60MG SMALL DOG N/A Matrix : Derivative Certiﬁcate Harvest/Lot … · 2020. 8. 13. · This report shall not be reproduced, unless in its entirety, without written approval from

This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation

Jorge SegredoLab Director

State License # n/aISO Accreditation # 97164 ___________________

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11/18/2019

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Kaycha Labs60MG SMALL DOG

N/AMatrix : Derivative

Certificateof Analysis

SAMPLE:DA91112011-001Harvest/Lot ID: K03V02

Seed to Sale #N/ABatch#: BMR0030/19

Sample Size: 28.5 gramOrdered : 11/12/19Sampled : 11/12/19

Completed: 11/18/19 Expires: 11/18/20Sampling Method: SOP Client Method

Nov 18, 2019 | Green Roads601 Fairway Drive Deerfield BeachFlorida, United States 33441

PASSED

PRODUCT IMAGE SAFETY RESULTS MISC.

PesticidesPASSED

Heavy MetalsPASSED

MicrobialsPASSED

MycotoxinsPASSED

ResidualsSolventsPASSED

FilthNOT TESTED

Water ActivityNOT TESTED

MoistureNOT TESTED

TerpenesTESTED

CANNABINOID RESULTS

Total THC

0.000%THC/Container :0.00 mg

Total CBD

0.177%CBD/Container :50.45 mg

ND ND 0.165 % ND ND ND ND ND ND ND ND

ND ND1.650mg/g ND ND ND ND ND ND ND ND

D9-THC THCA CBD CBDA CBN CBDV D8-THC THCV CBG CBGA CBC

Cannabinoid Profile TestAnalyst Weight Sample Prep : Extracted By :450 3.0273g 2019-11-13 02:11:54 574

Analysis Method -SOP.T.40.020, SOP.T.30.050Analytical Batch -DA007943

Reagent Dilution Consums. ID

40Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 for sample prep andShimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).




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11/18/2019

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Certificate of Analysis PASSED

Green Roads

601 Fairway Drive Deerfield BeachFlorida, United States 33441Telephone: 9546095537Email: [email protected]

Sample : DA91112011-001,Harvest/LOT ID: K03V02,

Batch# : BMR0030/19Sample Size : 28.5 gramOrdered : 11/12/19

Sampled : 11/12/19Completed : 11/18/19 Expires : 11/18/20Sample Method : SOP Client Method

2

Terpenes TESTED

Terpenes TEST RESULT (%)

ALPHA-CEDRENE NDALPHA-HUMULENE NDALPHA-PINENE NDALPHA-TERPINENE NDBETA-MYRCENE NDBETA-PINENE NDBORNEOL NDCAMPHENE NDCAMPHOR NDCARYOPHYLLENE OXIDE NDCEDROL NDALPHA-BISABOLOL NDISOPULEGOL NDCIS-NEROLIDOL ND3-CARENE NDFENCHYL ALCOHOL NDHEXAHYDROTHYMOL NDEUCALYPTOL NDISOBORNEOL NDFARNESENE NDFENCHONE NDGAMMA-TERPINENE NDGERANIOL NDGERANYL ACETATE NDGUAIOL NDLIMONENE NDLINALOOL NDNEROL NDOCIMENE NDALPHA-PHELLANDRENE NDPULEGONE NDSABINENE NDSABINENE HYDRATE ND

Terpenes TEST RESULT (%)

TERPINEOL ND

TERPINOLENE ND

TRANS-CARYOPHYLLENE ND

TRANS-NEROLIDOL ND

VALENCENE ND

Terpenes TESTED

Analyst Weight Sample Prep : Extracted By :585 0.9926g 2019-11-13 03:11:18 585

Analysis Method -SOP.T.40.090Analytical Batch -DA007922


10

Terpenoid profile screening is performed using GC-MS with Liquid Injection (Gas Chromatography –Mass Spectrometer) which can screen 38 terpenes using Method SOP.T.40.091 Terpenoid AnalysisVia GC/MS.

Total 0




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11/18/2019

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Green Roads





3

Pesticides PASSED

Pesticides LOQ Action Level Units ResultCHLORDANE 0.010 0.1 ppm NDCAPTAN 0.100 3 ppm NDBOSCALID 0.010 3000 PPM NDDIMETHOATE 0.010 0.1 ppm NDABAMECTIN B1A 0.020 0.3 ppm NDCIS-PERMETHRIN 0.050 1 ppm NDSPINETORAM 0.010 PPM NDACEPHATE 0.010 3 ppm NDDIMETHOMORPH 0.005 3 ppm NDETHOPROPHOS 0.010 0.1 ppm NDACEQUINOCYL 0.050 2 ppm NDACETAMIPRID 0.010 3 ppm NDETOFENPROX 0.010 0.1 ppm NDALDICARB 0.020 0.1 ppm NDETOXAZOLE 0.010 1.5 ppm NDAZOXYSTROBIN 0.010 3 ppm NDFENHEXAMID 0.010 3 ppm NDBIFENAZATE 0.010 3 ppm NDFENOXYCARB 0.010 0.1 ppm NDFENPYROXIMATE 0.010 2 ppm NDBIFENTHRIN 0.010 0.5 ppm NDCARBARYL 0.010 0.5 ppm NDFIPRONIL 0.020 0.1 ppm NDFLONICAMID 0.010 2 ppm NDCARBOFURAN 0.010 0.1 ppm NDCHLORANTRANILIPROLE 0.010 3 ppm NDFLUDIOXONIL 0.010 3 ppm NDHEXYTHIAZOX 0.010 2 ppm NDCHLORFENAPYR 0.010 0.1 ppm NDIMAZALIL 0.010 0.1 ppm NDCHLORPYRIFOS 0.010 0.1 ppm NDIMIDACLOPRID 0.010 3 ppm NDCLOFENTEZINE 0.010 0.5 ppm NDKRESOXIM-METHYL 0.010 1 ppm NDCOUMAPHOS 0.005 0.1 ppm NDMALATHION 0.010 2 ppm NDCYPERMETHRIN 0.020 1 ppm NDDAMINOZIDE 0.020 0.1 ppm NDMETALAXYL 0.010 3 ppm ND

Pesticides LOQ Action Level Units ResultDICHLORVOS 0.050 0.1 ppm NDMETHIOCARB 0.010 0.1 ppm NDMETHOMYL 0.010 0.1 ppm NDDIAZANON 0.010 0.2 ppm NDMEVINPHOS 0.010 0.1 ppm NDMYCLOBUTANIL 0.010 3 ppm NDNALED 0.010 0.5 ppm NDOXAMYL 0.010 0.5 ppm NDPACLOBUTRAZOL 0.010 0.1 ppm NDTRANS-PERMETHRIN 0.050 1 ppm NDPHOSMET 0.010 0.2 ppm NDPIPERONYL BUTOXIDE 0.010 3 ppm NDPRALLETHRIN 0.050 0.4 ppm NDPROPICONAZOLE 0.010 1 ppm NDPROPOXUR 0.010 0.1 ppm NDPYRETHRIN I 0.010 1 ppm NDPYRIDABEN 0.010 3 ppm NDSPINOSAD (SPINOSYN A) 0.010 3 ppm NDSPINOSAD (SPINOSYN D) 0.010 3 ppm NDSPIROMESIFEN 0.010 3 ppm NDSPIROTETRAMAT 0.020 3 ppm NDSPIROXAMINE 0.010 0.1 ppm NDTEBUCONAZOLE 0.010 1 ppm NDTHIACLOPRID 0.010 0.1 ppm NDTHIAMETHOXAM 0.010 1 ppm NDTRIFLOXYSTROBIN 0.010 3 ppm ND

Pesticides PASSED


Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch - DA007939

Reagent Dilution Consums. ID10

SOP.T.30.065, SOP.T.40.065




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11/18/2019

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Green Roads





4

Residual Solvents PASSED

SOLVENT ACTION LEVEL(PPM)

PASS/FAIL RESULT

PROPANE 2100 PASS ND

BUTANES (N-BUTANE) 2000 PASS ND

ETHYLENE OXIDE 5 PASS ND

METHANOL 250 PASS ND

ETHANOL 5000 PASS 170.946

PENTANES (N-PENTANE) 750 PASS ND

ETHYL ETHER 500 PASS ND

ACETONE 750 PASS ND

2-PROPANOL 500 PASS ND

ACETONITRILE 60 PASS ND

DICHLOROMETHANE 125 PASS ND

N-HEXANE 250 PASS ND

ETHYL ACETATE 400 PASS ND

BENZENE 1 PASS ND

HEPTANE 500 PASS ND

TOLUENE 150 PASS ND

CHLOROFORM 2 PASS ND

1,2-DICHLOROETHANE 2 PASS ND

TRICHLOROETHYLENE 25 PASS ND

1,1-DICHLOROETHENE 8 PASS ND

TOTAL XYLENES 150 PASS ND

Residual Solvents PASSED


Analysis Method -SOP.T.40.032Analytical Batch -DA007958


1 00268767161040-124151941

Residual solvents screening is performed using GC-MS which can detect below single digit ppmconcentrations. Currently we analyze for 34 Residual solvents. (Method: SOP.T.30.042 ResidualSolvents Analysis via GC-MS).




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11/18/2019

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5

Mycotoxins PASSED

Analyte Result Action LevelAFLATOXIN G2 NDAFLATOXIN G1 NDAFLATOXIN B2 NDAFLATOXIN B1 NDOCHRATOXIN A+ ND 0.02TOTAL AFLATOXINS 0.000 0.02


Microbials PASSED

Analyte ResultASPERGILLUS_FLAVUS not present in 1 gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_NIGER not present in 1 gram.ASPERGILLUS_TERREUS not present in 1 gram.ESCHERICHIA_COLI_SHIGELLA_SPP not present in 1 gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.

Heavy Metals PASSED


50

Metal Result Action Level

ARSENIC ND 1.5CADMIUM ND 0.5LEAD ND 0.5MERCURY ND 3


Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma– Mass Spectrometer) which can screen down to below single digit ppbconcentrations for regulated heavy metals using Method SOP.T.30.052 SamplePreparation for Heavy Metals Analysis via ICP-MS and SOP.T.40.050 HeavyMetals Analysis via ICP-MS.

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60MG SMALL DOG N/A Matrix : Derivative Certiﬁcate Harvest/Lot … · 2020. 8. 13. · This report shall not be reproduced, unless in its entirety, without written approval from