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URSIDBreak:.Other:.
BIANNUAL REPORTENHANCED GROUNDWATERREMEDIATION PROGRESSPERIOD COVERINGOCTOBER 1, 2003 TOMARCH 31, 2004LINDSAY MANUFACTURING COMPANY
ForU.S. Environmental Protection
[ Agency
URS Job No. = 33750799April 14, 2004
40174128
SUPERFUND RECORDS
1400 CENTURY SQUARE1501 FOURTH AVENUE
SEATTLE, WASHINGTON 98101Tel (206) 438-2700 Fax No. (206) 438-2699
Date:
TO:
LETTER OF TRANSMITTAL
April 14, 2004
United States Environmental Protection AgencySuperfund Division726 Minnesota AvenueKansas City, Kansas 66101
Our Project No. 33750799
Attention: Ms. Diane Easley
Subject: Biannual Report - Enhanced Groundwater Remediation Progress, Period Covering October 1,2003 to March 31, 2004, for Lindsay Manufacturing Company
We are sending you via Federal Express the following:
I• 3 copies of the document Biannual Report - Enhanced Groundwater Remediation Progress, Period
Covering October 1, 2003 to March 31, 2004, for Lindsay Manufacturing Companyi
If you have any questions regarding this shipment, please feel free to contact me at 206-438-2234.
1 URS CORPORATION
Karen MixonTask Manager
CC: Robert Jacobson, Lindsay Manufacturing (3 copies)John Cruden, U.S. Dept. of Justice (1 copy)Wade Gregson, NDEQ (1 copy)John & Leigh Preister (1 copy)Beller Corporation (1 copy)
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April 14, 2004
Ms. Diane EasleyEPA Project CoordinatorUnited States Environmental Protection AgencySuperfund Division726 Minnesota AvenueKansas City, KS 66101
Enhanced Groundwater RemediationProgress ReportU.S. v. Lindsay Manufacturing CompanyC.A. 8:92-00015URSJobNo.: 33750799
Dear Ms. Easley:
Lindsay Manufacturing Company is pleased to submit this Enhanced GroundwaterRemediation Progress Report summarizing the Consent Decree items completed orundertaken during the period from October 1, 2003 to March 31, 2004. This reportpresents a summary of groundwater remedial pumping and analytical results from thesixtieth (November 2003) and sixty-first (February 2004) quarterly rounds of groundwatersampling.
REMEDIAL PUMPING
During the sixtieth and sixty-first quarters, converted monitoring well MW89-12 was theonly well operated within the interceptor system. Pumping at MW89-12 was halted for thewinter on October 31, 2003. The total gallons pumped from October 1, 2003 throughMarch 31, 2004 are presented in Table 1. Pumping of well 89-12 is expected to resume onor before May 1, 2004. Additionally, to augment the current on-facility remedial actions,Lindsay will begin pumping interceptor well AOIW once the associated irrigation systemsare ready for operation. The water will be used for irrigation on properties south/southeastof the Lindsay facility.
URS Corporation1501 4th Avenue, Suite 1400
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United States Environmental Protection AgencyApril 14, 2004Page 2
GROUND WATER MONITORING
Groundwater samples from monitoring wells were collected in November 2003 (sixtiethquarter) and February 2004 (sixty-first quarter). An additional sample was collected froman irrigation well in January 2004 to assess the feasibility of using this well as a watersource for drilling of a new irrigation well as described in Task 5 of the Work Plan(Revision 1.0), Supplemental Remedial Actions, Lindsay Manufacturing, Lindsay,Nebraska (Work Plan) dated October 23, 2003. The work plan describes multiple tasksassociated with supplemental remedial actions resulting from the EPA Five-Year Reviewconducted at the Lindsay site in 2003.
A summary of wells sampled and the analytical program is presented in Table 2. Samplelocations are shown on Figures 1 and 2. Samples were analyzed for volatile organiccompounds (VOCs), metals and sulfate in accordance with the modified Statement ofWork (SOW) associated with the Consent Decree. Field measurements for pH,temperature and specific conductivity were recorded at the time of sample collection.Laboratory analytical results and field measurements are summarized in Tables 3, 4, and 5.Copies of data validation memoranda and laboratory data pages are included in AppendixA of] this report. Analytical anomalies were not identified during the data validationprocess.
Sample analytical data for VOCs, zinc, cadmium, chromium and lead were compared toestablished cleanup levels identified in the SOW associated with the Consent Decree. Thecleanup levels primarily consist of federal maximum contaminant levels (MCLs) andsecondary MCLs as described below. Sulfate, iron and pH were compared to alternatecleanup levels agreed upon by the State of Nebraska, EPA and Lindsay Manufacturing inDecember 2000.
PERCHED SAND CHANNEL
Groundwater quality in the perched sand channel located beneath the Lindsay facility ismonitored by wells MW89-13 and MW89-14. Monitoring well MW89-13 was sampledfor metals and inorganic parameters during the sixtieth quarter. Samples were collected formetals and inorganic parameters from MW89-14 during the sixtieth and sixty-firstquarters.
iConcentrations of cadmium, chromium, lead, and zinc in samples collected from wellsMW89-13 and MW89-14 were below primary and secondary MCLs during the sixtiethand sixty-first quarters with one exception. Zinc was detected at a concentration of 6.58mg/1, above the secondary MCL (5 mg/1), in the sample from well MW89-14 during the
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sixtieth quarter. Sulfate, pH and iron were below or within the acceptable range of thealternate cleanup levels for on-property wells at MW89-13 and MW89-14.
Samples for VOC analysis were collected from both MW89-13 and MW89-14 during thesixtieth and sixty-first quarters. Tetrachloroethene (PCE) was detected above the 'MCL (5ug/1) in samples collected from well MW89-13 in the sixty-first quarter and MW89-14during the sixtieth quarter. Concentrations of PCE ranged from 2.5 ug/1 to 5.8 ug/1, similarto the previous two quarters. Other VOCs were either not detected or detected below EPAprimary MCLs in samples collected from MW89-13 and MW89-14. The concentration oftotal VOCs detected at well MW89-13 ranged from 4 ug/1 to 5.8 ug/1. The concentration oftotal VOCs detected at well MW89-14 ranged from 2.5 ug/1 to 12 ug/1.
SAND AND GRAVEL AQUIFER
Groundwater quality in the Sand & Gravel Aquifer is monitored beneath the Lindsayfacility at wells MW89-15, MW89-12, MW87-3, OIW, and AOIW, and downgradient ofthe facility at MW92-3A and MW92-3B.
Samples were collected for metals and inorganic parameters at MW87-3 and MW89-15during the sixtieth and sixty-first quarters. Samples were collected at MW89-12, MW92-3A, and MW92-3B during the sixtieth quarter.
Concentrations of zinc, cadmium, chromium and lead detected in wells completed in theSand & Gravel Aquifer were below MCLs with the exception of groundwater collectedfrom wells MW89-15 and MW92-3A. Zinc was above the secondary MCL ingroundwater collected from well MW89-15 during the sixtieth and sixty-first quarters.Chromium was detected above the MCL during the sixtieth quarter in the sample collectedfrom well MW92-3A.
The alternate cleanup level for on-property wells for sulfate and iron was exceeded duringthe sixty-first quarter in groundwater collected from MW89-15. The alternate cleanuplevel for off-property wells for iron was exceeded during the sixtieth quarter ingroundwater collected from MW92-3A. The pH generally ranged from 5 to 7 ingroundwater collected from the aquifer.
ii
Samples for VOCs were collected at all wells included in the monitoring program duringthe sixtieth and sixty-first quarters. 1,1-Dichlorethene (1,1-DCE), 1,1,1-trichloroethane(1,1,1-TCA) and PCE were detected in several wells during both quarterly samplingrounds. 1,1-DCE and/or PCE were above MCLs in wells MW87-3, MW89-12, MW89-15,MW92-3A, OIW, and AOIW during both quarterly sampling rounds. 1,1,1-TCA wasbelow the MCL in wells sampled during this biannual period with the exception of well
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MW89-15 during the sixty-first quarter. 1,1,1-TCA was detected at 200 ug/1, equal to theMCL.
1,2-Dichloroethene (1,2-DCE), 1,2-dichloroethane (1,2-DCA), and trichloroethene (TCE)were not detected or detected below MCLs. 1,1-Dichloroethane (1,1-DC A) was detectedat MW87-3, MW89-15, MW89-12, MW92-3A, OIW, and the AOIW. No MCL orcleanup level has been established for 1,1-DCA.
DOMESTIC, STOCK, AND IRRIGATION WELL MONITORING RESULTS
In August 2003, Lindsay installed whole-house treatment systems at the Preister and Sellerhouseholds. Samples were collected during the sixtieth and sixty-first quarters from bothsystems at locations before the first filter (BFF), after the first filter (AFF), and after thelast filter (ALF). The samples collected after the last filter is indicative of the water qualityfor household use. The data are summarized on Tables 3,4, and 5.
The domestic water supply to the Preister household is provided by the Preister Domestic2003 well with treatment through the whole-house system installed in August 2003. Thedata indicate that low levels of 1,1-DCE, 1,1,1-TCA, and PCE are present but belowassociated MCLs. VOCs were not detected in the after treatment system samples,indicating the treatment system is performing. Additionally, a sample from the PreisterDomestic 2003 well (before treatment) was analyzed for inorganic analyses. Inorganicconstituents were either not detected or detected below MCLs or alternate cleanup levels.
Samples were collected for VOC analysis from the Beller domestic water supply bothbefore and after the treatment system. Low levels of 1,1-DCE, 1,1,1-TCA, and/or PCEwere detected in the "before" sample (Table 5) but below the associated MCLs. A lowconcentration of PCE was detected in the sample collected in February 2004 after l.he firstfilter but not in the post-treatment sample, indicating the treatment system is performingproperly.
In response to the Five-Year Review completed by EPA in July 2003 and as described inthe work plan dated October 23, 2003, Lindsay installed an irrigation well between theBeller and Preister domestic wells (Figure 2). Prior to drilling, a sample was collectedfrom the Beller East Irrigation Well (Figure 2) to assess the feasibility of using this well asa water supply during drilling. The sample was collected on January 23, 2004 for VOCanalysis. The data indicate VOCs were not detected (Table 5).
The new irrigation well was installed in February 2004. The well completion informationwas forwarded to EPA in a letter report dated March 22, 2004. Soil samples werecollected from the stockpiled cuttings from the well and analyzed for VOCs. Copies of thelaboratory reports are included in Appendix A. VOCs were not detected. The cuttings wi l l
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be dispersed on the ground surface at the drilling location. Diffusion bags to collectgroundwater samples were placed at three depths in the new well to assess verticaldistribution in the aquifer of VOCs at the well location. The samples were collected onApril 1, 2004. Additionally, samples were collected on April 1, 2004 for VOC analysisfrom Preister's old domestic well, Anthony Klassen's irrigation well (#33172), JohnKlassen's irrigation well (#56241), and Weylan Neal's irrigation well (#31798). Samplelocations are shown on Figure 2. These data will be used to assess a location for a newmonitoring well (Task 4 of the October 23,2003 Work Plan) near the south termi nus ofthe groundwater plume. The analytical results will be forwarded to EPA as soon as theyare available.
As follow-up to the February 2004 results from the Seller treatment system, a sample wascollected on April 1,2004 from Seller's domestic treatment system after the first filter.
CONCLUSIONS AND RECOMMENDATIONS
VOCs are detected at monitoring points in a line from the facility to an area just south andeast of the Preister house. The data indicate that the lateral dispersion of VOCs along thisline is narrow (Figure 2). The southern terminus is not exact, but based on the addition ofsample data in 2003 from numerous domestic and irrigation wells located south of thePreister house, VOCs have migrated to an area between irrigation wells #G31798 and#G33172.
As discussed in the previous biannual report (URS, October 2003), peaks in concentrationsat on-site wells MW89-12 and MW89-15 coincide with seasonal stress on the aquiferduring the summer irrigation season (Figures 3 and 4). It is typical for concentrations todecrease and stabilize during the following winter. As shown on Figure 4, the overallconcentrations of VOCs monitored at downgradient wells MW92-3A, MW92-3B, andPreister's Domestic well show an overall decrease or stabilized concentrations. Theconcentrations of VOCs decrease from the facility (represented by MW89-15) to thePreister Domestic wells (Figure 4).
Lindsay submitted a work plan to EPA in October 2003 to address action items in responseto EPA's Five-Year Review completed in July 2003. Action items included installation ofan irrigation well between the Seller and Preister households to prevent furtherdowngradient migration of VOCs toward the Preister household and to remove VOCs inthis portion of the Sand & Gravel Aquifer. This well was installed in February 2004 andwill begin pumping at the start of the irrigation season. The data collected from this welland samples collected from selected irrigation wells in April 2004 will be used to site anew monitoring well at the southern terminus of VOCs in the Sand & Gravel Aquifer. Theproposed location of the well will be provided to EPA and upon EPA's concurrence,Lindsay will schedule the installation.
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B Based on the quarterly data collected, URS recommends the following for the monitoringperiod from April 2004 to September 2004:
•j o Continue and maximize pumping of modified MW89-12 as an interceptor well
« Enhance the removal of VOCs from the aquifer beneath the facility by reinstating• the AOIW and/or OIW to the operating interceptor system in Spring 2004
• Collect samples from the new irrigation well during the May and August 2004• quarterly sampling rounds
If you have any questions regarding this Enhanced Groundwater Remediation Process• Report, please do not hesitate to contact URS at your convenience.
Very truly yours,
| URS CORPORATION
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Karen L. MixonTask Manager
Roy/W. ElliottVice President
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Table 1Summary of Pumping Volumes and pHSixtieth and Sixty-First QuartersOctober 1,2003 through March 31,2004Lindsay Manufacturing Company
Monthly Summary
Oclober-03
November-03
Decembcr-03January - 04
February - 04
March - 04
60th Quarter
October, November, December 2003
61st Quarter
January, February, March 2004
60th and 61st Quarters
TIW
Total Gal. pH Range
000000
0
0
0
NANANANANANA
NA
NA
NA
AOIWTotal GaL pH Range
0
00000
0
0
0
NANANANANANA
NA
NA
NA
orwTotal Gal. pH Range
000000
0
0
0
NANANANANANA
NA
NA
NA
MW 89.12Total Gal. pH Range
1.166.018
00000
1.166.018
0
1.166.018
NA6.12NANA6.09
NA
NA
NA
NA
TotalGallons
1,166,018
00000
1.166.018
0
1.166.018
NA = nol applicable or not available
k:/OOyLMsay/2004/Reports/April 2004.xls (Pump sum}Updated: 4/14/2004 Page 1 of 1 URS
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Table 2
Summary of Wells Sampled and Analytical PlanSUtielh through Sixty-First QuartersOctober 200J - March 2004Lindsay Manufacturing Company
Well ID
Samples Collected November 200387-3
89-1289 1389 M89-1592- 3 A92-3BOI WellAOI WellBeller Domestic (BFF)Keller Domestic (AFF)Beller Domestic (ALF)Preister's Domestic 2003 (BFF)Preister's Domestic 2003 (AFF)Preister's Domestic 2003 (ALF)
Sainoles Collected January 2004Beller East Irrigation Well
SaiDDles Collected February 200487-3
89-1289-1389-1489-1592-3A92-3BOI WellAOI WellBeller Domestic (BFF)Beller Domestic (AFF)Beller Domestic (ALF)Preister's Domestic 2003 (BFF)Preisler's Domestic 2003 (AFF)Preister's Domestic 2003 (ALF)
pll (lab)(F.PA Method
150.1)
X
X
X
XX
X
X
X
X
X
X
X
X
X
Volatile OrganicCompounds (EPA
Method K260)
X
X
X
XX
XX
X
X
X
X
X
X
X
X
X
X
XX
X
X
X
X
X
X
XX
XX
XX
Total Zinc(CLP Method)
X
X
X
XX
X
X
X
X
X
X
X
X
X
Sulfate(FJPA Method
375.2)
X
XX
XX
X
X
X
X
X
X
X
X
X
TotalCadmium
(CLP Method)
X
X
X
XX
X
X
X
X
X
X
X
X
X
TotalChromium
(CLP Method)
X
X
X
XX
X
X
X
X
X
X
X
X
X
Total Iron(CLP Method)
X
X
X
X
X
X
X
X
X
X
X
X
X
X
Total Lead(CLP Method)
XX
X
XX
X
X
X
X
X
X
X
X
X
1I1IIIII BFF - Before first Filter of whole-house treatment system installed August 2003.
AFF - After first filter of whole-house treatment system installed August 2003.ALF - After last filler of whole-house treatment system installed August 2003. Effluent water is used by the household.
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Table 3Summary of Analytical Results Tor Inorganic CompoundsFifty-Second ihnmjh Sixty-Fim QuarunNovember 2001 through February 2004Lindsay Manufacturlnf Company
Well IDLabID
Federal MCL
Alternate Cleanup Level0'- On Property
Alternate Cleanup Lever"'- Off Property
Historical Data:Old Llndiay Public Supply Well (Sampled January 1977)Old Lindsay Public Supply Well (Sampled 01/24*1)15261 (Sampled 01/28/83)15242 (Sampled 01/28/83)
Sarrmln Collected November 200187-389-1489-1592-3A92-3BPreiiler'i Domestic (BeforePreisler's Domestic (After
Samples Collected February 200281-389-1489-15Preiitcr'i Domestic (BeforePreister'i Domestic (After
Samoles Collected Mav 200287-389-1489-1592-3A92-38AOI WellOI WellPreister'i Domestic (BeforePreister'i Domestic (After
Samoles Collected Aunist 200287-389-1289-1389-1489-15Preislcr'i Domestic (BeforePreistci'i Domestic (After
01-19700-DU60D01-19697-DU60AOI-19698-DU60B01-19786-DU75A01-I9787-DU75B01-19701-DU60E01-19702-DU60F
ryz-ms-EB-nr.02-I443-EB74A02-1444-EB74B02-1502-EB89A02-1503-EB89B
02-6069-EJ19F02-6066-EII9C02-6067-EJ19D02-63I5-EJ54A02-6316- EJ34B02-6070-EJI9G02-606S-EI19E02-63 17-EI54C02-6318-E154D
02-I0830-EQ82F02-I0825-EQ82A02-10826-EQ82B02-10827-EQ82C02-10828-EQI2D02-10832-EQ82H02-I0833-EQ821
Fldd Measurement]
pH(Htld)
25.0
26.3
NANANANA
6.355.885.026.756416846.98
6 605.826.186636.80
6.615616.586776476396.676926.92
6.446.257.186.265.296526.60
pH(lab)
25.0
26.3
7.47.27.07.1
6.6 J6.3 J4.8 J6.9 J6.5 J7.0 J7.1 J
6.?J5816 2 J7017.1 J
6.7 J5.216.5 J8.0 J6.4 J6.4 J6.7 J6.9 J691
6.79 JNANA
6.26 J532J7.20 J7.2 U
WaterTemperature
(°C) (Held)
NS
NE
NE
NANANANA
11.511.612.611.712.216.116.5
12.210.510.59010.1
10.414.213.912.212.013811913815.1
13.214614.114.114.015514.7
SpecificConductivity(umhos/cm)
(field)
NS
NE
NE
NANANANA
949660
2010569724949951
7666901430981970
7!511101210459558381726818860
7228205138581330820834
Total Metals (mt/L)
Zinc
5.0-
NE
NE
NANA
0.110.11
0.21910.1127
0.0300.006 U0.0460.019
0.13616.171.50.0090.008
0.10717.643.8
0.0160.0082.05124
0.0200.006
1.221.66NA10.571.20.0090.007
Sulfate
500
400
NANA3.114.0
34170
110026170130130
25360600120140
2528032019J15046210170180
3429930
2005808788
Cadmium
0.005
NE
NE
NANAUU
0.002 U0.0030.007
0.002 U0002 U0002U0.002 U
OOOlo0.0040.002
0.002 U0.002U
0.002 U0.0060.002
0002U0002U0.002 U0002U0.002 U0.002 U
0.002 UNANA
0.0040.007
0002 U0.002 U
Chromium
0.05
NE
NE
NANA
U
U
0.0090.0270.01 U0.1020.087
0.005 U0.005 U
O.Oii00190.008
0.005 U0.005 U
0.01 2 J0.006 J0.005 J0.190JO.OMJ
0.005 UJ0.005 UJ0.011 J
0.005 UJ
0.013NANA
0.005 U0.006
0.005 U0.005 U
Iron
10
1
NANANANA
0.0833133.33.631.68
0.05 U0.05 U
0.1 12.421.84
0.05 U005U
0.112.210.361.920.540.140.25
0.05 U0.05 U
0.62005 U
NA1.1619.1
0.05 U005 U
Uad
0.05
NE
NE
NANAUU
0.001 U0.005
0.001 U0.002
0.001 U0.001 U0.001 U
O.uOl 00.003
0.001 U0.001
0.001 U
0.001 U0.002 U0.001 U0.001 U0.001 U0.001 U0001 u0.004
0.001 U
0.001 UNANA
0.001 U0.001 U0.001 U0.001 U
Table 3Summary of Analytical Results Tor Inorganic CompoundsFifty-Second through SJity-F.n>l Quarter*November Zwl through February 2W4Lindsay Manufacturini Company
Well ID LabID
Federal MCL
Alternate Cleanup Level01- On Property
Alternate Cleanup Level1"* Off Property
Hktnrinil Data:Old Lindsay Public Supply Well (Sampled January 1977)Old Lindsay Public Supply Well (Sampled 01/24*311J261 (Sampled 01/J8/83)15262 (Sampled OI/S/S3)
Samoles Collected November 200211-389-1289-1489-1592-3A92-3BProcter's Domestic (Before)Preisler's Domestic (After
Samoles Collected February 200387-389-1489-15Preislcr's Domestic (Before)Pieiita' t Drinking Witer (2- 1 4-03)
Samolrs Collected Mav 200387-3
89-1289-1389-1489-1592-3A92-3BOlWellAOI WellPrcilter's Domestic (Before)Prdtter'l Domestic (After)
W-1632I-EY32ICTM63I3-EY32A02-16315-EY32C02-163I6-EY32D02-16403-EY52A02-I6404-EY52B02-16407-EY52E02-16408-EY52F
03-1565-FFwl03-1562-FF64F03-1563-FF64G03-1787-FCOOC03-1788-FGOOD
03-5556-FL81F03-555 1-FL81 A03-5552-FL81B03-5553-FL81C03-5554-FU1D03-588S-FM10D03-5886-FMIOE03-5555-FL81E03-5557-FU1G03-5882-FM10A03-5883-FMIOB
Field MeuuremeuU
pH(field)
2 5 0
26.3
NANANANA
6.586.376.515.636.696.507.077.10
6.595.715.866.75NA
6.476397.105.216.286.736.406.67
6.226.816.86
pH(lab)
25.0 '
263
7 47.27.07.1
6.78NA
5.87 J5.70 J6.92 J6.53 J7.02 J7.12J
6.855.4216.31 J7 . I 2 J5.84 J
676J666J7.3 J
5.I4J639J6981659J6.75 J6.42 J7.05)7.10J
WaterTemperature(°C) (field)
NS
NE
NE
NANANANA
11612.911.311.511.4I I
13.613.8
12.4
9810.812.9NA
12 112.5I I . 414.914.7
11.611.813.712.7
14.213.9
SpecificConductivity(umhos/cm)
(field)
NS
NE
NE
NANANANA
92011727541920497651749773
9825941530827NA
7749604953451040448516643434722737
Total Metals (mt/L!
Zinc
5.0-
NE
NE
NANA0.110.11
0.3491.967.0894.8
0.0070.0090.006
0.006 U
0.2596.T462.4
0.0130.008
0.1551.16
0.3267.2349.4
0.02 U0.018 U
6.17
2.260.014 U0.007 U
Sulfate
500
400
NANA3.114.0
31NA15073017
ISO8788
321W3390100
2.5 U
262903618034015
11014052nono
Cadmium
0.005
NE
NE
NANAUU
0.002V!NA
0.0030.007
0.002 U0.002 U0.002 U0.002 U
0.002 U0.0010.005
0.002 U0.002 U
0002U0002U0.002 U0.0030.005
0.002 U0.002 U0.002 U0.002 U0.002 U0.002 U
Chromium
005
NE
NE
NANAUU
0.012NA
0.0070.01 U0.0850.156
0.005 U0.005 U
00080.005 U0.005 U0.005 U0.005 U
0.0090.005 U0005 U0.005 U0.0090.1510.135
0.005 U0.005 U0.005 U0.005 U
Iron
10
1
NANANANA
0.210.071.0819.21.982.13
005 UO O S U
0.060.873.41
0.05 U0.05 U
0.190.05 U0.05 U
1.413673.111.700.260.24
0.05 UO O S U
Lead
0.05
NE
NE
NANAUU
0.001 UNA
0.0010.001 U0.001 U0.001 U
0.0010.001
0001 U0.00100020.002
0.001 U
0.001 U0.001 U0.001 Uo.ooi u0.001 U0.002
0.001 U0.00300040.003
0.001 U
Table 3Summary at Analytical Results for Inorjunic CompoundsKitty-Second through Sixty-Flrat QuartersNovember 2001 through February 2004Lindsay Muiufacturlnf Company
WtlllD LabID
Federal MCL
Alternate Cleanup Level"*- On Property
Alternate Cleanup Level01- Off Property
Historical Data:
Old Lindsay Public Supply Well (Sampled January 1977)Old Lindsay Public Supply Well (Sampled 01/28/83)15261 (Sampled 01/28/83)1526: (Sampled 01/28/83)
Sarrmles Collected Aumst 2003
87-389-14
89-15Seller Domestic (BFF)Preister's Domestic 2003 (BFF)Preister's Domestic (Old, Before)Preister's Domestic (Old. After)
Samoles Collected. November 200387-389-1289-13Z9-14
89-1592-3A92-3BPreister'i Domestic 2003 (BFF)
Preister'i Domestic 2003 (ALF)
Samnles Collected February 2004
87-389-1489-15Belief's Domestic (BFF)Preistcr'l Domestic 2003 (BFF)
03-11012-FT48O03-1I007-FT48J03-IIOI3-FT48P03-10784-FT15A03-10787-FTI5D
03-I0790-FTI5G03-10791-FT15H
03-15016-FZ86L03-15005-FZ86A03-150I4-FZ86I03-1S017-F7J6M03-15018-FZ86N03-150S3-GA01A03-15084-CAOIB03-15009-FZ86E03-150II-FZ86G
04-I527-GG9SJ04-I673-GHI7A04-1674-GH17B04-15IS-GG9IA04-I521-GG98D
Field Measurements
pHWeld)
25.0
26.3
NANANANA
6.44
6.255.616.676.896.766.88
6.526.127.256.115.826.716.336.846.87
5.755.965 17
6496.82
pH(lab)
25.0
>6.3
7.4
7.27.07.1
6.66 J
5.80 J5.8 U6.97J7 . I O J709J7.20 J
6.81 J6.37 J7.44J5.36)
6.13)6.986.55
7.06 J7.10J
6.68 J5.535.48
681 J6.92 J
WaterTemperature(°CM!leH)
NS
NE
NE
NANA
NANA
14.013.4
14.014.813.215.21 4 1
11.913.511.311.4
11.811.711.711.110.0
11. 113.011.67.7108
SpecificConductivity(umbos/cm)
(Held)
NS
NE
NE
NANANANA
654709
1123802729734759
80912185055051124501632691699
8544571417785698
Total Metals (mg/L)
Zinc
5.0-
NE
NE
NANA0.110.11
0.9478.6260.10.007
0.006 U0.008
0006U
0.4183.33
0.2126JS48.8
0.0130.010047
0.006 U
0.306 J46051.0
0018JO O I O J
Sulfate
500
400
NANA
3.114.0
47
190520
39537272
55570341503301414044
42
401306804645
Cadmium
0.005
NE
NE
NANAUU
0.002 U0003
0.0050002U0002U0002 U0002U
0.002 U0.002 U0.002 U0.0020.004
0.002 U0.002 U0.002 U
0.002 U
0.002 U0002U0.004
0.002 U0.002 U
Chromium
0.05
NE
NE
NANAUU
0.0080.005 U0.015
0.005 U0.005 U0.005 U0.005 U
0.0080.005 U0.006
OOOJU0005 U0.1760.018
0.005 U0.005 U
0010
0X50.010
0.005 U0.005 U
Iron
10
1
NANANANA
0331.0821.0
0.05 U0.05 U0.05 U0.05 U
0.070.05 U0.050.643.092.930.18
0.05 U0.05 U
0.14
0.6855.0
0.05 U0.05 U
Lead
0.05
NE
NE
NANAUU
0.001 U0.001 U0.001
0001 U0.001 U0.001 U0.001 U
0.0020.001
0001 U0.0020.002
0.002 J0.001 J0002
0.001 U
0.001 U0.0010.0020.0010.013
Noltj;
' EPA Komdary MCL*NA • NM Analyzed cr Not AvailableNS. No StandardJ • Indicate! Out value U an ctiiimie either became quality control oiicna wen not mei. or became die value w
U • [odicaiei Uur the cocnpouod wu analyzed ftr. but not detectedBold looi bdicatct remit repotted ii above or equal to the MCL (vac. cadmium, chromium, or lead) <x (be applicable tlieraaic cleanup level (pH. nilfaic, iron).
'" Reference letter from Stale of Nebnika to Lindsay Monufacturini Conp«ny dated 12/14*0
BPF • Before fin I filler in wttolc nouie truUiaOit (yiiem. initalled in W)3.NE - Not Eflabbibed
u below ibe quantitauon limit.
Table 4Summary of Analytical Results for Organic CompoundsFifty-Second through Si*ty- First QuartersNovember 2001 through February 2004Lindsay Manufacturing Company
Well IDLabm
EPA MCLAlternate Cleanup Level !- On Property
Alternate Cleanup Level '- Off Property
Samoles Collected November 200187-389-1289-1389- H89-1592-3A92-3BAOI WellOl WellPreisler's Domestic (Before)Prdsltr's Domes;;;: (After)
Samples Collected February 200287-389-1289-1389-1489-1592-3A92-3BAOI Well01 WellPreister's Domestic (Before)Preister's Domestic (After)
Samples Collected March 2002S9-12
Samples Collected Mav 200287-389-1289-1389-1489-1592-3A92-3 BAOI Well01 WellPreister's Domestic (Before)Preister's Domestic (After)'
Samples Collected lunc 200289-12
01-19700-DU60D01-19704-DU60H01-19705-DU60I01-19697-DU60A01-19698-DU60B01-19786-DU75A01-19787-DU75B01-19706-DU60J01-19699-DU60C01-I9701-DU60E
01-19702-DU60F
02-I446-EB74D02-1430-EB74H02-1451-EB74I02-1443-EB74A02-1444-EB74B02-1504- EB89C02-1505-EB89D02-1448-EB74F02-1445-EB74C02-1502-EB89A02-1503-EB89B
02-3391-EE94A
02-6069-EJ19F02-6064- EJ19A02-6065-EJI9B02-6066-EJ19C02-6067-EJ19D02-6315-EJ54A02-6316-EJ54B02-0670- EJ19G02-6068-EJ19E02-6317-EJ54C02-63 18-EJ54D
02-8175-EM04A
PH(field)
>5.0
>6.3
6.356.476885.885.026.756.416.276.446.846.98
6.606.437.225.826.186.796.456.286.736.636.80
6.35
6.616.676.735.616.586.776.476.396.676.926.92
6.83
PH(lab)
2 5.0
>6.3
O.bJNANA
6.3 J4.8 J6.9 J6.5 JNANA7.0 J7.1 J
6.7 JNANA
5.8 J6.2 JNANANANA
7.0 J7.1 J
NA
6.7 JNANA
5.2 J
6.5 J8.0 J6.4 J6.4 J
6.7]6.9 J6.9 J
NA
WaterTemperature
(C°) (field)
NS
ME
NE
11.513.111.311.612.611.712.213.912.116.116.5
12.211.09.710.510.510.611.613.511.39.010.1
14.0
10.412.211.614.213.912.212.0n.s11.913.815.7
13.5
SpecificConductivity(umh os/cm)
(field)
NS
NE
NE
9499204566602010569724463929949951
7669745286901430568670379642981970
967
785109053611101210459558381726818860
949
1,1-DCEGig/L)
7
NE
NE
19545 U5 U14012
5U5 U28
38J1.2
22245 U5 U11016
5 U5 U20511.1
44
14
185 U5 U675 U5 U5 U18801.9
19 J
1,1 -DC A
(pg/L)
NSNE
NE
5 U295 U5 U205 U5 U5 U5U4.71.0
5 US US U5 U7
5U5U5 U5 U5.20.6
16
5U5 U5 U5 U5 USU51)5 U51)7.21.2
5 U J
1,2-DCE
0"g/L)
170
NE
NE
5 U6
3D5U13
5 U5U5 U5U2.2
0.2 U
5 U5 U5 U5 U5 U5U5 U5U5U2.4
0.2 U
5 U
5U5 US U5 U5 U5 U5 U< ij
5 U3.1
0.2 U
5UJ
1,2-DCA(fgfL)
5NE
NE
5 U5 U5U5U5 U5 U5U5 U5 U0.3 J0.2 U
5 U5 U5 U5 U5 U5 U5 U5 U5 U
1.0 U0.2 U
5 U
5U5U5 U5 U5 U5 U5 U< I 1
5UL O U0.2 U
5UJ
1,1,1-TCAG"g/U
200
NE
NE
301205 U8
20010016
5 U35
77 J5.8
3023
S U5 U13011010
5 U9
943.6
70
2210
5 U5899711
C IJ
71309.2
11 J
TCEOig/U
5
NE
NE
5 U5 U5 U5 U5 U5 U5 U5 U5U0.5
0.2 U
S U5 U5 U5 U5 U5 U5 U5 U5 U1.0 U0.2 U
5 U
5 U5 U5 U5 U5 U5 US UC 1 T
5 Ul . O U0.2 U
5 U J
PCE0"g/L>
5
NENE
5170S U5
110428
5 U23
37 J0.2 U
670S U693486
S U3249
0.2 U
ISO
532
5 U7
56426
5 U3363
0.2 U
28J
TotalOrganic
<«g/L)
54379ND13
48315424ND861598
58117ND6
340174
16ND612025.3
280
4160ND12
21213917
1 *LJ
5828312
58
April 20O4.jl, (o'fani
Updated: 4/14/M04 Pip I of 6
Table 4Summary of Analytical Results for Organic CompoundsFifty-Second through Silly- First QuartersNovember 2001 through February 2004Lindsay Manufacturing Company
Well ID - - • -
EPA MCLAlternate Cleanup Level '- On Property
Alternate Cleanup Level '- Off Property
Samples Collected Aueust 200287-389-1289-1389-1489-1592-3A92-3 BA01 WellOI WellPreister's Domestic (Before)
Prcister's nomcstic (After)1
Samples Collected September 2002
Preister's Domestic (Before)
Preister's Domestic (After)
Seller's Domestic (After)
Seller's Stock Well
Samples Collected October 2002
Preister's Drinking Water (10-14-02)
Preister's Drinking Water (10-29-02)
Preister's Slock'
Doug Seller's Domestic
Ron Pfeifer's Domestic (House)
Old Moravec well
Labro
02-IOS30-EQ82F02-10825-EQ82A02-108 26-EQ82B02-10827-EQ82C02-10828-EQ82D02-11036-EQ96A02-11037-EQ96B02-10831-EQ82G02-10829-EQ82E02-10832-EQ82H
02-i0833-EQ32i
02-14197-EV12A
02-14198-EV12B
02-14199-EV12C
02-14200-EV12D
02-15259-EW83A
02-16080-EX88A
02-14785-EV91B
02-14784-EV91A
02-15917-EX65A
02-15918-EX65B
pH(Held)
>5-0
>6-3
6.446.257.186.265.296.585.766.096.326.52
6.60
NANA
NANA
NA
NA
NA
NA
NA
NA
pH(lab)
>5.0
£6.3
6.79 JNANA
6.26 J5.32 J
NANANANA
7.20 J7.21 J
NA
NA
NANA
NA
NA
NA
NA
NANA
WaterTemperature(C°) (field)
NS
NE
NE
13.214.614.114.1
14.012.012.912.911.615.514.7
NA
NANA
NA
NA
NA
NA
NA
NA
NA
SpecificConductivity(umh os/cm)
(Held)
NS
NE
NE
72282051385813305477114751207820
834
NANA
NA
NA
NA
NA
NANA
NA
NA
1,1-DCE<Jig/L)
7
NE
NE
12 J78 J5UJ12 J180 J
105 U5UJ120 JJOJ31 j
29
261.4
21
LOU
L O U
LOU
LOU
L O U
L O U
1,1-DCA
Oig/L)
NS
NENE
5UJ46J5UJ5UJ54 J5 U5 U5UJ45 J3.0 J
4.3 J
2.83.4
1U6.9
L O U
L O U
LOU
LOU
L O U
L O U
1.2-DCE(M6/U
170
NE
NE
5UJ5UJ5UJ5UJ50]5 U5U5 U JI6J3UJ
1.0 J
1.0
L O U
1U1U
L O U
L O U
L O U
LOU
L O U
L O U
U-DCA(Mg/U
5
NE
NE
5 U J5 U J5UJ5 U J5UJ5 U5 U5UJ5UJ3UJ
0.2 UJ
LOU
L O U1 U
1 U
L O U
L O U
L O U
LOU
L O U1 0 U
1,1,1-TCA
200
NE
NE
13J84 J5UJ19J
290 J77 JI 2 J5UJ290 J54 J
69 J
53
491.8
29
L O U
L O U
L O U
LOU
L O U
LOU
TCE
5
NE
NE
5UJ5 U J5UJ5UJ5UJ5 U5 U5 U J5UJ3UJ
0.2 UJ
LOULOU
1 U1 U
L O U
LOU
LOU
LOUL O U
LOU
PCE
5
NE
NE
5 U J260 J5UJ9J
170 J235 U5UJ110JJOJ
0.2 UJ
24
L O U
4.265
LOU
1.0 U
LOU
LOU
LOU
LOU
TotalOrganics
Oig/L)
25468ND40744
11012
ND581117
105
110
787.4
122
ND
ND
NDND
NDND
April 10Q4j.it farf cm
Table 4Summary of Analytical Results for Organic CompoundsFifty-Second through Sixty- First QuartersNovember 2001 through February 2004Lindsay Manufacturing Company
Well IDLabID
EPA MCL
Alternate Cleanup Level '- On Property
Alternate Cleanup Level '- Off Property
Samples Collected November 2002
87-3
89-12
89-13
89-14
89-15
92-3A 4
92-3B
AOI Well
01 Well
Preister's Domestic (Before)
Preister's Domestic (After)
Preistcr's Drinking Water (1 1-12-02)
Preisler's Drinking Water (1 1-25-02)
Seller's Domestic (Before)
Seller's Domestic (Afler)
Seller's Slock
Samples Collected December 2002
Preister's Drinking Water ( 1 2-09-02)
Preister's Drinking Water (12-19-02)
Prrister's Drinking Water (12-30-02)
Old Moravec Well
S9-11B
Samples Collected Januarv 2003
Preister's Drinking Water (01-13-03)
Preisler's Drinking Water ( Kitchen, 01-27-03)
Premier's Basement (between fillers, 01-27-03)
02-1 632 1-EY32I
02-16313-EY32A
02-163 I4-EY32B
02-163 15-EY32C
02-16316-EY32D
02-16403-EY52A
02-16404-EY52B
02-16322-EY32J
02-1C317-EY32E
02-16407-EY52E
02-16408-EY52F
02-16661-EZOOA
02-I7375-FA14A
02-16318-EY32F
02-16319-EY32G
02-16320-EY32H
02-18063-FB12A
02-19062-FC51B
02-19323-FC83A
02-19061-FC51A
02-19063-FC51C
03-361-FD57A
03-793-FE41A
03-794-FE41B
pH(field)
>5-0
>6-3
6.58
637
7.29
6.51
5.63
6.69
6.50
6.18
6427.07
7.10
NA
NA
6.69
6.74
6.75
NANA
NANA
NA
NA
NA
NA
PH(lab)
>5.0
£6.3
6.78
NA
NA
5.87 J
5.70 J
6.92 J
6.53 J
NA
NA7.02 J
7 . I 2 J
NA
NA
NA
NANA
NANA
NA
NA
NA
NA
NA
NA
WaterTemperature<C°) (field)
NS
MENE
11.6
12.9
11.4
11.3
11.5
11.4
11
13
12.8
13.6
13.8
NA
NA
14.8
14
10.9
NA
NA
NA
NA
NA
NA
NA
NA
SpecificConductivity(umhos/coi)
(field)
NS
NE
NE
920
1172
583754
1920
497
651514
850
749
773NA
NA
906902
825
NA
NA
NANANA
NANA
NA
1,1-DCEOig/L)
7
NE
NE
17
74
5.0 U
8130
65.0 U
5.0 U
3527
16
1.0 U
1.0 U
2.2
1.8
20
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
i,i-ncAOig/U
NS
NE
NE
5.0 U
335.0 U
5.0 U
365.0 U
5.0 U
5.0 U
82.9
23
1.0 U
1.0 U
1.31.07.8
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1,2-DCE(Pg/L)
170
NE
NE
5.0 U
7
5.0 U
5.0 U
405.0 U
5.0 U
5.0 U
5.0 U
1.5
1.0 U
1.0 U
LOU
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
U-DCAUg/L)
5
NE
NE
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
l . O U
1.0 U
l . O U
l . O U
l . O U
l . O U
l . O U
l . O U
l . O U
l.OU
1,1,1-TCAOig/L)
200
NE
NE
5.0 U
1105.0 U
15
180639
5.0 U
59
50
29
l . O U
l . O U
2.8
l . O U
30
1 0 U
l . O U
l . O U
l . O U
l . O U
l . O U
l . O U
l.OU
TCE&S/L)
TCEUg/L)
5 5
NE
NE
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
l . O U
l . O U
l . O U
l . O U
l . O U
l .OU
l.OU
l . O U
l . O U
l .OU
l . O U
l .OU
l . O U
l . O U
l .OU
NE
NE
8280
5.0 U
11
11028
65.0 U
35
28
l . O U
l .OU
l . O U
1.2
7
86
l .OU
l . O U
l . O U
l . O U
1.4
l . O U
l . O U
l . O U
i
TotalOrganics
0<g/L)
25504
ND
34
496
97
15ND
137
109
47
ND
ND
7.59.8144
ND
NDNDND
1.4
ND
ND
ND
Pige J o f 0
Table 4Summary of Analytical Results for Organic CompoundsFifty-Second through Siity- First QuartersNovember 2001 through February 2004Lindsay Manufacturing Company
Well IDLabED
EPA MCL
Alternate Cleanup Level '- On Property
Alternate Cleanup Level '• Off Property
Samples Collected February 2003
87-3
S9-10B
89-1 IB
89-12
89-13
89- 1*
89-15
92-3A
92-3B
OI Well
AOI Well
Seller's Domestic (Before)
Piaster's Irrigation
Preistcr's Drinking Water (02-14-03)
Prcisler's Drinking Water (02-24-03)
Preister's Domestic (Before)
Ben Pfeifer's House
Bd Luctkenhaus House
Ron Pfeifer's Domestic (House)
Samples Collected March 2003
Preisler's Drinking Water (03-17-03)
Prcisler's Domestic (Between filter on RO unit, 03-17-03)
Samples Collected May 2003
87-3
89-12
S9-I3
89-14
89-15
92-jA
92-3B
OI Well
AOI Well
Preisler's Domestic (Before)
Preister's Domestic (After)
03-I565-FF64I
03-1559-FF64C
03-1558-FF64B
03-1560-FF64D
03-1561-FF64E
03-1562-FF64F
03-1563-FF64G
03-1785-FGOOA
03-i7S6-FGOOB
03-1564-FF64H
03-1367-FF64K
03-1557-FF64A
03-1719-FF91A
03-1788-FGOOD
03-2050-FG52A
03-1787-FGOOC
03-1720-FF91B
03-1721-FF91C
03-1722-FF91D
03-2853-FH83A
03-2854- FH83B
03-5556-FL81F
03-555 1-FL81 A
03-5552-FL81B
03-5353-FL81C
03-5554-FL81D
03-58SJ-FM10D
03-5885-FM10E
03-5555-FL81E
03-5557-FL81G
03-5882-FM10A
03-5883- FM10B
PH(field)
>5.0
>6.3
6.59
6.91
6.85
5.70
6.57
5.71
5.86
6.68
6.34
6.40
6.10
669NANANA6.75
NANANA
NANA
6.47
6.39
7.10
5.2!
6.28
6.V3
6.40
6.67
6.22
6.81
6.86
PH(lab)
>5.0
>6.3
6.85
NANANANA
5.42 J
6.31 J
NANANANA
NA
NA
5.84 J
NA
7.12J
NA
NA
NA
NA
NA
6.76 J
6.66 J
7.3 J
5.14J
6.39 J
6.98 J
6.59 J
6.75J
6.421
7.05 J
7.10J
WaterTemperature
(C°) (Held)
NSNENE
12.4
12 1
10411.5
10.4
9.810.8
10.6
11.0
13.0
12.4
13.4
NANANA12.9
NANANA
NANA
12.1
12.5
11.4
14.9
14.7
11.6
11.8
13.7
12.7
14.2
13.9
SpecificConductivity(u mhos/cm)
(field)
NSNENE
982474
6541270
6055941530
505576805521746NANANA827
NA
NA
NA
NA
NA
774
960
495
3451040
448
516
643434
722737
1,1-DCE(Mg/L)
7
NENE
275.0 U
5.0 U
425.0 U
5.0 U
465
5.0 U
135.0 U
2.31.0 U
1.0 U
1.0 U
241.0 U
1.0 U
1.0 U
1.0 U
1.0 U
23SO
5.0 U
5.0 U
5813
5.0 U
105.0 U
4016
1,1-DCA(dg/L)
NSNENE
5.0 U
5.0 U
5.0 U
155.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
1.41.0 U
1.0 U
1.0 U
2.81.0 U
1.0 U
1.0 U
1.0 U
1.0 U
5.0 U
155.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
3.91.8
1,2-DCE(Kg/L>
170
NE
NE
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.41.0 U
1.0 U
1.0 U
1.0 U
1.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
S O U1.9
1.0 U
U-DCA
^g/L>
5
NENE
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0U
1.0 U
1.0 U
1,1,1-TCA
(Mg/U
200NENE
295.0 U
5.0 U
675.0 U
5.0 U
51655116
3.016
1.0 U
1.0 U
47
1.0 U
1.0 U
1.0 U
1.0 U
1.0 U
2445
5.0 U
5.0 U
768166
5.0 U
7123
TCE0"g/L)
5NENE
5.0 U
5.0 U
5.0 U
55.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
1.0 U
1.0 U
I . O U
1.0 U
I . O U
I . O U
I . O U
I . O U
I . O U
I . O U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
I . O U
I .OU
PCE0"B/L)
5
NE
NE
85.0 U
5.0 U
400
5.0 U
63829
5.0 U
16
5.0 U
9.33.4
I . O U
I . O U
27I . O U
I . O U
I .OU
I . O U
I .OU
11180
5.0 U
85337
5.0 U
175.0 U
41
I . O U
TotalOrganics
(dgrt.)
64NDND529ND6
13599540
6
16
5
ND
ND102NDND
ND
NDND
58290ND8
187131633ND15841
Table 4Summary of Analytical Results for Organic CompoundsFifty-Second through Sixty. First QuartersNovember 2001 through February 2004Lindsay Manufacturing Company
wcu n> LabID
EPA MCLAlternate Cleanup Level '- On Property
Alternate Cleanup Level '- Off Property
Samples Collected Aueust 200387-3 Diffusion Bag'81089-10BS9-11B89-1289-1389-14
89-1592-3A92-3BOI WellA01 WellTI Well Diffusion ISO' to 1521'Tl Well Diffusion 165' lo 167''Tl Well Diffusion ISO' to 182''
Seller Domestic (BFF)3
Prcister's Domestic 2003 (BFF)!
Prcisicr's Domestic (Old, Before)
Samples Collected November 2003
87-3
89-12'
89-1389-1489-1592 -3 A92-3BOI WellAOI WellBtller Domestic (BFF)Preister's Domestic 2003 (BFF)7
03-1 101 1-FT48N03-11012-FT48003-I1000-FT48C03-I1004-FT48G03-10999-FT48B03-1 1003-FT48F03-11001-FT48J03-11013-FT48P03-11001-FT48D03-11002-FT48E03-10998-FT48A03-11006-FT48103-11008-FT48K03-1 1009-FT48L03-I1010-FT48M
03-10784-FT1SA
03-10787-FT15D03-10790- FT15G
03-I5016-FZ86L
03-15005-FZ86A03-15014-FZ86J03-15017-FZ86M03-15018-FZ86N03-15083-GA01A03-15084-GA01B03-15012-FZ86H03-15013-FZ86I03-15006-FZ86B
03-15009-FZ86E
PH(Held)
>5.0
>6.3
NA6.44
6.756.906.057.336.255616.686.316.436.19NANANA
6.67
6.896.76
6.52
6.127.256 1 15.826.716.336.436.116.77
6.84
PH(lab)
>5.0
>6.3
NA
6.66 JNA
NA
NA
NA5.80)5.81 J
NANANANANANANA
6.97 J
7.10J7.09 J
6.81 J
6.37 J7.44 J586J6.13 J6.98655NANANA
7.06 J
WaterTemperature
(C°) (Held)
NS
NE
NE
NA
14.0
14.8
13.114.7
12.213.414.0
13.312.811.815.0NANA
NA
14.8
13.2
15.2
11.9
13.511.311.411.811.711.711.212.013.1
11.1
SpecificConductivity(umh os/cm)
(field)
NS
NE
NE
NA654490682125256770911234875871099482NANA
NA
802
729734
809
12185055051124501632881585780
691
1,1-DCEOig/L)
7
NE
NE
229.3
1.0 U1.0 U95
1.0 U4.1
84
3.7
1.0 U44
5.01.0 U1.0 U1.0 U
2.0
2.418
16
901.0 U2.1552.22.33512
1.0 U
1.4
1,1 -DC A0>g/U
NS
NE
NE
6.22.5
1.0 U1.0 U
74
1.0 U1.0 U
231.9
1.0 U7.1
1.81.0 U1.0 U
1.0 U1.4
1.0 U2.1
1.5
571.0 U1.0 U7.91.8
1.0 U8.82.1
I .OU
1.0 U
1,2-DCE0<g/L>
170
NE
NE
I .OUI.OUi .OUI . O U23
I . O UI .OU
22
i .OUI . O U
1.7I .OUI . O UI . O UI . O U
I . O U
I . O UI .OU
i.ou19
I . O UI . O U2.8
I . O UI . O U3.3
I . O UI . O U
I . O U
1U-DCA(fi&L)
5
NE
NE
I . O UI .OUI .OUI.OUI.OUI .OUI.OUI .OUl.u UI .OUI .OU101.1
I . O UI . O UI . O U
I . O U
I . O UI . O U
I . O U
5.0 UI . O UI . O UI . O UI . O UI . O UI . O UI .OUI . O U
I . O U
1,1,1-TCA0"6/L)
200
NE
NE
1714
I . O UI . O U170
I . O U7.2130535.7
619.2
I .OUI .OUI . O U
2.3
4.7
33
14
170I . O U4.4
71
44
6.0
58
13
I . O U
2.6
TCE<J<g/L>
5
NE
NE
I . O UI.OUI . O UI .OU8.0
I . O UI.OU
1.7
I . O UI . O UI . O UI .OUI . O UI . O U1 0 U
1 0 U
I . O UI . O U
I . O U
5.0 UI . O UI . O U1 0 UI . O UI . O UI . O UI . O UI . O U
I . O U
PCEOig/L)
5
NE
NE
4.4
7.0I . O U1.03405.4
6.882243.8405.6
I .OUI . O UI . O U
6.8
3.3
19
10
1904.4
5.637
224.4
29133.9
1.5
1Total
OrganicsOig/L)
.
50
33
ND
1
710518
343831C
154
22NDND
ND
13
1072
42
5264
12174
70
13134
40
4
6
April 2QW_tli(ori,miU [Killed: 4/14/J004
Table 4Summary of Analytical Results for Organic CompoundsFifty-Second tbrough Sixty- First QuartersNovember 2001 through February 2004Lindsay Manufacturing Company
Well IDLabID
EPA MCL
Alternate Cleanup Level l- On Property
Alternate Cleanup Level '- Off Property
SamDles Collected Februarv 2004
87-3
89-12
89-1389-14
89-15 '92-3A92-3B01 WellAOI WellSeller Domestic (BFF)
Prdsler's Domestic 2003 (BFF) '
04-1527-GG98J
04-1524-GG98G04-1525-GG98I04-1673-GH17A
04-1674-GH17B04-1528-GG98K04-1529-GG98L04-1525-GG98H04-1676-GH17D04-15 l8-GGy»A
04-1521-GG98D
PH(Held)
>5.0
>6.3
5.75
6.097.025.96
5.176.406.366.396.08
PH(lab)
2 5.0
26.3
6.68 J
NANA5.53
5.48NANA
NA
NA
6.49 1 6.8 1J
6.S2 | 6.92 j
WaterTemperature
(C°) (field)
NSNENE
11.1
13.310.513.0
11.610.610.311.512.57.710.8
SpecificConductivity(umhos/on)
(field)
NSNENE
854
11505124571417486579830559785698
1,1-DCEOig/L)
7
NE
NE
20
501.0 U1.0 U
1106.21.613121.01.1
1,1-DCA0<g/L)
NSNENE
2.217
1.0 U1.0 U
471.9
1.0 U1.0 U4.0
1.0 U
1.0 U
1J-DCEOig/L)
170
NENE
1.0 U
61
1.0 U1.0 U
481.0 U1.0 U1.0 U
1.31.0 U
1.0 U
U-DCA0"g/L)
5NENE
1.0 U
1.0 U1.0 U1.0 U
1.0 U1.0 U1.0 U1.0 U1.0 U1.0 U
1.0 U
1,1,1-TCA0«g/U
200NENE
1866
1.0 U1.0 U
200543.711181.21.6
TCE0<g/L)
5NENE
1.0 U
3.41.0 U1.0 U
3.91.0 U1.0 U1.0 Ul . O U1.0 U
l . O U
PCE(Mg/L)
5NENE
8.5220 J5.82.5120
263.11512
4.9 J
1.3
TotalOrganlcs
0»g/L)
49
3635.82.5529888.439476.1
4.0
BFF - Before first filter in whole house treatment system, installed in 8/03. 1,1-DCE = 1,1-Dichloroelhene1,1-DCA = 1,1-Dichloroethane1.2-DCE = total of cis-1.2-dichloroethene and trans-1.2-dichloroethene1.2-DCA = 1,2-Dichloroethane1.1,1 -TC A = 1,1.1 -TnchloroethaneTCE = Trichloroethene
PCE = Tctrachloroethene
Notes:NA = Not Analyzed or Not AvailableND = Not DetectedNS = No StandardJ = Indicates that value is an estimate either because quality control criteria were not met, or because the value was below the quamitaiion limit.U = Indicates that the compound was analyzed for, but not detected.Bold font indicates result reported is above or equal lo the MCL.1 Reference letter from Stale of Nebraska to Lindsay Manufacturing Company dated 12/14/00; Melhylene Chloride (0.4 ug/L) and acetone (1.2 ug/L) were reported in the May 2002 sample and acetone (2.6 ug/L) in the August 2002 sample.These compounds are believed to be the result of laboratory contamination and not representative of the sample.
1 Carbon tctrachloride was delected at 2.4 ug/L lo 2.5 ug/L . The MCL is 5 ug/L.1A field duplicate was collected at 92-3 A. 1,1 -DCE reported in the table is from the duplicate analysis. The concentration in the parent sample was <5 ug/L.52-Butanone was delected in this sample during the August 2003 sampling event. Beller'sDomestic (BFF) 22 ug/L, Preislcr's New Domestic (BFF) 31 ug/L. The source of 2-buianone is mostl ikely glueing material used in plumbing and well installation.6 Acetone was detected in these samples. Assumed to be associated with laboratory water used for filling diffusion bag samplers Trichlorofluoromcthane (2.6 ug/L) was also detected in the diffusion bag sample from M W87-3,7 Melhylene chloride was detected at 11 ug/L in sampled 89-12, but is believed to be the result of laboratory contamination and not representative of the sample. Carbon tetrachloride was detected atI. I ug/L in Preister's Domestic 2003 (BFF).
1 Carbon tetrachloride detected at 1.3 ug/L in Preister's Domestic 2003. Acetone (110 ug/L), carbon disulfide (1.0 ug/L), and 2-butanone (30 ug/L) detected in sample from 89-15.
April 2004 j!l lurtaniUpiUud: ^140004
ary of Analytic*] Remlti for Oriole Compoondi - Aufuit 2003 • February 2004Doin«tJc, Stock mod Irritation Welb DowBfrwIInt of F*cllllyLJndujr
!Well ID 1
EPA MO.
Alternate Cleanup Level !- OB Property - j
Alternate Cleanup Level'. Off Property
Samnln collected AUVIUL 3003
Beller Doroeiuc (BFF)1
BcllsrDornsiac (AJF)V
Beller Dometlic (ALF)1
Beller'j nock mil
Beller'i trri£iiion well (54278)
Preiiler'i Doiwilic 2003 (BFP)1
PrciHer'i. Dornettic 2003 (AFF)'
Preillcr-i Domettic 2003 (ALF/
Preiiler'l Domaic (old. before)
Preilter'i Dofflenic (old, after)
PreilKr1! R O. Unil in Kitchen
Preiller'i Dock welt1
Preiiler'l iirijalion well (33637)1
Old Moravec home well
Dive Chonon home well
Tom Jareclcj houie well
Ron Pfeirer'l home well
Ron Pfeirer'i Irrigation (6S239)
Lecter Kftpecty t>nu;e well
Jim KJuien home
Jim Kleiien Irrigation
Anthony KJufen (33172)
John Kltiun Irrigation (56241)
Weylin Neal Irrigilion (31798)
Tom Mcfitrik houie well
Richard Wagner Irrigation
Samnla Collected NoTembcr 2003Beller Dometlic (BFF)Belter Domeiuc (AFF)Beller Dometlic (ALF)
Preijler'i Domestic 2003 (BFFJ1
PreUter'i Domestic 2003 (AFF)Preliler'i Domestic 2003 CALF)
SamDlei Collected Tanunrv 1004Beller East Irrigation Well
SaniDlei Collected Pf bruirv 2004Beller Domestic (BFF)Beller Domestic (AFF)BeUcr Domestic (ALF)
Preiiler'i Domestic 2003 (BFFJ1
Prcisler'i Domestic 2003 (AFF)Prciiler'i Domestic 2003 (ALF)
UbUJ
03-10784.FT15A
03.1075S-FT15B
03-10786-FTUC
03-10802-FTlSS
03-10803-FT1ST
03-I0787-FT15D
03-I0788-PT15E
03.I07S9-FTI5P
03.10790-FT15G
03.10791-FT15H
03-10792-FTISI
03-10800-FT1SQ
03.I0801-FT15R
03-10793-FTISJ
03-107M-FT15K
03-10795 -FTiSL
03-10796-FTISM
03.I1I44-FT6SA
03.10797-FT15N
03.10798-FTUO
03-1114S-FT65B
03.11005-FT48H
03.I1I46.FT6SC
03-11147-FT6SD
03-10799-FT15P
03-II148-FT6SE
03-I5006-FZ86B03-IS007-FZ86C03-1SCC8-FZS6D
03-I5009-FZS6E03-13010- FZ26F03-ISOI1-FZ86G
04-7I9-GO17A
04-IM8-GO98AM-IS19-GG93B04-152&OO98C
04-I521-OC9SD04-1S22-OO9IE(H-1523-GG98F
Ipll |
Ilkld) :
JS.O !
16.3
667
6.74
6.87
6.67
b.81
689
6.92
6.79
6.76
6.88
NA
691
6.56
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
6.77NA6.73
6.84NA6.87
6.JS
6.496.576.6*
6.826.69670
pH(Ub)
2S.O
2 6 3
6.97 J
NA
NA
NA
NA
7.10J
NA
NA
7.09 J
7.20 J
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NANANA
706JNA
7 10 J
NA
6.8 UNANA
692JNANA
Water Temperature
(C°)(neld>
NS
Nl
NE
14.8
13.4
13.0
14.2
13.9
13.2
13.3
12.4
1J2
14.1
NA
14
13
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
13.1NA11.1
II 1NA100
123
7.79.510.6
10812.3130
SpedlleConduetlvttr(umboi/cm)
(IWd)
NS
NT!
NE
802
801
800
720
53S
729
711
732734
759
NA
695
749
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
780NA
j 777
691NA699
| 507!|| 7!5i 79!
79!
698697
1 685
1,1-DCE(MM
7
NE
NE
2.0
1.0 U
10U
33
1.0 U
24
1.0 U
1.0 U
11
17
1.0 U
I O U
1.3
1.0 U
1.0 U
l.OU
1.0 U
1.0 U
l .UU
1.0 U
1.0 U
I O U
l .OU
21
I O U
I O U
1 OUI O U1 OU
1.4l .OUl.OU
l .OU
1.0l .OUl.OU
1 1l.OUI O U
1,1-DCA(W/U
NS
HE
NE
1 4
l .OU
l.OU
15
l .OU
l .OU
l .OU
l .OU
2 1
3.3
I O U
I O U
1 OU
l .OU
1 OU
l.OU
1.011
l .OU
l . O U
1 OU
l .OU
l . O U
l . O U
1.5
I O U
l .OU
l .OUl .OUl .OU
l . O Ul . O U1 OU
l . O U
l .OUl.OUl.OU
l .OUl .OUI O U
U-DCEOUJ/L)
170
NE
NE
l . O U
l .OU
l.OU
l .OU
l .OU
l . O U
I O U
l .OU
l .OU
1.2
l .OU
I O U
l .OU
l.OU
l .OU
l.OUi onl .OU
l .OU
l . O U
l.OU
l . O U
I O U
I O U
l .OU
1 OU
l .OUl .OUl .OU
l .OUl .OUl . O U
l . O U
l . O UI O Ul.OU
l .OUl .OUl .OU
U-DCA(M/LI
5
MS
NB
I O U
l .OU
l.OU
l .OU
l .OU
I O U
l.OU
l.OU
l .OU
l .OU
I O U
I O U
l .OU
l.OU
l .OU
l .OUi o n
l.OU
l.OU
l . O U
l.OU
l .OU
l . O U
l . O U
I O U
I O U
l .OUl .OUl.OU
l .OUl .OUI O U
l .OU
l.OUl.OUl.OU
l .OUl .OUI O U
1.1,1-TCA
(W/LI
200
NE
NE
2.3
l .OU
l.OU
47
l .OU4 7
I O U
l.OU
33
47
I O U
I O U
2.0
I O U
1 OU
l.OU
I.OU
I O U
l .OU
1 OU
l . O U
l . O U
I O U40
l .OU
l .OU
l .OUl . O Ul .OU
261 OUI O U
l .OU
1.2l .OUl.OU
1.6l .OUl . O U
TCE(n/L)
5
NE
NE
I O U
l . O U
l.OU
1.3
l .OU
I O U
I O U
I O U
I O U
l .OU
I O U
I O U
l .OU
1 OU
l.OU
l.OU
LO U
l .OU
l .OU
l .OU
l . O U
l .OU
l .OU
l .OU
l .OU
l .OU
l .OUl . O UI O U
I O UI O UI O U
I O U
l . O Ul . O Ul.OU
I O Ul .OUI O U
PCEIM/LI
5
NE
NE
6.8
l .OU
I O U
130
l . O U
J.3l . O U
l . O U
19
l . O U
l .OU
l .OU
S.4
l .OU
l . O U
l.OU
l .OU
l . O U
l .OU
l . O U
1 OU
I O U
I O U
II1 OU
I O U
3.9l . O Ul .OU
1.3l . O U
'• l . O U
: i .ou1! 4gj
221 l .OU
1 3l .OU
; I O U
ToutOriauki
(M/U
13
ND
ND
226
ND
10
ND
ND
72
79
ND
ND
9
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SI
ND
ND
4NDND
6NDND
ND
6.12.2ND
40NDND
NA . Not Anilyud or Not AviJUblcND •• Not DetectedN:> - Nw SUniUniJ a Inilicmta tint VM]UC a ut eftiautc cither becuxc quality control criierii wot not met. m becuie the vdee wu bdow the quntiiatian limit.U = Udiuta Out the compoand wu uilyzcd for. bit BM detected.Bold font indicates result irporttd b ibovt ci «pml *> (he MCL.1 Reference letter from Sute of Nebncki to Linduy M«nnf»cttjinj Compuy dcteO I2/1MX)1 Ca.'tca LttmchJorak wu deucttd u 2 4 uft/L In tb* Stud. Well ud 2.5 ipL b the Inipaon Weil The MCL u i o»/T-~
'2-Baiajioiic wu detected in diii nmpk dnrini the ABgut 2003 tunpliai cvcnL Beller'f Domestic (BFF) 22 ag/L, BcQer'i Domeiuc (AFF) II ug/L, Beller'i Donmtic (ALF) 22 ng/L. Prtuier'i New Domeitk (BFF) 51 ag/LPwter'i New Damenic (AFF) vg/L. Ptaiter'f New Domeitic (ALP) llOog/L. Thcmvccof 2-bot.u.oae U molt likely gloei*4 milerial ued in pbunbinx and wdJ miullaUtoa.
4 Cuboautnchtonde wu deucvd at l.iig/L(No* lQOJ)..ndBFF » Before Ttnt filter in new treatment tynan.AFF •> After fin I filter in new tmocent tyitsa.ALP • After lait filter in new treatment cyRem.
U-DCE- U-Dich!on>cthenil.l-DCA* 1.1-Dichkxoethuwl.I-DCE • total of cii-l.2-dichJoroeil.cne and trwu-1.2-did.ioroelhene1.2-DCAa 1.2-DichlMoethuie .I.l.l-TCA- l.U-TrichloroelhincTCE • TrichloTOeOwoe
PCE - Tetnchloroelheae
K:VXU\LLAluy\:o04\K(Toni\A[n] IUpdated. VltfWH
IRRIGATION WELLS
DOMESTIC WELLS
MONITORING WELLS
REMEDIATED SOIL SOURCE AREA
KNOWN BOUNDARY OF VOC CONTAMINATION
' ASSUMED BOUNDARY OF VOC CONTAMINATION
Job No. 33750799
SCALE: r=BOOP
Figure 1
MONITORING AND INTERCEPTOR WELL LOCATION
I
Lindsay ManufacturingLindsay, Nebraska
Yr'J]//'V <<r?>n^:. ' -y- -fa /3^-kW
V.
fcM\Yffrm^•4-W-Uv —-,r-
\ •(' If ! v Nx *v r<\ ' < 'VV-v* f" .• J ^—\> •' ' •
\ • V 1-- X '• ---. - " t>-" •• '- — -. x •- -^T // ' / ' Vk ' - "S
S\ \ \ ^- •"*.-.* ''- r ••"•-- . '* ' . ^//// -'"/\ v ^ . f /
\\A ! v--^^r^4,^f.f^^^(^fe?to§
|i|p;lp^J^o' L)V$^^ %i:\C^:'
WELL IDENTIFICATION
^ '•;-. V; _ I
^F"Cl ...v :t":-
I = Irrigation
L,
O Ben Pfeifer (D)
O Eddy Luetkenhaus (D)
O Doug Seller (D)
O Ron Pfeifer (D)
O Old Moravec (D)
O Seller Domestic
O Beller Stock
O Beller Irrigation (#54278)
0 Preister Stock Well
(E) Preister Domestic (Old)
(^ Tom Jarecki (D)
(£ Lester Kopecky (D)
(E) Jim Klassen (D)
(J> Tom Mefstrik (D)
(J) John Klassen (D)
onitorin'g Boundary j) 'v//-^-"-$>x^^pv','n "(x .I'ir- '.^^^^3^d=^4f--====^=^^——^—4 • 7-''c~^^v
Hog Confinement c,1-
New Preister Domestic (2003) -;.
Beller New Stock Well (2003) 1
Dave Chohan(D) "/,
Beller East Irrigation Well ~
WeylanNeal(G31798)(l) ;-
Richard Wagner (I) :\
Anthony Klassen (G33172) (I) >s!
John Klassen (G56241) (I) !i
Ron Pfeifer (G68239) (I) ;•
Jim Klassen (I)\
Preister Irrigation Well(33637) -
New Irrigation Well,February 2004
'" y/---..1^-^- ""-v"\ ° X . ;XO>'- ••. v-,vv \ ••-., j.'
Area of known VOC groundwater contamination
Inferred extent of VOC groundwater contamination
SOURCE: USGS 7.5-minute topographic map, Lindsay, Nebraska, revised 1985
Job No. 33750799
('^^ii:Vi^^^T^^);&r$l:)j\ '•:-''' 0^ : ^
Figure 2Domestic Well Locations
URS Lindsay ManufacturingLindsay, Nebraska
33750799 23.cdr
7000
co
c0OCo
OO
1000
0 t^Vv.^~
< >
89-1 289-15
Date
Job No. 33750799
Figure 3
MW89-12 and MW89-15 Concentration Trends
URS Lindsay ManufacturingLindsay, Nebraska
_24.c*r
1200
89-15(Residual Source Area, Upper Aquifer Monitoring Well)
o'cTOS>o
cg
2co
89-12(Downgradient Upper Aquifer Monitoring Well/Interceptor Well)
7000
6000
5000
4000
3000
2000
1000
0
A. ;
Date
<f>o'cE1
O^
92-3A(Off-Property, Upper Aquifer Monitoring Well)
1000
200
wo'c03s>O15o ^~>- O)c -2-g|cd>oc
Date
92-3B(Off-Property, Deep Aquifer Monitoring Well)
Date
- Preister
- Preister NewDomestic 2003
ino'croS>O
co•
c
c
Preister Old Domestic (Before) &Preister New Domestic 2003 (BFF)
1200n
1000
Date
Job No. 33750799
Figure 4
Concentration/Time Trends for Total Organics forWells 89-15, 89-12, 92-3A, 92-3B, and Preister Domestic
URS Lindsay ManufacturingLindsay, Nebraska
APPENDIXA
IIII
1APPENDIX A
Laboratory Analytical Reports and Data Review Reports
I
I
Memo
Century Square1501 4th Avenue, Suite 1400Seattle, Washington 98101206.438.2700 Telephone206.438.2699 Fax
To:
From:
RE:
Info:
Date:
Roy Elliott, Lead Consultant
Renee Prochazka, Environmental ScientistKaren Mixon, Senior Chemist o-^
QA/QC Data Summary Review60* Quarterly Ground water Sampling (November 2003)Organic DataLindsay Manufacturing 33750799
FINAL
February 18,2004
The data quality review of 16 ground water samples and one trip blank collected from November 3 throughNovember 5, 2003 has been completed. The samples were analyzed for volatile organic compounds at AnalyticalResources, Incorporated (ART) located in Tukwila, Washington. The analyses were performed in general accordancewith EPA Method 8260B. A complete data package was received from the laboratory that included summary sampleresults and associated QA/QC data. The following samples are associated with laboratory case numbers FZ86 andGA01:
Well ARIID
89-12Seller's Domestic BFFSeller's Domestic AFFHeller's Domestic ALFPreister's Domestic 2003 BFFPreister's Domestic 2003 AFFPreister's Domestic 2003 ALFOI WellAOI Well89-13Duplicate (87-1)87-389-1489-1592-3A92-3BTrip Blank
FZ86AFZ86BFZ86CFZ86DFZ86EFZ86FFZ86GFZ86HFZ86IFZ86JF7KMFZ86LFZ86MFZ86NGA01AGA01BGA01C
The following comments refer to ARI's performance in meeting the quality control specifications describedin EPA Method 8260B. Data were qualified based on the method criteria and guidance provided in the EPAdocument "USEPA Contract Laboratory Program National Functional Guidelines for Organic Data Review",October 1999.
Samples were shipped by overnight delivery to the laboratory.' Cooler temperatures ranged from 2.0°C to5.2°C. A trip blank was not submitted with sample group FZ86. Data were not qualified based on the omission.
1. Holding Time - Acceptable
K:\005\LINDSAY\QTRLYDV\2003\November 2003\60th QTR.VOC.docPage 1 of 3
URS
VOCs 60th Quarter, November 2003February 18,2004
2. GC/MS Instrument Performance Check - Acceptable
3. Initial and Continuing Calibration - Acceptable except as noted below:
The percent relative standard deviation (%RSD) exceeded the method criteria of 15% for cis-l,3-dichloropropene,toluene, trans-1,3-dichloropropene and 2-hexanone in the initial calibration associated with samples from GAOl.The %RSD for vinyl chloride was exceeded in the initial calibration associated with samples from 1^86. Thelaboratory elected to reevaluate these compounds using quadratic equations with six calibration points. Sample datafor these compounds were assessed using quadratic curves. None of the compounds were identified in the associatedsamples and no data were qualified based on the initial calibrations.
The percent difference for 2-hexanone was -37.7 in the continuing calibration associated with samples from GAOl.2-Hexanone was not detected in the associated samples. The reporting limit for 2-hexanone in samples 92-3A, 92-3B and Trip Blank is qualified as estimated and flagged "UJ".
4. Blanks - Acceptable
5. Surrogates - Acceptable
6. Matrix Spike/Matrix Spike Duplicate (MS/MSD) - Acceptable except as noted below:
MS/MSD pairs were performed on samples "89-12" and "92-3A". The percent recoveries for several analytes wereoutside of the project criteria of 75% to 125% as shown below:
Sample: 89-12 (FZ86)Analyte2-CVE
Sample: 92-3A (GAOl)Analyte1,2-dichloropropaneToluene2-CVE
%Rec MS / MSPNot Recovered
%Rec MS / MSP124/126126/103Not Recovered
%RPDNot Calculable
%RPD1.120Not Calculable
Qualifier AssignedR (all samples)
Qualifier AssignedNoneNoneR (all samples)
Pata are not typically qualified based on MS/MSP results alone; however, results for 2-chloroethylvinylether(2-CVE) indicate no recovery likely due to the acidic pH of the sample. As all of the samples associated with FZ86and GAOl were acidified for preservation, results for 2-CVE in all samples are rejected and flagged "R". Since theMS recovery for toluene and the MSD recovery for 1,2-dichloropropane were high and neither compound wasdetected in the associated samples, no data were qualified. A summary of data qualifiers assigned to samples in casenumbers FZ86 and GAOl is provided above.
7. Laboratory Control Sample (LCS) - Acceptable except as noted below:
The recoveries for the following analytes in laboratory control samples (LCSs) and laboratory control duplicatesamples (LCSPs) associated with sample analyses were outside of the project limits of 75% to 125% as shownbelow:
LCS/LCSP11/18/03(GAOl)
Analyte1,2-dichloropropane
%Rec LCS/LCSP % RPP123/127 2.6
Qualifier AssignedNone
1,2-Pichloropropane was not detected in associated samples. As the recoveries for 1,2-dichloropropane were biasedhigh, the data were not qualified based on the LCS/LCSP results.
K:\005\LINDSAY\QTRLYDV\2003\November 2003\60th QTR.VOC.docPage 2 of 3
URS
VOCs 60"1 Quarter, November 2003February 18,2004
8. Internal Standards - Acceptable
9. Target Compound Identification - Acceptable
10. Field Duplicate - Acceptable
A field duplicate was collected at "87-3". Data were comparable between the parent and duplicate samples.
11. Other Items of Note:
The laboratory noted in their narrative for GA01 that due to a power surge the GCMS reset the date to December 31,2000 (default date when the system was rebooted). The date discrepancy was noted by the analyst and manuallychanged on each hardcopy and the associated logbooks, and verified by another analyst. All notations wereproperty initialed and dated.
12. Type of Review - Summary
Overall Assessment of Data:
The usefulness of the data is based on the EPA guidance documents listed above. Upon consideration ofthe information presented above, the data are acceptable except where flagged with data qualifiers that modify theusefulness of the individual values. Data qualifiers do not affect the use of the data in relation to the project consentdecree. The required monitoring compounds (1,1-dichloroethene, 1,1-dichloroethane, cis-l,2-dichloroethene, trans-1,2-dichloroethene, 1,2-dichloroethane, trichloroethene, 1,1,1-trichloroethane, and tetrachloroethene) do not requirequalifiers based on review of the data.
Data Qualifiers:
U - The analyte was analyzed for, but was not detected above the reported sample quantitation limit.
J - The analyte was positively identified; the associated numerical value is the approximate concentration of theanalyte in the sample.
UJ - The analyte was not detected above the reported sample quantitation limit. However, the reported quantitationlimit is approximate and may or may not represent the actual limit of quantitation necessary to accurately andprecisely measure the analyte in the sample.
R - The sample results are rejected due to serious deficiencies in the ability to analyze the sample and meet qualitycontrol criteria. The presence or absence of the analyte cannot be verified.
K:\005\LtNDSAY\QTRLYDVA2003\November 2003\60th QTR.VOC.doc URSPage 3 of 3
ORGANICS ANALYSIS DATA SHEET
Volatiles by Purge & Trap GC/MS-Method 8260BPage 1 of 1
Sample ID: 89-12 w<illSAMPLE
ANALYTICAL iRESOURCESINCORPORATED
Lab Sample ID: FZ86ALIMS ID: 03-15005Matrix: WaterData Release Authorized:Reported: 11/20/03
Instrument/Analyst: NT3/PABDate Analyzed: 11/10/03 19:06
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled: 11/03/03 :
Date Received: 11/05/03
Sample Amount: 1.0 mLPurge Volume -. 5.0 mL
CAS Number Analyte RL, Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-1
ChloromethaneBromome thaneVinyl Chloride.ChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1-Dichloroethanetrans - 1, 2 -Dichloroethenecis -1, 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2 -Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichloromethane1 , 2 -Dichloropropanecis-1, 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -TrichloroethaneBenzenetrans -1, 3 -Dichloropropene2 -ChloroethylvinyletherBromof orm4-Methyl-2-Pentanone (MIBK)2 -HexanoneTetrachloroetheae1,1,2,2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorornethane1,1, 2-Trichloro -1, 2, 2-trif luoroe
Reported in p-g/L (ppb)
Volatile Surrogate Recovery
d4-l,2-Dichloroethane 101%d8 -Toluene 98.8%Bromof luorobenzene 93.3%d4 -1, 2-Dichlorobenzene 99.5%
5 .05.05.05 .010255.05.05.05.05.05.05 .0255.05.025
5 .65.05.05 .05.05.05.05.0255 .025255.05.05.05 . 05.05.05.010
< 5.0 U< 5.0 U< 5.0 U< 5.0 U
11< 25 U
< 5.0 U9057
< 5 . 0 U19
< 5 .0 U< 5.0 U< 25 U170
< 5.0 U< 25 U
< 5.0 U< 5 .0 U< 5.0 U< 5.0 U< 5 . 0 U< 5 . 0 U< 5 . 0 U< 5.0 U< 25 a
< 5 .0 U< 25 U< 25 U190
< 5.0 U< 5.0 U< 5.0 U< 5.0 U< 5.0 U< 5.0 U-< 10 U
000011FORM I
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MS-Method 8260BPage 1 of 1
ANALYTICAL (RESOURCESINCORPORATED
Sample ID: Seller's Dom BFFSAMPLE
Lab Sample ID: FZ86BLIMS ID: 03-15006Matrix: Water ./Data Release Authorized:eyReported: 11/20/03
Instrument/Analyst: NT3/PABDate Analyzed: 11/10/03 19:29
CAS Number Analyte
QC Report No:Project:
FZ86-LMC Lindsay Manufacturing Co.Ground Water807
Date Sampled: 11/03/03Date Received: 11/05/03
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-1
Chlorome thaneBromome thaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1, 1-Dichloroethanetrans-l, 2-Dichloroethenecis-1, 2-DichloroetheneChloroform1 , 2 -Dichloroethane2-Butanone1, 1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2 -Dichloropropanecis-l, 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1, 2 -TrichloroethaneBenzenetrans-l, 3 -Dichloropropene2 -ChloroethylviiiyletherBromof orm4 -Me Lhyl - 2 - Pentanone (MIBK.)2-HexanoneTetrachloroetheiie1,1,2,2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2, 2-trif luoroe
Reported in pig/L (ppb)
Volatile Surrogate Recovery
d4-l, 2 -Dichloroethane 101%d8 -Toluene 99.0%Bromof luorobenzene 92.4%d4 -1 , 2 -Dichlorobenzene 102%
1.01.01.01.02 .05.01 .01.01. 01 .01.01.01.05 .01 .01.05.01.01.01 .01.01 .01 .01 .01 . 05.01.05.05.01.01.01.01.01.01.01.02.0
< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 2 . 0 U< 5 . 0 U< 1 . 0 U
' < 1.0 U< 1.0 U< 1.0 U< 1 . 0 U< 1. 0 U< 1.0 U< 5.0 U< 1 . 0 U< 1 . 0 U< 5.0 U< 1. 0 U< 1.0 U< 1 . 0 U< 1.0 U< i . o a< 1 . 0 U< 1 . 0 U< 1 . 0 U< 5.0 U U<^< 1.0 U< 5 . 0 U< 5 . 0 U3.9
< 1.0 U< 1. 0 U< 1.0 U< 1.0 U< 1. 0 U< 1.0 U,< 2 . 0 U
__ r>
000012FORM T
ORGAKICS ANALYSIS DATA SHEETVolatiles by Purge t Trap GC/MS-Method 8260BPage 1 of 1
ANALYTICAL |RESOURCESINCORPORATED
Sample ID: Seller's Dom AFFSAMPLE
Lab Sample ID: FZ86CLIMS ID: 03-15007Matrix: WaterData Release Authorized:^*Reported: 11/20/03
Instrument/Analyst: NT3/PABDate Analyzed: 11/10/03 22:33
CAS Number Analyte
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled-. 11/03/03
Date Received: 11/05/03
Sample Amount: 5.00 mLPurge Volume: 5.0 mL . .
RL Result
74-74-75-75-75-67-75-75-75-15615667-10778-71-56-10875-78-
87-83-
39
01-400-09-64-15-35-34 --60
321043-
-59-66--0693-55-23--05
3-365-
52
2
427-487-
10061-79-12479-71-
01--48
501-56-1
00-S43-
10061-11075-10859112779-108108100100
-75
202-6-8
25-2-10-78-1834--88-90-41-42
75-69-76-13-
---
5----41
•164
3745
Chlorome thaneBromome thaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1 -Dichloroethene1, 1 -Dichloroethanetrans -1,2 -Dichloroethenecis-1, 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2 -Butanone1/1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1, 2-Dichloropropanecis-1 , 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -Tr ichloroethaneBenzenetrans -1,3 -Dichloropropene2 -Chloroe thylvinyletherBromof orm4-Methyl-2-Pentanone (MIBK)2-HexanoneTetrachloroetherie1,1,2, 2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luoromethane1,1, 2-Trichloro-l, 2 , 2 -trif luoroe
Reported in pg/L (ppb)
Volatile Surrogate Recovery
d4-l, 2 -Dichloroethane 110%d8 -Toluene 99.1%Bromof luorobenzene 89.7%d4 -1, 2-Dichlorobenzene 104%
1111251111111511511111111515511111112
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
. 0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
< 1.< 1.< 1.< 1.< 2 .< 5.< 1.< 1 .< 1.< 1-< 1 .< 1 .< 1.< 5.< 1 .< 1.< 5.< 1.< 1.< 1 .< 1.< 1 .< 1 .< 1.< 1.< 5.< 1.< 5 .< 5.< 1.< 1.< 1.< 1.< 1.< 1.< 1.< 2.
0000000000000000000000000000000000000
uuuuuuuuuuuauuuuuuuaaauuuuuuuuuuuuuuu'
/o3
FORM I0 0 0 0 1 3
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge t Trap GC/MS-Method 8260BPage 1 of 1
Sample ID: Seller's
SAMPLE
ANALYTICAL /RESOURCESINCORPORATED
Dom af ter LF
Lab Sample ID: FZ86DLIMS ID: 03-15008Matrix: WaterData Release Authorized:Reported: 11/20/03
Instrument/Analyst: NT3/PABDate Analyzed: 11/10/03 22:56
CAS Number Analyte
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled: 11/03/03Date Received: 11/05/03
Sample Amount: 5 . 00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2i f\ Q ~l r\ ~\— ~ • — - — . j_ \j O-^ J. \J ~ _fc
591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-1
Chlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1-Dichloroethanetrans -1, 2-Dichloroethenecis-1, 2-DichloroetheneChloroform1 , 2 -Dichloroethane2 -Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2 -Dichloropropanecis-1, 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1, 2-TrichloroethaneBenzenetrans- 1, 3 -Dichloropropene2 -ChloroethylvinyletherBromoformA Ijl 4- 1*. « » 1 "> -T">rt ri H — in— IT-I 1-1 / M T T> V \-— t riCLfiyi — z — Fentanoiit: VMIBKJ2 -HexanoneTetrachloroethene1,1,2, 2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2 , 2-trif luoroe
Reported in g/L (ppb)
Volatile Surrogate Recovery
d4 -1 , 2 -Dichloroethane 112%dS-Toluene 99.5%Bromof luorobenzene 91.1%d4 -1 , 2 -Dichlorobenzene 103%
1.01.01.01.02.05.01 . 01. 01 . 01. 01 . 01. 01.05.01.01.05.01 . 01 .01 .01.01 . 01 . 01.01 . 05 . 01.05 . u5 .01.01.01, 01.01.01.01.02.0
< 1. 0 U< 1 . 0 U< 1.0 U< 1 . 0 U< 2 . 0 U< 5 . 0 U< 1.0 U< 1.0 U< 1 . 0 U< 1 . 0 U< 1.0 U< 1 . 0 U< 1 . 0 U< 5 . 0 U< 1 . 0 U< 1 . 0 U< 5 .0 U< 1 . 0 U< 1 . 0 U< 1. 0 U< 1 - 0 U< 1 . 0 U< 1. 0 U< 1.0 U< 1 - 0 U< 5 . 0 U \^<L< 1.0 U< 5 . U U< 5.0 U< 1 . 0 U< 1.0 U< 1. 0 U< 1. 0 U< 1.0 U< 1.0 U< 1.0 U,< 2.0 U
'
nt& \o >\ \~ \
-\
FORM I
000014
ORGAKICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MS-Method 8260BPage 1 of 1
Sample ID: Preister'SAMPLE
ANALYTICAL |RESOURCESINCORPORATED
Dom before FF
Lab Sample ID: FZ86ELIMS ID: 03-15009Matrix.- Water-Data Release Authorized:Reported: 11/20/03
Instrument/Analyst: NT3/PABDate Analyzed: 11/10/03 23:19
CAS Number Analyte
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled: 11/03/03Date Received: 11/05/03
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-1
Chlorome thaneBromome thaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulficle1,1 -Dichloroethene1 , 1-Dichloroethanetrans-1, 2 -Dichloroethenecis-1, 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2 -Butanone1, 1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2 -Dichloropropanecis - 1 , 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -TrichloroethaneBenzenetrans-1, 3 -Dichloropropene2 -ChloroethylvinyletherBromoform4-Methyl-2-Pentanone (MIBK)2 -HexanoneTetrachloroethene1, 1, 2, 2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luoronie thane1,1, 2-Trichloro- 1, 2, 2-trif luoroe
Reported in g/L (ppb)
Volatile Surrogate Recovery
d4-l, 2 -Dichloroethane 113%d8-Toluene 99.8%Bromof luorobenzene 89.8%d4 -1, 2 -Dichlorobenzene 105%
1111251111111511511111111515511111112
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
. 0
.0
. 0
.0
.0
.0
. 0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
< 1.< 1.< 1 .< 1.< 2.< 5.< 1.1.
< 1 .< 1 .< 1.< 1.< 1 .< 5 .2 .1.
< 5.< 1.< 1 .< 1.< 1.< 1 .< 1 .< 1.< 1.< 5.< 1 .< 5.< 5.1.
< 1.< 1.< 1.< 1.< 1.< 1.< 2.
0000000400000061000000000000050000000
uuuuuuu
uuuuuu
uuuuuuuuuuuuu
uuuuuu.u
FORM I000015
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MS-Method 8260BPage 1 of 1
ANALYTICAL (RESOURCESINCORPORATED
Sample ID: Preister's Dom after FFSAMPLE
Lab Sample ID: FZ86FLIMS ID: 03-15010Matrix: WaterData Release Authorized:Reported: 11/20/03
Instrument/Analyst: NT3/PABDate Analyzed: 11/10/03 23:42
CAS Number Analyte
QC Report Mo -. FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled: 11/03/03
Date Received: 11/05/03
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475 -34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-21 Dfl -1 Q- 1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-1
Chlorome thaneB romome thaneVinyl ChlorideChio roe thaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1 , 1-Dichloroethanetrans -1, 2-Dichloroethenecis-1, 2-DichloroetheneChloroform1 , 2-Dichloroethcme2-Butanone1, 1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2 -Dichloropropanecis-1, 3-DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -TrichloroethaneBenzenetrans-l , 3 -Dichloropropene2 -ChloroethylvinyletherBromoform
— 4— Methy-1 — 2 — Perrt-arrorre — fMIBK)2 -HexanoneTetrachloroethene1,1,2, 2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2, 2-trif luoroe
Reported in ng/l> (ppb)
Volatile Surrogate Recovery
d4 -1 , 2-Dichloroethane 117%d8 -Toluene 99.2%Bromof luorobenzene 89.7%dl -1 , 2-Dichlorobenzene 105%
1.01.01.01.02 .05.01. 01.01.01.01.01.01.05.01.01.05.01.01.01.01.01 .01.01.01 . 05.01.0b . 05.01.01.01.01.01.01.01.02.0
< 1.< 1.< 1.< 1.< 2 .< 5 .< 1.< 1.< 1.< 1.< 1.< 1.< 1.< 5.< 1 .< 1.< 5.< 1.< 1.< 1.< 1.< 1.< 1.< 1.< 1 .< 5 .< 1.< 5 .< 5 .< 1.< 1.< 1.
.< 1-< 1.< 1.< 1.< 2.
o ao u0 U0 U0 U0 U0 U0 U0 U0 U0 U0 U0 U0 U0 U0 U0 U0 U0 U0 U0 U0 U0 U0 U0 U0 U UQ.0 U0 U0 U0 U0 U0 U0 U0 U0 U0 U,0 U
t jL? ^\~y~°^\
000016FORK I
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MS-Method 8260BPage 1 of 1
ANALYTICAL (RESOURCES INCORPORATED
Sample ID: Preister's Dom after LFSAMPLE
Lab Sample ID: FZ86GLIMS ID: 03-15011Matrix: Water ,Data Release Authorized :<n»Reported: 11/20/03
Instrument/Analyst: NT3/PABDate Analyzed: 11/11/03 00:05
CAS Number Analyte
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled: 11/03/03
Date Received: 11/05/03
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-4'76-13-1
Chlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1 , 1-Dichloroethanetrans-1, 2-Dichloroethenecis-1, 2-DichloroetheneChloroform1 , 2 -Di chloroethane2 -Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodi chlorome thane1 , 2 -Dichloropropanecis-1, 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1, 2 -Trichloroe thaneBenzenetrans -1,3 -Dichloropropene2 -ChloroethylvinyletherBromoform4-Methyl-2-Pentanone (MIBK)2-HexanoneTetrachloroetheiie1,1,2,2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luoromethane1,1, 2-Trichloro- 1,2,2 -trif luoroe
Reported in /jg/L (ppb)
Volatile Surrogate Recovery
d4-l, 2-Dichloroethane - 115%d8 -Toluene 98.1%Bromof luorobenzene 88.9%d4 -1 , 2 -Dichlorobenzene 106%
1.01.01.01.02 .05.01.01.01.01.01.01.01.05.01.01 .05.01.01.01.01.01.01.01.01.05.01.05.05.01.01.01.01.01.01.01.02 .0
< 1. 0 U< 1.0 U< 1. 0 U< 1.0 U< 2. 0 U< 5.0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1. 0 U< 1.0 U< 5.0 U< 1. 0 U< 1.0 U< 5. 0 U< 1. 0 U< 1.0 U< 1.0 U< 1.0 U< 1. 0 U< 1. 0 U< 1.0 U< 1.0 U< 5. 0 U< 1.0 U< 5.0 U< 5.0 U< 1. 0 U< i.o a< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U,< 2 . 0 U
000017FORM I
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MS-Method 8260BPaqe 1 of 1
ANALYTICAL tRESOURCESINCORPORATED
Sample ID: O I wellSAMPLE
Lab Sample ID: FZ86HLIMS ID: 03-15012Matrix: WaterData Release Authorized:Reported: 11/20/03
Instrument/Analyst: NT3/PABDate Analyzed: 11/11/03 00 : 28
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled: 11/03/03
Date Received: 11/05/03
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
CAS Number Analyte RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-510B-88-3108-90-7100-41-4100-42-575-69-476-13-1
Chlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1-Dichloroetbanetrans-1, 2-Dichloroethenecis-1, 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2 -Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2 -Dichloropropanecis-1, 3-DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -TrichloroethaneBenzenetrans -1,3 -Dichloropropene2 -ChloroethylviriyletherBromoform4 -Me thyl - 2 - Pentanone (MIBK)2 -HexanoneTetrachloroethene1,1,2, 2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2 , 2-trif luoroe
1.01.01.01.02 .05. 01.01.01.01.01.01.01.05.01.01.05.01.01.01.01.01.01.01.01 . 05 .01.05 .05.01.01.01.01.01.01.01.02.0
< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 2.0 U< 5.0 U< 1. 0 U
358.8
< 1.0 U3 .3
< 1.0 U< 1.0 U< 5.0 U
58< 1. 0 U< 5. 0 U< 1.0 U< 1.0 U< 1 .0 U< 1.0 U< 1 . 0 U<: 1.0 U< 1.0 U< 1 . 0 U< 5.0 U t-^ 9~< 1.0 U< 5. 0 U< 5 . 0 U
29< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1. 0 U< 1.0 U-< 2.0 U
Reported in g/L (ppb)
Volatile Surrogate Recovery
d4-l,2-Dichloroethane 113%d8-Toluene 99.1%Bromofluorobenzene 87.7%d4-l,2-Dichlorobenzene 103%
V
000018
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MS-Method 8260BPage 1 of 1
ANALYTICAL /RESOURCES^INCORPORATED
Sample ID: A O I w&llSAMPLE
Lab Sample ID-. FZ86ILIMS ID: 03-15013Matrix: WaterData Release Authorized:1^Reported: 11/20/03
Instrument/Analyst: NT3/PABDate Analyzed: 11/11/03 00:51
CAS Number Analyte
QC Report No-. FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled: 11/03/03
Date Received: 11/05/03
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-1
Chlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1 , 1-Dichloroethanetrans - 1, 2-Dichloroethenecis - 1, 2 -DichloroetheneChloroform1 , 2 -Dichloroetharie2 -Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodi chlorome thane1 , 2 -Dichloropropanecis- 1 , 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -TrichloroethaneBenzenetrans -1, 3 -Dichloropropene2 -ChloroethylvinyletherBromoform4 -Methyl -2 -Pentanone (MIBK)2-HexanoneTetrachloroetherie1,1,2,2 -Tetrachloroe thaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2 , 2-trif luoroe
Reported in p.g/L (ppb)
Volatile Surrogate Recovery
d4-l, 2-Dichloroethane 116%d8 -Toluene 99.6%Bromof luorobenzene 89.3%d4-l, 2-Dichlorobenzene 105%
1 . 01.01.01.02.05.01.01.01.01. 01. 01.01.05.01.01.05 .01.01 .01.01.01.01.01.01.05.01 .05.05.01.01.01.01.01.01.01.02.0
< 1.0 U< 1.0 U< 1.0 U< 1. 0 U< 2 .0 U< 5.0 U< 1.0 U
122.1
< 1.0 U< 1. 0 U< 1. 0 U< 1.0 U< 5. 0 U
13< l.O U< 5.0 U< 1. 0 U< 1.0 U< 1.0 U< 1.0 U< 1. 0 U< 1. 0 U< 1. 0 U< 1.0 U< 5. 0 U< 1.0 U< 5.0 U< 5.0 U
13< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U;< 2.0 u'
FORM I000019
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MS-Method 8260BPage 1 of 1
Sample ID: 89-13 wellSAMPLE
ANALYTICAL jRESOURCESV
INCORPORATED
Lab Sample ID: FZ86JLIM.S ID: 03-15014Matrix: WaterData Release Authorized:'/'Reported: 11/20/03
Instrument/Analyst: NT3/PABDate Analyzed: 11/11/03 01:14
CAS Number Analyte
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807 .Date Sampled: 11/03/03 :
Date Received: 11/05/03
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-3V4-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-b110-75-875-25-2108-10-1 ' '591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-1
Chlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1 , 1 -Dichloroethanetrans -1, 2 -Dichloroethenecis -1 , 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2 -Dichloropropariecis -1, 3 -DichloropropeneTrichloroetheneDibrocnochlorome thane1,1,2 -Trichloroe thaneBenzenetrans -1,3 -Dichloropropene2 -ChloroethylvinyletherBromoform4-Methyl-2-Pentanone (MIBK)2 -HexanoneTetrachloroethene1,1,2, 2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luoromethane1,1, 2-Trichloro-l, 2, 2-trifluoroe
1.01.01. 01.02.05.01.01.01.01.01.01.01.05.01.01.05.01.01 .01.01.01.01.01.01 . 05.01.05 .05.01.01.01.01.01.01.01.02 .0
< 1. 0 U< 1. 0 U< 1 . 0 U< 1 .0 U< 2.0 U< 5 . 0 U< 1 . 0 U< 1 . 0 U< 1. 0 U< 1.0 U< 1.0 U< 1 . 0 U< 1.0 U< 5.0 U< 1 . 0 U< 1. 0 U< 5.0 U< 1.0 U< 1.0 U< 1 . 0 U< 1 . 0 U< 1.0 U< 1 . 0 U< 1.0 U< 1 . 0 U< 5 . 0 U U Cl_< 1.0 U< 5 . 0 U< 5 . 0 U4.4
< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U,< 2.0 U
Reported in p.g/L (ppb)
Volatile Surrogate Recovery
d4-l,2-Dichloroethane 116%de-Toluene 99.8%Bromofluorobenzene 89.2%d4-l, 2-Dichlorobenzene 105%
000020
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge fc Trap GC/MS-Method 8260BPage 1 of 1
Sample ID: DuplicateSAMPLE
ANALYTICAL JRESOURCESV
INCORPORATED
Lab Sample ID: FZ86KLIMS ID: 03-1501£>Matrix: WaterData Release AuthorizedReported: 11/20/03
=«/
Instrument/Analyst: NT3/PABDate Analyzed: 11/11/03 01:37
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled:
Date Received: 11/05/03
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
CAS Number Analyte RL Result
74-87-374 -83"- 975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1 .591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-1
ChloromethaneBromome thaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1 , 1 -Dichloroethanetrans -1 , 2-Dichloroethenecis-1, 2 -DichloroetheneChloroform1, 2 -Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2 -Dichloropropanecis-1, 3-DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -TrichloroethaneBenzenetrans -1,3 -Dichloropropene2 -ChloroethylvinyletherBromoform4-Methyl-2-Pentanone (MIBK)2-HexanoneTetrachloroetherie1,1,2,2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luoromethane1,1, 2-Trichloro-l, 2 , 2 -trif luoroe
Reported in g/L (ppb)
Volatile Surrogate Recovery
d4-l, 2 -Dichloroethane 117%d8-Toluene 100%Bromof luorobenzene 90.5%d4-l, 2 -Dichlorobenzene 106%
1.01.01.01.02.05.01.01.01.01.01.01.01.05.01.01.05 .01.01.01.01.01.01.01.01.05.01.05.05.01.01.01.01.01.01.01.02.0
< 1. 0 U< 1. 0 U< 1. 0 U< 1.0 U< 2 . 0 U< 5.0 U< 1 . 0 U
161.5
< 1.0 U< 1. 0 U< 1.0 U< 1.0 U< 5 .0 U
14< 1-0 U< 5 . 0 U< 1.0 U< 1. 0 U< 1. 0 U< 1.0 U< 1.0 U< 1.0 U< 1 . 0 U< 1.0 U< 5. 0 U< 1.0 U< 5.0 U< 5.0 U
10< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U'< 2.0 U
000021
FORM I
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MS-Method 8260BPage 1 of 1
ANALYTICAL IRESOURCESINCORPORATED
Sample ID: 87-3 wellSAMPLE
Lab Sample ID: FZ86LLIMS ID: 03-15016Matrix: WaterData Release Authorized:Reported: 11/20/03
Instrument/Analyst: NT3/PABDate Analyzed: 11/11/03 02:00
CAS Number Analyte
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled: 11/04/03
Date Received: 11/05/03
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-4
79-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-1
Chlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1, 1 -Dichloroethanetrans -1,2 -Dichloroethenecis-1, 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2 -Dichloropropanecis-1, 3 -DichloropropeneTrichloroetheneDibromochlorome thane1 , 1 , 2 -TrichloroethaneBenzenetrans - 1 , 3 -Dichloropropene2 -ChloroethylvinyletherBromoform4-Methyl-2-Pentanone (MIBK)2 -HexanoneTetrachloroethene1,1,2,2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1,2 -Trichloro -1,2,2 - tri f luoroe
Reported in /*g/L (ppb)
Volatile Surrogate Recovery
d4-l, 2 -Dichloroethane 116%d8 -Toluene 100%Bromof luorobenzene 88.8%d4 -1, 2 -Dichlorobenzene 105%
1.01.01.01.02.05 .01.01.01.01.01.01.01.05. 01.01.05-01.01.01.01.01 .01.01.01.05.01.05 .05.01.01.01.01.01.01.01.02 .0
< 1 .0 U< 1. 0 U< 1. 0 U< 1. 0 U< 2.0 U< 5 .0 U< 1. 0 U
161.5
< 1.0 U< 1 . 0 U< 1. 0 U< 1. 0 U< 5.0 U
14< 1.0 U< 5.0 U< 1. 0 U< 1 . 0 U< 1 . 0 U< 1. 0 U< 1.0 U< 1 . 0 U< 1.0 U< i. o u< 5.0 U H (2-< 1 .0 U< 5.0 U< 5.0 U
10< 1.0 U< 1. 0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U,< 2.0 U
, — x r>
000022
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MS-Method 82GOBPage 1 of 1
Sample ID: 89-14 wellSAMPLE
ANALYTICAL /RESOURCESINCORPORATED
Lab Sample ID: FZ86ML1MS ID: 03-15017Matrix: Water /Data Release Authorized : *»*Reported: 11/20/03
Instrument/Analyst: NT3/PABDate Analyzed: 11/11/03 02:23
CAS Number Analyte
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled: 11/04/03
Date Received: 11/05/03
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-30-7100-41-4100-42-575-69-476-13-1
Chlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1- Dichloroethene1, 1 -Dichloroethanetrans- 1 , 2 -Dichloroethenecis- 1, 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2 -Butanone1,1, 1-Trichloroe thaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1, 2-Dichloropropanecis-1, 3-DichloropropeneTrichloroetheneDibrocnochloromet.hane ;
1 , 1, 2 -TrichloroethaneBenzenetrans -1,3 -Dichloropropene2 -ChloroethylvinyletherBromoform4-Methyl-2-Pentanone (MIBK)2-HexanoneTetrachloroethene1,1,2,2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorofluoromethane1,1, 2-Trichloro-l, 2, 2-trif luoroe
Reported in g/L (ppb)
Volatile Surrogate Recovery
d4 -1,2 -Dichloroethane 114%d8 -Toluene 98.5%Bromof luorobenzene 87.8%d4 -1 , 2 -Dichlorobenzene 106%
1111251111111511511111111515511111112
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
. 0
.0
.0
.0
. 0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
. 0
.0
.0
.0
.0
.0
.0
< 1< 1< 1< 1< 2< 5< 1
2< 1< 1< 1< 1< 1< 54
< 1< 5< 1< 1< 1< 1< 1< 1< 1< 1< 5< 1< 5< 55
< 1< 1< 1< 1< 1< 1< 2
.0
. 0
.0
.0
.0
.0
. 0
.1
. 0
.0
. 0
.0,0. 0.4. 0.0.0.0.0. 0.0. 0.0.0. 0. 0. 0.0.6.0. 0. 0.0.0.0.0
uuuuuuu
uuuuuu
uuuuuuuuuuuuuu
uuuauU-u
FORM I000023
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MS-Method 8260BPage 1 of 1
Sample ID: 89-15 wellSAMPLE
ANALYTICAL |RESOURCESINCORPORATED
Lab Sample ID: FZ86NLIMS ID: 03-15018Matrix: Water /Data Release Authorized :^pReported: 11/20/03
Instrument/Analyst: NT3/JADate Analyzed: 11/11/03 11:47
CAS Number Analyte
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled: 11/04/03
Date Received: 11/05/03
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-1
Chlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1- Dichloroethene1, 1- Dichloroethanetrans -1, 2 -Dichloroethenecis-1, 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2 -Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2 -Dichloropropanecis-1, 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1, 2 -Tr ichloroethaneBenzenetrans -1,3 -Dichloropropene2 -ChloroethylvinyletherBromof orm4-Methyl-2-Pentanone (MIBK)2-HexanoneTetrachloroethene1,1,2,2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro- 1, 2 , 2-trif luoroe
1.01.01.01.02 .05.01.01.01.01.01.01.01.05.01.01.05.01.01.01.01.01.01.01.01.0
5.01.05 .05.01.01.01.01.01.01.01.02.0
< 1. 0 U< i . o a< 1 .0 U< 1 . 0 U< 2 . 0 U< 5.0 U< 1.0 U
557.9
< 1 . 0 U2.8
< 1 . 0 U< 1 . 0 U< 5 . 0 U
71< 1 . 0 U< 5.0 a< 1 . 0 U< 1 .0 U< 1 . 0 U< 1 . 0 U< 1 . 0 U< 1.0 U< 1.0 U< 1 . 0 U
< 5.0 U v-1 <^< 1 .0 U< 5 . 0 U
< 5 . 0 U37
< 1.0 U< 1 . 0 U< 1 . 0 U< 1.0 U< 1. 0 U< 1.0 U'< 2.0 U
Reported in //g/L (ppb)
Volatile Surrogate Recovery,.
d4-1,2-Dichloroethane 106%d8-Toluene 98.6%Bromofluorobenzene 92.1%d4-l,2-Dichlorobenzene '103%
000024
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 1 of 1
Lab Sample ID: GA01ALIMS ID: 03-15083Matrix: WaterData Release Authorized -Reported: 11/20/03
Instrument/Analyst: FINN1/PABDate Analyzed: 11/18/03 05:21
CAS Number Analyte
Sample ID: 92-3A wellSAMPLE
QC Report No: GA01-URS Corp.Project: LMC Lindsay Quarterly
807Date Sampled: 11/05/03Date Received: 11/06/03
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
ANAJLVTiCAL /RESOURCES'INCORPORATED
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42^-575-69-476-13-1
ChloromethaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1-Dichioroe thanetrans-1, 2-Dichloroethenecis -1 , 2 -DichloroetheneChloroform1, 2 -Dichloroethane2 -Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodi Chloromethane1 , 2 -Dichloropropanecis-1, 3-DichloropropeneTrichloroetheneDibromochlorome thane1 , 1 , 2 -TrichloroethaneBenzenetrans-1, 3-Dichloropropene2 -ChloroethylvinyletherBromoform4-Methyl-2-Pentanone (MIBK)2 -HexanoneTetracbloroethene1,1,2,2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro- 1, 2 , 2-trif luoroe
Reported in pg/L (ppb)
Volatile Surrogate Recovery
d4-l, 2 -Dichloroethane 106%d8 -Toluene 96.1%Bromof luorobenzene 93 . 6%d4-l, 2-Dichlorobenzene 104%
1.1.1.1.2 .5.1.1.1.1.1.1.1.5 .1.1.5 .1.
1.1.
1.
1.
1.1.
1.
5 .1 .5.5.1.1.1.1.1.1.1.2 .
000000000000000000000000000
0000000000
< 1< 1< 1< 1< 2< 5< 121
< 1< 1< 1< 1< 5
< 1< 5< 1< 1< 1< 1< 1< 1< 1< 1< 5< 1< 5< 5
< 1< 1< 1< 1< 1< 1< 2
.0
.0
.0
.0
.0
.0
.0
.2
.8
.0
. 0
. 0
. 0
- 0.44. 0. 0.0. 0.0. 0. 0. 0. 0. 0.0. 0
.0
.022.0.0.0.0. 0.0.0
auuuuuu
uuuuu
uuuuuuuuuuu 1uuu
uuuuuu.u
urr
ooooio
FORM I
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge t Trap GC/MSPage 1 of 1
Lab Sample ID: GA01BLIMS ID: 03-15084Matirix: WaterData Release Authorized:Reported: 11/20/03
Instrument/Analyst: FINN1/PABDate Analyzed: 11/18/03 09:30
CAS Number Analyte
Sample ID: 92-3B wellSAMPLE
QC Report No: GA01-URS Corp.Project: LMC Lindsay Quarterly
807Date Sampled: 11/05/03Date Received: 11/06/03
Sample Amount: 5.00 mLPurge Volume: 5-0 mL
ANALYTICAL,RESOURCES'INCORPORATED
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-.05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-1
Chlorome thaneBromome thaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1, 1-Dichloroe thanetrans -1,2 -Dichloroethenecis-1, 2 -DichloroetheneChloroform1, 2-Dichloroethane2 -Butanone1, 1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1, 2 -Dichloropropanecis-1, 3-DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -TrichloroethaneBenzenetrans -1,3 -Dichloropropene2 -ChloroethylvinyletherBromoform
" 4-Methyl-2-Pentanone (MIBK)2-HexanoneTetrachloroethene1,1,2,2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2, 2-trif luoroe
Reported in /ig/L (ppb)
Volatile Surrogate Recovery
d4-l, 2-Dichloroethane 114%dS-Toluene 97.4%Bromof luorobenzene 94.3%d4 -1, 2-Dichlorobenzene 106%
1.01.01.01.02.05 .01.01.01.01.01.01.01 .05.01.01.05.01 .01 . 01 . 01 .01.01 .01.01 . 05 .01.05 .05.01.01.01 .01.01.01 .01.02.0
< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 2 . 0 U< 5.0 U< 1. 0 U
2.3< 1.0 U< 1 . 0 U< 1.0 U< 1.0 U< 1.0 U< 5.0 U6.0
< 1.0 U< 5 . 0 U< 1 .0 U< 1 . 0 U"<. 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1 . 0 U< 1 . 0 U< 5.0 u ue< 1.0 U< 5 .0 U< 5 . 0 U VJtT4.4
< 1.0 U< 1.0 U< 1 .0 U< 1.0 U< 1.0 U< 1 . 0 U,< 2.0 U
^T
\
000011
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 1 of 1
Lab Sample ID: GA01CLIMS ID: 03-15065Matrix: WaterData Release AuthorizedReported: 11/20/03
Instrument/Analyst; FINN1/PABDate Analyzed: 11/18/03 09:58
CAS Number Analyte
Sample ID: Trip BlankSAMPLE
QC Report No: GA01-URS Corp.Project: LMC Lindsay Quarterly
807Date Sampled:Date Received: 11/06/03
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
ANALYTICAL jRESOURCESV
INCORPORATED
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3.107-06-278-93-371-55-656-23-5108-05-47S-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-1
ChloromethaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1-Dichloroethanetrans- 1, 2 -Dichloroethenecis-1, 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2-Butanon.e1, 1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateB romod i ch 1 o rome t hane1 , 2 -Dichloropropanecis-1, 3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2 -TrichloroethaneBenzenetrans -1,3 -Dichloropropene2 -ChloroethylvinyletherBromoform4-Methyl-2-Pent:anone (MIBK)2-HexanoneTetrachloroethene1 , 1 , 2 , 2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2, 2-trif luoroe
Reported in /jg/L (ppb)
Volatile Surrogate Recovery
d4 -1,2 -Dichloroethane 110%d8 -Toluene 93.4%Bromof luorobenzene 90.5%d4-l, 2-Dichlorobenzene 104%
111125111111151151111111151S511111112
. 0
.0
.0
.0
.0
. 0
. 0
. 0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
< 1< 1< 1< 1< 2< 5< 1< 1< 1< 1< 1< 1< 1< 5< 1< 1< 5< 1< 1< 1< 1< 1< 1< 1< 1< 5< 1< 5< 5< 1< 1< 1< 1< 1< 1< 1< 2
.0
. 0
. 0
.0
.0
.0
. 0
.0
.0
.0
. 0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
. 0
.0
.0
.0
. 0
uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu.u
o-r
000012
FORM I
Memo
Century Square15014th A venue, Suite 1400Seattle, Washington 98101206.438.2700 Telephone206.438.26<>9 Fax
To: Roy Elliott, Lead Consultant Info: FINAL
_ Renee Prochazka, Environmental Scientist _ . _. , n „„„,From: ., .,. c . _,, . Date: February 18,2004
Karen Mixon, Senior Chemist \j
QA/QC Data Summary Review60* Quarterly Groundwater Sampling (November 2003)
•"'-• Inorganic DataLindsay Manufacturing 33750799
The data quality review of 10 groundwater samples collected from November 3 through November 5, 2003 hasbeen completed. The samples were analyzed for total metals (cadmium, chromium, lead, iron and zinc)', sulfate and pHby Analytical Resources, Incorporated (ARI) located in Tukwila, Washington. The analyses were performed in generalaccordance with EPA Methods 6010B, 7421, 375.2 and 150.1, respectively and EPA's Contract Laboratory Program(CLP) Statement of Work (SOW). A complete data package was received from the laboratory that included summarysample results and associated QA/QC data. The following samples are associated with laboratory case numbers FZ86andGAOl:
Client ED ARI Number
89-12 F286APreister's Domestic 2003 BFF FZ86EPreister's Domestic 2003 ALF FZ86G89-13 FZ86JDuplicate (87-3) FZ86K87-3 FZ86L89-14 FZ86M.89-15 FZ86N92-3 A GA01A92-3B GA01B
The following comments refer to ARI's performance in meeting the quality control specifications outlined inEPA Methods 6010B, 7421, 375.2 and 150.1. Data were qualified based on the method criteria and guidance providedin the EPA document "USEPA Contract Laboratory Program National Functional Guidelines for Inorganic DataReview", July 2002.
1. Holding Time - Acceptable (Metals only)
2. Initial and Continuing Calibration - Acceptable except as noted below:
The recovery of lead from the low check standard (CRT) was 55%. Sample results for lead in samples 92-3A and 92-3Bare qualified as estimated due to the low detections associated with these samples.
3. Blanks - Acceptable
4. Laboratory Duplicate Analysis - Acceptable
K.\n05\L[NDSAY\QTRLYDV\2003\Novemlxi 2003\60thQTR-mcl.doc URS
Page 1 of 2
Inorganics 60th Quarter, November 2003February 18,2004
5. Field Duplicate - Acceptable
The field duplicate was collected at "87-3". Data were generally comparable between the parent and duplicate sample.
6. Matrix Spike Analysis (MS) -
The percent recovery for zinc from the matrix spike performed on sample "89-12" was 76%. The sample concentrationexceeded the spiking level by more than 4X. Data were not qualified based on the matrix spike recovery.
7. Furnace Atomic Absorption QC (Post Digest Spike) - Acceptable
8. ICP Interference Check Sample - Acceptable
9. Laboratory Control Sample - Acceptable
10. ICP Serial Dilution
Per the method, the serial dilution was not required as these samples do not constitute an unusual matrix.
11. SulfateandpH
The 24-hour hold time was exceeded by 24 to 48 hours for pH analysis of samples 89-12, Preister's Domestic 2003BFF, Preister's Domestic 2003 ALF, 87-3, 89-13, Duplicate, 89-14 and 89-15 in group FZ86. The pH results for thesesamples are qualified as estimated and flagged "J".
12. Type of Review - Summary
Overall Assessment of Data:
The usefulness of the data is based on the EPA guidance documents listed above. Upon consideration ofthe information presented above, the data are acceptable except where flagged with data qualifiers that modify theusefulness of the individual values.
Data Qualifiers:
U - The analyte was analyzed for, but not detected above the reported sample quantitation limit.
J - The analyte was positively identified; the associated numerical value is the approximate concentration of theanalyte in the sample.
UJ - The analyte was not detected above the reported sample quantitation limit. However, the reported quantitationlimit is approximate and may or may not represent the actual limit of quantitation necessary to accurately andprecisely measure the analyte in the sample.
R - The sample results are rejected due to serious deficiencies in the ability to analyze the sample and meet qualitycontrol criteria. The presence or absence of the analyte cannot be verified.
K \p05\LlNDSAYM3TRLYPV\2003\Novcmbcr 2003\«0th QTR m«.doc URS
Page 2 of 2
INORGANICS ANALYSIS DATA SHEETTOTAL METALSPage 1 of 1
Lab Sample ID: FZ86ALIMS ID: 03-15005Matrix: Water /Vi -u 11 s^^^Data Release Authorized:rxJ.*>^Reported: 11/18/03 \J
ANALYTICAL /RESOURCES ^INCORPORATED
Sample ID: 89-12 wellSAMPLE
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled: 11/03/03
Date Received: 11/05/03
PrepMeth
3010A3010A3010A3020A
3010A
PrepDate
11/07/0311/07/0311/07/0311/13/0311/07/03
AnalysisMethod
6010B6010B6010B74216010B
AnalysisDate
11/12/0311/12/0311/12/0311/17/0311/12/03
CAS Number
7440-43-97440-47-37439-89-6
7439-92-17440-66-6
Analyte
CadmiumChromiumIronLead
Zinc
00
00
RL
.002
.0050.05.001.006
s
mg/L
00
0
0
3
002005.05001
.33
'Q
Uurj
U-Analyte undetected at given RLRL-Reporting Limit
FORM-1000033
INORGANICS ANALYSIS DATA SHEETTOTAL METALSPage 1 of 1
Lab Sample ID: F286ELIMS ID: 03-15009Matrix: WaterData Release Authorized:Reported: 11/18/03
ANALYTICAL jRESOURCESV
INCORPORATED
Sample ID: Preister's Dom before FFSAMPLE
QC Report .No: FZ86-LMC Lindsay Manufac tu r i ng Co.Project: Ground Water
807Date Sampled: 11/03/03
Date Received: 11/05/03
PrepMeth
3010A3010A3010A3020A
3010A
PrepDate
11/07/0311/07/0311/07/0311/13/03
11/07/03
AnalysisMethod
6010B6010B6010B74216010B
AnalysisDate
11/12/0311/12/0311/12/0311/17/03
11/12/03
CAS Number
7440-43-97440-47-37439-89-67439-92-1
7440-66-6
Analyte
CadmiumChromiumIronLead
Zinc
00
00
RL
.002
.0050.05.001.006
00
00
mg/L
.002
.0050.05.002.047
Q
UuU
U-Analyte undetected at given RLRL-Reporting Limit
FORM-1 000036
INORGANICS ANALYSIS DATA SHEETTOTAL METALSPage 1 of 1
Lab Sample ID: FZ86GLIMS ID: 03-15011Matrix: WaterData Release AuthorizedReported: 11/19/03
ANALYTICAL |RESOURCESINCORPORATED
Sample ID: Preister's Dom after LFSAMPLE
QC Report No: FZ86-LMC Lindsay M a n u f a c t u r i n g Co.Project: Ground Water
807.Date Sampled: 11/03/03
Date Received: 11/05/03
PrepMeth
3010A3010A3010A3020A3010A
PrepDate
11/07/0311/07/0311/07/0311/13/0311/07/03
AnalysisMethod
6010B6010B6010B74216010B
AnalysisDate
11/12/0311/12/0311/12/0311/17/0311/12/03
CAS Number
7440-43-97440-47-37439-89-67439-92-17440-66-6
Analyte
CadmiumChromiumIronLeadZinc
00
00
RL
.002
.0050.05.001.006
00
00
mg/L
.002
.0050.05.001.006
"Q
uuuuu
U-Analyte undetected at given RLRL-Reporting Limit
FORM-I 000037
INORGANICS ANALYSIS DATA SHEETTOTAL METALSPage 1 of 1
Lab Sample ID: FZ86JLIMS ID: 03-15014Matrix: WaterData Release Author izedReported: 11/18/03
ANALYTICAL jRESOURCESV
INCORPORATED
Sample ID: 89-13 wellSAMPLE
QC Report No: FZ86-LMC Lindsay Manufac tu r i ng Co.Project: Ground Water
807Date Sampled: 11/03/03
Date Received: 11/05/03
PropMeth
3010A3010A3010A3020A3010A
PrepDate
11/07/0311/07/0311/07/0311/13/0311/07/03
AnalysisMethod
6010B6010B6010B74216010B
AnalysisDate
11/12/0311/12/0311/12/0311/17/0311/12/03
CAS Number
7440-43-97440-47-37439-89-67439-92-17440-66-6
Analyte
CadmiumChromiumIronLeadZinc
00
00
RL
.002
.0015
O.OS
.-001
.006
00
00
mg/L
.002
.006
0.05
.001
.212
Q
U
Cl
U-Analyte undetected at given RLRL-Reporting Limit
FORM-I 000038
INORGANICS ANALYSIS DATA SHEETTOTAL METALSPage 1 of 1
Lab Sample ID: FZ86KLIMS ID: 03-15015Matrix: WaterData Release Author!zedReported: 11/18/03 (/'
ANALYTICAL |RESOURCES'INCORPORATED
Sample ID: DuplicateSAMPLE
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled:
Date Received: 11/05/03
PrepMeth
3010A3010A
3010A
3020A
3010A
PrepDate
11/07/0311/07/03
11/0-7/03
11/13/03
11/07/03
AnalysisMethod
6010B6010B
601 OB
7421
6010B'
AnalysisDate
-11/12/0311/12/03
11/12/03
11/17/03
11/12/03
CAS Number
7440-43-97440-47-3
7439-89-67439-92-1
7440-66-6
Analyte
CadmiumChromium
Iron
Lead
Zinc
00
0
0
RL
.002
.005
0.05
.001
.006
0
0
0
0
mg/L
.002
.006
0.08
.002
.530
Q
U
U-Analyte undetected at given RLRL-Reporting Limit
FORM-I 000039
INORGANICS ANALYSIS DATA SHEETTOTAL METALSPage 1 of 1
Lab Sample ID: FZ86LLIMS ID: 03-15016Matr ix : WaterData Release Authorized]Reported: 11/18/03
ANALYnCAL iRESOURCESINCORPORATED
Sample ID: 87-3 wellSAMPLE
QC Report No: FZ86-LMC Lindsay M a n u f a c t u r i n g Co.Project: Ground Water
807Date Sampled: 11/04/03
Date Received: 11/05/03
PrepMeth
3 010 A3010A3010A3020A3010A
PrepDate
11/07/0311/07/0311/07/0311/13/0311/07/03
AnalysisMethod
6010B6010B6010B74216010B
AnalysisDate
11/12/0311/12/0311/12/0311/17/0311/12/03
CAS Number
7440-43-97440-47-37439-89-67439-92-17440-66-6
Analyte
CadmiumChromiumIronLeadZinc
00
00
RL
.002
.0050.05.001.006
00
0
0
J-
mg/L
.002
.0080.07.002.418
Q
U
•
U-Analyte undetected at given RLRL-Reporting Limit
FORM-1 000040
INORGANICS ANALYSIS DATA SHEETTOTAL METALSPage 1 of 1
Lab Sample ID: FZ86MLIMS ID: 03-15017Matrix: WaterData ReleaseReported: 11/18/03
ANALYTICAL jRESOURCESINCORPORATED
Sample ID: 89-14 wellSAMPLE
QC Report No: FZ86-LMC Lindsay M a n u f a c t u r i n g Co.Project : Ground Water
807Date Sampled: 11/04/03
Date Received:'11/05/03
PrepMeth
3010A
3010A3010A
3020A3010A
PrepDate
11/07/0311/07/0311/07/03
11/13/0311/07/03
Analysis AnalysisMethod
6010B6010B6010B74216010B
Date
11/12/0311/12/0311/12/03
11/17/03
11/12/03
CAS Number
7440-43-97440-47-37439-89-67439-92-1
7440-66-6
Analyte
CadmiumChromiumIronLead
Zinc
RL
0.0020.005On c,
0.001
0.006
mq/L
0.0020.0050. 64
0. 002
6.58
Q
U
U-Analyte undetected at given RLRL-Reporting Limit
FORM-1 000041
INORGANICS ANALYSIS DATA SHEETTOTAL METALSPage 1 of 1
Lab Sample ID: FZ86NLIMS ID: 03-15018Matrix: WaterData Release Authorized:/]^ .__,Reported: 11/18/03 /£/
ANALYTICAL |RESOURCES^INCORPORATED
Sample ID: 89-15 w«llSAMPLE
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled: 11/04/03
Date Received: 11/05/03
PrepMeth
3010A.3010A3010A3020A3010A
PrepDate
11/07/0311/07/0311/07/0311/13/0311/07/03
AnalysisMethod
6010B6010B6010B74216010B
AnalysisDate
11/12/0311/12/0311/12/0311/17/0311/12/03
CAS Number
7440-43-97440-47-37439-89-67439-92-17440-66-6
Analyte
CadmiumChromiumIronLeadZinc
0
0
0
0
RL
.002
.0050.05
.001
.006
mg/L
0.0040.0053.09
0.00248.8
' Q
U,
U-Analyte undetected at given RLRL-Reporting Limit
FORM-1 000042
INORGANICS ANALYSIS DATA SHEETTOTAL METALSPage 1 of 1
Lab Sample ID: GA01ALIMS ID: 03-15083Matrix: Water A,Data Release Authorized /WReported: 11/20/03 ff
ANALYTICAL (RESOURCESINCORPORATED
Sample ID: 92-3A wellSAMPLE
QC Report No: GA01-URS Corp.Project: LMC Lindsay Quar te r ly
807Date Sampled: 11/05/03
Date Received: 11/06/03
PrepMeth
3010A3010A3010A
3020A
3010A
PrepDate
11/12/0311/12/03
11/12/03
11/12/03
11/12/03
AnalysisMethod
6010B6010B6010B
74216010B
Analysis:Date
11/14/0311/14/0311/14/03
11/14/03
11/14/03
CAS Number
7440-43-97440-47-3
7439-89-6
7439-92-1
7440-66-6
Analyte
CadmiumChromiumIron
Lead
Zinc
00
00
RL
.002
.0050.05.001
.006
00
0
0
mg/L
.002
.176
2.93.002 1
.013
'.Q
U
S~.',
U-Analyte undetected at given RLRL-Reporting Limit
FORM-I 000019
INORGANICS ANALYSIS DATA SHEETTOTAL. METALSPage 1 of 1
Lab Sample ID: GA01BLIMS ID: 03-15084Matrix: WaterData ReleaseReported: 11/20/03
ANALYTICAL (RESOURCES'INCORPORATED
J
Sample ID: 92-3B wellSAMPLE
QC Report No: GA01-URS Corp.Project: LMC Lindsay Quarterly
807Date Sampled: 11/05/03
Date Received: 11/06/03
PrepMeth
3010A3010A3010A3020A3010A
PrepDate
11/12/0311/12/0311/12/0311/12/0311/12/03
AnalysisMethod
6010B6010B6010B74216010B
AnalysisDate
11/14/0311/14/0311/14/0311/14/0311/14/03
CAS Number
7440-43-97440-47-37439-89-67439-92-17440-66-6
Analyte
CadmiumChromiumIronLeadZinc
RL
0.0020.0050.050.0010.006
mg/L
0.0020.0180.18o.ooi :0.010
"Q
U
-J--
U-Analyte undetected at given RLRL-Reporting Limit
FORM-I 000022
INORGANICS ANALYSIS DATA SHEETLABORATORY ANALYSIS OF CONVENTIONAL PARAMETERSPage 1 of 1
ANALYTICAL iRESOURCESINCORPORATED
Sample ID: 89-12 wellSAMPLE
Lab Sample ID: FZ36ALIMS ID: 03-15005Matrix: WaterData Release Authorized:Reported: 11/17/03
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled: 11/03/03
Date Received: 11/05/03
AnalysisAnalyte
pH
Sulfate
Date & Batch
11/05/0311050311
11/14/0311140311
Method
EPA 150.1
EPA 375.2
RL
0.01
20
Units
std units
mg/L
Result
6.37
370
RL Analytical reporting limitU Undetected at reported detection limit
Report for FZ86 Received 11/05/03 000045
INORGANICS ANALYSIS DATA SHEETLABORATORY ANALYSIS OF CONVENTIONAL PARAMETERSPage 1 of 1
ANALYTICAL |RESOURCESV
INCORPORATED
Sample ID: Preister's Dom before FFSAMPLE
Lab Sample ID: FZ86ELIMS ID: 03-15009Matrix: WaterData Release Authorized:Reported: 11/17/03
AnaJ-yte
QC Report No: FZ86-LMC Lindsay Manufactur ing Co.Project: Ground Water
807Date Sampled: 11/03/03
Date Received: 11/05/03
AnalysisDate & Batch Method RL Units Result
Sulfate
11/05/03 EPA 150.1110503*1
11/14/03 EPA 375.211140311
0.01 std units 7.06
4.0 mg/L 44
RL Analytical reporting limitU Undetected at reported detection limit
Report for FZ86 Received 11/05/03 000046
INORGANICS ANALYSIS DATA SHEETLABORATORY ANALYSIS OF CONVENTIONAL PARAMETERSPage 1 of 1
ANALYTICAL iRESOURCESINCORPORATED
Sample ID: Preister's Dom after LFSAMPLE
Lab Sample ID: FZ86GLIMS ID: 03-15011Matr ix : WaterData Release Authorized:Reported: 11/17/03
QC Report No: FZ86-LMC Lindsay Manufac tu r ing Co.Project: Ground Water
807Date Sampled: 11/03/03
Date Received: 11/05/03
AnalysisAnalyte
pH
Sulfate
Date & Batch
11/05/03110503ttl
11/14/03111403*1
Method
EPA 150. 1
EPA 375.2
RL
0.01
4.0
Units
std units
mg/L
Result
7.10
42
RL Analytical reporting limitU Undetected at reported detection limit
V\\
Report for FZ86 Received 11/05/030 U 0 U 4 7
INORGANICS ANALYSIS DATA SHEETLABORATORY ANALYSIS OF CONVENTIONAL PARAMETERSPage 1 of 1
ANALYTICAL (RESOURCESINCORPORATED
Sample ID: 89-13 wellSAMPLE
Lab Sample ID: -FZ86JLIMS ID: 03-15014Matrix: WaterData Release Authorized:Reported: 11/17/03
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled: 11/03/03
Date Received: 11/05/03
Analysisnalyte Date & Batch
H 11/05/03110503ft!
ulfate 11/14/0311140311
Method
EPA 150. 1
EPA 375.2
RL Units
0.01 std units
2.0 mg/L
Result
7.44
34
RL Analytical reporting limitU Undetected at reported detection limit
Report for FZ86 Received 11/05/03 000048
INORGANICS ANALYSIS DATA SHEETLABORATORY ANALYSIS OF CONVENTIONAL PARAMETERSPage 1 of 1
ANALYTICAL iRESOURCESINCORPORATED
Sample ID: DuplicateSAMPLE
Lab Sample ID: FZ86KLIMS ID: 03-15015Matrix: WaterData Release Authorized:Reported: 11/17/03
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled:
Date Received: 11/05/03
AnalysisAnalyte
pH
Sulfate
Date & Batch
11/05/0311050311
11/14/03111403»1
Method
EPA 150.1
EPA 375.2
RL Units
0.01 std units
4 . 0 mg/L
Result
6.82
58
RL Analytical reporting limitU Undetected at reported detection limit
Report for FZ86 Received 11/05/03 000049
TNORGANICS ANALYSIS DATA SHEETLABORATORY ANALYSIS OF CONVENTIONAL PARAMETERSPage 1 of 1
ANALYTICAL jRESOURCESV
INCORPORATED
Sample ID: 87-3 wellSAMPLE
Lab Sample ID: FZ86LLIMS ID: 03-15016Matrix: WaterData Release Authorized:Reported: 11/17/03
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled: 11/04/03Date Received: 11/05/03
AnalysisAnalyte
PH
Date & Batch
11/05/0311050311
Method
EPA 150.1
RL
0.01
Units
std units
Result
6.81
Sulfate 11/14/03 EPA 375.211140311
4.0 mg/L 55
RL Analytical reporting limitU Undetected at reported detection limit
Report for FZ86 Received 11/05/03 000050
INORGANICS ANALYSIS DATA SHEETLABORATORY ANALYSIS OF CONVENTIONAL PARAMETERSPage 1 of 1
ANALYTICALRESOURCESINCORPORATED
Sample ID: 89-14 wellSAMPLE
Lab Sample ID: FZ86MLIMS ID: 03-15017Matrix: WaterData Release Authorized:Reported: 11/17/03
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled: 11/04/03Date Received: 11/05/03
AnalysisAnalyte
PH
Sulfate
Date & Batch
11/05/03110503S1
11/14/0311140311
Method
EPA 150.1
EPA 375.2
RL
0.01
10
Units
std units
mg/L
Result
5.86
150
RL Analytical reporting limitU Undetected at reported detection limit
Report for FZ86 Received 11/05/03 000051
INORGANICS ANALYSIS DATA SHEETLABORATORY ANALYSIS OF CONVENTIONAL PARAMETERSPage 1 of 1
ANALYTICAL iRESOURCESINCORPORATED
Sample ID: 89-15 wellSAMPLE
Lab Sample ID: FZ86NLIMS ID: 03-15018Matrix: WaterData Release Authorized:Reported: 11/17/03
QC Report No: FZ86-LMC Lindsay Manufacturing Co.Project: Ground Water
807Date Sampled: 11/04/03
Date Received: 11/05/03
Analysisalyte Date & Batch
11/05/0311050311
Ifate 11/14/03111403*1
Method
EPA 150.1
EPA 375.2
RL
0.01
20
Units
std units
mg/L
Result
6.13
330
RL Analytical reporting limitU Undetected at reported detection limit
U,A/03
Report for FZ86 Received 11/05/03000052
INORGANICS ANALYSIS DATA SHEETLABORATORY ANALYSIS OF CONVENTIONAL PARAMETERSPage 1 of 1
ANALYTICAL /RESOURCESINCORPORATED
Sample ID: 92-3A wellSAMPLE
Lab Sample ID: GA01ALIMS ID: 03-15083Matrix: Water s\Data Release Authorized:!/Reported: 11/20/03 L/
QC Report No: GA01-URS Corp.Project: LMC Lindsay Quarterly
807Date Sampled: 11/05/03Date Received: 11/06/03
Analysisnalyte Date & Batch
H 11/06/03110603*1
ulfate 11/14/0311140381
Method
EPA 150.1
EPA 375.2
RL
0.01
2.0
Units
std units
mg/L
Result
6.98
14
RL Analytical reporting limitU Undetected at reported detection limit
Report for GA01 Received 11/06/03 000025
INORGANICS ANALYSIS DATA SHEETLABORATORY ANALYSIS OF CONVENTIONAL PARAMETERSPage 1 of 1
ANALYTICAL iRESOURCESS
INCORPORATED
Sample ID: 92-3B wellSAMPLE
Lab Sample ID: GA01BLIMS ID: 03-15084Matrix: WaterData Release Authorized?Reported: 11/20/03 '
QC Report No: GA01-URS Corp.Project: LMC Lindsay Quarterly
807Date Sampled: 11/05/03
Date Received: 11/06/03
Analysis.nalyte Date & Batch
H 11/06/03110603S1
ulfate 11/14/03111403&1
Method
EPA 150.1
EPA 375.2
RL
0.01
10
Units
std units
mg/L
Result
6.55
140
RL Analytical reporting limitU Undetected at reported detection limit
Report for GA01 Received 11/06/03 000026
Memo
Century Square1501 4lh Avenue, Suite 1400Seattle, Washington 98101206.438.2700 Telephone206.438.2699 Fax
To: Roy Elliott, Lead Consultant Info: FINAL
From: Karen Mixon, Senior Chemist JV\ Date: April 6, 2004
QA/QC Data Summary ReviewSeller's East Irrigation - Water for Drilling of New Irrigation WellOrganic DataLindsay Manufacturing 33750799
The data quality review of one groundwater sample collected on January 23, 2004 has been completed. Thesample was analyzed for volatile organic compounds at Analytical Resources, Incorporated (ART) located in Tukwila,Washington. The analyses were performed in general accordance with EPA Method 8260B. A complete data packagewas received from the laboratory that included summary sample results and associated QA/QC data.. The followingsample is associated with laboratory case number GG17:
Well ARIID
Seller's East Irrigation GG17A
The following comments refer to ARTs performance in meeting the quality control specifications describedin EPA Method 8260B. Data were qualified based on the method criteria and guidance provided in the EPAdocument "USEPA Contract Laboratory Program National Functional Guidelines for Organic Data Review",October 1999.
Samples were'shipped by overnight delivery to the laboratory, however due to the weekend, there was a twoday delay in laboratory receipt The laboratory indicated that most of the ice in the cooler had melted and the coolertemperature was 5.0°C.
1. Holding Time - Acceptable
2. GC/MS Instrument Performance Check - Acceptable
3. Initial and Continuing Calibration - Acceptable except as noted below:
The percent relative standard deviation (%RSD) exceeded the method criteria of 15% for methylene chloride and 2-chloroethylvinylether (2-CVE) in the initial calibration analyzed on January 22, 2004. Due to the exceedances, thelaboratory elected to evaluate the compounds based on alternative curve types of linear or quadratic fit rather thanaverage response factor. The correlation coefficients were acceptable for all curves. These compounds were notdetected in the associated sample. Data were not qualified based on the use of alternative curves.
The percent difference for 2-hexanone in the continuing calibration analyzed on February 2, 2004 was 20.9%, abovethe method criteria of 20%. As 2-hexanone was not detected in the associated sample, data were not qualified.
4. Blanks - Acceptable
5. Surrogates - Acceptable
K:\005\UNDSAY\2004\Analytical DalaMst Qtr 2004\Beller East Irrigation VOC.doc URSPage I of 2
VOCs Beller East Irrigation, January 2004April 6, 2004
6. Matrix Spike/Matrix Spike Duplicate (MS/MSD) - Acceptable except as noted below:
A MS/MSD pair was performed on sample "Keller's East Irrigation". The percent recoveries for tetrachloroetheneand 2-CVE were outside of the project criteria of 75% to 125% as shown below:
Analvte %Rec MS / MSP % RPD Qualifier Assigned2-CVE Not Recovered Not Calculable RTetrachloroethene 70.6/81.6 14.5 None
Data are not typically qualified based on MS/MSD results alone; however, results for 2-CVE indicate no recoverylikely due to the acidic pH of the sample. As the sample was acidified for preservation, results for 2-CVE in thesample are rejected and flagged "R". Since 2 of the 3 recovery/RPD values were within the project criteria,tetrachloroethene was not qualified in the associated sample.
7. Laboratory Control Sample (LCS) - Acceptable
8. Internal Standards - Acceptable
9. Target Compound Identification - Acceptable
10. Field Duplicate - Not Applicable
11. Type of Review - Summary
Overall Assessment of Data:
The usefulness of the data is based on the EPA guidance documents listed above. Upon consideration ofthe information presented above, the data are acceptable except where flagged with data qualifiers trial modify theusefulness of the individual values. Data qualifiers do not affect the use of the data in relation to the project consentdecree.
Data Qualifiers:
U - The analyte was analyzed for, but was not detected above the reported sample quantitation limit.
J - The analyte was positively identified; the associated numerical value is the approximate concentration of theanalyte in the sample.
UJ - The analyte was not detected above the reported sample quantitation limit. However, the reported quantitationlimit is approximate and may or may not represent the actual limit of quantitation necessary to accurately andprecisely measure the analyte in the sample.
R - The sample results are rejected due to serious deficiencies in the ability to analyze the sample and meet qualitycontrol criteria. The presence or absence of the analyte cannot be verified.
K:\005\LINDSAY\2004\Analytical DataMst Qtr 2004\Beller East Irrigation VOC.doc URSPage 2 of 2
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 1 of 2
Lab Sample ID: GG17ALIMS ID: 04-789Matrix: WaterData Release Authorized:Reported: 02/06/04
Instrument/Analyst: FINN5/PABDate Analyzed: 02/02/04 20:54
CAS Number Analyte
ANALYTICAL (RESOURCES^INCORPORATED
Sample ID: Seller's «;ast irrigation11,693
QC Report No: GG17-URS Corp.'Project: LMC Lindsay Monthly
16657-002-005Date Sampled: 01/23/04Date Received: 01/26/04
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-2 '10061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-1
Chi orome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1 -Dichloroethene1, 1 -Dichloroethanetrans-1, 2 -Dichloroethenecis-1, 2-DichloroetheneChloroform1 , 2 -Dichloroethane2 -Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2 -Dichloropropanecis-1, 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -TrichloroethaneBenzenetrans-l , 3 -Dichloropropene2 -ChloroethylvinyletherBromoform4-M(=t-hyl -2-Pentanone (MIBK)2 -HexanoneTetrachloroethene1,1,2, 2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2 , 2 -trif luoroe
1.01.01.01. 02.05.01. 01.01 . 01 . 01 . 01 . 01.05.01 . 01 . 05.01.01.01.01.01.01.01.0.1 . 05 . 01. 05.05 . 01.01.01.01. 01.01.01. 02.0
< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 2.0 U< 5.0 U< 1 . 0 U< 1.0 U< 1.0 U< 1.0 U< 1 . 0 U< 1 . 0 U< 1.0 U< 5.0 U< 1 . 0 U< 1 . 0 U< 5.0 U< 1.0 U< 1.0 U< 1.0 U< 1 . 0 U< 1 . 0 U< 1.0 U< 1 . 0 U< 1 . 0 U< 5.0 U f(< 1. 0 U< 5.0 U< 5 . 0 U< 1.0 U< 1. 0 U< 1.0 U< 1. 0 U< 1 .0 U< 1.0 U< 1. 0 U< 2 . 0 U
Reported in ng/L (ppb)
Volatile Surrogate Recovery
d4 - 1 , 2 -Dichloroethane
FORM I
123%
ooooii
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 2 of 2
Lab Sample ID: GG17ALIMS ID: 04-789Matrix: WaterDate Analyzed: 02/02/04 20:54
CAS Number Analyte
ANALYTICALRESOURCESINCORPORATED
Sample ID: Seller's east irrigation11,693
QC Report No: GG17-URS Corp.Project: LMC Lindsay Monthly
16657-002-005
Result
d8-Toluene 104%Bromofluorobenzene 97.8%d4-1,2-Dichlorobenzene 104%
FORM I
000012
Memo
Century Square1501 4'h A venue, Suite 1400Seattle, Washington 98101206.438.2700 Telephone206.438.2699 Fax
To:
From:
RE:
Roy Elliott, Lead Consultant
Karen Mixon, Senior Chemist
Info:
Date:
FINAL
April 6, 2004
QA/QC Data Summary Review61st Quarterly Groundwater Sampling (February 2004)Organic DataLindsay Manufacturing 33150199
The data quality review of 16 groundwater samples, 2 laboratory trip blanks, and one field rinse blank collectedfrom February 2 through February 4, 2004 has been completed. The samples were analyzed for volatile organiccompounds at Analytical Resources, Incorporated (ART) located in Tukwila, Washington. The analyse.5 were performedin general accordance with EPA Method 8260B. A complete data package was received from the laboratory thatincluded summary sample results and associated QA/QC data. The following samples are associated with laboratorycase numbers GG98 and GH17:
Well AR1ID
Seller's Domestic BFF GG98AHeller's Domestic AFF GG98BSeller's Domestic ALF GG98CPreister's Domestic 2003 BFF GG98DPreister's Domestic 2003 AFF GG98EPreister's Domestic 2003 ALF GG98F89-12 Well GG98GOI Well GG98H89-13 Well GG98I87-3 Well GG98J92-3A Well GG98K92-3B Well GG98LTrip B lank (Lab Provided) GG98M89-14 Well GH17A89-15 Well GH17BDuplicate (Field Duplicate of 89-14) GH17CAOI Well GH17DTrip Blank (Rinse Blank) GH17ELab B lank (Lab Provided) GH17F
The following comments refer to ARI's performance in meeting the quality control specifications describedin EPA Method 8260B. Data were qualified based on the method criteria and guidance provided in the EPAdocument "USEPA Contract Laboratory Program National Functional Guidelines for Organic Data Review",October 1999.
Samples were shipped by overnight delivery to the laboratory. Cooler temperatures ranged from 2.8°C to4.0°C.
K:\005\LrNDSAY\2CKM\Analytical DataUst Qtr 2004\6Ist QTR.VOC.docPage 1 of 3
URS
VOCs 61" Quarter, February 2004April 6, 2004
1. Holding Time - Acceptable
2. GC/MS Instrument Performance Check - Acceptable
3. Initial and Continuing Calibration - Acceptable except as noted below:
The percent relative standard deviation (%RSD) exceeded the method criteria of 15% for several compounds in theinitial calibration analyzed on February 9, 2004 (associated with the samples included in SDG GGS'8) and formethylene chloride and 2-chloroethylvijiylether (2-CVE) in the initial calibration analyzed on January 22, 2004(associated with samples included in SDG GH17). Due to the exceedances, the laboratory elected to evaluate thecompounds based on alternative curve types of linear or quadratic fit rather than average response factor. Thecorrelation coefficients were acceptable for all curves. With the exception of 1,1,1-trichloroethane and carbontetrachloride, the compounds evaluated by methods other than the average response factor were not detected in theassociated samples. Data were not qualified based on the use of alternative curves.
The percent difference for 2-CVE in the continuing calibration analyzed on February 11, 2004 was 23.9%, above themethod criteria of 20%. The percent difference for 2-CVE in the continuing calibration analyzed on February 12,2004 was 23.3%. The 2-CVE data are rejected based on other QA/QC issues identified later in this report and arenot further qualified based on the continuing calibration results.
4. Blanks
Acetone (43 ug/L) and 2-butanone (13 ug/L) were detected in 'Trip Blank" (GH17E). This sample represents thewater used for decontamination of non-dedicated equipment. As the wells associated with this blank have dedicatedpumps, acetone and 2-butanone results reported as detected in associated samples are not qualified. Only onesample, 89-15 Well, contained acetone (110 ug/L) and 2-butanone (30 ug/L).
5. Surrogates - Acceptable
6. Matrix Spike/Matrix Spike Duplicate (MS/MSD) - Acceptable except as noted below:
MS/MSD pairs were performed on samples "Seller's Domestic BFF" and "89-14 Well". The percent recoveries forseveral analytes were outside of the project criteria of 75% to 125% and the relative percent differences (RPDs)were above 20% as shown below:
Sample: Seller's Domestic BFF (GG98A)Analvte %Rec MS / MSP % RPD Qualifier Assigned2-CVE Not Recovered Not Calculable R (all samples)Tetrachloroethene 72.8/96.4 25.0 J (parent sample only)
Sample: 89-14 Well (GHI7A)Analvte %Rec MS / MSP % RPD Qualifier Assiened2-CVE Not Recovered Not Calculable R (all samples)
Data are not typically qualified based on MS/MSD results alone; however, results for 2-CVE indicate no recoverylikely due to the acidic pH of the sample. As all of the samples associated with GG98 and GH17 were acidified forpreservation, results for 2-CVE in all samples are rejected and flagged "R". Since 2 of the 3 recoveries/RPD valueswere outside of the project criteria, tetrachloroethene in sample 89-14 is qualified as estimated and flagged "J".
7. Laboratory Control Sample (LCS) - Acceptable except as noted below:
The recoveries for the following analytes in laboratory control samples (LCSs) and laboratory control duplicatesamples (LCSDs) associated with sample analyses were outside of the project limits of 80% to 120% as shownbelow:
K:\005\LINDSAY\2004\Analytical DataMst Qtr 2004\61st QTR.VOC.doc URSPage 2 of 3
VOCs 61st Quarter, February 2004April 6, 2004
LCS/LCSD Analyte02/10/04 (GG98) 1,1,2-Trichloro-l, 2, 2-trifluoroethane
02/11/04 2-CVE(GG98G- 89-l2dji)Tetrachloroethene
ChlorobenzeneEthylbenzeneStyreneBromomethane1,1,1 -TrichloroethaneBromodichloromethanem,p- xylenes
02/12/04(GH17)
Carbon Disulfide
%Rec LCS/LCSD121/116
73.0/68.6122 / 104125/106126 / 103126/10788.2/76.891.0/76.292.0/78.8121.0/98.4
109/122
%RPD4.4
QualifierNone
Previously RejectedJ
NoneNoneNoneNoneJNoneNone
2-CVE was previously rejected based on MS/MSD results. l,l,2-Trichloro-l,2,2-CrifIuoroethane, chlorobenzene,ethylbeazene, styrene, and m,p-xylenes were not detected in associated samples and the LCS/LCSD results indicate ahigh bias. Results for these compounds in associated samples are not qualified. Bromomethane andbromodichloromethane were not detected in the associated samples and are not qualified. Tetrachloroethene, 1,1,1-trichloroethane, and carbon disulfide are qualified as estimated if detected in associated samples and flagged "J".Results reported as not detected are not qualified.
8. Internal Standards - Acceptable
9. Target Compound Identification - Acceptable
10. Field Duplicate - Acceptable
A field duplicate was collected at "89-14 Well". Data were comparable between the parent and duplicate samples.
11. Type of Review - Summary
Overall Assessment of Data:
The usefulness of the data is based on the EPA guidance documents listed above. Upon consideration ofthe information presented above, the data are acceptable except where flagged with data qualifiers that modify theusefulness of the individual values. Data qualifiers do not affect the use of the data in relation to the project consentdecree.
Data Qualifiers:
U - The analyte was analyzed for, but was not detected above the reported sample quantitation limit.
J - The analyte was positively identified; the associated numerical value is the approximate concentration of theanalyte in the sample.
UJ - The analyte was not detected above the reported sample quantitation limit. However, the reported quantitationlimit is approximate and may or may not represent the actual limit of quantitation necessary to accurately andprecisely measure the analyte in the sample.
R - The sample results are rejected due to serious deficiencies in the ability to analyze the sample and meet qualitycontrol criteria. The presence or absence of the analyte cannot be verified.
K:\005\LINDSAY\2004\Analytical DalaMst Qtr 2004\6lst QTR VOC.docPage 3 of 3
URS
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 1 of 1
Lab Sample ID: GG98ALIMS ID: 04-1518Matrix: WaterData Release Authorized -.Reported: 02/12/04
Instrument/Analyst: FINN1/JADate Analyzed: 02/10/04 16:34
ANALYTICAL/RESOURCES'INCORPORATED
Sample ID: Sellers Dom Before FFSAMPLE
CAS Number Analyte
QC Report No: GG98-URS Corp.Project-. LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/02/04Date Received: 02/04/04
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2103-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-11330-20-795-47-6
Chlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethen.e1, 1-Dichloroethanetrans-1 , 2 -Dichloroethenecis - 1, 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2 -Butanone1,1, 1-Trichloroe thaneCarbon TetrachlorideVinyl AcetateBromodi chlorome thane1 , 2 -Dichloropropanecis -1,3 -DichloropropeneTrichloroetheneDibromochlorome thane1, 1, 2-Trichloroethan.eBenzenetrans -1,3 -Dichloropropene2 -ChloroethylvinyletherBromoform4-Methyl-2-Pentanone (MIBK)2-HexanoneTetrachloroethene1 , 1,2,2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
Trichlorof luorome thane1,1, 2-Trichloro-l, 2 , 2-trif luoroem,p-Xyleneo-Xylene
Reported in ^g/L (ppb)
Volatile Surrogate Recovery
d4-l, 2 -Dichloroethane 103%d8-Toluene 100%Bromof luorobenzene . 94.7%d4-l, 2 -Dichlorobenzene 97.8%
1.01.01.01.02.05.01.01.01.01 . 01.01. 01. 05.01.01.05.01. 01. 01. 01.01.01 .01.01.05.01 . 05 .05.01.01. 01.01.01 .01 . 0
1.02 .01. 01.0
< 1. 0 U< 1.0 U< 1.0 U< 1.0 U< 2 .0 U< 5.0 U< 1.0 U1.0
< 1.0 U< 1 .0 U< i .0 a< 1 .0 U< 1 . 0 U< 5 .0 U1.2
< 1 .0 U< 5.0 U< 1. 0 U< 1 .0 U< 1 . 0 U< 1 .0 U< 1.0 U< 1 .0 U< 1.0 U< 1.0 U< 5.0 U< 1 . 0 U< 5.0 U< 5.0 U4.9
< 1 . 0 U< 1 . 0 U< 1.0 U< 1 . 0 U< 1 . 0 U< 1.0 U< 2 . 0 U< 1. 0 U< 1.0 U
-
;p
000013
FORM I
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 1 of 1
Lab Sample ID: GG98BLIMS ID: 04-1519Matrix: WaterData Release Authorized :/j^Reported: 02/12/04
Instrument/Analyst; FIWN1/JADate Analyzed: 02/10/04 17:02
ANALYTICAL jRESOURCESy
INCORPORATEDSample ID: Sellers DOM after FF
SAMPLE
QC Report No: GG98-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/02/04Date Received: 02/04/04
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
CAS Number Analyte RL Result
74 -87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23 -5108-05-475-27 -478 -97 -510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-11330-20-795-47-6
Chlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1 -Dichloroethanetrans -1,2 -Dichloroethenecis-1, 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2 -Butanone1,1, 1-TrichloroethaneCarbon Tetrachlor ideVinyl AcetateB romod i ch 1 o rome thane1,2- Dichloropropanecis-1, 3 -DichloropropeneTrichloroeCheneDibromochlorome thane1,1,2 -Trichloroe thaneBenzenetrans-1, 3 -Dichloropropene2 -ChloroethylvinyletherBromoform4-Methyl-2-Pentanone (MIBK)2-HexanoneTetrachloroethene1,1,2 , 2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2, 2 -trif luoroem,p-Xyleneo-Xylene
Reported in pg/L (ppb)
Volatile Surrogate Recovery
d4 -1, 2 -Dichloroethane 104%d8-Toluene 98.9%BromoEluorobenzene 95.0%d4 -1, 2 -Dichlorobenzene 98.5%
1 . 01.01. 01.02.05.01.01. 01. 01.01.01.01.05 . 01 .01.05 .01 . 01 . 01.01 . 01 . 01 .01. 01 . 05 . 01.05.05.01.01.01.01. 01. 01.01. 02.01.01. 0
'
< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 2 . 0 U< 5 .0 U< 1 . 0 U< 1 . 0 U< 1 . 0 U< 1.0 U< 1.0 U< 1. 0 U< 1- 0 U< 5.0 U< 1 . 0 U< 1. 0 U< 5 . 0 U< 1 . 0 U< 1 . 0 U< 1 . 0 U< 1 . 0 U< 1. 0 U< 1.0 U< 1.0 U< 1 . 0 U< 5 . 0 U ^< 1. 0 U<• 5_0 -U< 5 . 0 U2.2
< 1. 0 U< 1.0 U< 1. 0 U< .1.0 U< 1.0 U< 1.0 U< 2 .0 U< 1.0 U< 1 . 0 U
Km 'I'/OM
000014
FORM I
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 1 of 1
ANALYTICALRESOURCESINCORPORATED
Sample ID: Sellers Dom After lastFilter
Lab Sample ID: GG98CLIMS ID: 04-1520Matrix: WaterData Release Authorized:Reported: 02/12/04
QC Report No: GG98-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/02/04
Date Received: 02/04/04
nt/Analyst: FINN1/JA Sample Amount:lyzed: 02/10/04 17:30 Purge Volume:
CAS Number Analyte
74-87-374-83-975-01-475-00-375-09-267-64 -175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108 -10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-11330-20-795-47-6
Chlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, l-Dichloroethanetrans- 1, 2-Dichloroethenecis-1, 2-DichloroetheneChloroform1 , 2 -Dichloroethaine2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2 -Dichloropropanecis-1, 3-DichloropropeneTrichloroetheneDibromochlorome thane1,1, 2-TrichloroethaneBenzenetrans-1, 3 -Dichloropropene2 -ChloroethylvinyletherBromoform4 -Methyl-2-Pentanone (MIBK)2-HexanoneTetrachloroethene1 , 1 , 2 , 2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2 , 2-trif luoroem, p-Xyleneo-Xylene
5.00 mL5. 0 mL
RL Result
1. 01 . 01 .01 .02 . 05 .01.01.01 .01 .01.01.01.05 .01 . 01.05 .01.01. 01 . 01-01.01.01.01.05.01 . 05 . 05 . 01.01 . 01 . 01.01.01.01.02.01. 01 . 0
< 1.0 U< 1 . 0 U< 1 .0 U< 1 .0 U< 2 .0 U< 5 .0 U< 1.0 U< 1.0 U< 1 .0 U< 1 .0 U< 1 .0 U< 1.0 U< 1.0 U< 5.0 U< 1.0 U< 1.0 U< 5.0 U< 1 .0 U< 1 . 0 U< 1 . 0 U< 1 . 0 U< 1.0 U< 1 . 0 U< 1.0 U< 1 . 0 U< 5.0 U< 1 . 0 U< 5 .0 U< 5 . 0 U< 1.0 U< 1 . 0 U< 1 . 0 U< 1.0 U< 1.0 U< 1 .0 U< 1.0 U< 2 .0 U< 1 .0 U< 1 .0 U
Reported in ^g/L (ppb)
Volatile Surrogate Recovery
d4-l,2-Dichloroethane 103%d8-Toluene 101%Bromofluorobenzene 97.4%d<l-l, 2-Dichlorobenzene 96.8%
0/0
000015
FORM I
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage. 1 of 1
Lab Sample ID: GG98DLIMS ID: 04-1521Matrix: WaterData Release Authorized:,Reported: 02/12/04
Instrument/Analyst: FINN1/JADate Analyzed: 02/10/04 17:59
ANALYTICAL (RESOURCES'INCORPORATED
Sample ID: Preister Dom Before FirstFilter
QC Report No: GG98-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/02/04
Date Received: 02/04/04
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
CAS Number Analyte RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-21 A O 1 A T_tu-s — to — ±591-78-6
127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-11330-20-795-47-6
Chlorome thaneB romome t haneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1-Dichloroethanetrans-1, 2-Dichloroethenecis - 1 , 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2 -Butanone1,1, 1-Tri chloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2 -Dichloropropanecis - 1 , 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -TrichloroethaneBenzenetrans -1,3 -Dichloropropene2 -ChloroethylvinyletherBromoform
— 4 — Mcbhy-1 — 2 — PerrtarTorre — (M1BK)2 -HexanoneTetrachloroethene1,1,2, 2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2 , 2-trif luoroem, p-Xyleneo-Xylene
Reported in ;ig/L (ppb)
Volatile Surrogate Recovery
d4-l, 2-Dichloroethane 104%d8-Toluene 99.1%Bromof luorobenzene 96.7%d4 -1 , 2 -Dichlorobenzene 99.8%
1.01.01.01. 02.05.01.01.01. 01. 01.01.01. 05 . 01.01. 05 . 01.01 . 01. 01. 01 . 01. 01.01. 05. 01.05 . 05.01.01.01. 01. 01.01.01.02.01 .01.0
< 1.0 U< 1 . 0 U< 1.0 U< 1.0 U< 2.0 U< 5 .0 V< 1.0 U1. 1
< 1 . 0 U< 1.0 U< 1.0 U< 1- 0 U< 1 . 0 U< 5 . 0 U1.61. 3
< 5.0 U< 1 . 0 U< 1 . 0 U< 1.0 U< 1 .0 U< 1.0 U< 1.0 U< 1 . 0 U< 1 . 0 U< 5.0 U f^< 1. 0 U< 5 . u u< 5.0 U1.3
< 1.0 U< 1. 0 U< 1.0 U .< 1.0 U< 1.0 U< 1.0 U< 2.0 U< 1.0 U< 1 . 0 U
000016
FORM I
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 1 of 1
Lab Sample ID: GG98ELIMS ID: 04-1522Matrix: WaterData Release AuthorizedReported: 02/12/04
Instrument/Analyst: FINN1/JADate Analyzed: 02/10/04 18:27
CAS Number Analyte
ANALYTICALRESOURCESINCORPORATED
Sample ID: Preister DOM After FirstFilter
QC Report No: GG98-LTRS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/02/04
Date Received: 02/04/04
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108 -90-7100-41-4100-42-575-69-476-13-11330-20-795-47-6
Chlorome thaneB romome t haneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, l-Dichloroethanetrans -1, 2 -Dichloroethenecis-1, 2-DichloroetheneChloroform1, 2 -Dichloroe thane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodi chlorome thane1 , 2 -Dichloropropanecis - 1 , 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -Trichloroe thaneBenzenetrans -1,3 -Dichloropropene2 -ChloroethylvinyletherBromof orm4-Methyl-2-Pentan.one (MIBK)2-HexanoneTetrachloroethene1,1,2,2 -Tetrachloroe thaneTolueneChlorobenzene
. EthylbenzeneStyreneTrichlorof luorome thane1,1,2 -Trichloro-1, 2, 2-trif luoroem, p-Xyleneo-Xylene
Reported in. g/L (ppb)
Volatile Surrogate Recovery
d4-l, 2-Dichloroethane 103%da-Toluene 101%Bromof luorobenzene 94.0%d4-l, 2-Dichlorobenzene 100%
1. 01 . 01.01.02.05.01.01. 01 . 01 . 01 . 01 . 01.05.01.01 . 05.01. 01. 01.01.01.01.01 . 01 . 05.01 . 05 . 05.01 . 01.01.01.01.01.01.02.01 . 01. 0
< i.o a< 1. 0 U< 1. 0 U< 1 . 0 U< 2 .0 U< 5 .0 a< 1.0 U< 1.0 U< 1.0 U< 1 .0 U< 1 . 0 U< 1 .0 U< 1.0 U< 5 . 0 U< 1 . 0 U< 1. 0 U< 5.0 U< 1.0 U< 1.0 U< 1.0 U< 1 .0 U<: 1.0 U< 1.0 U< 1.0 U< 1 .0 U< 5.0 U 1< 1 .0 U< 5.0 U< 5.0 U< 1-0 U< 1.0 U< 1.0 U< 1.0 U< 1 .0 U< 1 . 0 U< 1.0 U< 2.0 U< 1.0 U< 1.0 U
FORM Ioooo n
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 1 of 1
Lab Sample ID: GG98FLIMS ID: 04-1523Matrix: WaterData Release Authorized:Reported.- 02/12/04
Instrument/Analyst: FINN1/JADate Analyzed: 02/10/04 18:55
CAS Number Analyte
ANALYTICAL (RESOURCESINCORPORATED
Sample ID: Preister DOM After lastFilter
QC Report No-. GG98-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/02/04
Date Received: 02/04/04
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110--75-875-25-21 OR -10-1— . — „ — .. — -_ — „_ -t-y-o J. \J ±
591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-11330-20-795-47-6
Chlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Bisulfide1, 1 -Dichloroethene1, 1-Dichloroethanetrans- 1 , 2 -Dichloroethenecis-1, 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2 -Butanone1, 1, 1 -TrichloroethaneCarbon Tet rachlorideVinyl AcetateBromodichlorome thane1, 2-Dichloropropanecis-1 , 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -TrichloroethaneBenzenetrans -1,3 -Dichloropropene2 -ChloroethylvinyletherBromoform/I -Mpt-Vn/1 ? — Oprvt- .-i nt vrvp LM-TLn.Jt.'lM IHJ U 11 y J. £• £ U ir\_dlIOiiv~ \ "I JTDIV/
2-HexanoneTetrachloroethene1,1,2, 2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1,2 -Trichloro-1, 2 , 2-trif luoroem, p-Xyleneo-Xylene
Reported in p;g/L (ppb)
Volatile Surrogate Recovery
d4-l, 2 -Dichloroethane 102%d8-Toluene 99.2%Bromof luorobenzene 95.0%d4 -1, 2-Dichlorobenzene 100%
1.01.01 . 01.02.05.01.01. 01. 01. 01. 01. 01 . 05 . 01.01.05.01.01 . 01.01. 01. 01.01.01. 05 .01.0
— *5 — f\j . \J
S . 01. 01.01.01.01.01.01.02.01.01.0
< 1.0 U< 1.0 U< 1. 0 U< 1 . 0 U< 2 . 0 U< 5 .0 U< 1. 0 U< 1.0 U< 1. 0 U< 1 . 0 U< 1 . 0 U< 1.0 U< 1 . 0 U< 5 . 0 U< 1 . 0 U< 1 . 0 U< 5.0 U< 1.0 U< 1 . 0 U< 1. 0 U< 1.0 U< 1.0 U< 1 . 0 U< 1.0 U< 1 . 0 U< 5.0 U 1< 1 .0 U
— -? — — ft — H —< D . \J VJ
< 5.0 U< 1.0 U< 1.0 U< 1 . 0 U< 1.0 U< 1.0 U< 1.0 U< 1 . 0 U< 2. 0 U< 1 . 0 U< 1. 0 U
000018
FORM I
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 1 oE 1
Lab Sample ID: GG98GLIMS ID: 04-1524Matrix : ,WaterData Release Authorized:Reported: 02/12/04
Instrument/Analyst: FINN1/JADate Analyzed: 02/10/04 19:24
CAS Number Analyte
ANALYTICAL jRESOURCES'INCORPORATED
Sample ID: 89-12 Well11,700
QC Report No: GG98-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/02/04
Date Received: 02/04/04
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107 -06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43 -210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-11330-20-795-47-6
Chlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1-Dichloroethanetrans -1,2 -Dichloroethenecis -1, 2 -DichloroetheneChloroform1, 2 -Dichloroethane2-Butanone1, 1, 1-Trichloroe thaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2-Dichloropropanecis-1, 3 -DichloropropeneTrichloroetheneDibromochlorometharie1,1, 2-TrichloroethaneBenzenetrans -1,3 -Dichloropropene2 -ChloroethylvinyletherBromofrorm4-Methyl-2-Pentanone (MIBK)2-HexanoneTetrachloroethene1,1,2,2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2, 2 -trif luoroem, p-Xyleneo-Xylene
Reported in [iq/Li (ppb)
Volatile Surrogate Recovery
d4-l,2-Dichloroethane 103%d8-Toluene 100%Bromofluorobenzene 95-2%d4 -1 , 2-Dichlorobenzene 99.2%
1. 01.01.01.02.05.0I . 01.01.01.. 01.01.01. 05.01.01 . 05.01. 01.01 . 01. 01. 01.01. 01.05.01.05.05.01.01.01.01.01. 01.01.02.01.01.0
< 1 . 0 U< 1 . 0 U< 1. 0 U< 1.0 U< 2 . 0 U< 5.0 U< 1.0 U
5017
< 1 . 0 U6. 1
< 1 . 0 U< 1. 0 U< 5 . 0 U
66< 1. 0 U< 5 .0 U< 1. 0 U< 1.0 U< 1.0 U.3.4
< 1. 0 U< 1.0 U< 1 . 0 U< 1.0 U< 5.0 U |< 1 . 0 U< 5 . 0 U< 5.0 U230 E
< 1.0 U< 1.0 U< 1.0 U< 1. 0 U< 1.0 U< 1.0 U< 2 . 0 U< 1 .0 U< 1. 0 U
000019
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 1 of 1
Lab Sample ID: GG98GLIMS ID: 04-1524Matrix: -JWaterData Release Authorized:.Reported: 02/12/04
Instrument/Analyst: FINN1/JADate Analyzed: 02/11/04 15:38
CAS Number Analyte
Sample ID: 89-12 WellDILUTION
QC Report No.- GG98-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/02/04
Date Received: 02/04/04
Sample Amount: 1.67 mLPurge Volume: 5.0 mL
ANALYTICAL |RESOURCES^INCORPORATED
RL Result
74-87-3 -74-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-2 '10061-02-6110-75-875-25-2108-10^1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-11330-20-795-47-6
Chlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1-Dichloroethanetrans-1 , 2 -Dichloroethenecis-1, 2 -DichloroetheneChloroformI, 2 -Dichloroethane2 -Butanone1,1, 1-Trichloroe thaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2 -Dichloropropanecis -1,3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1, 2 -Tri chloroethaneBenzenetrans -1,3 -Dichloropropene2-ChloroethylvinyletherBromoform4-Methyl-2-Pentanone (MIBK)2-HexanoneTetrachloroethene1,1,2,2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luoromethane1,1, 2-Trichloro-l, 2, 2-trif luoroem, p-Xyleneo-Xylene
3 .03 .03 .03 . 06 . 015
3 . 03.03 .03 .03.03 .03 .015
3.03 .015
3 .03 .03.03.03 . 03 .03 .03 . 015
3 .01515
3.03 .03 .03 .03.03 .03 .06.03 . 03 . 0
< 3 .0 U< 3 .0 U< 3 .0 U< 3 .0 U< 6 .0 U< 15 U
< 3 .0 U4416
< 3 . 0 U5 .6
< 3 .0 U< 3 . 0 U< 15 U
56 -OT< 3 .0 U< 15 U
< 3 .0 U< 3 .0 U< 3 .0 U
3 .1< 3 .0 U< 3 .0 U< 3 .0 a< 3 . 0 U< 15 U R.
< 3.0 U< 15 U< 15 U220 "T
< 3 .0 U< 3 .0 U< 3 .0 U< 3 .0 U< 3 .0 U< 3 .0 U< 6 .0 U< 3 .0 U< 3 .0 U
Reported in p.g/L (ppb)
Volatile Surrogate Recovery
d4-1,2-Dichloroethane 104%d8-Toluene 97.6%Bromofluorobenzene 94.8%d4-1,2-Dichlorobenzene 105%
000020
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 1 of 1
Lab Sample ID: GG98HLIMS ID: 04-1525Matrix: WaterData Release Authorized:Reported: 02/12/04
Instrument/Analyst: FINN1/JADate Analyzed: 02/10/04 19:52
CAS Number Analyte
ANALYTICAL!RESOURCES^INCORPORATED
Sample ID: OI Well11,700
QC Report No: GG98-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/02/04
Date Received: 02/04/04
Sample Amount: 5.00 raLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-11330-20-795-47-6
ChloromethaneBromome thaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1 -Dichloroethanetrans-1, 2 -Dichloroethenecis - 1 , 2 -DichloroetheneChloroform1, 2 -Dichloroethane2-Butanone1, 1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodi chloromethane1, 2-Dichloropropanecis - 1 , 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1, 2-TrichloroethaneBenzenetrans -1,3 -Dichloropropene2 -ChloroethylvinyletherBromoform4-Methyl-2-Pentanone (MIBK)2-HexanoneTetrachloroethene1,1,2, 2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1,2 -Trichloro-1 ,2,2 -trif luoroem, p-Xyleneo-Xylene
Reported in pig/L (ppb)
Volatile Surrogate Recovery
d4-l, 2 -Dichloroethane 103%d8 -Toluene 99.5%Bromof luorobenzene 96.8%d4-l, 2 -Dichlorobenzene 99.2%
1.01.01.01.02.05.01.01.01 . 01. 01.01.01 . 05.01.01.05.01.01. 01 . 01.01.01 . 01. 01. 05.01.05. 05.01.01. 01.01.01. 01. 01.02.01.01.0
< 1.0 U< 1.0 U< 1 .0 U< 1.0 U< 2.0 U< 5 . 0 U< 1.0 U
13< 1.0 U< 1 .0 U< 1.0 U< 1.0 U< 1.0 U< 5 . 0 U
11< 1-0 U< 5.0 U< 1.0 U< 1 .0 U< 1.0 U< 1 . 0 U< 1.0 U< 1. 0 U< 1 .0 U< 1.0 U< 5.0 U i< 1.0 U< 5 .0 U< 5.0 U
15< 1.0 U< 1 . 0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 2 . 0 U< 1.0 U< 1.0 U
000021
ORGAHICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 1 oE 1
Lab Sample ID: GG98ILIMS ID: 04-1526Matrix: WaterData Release Authorized ~Reported: 02/12/04
Instrument/Analyst : FINN1/JADate Analyzed: 02/10/04 20:20
CAS Number Analyte
ANALYTICAL tRESOURCESINCORPORATED
Sample ID: 89-13 Well11,702
QC Report No: GG98-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/03/04
Date Received: 02/04/04
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-0.1-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43 -210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-11330-20-795-47-6
Chlorome thaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1-Dichloroethanetrans -1, 2 -Dichloroethenecis - 1, 2 -DichloroetheneChloroform1, 2 - Dich lor oe thane2 -Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2 -Dichloropropanecis-1, 3 -DichloropropeneTrichloroetheneDibromochlorome thane1, 1, 2-TrichloroethaneBenzenetrans- 1 , 3 -Dichloropropene2 -ChloroethylvinyletherBromoform4- M(=» t- Vi wl - O D p,n-i~ r>/-i n^ /-M-T-R-K-1'ic Uily j — &~-c e-rrtcrrftjrrc yrl JL D IV /
2 -HexanoneTetrachloroethene1 , 1 , 2 , 2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorotne thane1,1,2 -Trichloro-1, 2, 2-trif luoroem, p-Xyleneo-Xylene
1 .0
1.01 .01 .02 .05.01.01.01 .01 .01 .01 .01 .05 .01 .01 .05 .01.01 .01.01 .01.01.01.01 - 05 .01 .0C A^ . U
5 .01.01.01 .01.01.01.01 . 02.01.01. 0
< 1 .0 U< 1 . 0 U< 1.0 U< 1.0 U< 2.0 U< 5.0 U< 1.0 U< 1. 0 U< 1 . 0 U< 1 . 0 U< 1 . 0 U< 1 . 0 U< 1 . 0 U< 5 . 0 U< 1 .0 U< 1.0 U< 5 . 0 U< 1 .0 U< 1 . 0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1 .0 U< 5 .0 U R^< 1.0 U
< 5 .0 U5.8
< 1.0 U< 1 .0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 2.0 U< 1.0 U< 1.0 U
Reported in /^g/L (ppb)
Volatile Surrogate Recovery
td4-l,2-Dichloroethane 104%d8-Toluene 9 9 . 2 %Bromofluorobenzene 9 6 . 4 %d4-1, 2-Dichloroberizene 9 9 . 8 %
0 0 0 0 2 2
FORM I
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 1 of 1
Lab Sample ID: GG98JLIMS ID: 04-1527Matrix: WaterData Release Authorized :Reported: 02/12/04
Instrument/Analyst: FINN1/JADate Analyzed: 02/10/04 20:49
CAS Number Analyte
ANALYTICAL |RESOURCES'INCORPORATED
Sample ID: 87-3 Well11,703
QC Report No: GG98-LTRS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/03/04
Date Received: 02/04/04
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5'156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-11330-20-795-47-6
Chlorome thaneBromome thaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1 - Die hi o roe thanetrans-1 , 2 -Dichloroethenecis -1, 2 -DichloroetheneChloroform1, 2 -Dichlo roe thane2 -Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2 -Dichloropropanecis-1, 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -TrichloroethaneBenzenetrans-1 , 3 -Dichloropropene2 -ChloroethylvinyletherBromof orm4-Methyl-2-Pentanorve (MIBK)2 -HexanoneTetrachloroethene1,1,2,2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2 , 2-trif luoroem, p-Xyleneo-Xylene
Reported in ^g/L (ppb)
Volatile Surrogate Recovery
d4-l,2-Dichloroethane 103%d8-Toluene 99.9%Bromof luorobenzene 93.5%d4 - 1, 2 -Dichlorobeiizene 100%
1.01.0
. 1.01.02.05 . 01.01.01.01.01.01. 01. 05.01.01.05.01. 01. 01. 01. 01. 01. 01. 01.05.01 . 05 . 05.01.01.01.01.01.01.01.02.01.01.0
< 1 . 0 U< 1. 0 U< 1.0 U< 1.0 U< 2 . 0 U< 5.0 U< i.o a
202.2
< 1.0 U< 1 . 0 U< 1 . 0 U< 1 . 0 U< 5 . 0 U
18< 1 . 0 U< 5 .0 U< 1.0 U< 1.0 U< 1 . 0 U< 1 . 0 U< 1 . 0 U< 1 . 0 U< 1.0 U< 1 .0 U< 5.0 U< 1.0 U< 5 .0 U< 5.0 U8.5
< 1 .0 U< 1.0 U< 1.0 U< 1 . 0 U< 1. 0 U< 1.0 U< 2.0 U< 1.0 U< 1. 0 U
000023
FOKM T
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 1 of 1
Lab Sample ID: GG98KLIMS ID: 04-1528Matrix: WaterData Release AuthorizedReported: 02/12/04
Instrument /Analyst : FINN1/JADate Analyzed: 02/10/04 21:17
CAS Number Analyte
ANALYTICAL |RESOURCES^INCORPORATED
Sample ID: 92-3A Well11,704
QC Report No: GG98-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/03/04Date Received: 02/04/04
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124 -48-179-00-571-43-2
. 10061-02-6110-75-875-25-21-0-8 — 19 — 1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100 -42-575-69-476-13-11330-20-795-47-6
Chlorome thaneB romome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1-Dichloroethanetrans- 1 , 2 -Dichloroethenecis-1, 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2 -Butanone1, 1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1, 2-Dichloropropanecis-1, 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1, 2 -Trichloroet.haneBenzenetrans -1,3 -Dichloropropene2-ChloroethylvinyletherBromoform
- —t— Methyl- 2 -PeuLcUione (MIBK)2 -HexanoneTetrachloroethene'1,1,2, 2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2 , 2-trif luoroem, p-Xyleneo-Xylene
1. 01.01.01 . 02 .05 .01.01.01.01 .01 .01.01.05.01.01.05 . 01. 01.01.01.01 . 01 . 01.01 . o5 . 01.05 . 05 . 01.01.01.01,01.01 .01.02.01. 01 .0
< 1.0 U< 1 .0 U< 1.0 U< 1 . 0 U< 2 . 0 U< 5 .0 U< 1.0 U6.21.9
< 1 .0 U< 1.0 U< 1.0 U< 1. 0 U< 5.0 U
54< 1.0 U< 5 .0 U< 1.0 U< 1.0 (J< 1 . 0 U< 1 . 0 U< 1 . 0 U< 1 .0 U< 1 .0 U
• < i . o u< 5 .0 U fv< 1.0 U< 5 . 0 U< 5 . 0 U
26< 1.0 U< 1.0 U< 1.0 U< 1.0 U
• < i.o u< 1.0 U< 2.0 U< 1.0 U< 1.0 U
Reported in /ig/L (ppb)
Volatile Surrogate Recovery
d4-1,2-Dichloroethane 104%d8-Toluene 9 9 . 8 %Bromof luorobenze:ne 9 5 . 7 %d4-1 ,2 -Dich lo robenzene 100%
000024
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 1 of 1
Lab Sample ID: GG98LLIMS ID: 04-1529Matrix: WaterData Release Authorized:Reported: 02/12/04
Instrument/Analyst: FINN1/JADate Analyzed: 02/10/04 21:45
CAS Number Analyte
ANALYTICALRESOURCESINCORPORATED
Sample ID: 92-3B11,705
QC Report No: GG98-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/03/04
Date Received: 02/04/04
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25 -2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-11330-20-795-47-6
Chlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1-Dichloroethanetrans - 1 , 2 -Dichloroethenecis-1 , 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2 -Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodi chlorome thane1, 2 -Dichloropropanecis-1 , 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -TrichloroethaneBenzenetrans-1 , 3 -Dichloropropene2 -ChloroethylvinyletherBromoforrn4-Methyl-2-Pentanone (MIBK)2-HexanoneTetrachloroethene1,1,2,2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l ,2,2 -trif luoroem, p-Xyleneo-Xylene
Reported in g/L (ppb)
Volatile Surrogate Recovery
d4-l, 2 -Dichloroethane 104%dS-Toluene 101%Bromof luorobenzene 96.0%d4 - 1, 2 -Dichlorobenzene 96.6%
1.01.01.01.02.05.01.01.01.01.01.01.01.05.01.01.05.01.01.01.01.01.01.01.01.05.01 . 05.05.01.01.01.01.01.01-. 01.02.01.01.0
< 1.0 U< 1.0 U< 1.0 U< 1. 0 U< 2 . 0 U< 5 . 0 U< 1.0 U1.6
< 1. 0 U< 1 . 0 U< 1 .0 U< 1.0 U< 1 .0 U< 5 . 0 U
3 .7< 1.0 U< 5 -0 U< 1.0 U< 1.0 U< 1 . 0 U< 1 . 0 U< 1.0 U< 1 .0 U< 1 . 0 U< 1.0 U< 5 .0 U< 1 . 0 U< 5 . 0 U< 5.0 U
3 .1< 1.0 U< 1. 0 U< 1.0 U< 1 . 0 U< 1.0 U< 1.0 U< 2.0 U< 1.0 U< 1.0 U
000025
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge t Trap GC/MSPage 1 of 1
Lab Sample ID: GG9SMLIMS ID: 04-1530Matrix: Water ,Data Release Authorized ••Reported: 02/12/04
Instrument/Analyst ; FINN1/JADate Analyzed: 02/10/04 16:13
CAS Number Analyte
ANALYTICAL (RESOURCESV
INCORPORATEDSample ID: TRIP BLANK
SAMPLE
QC Report No: GG98-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled:
Date Received: 02/04/04
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124 -48-179-00-5•71-43-210061-02-6110-75-875-25-2108 -10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-11330-20-795-47-6
Chlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1-Dichloroethanetrans -1, 2 -Dichloroethenecis-1, 2 -DichloroetheneChloroform1, 2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1, 2 -Dichloropropanecis - 1 , 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -Tri chloroethaneBenzenetrans-l , 3 -Dichloropropene2 -ChloroethylvinyletherBromoform4-Mt:Lhyl-2-P"entanoiie (MIBK)2-HexanoneTetrachloroethene1,1,2,2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2 , 2-trif luoroem,p-Xyleneo-Xylene
1. 01.01. 01. 02.05.01. 01. 01.01. 01. 01. 01. 05.01.01. 05.01 . 01. 01 . 01.01. 01 . 01.01 . 05. 01.05 . 05.01. 01.01.01.01.01.01. 02.01. 01.0
< 1 .0 U< i.o u< 1 .0 U< 1.0 U< 2 .0 U< 5.0 U< 1 . 0 U< 1 . 0 U< 1 .0 U< 1 . 0 U< 1. 0 U< 1 .0 U< 1 . 0 U< 5.0 U< 1.0 U< 1 .0 U< 5.0 U< 1 . 0 U< 1 . 0 U< 1 . 0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1 . 0 U< 5.0 U <^.< 1.0 U< 5 . 0 U< 5.0 U< 1. 0 U< 1.0 U< 1. 0 U< 1.0 U< 1. 0 U< 1.0 U< 1 .0 U< 2.0 U< 1. 0 U< 1 . 0 U
Reported in ^g/L (ppb)
Volatile Surrogate Recovery
d4-1,2-Dichloroethane 97.8%d8-Toluene 99.9%Bromofluorobenzene 98.3%d4- 1,2-Dichlorobenzene 96.6%
FOPM T000026
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 1 of 1
Lab Sample ID: GH17ALIMS ID-. 04-1673Matrix: WaterData Release Authorized:/^Reported: 02/19/04 ^
Instrument/Analyst: FINN5/PABDate Analyzed: 02/12/04 16:22
Sample ID: 89-14 Well11,706
QC Report No: GH17-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/04/04
Date Received: 02/05/04
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
CAS Number Analyte RL
Reported in p.g/L (ppb)
Volatile Surrogate Recovery
d4-1,2-Dichloroethane 109%d8-Toluene 96.2%Bromofluorobenzene 94.1%d4-1,2-Dichlorobenzene 106%
Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-11330-20-795-47-6
ChloromethaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1- Dichloroethene1, 1 -Dichloroethanetrans -1, 2 -Dichloroethenecis-1, 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodi chloromethane1 , 2 -Dichloropropanecis-1, 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -TrichloroethaneBenzenetrans -1,3 -Dichloropropene2 -ChloroethylvinyletherBromof orm4-Methyl-2-Pentanoiie (MIBK)2-HexanoneTetrachloroethene1,1,2,2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2 , 2-trifluoroem, p-Xyleneo-Xylene
1.01.01.01.02.05.01.01.01.01. 01 .01 .01. 05 . 01 . 01 . 05 . 01. 01.01. 01. 01.01.01. 01. 05.01 . 05 . 05.01.01-01.01.01.01.01.02.01.01.0
< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 2.0 U< 5.0 U< 1.0 U< 1.0 U< 1. 0 U< 1.0 U< 1 .0 U< 1 .0 U< 1 . 0 U< 5 .0 U< 1 . 0 U< I .0 U< 5 . 0 U< 1 .0 U< 1.0 U< 1 . 0 U< 1 . 0 U< 1 . 0 U< 1 .0 U< 1 .0 U< 1 .0 U< 5 .0 U< 1 . 0 U< 5 .0 U< 5.0 U2.5
< 1.0 .U< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 2.0 U< 1 . 0 U< 1 . 0 U
ANALYTICAL |RESOURCES'INCORPORATED
00001 1FORM I
ORGANICS ANALYSIS DATA SHEETVolaitiles by Purge & Trap GC/MSPage 1 of 1
Lab Sample ID: GH17BLIMS ID: 04-1674Matrix: WaterData Release AuthorizedReported: 02/19/04
Instrument/Analyst: FIRN5/PABDate Analyzed: 02/12/04 16:52
CAS Number Analyte
Sample ID: 89-15 Well11,707
QC Report No: GH17-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/04/04
Date Received: 02/05/04
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
ANALYTICAL |RESOURCESV
INCORPORATED
RL
Reported in g/L (ppb)
Volatile Surrogate Recovery
d4-l,2-Dichloroethane 116%da-Toluene . 96.6%Bromofluorobenzene 92.8%d4 - 1,2-Dichlorobenzene 108%
Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-5•79-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-21-0-6 — r6 — 1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-11330-20-795-47-6
Chlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1-Dichloroethanetrans- 1, 2 -Dichloroethenecis-1, 2 -DichloroetlieneChloroform1 , 2-Dichloroethane2-Butan.one1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2 -Dichloropropanecis-1, 3 -DichloropropeneTrichloroetlieneDibromochlorome thane1, 1, 2-TrichloroethaneBenzenetrans -1 , 3 -Dichloropropene2 -ChloroethylvinyletherBromoform
— 4^M ethy l-2~=^PenLduou'5 ("MXB1C)2-HexanoneTetrachloroethene1,1,2, 2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2 , 2-trifluoroem, p-Xyleneo-Xylene
1.01.01.01 . 02 . 05 .01.01.01.01 .01.01 . 01.05.01.01 .05 .01 .01.01 .01.01 .01 .01 .01 . 05 . 01.05 . U5.01.01.01 . 01.01.01.01.02.01.01.0
< 1 .0 U< i . o a< i . o a< 1 . 0 U< 2.0 U1101.0 O~11047
< 1 .0 U48
< 1 .0 U< 1 .0 U
30200
< 1.0 U< 5 .0 U< 1 . 0 U< 1 .0 U< 1 .0 U3.9
< 1 . 0 U< 1 . 0 U< 1.0 U< 1 . 0 U< 5 .0 U <{< 1.0 U< b . 0 U< 5.0 U120
< 1.0 U< 1 . 0 U< 1 .0 U< 1.0 U< 1.0 U< 1 . 0 U< 2.0 U< 1.0 U< 1.0 U
000012
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge t Trap GC/MSPage 1 of 1
Lab Sample ID: GH17CLIMS ID: 04-1675Matrix: WaterData Release AuthorizedReported: 02/19/04
Instrument/Analyst: FINN5/PABDate Analyzed: 02/12/04 17:22
CAS Number Analyte,
ANALYTICAL |RESOURCES^INCORPORATED
Sample ID: DuplicateSAMPLE
QC Report Ho: GH17-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled:Date Received: 02/05/04
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-11330-20-795-47-6
Chlorome thaneBromome thaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1 -Dichloroethanetrans -1 , 2 -Dichloroethenecis-1, 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2 -Butanone1,1, 1-Trichloroe thaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1, 2-Dichloropropanecis-1, 3 -DichloropropeneTrichloroetheneDibromochloromethane1,1,2 -Trichloroe thaneBenzenetrans -1,3 -Dichloropropene2 -ChloroethylvinyletherBromofoon4-Methyl-2-Pentaiioiie (MIBK)2-HexanoneTetrachloroethene1,1,2, 2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2 , 2-trif luoroem, p-Xyleneo-Xylene
Reported in ng/L (ppb)
Volatile Surrogate Recovery
d4-l, 2 -Dichloroethane 112%d8-Toluene 99.8%Bromof luorobenzene 93.4%d4-l , 2 -Dichlorobenzene . 107%
1 . 01. 01.01.02 . 05.01 . 01.01 . 01 . 01.01.01.05.01 . 01. 05.01.01. 01 . 01. 01.01.01.01.05.01 .05 . 05 .01.01 . 01.01.01 . 01 . 01. 02.01.01.0
< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 2 . 0 U< 5.0 U< 1 . 0 U< 1 . 0 U< 1 . 0 U< 1.0 U< 1.0 U< 1 . 0 U< 1 .0 U< 5 .0 U< 1.0 U< 1 . 0 U< 5 . 0 U< 1 .0 U< 1.0 U< 1 .0 U< 1 .0 U< 1 . 0 U< 1 .0 U< 1 .0 U< 1 . 0 U< 5.0 U< 1.0 U< 5 . 0 U< 5.0 U2.2
< 1 . 0 U< 1 .0 U< 1 .0 U< 1 . 0 U< 1 . 0 U< 1.0 U< 2 . 0 U< 1 . 0 U< 1.0 U
000013
FORM I
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 1 of 1
Lab Sample ID: GH17DLIMS ID: 04-1676Matrix: Water <«,Data Release Authorized/>^Reported: 02/19/04 ^
Instrument/Analyst; FINN5/PABDate Analyzed: 02/12/04 17:52
ANALYTICAL /RESOURCES^INCORPORATED
Sample ID: AOI Well11,708
QC Report No: GH17-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/04/04
Date Received: 02/05/04
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
CAS Number Analyte RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-11330-20-795-47-6
Chlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1-Dichloroethanetrans-1, 2-Dichloroethenecis-1, 2-DichloroetheneChloroform1 , 2-Dichloroethane2 -Butanone1, 1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodi chlorome thane1, 2 -Dichloropropanecis - 1 , 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -Trichloroe thaneBenzenetrans- 1, 3 -Dichloropropene2 -ChloroethylvinyletherBromoform4-Methyl-2-Pentanone (MIBK)2-HexanoneTetrachloroethene1, 1, 2, 2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2, 2-trif luoroem, p-Xyleneo-Xylene
Reported in ng/L (ppb)
Volatile Surrogate Recovery
d4 -1 , 2 -Dichloroethane 111%d8 -Toluene 97.8%Bromof luorobenzene 95.6%d4 - 1 , 2-Dichlorobenzene 105%
1 .01 .01.01 .02 .05 .01.01.01.01.01.01 .01 . 05 .01 .01 . 05 . 01 . 01 . 01 . 01.01.01.01.01 . 05.01 .05.05 .01.01.01.01 . 01 . 01.01 . 02 .01 .01.0
< 1.0 U< i . o a< 1.0 U< 1.0 U< 2.0 U< 5.0 U< 1.0 U
124.0
< 1.0 CJ1.3
< 1 . 0 U< 1.0 U< 5 .0 U
18< 1 . 0 U< 5.0 U< 1 .0 U< 1 .0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1 . 0 U< 5 . 0 U R< 1.0 U< 5.0 U< 5 .0 U
12< 1.0 U< 1 .0 U< 1.0 U< 1.0 U< 1 . 0 U< 1 .0 U< 2 .0 U< 1.0 U< 1.0 U
I- Jjb/M
000014
FORM I
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 1 of 1
Lab Sample ID: GH17ELIMS ID: 04-1677Matrix: WaterData Release Authorized :Reported: 02/19/04
Instrument/Analyst: FINN5/PABDate Analyzed: 02/12/04 18:22
CAS Number Analyte
Sample ID: Trip Blank11,709
QC Report No: GH17-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/04/04
Date Received: 02/05/04
Sample Amount: 5.00 mLPurge Volume: 5.0 mL
ANALYTICAL (RESOURCES^INCORPORATED
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475 -27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6
127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-11330-20-795-47-6
Chlorome thaneB romome t haneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1 -Dichloroethanetrans- 1, 2-Dichloroethenecis-1, 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2-Butanone1, 1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateB romodi chl or ome thane1 , 2 -Dichloropropanecis-1, 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -Trichloroe thaneBenzenetrans -1,3 -Dichloropropene2 -ChloroethylvinyletherBromoform
. 4 -Methyl -2 -Pentanorie (MIBK)2 -HexanoneTetrachloroethene1 , 1,2,2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2, 2-trif luoroem, p-Xyleneo-Xylene
Reported in ng/L (ppb)
Volatile Surrogate Recovery
d4-l, 2 -Dichloroethane 118%d8 -Toluene 98.7%Bromof luorobenzene 97.1%d4-l, 2-Dichlorobenzene 106%
1.01.01.01 . 02 .05.01.01.0.1 .01 .01.01.01.05.01.01.05.01.01.01. 01.01.01.01. 01.05.01 . 05.05.01.01. 01.01.01. 01.01.02.01.01.0
< 1.0 U< 1.0 U< 1 .0 U< 1.0 U< 2 . 0 U
43< 1.0 U< 1 . 0 U< 1. 0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U
13< 1.0 U< 1 .0 U< 5.0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1.0 U< 1 .0 U< 1.0 U< 5.0 U< 1 .0 U< 5 .0 U< 5.0 U< 1.0 U< 1 .0 U< 1 .0 U< 1.0 U< 1 .0 U< 1.0 U< 1.0 U< 2.0 U< 1 .0 U< 1..0 U
000015
FORM I
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MSPage 1 of 1
Lab Sample ID: GH17FLIMS ID: 04-1678Matrix: WaterData Release Authorized:,^"Reported: 02/19/04 ^
ANALYTICAL (RESOURCESV
INCORPORATEDSample ID: Lab Blank (Trip)
SAMPLE
QC Report No: GH17-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled:
Date Received: 02/05/04
[nstrument/ Analyst : FINN5/PAB Sample Amount:)ate Analyzed: 02/12/04 18:51 Purge Volume:
CAS Number
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-11330-20-7
• 95-47-6
Analyte
Chlorome thaneBromome thaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1-Dichloroethanetrans -1 , 2 -Dichloroethenecis-1 , 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2 -Eutanone1, 1, 1 -TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1, 2-Dichloropropanecis-1 , 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -TrichloroethaneBenzenetrans -1,3 -Dichloropropene2 -ChloroethylvinyletherBromoform4-Methyl-2-Pentanone (MIBK)2 -HexanoneTetrachloroethene1,1,2,2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1,2 -Trichloro-1, 2 , 2 -trif luoroem, p-Xyleneo-Xylene
Reported in ,ug/L (ppb)
Volatile Surrogate Recovery
d4-l, 2 -Dichloroethane 110%de-Toluene 98.0%Bromof luorobenzene 93.2%d4 -1, 2-Dichlorobenzene 108%
5.00 mL5.0 mL
RL
1.01 . 01.01 . 02.05 . 01 .01. 01.01 . 01 . 01.01 . 05.01 . 01 .05.01-01.01 . 01. 01 . 01 . 01 . 01 . 05 .01 . 05.05 . 01.01.01.01 . 01 . 01.01 . 02.01 . 01 . 0 -
Result
< 1.0 U< 1. 0 U< 1.0 U< 1.0 U< 2.0 U< 5 .0 U< 1.0 U< 1 . 0 U< 1 . 0 U< 1 .0 U< 1.0 U< 1 . 0 U< 1.0 U< 5 . 0 U< 1 . 0 U< 1 . 0 U< 5 . 0 U< 1.0 U< 1 .0 U< 1.0 U< 1.0 Lf< 1.0 U< 1.0 U< 1 .0 U< 1 . 0 U< 5 .0 U Ift< 1 .0 U< 5.0 U< 5 . 0 U< 1 . 0 U< 1.0 U< 1 .0 U< 1 .0 U< 1.0 U< 1.0 U< 1 . 0 U< 2 .0 U< 1 . 0 U< 1 . 0 U
\J . J,
000016FORM I
Memo
Century Square1501 4'h Avenue, Suite 1400Seattle, Wellington 98101206.438.2VOO Telephone206.438.2699 Fax
To: Roy Elliott, Lead Consultant Info: FINAL
From: Karen Mixon, Senior Chemist V^ Date: April 6,2004
QA/QC Data Summary Review61st Quarterly Groundwater Sampling (February 2004)Inorganic DataLindsay Manufacturing 33750799
The data quality review of 6 groundwater samples and one rinse blank collected from February 2 throughFebruary 4, 2004 has been completed. The samples were analyzed for total metals (cadmium, chromium, lead, iron andzinc), sulfate and pH by Analytical Resources, Incorporated (ART) located in Tukwila, Washington. The analyses wereperformed in general accordance with EPA Methods 6010B, 7421, 375.2 and 150.1, respectively and EPA's Contract:Laboratory Program (CLP) Statement of Work (SOW). A complete data package was received from the laboratory thatincluded summary sample results and associated QA/QC data. The following samples are associated with laboratorycase numbers GG98 and GH17:
Client ID ARI Number
Seller's Domestic BIT GG98APreister's Domestic 2003 BFF GG98D87-3 Well GG98J89-14 Well GH17A89-15 Well GH17BDuplicate (Reid Duplicate of 89-14) GH17C
Trip Blank (Rinse Blank) GH17E
The following comments refer to ARI's performance in meeting the quality control specifications outlined inF.PA Methods 601OR, 7471, 375.7. and I *ifl. 1 Data-were qnalifiedJjased-on-the^method-criteria-and-guidaf4ce-pix>vid&d--in the EPA document "USEPA Contract Laboratory Program National Functional Guidelines for Inorganic DataReview", July 2002.
L. Holding Time - Acceptable (Metals only)
2. Initial and Continuing Calibration - Acceptable except as noted below:
The recovery of zinc from the low check standard (CRT) associated with sample group GG98 was 137%. Sample resultsfor zinc in samples Seller's Domestic BFF, Preister's Domestic 2003 BFF, and 87-3 Well are qualified as estimated ifreported as detected. Zinc results reported as not detected are not qualified.
3. Blanks
Zinc (0.013 mg/L) was detected in "Trip Blank" (GH17E). This sample is representative of water used todecontaminate non-dedicated sampling equipment. As the wells sampled have dedicated pumps or are sampled throughoutlets from the individual systems, data are not qualified based on this blank.
K.-VX>5\UNDSAY\20O»\AnnJytt:aJ DalaMsi Ou 2004\61lh QTR.m=t.doc URS
Page 1 of 2
Inorganics 61st Quarter, February 2004April 6, 2004
4. Laboratory Duplicate Analysis - Acceptable
5. Field Duplicate - Acceptable
The field duplicate was collected at "89-14 Well". Data were generally comparable between the parent and duplicatesample.
6. Matrix Spike Analysis (MS) -
The percent recovery for.zinc from the matrix spike performed on sample "89-14 Well" was 26%. The sampleconcentration exceeded the spiking level by more than 4X. Data were not qualified based on the matrix spike recovery.
7. Furnace Atomic Absorption QC (Post Digest Spike) - Acceptable
8. ICP Interference Check Sample - Acceptable
9. Laboratory Control Sample - Acceptable
10. ICP Serial Dilution
Per the method, the serial dilution was not required as these samples do not constitute an unusual matrix.
11. SulfateandpH
The 24-hour hold time was exceeded by 24 to 48 hours for pH analysis of samples Seller's Domestic BFF, Preister'sDomestic 2003 BFF, and 87-3 Weil in group GG98. The pH results for these samples are qualified as estimated andflagged "J".
12. Type of Review - Summary
Overall Assessment of Data:
The usefulness of the data is based on the EPA guidance documents listed above. Upon consideration ofthe information presented above, the data are acceptable except where flagged with data qualifiers that modify theusefulness of the individual values.
Data Qualifiers:
U - The analyte was analyzed for, but not detected above the reported sample quantitation limit.
J - The analyte was positively identified; the associated numerical value is the approximate concentration of theanalyte in the sample.
UJ - The analyte was not detected above the reported sample quantitation limit. However, the report^ quantitationlimit is approximate and may or may not represent the actual limit of quantitation necessary to accurately andprecisely measure the analyte in the sample.
R - The sample results are rejected due to serious deficiencies in the ability to analyze the sample and meet qualitycontrol criteria. The presence or absence of the analyte cannot be verified-
K¥X)5\U>TOS A Y\2004\AniUytiaUData\l si Qtr2004^1ih QTR.nxt.doc URS
Page 2 of 2
INORGANICS ANALYSIS DATA SHEETTOTAL METALSPage 1 of 1
ANALYTICAL {RESOURCES^INCORPORATED
Sample ID: Bellers Dom Before FFSAMPLE
Lab Sample ID: GG98ALIMS ID: 04-1518Matrix: WaterData ReleaseReported: 02/13/04
A. s.^-/TY ""(J
QC Report No: GG98-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02 /02 /04
Date Received: 02 /04/04
PrepMeth
3010A3010A3010A3020A
3010A
PrepDate
02/05/0402/05/0402/05/0402/05/04
02/05/04
AnalysisMethod
6010B6010B
6010B74216010B
AnalysisDate
02/12/0402/12/0402/12/0402/10/04
02/12/04
CAS Number
7440-43-97440-47-37439-89-67439-92-17440-66-6
Analyte
CadmiumChromiumIronLeadZinc
00
00
RL
.00.2
..005
0.05
.001
.00(5
00
0
0
mg/L
.002
.0050.05.001.018 -
Q
U
uU
~r
U-Analyte undetected at given RLRL-Reporting Limit
FORM-I000035
INORGANICS ANALYSIS DATA SHEETTOTAL METALSPage 1 of 1
Lab Sample ID: GG98DLIIMS ID: 04-1521Matrix: WaterData Release AuthorizecjOV>^"Reported: 02/13/04 'AJ> '
ANALYTICAL jRESOURCES^INCORPORATED
Sample ID: Preister Dom Before FirstFilter
QC Report No: GG98-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/02/04Date Received: 02/04/04
PrepMoth
3010A3010A3010A3020A3010A
PrepDate
02/05/0402/05/0402/05/0402/05/0402/05/04
AnalysisMethod
6010B6010B6010B74216010B
AnalysisDate
02/12/0402/12/0402/12/0402/10/0402/12/04
CAS Mumber
7440-43-97440-47-37439-89-67439-92-17440-66-6
Analyte
CadmiumChromiumIronLeadZinc
00
0
0
RL
.002
.0050.05.001
.006
00
0
0
mg/L
.002
.0050.05.013
.010 -
Q
uuu
T~
U-Analyte undetected at given RLRL-Reporting Limit
000038FORM-I
INORGANICS ANALYSIS DATA SHEETTOTAL METALSPage 1 of 1
Lab Sample ID: GG98JLIMS ID: 04-1527Matrix: WaterData Release Authorizec^2k>-Reported: 02/13/04 Af
ANALYTICAL (RESOURCESV
INCORPORATED
Sample ID: 87-3 Well11,703
QC Report No: GG98-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/03/04
Date Received: 02/04/04
PrepMath
3010A
3010A
3010A
3020A
3010A
PrepDate
02/05/04
02/05/04
02/05/04
02/05/04
02/05/04
AnalysisMethod
6010B
6010B
6010B
74216010B
AnalysisDate
02/12/04
02/12/04
02/12/04
02/10/04
02/12/04
CAS Nujnber
7440-43-9
7440-47-3
7439-89-6
7439-92-1
7440-66-6
Analyte
Cadmium
Chromium
Iron
Lead
Zinc
RL
0.002
0.005
0.05
0.0010.00(3
mg/L Q
0.002
0.010
0. 14
0.001
0.306
U-Analyte undetected at given RLRL-Reporting Limit
000039
FORM-I
INORGANICS ANALYSIS DATA SHEETLABORATORY ANALYSIS OF CONVENTIONAL PARAMETERSPage 1 of 1
ANALYTICAL,RESOURCESINCORPORATED
Sample ID: Sellers Dom Before FFSAMPLE
Lab Sample ID: GG98ALIMS ID: 04-1518Matrix: WaterData Release Authorized:Reported: 02/13/04
Aiialy te
QC Report No: GG98-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/02/04Date Received: 02/04/04
AnalysisDate & Batch Method RL Units Result
pH
Sulfate
02/04/04020404&1
02/09/04
EPA 150.1
EPA 375.2
0.01 Std units
4.0 mg/L
6.81
46020904#2
RL Analytical reporting limitU Undetected at reported detection limit
0 0 0 0 4 2
Report for GG98 Received 02/04/04
INORGANICS ANALYSIS DATA SHEKTLABORATORY ANALYSIS OF CONVENTIONAL PARAMETERSPage 1 of 1
ANALYTICAL |RESOURCESy
INCORPORATED
Sample ID: Preister Dom Before FirstFilter
Lab Sample ID: GG98DLIMS ID: 04-1521Matrix: WaterData Release Authorized:Reported: 02/13/04
QC Report No: GG98-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/02/04
Date Received: 02/04/04
AnalyteAnalysis
Date & Batch Method RL Units Result
PH
Sulfate
02/04/04 EPA 150.1020404#1
02/09/04 EPA 375.2020904#2
0.01 std units
4.0 mg/L
6.92
45
RL Analytical reporting limitU Undetected at reported detection limit
Report for GG98 Received 02/04/04 000043
INORGANICS ANALYSIS DATA SHEETLABORATORY ANALYSIS OF CONVENTIONAL PARAMETERSPage 1 of 1
ANALYTICAL (RESOURCES'INCORPORATED
Sample ID: 87-3 Well11,703
Lab Sample ID: GG98JLIMS ID: 04-1527Matrix: WaterData Release Authorized:Reported: 02/13/04
Analyte
QC Report No: GG98-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/03/04Date Received: 02/04/04
AnalysisDate & Batch Method RL Units Result
PH
Sulfate
02/04/04020404H1
02/09/04
EPA 150.1
EPA 375.2
0.01
4 . 0
std units
mg/L
6.68
40. 020904^2
RL Analytical reporting limitU Undetected at reported detection limit
'k/t
Report for GG98 Received 02/04/04000044
INORGANICS ANALYSIS DATA SHEETTOTAL METALSPage 1 of 1
Lab Sample ID: GH17ALIMS ID: 04-1673Matr ix : WaterDat:a Release Authorized/W/^"Reported: 0 2 / 1 7 / 0 4 (T,T
ANALYTICAL |
RESOURCES'INCORPORATED
Sample ID: 89-14 Well11,706
QC Report No: GH17-URS Corp.Project: LMC Lindsay Quar te r ly
16657-002-005Date Sampled: 0 2 / 0 4 / 0 4
Date Received: 0 2 / 0 5 / 0 4
PrepMeth
3010A3010A
3010A
3020A
3010A
PrepDate
02/09/0'!02/09/04
02/09/0402/09/04
02/09/04
AnalysisMethod
6010B6010B
6010B7421
6010B
AnalysisDate
02/16/0402/16/04
02/16/04
02/11/04
02/16/04
CAS Number
7440-43-97440-47-3
7439-89-67439-92-1
7440-66-6
Analyte
CadmiumChromiumIron
Lead
Zinc
00
00
RL
.002
.0050.05.001.006
00
0
mg/L
.002
.0050.68
.001
4. 60
Q
0
U-Analyte undetected at given RLRL-Reporting Limit
000023
FORM-1
ANALYTICAL tRESOURCESS
INCORPORATEDINORGANICS ANALYSIS DATA SHEETTOTAL METALS•Page 1 o£ 1
Lab Sample ID: GH17BLIMS ID: 04-1674Matrix: WaterData Release AuthorizecReported: 02/17/04
Sample ID: 89-15 Well11,707
QC Report No: GH17-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/04/04
Date Received: 02/05/04
PrepMeth
3010A
3010A
3010A
3020A
3010A
PrepDate
02/09/04
02/09/04
02/09/04
02/09/04
02/09/04
AnalysisMethod
6010B
6010B
6010B
74216010B
AnalysisDate
02/16/04
02/16/04
02/16/0'!
02/H/O'l
02/16/04
CAS Number
7440-43-97440-47-3
7439-89-6
7439-92-1
7440-66-6
Analyte
Cadmium
Chromium
Iron
Lead
Zinc
00
00
RL
.002
. 005
0.05
.001
.OOb
0
0
0
mg/L
.004
.010
55.0.00251.0
Q
U-Analyte undetected at given RLRL-Reporting Limit
FORM-I900026
ANALYTICAL |RESOURCES'INCORPORATED
INORGANICS ANALYSIS DATA SHEETTOTAL METALSPage 1 of 1
Lab Sample ID: GH17CLIMS ID: 04-1675Matrix: Water .Data Release AuthorizedWv<l__--Reported: 02/17/04
Sample ID: DuplicateSAMPLE
QC Report No: GH17-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled:Date Received: 02/05/04
PrepMeth
3010A30LOA3010A3020A3010A
PrepDate
02/09/0402/09/0402/09/0402/09/0402/09/04
AnalysisMethod
6010B6010B6010B74216010B
AnalysisDate
02/16/0402/16/0402/16/0402/11/0402/16/04
CAS Number
7440-43-97440-47-37439-89-67439-92-17440-66-6
Analyte
CadmiumChromiumIronLeadZinc
00
00
RL
.002
.0050.05.001.006
mg/L
0.0020.0050. 67
0.0014.33
Q
Uu
U
U-Analyte undetected at given RLRL~Reporting Limit
FORM-1000027
ANALYTICAL |RESOURCES'INCORPORATED
INORGANICS ANALYSIS DATA SHEETTOTAL METALSPage 1 of 1
Lab Sample ID: GH17ELIMS ID: 04-1677Matrix: WaterData Release AuthorizeReported: 02/17/04
Sample ID: Trip Blank11,709
QC Report No: GH17-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/04/04
Date Received: 02/05/04
PrepMeth
3010A3010A3010A3020A3010A
PrepDate
02/09/0402/09/0402/09/0402/09/0402/09/04
AnalysisMethod
6010B6010B6010B74216010B
AnalysisDate
02/16/0402/16/0402/16/0402/11/0402/16/04
CAS Number
7440-43-9'7440-47-37439-89-67439-92-17440-66-6
Analyte
CadmiumChromiumIronLeadZinc
00
00
RL
.002
.005 .0.05.001.006
00
00
mg/L
.002
.0050.05. 001.013
Q
uuuu
U-Analyte undetected at given RLRL-Reporting Limit
FORM-I 000028
INORGANICS ANALYSIS DATA SHKBTLABORATORY ANALYSIS OF CONVENTIONAL PARAMETERSPage 1 of 1
Sample ID: 89-14 Well11,706
Lab Sample ID: GH17ALIMS ID: 04-1673Matrix: WaterData Release Authorized:Reported: 02/13/04
QC Report No: GH17-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/04/04
Date Received: 02/05/04
Analysis
ANALYTICAL (RESOURCESV
INCORPORATED
Analyte
pH
Date t Batch
02/05/04020504ft!
Method
EPA 150.1
RL
0 .01
Unite
std units
Result
5.53
Sulfate 02/09/04 EPA 375.2020904#2
10 mg/L 130
RL Analytical reporting limitU Undetected at reported detection limit
Report for GH17 Received 02/05/04 000031
INORGANICS ANALYSIS DATA SHEETLABORATORY ANALYSIS. OF CONVENTIONAL PARAMETERSPage 1 of 1
ANALYTICAL |RESOURCES'INCORPORATED
Sample ID: 89-15 Well11,707
Lab Sample ID: GH17BLIMS ID: 04-1674Matrix: WaterData Release Authorized:Reported: 02/13/04
Analyte
QC Report No: GH17-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/04/04Date Received: 02/05/04
AnalysisDate & Batch Method RL Units Result
pH
Sulfate
02/05/04020504ft!
02/09/04
EPA 150.1
EPA 375.2
0 . 01
40
std units
mg/L
5.48
680020904H2
RL Analytical reporting limitU Undetected at reported detection limit
Report for GH17 Received 02/05/04 000032
INORGANICS ANALYSIS DATA SHEETLABORATORY ANALYSIS OF CONVENTIONAL PARAMETERSPage 1 of 1
ANALYTICAL (RESOURCES'INCORPORATED
Sample ID: DuplicateSAMPLE
Lab Sample ID: GH17CLIMS ID: 04-1675Matrix: WaterData Release Authorized:Reported: 02/13/04
QC Report No: GH17-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled:Date Received: 02/05/04
AnalysisAnalyte
PH
Date t Batch
02/05/04020504#1
Method
EPA 150.1
RL
0.01
Units
std units
Result
5.67
Sulfate 02/09/04 EPA 375.2 10 mg/L020904tt2
23
RL Analytical reporting limitU Undetected at reported detection limit
Report for GH17 Received 02/05/04 000033
INORGANICS ANALYSIS DATA SHEETLABORATORY ANALYSIS OF CONVENTIONAL PARAMETERSPage 1 of 1
Sample ID: Trip Blank11,709
Lab Sample ID: GH17ELIMS ID: 04-1677Matrix: WaterData Release Authorized:Reported: 02/13/04
Analyte
QC Report No: GH17-URS Corp.Project: LMC Lindsay Quarterly
16657-002-005Date Sampled: 02/04/04Date Received: 02/05/04
AnalysisDate & Batch
ANALYTICAL /RESOURCES'INCORPORATED
Method RL Units Result
pH
Sulfate
02/05/04 EPA 150.1 0.01 std units#1
02/09/04 EPA 375.2020904&2
2 . 0 mg/L
5.46
< 2 .0 U
RL Analytical reporting limitU Undetected at reported detection limit
Report for GH17 Received _02/05/04 000034
Memo
Century Square1501 4th Avenue, Suite 1400Seattle, Washington 98101206.438.2700 Telephone206.438.2609 Fax
To: Roy Elliott, Lead Consultant Info: FINAL
From: Karen Mixon, Senior Chemist Y>v Date: April 6,2004
QA/QC Data Summary ReviewCuttings Samples - New Irrigation Well
RE: Organic DataLindsay Manufacturing 33750799
The data quality review of 3 soil samples collected on February 25, 2004 from stockpiled cuttings has beencompleted. The samples were analyzed for volatile organic compounds at Analytical Resources, Incorporated (ART)located in Tukwila, Washington. The analyses were performed in general accordance with EPA Method 8260B. Acomplete data package was received from the laboratory that included summary sample results and associated QA/QCdata. The following samples are associated with laboratory case number GJ11:
Well ARIED
SP-1 GJ11ASP-2 GJ11BSP-3 GJHCSP-4 Archived
The following comments refer to ARI's performance in meeting the quality control specificaiions describedin EPA Method 8260B. Data were qualified based on the method criteria and guidance provided in the EPAdocument "USEPA Contract Laboratory Program National Functional Guidelines for Organic Data Review",October 1999.
Samples were shipped by overnight delivery to the laboratory. The laboratory indicated that the coolertemperature was 3.0°C. ^
1. Holding Time - Acceptable
2. GC/MS Instrument Performance Check - Acceptable
3. Initial and Continuing Calibration - Acceptable except as noted below:
The percent relative standard deviation (%RSD) exceeded the method criteria of 15% for methylene chloride and 2-chlorpethylvinylether (2-CVE) in the initial calibration analyzed on January 22, 2004. Due to the exceedances, thelaboratory elected to evaluate the compounds based on alternative curve types of linear or quadratic fit rather thanaverage response factor. The correlation coefficients were acceptable for all curves. These compounds were notdetected in the associated sample. Data were not qualified based on the use of alternative curves.
The percent differences for chloromethane (-34.1%), 2-CVE (-29.0%), 4-methyl-2-pentanone (+26.1%), and 2-hexanone (+31.4%) in the continuing calibration analyzed on March 1, 2004 were above the method criteria of 20%.These compounds were not detected in the associated samples. The reporting limits for chloromethane and 2-CVEare qualified as estimated and flagged "UJ".
K:\005\LINDSAY\2004\AnaIyucal DataMst Qlr 2004\New Irrigation Well - soils VOC.doe URSPage 1 of 3
VOCs Soil - New Irrigation Well, February 2004April 6, 2004
4. Blanks - Acceptable
5. Surrogates - Acceptable
6. Matrix Spike/Matrix Spike Duplicate (MS/MSD) - Acceptable except as noted below:
A MS/MSD pair was performed on sample "SP-1". The percent recoveries for several compounds were outside ofthe project criteria of 75% to 125% as shown below:
Analvte %Rec MS/MSD % RPD Qualifier Assigned2-CVE 62.3/64.0 3.9 UJ2-Hexanone 126/123 1.2 None2-Butanone 126/124 0.3 NoneVinyl Acetate 57.6/45.8 21.3 UJ
These compounds were not detected in the parent sample. As the data indicate high bias for 2-hexanone and 2-butanone, data are not qualified. The results for 2-CVE and vinyl acetate in sample SP-1 are qualified as estimatedand flagged "UJ" as they were not detected.
7. Laboratory Control Sample (LCS) - Acceptable except as noted below:
Several compound recoveries in the LCS and LCS duplicate analyzed on March 1, 2004 were outside of the 80% to120% limits as shown below:
Analvte %Rec LCS / LCSE) % RPD Qualifier AssignedChJoromethane 58.2/56.4 3.1 UJBromomethane 78.6/78.0 0.8 UJ2-CVE 68.6/72.2 5.1 UJ4-Methyl-2-pentanone 123 / 124 0.6 None2-Hexanone 124/126 1.0 NoneVinyl Chloride 80.2/76.0 5.4 NoneTrichlorofluoromethane 81.0/78.8 2.8 None
•\
None of these compounds were detected in the. associated samples. As 4-methyl-2-pentanone and 2-hexanoneindicate a high bias, data are not qualified. As only the LCSD was outside of the criteria for vinyl chloride andtrichlorofluoromethane, data are not qualified. The results for chloromethane, bromomethane, and 2-CVE inassociated samples are qualified as estimated and flagged "UJ".
8. Internal Standards - Acceptable
9. Target Compound Identification - Acceptable
10. Field Duplicate - Not Applicable
11. Type of Review - Summary
Overall Assessment of Data:
The usefulness of the data is based on the EPA guidance documents listed above. Upon consideration ofthe information presented above, the data are acceptable except where flagged with data qualifiers that modify theusefulness of the individual values. Data qualifiers do not affect the use of the data in relation to the project consentdecree.
K:\005\UNDSAY\2004\Analytical DataMst Qtr 2004\New Irrigation Well - soils VOC.doc URSPage 2 of 3
VOCs Soil - New Irrigation Well, February 2004April 6, 2004
Data Qualifiers:
U - The analyte was analyzed for, but was not detected above the reported sample quantitation limit.
J - The analyte was positively identified; the associated numerical value is the approximate concentration of theanalyte in the sample.
UJ - The analyte was not detected above the reported sample quantitation limit. However, the reported quantitationlimit is approximate and may or may not represent the actual limit of quantitation necessary to accurately andprecisely measure the analyte in the sample.
R - The sample results are rejected due to serious deficiencies in the ability to analyze the sample and meet qualitycontrol criteria. The presence or absence of the analyte cannot be verified.
K:\005\JLlNDSAY\2004\Analytical DataMst Qtr 2004\New Irrigation Well - soils VOC.doc LTRSPage 3 of 3
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MS-Met:hod 8260BPage 1 of 1
Sample ID: SP-1SAMPLE
Lab Sample ID: GJ11AL.IMS ID: 04-2953Matrix: SoilData Release Authorized:/^'Reported: 03/08/04
Instrument/Analyst: FINN5/PABDate Analyzed: 03/01/04 12:58
CAS Number Analyte
QC Report No: GJ11-URS CorpProject: Lindsay Mfg
Date Sampled: 02/25/04Date Received: 02/26/04
Sample Amount: 4.76 g-dry-wtPercent Moisture: 5.9%
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-1
Chlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1 , 1 -Dichloroethanetrans -1, 2-Dichloroethenecis - 1 , 2 -DichloroetheneChloroform1, 2 -Dichloroethane2 -Butanone1, 1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2 -Dichloropropanecis -1,3 -DichloropropeneTrichloroetheneDibrotnochlorome thane1,1,2 -TrichloroethaneBenzenetrans-1, 3 -Dichloropropene2 -ChloroethylvinyletherBromof orm4-Methyl-2-Pentaiione (MIBK)2 -HexanoneTetrachloroethene1,1,2,2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1, 2-Trichloro-l, 2 , 2-trif luoroe
Reported in /^g/kg (ppb)
Volatile Surrogate Recovery
d4 -1, 2 -Dichloroethane 109%de-Toluene 100%Bromof luorobenzene 90.5%d.4-1, 2-Dichlorobenzene 94.5%
1.11. 11 . 11. 12 . 15.31.11. 11 . 11. 11.11. 11 . 15.31 . 11. 15.31.11. 11.11.11. 11 . 11.11. 15.31 . 15.35.31 . 11.11.11.11.11.11.12.1
< 1 . 1 U< 1 . 1 U< 1 . 1 U< 1. 1 U< 2 . 1 U< 5.3 U< 1. 1 U< 1-1 U< 1.1 U< 1.1 U< 1 . 1 U< 1 . 1 U< 1. 1 U< 5 . 3 U< 1. 1 U< 1 . 1 U< 5 . 3 U< 1.1 U< 1 . 1 U< 1 . 1 U< 1 . 1 U< 1 . 1 U< 1 . 1 U< 1.1 U< 1.1 U< 5 . 3 U< 1 . 1 U< 5 . 3 U< 5.3 U< 1.1 U< 1 . 1 U< 1.1 U< 1.1 U< 1.1 U< 1-1 U< 1.1 U< 2 . 1 U
ANALYTICAL (RESOURCES'INCORPORATED
ucr
ucr
000010
FORM I
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge & Trap GC/MS-Method 8260BPage 1 of 1
ANALYTICAL jRESOURCESV
INCORPORATEDSample ID: SP-2
SAMPLE
Lab Sample ID: GJ11BLIMS ID: 04-2954Matrix: SoilData Release Authorized;Reported: 03/08/04
Instrument/Analyst: FINN5/PABDate Analyzed: 03/01/04 13:29
QC Report No: GJ11-URS CorpProject: Lindsay Mfg
Date Sampled: 02/25/04Date Received: 02/26/04
Sample Amount: 4.75 g-dry-wtPercent Moisture: 5.4%
CAS Number Analyte RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-21 OR-10-1591-78-6127-18-4
- 79-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-1
Chlorome thaneB romome t ha neVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1 -Dichloroethanetrans -1, 2 -Dichloroethenecis-1, 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2-Butanone1,1, 1 -TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2 -Dichloropropanecis - 1 , 3 -DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -TrichloroethaneBenzenetrans- 1, 3 -Dichloropropene2 -ChloroethylvinyletherBromoform4 -Methyl -2^Pentanone (MIBK)2 -HexanoneTetrachloroethene1,1,2, 2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luorome thane1,1; 2-Trichloro-l, 2, 2-trif luoroe
Reported in pig/kg (ppb)
Volatile Surrogate Recovery
d4-l, 2 -Dichloroethane 111%d8-Toluene 103%Bromof luorobenzene 90.8%d4-l , 2 -Dichlorobenzene 94.0%
1 . 11.11.11 . 12 . 15.31 . 11 .11.11.11 . 11 . 11.15 .31 . i1. 1*5.31.11. 11. 11 . 11 . 11. 11.11 . 15 .31.1c -i
5 .31.11.11.11.11. 11 . 11.12.1
< 1. 1 U< 1. 1 U< 1. 1 U< 1. 1 U< 2 . 1 U< 5.3 U< 1. 1 U< 1. 1 U< 1. 1 U< 1 . 1 U< 1. 1 U< 1. 1 U< 1. 1 U< 5. 3 U< 1. 1 U< 1. 1 U< 5.3 U< 1.1 U< 1. 1 U< 1. 1 U< 1 . 1 U< 1. 1 U< 1 . 1 U< 1 . 1 U< 1 . 1 U< 5 . 3 U< 1.1 U< 5 3 U< 5. 3 U< 1.1 U< 1.1 U< 1.1 U< 1.1 a< 1. 1 U< 1. 1 U< 1.1 U< 2 . 1 U
'JC5-<J3T
\->3~
K~
000011
FORM I
ORGANICS ANALYSIS DATA SHEETVolatiles by Purge £ Trap GC/MS-Method 8260BPage 1 of 1
Sample ID: SP-3SAMPLE
Lab Sample ID: GJ11CLIMS ID: 04-2955Matrix: SoilData ReleaseReported: 03/08/04
Instrument/Analyst : FINN5/PABDate Analyzed: 03/01/04 13:59
CAS Kumber Analyte
QC Report No: GJ11-URS CorpProject; Lindsay Mfg
Date Sampled: 02/25/04Date Received: 02/26/04
Sample Amount: 4.40 g-dry-wtPercent Moisture.- 12.1%
RL Result
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-5156-59-267-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-6110-75-875-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-575-69-476-13-1
Chlorome thaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1, 1 -Dichloroethene1 , 1 -Dichloroethanetrans -1, 2 -Dichloroethenecis-1, 2 -DichloroetheneChloroform1 , 2 -Dichloroethane2 -Butanone1,1,1 -TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane1 , 2 -Dichloropropanecis-1, 3-DichloropropeneTrichloroetheneDibromochlorome thane1,1,2 -TrichloroethaneBenzenetrans - 1 , 3 -Dichloropropene2 -ChloroethylvinyletherBromof orm4-Methyl-2-Pentanone (MIBK)2 -HexanoneTetrachloroethene1 , 1 , 2 , 2 -TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneTrichlorof luoromethane1,1, 2-Trichloro-l, 2 , 2 -trif lyp.roe
Reported in A*g/kg (ppb)
Volatile Surrogate Recovery
d4-l, 2 -Dichloroethane 113%d8-Toluene 102%Bromof luorobenzene 90.3%d.4-1, 2 -Dichlorobenzene 92.2%
1.11. 11.11.12 .35 .71 . 11 . 11 . 11 . 11 . 1
•1.11 . 15 .71 . 11. 15.71. 11.11 . 11 . 11 . 11 . 11.11. 15.71 . 15.75.7
1.11.11. 11.11 . 11. 11.12.3
< 1. 1 U< 1 . 1 U< 1.1 U< 1. 1 U< 2 . 3 U< 5.7 U< 1. 1 U< 1 . 1 U< 1. 1 U< 1. 1 U< 1.1 U< 1. 1 U< 1. 1 U< 5.7 U< 1.1 U< 1. 1 U< 5. 7 U< 1.1 U< 1.1 U< 1. 1 U< 1. 1 U< 1.1 U< 1.1 U< 1. 1 U< 1. 1 U< 5.7 U< 1. 1 U< 5 .7 a< 5.7 U< 1. 1 U< 1. 1 U< 1 . 1 U< 1.1 U< 1.1 U< 1 . 1 U< 1.1 U< 2.3 U
ANALYTICAL |RESOURCES'INCORPORATED
000012
FORM I