 0.02 8 1.0 8
8 0.01 8 0.05 8
8 0.01 8 0.5 8
48 0.03 40 3.0 48
58 0.02 41 2 58
119
13-01-276_本文_MK.indd 11913-01-276_本文_MK.indd 119 2013/01/24 21:17:042013/01/24 21:17:04
(mg/kg)
(ppm)
1 0.02 1 5 1
8 0.01 8 1.0 8
8 0.01 8 1.0 8
8 0.03 8 1 8
21 0.1 20 0.5 21
MEP
8 0.01 8 0.2 8
8 0.05 8 0.1 8
BPMC
25 0.01 24 2.0 25
MPP
8 0.01 8 5 8
PAP
8 0.01 8 0.1 8
8 0.03 8 0.50 8
27 0.02 26 0.5 27
22 0.02 21 2 22
8 0.01 8 0.05 8
8 0.03 8 0.05 8
10 0.025 9 0.7 10
8 0.01 8 0.5 8
73 0.02 49 1 73
65 0.03 28 5 65
DCPA 8 0.02 8 0.1 8
8 0.02 8 0.1 8
PHC 8 0.02 8 2 8
8 0.02 8 0.02 8
18 0.02 18 2 18
8 0.02 8 0.03 8
60 0.02 54 3.0 60
8 0.02 8 0.02 8
120
13-01-276_本文_MK.indd 12013-01-276_本文_MK.indd 120 2013/01/24 21:17:042013/01/24 21:17:04
(mg/kg)
(ppm)
3 0.02 2 10 3
14 0.02 12 0.1 14
8 0.02 8 0.02 8
46 0.03 46 0.5 46
38 0.02 28 1.0 38
20 0.03 19 0.7 20
30 0.01 28 2.0 30
77 0.02 71 2 77
DMTP
17 0.02 17 0.1 17
3 0.02 2 3 3
25 0.05 22 1 25
121
13-01-276_本文_MK.indd 12113-01-276_本文_MK.indd 121 2013/01/24 21:17:042013/01/24 21:17:04
3.1.3.30.
2122 239 74
9
74
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
239 0.01 19 < 0.01 0.11 0.03 0.03
3.1.3.31.
122
3.1.3.31.3.1.3.31.
13-01-276_本文_MK.indd 12213-01-276_本文_MK.indd 122 2013/01/24 21:17:042013/01/24 21:17:04
3.1.3.30.
3.1.3.31.
16 18 301 75
75
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
101 0.03 101 - - 0.02 -
100 0.01 100 - - 0.003 -
100 0.001 100 - - 0.0005 -
20 22 35 284 744 76
211 0.02 mg/kg
76
(mg/kg)
(ppm)
80 0.02 61 3 80
35 0.01 23 3 35
4 0.03 4 0.1 4
123
3.1.3.32.3.1.3.32.
13-01-276_本文_MK.indd 12313-01-276_本文_MK.indd 123 2013/01/24 21:17:042013/01/24 21:17:04
(mg/kg)
(ppm)
2 0.05 2 5.0 2
84 0.02 83 2.8 84
54 0.02 45 5 54
1 0.01 1 5 1
1 0.01 0 0.01 0
1 0.05 1 2.0 1
TPN 1 0.01 1 5 1
CYAP 1 0.02 1 0.05 1
ECP
8 0.01 8 0.03 8
DDVP
9 0.01 9 0.2 9
28 0.01 27 0.2 28
14 0.05 14 0.5 14
3 0.1 3 1 3
5 0.02 5 0.2 5
24 0.02 24 0.3 24
2 0.02 2 0.2 2
3 0.03 3 1 3
28 0.03 22 1 28
28 0.02 28 0.2 28
5 0.02 5 0.2 5
MEP
1 0.01 1 0.5 1
PAP 26 0.02 26 0.1 26
44 0.02 37 2.0 44
140 0.03 91 5 140
36 0.02 27 1 36
1 0.03 0 1 1
8 0.01 5 2 8
124
13-01-276_本文_MK.indd 12413-01-276_本文_MK.indd 124 2013/01/24 21:17:042013/01/24 21:17:04
(mg/kg)
(ppm)
10 0.02 10 3.0 10
44 0.03 44 2.0 44
2 0.02 2 2 2
5 0.02 5 0.3 5
6 0.02 6 0.01 6
125
13-01-276_本文_MK.indd 12513-01-276_本文_MK.indd 125 2013/01/24 21:17:042013/01/24 21:17:04
3.1.3.32.
1719 22 86 266 1,935
77
77
(mg/kg)
(ppm)
BHC 18 0.02 18 1 18
DDT 18 0.01 18 0.5 18
11 0.02 9 3 11
33 0.01 32 0.5 33
18 0.01 18 3.0 18
18 0.02 18 0.02 18
25 0.07 25 0.1 25
23 0.05 23 5.0 23
7 0.02 7 2.5 7
18 0.01 18 0.3 18
128 0.02 65 5 128
18 0.01 18 0.005 18
18 0.01 18 0.01 18
18 0.03 18 0.5 18
19 0.05 18 5 19
NAC 18 0.02 18 4 18
18 0.01 18 0.05 18
18 0.01 18 0.05 18
8 0.005 7 2 8
18 0.01 18 0.3 18
18 0.01 18 0.03 18
126
3.1.3.33.3.1.3.33.
13-01-276_本文_MK.indd 12613-01-276_本文_MK.indd 126 2013/01/24 21:17:052013/01/24 21:17:05
3.1.3.32.
(mg/kg)
(ppm)
CVP 18 0.02 18 0.2 18
20 0.05 20 2.0 20
IPC
18 0.03 18 0.05 18
18 0.02 18 0.02 18
6 0.03 4 5 6
51 0.05 51 5.0 51
ECP
5 0.01 5 0.03 5
18 0.02 18 3 18
19 0.01 12 2 19
18 0.02 18 1.0 18
19 0.05 19 2 19
18 0.03 18 0.05 18
133 0.05 91 5.0 133
18 0.1 18 1 18
2 0.01 2 10 2
18 0.02 18 0.05 18
6 0.05 1 2 6
37 0.02 37 0.1 37
39 0.02 39 0.3 39
18 0.04 18 0.5 18
24 0.05 24 0.03 24
18 0.005 18 0.1 18
20 0.03 19 1 20
18 0.01 18 0.005 18
18 0.03 18 0.1 18
18 0.02 18 0.1 18
18 0.04 18 1.0 18
127
13-01-276_本文_MK.indd 12713-01-276_本文_MK.indd 127 2013/01/24 21:17:052013/01/24 21:17:05
(mg/kg)
(ppm)
27 0.01 27 0.05 27
18 0.02 18 2.0 18
18 0.01 18 0.08 18
18 0.02 18 1.0 18
18 0.01 18 0.05 18
18 0.01 18 0.5 18
20 0.03 19 2.0 20
1 0.02 0 5 1
18 0.01 18 0.50 18
18 0.01 18 1.0 18
18 0.03 18 1 18
18 0.02 18 0.5 18
MEP
72 0.01 67 0.5 72
18 0.05 18 0.1 18
BPMC
18 0.01 18 0.3 18
PAP 18 0.01 18 0.1 18
18 0.03 17 1 18
46 0.02 33 2.0 46
3 0.03 1 5 3
23 0.03 23 2.0 23
19 0.025 19 2.0 19
19 0.02 18 5 19
18 0.01 18 1 18
DCPA 18 0.02 18 0.1 18
18 0.02 18 1 18
PHC 18 0.02 18 2 18
18 0.02 18 0.02 18
18 0.02 18 2 18
18 0.02 18 0.02 18
128
13-01-276_本文_MK.indd 12813-01-276_本文_MK.indd 128 2013/01/24 21:17:052013/01/24 21:17:05
(mg/kg)
(ppm)
37 0.02 28 3.0 37
19 0.05 19 0.2 19
18 0.02 18 0.5 18
18 0.02 18 0.2 18
49 0.03 49 2.0 49
33 0.01 32 0.5 33
DMTP
18 0.01 18 0.1 18
31 0.02 31 0.3 31
1 0.02 1 0.2 1
129
13-01-276_本文_MK.indd 12913-01-276_本文_MK.indd 129 2013/01/24 21:17:052013/01/24 21:17:05
3.1.3.33.
1518 300 78
1
78
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
100 0.05 100 - - 0.02 -
100 0.01 99 < 0.01 0.01 0.005 -
100 0.001 100 - - 0.0004 -
1822 57 506 3,858
79
79
(mg/kg)
(ppm)
36 0.01 29 2 36
165 0.02 98 3 165
277 0.01 213 10 277
7 0.07 7 0.2 7
18 0.05 9 20 18
130
3.1.3.34.3.1.3.34.
13-01-276_本文_MK.indd 13013-01-276_本文_MK.indd 130 2013/01/24 21:17:052013/01/24 21:17:05
3.1.3.33.
(mg/kg)
(ppm)
14 0.02 14 0.5 14
88 0.03 80 0.5 88
1 0.03 1 0.5 1
2 0.01 2 0.1 2
40 0.01 37 20 40
152 0.02 93 5 152
271 0.02 271 5 271
97 0.05 94 2.0 97
9 0.03 9 0.7 9
195 0.05 195 5.0 195
DDVP
1 0.01 1 0.3 1
17 0.02 10 5 17
100 0.05 95 5 100
15 0.05 15 2.0 15
21 0.02 19 1 21
33 0.02 33 0.1 33
52 0.03 36 5 52
2 0.02 2 5 2
36 0.01 36 1 36
9 0.03 7 2 9
39 0.03 37 1 39
14 0.02 14 1 14
114 0.01 87 1 114
1 0.02 1 0.1 1
117 0.03 116 1 117
DEP 28 0.01 27 1.0 28
282 0.05 257 2.0 282
256 0.02 230 1.0 256
60 0.03 59 2.0 60
125 0.02 113 5 125
15 0.02 15 0.3 15
131
13-01-276_本文_MK.indd 13113-01-276_本文_MK.indd 131 2013/01/24 21:17:052013/01/24 21:17:05
(mg/kg)
(ppm)
70 0.1 68 1.0 70
MEP
4 0.01 4 0.2 4
BPMC
8 0.01 7 2.0 8
41 0.02 38 0.5 41
47 0.02 47 5 47
68 0.03 56 5 68
16 0.01 10 1.0 16
137 0.02 133 0.5 137
81 0.01 73 2 81
58 0.03 17 10 58
5 0.02 5 0.3 5
84 0.02 72 2 84
11 0.02 11 1.0 11
8 0.02 2 15 8
18 0.02 17 0.05 18
58 0.03 58 0.5 58
133 0.02 96 1.0 133
174 0.02 174 1 174
46 0.02 46 7 46
4 0.02 4 2 4
78 0.05 73 1 78
3.1.4.1.
132
13-01-276_本文_MK.indd 13213-01-276_本文_MK.indd 132 2013/01/24 21:17:052013/01/24 21:17:05
3.1.4.
3.1.4.1.
1518 120 181
80 81
80
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
40 0.02 40 - - 0.01 -
40 0.01 40 - - 0.004 -
40 0.001 40 - - 0.0003 -
81
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
61 0.04 61 - - 0.01 -
60 0.01 60 - - 0.003 -
60 0.001 60 - - 0.0003 -
1719 92 278 5,903
82
133
13-01-276_本文_MK.indd 13313-01-276_本文_MK.indd 133 2013/01/24 21:17:052013/01/24 21:17:05
82
(mg/kg)
(ppm)
BHC 60 0.02 60 0.2 60
DDT 60 0.01 60 0.2 60
XMC 68 0.01 68 0.2 68
147 0.01 139 5.0 147
60 0.01 60 1.0 60
60 0.02 60 0.02 60
1 0.01 1 2 1
60 0.07 60 0.2 60
64 0.05 64 10 64
60 0.01 60 5 60
9 0.03 9 1 9
60 0.02 60 2 60
60 0.01 60 0.005 60
60 0.01 60 0.2 60
60 0.03 60 0.5 60
60 0.01 60 1 60
60 0.01 60 0.01 60
NAC 73 0.05 73 1.0 73
60 0.01 60 0.02 60
172 0.02 172 2 172
68 0.01 68 1 68
60 0.01 60 1 60
132 0.01 132 0.5 132
CVP 60 0.02 60 0.1 60
60 0.02 60 2.0 60
IPC 60 0.03 60 0.05 60
134
13-01-276_本文_MK.indd 13413-01-276_本文_MK.indd 134 2013/01/24 21:17:062013/01/24 21:17:06
(mg/kg)
(ppm)
60 0.02 60 5.0 60
1 0.03 1 0.7 1
61 0.02 61 5.0 61
DDVP
9 0.01 9 0.1 9
60 0.02 60 3.0 60
60 0.02 60 0.5 60
60 0.05 60 0.5 60
76 0.03 76 1.0 76
32 0.02 32 0.1 32
60 0.05 60 2.0 60
74 0.1 74 1.0 74
60 0.02 60 0.05 60
60 0.01 60 0.1 60
19 0.02 19 0.5 19
64 0.04 64 1 64
60 0.02 60 2 60
60 0.01 60 0.1 60
60 0.02 60 0.1 60
60 0.01 60 0.005 60
60 0.03 60 0.1 60
60 0.02 60 0.1 60
60 0.04 60 2.0 60
60 0.01 60 0.05 60
60 0.02 60 0.1 60
60 0.01 60 0.5 60
60 0.01 60 0.3 60
60 0.02 60 0.2 60
60 0.02 60 0.05 60
60 0.01 60 0.05 60
82 0.01 82 0.1 82
135
13-01-276_本文_MK.indd 13513-01-276_本文_MK.indd 135 2013/01/24 21:17:062013/01/24 21:17:06
(mg/kg)
(ppm)
86 0.03 86 0.2 86
60 0.01 60 0.05 60
60 0.01 60 0.10 60
60 0.03 60 1 60
60 0.02 60 1.0 60
MEP 72 0.01 72 0.2 72
60 0.05 60 0.1 60
2 0.05 2 0.5 2
BPMC 60 0.01 60 0.3 60
MPP 60 0.01 60 2 60
PAP 79 0.02 79 0.1 79
61 0.1 61 0.20 61
79 0.02 79 0.5 79
108 0.02 108 0.5 108
60 0.01 60 0.05 60
86 0.05 86 0.3 86
60 0.03 60 0.10 60
62 0.01 62 0.5 62
60 0.02 60 0.3 60
61 0.03 61 1 61
60 0.01 60 0.05 60
DCPA 60 0.02 60 0.1 60
60 0.02 60 0.05 60
PHC 60 0.02 60 1 60
60 0.02 60 0.02 60
60 0.02 60 0.5 60
60 0.02 60 0.01 60
60 0.02 60 0.5 60
60 0.05 60 0.05 60
62 0.03 62 1 62
136
13-01-276_本文_MK.indd 13613-01-276_本文_MK.indd 136 2013/01/24 21:17:062013/01/24 21:17:06
(mg/kg)
(ppm)
60 0.02 60 0.05 60
60 0.01 60 0.5 60
60 0.03 60 1 60
109 0.01 109 1 109
63 0.02 62 1 63
DMTP 221 0.02 221 5 221
137
13-01-276_本文_MK.indd 13713-01-276_本文_MK.indd 137 2013/01/24 21:17:062013/01/24 21:17:06
3.1.4.2.
1518 210
90 88 83 85
83
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
70 0.02 69 < 0.02 0.02 0.01 -
70 0.01 70 - - 0.003 -
70 0.001 70 - - 0.0004 -
84
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
30 0.04 30 - - 0.02 -
30 0.01 30 - - 0.003 -
30 0.001 30 - - 0.0004 -
85
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
30 0.04 28 < 0.04 0.05 0.02 -
30 0.01 30 - - 0.003 -
28 0.001 28 - - 0.0008 -
3.1.4.3.
138
13-01-276_本文_MK.indd 13813-01-276_本文_MK.indd 138 2013/01/24 21:17:062013/01/24 21:17:06
3.1.4.2.
3.1.4.3.
1785 2 170
86
86
(mg/kg)
(ppm)
DDT 2 0.01 2 0.5 2
XMC 2 0.01 2 0.2 2
2 0.01 2 5.0 2
2 0.01 2 1.0 2
2 0.02 2 0.02 2
2 0.07 2 0.2 2
2 0.03 2 10 2
2 0.01 2 5 2
2 0.02 2 5 2
2 0.01 2 0.2 2
2 0.01 2 0.005 2
2 0.03 2 0.5 2
2 0.005 2 0.01 2
2 0.01 2 1 2
NAC 2 0.02 2 7 2
2 0.01 2 0.01 2
2 0.01 2 0.8 2
2 0.01 2 10 2
2 0.01 2 1 2
2 0.01 2 0.5 2
2 0.01 2 2 2
139
13-01-276_本文_MK.indd 13913-01-276_本文_MK.indd 139 2013/01/24 21:17:062013/01/24 21:17:06
(mg/kg)
(ppm)
CVP 2 0.02 2 5.0 2
2 0.02 2 2.0 2
IPC
2 0.03 2 0.05 2
2 0.02 2 5.0 2
2 0.02 2 5.0 2
2 0.02 2 5 2
2 0.02 2 1.0 2
2 0.01 2 5 2
2 0.05 2 2.0 2
2 0.03 2 3.0 2
2 0.05 2 2.0 2
2 0.1 2 2 2
2 0.02 2 0.05 2
2 0.01 2 0.1 2
2 0.04 2 10 2
2 0.02 2 2 2
2 0.01 2 1 2
2 0.02 2 1 2
2 0.01 2 0.005 2
2 0.03 2 0.1 2
2 0.02 2 0.1 2
2 0.04 2 2.0 2
2 0.01 2 0.05 2
2 0.02 2 0.1 2
2 0.01 2 0.5 2
2 0.02 2 0.2 2
2 0.02 2 1 2
2 0.01 2 0.05 2
2 0.01 2 2 2
2 0.01 2 2.0 2
140
13-01-276_本文_MK.indd 14013-01-276_本文_MK.indd 140 2013/01/24 21:17:062013/01/24 21:17:06
(mg/kg)
(ppm)
2 0.01 2 0.05 2
2 0.01 2 5.0 2
2 0.03 2 1 2
2 0.02 2 2.0 2
MEP
2 0.01 2 2.0 2
2 0.05 2 0.1 2
BPMC
2 0.01 2 7.0 2
MPP 2 0.01 2 2 2
PAP 2 0.01 2 0.1 2
2 0.03 2 2.0 2
2 0.02 2 1.0 2
2 0.02 2 5 2
2 0.01 2 0.05 2
2 0.01 2 2.5 2
2 0.03 2 2.0 2
2 0.01 2 2.0 2
2 0.02 2 2 2
2 0.01 2 0.5 2
2 0.01 2 0.1 2
DCPA 2 0.02 2 0.1 2
2 0.02 2 0.05 2
PHC 2 0.02 2 1 2
2 0.02 2 0.02 2
2 0.02 2 2 2
2 0.02 2 0.01 2
2 0.02 2 5.0 2
2 0.05 2 0.05 2
2 0.02 2 1 2
2 0.02 2 0.05 2
2 0.01 2 4.0 2
141
13-01-276_本文_MK.indd 14113-01-276_本文_MK.indd 141 2013/01/24 21:17:062013/01/24 21:17:06
(mg/kg)
(ppm)
2 0.03 2 10 2
2 0.01 2 1 2
2 0.01 2 1 2
DMTP
2 0.01 1 5 2
3.1.4.4.
142
13-01-276_本文_MK.indd 14213-01-276_本文_MK.indd 142 2013/01/24 21:17:072013/01/24 21:17:07
3.1.4.4.
1518 20 598 87
3
87
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
400 0.04 400 - - 0.01 -
99 0.01 96 < 0.01 0.03 0.004 -
99 0.001 99 - - 0.0005 -
1517 19 16 88
88 pg-TEQ/g
16 0.0011 0.0062 0.0024
143
13-01-276_本文_MK.indd 14313-01-276_本文_MK.indd 143 2013/01/24 21:17:072013/01/24 21:17:07
1822 63 350 3,326
89
89
(mg/kg)
(ppm)
6 0.01 4 0.5 6
119 0.02 71 5 119
4 0.01 4 2 4
15 0.01 14 2 15
20 0.05 16 10 20
5 0.02 5 0.5 5
40 0.03 40 0.5 40
NAC 88 0.05 86 1.0 88
125 0.01 106 5.0 125
252 0.02 183 5 252
49 0.005 43 1 49
285 0.01 247 1.0 285
26 0.01 11 1 26
8 0.05 8 2.0 8
TPN 6 0.01 6 2 6
CYAP 114 0.02 113 0.2 114
DDVP
16 0.01 16 0.1 16
45 0.01 31 0.5 45
135 0.05 130 0.4 135
239 0.02 239 1 239
95 0.05 95 1.0 95
91 0.03 87 1.0 91
144
13-01-276_本文_MK.indd 14413-01-276_本文_MK.indd 144 2013/01/24 21:17:072013/01/24 21:17:07
(mg/kg)
(ppm)
118 0.03 108 5 118
5 0.05 5 2.0 5
111 0.02 111 0.1 111
137 0.03 130 2 137
10 0.02 10 0.3 10
2 0.01 2 3 2
3 0.02 3 0.5 3
48 0.1 48 0.2 48
53 0.02 53 1.0 53
30 0.01 25 0.5 30
48 0.03 47 0.5 48
3 0.01 3 0.5 3
1 0.03 1 0.5 1
3 0.02 3 0.5 3
15 0.05 15 2.0 15
137 0.02 94 3 137
1 0.02 1 0.1 1
5 0.01 5 0.6 5
45 0.01 35 1 45
4 0.03 4 2.0 4
102 0.1 102 1.0 102
MEP
26 0.01 25 0.2 26
PAP
122 0.02 122 0.1 122
3 0.1 3 2.0 3
1 0.02 0 0.5 1
131 0.02 25 5 131
10 0.05 10 0.5 10
7 0.03 5 2 7
5 0.01 2 0.5 5
38 0.02 38 1 38
145
13-01-276_本文_MK.indd 14513-01-276_本文_MK.indd 145 2013/01/24 21:17:072013/01/24 21:17:07
(mg/kg)
(ppm)
7 0.01 5 1 7
1 0.03 1 0.5 1
6 0.02 6 0.3 6
70 0.01 70 0.5 70
1 0.02 1 1 1
2 0.02 1 2.0 2
40 0.02 13 3.0 40
6 0.03 6 0.5 6
1 0.02 1 5.0 1
DMTP
182 0.02 182 0.5 182
3 0.02 3 2 3
3.1.4.5.
146
13-01-276_本文_MK.indd 14613-01-276_本文_MK.indd 146 2013/01/24 21:17:072013/01/24 21:17:07
3.1.4.5.
1618 20 600 90
1
90
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
400 0.02 400 - - 0.01 -
100 0.01 99 < 0.01 0.02 0.004 -
100 0.001 100 - - 0.0007 -
1517 19 12 91
91 pg-TEQ/g
12 0.0000062 0.0074 0.0026
147
13-01-276_本文_MK.indd 14713-01-276_本文_MK.indd 147 2013/01/24 21:17:072013/01/24 21:17:07
3.1.4.6.
1518 20 600 92
8
92
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
400 0.05 400 - - 0.02 -
100 0.01 92 < 0.01 0.03 0.005 -
100 0.001 100 - - 0.0004 -
1517 19 18 93
93 pg-TEQ/g
18 0.0000050 0.47 0.030
148
13-01-276_本文_MK.indd 14813-01-276_本文_MK.indd 148 2013/01/24 21:17:072013/01/24 21:17:07
3.1.4.6.
1830 94 385
94
94
(mg/kg)
(ppm)
56 0.01 53 2 56
4 0.01 4 1 4
18 0.01 18 2 18
2 0.07 2 0.2 2
1 0.02 1 2 1
NAC 1 0.02 1 1.0 1
45 0.01 38 5 45
5 0.01 5 1 5
2 0.02 2 2.0 2
CYAP 4 0.01 4 0.2 4
2 0.02 2 5.0 2
4 0.02 4 0.5 4
13 0.02 12 1 13
15 0.05 13 2.0 15
4 0.01 4 0.1 4
2 0.01 2 3 2
1 0.01 1 0.5 1
2 0.02 2 0.5 2
3 0.04 3 2.0 3
8 0.01 7 0.5 8
5 0.02 5 1.0 5
MEP 48 0.01 48 0.2 48
PAP 1 0.01 1 0.1 1
149
13-01-276_本文_MK.indd 14913-01-276_本文_MK.indd 149 2013/01/24 21:17:082013/01/24 21:17:08
(mg/kg)
(ppm)
5 0.03 5 1.0 5
9 0.02 4 2 9
3 0.01 0 1.0 3
36 0.01 34 0.2 36
1 0.01 1 0.5 1
7 0.01 5 1 7
DMTP 78 0.01 78 0.2 78
3.1.4.7.
150
13-01-276_本文_MK.indd 15013-01-276_本文_MK.indd 150 2013/01/24 21:17:082013/01/24 21:17:08
3.1.4.7.
1618 300 95
2
95
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
100 0.02 100 - - 0.01 -
100 0.01 98 < 0.01 0.01 0.004 -
100 0.001 100 - - 0.0005 -
1719 22 102 264 3,566
96
96
(mg/kg)
(ppm)
BHC 20 0.02 20 0.2 20
DDT 20 0.01 20 0.2 20
XMC 20 0.01 20 0.2 20
40 0.01 40 0.2 40
112 0.02 101 5 112
151
13-01-276_本文_MK.indd 15113-01-276_本文_MK.indd 151 2013/01/24 21:17:082013/01/24 21:17:08
(mg/kg)
(ppm)
78 0.01 74 1.5 78
20 0.02 20 0.02 20
20 0.07 20 0.2 20
71 0.05 51 10 71
32 0.02 30 0.5 32
20 0.01 20 0.3 20
4 0.03 4 0.1 4
20 0.02 20 2 20
20 0.01 20 0.1 20
20 0.01 20 0.05 20
20 0.03 20 1 20
20 0.01 20 1 20
NAC 27 0.05 27 1.0 27
20 0.01 20 0.02 20
2 0.01 2 15 2
67 0.02 66 1 67
37 0.005 20 0.7 37
131 0.01 131 1.0 131
20 0.01 20 0.5 20
38 0.02 38 0.05 38
CVP 20 0.02 20 0.05 20
20 0.02 20 2.0 20
IPC
20 0.03 20 0.05 20
20 0.02 20 0.02 20
TPN
41 0.01 38 2 41
CYAP 46 0.02 46 0.2 46
20 0.02 20 5.0 20
DDVP
12 0.01 12 0.1 12
152
13-01-276_本文_MK.indd 15213-01-276_本文_MK.indd 152 2013/01/24 21:17:082013/01/24 21:17:08
(mg/kg)
(ppm)
20 0.02 20 3.0 20
47 0.01 23 3 47
23 0.05 23 0.5 23
20 0.02 20 1 20
28 0.05 28 1.0 28
38 0.03 38 0.05 38
21 0.05 21 2.0 21
20 0.1 20 1 20
20 0.02 20 0.1 20
17 0.02 17 0.2 17
106 0.02 106 0.1 106
107 0.03 84 1 107
1 0.02 1 0.5 1
52 0.04 52 2 52
93 0.1 93 1 93
38 0.02 38 0.5 38
20 0.01 20 0.5 20
69 0.03 69 0.3 69
20 0.01 20 0.005 20
1 0.01 1 0.5 1
20 0.03 20 0.1 20
20 0.02 20 0.1 20
41 0.05 41 2.0 41
20 0.01 20 0.05 20
3 0.02 3 0.2 3
20 0.02 20 0.1 20
3 0.01 3 0.2 3
20 0.01 20 0.5 20
20 0.01 20 0.3 20
153
13-01-276_本文_MK.indd 15313-01-276_本文_MK.indd 153 2013/01/24 21:17:082013/01/24 21:17:08
(mg/kg)
(ppm)
20 0.02 20 0.2 20
20 0.02 20 0.1 20
100 0.02 71 1.0 100
31 0.01 31 0.1 31
20 0.01 20 2.0 20
20 0.01 20 0.50 20
20 0.01 20 0.10 20
20 0.03 20 1 20
28 0.1 28 1.0 28
MEP
67 0.01 67 0.2 67
20 0.05 20 0.1 20
BPMC
20 0.01 20 0.3 20
MPP 20 0.01 20 5 20
PAP 26 0.02 26 0.1 26
31 0.1 31 5.0 31
25 0.02 25 0.1 25
54 0.02 54 1 54
20 0.01 20 1 20
179 0.05 178 1 179
20 0.03 20 0.50 20
24 0.01 24 0.2 24
111 0.02 111 0.1 111
39 0.01 39 0.05 39
38 0.03 35 3 38
DCPA 20 0.02 20 0.1 20
20 0.02 20 1.0 20
PHC 20 0.02 20 1 20
83 0.01 82 0.1 83
20 0.02 20 0.02 20
154
13-01-276_本文_MK.indd 15413-01-276_本文_MK.indd 154 2013/01/24 21:17:082013/01/24 21:17:08
(mg/kg)
(ppm)
20 0.02 20 1 20
20 0.02 20 0.01 20
119 0.02 119 2.0 119
20 0.05 20 0.05 20
20 0.02 20 2 20
21 0.02 17 1.7 21
20 0.02 20 0.05 20
29 0.03 29 0.5 29
43 0.03 40 2 43
20 0.01 20 1.0 20
DMTP
72 0.02 72 0.2 72
155
13-01-276_本文_MK.indd 15513-01-276_本文_MK.indd 155 2013/01/24 21:17:082013/01/24 21:17:08
3.1.4.8.
1618 20 599 97
1
97
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
399 0.03 399 - - 0.02 -
100 0.01 99 < 0.01 0.01 0.004 -
100 0.001 100 - - 0.0006 -
1517 19 28 98
98 pg-TEQ/g
28 0.000038 0.053 0.0098
156
13-01-276_本文_MK.indd 15613-01-276_本文_MK.indd 156 2013/01/24 21:17:082013/01/24 21:17:08
3.1.4.8.
1719 22 106 316 7,250
99
99
(mg/kg)
(ppm)
BHC 62 0.02 62 0.2 62
DDT 62 0.01 62 0.2 62
XMC 62 0.01 62 0.2 62
41 0.01 41 2 41
78 0.02 68 5 78
177 0.01 132 5.0 177
218 0.01 103 10 218
62 0.02 62 0.02 62
62 0.01 62 0.01 62
62 0.07 62 0.2 62
110 0.05 107 25 110
61 0.02 25 3 61
62 0.01 62 0.3 62
6 0.03 5 0.5 6
62 0.01 62 0.02 62
62 0.01 62 0.2 62
62 0.03 62 1 62
63 0.05 63 1 63
NAC 119 0.05 117 1.0 119
62 0.01 62 0.02 62
45 0.01 38 5 45
210 0.02 139 15 210
19 0.005 15 5 19
157
13-01-276_本文_MK.indd 15713-01-276_本文_MK.indd 157 2013/01/24 21:17:092013/01/24 21:17:09
(mg/kg)
(ppm)
65 0.01 64 1.0 65
62 0.01 62 0.2 62
132 0.02 99 5 132
CVP 62 0.02 62 0.05 62
62 0.02 62 2.0 62
IPC
62 0.03 62 0.05 62
62 0.02 62 0.02 62
TPN 3 0.01 3 0.5 3
30 0.03 23 10 30
CYAP 1 0.02 1 0.2 1
97 0.05 97 5.0 97
DDVP
2 0.01 2 0.1 2
62 0.02 62 3.0 62
27 0.01 21 10 27
62 0.02 62 1.0 62
62 0.02 62 0.5 62
76 0.05 73 1.0 76
62 0.03 62 0.05 62
88 0.03 63 5 88
77 0.05 76 2.0 77
62 0.1 62 1 62
183 0.02 183 1 183
80 0.02 80 0.1 80
29 0.03 25 5 29
10 0.02 9 2 10
62 0.04 62 5 62
18 0.1 15 10 18
62 0.02 62 0.5 62
72 0.01 70 0.5 72
158
13-01-276_本文_MK.indd 15813-01-276_本文_MK.indd 158 2013/01/24 21:17:092013/01/24 21:17:09
(mg/kg)
(ppm)
62 0.01 62 0.1 62
62 0.02 62 1 62
62 0.01 62 0.005 62
15 0.01 10 0.5 15
62 0.03 62 0.5 62
62 0.02 62 0.5 62
DEP 1 0.01 1 0.50 1
79 0.05 79 2.0 79
62 0.01 62 0.05 62
9 0.02 9 5 9
62 0.02 62 0.1 62
62 0.01 62 0.5 62
62 0.01 62 0.3 62
62 0.02 62 0.2 62
62 0.01 62 0.05 62
87 0.01 81 2 87
62 0.01 62 2.0 62
62 0.01 62 0.50 62
62 0.01 62 1.0 62
62 0.03 62 1 62
62 0.02 62 1.0 62
MEP 164 0.01 162 0.2 164
62 0.05 62 0.1 62
BPMC 62 0.01 62 0.3 62
MPP 62 0.01 61 2 62
PAP 91 0.02 91 0.1 91
62 0.03 62 5.0 62
75 0.02 70 2.0 75
66 0.02 65 5 66
159
13-01-276_本文_MK.indd 15913-01-276_本文_MK.indd 159 2013/01/24 21:17:092013/01/24 21:17:09
(mg/kg)
(ppm)
62 0.01 62 0.05 62
98 0.05 98 1 98
48 0.03 45 5 48
62 0.03 62 2.0 62
102 0.01 98 2.0 102
62 0.02 62 2 62
62 0.01 62 5 62
65 0.02 65 2.0 65
DCPA 62 0.02 62 0.1 62
62 0.02 62 0.5 62
PHC 62 0.02 62 1 62
62 0.02 62 0.02 62
62 0.02 62 2 62
62 0.02 62 0.01 62
134 0.02 98 5.0 134
62 0.05 62 0.1 62
62 0.02 62 1 62
1 0.02 0 10 1
62 0.02 62 0.05 62
84 0.03 84 8.0 84
62 0.03 62 5 62
177 0.01 148 3 177
105 0.02 103 1 105
DMTP
116 0.02 116 1 116
62 0.02 61 5 62
3.1.4.9.
160
13-01-276_本文_MK.indd 16013-01-276_本文_MK.indd 160 2013/01/24 21:17:092013/01/24 21:17:09
3.1.4.9.
15 18 21089 100 101
1
100
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
70 0.03 69 < 0.03 0.03 0.02 -
70 0.01 69 < 0.01 0.01 0.004 -
70 0.001 70 - - 0.0005 -
101
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
29 0.05 29 - - 0.02 -
30 0.01 30 - - 0.003 -
30 0.001 30 - - 0.0004 -
161
13-01-276_本文_MK.indd 16113-01-276_本文_MK.indd 161 2013/01/24 21:17:092013/01/24 21:17:09
3.1.5.
3.1.5.1.
1517 19 22 24 102
102 pg-TEQ/g
16 0.016 0.21 0.065
8 0.023 0.25 0.13
1739 8 312
103
103
(mg/kg)
(ppm)
BHC 8 0.05 8 0.2 8
DDT 8 0.05 8 0.2 8
XMC 8 0.5 8 10 8
162
13-01-276_本文_MK.indd 16213-01-276_本文_MK.indd 162 2013/01/24 21:17:092013/01/24 21:17:09
3.1.5.1.
(mg/kg)
(ppm)
8 2 8 20 8
8 0.1 8 0.3 8
8 2 8 10 8
8 0.05 8 30 8
8 1 8 20 8
8 0.5 8 10 8
8 1 8 10 8
8 2 8 10 8
8 0.2 8 20 8
8 2 8 20 8
8 0.1 8 20 8
8 0.2 8 1 8
8 0.05 8 0.1 8
8 2 8 0.5 8
8 0.5 8 2 8
8 2 8 20 8
8 0.02 8 0.05 8
8 0.1 8 0.3 8
8 0.1 8 0.2 8
8 0.1 8 10 8
8 0.5 8 10 8
8 2 8 5 8
8 0.5 8 10 8
8 1 8 3 8
MEP
8 0.1 8 0.2 8
BPMC 8 0.1 8 0.5 8
PAP 8 0.05 8 0.1 8
8 0.05 8 1 8
8 1 8 10 8
163
13-01-276_本文_MK.indd 16313-01-276_本文_MK.indd 163 2013/01/24 21:17:092013/01/24 21:17:09
(mg/kg)
(ppm)
8 0.5 8 10 8
8 1 8 15 8
8 0.5 8 5 8
8 1 8 15 8
8 2 8 35 8
8 0.1 8 20 8
8 0.5 8 20 8
3.1.5.2.
164
13-01-276_本文_MK.indd 16413-01-276_本文_MK.indd 164 2013/01/24 21:17:092013/01/24 21:17:09
3.1.5.2.
1518 300 104
2
9
104
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
100 0.04 98 < 0.04 0.09 0.02 -
100 0.01 45 < 0.01 0.14 0.02 0.01
100 0.001 6 < 0.001 0.01 0.003 0.003
165
13-01-276_本文_MK.indd 16513-01-276_本文_MK.indd 165 2013/01/24 21:17:102013/01/24 21:17:10
3.2.
18 2022 585 105
105 pg-TEQ/g
85 0.00003 0.039 0.0068
60 0.00006 0.27 0.088
105 0 1.5 0.23
20 0 2.2 0.23
85 0.00018 0.076 0.0078
85 0.00012 0.23 0.039
85 0.00057 0.20 0.032
30 0 0.17 0.016
30 0.031 0.57 0.22
0 18
166
13-01-276_本文_MK.indd 16613-01-276_本文_MK.indd 166 2013/01/24 21:17:102013/01/24 21:17:10
3.3.
3.3.1.
18 20 770 670 106 107
3
106
(mg/kg)
(mg/kg) (mg/kg)
(mg/kg) (mg/kg)
299 0.05 0 28 160 93 92 71 0.05 0 2.1 20 6 5.5
200 0.05 0 25 110 53 51 100 0.05 0 15 52 33 33
100 0.05 0 13 51 25 23
107
(mg/kg)
(mg/kg) (mg/kg)
(mg/kg) (mg/kg)
299 0.5 0 4.5 130 67 68 71 0.5 3 < 0.5 17 3.6 3.2
100 0.5 100 - - 0.19 -
100 0.5 100 - - 0.15 -
100 0.5 100 - - 0.16 -
167
13-01-276_本文_MK.indd 16713-01-276_本文_MK.indd 167 2013/01/24 21:48:222013/01/24 21:48:22
3.3.2.
1922 1,800
108 109
108
(mg/kg)
(mg/kg) (mg/kg)
(mg/kg) (mg/kg)
120 0.01 0 0.05 1.4 0.26 0.17
120 0.01 0 0.27 2.3 0.69 0.65
120 0.01 0 0.14 2.0 0.49 0.43
120 0.01 0 0.17 1.4 0.52 0.48
120 0.01 0 0.28 4.4 0.81 0.58
120 0.01 0 0.10 0.59 0.32 0.33
120 0.01 0 0.18 2.3 0.64 0.46
120 0.01 0 0.10 24 2.0 0.86
120 0.01 0 0.07 1.4 0.40 0.35
120 0.01 0 0.05 3.9 1.3 1.2
120 0.01 1 < 0.01 0.39 0.15 0.16
120 0.01 0 0.10 2.8 0.77 0.70
120 0.01 0 0.30 2.5 0.74 0.62
120 0.01 0 0.01 0.32 0.06 0.04
120 0.01 0 0.02 0.20 0.09 0.08
168
13-01-276_本文_MK.indd 16813-01-276_本文_MK.indd 168 2013/01/24 21:17:102013/01/24 21:17:10
109
(mg/kg)
(mg/kg) (mg/kg)
(mg/kg) (mg/kg)
120 0.01 0 0.04 1.2 0.23 0.13
120 0.01 0 0.26 1.8 0.60 0.55
120 0.01 0 0.12 1.7 0.42 0.36
120 0.01 0 0.15 1.1 0.44 0.40
120 0.01 0 0.26 2.9 0.69 0.52
120 0.01 0 0.08 0.43 0.27 0.28
120 0.01 0 0.16 2.0 0.55 0.40
120 0.01 0 0.03 1.1 0.25 0.20
120 0.01 0 0.06 1.2 0.33 0.29
120 0.01 0 0.04 2.8 1.1 1.0
120 0.01 4 < 0.01 0.35 0.13 0.14
120 0.01 0 0.07 2.2 0.65 0.58
120 0.01 0 0.25 2.2 0.66 0.57
120 0.01 0 0.01 0.28 0.05 0.03
120 0.01 0 0.02 0.19 0.08 0.07
22 1,800 110
110
(mg/kg)
(mg/kg) (mg/kg)
(mg/kg) (mg/kg)
300 0.03 0 0.03 1.0 0.25 0.22
300 0.03 0 1.7 48 15 14
300 0.03 3 < 0.03 1.6 0.45 0.32
169
13-01-276_本文_MK.indd 16913-01-276_本文_MK.indd 169 2013/01/24 21:17:102013/01/24 21:17:10
(mg/kg)
(mg/kg) (mg/kg)
(mg/kg) (mg/kg)
300 0.03 0 7.3 68 33 31 300 0.03 0 0.59 6.0 2.2 2.1
300 0.03 0 0.15 1.3 0.43 0.29
1522 688 111
111 pg-TEQ/g
59 0.082 1.1 0.41
60 0.43 6.5 2.0
90 0.25 7.8 2.2
91 0.096 3.7 1.1
89 0.17 3.5 0.85
59 0.18 2.6 0.99
50 0.26 5.5 3.2
49 0.74 4.0 2.4
44 1.1 3.9 2.0
170
13-01-276_本文_MK.indd 17013-01-276_本文_MK.indd 170 2013/01/24 21:17:102013/01/24 21:17:10
48 0.38 2.1 0.68
49 0.21 6.1 0.64
0 15 20 15 20 22 15 19
21 16 17 19 21
171
13-01-276_本文_MK.indd 17113-01-276_本文_MK.indd 171 2013/01/24 21:17:102013/01/24 21:17:10
3.4.
3.4.1.
3.4.1.1.
DON NIV20 50 100 112
NIV DON 2
112
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
DON 50 0.04 48 < 0.04 0.04 0.022 -NIV 50 0.03 50 - - 0.02 -
3.4.1.2.
172
13-01-276_本文_MK.indd 17213-01-276_本文_MK.indd 172 2013/01/24 21:17:112013/01/24 21:17:11
3.4.1.1.
3.4.1.2.
DON NIV18 19 65 130 113
NIV DON 9
113
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
DON 65 0.04 60 < 0.04 0.06 0.024 -NIV 65 0.05 65 - - 0.02 -
17 30 114
114
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
15 0.02 15 - - 0.02 -
5 0.02 5 - - 0.02 -
10 0.02 10 - - 0.02 -
173
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3.4.1.3.
DONNIV 18 19 75
150 115 NIV DON 2
115
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
DON 75 0.04 73 < 0.04 0.08 0.022 -NIV 75 0.03 75 - - 0.02 -
3.4.1.4.
174
13-01-276_本文_MK.indd 17413-01-276_本文_MK.indd 174 2013/01/24 21:17:112013/01/24 21:17:11
3.4.1.3.
3.4.1.4.
DON NIV 19 30 60 116
DON NIV
116
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
DON 30 0.04 30 - - 0.021 -NIV 30 0.04 30 - - 0.02 -
175
13-01-276_本文_MK.indd 17513-01-276_本文_MK.indd 175 2013/01/24 21:17:112013/01/24 21:17:11
3.4.1.5.
DON NIV19 20 40 117
NIV DON 1
117
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
DON 20 0.04 19 < 0.04 0.04 0.024 -NIV 20 0.04 20 - - 0.02 -
16 30 118
7
118
(mg/kg)
(mg/kg)
(mg/kg) (mg/kg)
(mg/kg)
30 0.02 9 < 0.02 0.08 0.03 0.03
3.4.1.6.
176
13-01-276_本文_MK.indd 17613-01-276_本文_MK.indd 176 2013/01/24 21:17:112013/01/24 21:17:11
3.4.1.5.
3.4.1.6.
DON NIV19 20 40 119
NIV DON 3
119
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
DON 20 0.04 17 < 0.04 0.10 0.026 -NIV 20 0.04 20 - - 0.02 -
177
13-01-276_本文_MK.indd 17713-01-276_本文_MK.indd 177 2013/01/24 21:17:112013/01/24 21:17:11
3.4.1.7.
2230 120
9
120
(mg/kg)
(mg/kg)
(mg/kg) (mg/kg)
(mg/kg)
30 0.005 2 < 0.005 0.634 0.093 0.078
3.4.2.1.
178
13-01-276_本文_MK.indd 17813-01-276_本文_MK.indd 178 2013/01/24 21:17:112013/01/24 21:17:11
3.4.1.7.
3.4.2.
3.4.2.1.
17 30 121
121 17
(mg/kg)
(mg/kg) (mg/kg) (mg/kg)
(mg/kg)
30 0.02 0 0.12 0.91 0.38 0.38
19 180 122
17
122 19
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
180 0.020 0 0.090 1.5 0.41 0.38
179
13-01-276_本文_MK.indd 17913-01-276_本文_MK.indd 179 2013/01/24 21:17:122013/01/24 21:17:12
3.4.2.2.
2030 123
123
(μg/kg)
μg/kg μg/kg μg/kg
μg/kg
30 1.0 30 - - 0.40 -
3.4.2.3.
180
13-01-276_本文_MK.indd 18013-01-276_本文_MK.indd 180 2013/01/24 21:17:122013/01/24 21:17:12
3.4.2.2.
3.4.2.3.
20 30 124 1
124
(μg/kg)
(μg/kg) (μg/kg) (μg/kg)
(μg/kg)
30 1.3 29 < 1.3 1.3 1.0 -
181
13-01-276_本文_MK.indd 18113-01-276_本文_MK.indd 181 2013/01/24 21:17:122013/01/24 21:17:12
3.4.2.4.
2010 125
125
(μg/kg)
(μg/kg) (μg/kg) (μg/kg)
(μg/kg)
10 1.3 5 < 1.3 2.3 1.1 -
182
13-01-276_本文_MK.indd 18213-01-276_本文_MK.indd 182 2013/01/24 21:17:122013/01/24 21:17:12
3.4.2.4.
3.4.3.
20 50 126
126
(mg/kg)
(mg/kg) (mg/kg)
(mg/kg)
(mg/kg)
50 0.027 0 0.035 2.3 0.46 0.22
30 2930 60
20 127 130
127
(mg/kg)
(mg/kg) (mg/kg)
(mg/kg) (mg/kg)
15 0.03 0 0.09 1.6 0.73 0.41
10 0.03 4 < 0.03 0.38 0.09 0.04
5 0.03 0 0.13 0.22 0.17 0.15
183
13-01-276_本文_MK.indd 18313-01-276_本文_MK.indd 183 2013/01/24 21:17:122013/01/24 21:17:12
128
(mg/kg)
(mg/kg) (mg/kg)
(mg/kg) (mg/kg)
14 0.02 0 0.11 2.9 1.0 0.97
15 0.02 15 - - 0.005 -
129
(mg/kg)
(mg/kg) (mg/kg)
(mg/kg) (mg/kg)
15 0.02 2 < 0.02 0.47 0.25 0.34
15 0.02 2 < 0.02 0.35 0.09 0.05
130
(mg/kg)
(mg/kg) (mg/kg)
(mg/kg) (mg/kg)
10 0.03 3 < 0.03 0.87 0.19 0.14
10 0.03 10 - - 0.008 -
10 0.03 2 < 0.03 0.32 0.11 0.06
10 0.03 10 - - 0.01 -
10 0.03 0 0.05 0.92 0.42 0.37
10 0.03 10 - - 0.008 -
3.4.4.1.
184
13-01-276_本文_MK.indd 18413-01-276_本文_MK.indd 184 2013/01/24 21:17:122013/01/24 21:17:12
3.4.4.
3.4.4.1.
22 92 131
90%
131
(mg/kg)
(mg/kg) (mg/kg)
(mg/kg) (mg/kg)
24 30 24 - - 10 - 42 30 42 - - 10 -
26 30 20 < 30 2500 180 -
20 40 132
7
185
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132
(μg/kg)
(μg/kg) (μg/kg) (μg/kg)
(μg/kg)
40 1.3 12 < 1.3 22 5.8 3.4
3.4.4.2.
186
13-01-276_本文_MK.indd 18613-01-276_本文_MK.indd 186 2013/01/24 21:17:132013/01/24 21:17:13
3.4.4.2.
20 20 133 1
133
(μg/kg)
(μg/kg) (μg/kg) (μg/kg)
(μg/kg)
20 1.0 19 < 1.0 1.3 0.48 -
187
13-01-276_本文_MK.indd 18713-01-276_本文_MK.indd 187 2013/01/24 21:17:132013/01/24 21:17:13
3.4.4.3.
PAHs
PAHs 13416 PAH 20 100 1,600
135 137
PAH
134 PAH
[a] BaA
[b] BbFL
[c] BcFL
[b] BbFA
[j] BjFA
[k] BkFA
[g,h,i] BghiP
[a] BaP
CHR
[a,h] DBahA
[a,e] DBaeP
[a,h] DBahP
[a,i] DBaiP
[a,l] DBalP
[1,2,3-c,d] IP
5- MCH
188
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3.4.4.3.
135 PAH
(μg/kg)
(μg/kg)
(μg/kg)
(μg/kg)
(μg/kg)
BaA 50 0.17 0 0.32 930 128 120
BbFL 50 0.08 0 0.09 250 38 34
BcFL 50 0.08 1 < 0.08 130 22 20
BbFA 50 0.18 0 0.18 220 31 29
BkFA 50 0.06 0 0.08 120 16 15
BjFA 50 0.14 2 < 0.14 160 22 22
BghiP 50 0.07 0 0.08 70 8.8 8
BaP 50 0.11 0 0.16 200 29 27
CHR 50 0.4 0 0.5 1100 169 160
DBahA 50 0.17 4 < 0.17 17 2.1 1.9
DBaeP 50 0.10 3 < 0.10 6.3 0.88 0.74
DBahP 50 0.10 12 < 0.10 1.9 0.26 0.23
DBaiP 50 0.16 5 < 0.16 5.6 0.61 0.44
DBalP 50 0.3 5 < 0.3 17 2.6 2.2
IP 50 0.20 2 < 0.20 33 11 12
MCH 50 0.13 8 < 0.13 1.8 0.38 0.28
189
13-01-276_本文_MK.indd 18913-01-276_本文_MK.indd 189 2013/01/24 21:17:132013/01/24 21:17:13
136 PAH
(μg/kg)
(μg/kg)
(μg/kg)
(μg/kg)
(μg/kg)
BaA 16 0.17 0 0.61 66 21 12
BbFL 16 0.08 0 0.19 20 5.2 3.0
BcFL 16 0.08 0 0.12 14 3.5 1.6
BbFA 16 0.18 1 < 0.18 20 5.9 2.9
BjFA 16 0.14 1 < 0.14 16 4.3 1.8
BkFA 16 0.06 0 0.08 10 2.8 1.2
BghiP 16 0.07 1 < 0.07 5.6 1.6 0.73
BaP 16 0.11 0 0.15 21 5.6 2.2
CHR 16 0.4 0 0.7 86 25 16
DBahA 16 0.17 6 0.17 1.5 0.45 0.20
DBaeP 16 0.10 10 < 0.10 0.50 0.17 -
DBahP 16 0.14 14 < 0.14 0.24 0.09 -
DBaiP 16 0.16 10 < 0.16 0.42 0.16 -
DBalP 16 0.3 10 < 0.3 1.4 0.44 -
IP 16 0.20 3 < 0.20 8.1 2.3 1.1
MCH 16 0.13 11 < 0.13 0.49 0.14 -
190
13-01-276_本文_MK.indd 19013-01-276_本文_MK.indd 190 2013/01/24 21:17:132013/01/24 21:17:13
137 PAH
(μg/kg)
(μg/kg)
(μg/kg)
(μg/kg)
(μg/kg)
BaA 34 0.17 27 < 0.17 38 1.26 -
BbFL 34 0.08 31 < 0.08 13 0.43 -
BcFL 34 0.05 29 < 0.05 9 0.30 -
BbFA 34 0.13 31 < 0.13 9.1 0.34 -
BjFA 34 0.10 31 <0.10 7 0.26 -
BkFA 34 0.17 33 < 0.17 5.2 0.23 -
BghiP 34 0.09 33 < 0.09 3.5 0.15 -
BaP 34 0.11 31 < 0.11 11 0.38 -
CHR 34 0.3 29 < 0.3 47 1.6 -
DBahA 34 0.08 33 < 0.08 0.89 0.07 -
DBaeP 34 0.15 33 < 0.15 0.51 0.07 -
DBahP 34 0.13 33 < 0.13 0.14 0.05 -
DBaiP 34 0.09 33 < 0.09 0.39 0.05 -
DBalP 34 0.15 33 < 0.15 1.6 0.11 -
IP 34 0.11 33 < 0.11 5 0.20 -
MCH 34 0.11 34 < 0.11 - 0.04 -
191
13-01-276_本文_MK.indd 19113-01-276_本文_MK.indd 191 2013/01/24 21:17:132013/01/24 21:17:13
22 332 138
90%
138
(mg/kg)
(mg/kg) (mg/kg)
(mg/kg) (mg/kg)
44 30 40 < 30 260 26 -
100 30 93 < 30 320 19 -
87 30 87 - - 10 -
59 30 54 < 30 42 13 -
42 30 24 < 30 660 140 -
3.4.5.1.
192
13-01-276_本文_MK.indd 19213-01-276_本文_MK.indd 192 2013/01/24 21:17:132013/01/24 21:17:13
3.4.5.
3.4.5.1.
DON NIV19 10 20 139
DON NIV
139
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
DON 10 0.04 10 - - 0.02 -NIV 10 0.04 10 - - 0.02 -
17 30 140
1
140
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
30 0.02 1 < 0.02 0.46 0.18 0.16
193
13-01-276_本文_MK.indd 19313-01-276_本文_MK.indd 193 2013/01/24 21:17:142013/01/24 21:17:14
3.4.5.2.
16 60 141
2
141 16
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
30 0.02 0 0.03 4.7 1.2 0.94
30 0.02 2 < 0.02 0.32 0.14 0.14
18 19541 142
1
142 18-19
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
541 0.020 1 < 0.020 5.5 1.1 0.94
22
39
194
13-01-276_本文_MK.indd 19413-01-276_本文_MK.indd 194 2013/01/24 21:17:142013/01/24 21:17:14
3.4.5.2.
20 143
1
143 22
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
39 0.005 0 0.007 1.15 0.166 0.106
20 0.005 1 < 0.005 2.86 0.314 0.154
195
13-01-276_本文_MK.indd 19513-01-276_本文_MK.indd 195 2013/01/24 21:17:142013/01/24 21:17:14
3.4.5.3.
16 30 144
144 16
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
30 0.02 0 0.03 0.50 0.13 0.08
21
143 145
145 21
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
48
0.007
0.028
0 0.047 1.77 0.166 0.104
48 2 < 0.028 0.369 0.114 0.093
47 0 0.035 0.676 0.179 0.136
3.4.5.4.
196
13-01-276_本文_MK.indd 19613-01-276_本文_MK.indd 196 2013/01/24 21:17:142013/01/24 21:17:14
3.4.5.3.
3.4.5.4.
17 18 230 146
7
146
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
80 0.020 4 < 0.020 0.80 0.21 0.15
20 0.020 0 0.061 0.34 0.17 0.15
56 0.020 23 < 0.020 0.52 0.054 0.021
30 0.020 20 < 0.020 0.083 0.025 -
24 0.020 3 < 0.020 1.0 0.22 0.13
20 0.020 19 < 0.020 0.030 0.021 -
197
13-01-276_本文_MK.indd 19713-01-276_本文_MK.indd 197 2013/01/24 21:17:142013/01/24 21:17:14
3.4.5.5.
21 30 147
147
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
30 0.007 0 0.015 0.132 0.047 0.045
3.4.6.1.
198
13-01-276_本文_MK.indd 19813-01-276_本文_MK.indd 198 2013/01/24 21:17:142013/01/24 21:17:14
3.4.5.5.
3.4.6.
3.4.6.1.
DON NIV20 20 40
148 NIV DON 1
148
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
DON 20 0.05 19 < 0.05 0.05 0.022 -NIV 20 0.05 20 - - 0.02 -
199
13-01-276_本文_MK.indd 19913-01-276_本文_MK.indd 199 2013/01/24 21:17:142013/01/24 21:17:14
3.4.6.2.
DON NIV20
40 80 149 150
DON NIV
149
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
DON 20 0.04 19 < 0.04 0.49 0.04 -NIV 20 0.06 19 < 0.06 0.19 0.04 -
150
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
DON 20 0.05 20 - - 0.02 -NIV 20 0.04 20 - - 0.02 -
16 18 151
200
13-01-276_本文_MK.indd 20013-01-276_本文_MK.indd 200 2013/01/24 21:17:152013/01/24 21:17:15
3.4.6.2.
151
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
18 0.02 0 0.14 0.51 0.32 0.32
20 10 152
152
(μg/kg)
(μg/kg) (μg/kg) (μg/kg)
(μg/kg)
10 0.5 5 < 0.5 8.8 2.1 -
201
13-01-276_本文_MK.indd 20113-01-276_本文_MK.indd 201 2013/01/24 21:17:152013/01/24 21:17:15
3.4.6.3.
16 18 153
153
(mg/kg)
(mg/kg) (mg/kg) (mg/kg)
(mg/kg)
18 0.02 0 0.19 1.1 0.45 0.36
20 10 154
154
(μg/kg)
(μg/kg)
(μg/kg) (μg/kg)
(μg/kg)
10 0.5 0 3.6 16 8.7 8.3
3.4.6.4.
202
13-01-276_本文_MK.indd 20213-01-276_本文_MK.indd 202 2013/01/24 21:17:152013/01/24 21:17:15
3.4.6.3.
3.4.6.4.
19 30 155 1
155
(μg/kg)
(μg/kg)
(μg/kg) (μg/kg) (μg/kg)
30 0.4 1 < 0.4 3.3 1.4 1.3
203
13-01-276_本文_MK.indd 20313-01-276_本文_MK.indd 203 2013/01/24 21:17:152013/01/24 21:17:15
3.4.6.5.
17 60 156
156
(mg/kg)
(mg/kg) (mg/kg) (mg/kg)
(mg/kg)
30 0.002 0 0.0043 0.020 0.0088 0.0089
30 0.002 0 0.0051 0.014 0.0094 0.0089
21121 157
157
(mg/kg)
(mg/kg) (mg/kg) (mg/kg)
(mg/kg)
121 0.008 0 0.073 0.334 0.162 0.158
204
13-01-276_本文_MK.indd 20413-01-276_本文_MK.indd 204 2013/01/24 21:17:152013/01/24 21:17:15
3.4.6.5.
19 20 110 158
158
(μg/kg)
(μg/kg) (μg/kg) (μg/kg)
(μg/kg)
80 0.4 0 4.1 150 65 63
30 0.5 0 5.8 150 34 24
14
15
205
13-01-276_本文_MK.indd 20513-01-276_本文_MK.indd 205 2013/01/24 21:17:152013/01/24 21:17:15
3.4.6.6.
15 17 631 159
159
(mg/kg)
(mg/kg)
631 0.01 584 0.05 631
19 30 160 2
160
(μg/kg)
(μg/kg) (μg/kg) (μg/kg)
(μg/kg)
30 0.4 2 < 0.4 5.4 2.2 1.8
3.4.6.7.
206
13-01-276_本文_MK.indd 20613-01-276_本文_MK.indd 206 2013/01/24 21:17:152013/01/24 21:17:15
3.4.6.6.
3.4.6.7.
2010 161
8
161
(μg/kg)
(μg/kg) (μg/kg) (μg/kg)
(μg/kg)
10 0.5 8 < 0.5 2.4 0.55 -
207
13-01-276_本文_MK.indd 20713-01-276_本文_MK.indd 207 2013/01/24 21:17:162013/01/24 21:17:16
3.4.6.8.
21 30 162
162
(mg/kg)
(mg/kg) (mg/kg) (mg/kg)
(mg/kg)
30 0.004 0 0.011
(0.0002)0.303
(0.019)
0.065
(0.004) 0.042
(0.004)
mg/L
3.4.7.1. 16
208
13-01-276_本文_MK.indd 20813-01-276_本文_MK.indd 208 2013/01/24 21:17:162013/01/24 21:17:16
3.4.6.8.
3.4.7.
3.4.7.1. 16
DON NIV20 20 40 163
DON NIV
163
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
DON 20 0.05 20 - - 0.02 -NIV 20 0.05 20 - - 0.02 -
18 50 164 9
0.006 mg/kg
16
209
13-01-276_本文_MK.indd 20913-01-276_本文_MK.indd 209 2013/01/24 21:17:162013/01/24 21:17:16
164
(mg/kg)
(mg/kg) (mg/kg) (mg/kg)
(mg/kg)
30 0.004 26 < 0.004 0.006 0.003 -
10 0.004 10 - - 0.003 -
10 0.004 10 - - 0.003 -
3--1,2- 3-MCPD 16
17 104 18 19 120157 165
91
3-MCPD
165 3-MCPD 16
(mg/kg)
(mg/kg) (mg/kg) (mg/kg) (mg/kg)
104 0.004 93 < 0.004 0.008 0.003 -
120 0.004 1 < 0.004 7.8 0.21 0.016
17
6 8
18 19
210
13-01-276_本文_MK.indd 21013-01-276_本文_MK.indd 210 2013/01/24 21:17:162013/01/24 21:17:16
(mg/kg)
(mg/kg) (mg/kg) (mg/kg) (mg/kg)
148 0.004 0 0.004 0.14 0.047 0.049
9 0.004 0 0.10 44 8.4 2.7
17 18 3-MCPD215
430 166 1673-MCPD 1,3-
-2- 1,3-DCP
3-MCPD
1,3-DCP 7 3-MCPD
166
17
(mg/kg)
(mg/kg) (mg/kg) (mg/kg) (mg/kg)
3-MCPD40 0.004 0 0.019 33 6.1 3.6
3-MCPD40 0.004 0 0.014 17 2.3 1.5
1,3-DCP40 0.004 30 < 0.004 0.070 0.007 -
1,3-DCP40 0.004 33 < 0.004 0.022 0.003 -
211
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167
18
(mg/kg)
(mg/kg) (mg/kg) (mg/kg) (mg/kg)
3-MCPD81 0.004 0 0.009 57 6.6 2.2
3-MCPD54 0.004 0 0.010 20 2.2 0.83
1,3-DCP81 0.004 66 < 0.004 1.0 0.020 -
1,3-DCP54 0.004 48 < 0.004 0.023 0.003 -
18 3-MCPD 168
3-MCPD 20 6
168 3-MCPD 18
(mg/kg)
(mg/kg) (mg/kg) (mg/kg) (mg/kg)
31 0.004 0 0.009 0.30 0.099 0.053
50 0.004 0 0.13 57 11 3.3
21103
169
212
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3-MCPD 18 1/10
1/5
169 3-MCPD 21
(mg/kg)
(mg/kg) (mg/kg) (mg/kg) (mg/kg)
3-MCPD48 0.004 0 0.017 10 1.3 0.14
3-MCPD55 0.004 0 0.009 4.6 0.49 0.069
19 50 170
170
(μg/kg)
(μg/kg) (μg/kg) (μg/kg)
(μg/kg)
30 0.4 0 16 100 40 37
20 0.4 0 19 100 45 43
213
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3.4.7.2.
DON NIV20 20 40 171
DON NIV
171
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
DON 20 0.06 20 - - 0.03 -NIV 20 0.03 20 - - 0.02 -
18 50 172
172
(mg/kg)
(mg/kg) (mg/kg) (mg/kg)
(mg/kg)
30 0.020 30 - - 0.008 -
10 0.020 10 - - 0.005 -
10 0.020 10 - - 0.017 -
214
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3.4.7.2.
1920 60 173
173
(μg/kg)
(μg/kg) (μg/kg) (μg/kg)
(μg/kg)
27 1.1 0 2.0 51 16 11
33 1.3 0 87 770 240 210
215
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3.4.7.3.
19 100 174
17
1
174
(mg/kg)
(mg/kg) (mg/kg) (mg/kg)
(mg/kg)
80 0.012 1 < 0.012 0.58 0.11 0.078
10 0.012 7 < 0.012 0.067 0.021 -
10 0.012 0 0.022 0.12 0.043 0.033
3.4.7.4.
216
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3.4.7.3.
3.4.7.4.
20 10 175
175
(μg/kg)
(μg/kg) (μg/kg) (μg/kg)
(μg/kg)
10 0.5 0 4.3 13 8.8 10
217
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3.4.7.5.
19 20 176
8
176
(μg/kg)
(μg/kg) (μg/kg) (μg/kg)
(μg/kg)
20 1.3 3 < 1.3 58 25 31
3.4.8.1.
218
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3.4.7.5.
3.4.8.
3.4.8.1.
22 112 177
177
(mg/kg)
(mg/kg) (mg/kg)
(mg/kg) (mg/kg)
46 30 46 - - 10 - 18 30 18 - - 10 -
48 30 48 - - 10 -
19 20 90 178
219
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178
(μg/kg)
(μg/kg) (μg/kg) (μg/kg)
(μg/kg)
10 1.0 0 7.4 54 29 31
30 1.3 1 < 1.3 79 9.3 3.5
15 1.3 0 11 140 69 67
5 1.3 0 18 130 73 87
10 1.3 0 7.7 44 19 15
20 1.3 0 3.2 300 76 72
3.4.8.2.
220
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3.4.8.2.
19 100 179
96
1
179
(mg/kg)
(mg/kg) (mg/kg) (mg/kg)
(mg/kg)
80 0.012 3 < 0.012 0.084 0.034 0.026
10 0.012 6 0.016 0.035 0.015 -
10 0.012 0 0.014 0.064 0.043 0.047
19 100 180
221
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180
(μg/kg)
(μg/kg) (μg/kg) (μg/kg)
(μg/kg)
100 1.3 0 4.5 140 42 36
3.4.8.3.
222
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3.4.8.3.
19 100 181
181
(μg/kg)
(μg/kg) (μg/kg) (μg/kg)
(μg/kg)
40 1.3 0 8.7 86 30 24
40 1.3 0 3.6 140 24 19
20 0.4 5 < 0.4 30 4.4 2.6
223
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4.1.
2 kg
4 23
1
DON, NIV
20 20 4 1 19 14729/
84/16 DON 3-Ac-DON 15-Ac-DON NIV4-Ac-NIV LC/MS
GC/MS
20 http://www.famic.go.jp/ffis/feed/bunseki/bunsekikijun.html
224
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20 4 1 19 147295 6.2
/ 84/16 LC/MS
A
AOAC Official Method 2000.03 / (60/40) A
HPLC-FL
21 34 12 28370
21 http://www.nihs.go.jp/dmb/paturin.html
225
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4.2.
4.2.1.
45 10
23 475200 g
3 ~ 15
1 kg
1 4
4 5 2200 g
250 g 5
2 kg 1 25 g 250 g
10 1 kg 1 25 g 1 kg
226
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300 1 200 g 10
34 12 28 370ICP-OES
ICP-MS
10 50 g
AOAC Official Method 982.23 DICP-OES
ICP-MS
AOAC Official Method 999.11
227
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4.2.2.
1 kg
1 kg
5 g 350 500 °C2.5 mg/L 0.5 mL 25 mL
ICP-MS
AOAC Official Method 972.25 999.11
228
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AOAC Official Method 971.21
AOAC Official Method 963.21 AOAC Official Method 986.15
HPLC-ICPMS 22
22 M.H.Nagaoka et al, "Evaluation of a Nitric Acid-based Partial-digestion Method for
Selective Determination of Inorganic Arsenic in Rice", J.Food Hyg. Soc. Jpn. Vol.49, No.2, pp.95-99, .April 2008.
229
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4.2.3.
300-500 g 200-300 g
1.0 g /60% 1/1 6 mL 5 mL200 °C
100 mL 182
182
HG-200
253.7 nm
1 5 g 9 mol/L 5 mL 35 mL10
2,500 rpm 10 20%10 mL 2
230
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10 mL2,500 rpm 10 6 mL
0.5 mL 4 mL 1020% 10 mL 2
183
183
6890N (Agilent Technologies, Inc.)
ULBON HR-Thermon-Hg 0.53 mm i.d. × 15 m
150 °C 200 °C 200 °C
10 mL/
ECD
1 μL
231
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4.3.
1 4 45 200 g
1 L 1 kg
1 1 kg 1 kg
40 1
10
1 kg 1
48 7 4620 2
232
13-01-276_本文_MK.indd 23213-01-276_本文_MK.indd 232 2013/01/24 21:17:192013/01/24 21:17:19
22 23 184
184
pg/g-
PCDD 4 -p- 0.003
5 -p- 0.003
6 -p- 1,2,3,4,7,8-
6 -p- 1,2,3,6,7,8-
6 -p- 1,2,3,7,8,9-
0.007 0.005 0.004
7 -p- 0.005
8 -p- 0.01
PCDF 4 0.003
5 1,2,3,7,8-
5 2,3,4,7,8-
0.003 0.002
6 1,2,3,4,7,8-
6 1,2,3,6,7,8-
6 1,2,3,7,8,9-
6 2,3,4,6,7,8-
0.008 0.004 0.007 0.006
7 1,2,3,4,6,7,8-
7 1,2,3,4,7,8,9-
0.004 0.005
8 0.01
Co-PCB Co-PCBs #77 0.01
Co-PCBs #81 0.005
Co-PCBs #126, #129 0.003
Co-PCBs #105 0.09
Co-PCBs #114, #156, #167 0.1
Co-PCBs #118 0.2
Co-PCBs #123, #189 0.08
Co-PCBs #157 0.06
0
23 JIS K0312 (2005)
7.5.2
233
13-01-276_本文_MK.indd 23313-01-276_本文_MK.indd 233 2013/01/24 21:17:192013/01/24 21:17:19
185 186
185
pg/g )
PCDD 4 -p- 0.005 0.01
5 - p - 0.005 0.01
6 - p - 0.01 0.02
7 - p - 0.01 0.02
8 - p - 0.02 0.05
PCDF 4 0.005 0.01
5 0.005 0.01
6 0.01 0.02
7 0.01 0.02
8 0.02 0.05
Co-PCB Co-PCBs 0.1 0.1
Co-PCBs 1 1
0
186 pg/g
PCDD 4 -p- 0.01
5 -p- 0.01
6 -p- 0.02
7 -p- 0.02
8 -p- 0.05
PCDF 4 0.01
5 0.01
6 0.02
234
13-01-276_本文_MK.indd 23413-01-276_本文_MK.indd 234 2013/01/24 21:17:192013/01/24 21:17:19
7 0.02
8 0.05
Co-PCB Co-PCBs 0.1
Co-PCBs 1
0
235
13-01-276_本文_MK.indd 23513-01-276_本文_MK.indd 235 2013/01/24 21:17:202013/01/24 21:17:20
4.4.
6
6 23
86
236
13-01-276_本文_MK.indd 23613-01-276_本文_MK.indd 236 2013/01/24 21:17:202013/01/24 21:17:20
3 g 100 mL -d3 1 μg20 mL 1
10 2,000 rpm 10 40 mL Sep-Pak® C18
Sep-Pak® AC-2 5 mL/ Sep-Pak® AC-2
Sep-Pak® AC-2
5 mL5 %(w/v) 0.1 mL
1 mL5 %(w/v) 0.1 mL 0.3 mol/L
0.1 mL 40 °C 2
5 mL 2 g2 mL
1 μL GC/MS GC/MS 187
187 GC/MS
6890/5973N (Agilent Technologies, Inc.)
16 SPB-5 (sigma-aldrich Company SUPELCO division)
0.25 mm i.d. × 30 m, 0.25 μm 17 19
DB-5 (Agilent Technologies, Inc.)
0.25 mm i.d. × 30 m, 0.25 μm
16 300 °C
237
13-01-276_本文_MK.indd 23713-01-276_本文_MK.indd 237 2013/01/24 21:17:202013/01/24 21:17:20
40 °C 2 20 °C/ 300 °C 17 19
250 °C 40 °C 2 20 °C/ 300 °C
1 mL/
EI
230 °C 70 eV
(m/z) 251, 234
254
1 g 100 mL -d3 1 μg20 mL 1
3 g 100 mL -d3 1 μg20 mL 1
10 2,000 rpm 1040 mL Sep-Pak® C18
Sep-Pak® AC-2 5 mL/Sep-Pak® AC-2
Sep-Pak® AC-2 5 mL
10 %(w/v) 0.1 mL
238
13-01-276_本文_MK.indd 23813-01-276_本文_MK.indd 238 2013/01/24 21:17:202013/01/24 21:17:20
30 g 70 mL -d3 1 μg1
10 g 100 mL -d3 2 μg1
10 2,000 rpm 10 20 mL Extrelut® NT 20 30
150 mL 10 %(w/v)
0.1 mL40 mL Sep-Pak® C18 Sep-Pak® AC-2 5 mL/
Sep-Pak® AC-2
10 g -d3 0.4 μg20 mL Extrelut®NT 20
2.0 g 100 μg/mL - 1-13C20 μL 40 mL 2
2,600 rpm 10 50 mL
10 mL 5 23,000 rpm 10
239
13-01-276_本文_MK.indd 23913-01-276_本文_MK.indd 239 2013/01/24 21:17:202013/01/24 21:17:20
5 mol/L pH 1 10 g0.1 mol/L 6 mL4~10°C 90
1 mol/L10 mL 5
2 3,000 rpm 10
10% 2 mLSep-Pak® PLUS 10 mL
10%1 mL 210% 6 mL 20%
15 mL0.5 mL 20 μL
2 μL GC/MS
GC/MS 188
188 GC/MS
GCMS-QP2010 Plus
TC-WAX J&W Scientific 0.25 mm i.d. × 30 m, 0.25 μm
J&W Scientific 0.25 mm i.d. × 2 m
250 °C 50 °C 1 15 °C/ 240 °C 11.3
240 °C
1 mL/
EI
70 eV
(m/z) 149, 151
150, 152
240
13-01-276_本文_MK.indd 24013-01-276_本文_MK.indd 240 2013/01/24 21:17:202013/01/24 21:17:20
10 g 1 ng/mL - 1,2,3-13C3
30 μL 15 mL 50 mL
10 mL 3 15 mL 40 °C
10 mL 2 1 3,000 rpm 5
20 mL 1 3,000 rpm 5
15 mL
Bond Elut® C18 Bond Elut® SCX10 mL 10 mL
5 mL2 mL 2 10
mL 10 μL -
LC/MS/MS LC/MS/MS 189
189 LC/MS/MS
Alliance 2695 + Quattro micro Waters
HPLC
SunFire C18 Waters 2.1 mm i.d. ×150 mm, 3.5 μm
Develosil C30-UG-5 2.0 mm i.d. × 150 mm
40 °C
/ 0.1% 10/90
0.2 mL/
241
13-01-276_本文_MK.indd 24113-01-276_本文_MK.indd 241 2013/01/24 21:17:202013/01/24 21:17:20
MS/MS
ESI 3 kV
2 V RF 0.1 V
120 °C 450 °C 50 L/h 600 L/h
(m/z) 71.7 54.8
74.8 57.9
1.0 g 1 ng/mL 1,2,3-13C3
50 μL 0.1 1 mL 9 mL 20 12,000 rpm 15
5 mL 2 mL9,000 rpm 4
0.45 μm Oasis® HLB 3.5 mL 3.5 mL
1.5 mL0.5 mL 1.5 mL
0.5 mL 2.5 mL 2.5 mL
Bond Elut® AccuCatOasis® HLB 1.0 mL
10 μL -
LC/MS/MS LC/MS/MS 190
242
13-01-276_本文_MK.indd 24213-01-276_本文_MK.indd 242 2013/01/24 21:17:202013/01/24 21:17:20
190 LC/MS/MS
LC/MS/MS API4000 QTRAP AB SCIEX
HPLC Atlantis dC18 Waters 2.1 mm i.d. ×150 mm, 3 μm
Cartridge Gurad Column Waters 2.1 mm i.d. × 20 mm
40 °C
0.1% / 99.5/0.5
0.2 mL/
MS/MS
ESI 5500V
600 °C 51 V 46 V 17 V
(m/z) 72 55
75 58
1.0 g 10 μg/mL 1,2,3-13C3
50 μL 15 mL 20 mL NH2 1.5g10 3,000 rpm 5
Sep-Pak® tC18 Sep-Pak®
AC-2 15 mL 15 mL15 mL 15 mL
1 15 mL 0.5 mL
40°C 1 mL
10 μL -LC/MS/MS LC/MS/MS 191
243
13-01-276_本文_MK.indd 24313-01-276_本文_MK.indd 243 2013/01/24 21:17:212013/01/24 21:17:21
191 LC/MS/MS
LC: ACQUITY UPLC Waters MS/MS: 3200 Q Trap Applied Biosystems
HPLC ACQUITY UPLC BEH C18 Waters 2.1 mm i.d. ×100 mm, 1,7 μm
55 °C
Solvent A: 5 mM Solvent B:
0 A/B 90/10 3 A/B 90/10 6 A/B 0/100 14 A/B
0/100
0.15 mL/
MS/MS
ESI 5500V
300 °C 20.00
3.00 70.00 PSI
AUX 80.00 PSI 51 V 46 V 15 V 27 V 25 V
(m/z) 72.1 55.0 72.1 44.1
75.07 58.1 75.07 45.1
3-MCPD
244
13-01-276_本文_MK.indd 24413-01-276_本文_MK.indd 244 2013/01/24 21:17:212013/01/24 21:17:21
4.5.
4.5.1. 3- -1,2- 3-MCPD
4 g 3-MCPD-d5 0.8 μg
10 mL Extrelut® NT 2030 150 mL 3-MCPD
4 mL1 mL 2 % (w/v) 0.1 mL
5 Sep-Pac® 10 mL
: 20:80 15 mL 2 3-MCPD
1 mL 1 μL GC/MS GC/MS 192
192 3-MCPD GC/MS
16 18 6890/5973 (Hewlett Packard Co.)
21 6890N/5973B InertXL (Agilent Technologies Inc.)
16 18 DB-5 MS (Agilent Technologies, Inc.)
0.25 mm i.d. × 30 m, 0.25 μm 21
DB-5 MS +DG (Agilent Technologies Inc.)
0.25 mm i.d. × 30 m, 0.25 μm
245
13-01-276_本文_MK.indd 24513-01-276_本文_MK.indd 245 2013/01/24 21:17:212013/01/24 21:17:21
16 18 220 °C
70 °C 1 15 °C/ 240 °C 21
240 °C 70 °C 1 15 °C/ 280 °C
1 mL/
EI
230 °C 70 eV
m/z 3-MCPD 196, 147 150
1,3-DCP
246
13-01-276_本文_MK.indd 24613-01-276_本文_MK.indd 246 2013/01/24 21:17:212013/01/24 21:17:21
4.5.2. 1,3- -2- 1,3-DCP
4 g 20 mL 8 g
4 mL 1
2 μL GC/MS GC/MS 193
193 1,3-DCP GC/MS
6890N/5973 inert (Agilent Technology Inc.)
DB-WAX (Agilent Technologies, Inc.)
0.25 mm i.d. × 30 m, 0.25 μm
220 °C 70 °C 1 10 °C / 240 °C
1 mL/
EI
230 °C 70 eV
m/z 79, 81
247
13-01-276_本文_MK.indd 24713-01-276_本文_MK.indd 247 2013/01/24 21:17:212013/01/24 21:17:21
4.6. PAHs
1
10 g 20 g 0.02 mg/L
5- -d3 0.002 mg/L 0.5 mL 1 mol/L 50 mL
100 mL 15 30
1:1 20 mL 50 mL50 mL 10
50 mL
50 mL30 25 mL
20 g5 ml 25 °C
5 g 99:1
30 mL99:1 60 mL 5 ml
25 °C 0.05 mg/L 0.5 mL0.5 mL
1 μL GC/MSGC/MS 194
248
13-01-276_本文_MK.indd 24813-01-276_本文_MK.indd 248 2013/01/24 21:17:212013/01/24 21:17:21
PAHs
[a] -d12 [b] -d12 [k] -d12
[k] [j] [g,h,i] -d12 [a] -d12 -d12 [a,h] -d14 [a,i] -d14
[a,l] [a,e] [a,h][a,i]
[1,2,3-c,d] -d12 5- -d3
p- -d14
194 PAH GC/MS
GC Agilent 6890 Agilent Technologies, Inc. MS JMS-700D
DB-17MS J&W Scientific 0.25 mm i.d. × 30 m 0.25 μm
DB-5 MS J&W Scientific 0.25 mm i.d. × 60 m 0.25 μm
270 °C
50 °C 2 20 °C / 220 °C 0 5°C/ 280 °C 0 15 °C / 340 °C 10
2
50 °C 1 20 °C/ 220 °C 0
249
13-01-276_本文_MK.indd 24913-01-276_本文_MK.indd 249 2013/01/24 21:17:222013/01/24 21:17:22
7 °C / 320 °C 7 20 °C / 340 °C 12
195
1.0 mL/
EI
310 °C 38 eV
195
250
13-01-276_本文_MK.indd 25013-01-276_本文_MK.indd 250 2013/01/24 21:17:222013/01/24 21:17:22
195 PAH GC/MS
[a] 1 228.0939 229.0973
[b] 1 216.0939 217.0973
[c] 1 216.0939 217.0973
[b] 1 252.0939 253.0973
[j] 1 252.0939 253.0973
[k] 1 252.0939 253.0973
[g,h,i] 1 276.0939 277.0973
[a] 1 252.0939 253.0973
1 228.0939 229.0973
[a,h] 2 278.1096 279.1129
[a,e] 2 302.1096 303.1129
[a,h] 2 302.1096 303.1129
[a,i] 2 302.1096 303.1129
[a,l] 2 302.1096 303.1129
[1,2,3-c,d] 2 276.0939 277.0973
5- 1 242.1096 243.1129
[a] -d12 1 240.1692 241.1726
[b] -d12 1 264.1692 265.1726
[k] -d12 1 264.1692 265.1726
[g,h,i] -d12 1 288.1692 289.1726
[a] -d12 1 264.1692 265.1726
-d12 1 240.1692 241.1726
[a,h] -d14 2 292.1974 293.2008
[a,i] -d14 2 316.1974 317.2008
[1,2,3-c,d] -d12 2 288.1692 289.1726
5- -d3 1 245.1284 246.1317
p- -d14 1,2 244.1974 -
251
13-01-276_本文_MK.indd 25113-01-276_本文_MK.indd 251 2013/01/24 21:17:222013/01/24 21:17:22
4.7.
2 g 0.2 mol/L 20 mL 12 mL
5 mL 100 μg/mL4 mL 30 %
(w/v) 0.7 mL 1 %(w/v)
- 5 mL 37 °C 14 184 mL 10
2 mL HPLC-UV HPLC-UV 196
196 HPLC-UV
LC-10ADXR
Shim-pack XR-ODS 3.0 mm i.d. × 75 mm
45 °C
/ /0.01 mol/L 2/3/2
1.0 mL/
254 nm
1.0 μL
252
13-01-276_本文_MK.indd 25213-01-276_本文_MK.indd 252 2013/01/24 21:17:222013/01/24 21:17:22
4.8.
86 1 2
1
4 g 80 °C 30 1 4 g
10 mL
5 μg/mL -d4 10 μL
HS-GC/MS 197 198
197 -
19 7694 Agilent Technologies, Inc. 20 G1888 Agilent Technologies, Inc.
45 °C 60 °C
30
100 °C
130 °C
0.3
253
13-01-276_本文_MK.indd 25313-01-276_本文_MK.indd 253 2013/01/24 21:17:222013/01/24 21:17:22
198 GC/MS
6890N/5973N (Agilent Technology Inc.)
DB-WAX (Agilent Technologies, Inc.)
0.25 mm i.d. × 60 m, 0.25 μm
1:40
200 °C 19 40 °C 20 40 °C 10 15 °C/
200 °C 5
) 1 mL/
EI
230 °C 70 eV
m/z 68, 39
72
Yoshida I, Isagawa S, Kibune N, Hamano-Nagaoka M, Maitani T, Rapid and improved determination of furan in baby food and infant formulas by headspace GC/MS. Journal of the Food Hygienic Society of Japan 48, 83-89(2007)
254
13-01-276_本文_MK.indd 25413-01-276_本文_MK.indd 254 2013/01/24 21:17:222013/01/24 21:17:22
4.9.
1 kg5 2 kg
24 17 1 24 01240012 3
10 1
70 120 %
24 http://www.mhlw.go.jp/topics/bukyoku/iyaku/syoku-anzen/zanryu3/siken.html
255
13-01-276_本文_MK.indd 25513-01-276_本文_MK.indd 255 2013/01/24 21:17:222013/01/24 21:17:22
5.1.
1950
120 °C
A A
A
256
13-01-276_本文_MK.indd 25613-01-276_本文_MK.indd 256 2013/01/24 21:17:232013/01/24 21:17:23
0.4 mg/kg
3-MCPD 1,3-DCP
3- -1,2- 3-MCPD
1,3- -2-1,3-DCP
3-MCPD 1,3-DCP
3-MCPD 2008 3-MCPD
257
13-01-276_本文_MK.indd 25713-01-276_本文_MK.indd 257 2013/01/24 21:17:232013/01/24 21:17:23
PAH: Polycyclic Aromatic Hydrocarbon PAH
PAH
PAHs[a] BaP BaP
PAH
PAH
258
13-01-276_本文_MK.indd 25813-01-276_本文_MK.indd 258 2013/01/24 21:17:232013/01/24 21:17:23
DON NIV DON NIV
DON NIV
DON NIV
DON NIV
150 °C
259
13-01-276_本文_MK.indd 25913-01-276_本文_MK.indd 259 2013/01/24 21:17:232013/01/24 21:17:23
C
260
13-01-276_本文_MK.indd 26013-01-276_本文_MK.indd 260 2013/01/24 21:17:232013/01/24 21:17:23
261
13-01-276_本文_MK.indd 26113-01-276_本文_MK.indd 261 2013/01/24 21:17:232013/01/24 21:17:23
5.2.
mg 1 mg 1,000 1 g
m1,000 1
g
1 g 100 1 g
100 1 pg
1 pg 1 1 g p
1 1 ppm
ppm parts per million 1001 ppm 1 mg/kg
262
13-01-276_本文_MK.indd 26213-01-276_本文_MK.indd 262 2013/01/24 21:17:232013/01/24 21:17:23
GEMS/Food
25
6 6
1/2
GEMS/Food
WHO Global Environmental Monitoring System/ Food Contamination Monitoring and Assessment Programme 26
GEMS/Food
2
25 WHO, GEMS/Food, Instructions for Electronic Submission of Data on Chemical
Contaminants in Food and the Diet, 2003 26 http://www.who.int/foodsafety/chem/gems/en/
263
13-01-276_本文_MK.indd 26313-01-276_本文_MK.indd 263 2013/01/24 21:17:232013/01/24 21:17:23
%
70-120 %
2
Atomic Absorption Spectrometry, AAS
-
264
13-01-276_本文_MK.indd 26413-01-276_本文_MK.indd 264 2013/01/24 21:17:242013/01/24 21:17:24
Inductively Coupled Plasma, ICP
°C1 °C
ICP-Optical Emission Spectrometry ICP-OES
ICP
ICP-AES ICP - Atomic Emission Spectrometry
ICP - Mass Spectrometry, ICP-MS
ICP
GC
265
13-01-276_本文_MK.indd 26513-01-276_本文_MK.indd 265 2013/01/24 21:17:242013/01/24 21:17:24
HPLC
HPLC-UV
HPLC UV
UVHPLC
HPLC-FL
HPLC FL
fluorescence, FL
HPLC
MS
266
13-01-276_本文_MK.indd 26613-01-276_本文_MK.indd 266 2013/01/24 21:17:242013/01/24 21:17:24
1 2
HPLC GC
GC/MS
GC MS
LC/MS LC MS
- LC/MS/MS HPLC MS
2
HPLC 1 MS
22 MS
13C
267
13-01-276_本文_MK.indd 26713-01-276_本文_MK.indd 267 2013/01/24 21:17:242013/01/24 21:17:24
13C
13C
268
13-01-276_本文_MK.indd 26813-01-276_本文_MK.indd 268 2013/01/24 21:17:242013/01/24 21:17:24
GC/MS
269
13-01-276_本文_MK.indd 26913-01-276_本文_MK.indd 269 2013/01/24 21:17:242013/01/24 21:17:24
1 .................................................................................. 17 2 ............................................................. 18 3 ............................................................. 19 4 ....................................................................... 19 5 .................................................................................. 20 6 ............................................................................... 26 7 .................................................................... 27 8 ............................................................................... 28 9 ............................................................................... 30 10 .................................................................. 31 11 ............................................................................. 31 12 A ............................................... 33 13 ............................................................................. 34 14 .................................................................. 34 15 ............................................................................. 35 16 .................................................................. 38 17 .................................................................. 39 18 ..................................................................... 43 19 ........................................................... 43 20 ................................................... 44 21 ..................................... 44 22 ........................................................... 45 23 .................................................................. 46 24 ..................................................................... 47 25 ..................................................................... 48 26 ..................................................................... 52 27 ..................................................................... 53 28 ..................................................................... 57 29 ..................................................................... 58 30 ........................................................... 58 31 ..................................................................... 59 32 ..................................................................... 63 33 ........................................................... 63
270
13-01-276_本文_MK.indd 27013-01-276_本文_MK.indd 270 2013/01/24 21:17:242013/01/24 21:17:24
34 ..................................................................... 64 35 .......................................................... 68 36 ..................................................................... 68 37 ................................................... 70 38 .............................................................. 71 39 ......................................................................... 72 40 .......................................................... 73 41 .............................................................. 74 42 ................................................... 74 43 .............................................................. 75 44 .............................................................. 79 45 ...................................................... 79 46 ................................................................. 80 47 ......................................................................... 81 48 .............................................................. 81 49 ......................................................................... 82 50 .............................................................. 86 51 ................................................... 87 52 .............................................................. 87 53 ............................................................................ 89 54 ............................................................................ 91 55 ................................................................. 91 56 ..................................................................... 92 57 .............................................................. 93 58 ................................................................. 94 59 ..................................................................... 95 60 .......................................................... 96 61 ..................................................................... 97 62 .......................................................... 97 63 ..................................................................... 98 64 ................................................................... 103 65 ........................................................ 103 66 ................................................................... 104 67 ........................................................ 107 68 ................................................................... 107 69 .......................................................................... 111
271
13-01-276_本文_MK.indd 27113-01-276_本文_MK.indd 271 2013/01/24 21:17:242013/01/24 21:17:24
70 ....................................................................... 112 71 ....................................................................... 112 72 ................................................................... 117 73 ................................................................... 117 74 ................................................................... 122 75 ............................................................ 123 76 ............................................................ 123 77 ................................................................... 126 78 ....................................................................... 130 79 ....................................................................... 130 80 .............................................. 133 81 ............................... 133 82 ....................................................................... 134 83 ...................................... 138 84 ........................ 138 85 ................................................. 138 86 ........................................................................... 139 87 ....................................................................... 143 88 ............................................................ 143 89 ....................................................................... 144 90 ........................................................................... 147 91 ................................................................ 147 92 ........................................................................... 148 93 ................................................................ 148 94 ........................................................................... 149 95 ........................................................................... 151 96 ........................................................................... 151 97 ....................................................................... 156 98 ............................................................ 156 99 ....................................................................... 157 100 ................................. 161 101 .................. 161 102 ................................................................. 162 103 ............................................................................ 162 104 ................................................................. 165 105 .......................................................... 166
272
13-01-276_本文_MK.indd 27213-01-276_本文_MK.indd 272 2013/01/24 21:17:252013/01/24 21:17:25
106 ........................................................................ 167 107 ..................................................................... 167 108 ............................................................................ 168 109 ..................................................................... 169 110 ................................................................. 169 111 .......................................................... 170 112 ........................................................................ 172 113 ........................................................................ 173 114 .......................................................... 173 115 ..................................................................... 174 116 ................................................................. 175 117 ............................................................. 176 118 ............................................... 176 119 ..................................................................... 177 120 ............................................... 178 121 17 ................ 179 122 19 ................ 179 123 ............................................................................ 180 124 .......................................................... 181 125 ............................................................................ 182 126 ...................................................... 183 127 ............................................... 183 128 ................................................................. 184 129 ......................... 184 130 ...................................................... 184 131 .......................................................... 185 132 ........... 186 133 ............................................................. 187 134 PAH ......................................................................... 188 135 PAH ....................................................... 189 136 PAH ...................................................................... 190 137 PAH ...................................................................... 191 138 .............. 192 139 ............................................................. 193 140 ............................................... 193 141 16 ................... 194
273
13-01-276_本文_MK.indd 27313-01-276_本文_MK.indd 273 2013/01/24 21:17:252013/01/24 21:17:25
142 18-19 ............... 194 143 22 .................... 195 144 16 .................................. 196 145 21 ......... 196 146 ............................................ 197 147 ....................................................... 198 148 .......................................................... 199 149 ............................................... 200 150 ............................................... 200 151 ................................. 201 152 ............................................... 201 153 ........................................ 202 154 ........................................ 202 155 ................................. 203 156 .......................... 204 157 ................................................... 204 158 ................................................................. 205 159 .............................................................. 206 160 .......................................................... 206 161 ............................................................................ 207 162 ....................................................... 208 163 ..................................................................... 209 164 ....................................................... 210 165 3-MCPD 16 ........... 210 166 17
........................................................................................................................... 211 167 18
........................................................................................................................... 212 168 3-MCPD 18 ....... 212 169 3-MCPD 21 ........... 213 170 .................. 213 171 ............................................................................ 214 172 .............................................................. 214 173 ............................................................................ 215 174 .............................................................. 216 175 .................................... 217
274
13-01-276_本文_MK.indd 27413-01-276_本文_MK.indd 274 2013/01/24 21:17:252013/01/24 21:17:25
176 ...................................................... 218 177 ................................................................. 219 178 .......................................................... 220 179 ........... 221 180 .................................................. 222 181 ............................................................. 223 182 ...................................................... 230 183 ............................................... 231 184 ...................................................... 233 185 ...................................................... 234 186 ...................................................... 234 187 GC/MS ....................................................... 237 188 GC/MS ....................................................... 240 189 LC/MS/MS ................................................ 241 190 LC/MS/MS ................................................ 243 191 LC/MS/MS ................................................ 244 192 3-MCPD GC/MS .................................................................... 245 193 1,3-DCP GC/MS ..................................................................... 247 194 PAH GC/MS ........................................................................... 249 195 PAH GC/MS ............................... 251 196 HPLC-UV ............................................................ 252 197 - .......................................... 253 198 GC/MS ......................................................................... 254
275
13-01-276_本文_MK.indd 27513-01-276_本文_MK.indd 275 2013/01/24 21:17:252013/01/24 21:17:25
15 22
276（白）13-01-276_本文_MK.indd 27613-01-276_本文_MK.indd 276 2013/01/24 21:17:252013/01/24 21:17:25
15 22
24 10 31
100-8950
1-2-1 TEL 03-3502-8111
277 かくし13-01-276_本文_MK.indd 27713-01-276_本文_MK.indd 277 2013/01/24 21:17:252013/01/24 21:17:25
278（白）13-01-276_本文_MK.indd 27813-01-276_本文_MK.indd 278 2013/01/24 21:17:252013/01/24 21:17:25
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