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[This report shall not be reproduced except in full without the written authority of the Laboratory.]
28-JUN-18
Lab Work Order #: L2121059
Date Received:GOVERNMENT OF YUKON
P.O. Box 2703 (E-1)Whitehorse YT Y1A 2C6
ATTN: Miles HumeFINAL 05-JUL-18 17:27 (MT)Report Date:
Version:
Certificate of Analysis
ALS CANADA LTD Part of the ALS Group An ALS Limited Company
____________________________________________
Heather McKenzieAccount Manager
ADDRESS: 8081 Lougheed Hwy, Suite 100, Burnaby, BC V5A 1W9 Canada | Phone: +1 604 253 4188 | Fax: +1 604 253 6700
Client Phone: 604-253-4188
Job Reference: NOT SUBMITTEDProject P.O. #:
17-653378, 17-653379, 17-653380, 17-653381, 17-653382
C of C Numbers:
Legal Site Desc:
05-JUL-18 17:27 (MT)
Sample ID Description
Client ID
Sampled Date
Grouping Analyte
Sampled Time
ALS ENVIRONMENTAL ANALYTICAL REPORT
L2121059 CONTD....
2PAGE of
Version: FINAL
13
WATER
Water Water Water Water Water28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18
DF1 INTERMEDIATE
WING
BS1 INTERMEDIATE
WING
BS2 INTERMEDIATE
WING
BS3 INTERMEDIATE
WING
DF2 INTERMEDIATE
WING
L2121059-1 L2121059-2 L2121059-3 L2121059-4 L2121059-5
10:00 10:01 10:02 10:03 10:04
Lead (Pb)-Total (mg/L) 0.000406 0.00275 0.00112 0.0179 0.00810Total Metals
05-JUL-18 17:27 (MT)
Sample ID Description
Client ID
Sampled Date
Grouping Analyte
Sampled Time
ALS ENVIRONMENTAL ANALYTICAL REPORT
L2121059 CONTD....
3PAGE of
Version: FINAL
13
WATER
Water Water Water Water Water28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18
DF3 INTERMEDIATE
WING
*BS4 INTERMEDIATE
WING
BS5 INTERMEDIATE
WING
BS6 INTERMEDIATE
WING
CS1 INTERMEDIATE
WING
L2121059-6 L2121059-7 L2121059-8 L2121059-9 L2121059-10
10:05 10:06 10:07 10:08 10:09
Lead (Pb)-Total (mg/L) 0.00204 0.00937 0.00148 0.0216 0.00438Total Metals
05-JUL-18 17:27 (MT)
Sample ID Description
Client ID
Sampled Date
Grouping Analyte
Sampled Time
ALS ENVIRONMENTAL ANALYTICAL REPORT
L2121059 CONTD....
4PAGE of
Version: FINAL
13
WATER
Water Water Water Water Water28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18
CS2 INTERMEDIATE
WING
BS7 INTERMEDIATE
WING
BS8 INTERMEDIATE
WING (MAP)
CS3 INTERMEDIATE
WING
CF1 INTERMEDIATE
WING
L2121059-11 L2121059-12 L2121059-13 L2121059-14 L2121059-15
10:10 10:11 10:12 10:14 10:16
Lead (Pb)-Total (mg/L) 0.0108 0.00276 0.00201 0.00214 0.000789Total Metals
05-JUL-18 17:27 (MT)
Sample ID Description
Client ID
Sampled Date
Grouping Analyte
Sampled Time
ALS ENVIRONMENTAL ANALYTICAL REPORT
L2121059 CONTD....
5PAGE of
Version: FINAL
13
WATER
Water Water Water Water Water28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18
BS9 INTERMEDIATE
WING
BS10 INTERMEDIATE
WING
CS4 INTERMEDIATE
WING
CF2 INTERMEDIATE
WING
CS5 INTERMEDIATE
WING
L2121059-16 L2121059-17 L2121059-18 L2121059-19 L2121059-20
10:18 10:19 10:20 10:21 10:22
Lead (Pb)-Total (mg/L) 0.00305 0.00338 0.00253 0.000832 0.00288Total Metals
05-JUL-18 17:27 (MT)
Sample ID Description
Client ID
Sampled Date
Grouping Analyte
Sampled Time
ALS ENVIRONMENTAL ANALYTICAL REPORT
L2121059 CONTD....
6PAGE of
Version: FINAL
13
WATER
Water Water Water Water Water28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18
CF3 INTERMEDIATE
WING
LS1 MAIN HALL DENS1 MAIN HALL DENS2 MAIN HALL BS11 MAIN HALL (
L2121059-21 L2121059-22 L2121059-23 L2121059-24 L2121059-25
10:23 10:24 10:24 10:24 10:24
Lead (Pb)-Total (mg/L) 0.000580 0.0157 0.00349 0.00443 0.00268Total Metals
05-JUL-18 17:27 (MT)
Sample ID Description
Client ID
Sampled Date
Grouping Analyte
Sampled Time
ALS ENVIRONMENTAL ANALYTICAL REPORT
L2121059 CONTD....
7PAGE of
Version: FINAL
13
WATER
Water Water Water Water Water28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18
BS12 BS13 BS14 BS15 BS16
L2121059-26 L2121059-27 L2121059-28 L2121059-29 L2121059-30
10:25 10:25 10:25 10:26 10:26
Lead (Pb)-Total (mg/L) 0.00631 0.00905 0.00190 0.00451 0.00172Total Metals
05-JUL-18 17:27 (MT)
Sample ID Description
Client ID
Sampled Date
Grouping Analyte
Sampled Time
ALS ENVIRONMENTAL ANALYTICAL REPORT
L2121059 CONTD....
8PAGE of
Version: FINAL
13
WATER
Water Water Water Water Water28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18
*BS17 (SPRAY NOZZLE)
DF4 DF5 DF6 DF7
L2121059-31 L2121059-32 L2121059-33 L2121059-34 L2121059-35
10:27 10:28 10:28 10:29 10:29
Lead (Pb)-Total (mg/L) 0.00298 0.00546 0.00259 0.00467 0.00742Total Metals
05-JUL-18 17:27 (MT)
Sample ID Description
Client ID
Sampled Date
Grouping Analyte
Sampled Time
ALS ENVIRONMENTAL ANALYTICAL REPORT
L2121059 CONTD....
9PAGE of
Version: FINAL
13
WATER
Water Water Water Water Water28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18
CS6 (PRIMARY) CBS1 (PRIMARY WING)
BS18 CS7 CBS2
L2121059-36 L2121059-37 L2121059-38 L2121059-39 L2121059-40
10:29 10:30 10:32 10:32 10:33
Lead (Pb)-Total (mg/L) 0.00366 0.000403 0.00337 0.00521 0.00397Total Metals
05-JUL-18 17:27 (MT)
Sample ID Description
Client ID
Sampled Date
Grouping Analyte
Sampled Time
ALS ENVIRONMENTAL ANALYTICAL REPORT
L2121059 CONTD....
10PAGE of
Version: FINAL
13
WATER
Water Water Water Water Water28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18
CS8 CS9 OB1 CS10 CS11
L2121059-41 L2121059-42 L2121059-43 L2121059-44 L2121059-45
10:34 10:34 10:35 10:35 10:36
Lead (Pb)-Total (mg/L) 0.00129 0.00122 0.00257 0.00136 0.00139Total Metals
05-JUL-18 17:27 (MT)
Sample ID Description
Client ID
Sampled Date
Grouping Analyte
Sampled Time
ALS ENVIRONMENTAL ANALYTICAL REPORT
L2121059 CONTD....
11PAGE of
Version: FINAL
13
WATER
Water Water Water Water Water28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18
CS12 CS13 KS1 BS19 BS20
L2121059-46 L2121059-47 L2121059-48 L2121059-49 L2121059-50
10:36 10:37 10:37 10:40 10:42
Lead (Pb)-Total (mg/L) 0.00101 0.00176 0.00612 0.0230 0.0260Total Metals
05-JUL-18 17:27 (MT)
Sample ID Description
Client ID
Sampled Date
Grouping Analyte
Sampled Time
ALS ENVIRONMENTAL ANALYTICAL REPORT
L2121059 CONTD....
12PAGE of
Version: FINAL
13
WATER
Water Water Water28-JUN-18 28-JUN-18 28-JUN-18
T2-1 T2-2 T3-3
L2121059-51 L2121059-52 L2121059-53
10:44 10:45 10:46
Lead (Pb)-Total (mg/L) 0.000180 0.000176 0.000318Total Metals
Reference Information 05-JUL-18 17:27 (MT)
L2121059 CONTD....
13PAGE of
MET-T-CCMS-VA Total Metals in Water by CRC ICPMS
Water samples are digested with nitric and hydrochloric acids, and analyzed by CRC ICPMS.
Method Limitation (re: Sulfur): Sulfide and volatile sulfur species may not be recovered by this method.
ALS Test Code Test Description
Water EPA 200.2/6020A (mod)
Method Reference**
** ALS test methods may incorporate modifications from specified reference methods to improve performance.
Matrix
The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below:
Laboratory Definition Code Laboratory Location
VA ALS ENVIRONMENTAL - VANCOUVER, BRITISH COLUMBIA, CANADA
GLOSSARY OF REPORT TERMSSurrogate - A compound that is similar in behaviour to target analyte(s), but that does not occur naturally in environmental samples. Forapplicable tests, surrogates are added to samples prior to analysis as a check on recovery.mg/kg - milligrams per kilogram based on dry weight of sample.mg/kg wwt - milligrams per kilogram based on wet weight of sample.mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight of sample.mg/L - milligrams per litre.< - Less than.D.L. - The reported Detection Limit, also known as the Limit of Reporting (LOR).N/A - Result not available. Refer to qualifier code and definition for explanation.
Test results reported relate only to the samples as received by the laboratory.UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION.Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.
Test Method References:
Chain of Custody Numbers:
17-653378 17-653379 17-653380 17-653381 17-653382
Version: FINAL
13
[This report shall not be reproduced except in full without the written authority of the Laboratory.]
29-JUN-18
Lab Work Order #: L2121514
Date Received:GOVERNMENT OF YUKON
113 Industrial RoadWhitehorse YT Y1A 2T8
ATTN: Trevor JustasonFINAL 06-JUL-18 09:51 (MT)Report Date:
Version:
Certificate of Analysis
ALS CANADA LTD Part of the ALS Group An ALS Limited Company
____________________________________________
Carla FuginskiAccount Manager
ADDRESS: 8081 Lougheed Hwy, Suite 100, Burnaby, BC V5A 1W9 Canada | Phone: +1 604 253 4188 | Fax: +1 604 253 6700
Client Phone: 604-253-4188
Job Reference: NOT SUBMITTEDProject P.O. #:
17-653392C of C Numbers: Legal Site Desc:
06-JUL-18 09:51 (MT)
Sample ID Description
Client ID
Sampled Date
Grouping Analyte
Sampled Time
ALS ENVIRONMENTAL ANALYTICAL REPORT
L2121514 CONTD....
2PAGE of
* Please refer to the Reference Information section for an explanation of any qualifiers detected.
Version: FINAL
3
WATER
water29-JUN-18
MECH ROOM 1
L2121514-1
10:30
Hardness (as CaCO3) (mg/L)
Aluminum (Al)-Total (mg/L)
Antimony (Sb)-Total (mg/L)
Arsenic (As)-Total (mg/L)
Barium (Ba)-Total (mg/L)
Boron (B)-Total (mg/L)
Cadmium (Cd)-Total (mg/L)
Calcium (Ca)-Total (mg/L)
Chromium (Cr)-Total (mg/L)
Copper (Cu)-Total (mg/L)
Iron (Fe)-Total (mg/L)
Lead (Pb)-Total (mg/L)
Magnesium (Mg)-Total (mg/L)
Manganese (Mn)-Total (mg/L)
Mercury (Hg)-Total (mg/L)
Potassium (K)-Total (mg/L)
Selenium (Se)-Total (mg/L)
Sodium (Na)-Total (mg/L)
Uranium (U)-Total (mg/L)
Zinc (Zn)-Total (mg/L)
136
<0.010
<0.00050
0.00465
0.039
<0.10
<0.00020
25.3
<0.0020
0.0056
<0.030
<0.00050
17.7
0.0036
<0.00020
1.80
<0.0010
7.9
0.00219
<0.050
Physical Tests
Total Metals
HTC
Reference Information
HTC Hardness was calculated from Total Ca and/or Mg concentrations and may be biased high (dissolved Ca/Mg results unavailable).
Qualifiers for Individual Parameters Listed:
Description Qualifier
06-JUL-18 09:51 (MT)
L2121514 CONTD....
3PAGE of
HARDNESS-CALC-VA
HG-TOT-CVAFS-VA
MET-T-CCMS-VA
Hardness
Total Hg in Water by CVAFS LOR=50ppt
Total Metals in Water by CRC ICPMS
Hardness (also known as Total Hardness) is calculated from the sum of Calcium and Magnesium concentrations, expressed in CaCO3 equivalents. Dissolved Calcium and Magnesium concentrations are preferentially used for the hardness calculation.
This analysis is carried out using procedures adapted from "Standard Methods for the Examination of Water and Wastewater" published by the American Public Health Association, and with procedures adapted from "Test Methods for Evaluating Solid Waste" SW-846 published by the United States Environmental Protection Agency (EPA). The procedure involves a cold-oxidation of the acidified sample using bromine monochloride prior to reduction of the sample with stannous chloride. Instrumental analysis is by cold vapour atomic fluorescence spectrophotometry or atomic absorption spectrophotometry (EPA Method 245.7).
Water samples are digested with nitric and hydrochloric acids, and analyzed by CRC ICPMS.
Method Limitation (re: Sulfur): Sulfide and volatile sulfur species may not be recovered by this method.
ALS Test Code Test Description
Water
Water
Water
APHA 2340B
EPA 1631E (mod)
EPA 200.2/6020A (mod)
Method Reference**
** ALS test methods may incorporate modifications from specified reference methods to improve performance.
Matrix
The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below:
Laboratory Definition Code Laboratory Location
VA ALS ENVIRONMENTAL - VANCOUVER, BRITISH COLUMBIA, CANADA
GLOSSARY OF REPORT TERMSSurrogate - A compound that is similar in behaviour to target analyte(s), but that does not occur naturally in environmental samples. Forapplicable tests, surrogates are added to samples prior to analysis as a check on recovery.mg/kg - milligrams per kilogram based on dry weight of sample.mg/kg wwt - milligrams per kilogram based on wet weight of sample.mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight of sample.mg/L - milligrams per litre.< - Less than.D.L. - The reported Detection Limit, also known as the Limit of Reporting (LOR).N/A - Result not available. Refer to qualifier code and definition for explanation.
Test results reported relate only to the samples as received by the laboratory.UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION.Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.
Test Method References:
Chain of Custody Numbers:
17-653392
Version: FINAL
3