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Variability on a Variability on a Small Scale Small Scale Optimizing Sampling Protocol Implementing Sampling Protoc Preserving Sample Integrity Analytical Error Intro 1 INTRODUCTION

B Introduction to the TOS - QA-QC.ppt

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  • Variability on a Small Scale Optimizing Sampling Protocol Implementing Sampling Protocol Preserving Sample Integrity Analytical ErrorIntro 1INTRODUCTION

  • Optimizing Sampling Protocol In Situ Nugget Effect Fundamental Sampling Error Grouping & Segregation ErrorIntro 2

  • Implementing Sampling Protocol Increment Delimitation Error Increment Extraction ErrorIntro 3 Increment Weighting Error

  • Preserving Sample Integrity Increment Preparation Errors

    Contamination Error Loss Error Alteration Error Human Error Fraud & SabotageIntro 4

  • Analytical Error Scope Versus Principle Additive Interferences Proportional Interferences Drying Temperature Baseline Dissolution Technique Composition of Dissolution Residues Contamination and LossesIntro 5

  • Variability on a Large Scale Interpolation Error Time Space

    Periodic Error Increment Weighting ErrorIntro 6

  • Setting PrioritiesEffect of Problem

    Large

    Small SmallLarge

    Cost of fixing problemYes

    by all means!Yes

    but do a feasibility studyYes

    nothing tolooseNoIntro 7

  • Setting Priorities for Sampling Gold,or base metalsEffect of Problem

    Large

    Small SmallLarge

    Cost of fixing problemSPC6 sigmaTQMFSEIPEGSEIDE IEEAESampling IntervalIn Situ Nugget EffectSampling Mode

    IWEIntro 8Bias TestCorrecting FactorRound Robin

  • The Three-legged TableCompany Benefits

    EffectiveManagementCorrectSampling

    UnderstandingVariabilityIntro 9

  • Effective Management Identify Structural ProblemsIntro 10 Invest in Solutions to Structural Problems Identify Circumstantial Problems Time & Money Can Be Saved on Circumstantial Problems Understand and Act on All Sources of Variability Be Proactive Instead of Reactive

  • Correct Sampling In Situ Nugget EffectIntro 11 Grouping & Segregation Error Increment Delimitation ErrorIncrement Extraction Error Analytical Error Fundamental Sampling Error Increment Preparation Errors Interpolation Error Periodic Error Increment Weighting Error

  • Understanding Variability Variability Generates Visible and Invisible CostsIntro 12 Variability is a Problem and an Opportunity There are Many Kinds of Variability Minimize Variability by a Constant Improvement Strategy All Sampling Errors Magnify Variability Geostatistics Analyzes Variability at the Mine Chronostatistics Analyzes Variability at the Plant