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Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Nagano a , Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg Soumagne, Tsukasa Hori, Kouji Kakizaki a , Akira Sumitani, Junichi Fujimoto b , Hakaru Mizoguchi b and Akira Endo c EUVA, Japan a KOMATSU Ltd., Japan b Gigaphoton Inc., Japan c Waseda University, Japan Characterization and optimization of tin particle mitigation and EUV conversion efficiency in a laser produced plasma EUV light source [7969-100]

Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

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Page 1: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Confidential

SPIE Advanced Lithography 2011

Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai,Georg Soumagne, Tsukasa Hori, Kouji Kakizakia, Akira Sumitani, Junichi Fujimotob,Hakaru Mizoguchib and Akira Endoc

EUVA, JapanaKOMATSU Ltd., JapanbGigaphoton Inc., JapancWaseda University, Japan

Characterization and optimization of tin particle mitigation and EUV conversion efficiency in a laser produced plasma EUV light source

[7969-100]

Page 2: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 2

Outline

1. Introduction

2. Concept of Sn particle mitigation

3. Experimental setup

4. Experimental results

4-1. Sn fragment Imaging

4-2. LIF measurement of Sn neutrals

4-3. EUV CE measurements

5. Summary

Page 3: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 3

SOR,HHGX-LaserLPP/DPP

Laser Produced Plasma (LPP)Discharge Produced Plasma(DPP)

Mo/Si Mo/Si multilayer mirror multilayer mirror (R=70%)(R=70%)IF (Intermediate focus)IF (Intermediate focus)

EUVL based on High vacuum environment, Multilayer coated reflective opticsEUV Lithography system

Page 4: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 4

CO2 laser + Sn target+ Magnetic field plasma guiding

High power pulsed CO2 Laser

LPP EUV Light Source

High EUV powerLong collector mirror lifetimeEUV StabilityLow CoG / CoOReliability,・・・

Requirements for HVM EUV source

Sn target supply

Magnetic field plasma guiding

IF(Intermediate Focus)

EUVA LPP concept

Page 5: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 5

Outline

1. Introduction

2. Concept of Sn particle mitigation

3. Experimental setup

4. Experimental results

4-1. Sn fragment Imaging

4-2. LIF measurement of Sn neutrals

4-3. EUV CE measurements

5. Summary

Page 6: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 6

Characteristics of produced Sn particles (debris)

Fragments

Neutral atoms Ions

Velocity distribution

Ions Neutral atoms Fragments

Direction of expansion

Towards the laser incident direction All direction Same direction as

laser pulse

Velocity 10 - 100 km/s 5 - 40 km/s 0.01 - 0.5 km/s

Kinetic energy 60 - 6000 eV 15 - 980 eV -

Sn particles are classified into fragments, neutral atoms, ions

Page 7: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 7

Concept of Sn particle mitigationIn our LPP system, Sn particles are reduced to practical levelby the following method,

Mass limited Sn supplyFragments are vaporized and ionized by the main pulse laser.Ions are trapped by the magnetic field and collected.Residual Sn particles are cleaned.

Masslimitedtarget

Pre-pulse laser

Fragments

Main pulse laser

Neutral atoms

Ions

Vaporized

Ionized

Mag

netic

shi

ed

Cle

anin

g

Col

lect

or m

irror

Res

idua

lpar

ticle

s

Page 8: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 8

Subject of this workWe investigated behavior of Sn particles, and studied the optimization ofparticle mitigation condition with a compact EUV experimental system.

Fragments observation with a shadowgraph imaging (20 μm droplet target)

Neutral atoms imaging in a strong magnetic field by a laser induced fluorescence (LIF) method. (Planar target)

EUV Conversion Efficiency (CE) with smaller droplets are also optimized.

Page 9: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 9

Outline

1. Introduction

2. Concept of Sn particle mitigation

3. Experimental setup

4. Experimental results

4-1. Sn fragment Imaging

4-2. LIF measurement of Sn neutrals

4-3. EUV CE measurements

5. Summary

Page 10: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 10

Experimental setup of a compact EUV systemIt can simulate a same condition as our high-power EUV light source except for apulse repetition rate.

・System configurationDroplet generator, Pre-pulse laser, Main CO2 pulse laser, Magnetic fieldPulse repetition rate : 10Hz

・Measurement toolsShadowgraph for fragmentsLIF for neutral atomsEUV sensor(power, image, …)

Back

illuminator

CCD

cameraEUV

sensor

Drive laser

Sn dropletLIFcamera

EUV/DebrisMeasurementport

Corrector mirror

Intermediate focus

EUV/DebrisMeasurementport

Page 11: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 11

Outlook of the EUV system

Upper view

Drive laser

Droplet

Intermediate focus direction

LIFmeasurementEUV sensor

Size : 2 m X 3 m X 2 m

Page 12: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 12

Outline

1. Introduction

2. Concept of Sn particle mitigation

3. Experimental setup

4. Experimental results

4-1. Sn fragment Imaging

4-2. LIF measurement of Sn neutrals

4-3. EUV CE measurements

5. Summary

Page 13: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 13

Shadowgraph imaging for Sn fragment measurementTime resolution ~ 40 nsSpatial resolution ~ 6 μm60 degree observation angle to laser axis

Pre-pulse

Main pulse60°

Camera + Lens

Flash illuminator

100 μm

Example of shadowgraph image( 20μm droplet)

Page 14: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 14

a) without main-pulse laser

Pre-pulse irradiation Time

Main pulse laser/ EUV emission After EUV emission

b) with main-pulse laser

Sn fragments after laser irradiation

20 μm droplet, pre-pulse + main-pulse lasersFragments generated after pre-pulse irradiation.Quite a few fragments still remain without vaporization after EUV emission.

Wrong laser condition

Page 15: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 15

Sn fragments after laser irradiation

Fragments are vanished after EUV emission.We believe almost all of the fragments are vaporized, then probably ionized.

Appropriate laser condition

a) without main-pulse laser

Pre-pulse irradiation Time

Main pulse laser/ EUV emission After EUV emission

b) with main-pulse laser

Fragments are vanished

LASER

Page 16: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 16

Outline

1. Introduction

2. Concept of Sn particle mitigation

3. Experimental setup

4. Experimental results

4-1. Sn fragment Imaging

4-2. LIF measurement of Sn neutrals

4-3. EUV CE measurements

5. Summary

Page 17: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 17

Laser induced fluorescence (LIF) imaging for Sn atoms

λfluorescence

0 cm-1

λabsorption

5p6s3Po1

5p2 3P0

5p2 3P1

286.3 nm 317.5 nm

Energy level of Sn atom

Advantages

Spectrally selective pumping and observation

High sensitivity

Cross sectional imaging with a sheet laser beam

Page 18: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 18

laser

Surface of a Sn plate

a) Without the magnetic field b) With the magnetic field

B-field

Isotropic expansion Sn atoms strongly converge on the direction of the magnetic field.

2D LIF image of Sn atom distribution at 1 μs after laser irradiation

Sn neutral distribution under strong magnetic fieldPlanar target + pre-pulse laser with / without magnetic fieldMagnetic field helps guiding the Sn particles of not only the charged particle

but also the neutral atom.

Page 19: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 19

Outline

1. Introduction

2. Concept of Sn particle mitigation

3. Experimental setup

4. Experimental results

4-1. Sn fragment Imaging

4-2. LIF measurement of Sn neutrals

4-3. EUV CE measurements

5. Summary

Page 20: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 20

Droplet size vs. EUV CE

Pre-pulse laser irradiation is a key parameter for a higher EUV CE.

EUV CE reached to 3.4% for a 20 μm droplet by optimizing the pre-pulse laser conditions.

0

0.5

1

1.5

2

2.5

3

3.5

4

10 15 20 25 30 35 40 45 50

EUV

CE

(%)

Droplet diameter (μm)

Without a pre-pulse irradiation

With a pre-pulse irradiation

With a Improved pre-pulse irradiation

Page 21: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 21

0

0.2

0.4

0.6

0.8

1

1.2

0 20 40 60 80 100 120 140

EUV

cle

an p

ulse

ene

rgy

(mJ)

CO2 pulse energy (mJ)

100

120

80

60

40

20

0EUV

cle

an p

ower

ass

umin

g a

100k

Hz

oper

atio

n (W

)

EUV CE doesn’t saturate at leastup to 134mJ CO2 laser input.

Clean EUV power of 100 W isexpected for our developing system with a pulse repletion rate of 100kHz.

CO2 laser pulse energy vs. EUV pulse energy

Page 22: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 22

SummaryThe optimization of tin debris mitigation and EUV CE with the compact EUV generation system is presented.

1. Sn fragments generated from the 20 μm diameter droplet was vaporized almost entirely by the laser optimization.

2. Sn neutrals generated after the pre-pulse irradiation converge to themagnetic field. (planar target)The magnetic field is beneficial to the Sn particles guiding of not only the ions but also the neutrals.

3. No EUV CE degradation even for 20 μm diameter dropletMaximum EUV CE of 3.4% for 20 μm diameter dropletClean EUV power of 100 W is expected for our developing system.

Page 23: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg

Copyright 2011 GIGAPHOTON INC. all rights reserved. 2 Mar. 2011 SPIE Advanced Lithography, [7969-100] 23

Acknowledgement

A part of this work was supported by the New Energy andIndustrial Technology Development Organization (NEDO),Japan.

Page 24: Characterization and optimization of tin particle …...Confidential SPIE Advanced Lithography 2011 Tatsuya Yanagida, Hitoshi Naganoa, Yasunori Wada, Takayuki Yabu, Shinji Nagai, Georg