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    Fracture behaviors of a new steel fiber reinforced recycled

    aggregate concrete with crumb rubber

    Y.C. Guo a,, J.H. Zhang a, G. Chen a, G.M. Chen a, Z.H. Xie b

    a Faculty of Civil and Transportation Engineering, Guangdong University of Technology, Guangzhou, Chinab School of Civil Engineering and Transportation, South China University of Technology, Guangzhou, China

    h i g h l i g h t s

    The fracture behaviors of steel fiber-reinforced RA concrete which consists of crumb rubber were investigated.

    The effects of rubber content on the fracture behaviors of the RSRAC subjected to different temperatures were analyzed.

    The fracture properties were obtained in different temperatures.

    The fracture toughness and fracture energy first increase and then decrease.

    The thermal damage increases the fracture energy and CMODc.

    a r t i c l e i n f o

    Article history:

    Received 16 September 2013

    Received in revised form 1 November 2013

    Accepted 20 November 2013

    Available online 18 December 2013

    Keywords:Steel fiber reinforced concrete

    Recycled aggregate

    Crumb rubber

    Fracture properties

    High temperature

    a b s t r a c t

    This paper investigated the fracture behaviors of a new Steel fiber reinforced Recycled Aggregate Con-

    crete which consists of crumb Rubber (RSRAC). The effects of rubber content on the fracture behaviors

    of the RSRAC subjected to different temperatures were analyzed. In RSRAC, the steel fiber was used to

    improve the crack resistance of concrete, and the inclusion of crumb rubber is mainly for environment

    protection, energy dissipation and reducing the risk of explosive spalling during exposure to high temper-

    atures. A series of concrete mixes were prepared with ordinary Portland cement, recycled coarse aggre-

    gates (RCA) or natural coarse aggregates (NCA), steel fiber with volume-ratio of 1% and crumb rubber

    with different replacement ratios of 0%, 4%, 8%, 12% and 16% for fine aggregate (sand). The fracture prop-

    erties, including fracture toughness (KIC) and fracture energy (GF), of the different concrete mixes sub-

    jected to different temperatures (25 C, 200 C, 400 C and 600 C), were obtained through three-point

    bending tests on 72 notched beams with sizes of 100 mm100 mm515 mm. The results indicated

    that both the fracture toughness and fracture energy first increase and then decrease with increase of

    the rubber content; at certain rubber content, the mixes had the highest toughness. The thermal damage

    due to heating from 25 C to 600 C also obviously increased the fracture energy and critical crack mouth

    opening displacement (CMODcri), but it was not the case for the fracture toughness. It demonstrated that

    exposure to high temperature made all cementitious materials tested significantly more ductile and less

    resistant to crack propagation.

    2013 Elsevier Ltd. All rights reserved.

    1. Introduction

    A new type of Steel fiber reinforced Recycled Aggregate Con-

    crete (RSRAC), which consists of crumb rubber, is a concrete mate-

    rial patented by the authors (China invention patent No.: ZL.

    201010019345.3). This new material has been coined on the fol-

    lowing considerations: (1) the inclusion of recycled concrete aggre-

    gate (RCA) and rubber particles is mainly for the environmental

    and economic significance [13], (2) the steel fiber and rubber par-

    ticles are used to improve the performances of concrete both

    before [46]and after[7] exposure to different temperatures, (3)the advantageous interaction exists between steel-fiber and rubber

    as mentioned in the literature[810].

    Strength, stiffness, toughness and brittleness are the fundamen-

    tal mechanical properties of concrete. The changes of these proper-

    ties after exposure to high temperatures are of great importance

    for the design of concrete structures [11]. It is, thus, more impor-

    tant to investigate the mechanical properties of concrete in the

    structures subjected to long-term high temperatures. More and

    more attentions[12,13]have been paid to the mechanical proper-

    ties of concrete at high temperature or the residual properties of

    concrete after exposure to high temperatures. Moreover, the com-

    pressive properties of RSRAC mixes have already been analyzed

    0950-0618/$ - see front matter 2013 Elsevier Ltd. All rights reserved.http://dx.doi.org/10.1016/j.conbuildmat.2013.11.075

    Corresponding author. Tel.: +86 20 39322538; fax: +86 20 39322511.

    E-mail address: [email protected](Y.C. Guo).

    Construction and Building Materials 53 (2014) 3239

    Contents lists available at ScienceDirect

    Construction and Building Materials

    j o u r n a l h o m e p a g e : w w w . e l s e v i e r . c o m / l o c a t e / c o n b u i l d m a t

    http://dx.doi.org/10.1016/j.conbuildmat.2013.11.075mailto:[email protected]://dx.doi.org/10.1016/j.conbuildmat.2013.11.075http://www.sciencedirect.com/science/journal/09500618http://www.elsevier.com/locate/conbuildmathttp://www.elsevier.com/locate/conbuildmathttp://www.sciencedirect.com/science/journal/09500618http://dx.doi.org/10.1016/j.conbuildmat.2013.11.075mailto:[email protected]://dx.doi.org/10.1016/j.conbuildmat.2013.11.075http://crossmark.crossref.org/dialog/?doi=10.1016/j.conbuildmat.2013.11.075&domain=pdf
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    and discussed by the authors, and the relevant achievements have

    been reported in a separate paper, which is under review. In addi-

    tion, the poor performance of the RCA is associated with the cracks

    and fissures formed in processing recycled aggregates, which

    makes concrete prepared with RCA suffer brittleness problems

    [14]. Therefore, the experimental research on the fracture proper-

    ties of RSRAC mixes in this paper is in urgent need.

    The fracture properties of concrete significantly influence the

    structural behavior of concrete components at high temperatures

    [11]. Studies on the fracture properties of concrete have recently

    attracted more attentions. The fracture energy is defined as the en-

    ergy absorbed to create a unit area of fracture surface, representing

    the energy dissipation capacity of overall loading process. RILEM

    [15] recommended the three-point bending method for determina-

    tion of the fracture energy with specimens of notched beams. Me-

    nou et al. [16] examined the residual fracture energy of cement

    paste, mortar and concrete subjected to high temperature and

    found that the thermal damage due to heating from 120 to

    400 C increases the fracture energy by 50% compared with the ref-

    erence tests at room temperature. Peng et al. [13] conducted an

    experimental research to explore the relationship between explo-

    sive spalling and the residual fracture properties of concrete ex-

    posed to high temperatures; their results showed that the

    residual fracture energy increased after heating. Nielsen et al.

    [17]also suggested that the damage introduced by a temperature

    within 300400 C increased the fracture energy by 50% compared

    with the tests at room temperature. Since the fracture toughness

    represents the resistance to instable crack propagation, namely

    the resistance to brittle fracture, Hisham Abdel-Fattah et al. [18]

    experimentally investigated the variation of the residual fracture

    toughness of concrete with different temperatures and pointed

    out that the residual fracture toughness of concrete decreases with

    the increase in temperature.

    This paper studies the fracture behaviors properties (including

    the fracture energy GFand fracture toughnessKIC) of a new steel fi-

    ber reinforced Recycled Aggregate Concrete (RSRAC) subjected to

    different temperatures. From the test results, a preliminary under-standing of the fracture failure mechanism of RSRAC after exposure

    to different temperatures can be achieved. This study may provide

    a basis for the further research on RSRAC and its potential

    applications.

    2. Experimental details

    2.1. General

    A total of six groups of mixes, named NC-R0, RC-R0, RC-R4, RC-R8, RC-R12 and

    RC-R16, were prepared using 100% recycled concrete aggregate (RCA) or natural

    concrete aggregate (NCA), 1% steel fiber and rubber crumb with varied content

    (0%, 4%, 8%, 12% and 16%). Each type of concrete mixes includes 12 cylinders with

    dimensions of 150 mm300 mm (diameter and height) and 12 notched beams

    with dimensions of 100 mm100 mm515mm, every three of which were ex-

    posed to a temperature (25 C, 200 C, 400 C and 600 C). The proportions and

    compressive strengths are presented in Table 1.

    Crumb rubber, obtained from waste tires, has an average particle diameter of

    14 20 sieve size (i.e. 0.85 1.40 mm according to ASTM-E11-09e1), a specific

    gravity of 1.05, and a melting temperature of 170 C. The steel fibers were cut

    and shapedfromsteelplate, witha lengthof 32mm, anaspectratio of 45anda ten-

    sile strength of 600 MPa. This type of steel fibers, which were made from ordinary

    steel, with a melting temperature of 1538 C and a density of 7.82 g/cm3, are loose

    informat delivery (Fig. 1). In addition, a commercially available naphthalene-basedsuper-plasticizer with a solid content of 30% and a water reducing rate of 20% was

    used as admixture to achieve slump of the concrete mixes around 150 mm. The

    amount of plasticizer was 1.0% by weight of cement based on slump tests according

    to BS 1881: Part 102 (1983). Recycled concrete aggregates, crumb rubber and steel

    fibers are shown inFig. 1.

    2.2. High temperature program

    Among 12 cylindrical specimens in each mix, three were tested immediately

    after conditioning without being unheated (at the room temperature of 25 C),

    the remaining 9 specimens were divided into 3 groups and exposed to 3 tempera-

    tures (200 C, 400 C and 600 C) in an electrical furnace, respectively. In the fur-

    nace, the specimens were heated at a constant rate of 8 C/min, from the room

    temperature to the prescribed temperatures. The temperaturetime curves used

    in heating of the test specimens are showed inFig. 2, which were adopted from

    the paper [13]. The target temperature was maintained for 120 min before the elec-trical furnace was turned off andthe specimenswere then naturally cooleddownto

    the room temperature. During the heating period, water was allowed to evaporate

    freely.

    2.3. Methods of three-point bending tests

    A three-point bending method was used in the study to determine the fracture

    performance of the new concrete material RSRAC in accordance with the recom-

    mendation of RILEM Fracture Mechanics Committee (TC50-FMC) [15]. As showed

    inFig. 3(a), the notched beams used for the three-point bending test had dimen-

    sions of 100 mm100 mm515mm anda span of 400 mm; a notch with a depth

    of 30mm (a0/h= 0.3) was located in the mid-span place. The test was conducted on

    a closed-loop Electro Hydraulic universal testing machine with a 500-kN capacity

    and three control modes: load control, displacement control and strain control. In

    the study of the fracture properties, a 50-kN load cell with the precision of 1 N

    and a 50-mm displacement transducer (LVDT) with the accuracy of 0.01 mm were

    applied to obtain the load and deflection at the mid-span respectively, while the

    crack mouth opening displacement (CMOD) was measured with a 10-mm clip-on

    gages with the accuracy of 0.001 mm. All the data were recorded via the synchro-

    nous collection system of TDS-530. During the loading process, a constant displace-

    ment rate of 0.05 mm/min with the central deflection as the control parameter was

    applied until the final failure of the specimen. In addition, a testing strategy used in

    the three-point bending method [Fig. 3(b)] was designed to eliminate the negative

    effect of compressive plastic deformation on the compressed parts of specimens

    (e.g. the pedestal and actuator head) on the measurement. An advantage of the de-

    signed testing strategy is that the reference points located on the neutral axis of the

    notched beams were applied to measure the mid-span deflection in order to re-

    move the compressive plastic deformation on the other parts of specimens from

    the measured deflection. As a result, the measured values are authentic deflection

    of the tested beams. Both the specially designed testing system and the precision

    of measurement ensure the accuracy of the loaddeflection (Pd) curves and

    load-CMOD (P-CMOD) curves. The specimen and set-up of three-point-bending test

    are shown inFig. 3.

    Table 1

    Mix proportions and compressive strengths.

    Mix Compressive strength (MPa) Mix proportions (unit weight:kg/m3)

    W/C W OPC S NCA RCA AW SF R WRA

    NC-R0 56.52 0.35 170 485 645 1052 78 4.5

    RC-R0 51.41 0.35 170 485 645 954 37 78 4.5

    RC-R4 49.06 0.35 170 485 625 954 37 78 7.9 4.5

    RC-R8 39.41 0.35 170 485 605 954 37 78 15.7 4.5

    RC-R12 37.61 0.35 170 485 585 954 37 78 23.6 4.5

    RC-R16 35.88 0.35 170 485 565 954 37 78 31.5 4.5

    Note: NC = natural concrete, RC = recycled concrete, R0, R4, R8, R12 and R16 for volume substitution ratio of rubber is 0%, 4%, 8%, 12% and16%, W/C= water/cement

    ratio(mass), W = water, OPC = ordinary Portland cement, S = sand, NCA = natural coarse aggregate, RCA = recycled concrete aggregate, AW = additional water, SF = steel fiber,R = crumb rubber, WRA = naphthalene-based high-range water-reducing admixture.

    Y.C. Guo et al. / Construction and Building Materials 53 (2014) 3239 33

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    2.4. Determination of the fracture energy

    The fracture energy, defined as the total energy dissipated over a unit area of

    the cracked ligament, is obtained from the work done by the force (the area under

    the loaddeflection curve). The fracture energy of the notched beams includes 4

    parts (Fig. 4)[11], which can be expressed as:

    W W0 W1 W2 W3 2-1

    Here, W0 is theworkdoneby the external force P, (i.e. theenveloping area of the

    loaddeflection curves) which is recorded by the data acquisition system (DAS); W1is the work done by the self-weight of the beams before application of the external

    force P, but neglected in this paper as it is extremelysmall; W2and W3arethe addi-

    tional work done during the loading process by the self-weight of the beams, in

    whichthereexists a equationofW2 0:5 mgd0; W3, the end part ofthe curves after

    d0, cannot be measured in tests. The computational steps of the fracture energy are

    as follow:

    (1) W0 Rd0

    0 Pdd.

    (2) W2 0:5mgd0, in which mg (g= 9.81m/s2) is the self-weight of the beams

    scaled byS/L of the total weight (hereinafter referred to scaled weight).

    (3) Calculating the additional work W3 done by scaled weight. First, the

    descending branch of the loaddeflection (Pd) curve is artificially extendedby curve-fitting based on the power function method[19]:

    (a) Recycled concrete aggregates

    (b) Crumb rubber

    (c) Steel fibers

    Fig. 1. Material components.

    0

    100

    200

    300

    400

    500

    600

    700

    0 50 100 150 200 250 300

    Time (min)

    T

    emperature(C)

    200400600

    CCC

    Fig. 2. Temperaturetime curves in heating of the test specimens.

    (a) Notched beam of three-point-bending test

    (b) Set-up of three-point-bending test

    (c) A complete loading system in 500 kN testing machine

    Clip-on

    Gages=400 mm

    l=515 mm

    57.557.5

    t=100

    h=100

    P

    a0=30 mm

    LVDT

    Load

    Cell

    Fig. 3. specimen and set-up of three-point-bending test.

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    P bdk P 0b; k> 0

    lnP b k ln d2-2

    (4) The reliability of the fitting curves is represented by the reliability coeffi-

    cient, R2, and thespecific fitting parameters (i.e. b, k, R2) are listedin Table 2.

    Thus, W3can be calculated by the following formula (2-3).

    W3

    Z 1d0

    b

    dkdd

    b

    k 1dk10

    2-3

    (5) The real fracture energy of NC-R0 and RSRAC mixes is obtained in accor-

    dance to the formula (24) after W0, W2 andW3 are obtained. Here, Aligis

    the area of ligament, namely Alig= t(h-a0).

    GFW0 W1 W2 W3

    Alig2-4

    The calculated results of the fracture energy of NC-R0 and RSRAC mixes with

    various contents of crumb rubber are summarized in Table 2. It should be noted

    that no more than one testing curve was rejected as they are significantly different

    from the remaining two. Effective cross-sectional size and non-uniformed distribu-

    tion of steel fiber contribute to the discreteness. As a result, each listed value is the

    average of two or three measurements.

    2.5. Determination of the fracture toughness

    The fracture toughness (KIC) of concrete is another important parameter to de-

    scribe the fracture performance of concrete, it reflects the ability of concrete mate-

    rial to resist crack extension, namely the ability of resisting brittle fracture. The

    fracture toughness KICof a concrete material is calculated by formula (25) as in

    ASTM E399-74 (American Society for Testing and Material).

    KICPmaxS

    th3=2

    f a

    h

    2-5

    where Pmaxis the vertical peak load;h,tand Sare respectively the height, width and

    the span of the specimens (Fig. 3);a0is the notch depth; fahis the geometric shape

    factor, calculated by formula (2-6).

    f a

    h

    2:9

    a

    h

    1=2 4:6

    a

    h

    3=2 21:8

    a

    h

    5=2 37:6

    a

    h

    7=2 38:7

    a

    h

    9=22-6

    The inclusion of steel fiber introduces the anchoring force between steel fiber and

    concrete matrix, which causes the fracture process zone of steel fiber reinforced con-

    crete larger than that of plain concrete. Theformula of calculating fracture toughness

    recommended by ASTM, however, is based on the plain concrete material. The influ-

    ence of fracture process zone on adhesive fracture toughness of steel fiber reinforced

    concrete is included by the replacement ofawiththe effective crack length acin for-

    mula (2-6)[20].The effective crack length (ac) was calculated byac= a0+Dac. When

    the testing load (P) reaches its maximum (Pmax), the crack mouth opening displace-

    ment gets its critical value (CMODc), and the real length of pre-crack also develops

    from the initial value (a0) to the critical effective crack length (ac). Hence according

    to the linear asymptotic superposition principle,accan be calculated by a LEFM for-

    mula (2-7)[21]:

    ac2

    ph h0 arctan

    ffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffitECMOD

    c

    32:6Pmax 0:1135

    s h0 2-7

    whereh0is the thickness of steel sheet used to set up the clip-on gages on the crack

    mouth (i.e. additional thickness); (CMOD)c is the critical value of the crack mouth

    opening displacement;Eis the modulus of rupture, expressed by formula (2-8):

    E 1

    tci3:70 32:60tan2p

    2a0 h0h h0

    2-8

    whereci CMODi

    Pi(case in the table) is a initial value determined at a arbitrary point

    (P, CMOD) on the ascent stage ofP-CMOD curves (Fig. 6). The calculated parameters

    and results of the fracture toughness (KIC) of NC-R0 and RSRAC mixes are summa-

    rized inTable 3.

    3. Results and discussion

    The fracture properties of mixes including NC-R0 and RSRAC are

    determined by the three-point bending tests on centrally notched

    beams (seeFig. 3) according to the RILEM fracture mechanics of

    concrete (TC50-FMC) [15]. The measured loaddeflection (Pd)

    curves and load-crack mouth opening displacement (P-CMOD)

    curves are presented inFigs. 5 and 6 respectively.

    The fracture energy (GF) and fracture toughness (KIC) of concrete

    mixes are calculated (seeTable 4) and analyzed based on Pd and

    P-CMOD curves. It should be noted that each value in Table 4 is the

    average calculated from two or three specimens in a group.

    3.1. Fracture energy

    The fracture energy of each concrete mix, including both un-

    heated and heated specimens, was shown inTable 4. The effects

    W2

    W0

    0

    W3W1

    P P

    Pmax

    c

    Fig. 4. Determination of fracture energy of concrete by means of three-point

    bending method.

    Table 2

    Parameters of the fitted cure and values of the fracture energy.

    Specimens a0(mm) mg (N) d0(mm) b k R2 W0(Nm) W2 (Nm) W3(Nm) Alig(m

    2) GF(N/m)

    NC-R0-T25-1 30.6 91.433 3.345 1.9991 1.1807 0.9746 11.5341 0.1529 8.8944 0.00306 6725.96NC-R0-T25-3 31.2 92.195 3.498 2.0525 1.1953 0.9789 10.8925 0.1612 8.2295 0.00312 6180.53

    Average 6453.24

    RC-R0-T25-1 31.4 91.814 5.001 3.2077 2.7761 0.9801 11.3739 0.2296 0.1035 0.00314 3728.35

    RC-R0-T25-2 30.8 91.433 3.245 6.5399 7.7801 0.9727 9.5236 0.1484 0.0003 0.00308 3140.35

    Average 3434.35

    RC-R4-T25-2 31.7 88.766 9.000 2.5172 1.4368 0.9797 17.9374 0.3994 2.2071 0.00317 6480.74

    RC-R4-T25-3 29.5 88.385 7.707 1.2241 1.3028 0.9834 16.2312 0.3406 2.1783 0.00295 6355.95

    Average 6418.35

    RC-R8-T25-1 30.8 86.099 8.851 2.9284 1.3969 0.9845 23.1908 0.3810 3.1052 0.00308 8661.37

    RC-R8-T25-2 29.5 86.099 8.392 2.0653 1.3455 0.9814 20.6545 0.3613 2.8664 0.00295 8095.66

    RC-R8-T25-3 29.8 85.718 8.958 2.5054 1.3559 0.9856 21.2141 0.3839 3.2259 0.00298 8330.19

    Average 8362.41

    RC-R12-T25-1 29.6 83.433 9.000 1.9526 1.3523 0.9906 12.8667 0.3754 2.5558 0.00296 5337.13

    RC-R12-T25-3 31.6 84.957 9.000 3.0155 1.4515 0.9937 14.0124 0.3823 2.4766 0.00316 5339.03

    Average 5338.08

    RC-R16-T25-1 30.2 83.052 8.841 2.1846 1.7259 0.9878 10.3178 0.3671 0.6186 0.00302 3742.90

    RC-R16-T25-2 31.9 84.195 8.931 2.8587 1.7336 0.9845 11.8971 0.3760 0.7819 0.00319 4092.45

    Average 3917.68

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    0

    1

    2

    3

    4

    5

    6

    7

    0 2 4 6 8 10 12

    Deflection (mm)

    L

    oad(P,

    kN)

    NC-R0-T25

    RC-R0-T25

    RC-R4-T25

    RC-R8-T25

    RC-R12-T25

    RC-R16-T25

    (a) Load-deflection curves of mixes at room temperature

    0

    1

    2

    3

    4

    5

    6

    7

    0 2 4 6 8 10 12

    Deflection (mm)

    Load

    (P,

    kN)

    NC-R0-T200

    RC-R0-T200

    RC-R4-T200

    RC-R8-T200

    RC-R12-T200

    RC-R16-T200

    (b) Load-deflection curves of mixes exposed to 200 C

    0

    1

    2

    3

    4

    5

    6

    7

    0 2 4 6 8 10 12

    Deflection (mm)

    Load(P,

    kN)

    NC-R0-T400

    RC-R0-T400

    RC-R4-T400

    RC-R8-T400

    RC-R12-T400

    RC-R16-T400

    (c) Load-deflection curves of mixes exposed to 400 C

    0

    1

    2

    3

    4

    5

    6

    7

    0 2 4 6 8 10 12

    Deflection (mm)

    Load

    (P,

    kN)

    NC-R0-T600

    RC-R0-T600

    RC-R4-T600

    RC-R8-T600

    RC-R12-T600

    RC-R16-T600

    (d) Load-deflection curves of mixes exposed to 600 C

    Fig. 5. Measured loaddeflection curves of mixes.

    0

    1

    2

    3

    4

    5

    6

    7

    8

    0 2 4 6 8 10 12

    CMOD (mm)

    Load(P,

    kN)

    NC-R0-T400

    RC-R0-T400

    RC-R4-T400

    RC-R8-T400

    RC-R12-T400

    RC-R16-T400

    (c) Load-CMODcurves of mixes exposed to 400 C

    0

    1

    2

    3

    4

    5

    6

    7

    0 2 4 6 8 10 12

    CMOD (mm)

    Load(P,

    kN)

    NC-R0-T600

    RC-R0-T600

    RC-R4-T600

    RC-R8-T600

    RC-R12-T600

    RC-R16-T600

    (d) Load-CMODcurves of mixes exposed to 600 C

    0

    1

    2

    3

    4

    5

    6

    7

    0 2 4 6 8 10 12

    CMOD (mm)

    Load(P,

    kN)

    NC-R0-T25

    RC-R0-T25

    RC-R4-T25

    RC-R8-T25

    RC-R12-T25

    RC-R16-T25

    (a) Load-CMODcurves of mixes at room temperature

    0

    1

    2

    3

    4

    5

    6

    7

    0 2 4 6 8 10 12

    CMOD (mm)

    Load(P,

    kN)

    NC-R0-T200

    RC-R0-T200

    RC-R4-T200

    RC-R8-T200

    RC-R12-T200

    RC-R16-T200

    (b) Load-CMODcurves of mixes exposed to 200

    Fig. 6. Measured Load-CMOD curves of mixes.

    36 Y.C. Guo et al. / Construction and Building Materials 53 (2014) 3239

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    of temperature and rubber content on the fracture energy of con-

    crete mixes were shown in Fig. 7(a and b), respectively. It can be

    seen fromTable 4andFig. 7(a) that, the temperature has remark-

    able effects on the fracture energy of concrete mixes. Averagely

    speaking, the fracture energy of the concrete mixes increases

    1.80 times after exposure to 200 C, which further increases 2.81

    and 2.78 times after exposure to 400 C and 600 C respectively.

    This was consistent with the results of Peng et al. [13], Menou

    et al.[16]and Nielsen et al.[17]on the fracture energy. Exposure

    to high temperature, on the one hand, may degrade the compres-sive strength of concrete mixes for the severe thermal decomposi-

    tion (seeTable 4); on the other hand, it can improve the fracture

    properties, especially the fracture energy [seeFig. 7(a)]. The main

    mechanism responsible for this observation is that thermal dam-

    age makes the cracks develop along a tortuous rather than a sharp

    routine as at room temperature [16], which dissipates more

    energy.

    It should be noted that the fracture energy gradually becomes

    flat when the temperature exceeded 400 C [see Fig. 7(a)]. The frac-

    ture energy of several concrete mixes (e.g. NC-R0, RC-R4 and RC-

    R8) slightly decreases, while the others kept rising with the tem-perature increasing from 400 C to 600 C.

    Table 3

    Parameters and values of fracture toughness of mixes.

    Specimens a0(mm) Ci (lm/KN) h0(mm) mg (N) Pmax (kN) dc(mm) CMODc (mm) E(Gpa) ac(mm) KIC (MPa m1/2)

    NC-R0-T25-1 30.6 6.925 1.45 91.433 6.021 0.372 0.118 19.143 49.867 2.036

    NC-R0-T25-3 31.2 7.138 1.45 92.195 6.545 0.423 0.158 19.176 53.579 2.502

    Average 2.269

    RC-R0-T25-1 31.4 6.947 1.45 91.814 6.192 0.652 0.301 19.914 65.491 3.701

    RC-R0-T25-2 30.8 6.996 1.45 91.433 5.653 0.482 0.343 19.152 68.107 3.764

    Average 3.732RC-R4-T25-2 31.7 7.086 1.45 88.766 6.521 0.514 0.408 19.839 69.015 4.504

    RC-R4-T25-3 29.5 6.971 1.45 88.385 6.385 0.448 0.319 17.934 64.340 3.641

    Average 4.073

    RC-R8-T25-1 30.8 7.752 1.45 86.099 6.821 0.591 0.435 17.284 67.366 4.397

    RC-R8-T25-2 29.5 6.978 1.45 86.099 6.778 0.608 0.412 17.916 67.194 4.338

    RC-R8-T25-3 29.8 7.563 1.45 85.718 7.065 0.791 0.378 16.797 64.385 4.033

    Average 4.256

    RC-R12-T25-1 29.6 7.219 1.45 83.433 5.261 0.358 0.345 17.410 67.861 3.467

    RC-R12-T25-3 31.6 6.989 1.45 84.957 5.662 0.386 0.371 20.007 69.753 4.037

    Average 3.752

    RC-R16-T25-1 30.2 6.945 1.45 83.052 5.079 0.502 0.323 18.685 68.417 3.426

    RC-R16-T25-2 31.9 7.139 1.45 84.195 6.074 0.531 0.302 19.903 65.814 3.676

    Average 3.551

    Table 4

    The experimental and calculated results of three-point bending tests.

    Results NC-R0-T25 RC-R0-T25 RC-R4-T25 RC-R8-T25 RC-R12-T25 RC-R16-T25

    (a) The experimental and calculated results of mixes at 25C

    Compressive strength/(MPa) 56.52 51.41 49.06 39.41 37.61 35.88

    Pmax/(kN) 6.283 5.923 6.453 6.922 5.462 5.577

    dC/(mm) 0.398 0.567 0.481 0.699 0.372 0.517

    CMODC/(mm) 0.138 0.322 0.364 0.395 0.358 0.313

    GF/(N/m) 6453.24 3434.35 6418.35 8362.41 5338.08 3917.68

    KIC/(MPa m1/2) 2.269 3.732 4.073 4.256 3.746 3.551

    Results NC-R0-T200 RC-R0-T200 RC-R4-T200 RC-R8-T200 RC-R12-T200 RC-R16-T200

    (b) The experimental and calculated results of mixes at 200C

    Compressive strength/(MPa) 45.66 43.55 40.44 34.54 32.15 31.18

    Pmax/(kN) 5.416 5.929 5.247 5.781 5.126 4.903

    dC/(mm) 0.672 0.982 1.051 1.061 1.077 0.741

    CMODC/(mm) 0.379 1.033 0.821 0.843 0.675 0.457GF/(N/m) 8552.75 7127.89 9571.71 16544.98 13490.84 5740.96

    KIC/(MPa m1/2) 2.219 3.470 3.730 3.723 3.190 2.952

    Results NC-R0-T400 RC-R0-T400 RC-R4-T400 RC-R8-T400 RC-R12-T400 RC-R16-T400

    (c) The experimental and calculated results of mixes at 400C

    Compressive strength/(MPa) 24.71 28.64 26.21 19.71 17.61 17.17

    Pmax/(kN) 5.315 6.468 6.294 6.782 6.269 5.819

    dC/(mm) 1.445 1.270 1.550 1.227 1.405 1.445

    CMODC/(mm) 1.261 1.141 1.349 1.123 0.974 1.182

    GF/(N/m) 16695.00 15412.22 18230.00 18095.25 14027.35 12755.09

    KIC/(MPa m1/2) 3.344 3.861 4.344 3.317 2.203 2.089

    Results NC-R0-T600 RC-R0-T600 RC-R4-T600 RC-R8-T600 RC-R12-T600 RC-R16-T600

    (d) The experimental and calculated results of mixes at 600C

    Compressive strength/(MPa) 16.28 10.98 12.79 10.21 8.31 8.28

    Pmax/(kN) 4.846 6.311 6.545 6.191 6.080 5.970

    dC

    /(mm) 1.155 1.155 1.611 1.870 2.105 1.920

    CMODC/(mm) 0.903 1.032 1.514 1.046 1.402 1.476

    GF/(N/m) 16095.19 16176.88 16585.55 16683.09 15092.3 13763.07

    KIC/(MPa m1/2) 2.600 3.114 3.768 3.373 3.513 3.578

    Y.C. Guo et al. / Construction and Building Materials 53 (2014) 3239 37

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    It can be seen fromTable 4andFig. 7(b) that, for the concrete

    specimens after exposure to high temperatures except for 600 C,

    a full replacement of NCA by RCA only results in a clear decrease

    in the fracture energy, as the descending branch ofP-CMOD curves

    for the mixes prepared with RCA drops faster after peak load (see

    Fig. 6). When the rubber content increased from 4% to 16%, the

    fracture energy first increased and then decreased with increase

    of rubber content, with RC-R8 having the highest fracture energy

    at the high temperatures, indicating that an appropriate rubber

    content enhances the energy absorption capacity of the concrete

    but too much rubber may have a negative effect on the energy

    absorption capacity. Thus, to effectively improve of the energy

    absorption capacity of concrete mixes (both unheated and heated

    specimens), an appropriate amount of rubber should be selected.

    3.2. Fracture toughness

    The effects of temperature and rubber content on the fracture

    toughness of concrete mixes were shown in Fig. 8(a and b), respec-

    tively. It can be seen fromTable 4andFig. 8(a) that the fracture

    toughness of the concretes mixes changes obviously after exposure

    to a high temperature. However, with the different replacement ra-

    tios of crumb rubber, the influences of temperature on the fracture

    toughness of the concretes mixes are not consistent. For RC-R8, RC-

    R12 and RC-R16 specimens, the fracture energy first decreased and

    then increased with increase of rubber content, with the fracturetoughness being smallest at the temperature 400 C [see

    Fig. 8(a)]. For other groups of specimens, the fracture toughness

    of the concretes mixes changed in a different trend, this may be

    caused by the non-uniform distribution of the steel fiber in the

    crack surface and worth of a separate investigation.

    It can be seen from Table 4andFig. 8(b) that a full replacement

    of NCA by RCA leads to a significant increase in the fracture tough-

    ness, and that the concrete mixes with RCA have high resistance to

    brittle fracture. It is well known that the concrete strength depends

    on the strength of the cement paste, the aggregates and the inter-

    facial bond between the cement paste and the aggregates [22]. Forconcrete mixes prepared with natural aggregates and recycled

    aggregates, the difference in the peak stress and fracture toughness

    might be related to the strength of the interfacial bond. During

    vibration, the water inside the cement paste may move to the recy-

    cled aggregates due to their high water absorption capacity, creat-

    ing a relatively high w/c value in the vicinity of recycled

    aggregates. As a result, a stronger bond might be formed between

    the cement paste and RCA. It is also noted that when the rubber

    content increases from 4% to 16%, the fracture toughness first in-

    creases and then decreases with increase of rubber content, with

    RC-R4 or RC-R8, having the highest fracture toughness [see

    Fig. 8(b)], which indicates that an appropriate rubber content im-

    proves the resistance to brittle fracture of the concrete mixes but

    too much rubber content may have a negative effect on the resis-tance to brittle fracture.

    0

    2000

    4000

    6000

    8000

    10000

    12000

    14000

    16000

    18000

    20000

    25 200 400 600

    Temperatures

    Fracturee

    nergy(N/m)

    NC-R0RC-R0RC-R4RC-R8RC-R12RC-R16

    (a) Effects of temperature on the fracture energy

    0

    2000

    4000

    6000

    8000

    10000

    12000

    14000

    16000

    18000

    20000

    NC-R0 RC-R0 RC-R4 RC-R8 RC-R12 RC-R16

    Mix

    Fractureenergy(N/m)

    T25

    T200

    T400

    T600

    (b) Effects of rubber content on the fracture energy

    Fig. 7. Effects of temperature and rubber content on the fracture energy.

    1.0

    1.5

    2.0

    2.5

    3.0

    3.5

    4.0

    4.5

    5.0

    25 200 400 600

    Temperatures

    NC-R0RC-R0RC-R4RC-R8RC-R12RC-R16

    (a) Effects of temperature on the fracture

    toughness

    1.5

    2.0

    2.5

    3.0

    3.5

    4.0

    4.5

    NC-R0 RC-R0 RC-R4 RC-R8 RC-R12 RC-R16

    Mix

    Fracturetoughness(MPam

    1/2)

    T25

    T200

    T400

    T600

    (b) Effects of rubber content on the fracture toughness

    Fracturetough

    ness(MPam

    1/2)

    Fig. 8. Effects of temperature and rubber content on the fracture toughness.

    38 Y.C. Guo et al. / Construction and Building Materials 53 (2014) 3239

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    4. Conclusions

    In this paper, a series of three-point bending tests on notched

    beams of 100 mm100 mm515 mm were conducted in accor-

    dance to the recommendation of RILEM. The fracture energy and

    fracture toughness were calculated and the effects of heating and

    rubber contents on them were analyzed. The following conclusions

    can be drawn from this research:

    (1) A severe degradation of compressive strength has been

    found for all concrete mixes after exposure to high temper-

    atures, however, averagely the fracture energy of the con-

    crete mixes increased 1.80 times after exposure to 200 C,

    further increased to 2.81 and 2.78 times after exposure to

    400 C and 600 C respectively. This indicates that the

    energy dissipation capacity of concrete mixes increases as

    the temperatures rise, which is opposite to the trend of the

    compressive strength.

    (2) The main mechanism responsible for the increase in the

    fracture energy is that, the thermal damage makes the

    cracks develop in a more tortuous routine rather than

    sharp one as at room temperature, which dissipates more

    energy.

    (3) A full replacement of NCA by RCA results in an evident

    decrease in the fracture energy, as after the peak load the

    descending part of the fracture energy for the concrete

    mixes prepared with RCA dropped faster. The fracture

    energy first increased and then decreased with increase of

    rubber content from 0% to 16%, with RC-R8 having the high-

    est fracture energy at high temperatures.

    (4) The fracture energy represents the energy dissipation capac-

    ity of concrete mixes, while the fracture toughness reflects

    resistance to brittle fracture of concrete mixes. A full

    replacement of NCA by RCA leads to a significant increase

    in the fracture toughness. While the rubber content

    increased from 4% to 16%, the fracture toughness first

    increased and then decreased with increase of rubber con-tent, with RC-R4 or RC-R8 having the highest fracture

    toughness.

    (5) Appropriate rubber content increases the ductility of the

    concrete mixes but too much rubber may have a negative

    effect on the ductility of the concrete mixes.

    Acknowledgments

    The authors gratefully acknowledge the financial support

    provided by the National Natural Science Foundation (Project

    Nos. 51278132, 11372076), and Science and Technology Planning

    Project of Guangdong Province (2011B010400024), Technology

    Planning Project of Huangpu District (201356) and Foundation of

    Guangdong Provincial Department of Transport (Project Nos.

    2013-02-017, 2013-04-006).

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