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*Total CBD = CBD + CBDA x 0.877
CERTIFICATE OF ANALYSISOrder #: 30604Order Name: GranddaddyPurple 350mgBatch#: GDP9135Completed: 05/06/2019
Arise Bioscience Inc.4855 Technology Way Suite 500Boca Raton Florida, 33431(866) 407-1164
Sample
0.000% D9-THC
33.059% Total CBD
Cannabinoids Testcannabinoids weight(%) mg/gDELTA-9-TETRAHYDROCANNABINOL D9-THC N/D N/DTETRAHYDROCANNABINOLIC ACID THCA N/D N/DCANNABIDIOL CBD 33.059% 330.593CANNABIDIOLIC ACID CBDA N/D N/DCANNABIDIVARIN CBDV 0.099% 0.987CANNABICHROMENE CBC 0.401% 4.010CANNABINOL CBN 0.281% 2.811CANNABIGEROL CBG 0.045% 0.449CANNABIGEROLIC ACID CBGA N/D N/DDELTA-8-TETRAHYDROCANNABINOL D8-THC N/D N/DTETRAHYDROCANNABIVARIN THCV N/D N/D
TOTAL D9-THC N/D N/DTOTAL CBD* 33.059% 330.593TOTAL CANNABINOIDS 33.885% 338.850
4001 SW 47th Avenue Suite 207Davie, FL [email protected]
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.
CERTIFICATE OF ANALYSISOrder #: 30604Order Name: GranddaddyPurple 350mgBatch#: GDP9135Completed: 05/06/2019
Arise Bioscience Inc.4855 Technology Way Suite 500Boca Raton Florida, 33431(866) 407-1164
TERPENES: TOTAL (1.666%)GC-Headspace - Shimadzu GCMS QP2020 with HS20
Terpene Results (%)(1R)-ENDO-(+)-FENCHYL ALCOHOL 0.004%ALPHA-PINENE 0.059%BETA-MYRCENE 0.304%CAMPHOR 0.004%CARYOPHYLLENE 0.067%CARYOPHYLLENE OXIDE 0.010%HUMULENE 0.371%LIMONENE 0.046%LINALOOL 0.793%MENTHOL 0.002%TERPINOLENE 0.006%
Terpenes Breakdown
Top Terpenes Results:
Tested for but not present:
3-CARENE, ALPHA-BISABOLOL, ALPHA-CEDRENE, ALPHA-TERPINENE, ALPHA.-PHELLANDRENE, BETA-PINENE, BORNEOL (MIX OF ISOMERS), CAMPHENE, CAMPHOR (MIX OF ISOMERS), CEDROL,CIS-BETA-OCIMENE, CIS-NEROLIDOL, EUCALYPTOL, FENCHONE, FENCHONE (ISOMER), GAMMA-TERPINEOL, GAMMA.-TERPINENE, GERANIOL, GERANYL ACETATE, GUAIOL, ISOBORNEOL,ISOPULEGOL, NEROL, PULEGONE, SABINENE, SABINENE HYDRATE, TERPINEOL (MIX OF ISOMERS), TRANS-BETA-OCIMENE, TRANS-NEROLIDOL, VALENCENE
4001 SW 47th Avenue Suite 207Davie, FL [email protected]
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.
N/D = Not Detected, B/LOQ = Below LOQ Level, B/LOD = Below LOD Level
CERTIFICATE OF ANALYSISOrder #: 30604Order Name: GranddaddyPurple 350mgBatch#: GDP9135Completed: 05/06/2019
Arise Bioscience Inc.4855 Technology Way Suite 500Boca Raton Florida, 33431(866) 407-1164
PESTICIDE ANALYSIS:GC QQQ - Shimadzu GCMS-TQ8040
Pesticide Action Level(ppm)
Results(ppm)
LOQ(ppm)
LOD(ppm)
ABAMECTIN B1A 0.100 N/D 0.003 0.001ACEPHATE 0.100 N/D 0.003 0.001ACEQUINOCYL 0.100 N/D 0.003 0.001ACETAMIPRID 0.100 N/D 0.003 0.001ALDICARB 0.100 N/D 0.003 0.001AZOXYSTROBIN 0.100 N/D 0.003 0.001BIFENAZATE 0.100 N/D 0.003 0.001BIFENTHRIN 3.000 N/D 0.003 0.001BOSCALID 0.100 N/D 0.003 0.001CARBARYL 0.500 N/D 0.003 0.001CARBOFURAN 0.100 N/D 0.003 0.001CHLORANTRANILIPROLE 10.000 N/D 0.003 0.001CHLORPYRIFOS 0.100 N/D 0.003 0.001CLOFENTEZINE 0.100 N/D 0.003 0.001DAMINOZIDE 0.100 N/D 0.003 0.001DIAZANON 0.100 N/D 0.003 0.001DICHLORVOS 0.100 N/D 0.003 0.001DIMETHOATE 0.100 N/D 0.003 0.001DIMETHOMORPH 2.000 N/D 0.003 0.001ETHOPROPHOS 0.100 N/D 0.003 0.001ETOFENPROX 0.100 N/D 0.003 0.001ETOXAZOLE 0.100 N/D 0.003 0.001FENHEXAMID 0.100 N/D 0.003 0.001FENOXYCARB 0.100 N/D 0.003 0.001FENPYROXIMATE 0.100 N/D 0.003 0.001FIPRONIL 0.100 N/D 0.003 0.001FLONICAMID 0.100 N/D 0.003 0.001FLUDIOXONIL 0.100 N/D 0.003 0.001HEXYTHIAZOX 0.100 N/D 0.003 0.001
PESTICIDE ANALYSIS:GC QQQ - Shimadzu LCMS-8060
Pesticide Action Level(ppm)
Results(ppm)
LOQ(ppm)
LOD(ppm)
IMAZALIL 0.100 N/D 0.003 0.001IMIDACLOPRID 5.000 N/D 0.003 0.001KRESOXIM-METHYL 0.100 N/D 0.003 0.001MALATHION 0.500 N/D 0.003 0.001METALAXYL 2.000 N/D 0.003 0.001METHIOCARB 0.100 N/D 0.003 0.001METHOMYL 1.000 N/D 0.003 0.001MEVINPHOS 0.100 N/D 0.003 0.001MYCLOBUTANIL 0.100 N/D 0.003 0.001NALED 0.100 N/D 0.003 0.001OXAMYL 0.500 N/D 0.003 0.001PACLOBUTRAZOL 0.100 N/D 0.003 0.001PERMETHRINS 0.500 N/D 0.003 0.001PHOSMET 0.100 N/D 0.003 0.001PIPERONYLBUTOXIDE
3.000 0.011 0.003 0.001
PRALLETHRIN 0.100 N/D 0.003 0.001PROPICONAZOLE 0.100 N/D 0.003 0.001PROPOXUR 0.100 N/D 0.003 0.001PYRETHRINS(PYRETHRIN I)
0.500 N/D 0.003 0.001
PYRIDABEN 0.100 N/D 0.003 0.001SPINETORAM 0.100 N/D 0.003 0.001SPINOSAD 0.100 N/D 0.003 0.001SPIROMESIFEN 0.100 N/D 0.003 0.001SPIROTETRAMAT 0.100 N/D 0.003 0.001SPIROXAMINE 0.100 N/D 0.003 0.001TEBUCONAZOLE 0.100 N/D 0.003 0.001THIACLOPRID 0.100 N/D 0.003 0.001THIAMETHOXAM 5.000 N/D 0.003 0.001TRIFLOXYSTROBIN 0.100 N/D 0.003 0.001
4001 SW 47th Avenue Suite 207Davie, FL [email protected]
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.
CERTIFICATE OF ANALYSISOrder #: 30604Order Name: GranddaddyPurple 350mgBatch#: GDP9135Completed: 05/06/2019
Arise Bioscience Inc.4855 Technology Way Suite 500Boca Raton Florida, 33431(866) 407-1164
RESIDUAL SOLVENTS:GC-Headspace - Shimadzu GCMS QP2020 with HS20
Residual Solvent Action Level (ppm) Results (ppm)ACETONE 5,000.000 N/DACETONITRILE 410.000 N/DBENZENE 1.000 N/DBUTANE 5,000.000 N/DCHLOROFORM 1.000 N/DDICHLOROETHANE 1.000 N/DDICHLOROMETHANE 1.000 N/DETHANOL 5,000.000 N/DETHYL ACETATE 5,000.000 N/DETHYL ETHER 5,000.000 N/DISOPROPYL ALCOHOL 5,000.000 N/DMETHANOL 3,000.000 N/DN-HEPTANE 5,000.000 N/DN-HEXANE 290.000 N/DPENTANE 5,000.000 N/DPROPANE 5,000.000 N/DTOLUENE 890.000 N/DTRICHLOROETHANE 1.000 N/DXYLENES 2,170.000 N/D
4001 SW 47th Avenue Suite 207Davie, FL [email protected]
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.
CERTIFICATE OF ANALYSISOrder #: 30604Order Name: GranddaddyPurple 350mgBatch#: GDP9135Completed: 05/06/2019
Arise Bioscience Inc.4855 Technology Way Suite 500Boca Raton Florida, 33431(866) 407-1164
Mycotoxin Analysis:LC-MS - Shimadzu LCMS-8060
Analyte Action Lvl (ppb) Results (ppb)AFLATOXIN B1 20.000 N/DAFLATOXIN B2 20.000 N/DAFLATOXIN G1 20.000 N/DAFLATOXIN G2 20.000 N/DOCHRATOXIN A 20.000 N/D
Heavy Metals Analysis:ICP-MS - Shimadzu ICPMS-2030
Metal Action Level (ppb) Result (ppb)ARSENIC (AS) 200.000 4.170CADMIUM (CD) 200.000 1.090MERCURY (HG) 100.000 10.400LEAD (PB) 500.000 7.600
*Lower Limit of Quantitation (LOQ) is 1 ppb
Microbial Analysis:PCR - Agilent AriaMX
Test Test MethodUsed Device Used LOD Allowable Amount Actual
Result Pass/Fail
STEC E. COLI* USP 61/62† ARIAMX PCR 2 COPIES OF DNA PRESENCE / ABSENTBELOW
LODPASS
SALMONELLA* USP 61/62† ARIAMX PCR 5 COPIES OF DNA PRESENCE / ABSENTBELOW
LODPASS
ASPERGILLUS USP 61/62† ARIAMX PCR ASP_LOD*** PRESENCE / ABSENTBELOW
LODPASS
† USP 61 (enumeration of bacteria TAC, TYM, and ENT/Coliform), USP 62 (identifying specific species E.coli Aspergillus etc) * STEC and Salmonella run as Multiplex *** Flavus = 2 Copies of DNA / Fumigatis = 2 Copies of DNA Niger = 20 Copies of DNA / Terrus = 10 copies of DNA
4001 SW 47th Avenue Suite 207Davie, FL [email protected]
Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.