12
13 4. Appendices 4.1 Sample calculations 4.1.1. Power requirement calculations For an impeller speed reading of 55 RPM operated in an Baffled tank with size 4flat blade impeller Actual Impeller Speed: Actual RPM = (1.26*RPM reading) 40.84 = (1.26*55 RPM) 40.84 = 28.46 RPM RPM to RPS: N = RPM/60 = 28.46 RPM/60s = 0.4743 RPS Angular velocity: ω= 2πN = 2Π(0.4743 RPS) = 2.9803 rad/s Force reading conversion from g to N: F g = 9g = 0.0882 N Average Force: F ave = (F N + F g )/2 = (0.09N + 0.0882N)/2 = 0.0891N Torque: τ = F ave * Moment Arm = 0.0891N * 0.11m = 0.0098 J Experimental Power Requirement: Reynolds Number: Power Number, N Po : from plot of N Po vs N Re shown in appendix 4.2 using curve no. 10 for baffled tank and curve no.29 for unbaffled tank

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Page 1: Appendix AG

13

4. Appendices

4.1 Sample calculations

4.1.1. Power requirement calculations

For an impeller speed reading of 55 RPM operated in an Baffled tank with size

4flat blade impeller

Actual Impeller Speed:

Actual RPM = (1.26*RPM reading) – 40.84

= (1.26*55 RPM) – 40.84 = 28.46 RPM

RPM to RPS:

N = RPM/60 = 28.46 RPM/60s = 0.4743 RPS

Angular velocity:

ω= 2πN = 2Π(0.4743 RPS) = 2.9803 rad/s

Force reading conversion from g to N:

Fg = 9g

= 0.0882 N

Average Force:

Fave = (FN + Fg)/2 = (0.09N + 0.0882N)/2 = 0.0891N

Torque:

τ = Fave * Moment Arm = 0.0891N * 0.11m = 0.0098 J

Experimental Power Requirement:

Reynolds Number:

Power Number, NPo:

from plot of NPo vs NRe shown in appendix 4.2 using curve no. 10 for

baffled tank and curve no.29 for unbaffled tank

Page 2: Appendix AG

14

Power from graph:

Correction factor:

Theoretical Power requirement:

Percent Difference:

4.1.2. Conductivity measurements

For baffled tank with size 4 flat blade impeller

Average initial conductivity:

Time of mixing:

Time at which conductivity is stable within 1 percent of the reading

4.1.3. Scale-up calculations (V2= 15m3)

For size 4 flat blade impelle

Scale-up ratio:

Scaling -up dimensions:

Tank Diameter:

Tank Height:

Liquid Height:

Page 3: Appendix AG

15

Impeller Diameter:

Impeller Elevation:

Impeller speed:

Where n=2/3, for equal power per unit volume, n=1, for equal liquid

motion and n=0.5, for equal Froude number

Scaling up power requirement:

Scaling up time of mixing:

Page 4: Appendix AG

16

4.2. Processed Data Tables

Table 4.2-1 Baffled Tank with Size 4 flat blade impeller experimental power requirement

Table 4.2-2 Unbaffled Tank with Size 4 flat blade impeller experimental power requirement

Impeller

Speed (RPM)

Actual Impeller

Speed

(RPM)

Actual Impeller

Speed

(RPS)

Angular

Speed (rad/s)

Force Balance Reading

Average

Force (N)

Torque

(J)

Experimental

Power (W)

Initial N Reading

Final N Reading

Actual

N

Reading

Initial g Reading

Final g Reading

Actual g Reading

Actual

N (from g

reading)

50.00 22.16 0.3693 2.3206

1.21

1.25 0.04

122.00

129.00 7.00 0.07 0.0543 0.0060 0.0139

80.00 59.96 0.9993 6.2790 1.29 0.08 132.00 10.00 0.10 0.0890 0.0098 0.0615

120.00 110.36 1.8393 11.5569 1.32 0.11 134.00 12.00 0.12 0.1138 0.0125 0.1447

150.00 148.16 2.4693 15.5153 1.35 0.14 140.00 18.00 0.18 0.1582 0.0174 0.2700

180.00 185.96 3.0993 19.4737 1.45 0.24 150.00 28.00 0.27 0.2572 0.0283 0.5509

215.00 230.06 3.8343 24.0918 2.00 0.79 205.00 83.00 0.81 0.8017 0.0882 2.1246

Impeller

Speed (RPM)

Actual Impeller

Speed

(RPM)

Actual Impeller

Speed

(RPS)

Angular

Speed (rad/s)

Force Balance Reading Average

Force (N)

Torque

(J)

Experimental

Power (W)

Initial N Reading

Final N Reading

Actual N Reading

Initial g Reading

Final g Reading

Actual g Reading

Actual N

(from g

reading)

55.00 28.46 0.4743 2.9803

1.21

1.30 0.09

122.00

131.00 9.00 0.0882 0.0891 0.0098 0.0292

85.00 66.26 1.1043 6.9387 1.45 0.24 146.00 24.00 0.2352 0.2376 0.0261 0.1814

110.00 97.76 1.6293 10.2374 2.29 1.08 231.00 109.00 1.0682 1.0741 0.1182 1.2096

Page 5: Appendix AG

17

Table 4.2-3. Baffled Tank with Size 4 flat blade impeller theoretical power requirement

and percent difference

NRe NPo N3D'

Power from

graph (W)

Theoretical

Power (W) % Difference

23089.7862 1.80 0.0340 0.0612 0.0286 2.14

53757.1763 1.80 0.4292 0.7726 0.3609 49.75

79313.3346 1.80 1.3785 2.4814 1.1591 4.36

Table 4.2-4. Unbaffled Tank with Size 4 flat blade impeller theoretical power requirement

and percent difference

NRe NPo N3D'

Power from graph (W)

Theoretical Power (W)

% Difference

17978.5546 0.18 0.0161 0.0029 0.0057 142.01

48645.9446 0.17 0.3181 0.0541 0.1072 42.63

89535.7980 0.15 1.9832 0.2975 0.5895 75.46

120203.1880 0.14 4.7988 0.6718 1.3314 79.72

150870.5780 0.14 9.4885 1.3284 2.6325 79.07

186649.1997 0.14 17.9664 2.5153 4.9847 57.38

Table 4.2-5. Baffled Tank with Size 5 flat blade impeller theoretical power requirement

and percent difference

NRe NPo N3D'

Power from graph (W)

Theoretical Power (W)

% Difference

22338.0263 1.80 0.0620 0.1115 0.0585 42.48

42581.0593 1.80 0.4292 0.7726 0.4055 54.34

54726.8792 1.80 0.9113 1.6403 0.8609 54.89

62824.0924 1.80 1.3785 2.4814 1.3023 38.38

Table 4.2-6. Unbaffled Tank with Size 5 flat blade impeller theoretical power requirement

and percent difference

NRe NPo N3D'

Power from

graph (W)

Theoretical

Power (W) % Difference

14240.8131 0.20 0.0161 0.0032 0.0072 93.49

30435.2395 0.18 0.1567 0.0282 0.0628 35.74

79018.5188 0.16 2.7430 0.4389 0.9772 85.67

95212.9452 0.16 4.7988 0.7678 1.7096 88.15

135699.0113 0.15 13.8923 2.0838 4.6400 90.66

151893.4377 0.15 19.4832 2.9225 6.5074 90.89

168087.8641 0.15 26.4029 3.9604 8.8186 91.21

Page 6: Appendix AG

18

Table 4.2-7 Baffled Tank with Size 5 flat blade impeller experimental power requirement

Impeller Speed

(RPM)

Actual

Impeller

Speed (RPM)

Actual

Impeller

Speed (RPS)

Angular Speed

(rad/s)

Force Balance Reading

Average Force

(N)

Torque

(J)

Experimental Power

(W) Initial N

Reading

Final N

Reading

Actual

N Reading

Initial g

Reading

Final g

Reading

Actual g

Reading

Actual

N (from

g

reading)

60.00 34.76 0.5793 3.6401

1.24

1.32 0.08

126.00

135.00 9.00 0.09 0.0841 0.0093 0.0337

85.00 66.26 1.1043 6.9387 1.49 0.25 150.00 24.00 0.24 0.2426 0.0267 0.1852

100.00 85.16 1.4193 8.9179 1.63 0.39 167.00 41.00 0.40 0.3959 0.0435 0.3884

110.00 97.76 1.6293 10.2374 1.94 0.70 200.00 74.00 0.73 0.7126 0.0784 0.8025

Table 4.2-7 Unbaffled Tank with Size 5 flat blade impeller experimental power requirement

Impeller

Speed

(RPM)

Actual Impeller

Speed

(RPM)

Actual Impeller

Speed

(RPS)

Angular

Speed

(rad/s)

Force Balance Reading

Average

Force

(N)

Torque

(J)

Experimental

Power

(W) Initial N Reading

Final N Reading

Actual

N

Reading

Initial g Reading

Final g Reading

Actual g Reading

Actual

N (from g

reading)

50.00 22.16 0.3693 2.3206

1.21

1.24 0.03

122.00

130.00 8.00 0.08 0.0542 0.0060 0.0138

70.00 47.36 0.7893 4.9595 1.26 0.05 132.00 10.00 0.10 0.0740 0.0081 0.0404

130.00 122.96 2.0493 12.8763 1.30 0.09 133.00 11.00 0.11 0.0989 0.0109 0.1401

150.00 148.16 2.4693 15.5153 1.32 0.11 135.00 13.00 0.13 0.1187 0.0131 0.2026

200.00 211.16 3.5193 22.1126 1.39 0.18 140.00 18.00 0.18 0.1782 0.0196 0.4335

220.00 236.36 3.9393 24.7516 1.42 0.21 145.00 23.00 0.23 0.2177 0.0239 0.5927

240.00 261.56 4.3593 27.3905 1.45 0.24 150.00 28.00 0.27 0.2572 0.0283 0.7749

Page 7: Appendix AG

19

Table 4.2-8 Initial Conductivity

Time (s)

Size 4 flat blade impeller Size 5 flat blade impeller

Conductivity, K (mS/cm) Conductivity, K (mS/cm)

Baffled Unbaffled Baffled Unbaffled

0 1.58 1.51 1.53 1.53

5 1.54 1.54 1.56 1.58

10 1.56 1.56 1.54 1.54

15 1.57 1.54 1.54 1.58

20 1.54 1.53 1.53 1.54

25 1.58 1.54 1.56 1.51

30 1.54 1.56 1.57 1.54

35 1.54 1.55 1.53 1.58

40 1.58 1.57 1.54 1.5

45 1.57 1.54 1.54 1.54

50 1.53 1.55 1.55 1.57

Kave 1.56 1.54 1.54 1.55

Page 8: Appendix AG

20

Table 4.2-9 Conductivity as a function of time (time of mixing)

Time (s)

Size 4 flat blade impeller Size 5 flat blade impeller

Conductivity, K (mS/cm) Conductivity, K (mS/cm)

B ΔK % diff UnB ΔK % diff B ΔK % diff UnB ΔK % diff

0 1.56 - - 1.54 - - 1.54 - 1.55 - -

3 4.71 3.15 - 2.04 0.50 - 4.70 3.16 - 3.50 1.95 -

6 4.02 0.69 78.10 3.52 1.48 196.00 4.05 0.65 79.43 6.01 2.51 28.72

9 4.08 0.06 91.30 3.65 0.13 91.22 4.02 0.03 95.38 5.04 0.97 61.35

12 4.07 0.01 83.33 6.52 2.87 2107.69 4.01 0.01 66.67 4.51 0.53 45.36

15 4.08 0.01 0.00 3.51 3.01 4.88 4.02 0.01 0.00 4.16 0.35 33.96

18 4.07 0.01 0.00 3.50 0.01 99.67 4.01 0.01 0.00 4.08 0.08 77.14

21 4.08 0.01 0.00 3.56 0.06 500.00 4.02 0.01 0.00 4.00 0.08 0.00

24 4.04 0.04 300.00 3.53 0.03 50.00 4.00 0.02 100.00 3.59 0.41 412.50

27 4.07 0.03 25.00 3.54 0.01 66.67 4.01 0.01 50.00 3.58 0.01 97.56

30 4.05 0.02 33.33 3.53 0.01 0.00 4.02 0.01 0.00 3.57 0.01 0.00

33 4.07 0.02 0.00 3.55 0.02 100.00 4.02 0.00 100.00 3.56 0.01 0.00

36 4.05 0.02 0.00 3.54 0.01 50.00 4.01 0.01 0 3.57 0.01 0.00

39 4.04 0.01 50.00 3.51 0.03 200.00 4.02 0.01 0.00 3.54 0.03 200.00

42 4.06 0.02 100.00 3.56 0.05 66.67 4.00 0.02 100.00 3.56 0.02 33.33

45 4.08 0.02 0.00 3.53 0.03 40.00 4.02 0.02 0.00 3.57 0.01 50.00

48 4.05 0.03 50.00 3.52 0.01 66.67 4.02 0.00 100.00 3.58 0.01 0.00

51 4.06 0.01 66.67 3.55 0.03 200.00 4.00 0.02 0 3.55 0.03 200.00

54 4.06 0.00 100.00 3.54 0.01 66.67 4.01 0.01 50.00 3.56 0.01 66.67

57 4.05 0.01 0 3.53 0.01 0.00 4.01 0.00 100.00 3.56 0.00 100.00

60 4.05 0.00 100.00 3.56 0.03 200.00 4.01 0.00 0 3.56 0.00 0

63 4.04 0.01 0 3.54 0.02 33.33 4.02 0.01 0 3.55 0.01 0

66 4.05 0.01 0.00 3.56 0.02 0.00 4.03 0.01 0.00 3.54 0.01 0.00

69 4.06 0.01 0.00 3.55 0.01 50.00 4.02 0.01 0.00 3.55 0.01 0.00

72 4.04 0.02 100.00 3.55 0.00 100.00 4.01 0.01 0.00 3.55 0.00 100.00

75 4.05 0.01 50.00 3.53 0.02 0 4.01 0.00 100.00 3.59 0.04 0

78 4.04 0.01 0.00 3.55 0.02 0.00 4.00 0.01 0 3.57 0.02 50.00

81 4.06 0.02 100.00 3.54 0.01 50.00 4.02 0.02 100.00 3.56 0.01 50.00

84 4.05 0.01 50.00 3.55 0.01 0.00 4.03 0.01 50.00 3.56 0.00 100.00

87 4.05 0.00 100.00 3.56 0.01 0.00 4.02 0.01 0.00 3.55 0.01 0

90 4.03 0.02 0 3.53 0.03 200.00 4.02 0.00 100.00 3.59 0.04 300.00

93 4.04 0.01 50.00 3.53 0.00 100.00 4.02 0.00 0 3.59 0.00 100.00

96 4.03 0.01 0.00 3.56 0.03 0 4.02 0.00 0 3.55 0.04 0

Page 9: Appendix AG

21

Table 4.2-10 Scale up dimensions

Dimensions

Small Scale Large Scale

Size 4 flat blade

Size 5 flat blade

Size 4 flat blade

Size 5

flat blade

Impeller Diameter, D' (m) 0.200 0.178 1.6369 1.4568

Elevation, Zi(m) 0.110 0.105 0.9003 0.8594

Tank

Diameter,DT(m) 0.288 2.3571

Height, HT (m) 0.420 3.4375

Volume, V(m3) 0.027 15.0000

Liquid Height, Zl(m) 0.300 2.4553

Scale-up ratio, R 8.184441282

Time (s)

Size 4 flat blade impeller Size 5 flat blade impeller

Conductivity, K (mS/cm) Conductivity, K (mS/cm)

B ΔK % diff UnB ΔK % diff B ΔK % diff UnB ΔK % diff

99 4.03 0.00 100.00 3.54 0.02 33.33 4.01 0.01 0 3.59 0.04 0.00

102 4.03 0.00 0 3.52 0.02 0.00 4.00 0.01 0.00 3.56 0.03 25.00

105 4.04 0.01 0 3.54 0.02 0.00 4.01 0.01 0.00 3.56 0.00 100.00

108 4.05 0.01 0.00 3.55 0.01 50.00 4.01 0.00 100.00 3.55 0.01 0

111 4.03 0.02 100.00 3.54 0.01 0.00 4.02 0.01 0 3.56 0.01 0.00

114 4.04 0.01 50.00 3.54 0.00 100.00 4.00 0.02 100.00 3.56 0.00 100.00

117 4.02 0.02 100.00 3.53 0.01 0 4.03 0.03 50.00 3.55 0.01 0

120 4.04 0.02 0.00 3.54 0.01 0.00 4.00 0.03 0.00 3.56 0.01 0.00

130 4.05 0.01 50.00 3.53 0.01 0.00 4.01 0.01 66.67 3.56 0.00 100.00

140 4.02 0.03 200.00 3.54 0.01 0.00 4.03 0.02 100.00 3.54 0.02 0

150 4.02 0.00 100.00 3.56 0.02 100.00 4.03 0.00 100.00 3.54 0.00 100.00

160 4.04 0.02 0 3.54 0.02 0.00 4.01 0.02 0 3.54 0.00 0

170 4.03 0.01 50.00 3.53 0.01 50.00 4.00 0.01 50.00 3.59 0.05 0

180 4.02 0.01 0.00 3.53 0.00 100.00 4.01 0.01 0.00 3.53 0.06 20.00

190 4.05 0.03 200.00 3.52 0.01 0 4.02 0.01 0.00 3.56 0.03 50.00

200 4.01 0.04 33.33 3.54 0.02 100.00 4.02 0.00 100.00 3.54 0.02 33.33

210 4.03 0.02 50.00 3.53 0.01 50.00 4.02 0.00 0 3.54 0.00 100.00

220 4.04 0.01 50.00 3.54 0.01 0.00 4.01 0.01 0 3.59 0.05 0

230 4.02 0.02 100.00 3.52 0.02 100.00 4.00 0.01 0.00 3.54 0.05 0.00

240 4.03 0.01 50.00 3.54 0.02 0.00 4.00 0.00 100.00 3.55 0.01 80.00

250 4.02 0.01 0.00 3.53 0.01 50.00 4.00 0.00 0 3.54 0.01 0.00

Page 10: Appendix AG

22

Table 4.2-11 Scaled-up power requirement and mixing time of baffled tank with Size 4 flat

blade impeller

n N1(rps) N2

(rps) Nre Npo N

3D'

5ρ Pgraph (W) Pth (W) tm (s)

0.67

0.4743 0.1160 3.7818E+05 1.80 18.2591 32.8664 15.3519 69.47

1.1043 0.2700 8.8046E+05 1.80 230.4250 414.7650 193.7365 29.84

1.6293 0.3984 1.2990E+06 1.80 740.0464 1332.0834 622.2153 20.23

1.00

0.4743 0.0580 1.8898E+05 1.80 2.2784 4.1010 1.9156 139.03

1.1043 0.1349 4.3997E+05 1.80 28.7522 51.7539 24.1742 59.72

1.6293 0.1991 6.4914E+05 1.80 92.3421 166.2158 77.6393 40.47

0.50

0.4743 0.1658 5.4063E+05 1.80 53.3463 96.0234 44.8525 48.60

1.1043 0.3860 1.2587E+06 1.80 673.2154 1211.7877 566.0253 20.87

1.6293 0.5695 1.8571E+06 1.80 2162.1376 3891.8477 1817.8796 14.15

Table 4.2-12 Scaled-up power requirement and mixing time of unbaffled tank with Size 4

flat blade impeller

n N1(rps) N2

(rps) Nre Npo N

3D'

5ρ Pgraph (W) Pth (W) tm(s)

0.67

0.3693 0.0903 2.9446E+05 0.15 8.6196 1.2929 0.6465 202.59

0.9993 0.2443 7.9675E+05 0.13 170.7498 22.1975 11.0987 78.49

1.8393 0.4497 1.4665E+06 0.12 1064.6587 127.7590 63.8795 43.79

1.00

0.3693 0.0451 1.4714E+05 0.16 1.0755 0.1721 0.0860 396.88

0.9993 0.1221 3.9814E+05 0.13 21.3060 2.7698 1.3849 157.08

1.8393 0.2247 7.3280E+05 0.12 132.8469 15.9416 7.9708 87.63

0.50

0.3693 0.1291 4.2096E+05 0.15 25.1831 3.7775 1.8887 141.71

0.9993 0.3493 1.1390E+06 0.13 498.8668 64.8527 32.4263 54.91

1.8393 0.6429 2.0964E+06 0.12 3110.5331 373.2640 186.6320 30.63

Page 11: Appendix AG

23

Table 4.2-13 Scaled-up power requirement and mixing time of baffled tank with Size 5 flat

blade impeller

n N1(rps) N2

(rps) Nre Npo N

3D'

5ρ Pgraph (W) Pth(W) tm (s)

0.67

0.5793 0.1417 3.6586E+05 1.80 18.5765 33.4378 17.5492 73.93

1.1043 0.2700 6.9742E+05 1.80 128.6707 231.6073 121.5546 38.78

1.4193 0.3470 8.9635E+05 1.80 273.1696 491.7052 258.0620 30.18

1.00

0.5793 0.0708 1.8282E+05 1.80 2.3180 4.1723 2.1898 147.95

1.1043 0.1349 3.4850E+05 1.80 16.0554 28.8997 15.1674 77.61

1.4193 0.1734 4.4791E+05 1.80 34.0858 61.3544 32.2007 60.39

0.50

0.5793 0.2025 5.2303E+05 1.80 54.2737 97.6926 51.2721 51.71

1.1043 0.3860 9.9701E+05 1.80 375.9275 676.6695 355.1369 27.13

1.4193 0.4961 1.2814E+06 1.80 798.0990 1436.5781 753.9604 21.11

Table 4.2-14 Scaled-up power requirement and mixing time of unbaffled tank with Size 5

flat blade impeller

n N1(rps) N2

(rps) Nre Npo N

3D'

5ρ Pgraph (W) Pth (W) tm (s)

0.67

0.3693 0.0903 2.3324E+05 0.15 4.8132 0.7220 1.6076 263.31

0.7893 0.1930 4.9849E+05 0.13 46.9851 6.1081 13.6006 129.16

2.0493 0.5011 1.2942E+06 0.12 822.2747 98.6730 219.7120 51.08

1.00

0.3693 0.0451 1.1655E+05 0.16 0.6006 0.0961 0.2140 515.82

0.7893 0.0964 2.4910E+05 0.13 5.8627 0.7622 1.6971 258.47

2.0493 0.2504 6.4672E+05 0.12 102.6025 12.3123 27.4154 102.22

0.50

0.3693 0.1291 3.3344E+05 0.14 14.0624 1.9687 4.3837 188.43

0.7893 0.2759 7.1262E+05 0.13 137.2729 17.8455 39.7360 90.35

2.0493 0.7163 1.8502E+06 0.12 2402.3780 288.2854 641.9159 35.73

Page 12: Appendix AG

24

Figure 4.2-1 Power Consumption of various agitators expressed in terms of Po as a

function of Reynolds number, Re. For curves marked with ° surface effects become

important and the Froude number Fr = g/n2D’ is included as indicated for Re > 300.