510 DRIGGS AVENUE BROOKLYN, NEW YORK Block 2312 Lot 23 … · 2019-03-15 · FORMER STERLING TRANSFORMER CORP. 510 DRIGGS AVENUE BROOKLYN, NEW YORK Block 2312 Lot 23 SITE No. C224203

FORMER STERLING TRANSFORMER CORP. 510 DRIGGS AVENUE

BROOKLYN, NEW YORK Block 2312 Lot 23 SITE No. C224203

REMEDIAL INVESTIGATION REPORT

January 2016 Revised June 2016

Prepared for:

187 North 8 Street Owner LLC 266 Broadway Suite 501

Brooklyn, NY 11211

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1808 Middle Country Road Ridge, NY 11961

Environmental Business Consultants

TABLE OF CONTENTS Remedial Investigation Report Former Sterling Transformer

1.0 INTRODUCTION..................................................................................................................... 1 1.1 Project Background...................................................................................................... 1 1.2 Site Location and Description ..................................................................................... 1 1.3 Redevelopment Plans ................................................................................................... 2 1.4 Site History.................................................................................................................... 2 1.5 Summary of Previous Investigations .......................................................................... 2

1.5.1 Phase I Environmental Site Assessment Screening (DPV -Mar. 2014).......2 1.5.2 Geophysical Survey (H-R Geoscience – Mar. 2014) ...................................3 1.5.3 Phase II Investigation - Data Summary (EBC – Sept. 2014).......................4

2.0 REMEDIAL INVESTIGATION ............................................................................................. 5 2.1 Field Investigation ........................................................................................................ 5 2.2 Deviations from the Remedial Investigation Work Plan .......................................... 5 2.3 Soil Sampling................................................................................................................. 5

2.3.1 Soil Borings ...................................................................................................... 5 2.4 Monitoring Well Installation ....................................................................................... 6

2.4.1 Groundwater Sampling .................................................................................... 6 2.5 Soil Vapor Sampling..................................................................................................... 7

2.5.1 Installation of Soil Vapor Implants .................................................................. 7 2.5.2 Surface Seal Test Procedure ............................................................................ 7 2.5.3 Soil vapor Sample Collection ........................................................................... 7

2.6 Laboratory Analysis .................................................................................................... 8 2.6.1 Analytical Results - Soil Samples ..................................................................... 8 2.6.2 Analytical Results - Groundwater Samples .................................................... 11 2.6.3 Analytical Results - Soil vapor Samples ......................................................... 12 2.6.4 Data Usability Summary Report..................................................................... 12

3.0 HYDROGEOLOGIC ASSESSMENT AND PHYSICAL SETTING .................................. 13 3.1 Site Topography.......................................................................................................... 13 3.2 Surrounding Land Use ............................................................................................... 13 3.3 Regional Geology / Hydrogeology ............................................................................. 13 3.4 Site Geology / Hydrogeology...................................................................................... 14

4.0 NATURE AND EXTENT OF CONTAMINATION............................................................ 15 4.1 Identification of Source Areas ................................................................................... 15 4.2 Groundwater Impacts ................................................................................................ 15 4.3 Soil Vapor Impacts ..................................................................................................... 15 4.4 Site Conceptual Model ............................................................................................... 16

5.0 QUALITATIVE EXPOSURE ASSESSMENT .................................................................... 17 5.1 Contaminant Areas..................................................................................................... 17 5.2 Contaminant Release and Transport Mechanism ................................................... 17 5.3 Point of Exposure, Route of Exposure and Potentially Exposed Populations....... 17

6.0 CONCLUSIONS AND RECOMENDATIONS .................................................................... 19 7.0 REFERENCES ........................................................................................................................ 21

TABLE OF CONTENTS Remedial Investigation Report Former Sterling Transformer

TABLES

Table 1 Summary of Sampling Program Rationale and Analysis Table 2 Monitoring Well Specifications and Elevation Table 3 Laboratory Results – Soil Samples, Volatile Organic Compounds Table 4 Laboratory Results – Soil Samples, Semi-Volatile Organic Compounds Table 5 Laboratory Results – Soil Samples, Pesticides/PCBs Table 6 Laboratory Results – Soil Samples, TAL Metals Table 7 Laboratory Results – Groundwater Samples, Volatile Organic Compounds Table 8 Laboratory Results – Groundwater Samples, Semi-Volatile Organic Compounds Table 9 Laboratory Results – Groundwater Samples, Pesticides/PCBs Table 10 Laboratory Results – Groundwater Samples, Total Metals Table 11 Laboratory Results – Groundwater Samples, Dissolved Metals Table 12 Laboratory Results – Soil Vapor Samples, Volatile Organic Compounds Table 13 Parameters Detected Above Track 1 Soil Cleanup Objectives Table 14 Parameters Detected Above Ambient Groundwater Standards

FIGURES

Figure 1 Site Location Map Figure 2 Site Plan Figure 3 Soil Boring Locations Figure 4 Monitoring Well Locations Figure 5 Groundwater Elevation Map Figure 6 Soil Vapor Sampling Locations Figure 7 Posted Soil Results above Unrestricted / Restricted Residential SCOs Figure 8 Geologic Cross Section Figure 9 Posted Groundwater Results above AWQS Figure 10 Soil Vapor Detections

APPENDICES

Appendix A Soil Boring Logs Appendix B Monitoring Well Completion Reports Appendix C Groundwater Sampling Logs Appendix D Soil Vapor Sampling Log Appendix E Laboratory Reports (On Disk) Appendix F Data Usability Summary Reports

LIST OF ACRONYMS

Acronym Definition

AOC Area of Concern AST Aboveground Storage Tank BCP Brownfields Cleanup Program BCA Brownfield Site Cleanup Agreement CVOC Chlorinated VOC ESA Environmental Site Assessment EBC Environmental Business Consultants IRM Interim Remedial Measure Work Plan NYCDEP New York City Department of Environmental Protection NYSDEC New York State Department of Environmental Conservation NYSDOH New York State Department of Health PID Photo-Ionization Detector PCB Polychlorinated Biphenyls REC Recognized Environmental Condition RI Remedial Investigation RIWR Remedial Investigation Work Plan SVOC Semi-Volatile Organic Compound UST Underground Storage Tank VOC Volatile Organic Compound

REPORT CERTIFICAION I, Charles Sosik, certify that I am currently a Qualified Environmental Professional as defined in 6 NYCRR Part 375 and that this Remedial Investigation Report was prepared in accordance with all applicable statutes and regulations and in substantial conformance with the DER Technical Guidance for Site Investigation and Remediation (DER-10) and that all activities were performed in full accordance with the DER-approved work plan and any DER-approved modifications.

Charles Sosik, PG Date: 6-29-2016 Principal

Former Sterling Transformer 510 Driggs Avenue, Brooklyn, NY Remedial Investigation Report

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Environmental Business Consultants 1808 Middle Country Road Ridge, NY 11961

Phone: 631.504.6000 Fax: 631.924.2870

1.0 INTRODUCTION 1.1 Project Background This Remedial Investigation Report (RIR) was prepared on behalf of 187 North 8 Street Owner LLC for the property known as the Former Sterling Transformer Corp. Site, located at 510 Driggs Avenue, Brooklyn, New York. An application for acceptance into the New York State Brownfield Cleanup Program (BCP) was submitted to the New York State Department of Environmental Conservation (NYSDEC) on December 2, 2014. The application was determined to be complete on December 12, 2014. On March 6, 2015, the DEC notified the North 8 Street Owner LLC that the Site had been accepted to the BCP (Site No. C224203) with the applicant defined as a Volunteer. The Brownfield Cleanup Agreement was executed on June 1 2015. The purpose of this Remedial Investigation Report to document the data collected during the Remedial Investigation to characterize the nature and extent of contamination and to complete a qualitative exposure assessment for future occupants of the proposed building and the surrounding community. The overall objectives of the project are to prepare the Site for unrestricted use as defined in the Brownfield Cleanup Agreement and to remediate known and unknown environmental conditions at the Site to the satisfaction of the NYSDEC and the New York State Department of Health (NYSDOH). The field work portion of the RI was conducted by EBC from August 24, 2015 through September 9, 2015. 1.2 Site Location and Description The street address for the Site is 510 Driggs Avenue, Brooklyn, NY (Figure 1). The Site is located in the City of New York and Borough of Brooklyn. The Site has approximately 175 ft of street frontage on Driggs Avenue and 100 feet of street frontage on N. 8th Street (Figure 2). Currently the property is an asphalt paved vacant lot surrounded by an 8 foot high chain link fence. The Site was previously used as a warehouse, transformer manufacturer, a chair manufacturer and a garage with underground tanks. The elevation of the Site ranges from 18 to 21 feet above the National Geodetic Vertical Datum (NGVD). The area topography gradually slopes to the north. The depth to groundwater beneath the Site is approximately 12 feet below grade. Based on regional groundwater elevation maps, groundwater flows to the north. The area surrounding the property is highly urbanized and predominantly consists of multi-family residential buildings with mixed-use buildings (residential w/ first floor retail) along main corridors such as Driggs Avenue which borders the property to the east and Bedford Avenue located just one block to the northwest. The area is marked by late 19th and early 20th century rowhouses with commercial and industrial properties interspersed throughout the residential sections.


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The land use in the immediate vicinity of the Site includes commercial (manufacturing) and a mixed-use (1st floor retail) properties to the east, mixed use buildings to the north, mixed-use buildings and a parking lot to the south and single family residential homes to the west. There are no schools or daycare centers in the immediate area of the Site, however there are several schools located to the south and southeast within 1,200 ft of the Site. There are no other identified sensitive receptors (i.e. nursing homes, hospitals, etc.) located in the vicinity of the Site. 1.3 Redevelopment Plans The redevelopment project consists of the construction of a new 6 story mixed-use commercial- residential building which will cover the entire Site. Plans include a full height basement level requiring excavation of the entire Site to a depth of 25 ft below grade. With groundwater present at 12 feet below grade, extensive dewatering will be required during construction of the building's foundation. The project includes 51,000 sf of commercial / retail space and 18,000 sf of residential apartments. The basement level will be used for parking, meter rooms, residential storage space and bicycle racks. 1.4 Site History A review of Sanborn maps shows that in 1887 the Site was developed at this time with three single family residential homes. Between 1905 and 1916, the northern portion of the site was developed with a commercial storage building. By 1942, southern portions of the site were developed with a garage. Between 1942 and 1951, the garage was converted to an industrial building and occupied by a chair manufacturer. The chair manufacturer was replaced by a transformer manufacturer (Sterling Transformer) circa 1965 and later by food warehouse circa 1991. Both buildings were demolished in 2006. In addition to the history as documented above, EBC was provided with an 1885 map obtained by National Grid, which appears to indicate that a gas holder, typically associated with the storage of gas from manufactured gas plants (MGP) may have been present on the Site. 1.5 Summary of Previous Investigations Environmental investigations performed at the Site include the following:

Phase I Environmental Site Assessment Report - DPV (March 2014) Geophysical Survey - Hager-Richter Geoscience, Inc. (March 2014) Phase II Subsurface Investigation Data Summary - EBC (October 2014)

1.5.1 March 2014 – Phase I Environmental Site Assessment (DPV) DPV concluded that "Based on the results of the site inspection, records review and interviews, it


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was determined that there were several RECs identified with regard to the subject site. RECs are those conditions which could adversely affect the environmental integrity of the property." DPV identified the following RECs:

The 1942 Sanborn map depicts the presence of a gasoline tank at the south-central portion of the site. No information regarding the current status of this tank and/or soil quality in its vicinity was available for review. As such, there is a potential for spills or release from the tank to have impacted the subsurface.

The Sanborn maps indicated that portions of the subject property were historically occupied

by a garage, chair manufacturer and a transformer manufacturer. As such, there is a potential for historic site operations to have impacted soil, groundwater and/or soil vapor quality beneath the subject property. Further, the subject property was identified as a New York City Department of City Planning (NYCDCP) Environmental "E" declaration site due to its historic use and the presence of the UST.

Based upon its findings, DPV recommended the following:

A geophysical survey (e.g., magnetometer and/or ground penetrating radar surveys) should be conducted on the southern portion of the property to evaluate the presence of the suspected underground storage tank (UST), as well as the configurations of existing underground utilities in advance of a soil boring program. It is important to note that clearing of all vehicles or other obstructions in the vicinity of the suspected USTs would be necessary to facilitate the geophysical survey and any subsequent sampling.

If present, any historic USTs should be removed in accordance with New York State

Department of Environmental Conservation (NYSDEC) and New York City Fire Department (FDNY) regulations. Any identified geophysical anomalies should be further investigated through the excavation of test pits, with soil samples collected for laboratory analysis as warranted. It is important to note that excavation areas may be necessary to facilitate the geophysical survey and any subsequent sampling.

To evaluate potential impacts related to historic usage of the subject property and to satisfy

the NYCDCP and New York City Office of Environmental Remediation (NYCOER) requirements related to the site's listing as an "E"-designated property, a subsurface investigation should be performed. At a minimum, the investigation should include the installation of soil borings with the collection of representative soil, groundwater and/or soil vapor samples for laboratory analysis to document subsurface conditions and determine the nature and extent of contamination (if present).

1.5.2 March 2014 - Geophysical Survey (H-R Geoscience) Harer-Richter Geoscience, Inc. (H-R) performed a geophysical survey of the Site on March 7, 2014 to locate underground storage tanks and utilitity conduits that mey have been present on the Site. The geophysical survey was conducted using three complementary geophysical methods: time domain electromagnetic induction (EM61), ground penetrating radar (GPR), and precision utility location (PUL).


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H-R concluded the following:

No UST with: (1) electrical properties sufficiently contrasting with the surrounding soils to produce an EM anomaly or GPR reflections, or (2) a capacity of 500 gallons or more was detected within the effective depth of penetration of the GPR signal. Whether a UST occurs at a depth greater than the effective depth of penetration of the GPR signal (approximately 3-4 feet) or in areas inaccessible to the geophysical survey cannot be determined from the geophysical data.

Dry wells and associated piping were detected. Segments of possible utilities and small unidentified buried objects were detected. A small area of buried metal was detected.

1.5.3 October 2014 - Phase II Invesitgation Data Summary (EBC) The field work portion of the Phase II was performed on September 30, 2014 and included the installation of three soil borings and three groundwater samples. Shallow soil samples were analyzed for RCRA metals, TCLP lead and PCBs. Deep samples, from the water table interface, could only be obtained from two borings and were analyzed for VOCs by USEPA 8260 and SVOCs by USEPA 8270. Groundwater samples were analyzed for VOCs only. Laboratory services were provided by Phoenix Environmental Laboratories of Manchester, CT 06040, a New York State ELAP certified environmental laboratory (ELAP Certification No. 11301). The depth to groundwater at the site is approximately 12 feet below grade. Soil at the site is described as historic fill materials to a depth of approximately 15 feet below the surface followed by native brown fine sand with silt and some clay. Laboratory results identified petroleum VOCs including benzene above Restricted Residential Soil Cleanup Objectives (SCOs) and trimethylbenzene, ethylbenzene, toluene and xylene above unrestricted and groundwater protection SCOs. The concentration of total VOCs (when including naphthalene) were reported as high as 1,173,800 ug/kg. SVOCs including chysene, fluoranthene, fluorine, ideno(1,2,3-cd)pyrene, naphthalene, phrenanthene and pyrene were all reported above Restricted Residential SCOs. Total SVOCs were reported at 4,358,000 ug/kg at the B3 location. VOCs were reported in all three groundwater samples above water quality standards and included both petroleum and chlorinated solvent compounds. Total petroleum VOCs were reported to 20,850 ug/L with chlorinated VOCs to 1,027 ug/L.


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2.0 REMEDIAL INVESTIGATION 2.1 Field Investigation The field work portion of the RI was conducted by EBC from August 24 through September 9, 2015. The field investigation consisted of environmental sampling, field observations and measurements to determine:

Local geologic/hydro geological conditions; Definition of source areas; Potential migration of contaminants from the Site to surrounding areas; and, Overall characterization of site-related contamination in all media.

The field effort included the collection and analysis of soil, groundwater and soil vapor samples. Laboratory services for soil, groundwater and soil vapor analysis were provided by Phoenix Environmental Laboratories of Manchester, CT (NY Cert No. 11301). A sample matrix showing the number, type and analysis of samples collected during the Remedial Investigation is provided as Table 1. 2.2 Deviations from the Remedial Investigation Work Plan The following changes were made in performing the Remedial Investigation:

Boring 14B1 was advanced to 15 ft due to refusal Boring 14B3 was advanced to 18.5 ft due to refusal Boring 14B4 was advanced to 21 ft due to refusal Boring 14B5 was advanced to 19.5 ft due to refusal Boring 14B6 was advanced to 19 ft due to refusal Boring 14B7 was advanced to 19.5 ft due to refusal Two soil samples were retained from boring 14B1, due to refusal A groundwater sample was not obtained from MW2 due to the presence of non-aqueous

phase liquid (NAPL)

2.3 Soil Sampling 2.3.1 Soil Borings A total of eight soil borings (14B1-14B8) were advanced on August 25, 2015 to identify source areas and to obtain general soil quality information present at the Site (Figure 3). At each soil boring location soil samples were collected continuously in 5-foot intervals from grade to a depth of 15 to 25 feet below grade using a Geoprobe™ 6720DT, probe drilling machine. The Geoprobe™ system uses a direct push hydraulic percussion system to drive and retrieve core samplers. Soil samples were retrieved using a 1.25-inch diameter, 5-foot long dual-tube sampler with disposable acetate liners. Soil recovered from each soil boring was field screened by an


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environmental professional for the presence of VOCs with a photo-ionization detector (PID) and visually inspected for evidence of contamination. In accordance with the RI work plan three soil samples were retained for laboratory analysis from all borings with the exception of 14SB1 in which two samples were retained. Retained samples were submitted for laboratory analysis of one or more of the following analyses: volatile organic compounds (VOCs) by EPA Method 8260, semi-volatile organic compounds (SVOCs) by EPA Method 8270, TAL Metals, pesticides and PCBs by EPA Method 8081/8082. Soil boring locations are identified in Figure 3. Soil boring logs are provided in Appendix A. 2.4 Monitoring Well Installation Seven groundwater monitoring wells, MW1 through MW7, were installed at the Site on August 26, 2015. All of the wells were installed with a track mounted probe drilling machine. Wells MW1-MW3 and MW6 were installed to a depth of approximately 20 feet below grade with 10 feet of 1-inch diameter 0.010-inch slotted PVC well screen and 10 feet of PVC riser. Wells MW1 and MW5-MW7 were installed to a depth of 20 ft with 10 ft of well screen. Wells MW2 and MW3 were installed to depths of 19 ft and 17 ft, respectively with 10 ft of well screen. A No. 00 morie filter-pack sand filled the annulus surrounding the screen within two feet above the top of the screen. A one-foot hydrated bentonite seal was then placed on top of the filter sand and the remainder of the borehole was backfilled to grade. Following installation, each of the wells were surveyed to determine relative casing elevation to the nearest 0.01 ft and horizontal position to the nearest 0.1 ft. Monitoring well specifications, elevation and depth to water readings are provided in Table 2. Monitoring well locations are identified in Figure 4. Well completion reports detailing monitoring well construction are provided in Appendix B. Prior to sampling, a synoptic round of depth-to-groundwater (DTW) measurements was obtained from the wells on September 9, 2015 to determine the water table elevation and to calculate the volume of standing water in the well. A groundwater elevation map, from the September 2015 depth to water readings, is provided in Figure 5. 2.4.1 Groundwater Sampling Wells MW5-MW7 were sampled on September 8. Wells MW1, MW3 and MW4 were sampled on September 9, 2015. MW2 was not sampled due to the presence of NAPL in the well during the sampling event. The NAPL was highly viscous and could not be measured as it coated the interface probe and bottom loading bailer interfering with quantitative and qualitative measurements. Samples were collected from the monitoring wells using low-flow sampling techniques and were monitored continuously until parameters stabilized. A peristaltic pump and polyethylene sampling tube were used to purge and collect samples from each well location. Sample tubing and the silicone pump tubing were replaced between each sample location. Samples were collected directly into pre-cleaned laboratory supplied glassware, stored in a cooler with ice and submitted to Phoenix Environmental Laboratories of Manchester, CT, a New York State ELAP certified environmental laboratory (ELAP Certification No. 11301). Groundwater sampling logs are provided in Appendix C.


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All groundwater samples from the monitoring wells were analyzed for VOCs / SVOCs by EPA method 8260 / 8270, target analyte list (TAL) metals by EPA method 6010 and Pesticides/PCBs by method 8081/8082. 2.5 Soil Vapor Sampling Seven soil vapor samples were collected during the RI on September 8, 2015. Samples were collected from implants installed at a depth of 8 feet below grade. The soil vapor sampling locations are shown on Figure 6. All soil vapor samples were collected over a 2-hr sampling period. Soil vapor samples were collected in accordance with the procedures as described in the Guidance for Evaluating Soil Vapor Intrusion in the State of New York (NYSDOH 10/06). 2.5.1 Installation of Soil Vapor Implants Seven soil vapor implants were installed at the Site on September 8, 2015. The vapor implants (Geoprobe™ Model AT86 series), were constructed of a 6-inch length of double woven stainless steel wire and installed to a depth of 8 ft below existing slab grade at all locations. During installation, the barbed end of each implant was attached to ¼ inch polyethylene tubing which extended approximately 24 inches beyond that needed to reach the surface. The tubing was capped with a ¼ inch plastic end to prevent the infiltration of foreign particles into the tube. Coarse sand was placed around the vapor implant to a height of approximately 1 foot above the bottom of the implant. The remainder of the borehole was sealed with a bentonite slurry to the surface. The tubing and borehole were then sealed at the surface with hydrated granular bentonite and a 6” x 6” (approx.) plastic sheet. 2.5.2 Surface Seal Test Procedure In accordance with NYSDOH guidance, a tracer gas (helium) was used as a quality assurance/quality control device to verify the integrity of the sampling point seal prior to collecting the samples. This was accomplished by enriching the air space above the seal with a tracer gas (helium) while continuously monitoring air drawn from the implant with a helium detector (Ionscience Gas Check G). The tracer gas test procedure was employed at all soil vapor sampling locations. All seals tested tight with no infiltration of helium through the surface. 2.5.3 Soil Vapor Sample Collection Following verification that the surface seal was tight, one to three volumes (i.e., the volume of the sample probe and tube) were purged with a handheld vacuum pump prior to collecting the samples to ensure samples collected were representative. After purging, a 6-liter summa canister, fitted with a 2-hour flow regulator was attached to the surface tube of each of the sampling points and the valve opened to initiate sampling. Sample identification, date, start time, start vacuum, end time and end vacuum were recorded on tags attached to each canister and on a sample log sheet (Appendix D). When the remaining vacuum in the canisters was between 0 and 7 inches Hg, (after approximately 2 hrs of run-time) the valve was closed and the canisters were detached from the sampling tube. Sample canisters were picked up the following day by a Phoenix laboratory courier and delivered to the laboratory for analysis of VOCs by USEPA Method TO-15.


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2.6 Laboratory Analysis Data tables summarizing the laboratory results are provided in Tables 3 through 12 and copies of the laboratory reports (with chains-of-custody) are included in digital format in Appendix E. Soil sample results were compared to both Unrestricted Use and Restricted Residential Soil Cleanup Objectives (SCOs) as promulgated in 6 NYCRR Subpart 375-6. Groundwater results were compared to NYSDEC Division of Water, Technical & Operational Guidance Series 1.1.1, Ambient Water Quality Standards and Guidance Values (AWQS), June 1998. Soil vapor analytical results were compared to Outdoor Background Levels for Selected Compounds and sub-slab and indoor air guidance levels as presented in the NYSDOH Guidance for Evaluating Soil Vapor Intrusion in the State of New York, October 2006. Table 13 contains a list of parameters detected above Track 1 unrestricted soil cleanup objectives and the range in detections. Table 14 contains a list of parameters detected above ambient groundwater standards and the range in detections. 2.6.1 Analytical Results – Soil Samples A total of twenty-three soil samples were collected from 8 soil borings for laboratory analysis of VOCs (EPA Method 8260), SVOCs (EPA Method 8270), TAL metals and pesticides/PCBs (EPA Method 8081/8082). Soil sampling results are summarized in Tables 3 through 6. All soil results above Unrestricted Use SCOs are presented in Table 13 and posted on Figure 7. A cross-section showing PID readings and other observations is provided as Figure 8. Soil samples collected from the borings had elevated levels of VOCs, SVOCs, pesticides and heavy metals that exceeded either unrestricted use or restricted residential use SCOs as follows: VOCs in Soil Above Unrestricted Use SCOs:

14SB3 (10-15ft) – 1,2,4-trimethyl benzene (14,000 µg/kg), 1,3,5-trimethyl benzene (9,600 µg/kg), benzene (4,100 ug/kg), cis-1,2-dichloroethene (870 ug/kg), ethylbenzene (7,000 ug/kg), m&p Xylenes (17,000 µg/kg), o Xylene (9,200 µg/kg), toluene (8,600 ug/kg), trichloroethene (3,300 ug/kg), vinyl chloride (290 ug/kg). 14SB3 (15-18ft) – benzene (2,800 ug/kg), cis-1,2-dichloroethene (7,600 ug/kg), m&p Xylenes (820 µg/kg), trichloroethene (3,700 ug/kg). 14SB4 (10-15ft) – cis-1,2-dichloroethene (570 ug/kg). 14SB4 (20-21ft) – 1,2,4-trimethyl benzene (27,000 µg/kg), 1,3,5-trimethyl benzene (16,000 µg/kg), cis-1,2-dichloroethene (730 ug/kg), ethylbenzene (21,000 ug/kg), m&p Xylenes (62,000 µg/kg), o Xylene (21,000 µg/kg), toluene (22,000 ug/kg) 14SB5 (15-19.5ft) – benzene (160 ug/kg) 14SB6 (15-17ft) – benzene (890 ug/kg), cis-1,2-dichloroethene (8,700 ug/kg), m&p xylenes (270 µg/kg), trichloroethene (14,000 ug/kg)


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VOCs in Soil Above Restricted Residential Use SCOs:

14B3 (10-15ft) – napthalene (300,000 µg/kg) 14B3 (10-15ft) – vinyl chloride (2,600 ug/kg) 14B4 (20-21ft) – napthalene (620,000 µg/kg) 14B6 (15-17ft) – vinyl chloride (1,100 ug/kg) SVOCs in Soil Above Unrestricted Use SCOs:

14B1 (0-5ft) - Benzo(k)fluoranthene (3,400 µg/kg), Chrysene (3,300 µg/kg) 14B3 (0-5ft) – Benzo(k)fluoranthene (850 ug/kg) 14B3 (10-15ft) – dibenzofuran (12,000 ug/kg), napthalene (43,000 µg/kg) 14B4 (10-15ft) –Benzo(k)fluoranthene (2,900 µg/kg), chrysene (1,800 µg/kg) 14B4 (20-21ft) – dibenzofuran (43,000 ug/kg), fluorene (66,000 µg/kg) 14B5 (0-5ft) –Benzo(k)fluoranthene (870 µg/kg) 14B5 (10-15ft) –Benzo(k)fluoranthene (2,700 µg/kg), chrysene (2,600 µg/kg) 14B7 (0-5ft) –Benzo(k)fluoranthene (960 µg/kg), chrysene (1,400 µg/kg) 14B8 (0-5ft) –Benzo(k)fluoranthene (980 µg/kg), chrysene (1,100 µg/kg) SVOCs in Soil Above Restricted Residential SCOs:

14B1 (0-5ft) - Benzo(a)anthracene (3,500 µg/kg), Benzo(a)pyrene (3,200 µg/kg), Benzo(b)fluoranthene (4,500 µg/kg), Dibenzo(a,h)anthracene (1,400 µg/kg), Indeno(1,2,3-cd)pyrene (3,900 µg/kg) 14B1 (10-15ft) - Benzo(a)anthracene (16,000 µg/kg), Benzo(a)pyrene (13,000 µg/kg), Benzo(b)fluoranthene (11,000 µg/kg), Dibenzo(a,h)anthracene (1,300 µg/kg), Indeno(1,2,3-cd)pyrene (7,200 µg/kg), chrysene (16,000 µg/kg) 14B2 (0-5ft) - Indeno(1,2,3-cd)pyrene (570 µg/kg) 14B3 (0-5ft) – Indeno(1,2,3-cd)pyrene (600 µg/kg) 14B3 (10-15ft) – Benzo(a)anthracene (14,000 µg/kg), Benzo(a)pyrene (13,000 µg/kg), Benzo(b)fluoranthene (9,900 µg/kg)


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14B4 (10-15ft) – Benzo(a)anthracene (1,800 µg/kg), Benzo(a)pyrene (3,600 µg/kg), Benzo(b)fluoranthene (2,300 µg/kg), Benzo(k)fluoranthene (10,000 µg/kg), chrysene (13,000 µg/kg), Dibenzo(a,h)anthracene (500 µg/kg), Indeno(1,2,3-cd)pyrene (3,400 µg/kg) 14B4 (20-21ft) – Benzo(a)anthracene (41,000 µg/kg), Benzo(a)pyrene (28,000 µg/kg), Benzo(b)fluoranthene (21,000 µg/kg), Benzo(k)fluoranthene (26,000 µg/kg), chrysene (38,000 µg/kg), Dibenzo(a,h)anthracene (3,800 µg/kg), Indeno(1,2,3-cd)pyrene (11,000 µg/kg), napthalene (190,000 µg/kg), phenanthrene (140,000 µg/kg) 14B4 (0-5ft) – Indeno(1,2,3-cd)pyrene (710 µg/kg) 14B5 (10-15ft) – Benzo(a)anthracene (2,700 µg/kg), Benzo(a)pyrene (3,000 µg/kg), Benzo(b)fluoranthene (2,200 µg/kg), dibenzo(a,h)anthracene (440 µg/kg), Indeno(1,2,3-cd)pyrene (1,600 µg/kg) 14B5 (15-19.5ft) – Benzo(a)anthracene (8,000 µg/kg), Benzo(a)pyrene (14,000 µg/kg), Benzo(b)fluoranthene (9,700 µg/kg), Benzo(k)fluoranthene (6,500 µg/kg), chrysene (8,200 µg/kg), Dibenzo(a,h)anthracene (4,200 µg/kg), Indeno(1,2,3-cd)pyrene (7,400 µg/kg) 14B6 (15-17ft) – Benzo(a)anthracene (6,300 µg/kg), Benzo(a)pyrene (2,100 µg/kg), Benzo(b)fluoranthene (8,800 µg/kg), Benzo(k)fluoranthene (4,600 µg/kg), chrysene (6,100 µg/kg), Dibenzo(a,h)anthracene (1,900 µg/kg), Indeno(1,2,3-cd)pyrene (6,200 µg/kg) 14B7 (0-5ft) – Benzo(a)anthracene (1,200 µg/kg), Benzo(a)pyrene (1,100 µg/kg), Indeno(1,2,3-cd)pyrene (720 µg/kg) 14B8 (0-5ft) – Benzo(a)anthracene (1,100 µg/kg), Indeno(1,2,3-cd)pyrene (680 µg/kg) Metals in Soil Above Unrestricted Use SCOs:

14B2 (0-5ft) – Chromium (31.3 mg/kg), Lead (102 mg/kg), Mercury (0.58 mg/kg), Nickel (36.3 mg/kg) 14B2 (20-25ft) – Mercury (0.19 mg/kg) 14B3 (15-18ft) – Lead (121 mg/kg) 14B4 (0-5ft) – Mercury (0.41 mg/kg) 14B4 (20-21ft) – Lead (79.2 mg/kg) 14B5 (0-5ft) – Mercury (0.23 mg/kg) 14B6 (15-17ft) – Lead (107 mg/kg) There were no metals reported above Restricted Residential Use SCOs.


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Pesticides Above Unrestricted SCOs:

14B1 (0-5ft) – Chlordane (510 µg//kg) 14B2 (20-25ft) – 4,4’-DDT (7.1 µg//kg), a-Chlordane (110 µg//kg), Chlordane (970 µg//kg), Deildrin (9.4 µg//kg) 14B3 (0-5ft) – a-Chlordane (130 µg//kg) 14B3 (15-18ft) – Chlordane (1,300 µg//kg) 14B4 (0-5ft) – 4,4’-DDD (4.3 µg//kg), 14B4 (20-21ft) – 4,4’-DDE (4 µg//kg), a-Chlordane (170 µg//kg), Chlordane (120 µg//kg) 14B5 (0-5ft) – Chlordane (650 µg//kg) 14B7 (0-5ft) – Chlordane (320 µg//kg) 14B7 (15-20ft) – Deildrin (13 µg//kg) 14B8 (0-5ft) – Chlordane (220 µg//kg) There were no pesticides reported above Restricted Residential Use SCOs and no PCBs detected above either Unrestricted Use or Restricted Residential Use SCOs. 2.6.2 Analytical Results – Groundwater Samples A total of six groundwater samples were collected from the seven groundwater monitoring wells for laboratory analysis of VOCs (EPA Method 8260), SVOCs (EPA Method 8270), TAL metals and pesticides/PCBs (EPA Method 8081/8082). The results of groundwater samples collected during the RI are summarized in Tables 7 through 11. Several VOC detections were in excess of the NYSDEC Division of Water, Technical & Operational Guidance Series 1.1.1, Ambient Water Quality Standards and Guidance Values (AWQS), June 1998. VOCs in Groundwater Above NYSDEC AWQS:

MW1 - benzene (18 µg/L), cis-1,2-dichloroethene (70 µg/L), trans-1,2-dichloroethene (6.3 µg/L), trichloroethene (6.3 µg/L), vinyl chloride (36 µg/L)

MW3 - 1,1-dichloroethene (5.8 µg/L), benzene (23 µg/L), cis-1,2-dichloroethene (1,200 µg/L), trans-1,2-dichloroethene (12 µg/L), trichloroethene (12 µg/L), vinyl chloride (470 µg/L)

MW4 - cis-1,2-dichloroethene (51 µg/L) MW5 - cis-1,2-dichloroethene (8.4 µg/L)


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MW6 - cis-1,2-dichloroethene (16 µg/L) MW7 - cis-1,2-dichloroethene (14 µg/L) SVOCs in Groundwater Above NYSDEC AWQS:

SVOC detections above groundwater standards were limited to benzo(a)pyrene which was reported above the standard of non-detect in two locations. Several PAH parameters were reported above the 2 part per trillion guidance values for these compounds in MW3, MW5 and MW7. Total Metals in Groundwater Above NYSDEC AWQS:

Metals including sodium, magnesium and manganese were reported above standards in the majority of the wells. These metals are commonly reported in groundwater in Brooklyn and are related to historic over pumping of the aquifer and salt water intrusion. Groundwater parameters reported above groundwater standards are presented in Table 14 and posted on Figure 9. 2.6.3 Analytical Results – Soil Vapor Samples In order to determine the vapor quality in the soil beneath the Site, soil vapor samples were collected from seven soil vapor implants (SG1 - SG7). Analytical results were compared to the Summary of Background Levels for Selected Compounds (NYSDOH Database, Outdoor values, 2003). With the exception of benzene in one sample (SG5), Total petroleum-related VOCs (BTEX) were generally low in soil vapor samples and ranged from 39.47 (SG1) to 424.08 µg/m3 (SG7) at all other soil vapor locations. The total BTEX concentration in SG3 including benzene was 1,301.96 µg/m3. CVOCs were reported in all of the soil vapor samples with tetrachloroethylene (PCE) reported in all 7 samples at concentrations ranging from 4.74 µg/m3 (SG6) to 113 µg/m3 (SG2), Trichloroethylene (TCE) reported in all 7 samples at concentrations ranging from 763 µg/m3 (SG6) to 16,900 µg/m3 (SG2), cis-1,2-dichloroethene in all 7 samples at concentrations ranging from 5.27 µg/m3 (SG6) to 44,400 µg/m3 (SG5), trans-1,2-dichloroethene in 5 samples ranging from 3.48 µg/m3 (SG3) to 1,380 µg/m3 (SG5), and vinyl chloride in 4 samples ranging from 0.82 µg/m3 (SG1) to 116,000 µg/m3 (SG5). Soil vapor results are summarized on Table 12 and posted on Figure 10. 2.6.4 Data Usability Summary Report Data validation services were provided by H&S Environmental of Westborough, Massachusetts. H&S reported that, in general, the data are valid as reported and may be used for decision making purposes. Selected data points were qualified due to nonconformance of certain Quality Control criteria. The Data Usability Summary Reports prepared by H&S are provided in Appendix F.


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3.0 HYDROGEOLOGIC ASSESSMENT AND PHYSICAL SETTING 3.1 Site Topography The elevation of the Site is ranges from 18 to 21 feet above the National Geodetic Vertical Datum (NGVD). The area topography gradually slopes to the north. 3.2 Surrounding Land Use The area surrounding the property is highly urbanized and predominantly consists of multi-family residential buildings with mixed-use buildings (residential w/ first floor retail) along main corridors such as Driggs Avenue which borders the property to the east and Bedford Avenue located just one block to the northwest. The area is marked by late 19th and early 20th century rowhouses with commercial and industrial properties interspersed throughout the residential sections. The area to the west of the Site was historically characterized by heavy industry and manufacturing. Following a steady decline of manufacturing in the area from the late 1960's through the 1980's, many of the industrial properties were vacated leaving the buildings to be vandalized and become derelict. There are no identified sensitive receptors (i.e. nursing homes, day care centers, etc.) in the immediate area of the Site. 3.3 Regional Geology / Hydrogeology Long Island's present configuration is primarily the result of glaciation which during the Pleistocene Era, predominately that of the last ice age, the Wisconsin, which ended about ten thousand years ago. Two advances of the Wisconsin ice sheet during the Upper Pleistocene of the Quaternary Period caused the island to be blanketed with till, ice contact stratified drift, outwash deposits and deposits composed of clay, silt, sand, gravel and boulders. The terminal moraines and the north shore are composed primarily of stratified drift with some till. The area between the moraines and south of them are mostly the outwash deposits. Central and South Long Island are of the glaciofluvial origin. The Pleistocene deposits lie atop the gently-dipping Cretaceous rocks. The bedrock was eroded to a peneplain before the overlying Cretaceous sediments were deposited; its surface shows signs of later erosion by Pleistocene glaciation in the north. Bedrock crops out in northwestern Queens County near the East River and slopes southward at about eighty (80) feet per mile. Consequently, the overlying formations form a southward-dipping wedge that attains a maximum thickness of one-thousand fifty (1,050) feet in the southeast corner of Queens County. The maximum thickness of unconsolidated deposits in Kings County is about eight-hundred (800) feet in southeast Kings. Overlying bedrock is the Raritan Formation of Late Cretaceous age, consisting of the Lloyd Sand Member and an upper, unnamed clay member. Overlying the Raritan Formation is the Magothy Formation and Matawan Group, undifferentiated, also of Late Cretaceous age, the Jameco Gravel of Pleistocene age, the Gardiners Clay of Pleistocene age, upper Pleistocene deposits of Wisconsin age, and a generally thin soil mantle of Holocene age. Holocene beach deposits make up most of the Rockaway Peninsula and Coney Island in the south, and Holocene salt-marsh deposits underlie and fringe the south-shore bay areas. Artificial filling has been done in low and swampy shoreline areas.


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Because Holocene deposits occur in relative small areas of Kings and Queens and are not significant water bearers, they are not included in the geologic descriptions that follow. The four distinct formations on Long Island: The Upper Glacial, the Jameco, the Magothy and the Lloyd aquifers. They all occur in the unconsolidated materials overlying the bedrock. 3.4 Site Geology / Hydrogeology Soil at the site is described as historic fill materials to a depth of approximately 15 feet below the surface followed by native brown fine sand with silt and some clay (see Figure 8). Groundwater at the Site is present under water table conditions at a depth of 11.85 to 13.89 feet below grade (Table 2). Based upon on-site measurements, groundwater flow is to the northeast (Figure 5). Considering the poor quality of groundwater in the area, including high levels of sodium and magnesium associated with saltwater intrusion and impacts from petroleum and industrial solvents related to the former commercial / industrial use of the area, there is no anticipated future groundwater use.


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4.0 NATURE AND EXTENT OF CONTAMINATION 4.1 Identification of Source Areas The source area identified during the RI includes an area in mid-central portion of the Site where the former MGP holder is suspected of being located (vicinity of 14B3), extending southeast to 14B4 and 14B6. The source area includes petroleum VOCs, chlorinated VOCs (CVOCs) and naphthalene. The highest petroleum VOCs (181,120 ug/kg) were located at 14B4 in the southern area of the site near a former UST, at a depth of 21 ft below grade. CVOCs were highest at 14B6 (23,800 ug/kg ) in the southeastern area of the site at a depth of 17 ft. Napthalene was highest at the 14B4 location at a concentration of 620,000 ug/kg. SVOCs were also associated with the 14B4 location at 21 feet. Although SVOCs were reported in other borings, the depth at which they were present and the higher concentrations indicate that they are related to petroleum at this location and not fill materials. Historic fill material has been identified across the Site to depths as great as 15 feet below grade. The historic fill material contains semi-volatile organic compounds and metals including chromium, lead, mercury and nickel above unrestricted use SCOs. 4.2 Groundwater Impacts Groundwater impacts from petroleum were limited to benzene in three wells (MW1, MW3, MW6) at concentrations ranging from 2.1 ug/L to 23 ug/L. The highest concentrations were reported in MW1 and MW3 located in the southeast area of the Site. CVOCs were reported in all of the groundwater sampling locations with the highest concentrations reported in MW1 (119 ug/L) and MW3 (1,700 ug/L) SVOC detections above groundwater standards were limited to those polynuclear aromatic hydrocarbons (PAHs) with a 2 per trillion standard. Exceedances of the part per trillion standards for PAHs were reported in wells MW3, MW5 and MW7. SVOCs reported in the parts per trillion range are a function of the laboratories ability to achieve extremely low detection limits and general background conditions. Several dissolved metals were detected above standards including sodium, iron and manganese were detected above standards throughout the Site. The metals detected in groundwater are consistent with general groundwater quality throughout the area and are generally considered to be associated with over pumping of the aquifer in the past and saltwater intrusion. 4.3 Soil-Vapor Impacts With the exception of benzene in one sample (SG5), Total petroleum-related VOCs were generally low in soil vapor samples across the Site. There did not appear to be any correlation in concentration or distribution of petroleum VOCs in soil vapor with the source area.


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CVOCs were reported in all of the soil vapor samples with concentrations ranging from 767.74 µg/m3 in SG6 to 167,479 µg/m3 in SG5. Of these PCE, which was detected in all samples, ranged from 4.74 µg/m3 in SG6 to 113 µg/m3 in SG2. TCE, detected in all samples, ranged from 763 µg/m3 in SG6 to 16,900 µg/m3 in SG2. Cis-DCE, detected in all samples, ranged from 5.43 µg/m3 in SG1 to 44,000 µg/m3 in SG5. Vinyl chloride, detected in 4 of 7 samples ranged from 0.82 µg/m3 in SG1 to 116,000 µg/m3 in SG5. There did not appear to be a direct correlation of CVOCs in soil and that in soil vapor though concentrations in soil gas were generally highest in the eastern portion of the Site while CVOCs in soil were highest in the south-central and southeastern areas of the Site. 4.4 Site Conceptual Model VOC contamination at the Site consists of petroleum related contaminants in soil to a minimum depth of 20 feet in the central and south central area of the Site. This same area also had the highest concentrations of naphthalene. Although a UST was known to be historically located in the south central area of the Site in the vicinity of highest petroleum VOCs and napthalene, the presence of the these same compounds in the central area of the Site combined with the high concentrations of naphthalene suggest it may be related to condensate associated with a MGP gas holder which may have been present on the Site. However if a gas holder were present and removed, fill materials should be considerable deeper than the 10 to 15 feet of fill documented at the Site. It is therefore also possible that the release occurred from former underground petroleum tanks and then migrated north with groundwater flow. This scenario is plausible as both the petroleum VOCs and naphthalene were higher in 14B4 at the southern end of the Site than they were in 14B3 to the north. In either case there appears to be very little transfer of petroleum VOCs or naphthalene to the dissolved phase as groundwater was only impacted with relatively low levels of benzene. NAPL did appear to be present, however, in MW2. CVOCs consisting mainly of TCE and its degradents were present in soil in the central and southeastern areas of the Site. The property was known to have been occupied by a manufacturer of small transformers used in radios and other electronic deices so it is reasonable to conclude that TCE was historically stored and used at the Site. However, the distribution of CVOCs in soil is similar to that of the petroleum VOCs / naphthalene though the highest concentrations were reported in the 14B6 (southeast area) and 14B3 (central area) and not in 14B4 (south property line). The TCE is undergoing reductive dechlorinization as evidenced by the presence of cis-DCE and vinyl chloride. The TCE have migrated from the source area through the soil column to the water table and has transferred to the dissolved phase. Although cis-DCE was found in low but elevated concentrations throughout the Site, the CVOCs in groundwater are generally limited to the southeast corner of the property and do not appear to be migrating with groundwater flow. The CVOCs in soil are also transferring to the vapor phase and appear to be migrating north along the eastern half of the property, though the potential exists to migrate in other directions as well.


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5.0 QUALITATIVE EXPOSURE ASSESSMENT The objective of the qualitative exposure assessment under the Brownfields Cleanup Program (BCP) is to identify potential receptors to the contaminants of concern (COC) that are present at, or migrating from, the Site. The identification of exposure pathways describes the route that the COC takes to travel from the source to the receptor. An identified pathway indicates that the potential for exposure exists; it does not imply that exposures actually occur. An exposure pathway has five elements; a contaminant source, release and transport mechanisms, point of exposure, route of exposure and a receptor population. The potential exposure pathways identified below, represent both current and future exposure scenarios. 5.1 Contaminant Source Source areas of the Site include petroleum VOCs /SVOCs and naphthalene in the central and south central area of the Site and CVOCs in the central and southeastern area of the Site. Elevated levels of metals and PAHs are also present in fill materials throughout the Site. 5.2 Contaminant Release and Transport Mechanism Petroleum / naphthalene contamination is present in subsurface soil in the central and south central areas of the Site. The contamination extends vertically to the groundwater interface. There appears to be limited transfer of petroleum VOC / naphthalene contaminants in soil to the groundwater despite the fact that impacted soil is in contact with the groundwater. There does not appear to be any significant transfer of petroleum VOCs / naphthalene to the vapor phase or concern for off-site vapor migration. CVOCs present in soil in the central and southeastern areas of the site have also migrated to the water table resulting in some limited transfer to the dissolved phase. There appears to be minimal transport of CVOCs in groundwater however. CVOCs are transferring from impacted soil to the vapor phase in high concentrations and are migrating along north in the eastern half of the property though the potential exists to migrate in other directions as well. 5.3 Point of Exposure, Route of Exposure and Potentially Exposed Populations Potential On-Site Exposures: Remediation workers and construction workers engaged in the excavation of impacted and non-impacted soil at the site may be exposed to petroleum VOCs / SVOCs, CVOCs and heavy metals through several routes including inhalation, ingestion and dermal contact. A site specific Health and Safety Plan has been developed to identify and minimize the potential hazards to on-site workers. Site trespassers could also be exposed to impacted soil during excavation, however security measures including an 8 ft high construction fence and 24 hr security will minimize potential exposure through this route.


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Potential Off-Site Exposures: Off-Site residents could also be exposed to dust or vapors during the excavation of impacted soil. A site specific Community Air Monitoring Plan has been developed to identify and minimize the potential for off-site exposure to residents through continuous air monitoring during excavation activity. CVOCs in soil vapor may also be migrating off-site in multiple directions; particularly near there east and northeast property lines. The adjacent multi-use building to the north includes commercial retail and garage space on the first floor and residential apartments on floors 2-4. The building also has a basement level which is used for utilities, storage and a tenant laundry room. The entire area is serviced by the New York City Water System which distributes water from the Croton Reservoir system. Since there are no public or private potable supply wells in the area, exposure from contact with tap water is not a concern. Potential Off-Site Environmental Impacts: Since petroleum VOCs and CVOCs in groundwater may be migrating from and beneath the Site at low concentrations in an easterly direction, the groundwater to surface water discharge pathway was evaluated. The nearest body of water is the East River located ½ mile to the west. Therefore, based on the concentrations of contaminants currently in groundwater beneath the Site, the groundwater flow direction (northeast) and the disctance and location to the East River (1/2 mile west) there are no expected impacts to surface water environments from contaminants migrating from the Site.


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6.0 CONCLUSIONS AND RECOMENDATIONS

Subsurface soils at the Site consist of historic fill materials from surface to a depth of approximately 15 feet below grade. Native silty sand w/some clay reported is present immediately below the fill layer. Groundwater occurs beneath the Site at a depth Groundwater at the Site is present under water table conditions at a depth of 11.85 to 13.89 feet below grade and flows to the northeast. The results of sampling performed during this RI, identified petroleum related VOCs (high conc. of 181,120 ug/kg) and naphthalene (high conc. of 620,000 ug/kg) in soil to a minimum depth of 20 feet in the central and south central area of the Site. The source may be related to historic USTs or condensate associated with an MGP gas holder which may have been present on the Site. SVOCs related to petroleum were also present in soil in the southern portion of the site in an area where a historic UST was located. Historic fill material has been identified across the Site to depths as great as 15 feet below grade. The historic fill material contains SVOCs and metals including chromium, lead, mercury and nickel above unrestricted use SCOs. Groundwater impacts from petroleum were limited to benzene in three wells at relatively low concentrations. The highest concentrations (18-23 ug/L) were reported in wells located in the southeast area of the Site. CVOCs were reported in all of the groundwater sampling locations with the highest concentrations (1,700 ug/L) also reported in the southeastern corner of the Site. Soil vapor sampling identified generally low levels of petroleum related volatile organic compounds (BTEX) and there did not appear to be any correlation in concentration or distribution of petroleum VOCs in soil vapor with the source area. CVOCs were reported in all of the soil vapor samples with concentrations to 167,479 µg/m3. There did not appear to be a direct correlation of CVOCs in soil and that in soil vapor though concentrations in soil gas were generally highest in the eastern portion of the Site while CVOCs in soil were highest in the south-central and southeastern areas of the Site. The qualitative exposure assessment identified potential completed routes of exposure to construction workers and remediation workers through inhalation, ingestion and dermal contact of petroleum VOCs, SVOCs, CVOCs, pesticides and heavy metals during excavation activities. The Health and Safety Plan prepared for the site identifies such exposures and provides instructions for on-site workers to minimize potential exposure. Off-Site residents could also be exposed to dust or vapors during the excavation of impacted soil. A site specific Community Air Monitoring Plan has been developed to identify and minimize the potential for off-site exposure to residents through continuous air monitoring during excavation activity. CVOCs in soil vapor may also be migrating off-site in multiple directions; especially near the east and northeast property lines. The adjacent multi-use building to the north includes commercial retail


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and garage space on the first floor and residential apartments on floors 2-4. The building also has a basement level which is used for utilities, storage and a tenant laundry room. Potential environmental impacts through the groundwater to surface water discharge were considered unlikely based on the concentrations of VOCs in groundwater, the groundwater flow direction (northeast) and the distance (1.2 mile) and location (west) of the nearest surface water receptor. Recommendations include excavation and disposal of petroleum and CVOC contaminated soil within the source areas and proper handling and disposal of all soils excavated for structural elements of the new building. Since the highest levels of petroleum impacts in soil were reported in the 18 to 21 ft interval, the vertical extent has not been established at several locations in the southern half of the Site. This information will be obtained during waste characterization sampling for soil disposal, and prior to beginning excavation at the Site. It is recommended that vapor impacts to the new building be reevaluated following the removal of impacted soil. This work would be performed under an approved Remedial Action Work Plan which includes a Soil Management Plan, a Construction Health and Safety Plan and a Community Air Monitoring Plan.


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7.0 REFERENCES 6 NYCRR Part 375 Environmental Remediation Programs Subparts 375-1, 375-3 and 375-6 DPV, March 2014, Phase I Environmental Site Assessment H-R Geoscience, March 2014, Geophysical Survey Environmental Business Consultants, September 2014, Phase II Investigation - Data Summary Environmental Business Consultants, July 2015, Remedial Investigation Work Plan NYSDEC, Division of Environmental Remediation, May 2004, Draft Brownfield Program Cleanup Guide. NYSDEC, Division of Environmental Remediation, December 2002, DER-10, Technical Guidance for Site Investigation and Remediation. NYSDEC, Division of Environmental Remediation, December 14, 2006, 6 NYCRR Part 375, Environmental Remediation Programs, subparts 375-1 to 375-4 & 375-6. NYSDEC, Division of Water, June 1998, Addendum April 2000, Technical and Administrative Guidance Series 1:1:1, Ambient Water Quality Standards and Guidance Values and Groundwater Effluent Limitations. NYSDOH, Center for Environmental Health, October 2006, Final Guidance for Evaluating Soil Vapor Intrusion in the State of New York.

TABLES

TABLE 1Former Sterling Transformer

510 Driggs Avenue, Brooklyn, New YorkRemedial Investigation Sampling Summary

Matrix Location Number of

SamplesRationale for Sampling Laboratory Analysis

Total (Soils) 23

Subsurface soil (0 to 5 feet)

8 soil borings throughout the Site. 8To evaluate the extent of soil impact and obtain information on soil quality at the Site.

VOCs EPA Method 8260B, SVOCs EPA Method 8270, Pesticides / PCBs EPA Method 8081/8082, TAL Metals


8 soil borings throughout the Site. 8To evaluate the extent of soil impact and obtain information on soil quality at the Site.

VOCs EPA Method 8260B, SVOCs EPA Method 8270


1 soil boring throughout the Site. 7To evaluate the extent of soil impact and obtain information on soil quality at the Site.

VOCs EPA Method 8260B, SVOCs EPA Method 8270, Pesticides / PCBs EPA Method 8081/8082, TAL Metals

Total (Groundwater) 6

Groundwater (below water table)

From 6 monitoring wells across the Site. 6To assess groundwater quality at the Site.

VOCs EPA Method 8260B, SVOCs EPA Method 8270, Pesticide / PCBs EPA Method 8081/8082, Dissolved Metals

Total (Soil Gas) 7

Soil Gas (8 ft below grade)

7 soil gas implant locations installed 8 ft beneath the first floor level across the Site.

7 To evaluate soil gas across the Site. VOCs EPA Method TO15

MS/MSDMatrix spike and Matrix spike duplicates at the rate 5%

3To meet requirements of QA / QC program

1 soil 2 GW for VOCs EPA Method 8260B, SVOCs EPA Method 8270, pesticide / PCBs EPA Method 8081/8082, TAL metals..

Trip BlanksOne laboratory prepared trip blank to accompany samples each time they are delivered to the laboratory.

4To meet requirements of QA / QC program

VOCs EPA Method 8260B

Total (QA / QC Samples) 7


510 Driggs Avenue, Brooklyn, New YorkMonitoring Well Specifications and Elevation

DTW GW ELV9/8/2015 11/17/2015

14MW1 1 20 10 to 20 2.360 97.64 13.89 - - 83.7514MW2 1 19 9 to 19 3.550 96.45 12.72 - - 83.7314MW3 1 17 7 to 17 4.120 95.88 12.15 - - 83.7314MW4 1 20 10 to 20 5.660 94.34 10.97 - - 83.3714MW5 1 20 10 to 20 5.180 94.82 11.75 - - 83.0714MW6 1 20 10 to 20 5.910 94.09 10.85 - - 83.2414MW7 1 20 10 to 20 4.590 95.41 12.05 - - 83.36

DTP PTWell No. Well

Diameter Total Well Depth (ft)

Screened Interval (ft)

Survey Reading

Casing Elevation


510 Driggs Avenue, Brooklyn, New YorkSoil Analytical Results

Volatile Organic Compounds

Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL

1,1,1,2-Tetrachlorothane < 20 20 < 22 22 < 16 16 < 22 22 < 4.4 4.4 < 23 23 < 1200 1,200 < 700 700 < 24 24 < 32 32 < 24000 24,000

1,1,1-Trichloroethane 680 100,000 < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

1,1,2,2-Tetrachloroethane < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

1,1,2-Trichloroethane < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

1,1-Dichloroethane 270 26,000 < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 250 250 < 250 250 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

1,1-Dichloroethene 330 100,000 < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 0.5 4.4 < 5.8 5.8 < 300 300 < 250 250 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

1,1-Dichloropropene < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

1,2,3-Trichlorobenzene < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 270 270 < 7.9 7.9 < 6000 6,000

1,2,3-Trichloropropane < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 270 270 < 7.9 7.9 < 6000 6,000

1,2,4-Trichlorobenzene < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 270 270 < 7.9 7.9 < 6000 6,000

1,2,4-Trimethylbenzene 3,600 52,000 < 4.9 4.9 < 5.6 5.6 0.43 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 14,000 3,000 240 700 < 270 270 < 7.9 7.9 27,000 6,000

1,2-Dibromo-3-chloropropane < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 270 270 < 7.9 7.9 < 6000 6,000

1,2-Dibromomethane < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

1,2-Dichlorobenzene 1,100 100,000 < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 270 270 < 7.9 7.9 < 6000 6,000

1,2-Dichloroethane 20 3,100 < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

1,2-Dichloropropane < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

1,3,5-Trimethylbenzene 8,400 52,000 < 4.9 4.9 < 5.6 5.6 1.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 9,600 300 89 700 < 270 270 < 7.9 7.9 16,000 6,000




1,4-dioxane < 99 99 < 100 100 < 81 81 < 100 100 < 87 87 < 100 100 < 6000 6,000 < 14000 14,000 < 100 100 < 100 100 < 120000 ######


2-Chlorotoluene < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 270 270 < 7.9 7.9 < 6000 6,000

2-Hexanone (Methyl Butyl Ketone) < 25 25 < 28 28 < 20 20 < 28 28 < 22 22 < 29 29 < 1500 1,500 < 3500 3,500 < 30 30 < 40 40 < 30000 30,000

2-Isopropyltoluene < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 270 270 < 7.9 7.9 < 6000 6,000

4-Chlorotoluene < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 270 270 < 7.9 7.9 < 6000 6,000

4-Methyl-2-Pentanone < 25 25 < 28 28 < 20 20 < 28 28 < 22 22 < 29 29 < 1500 1,500 < 3500 3,500 < 30 30 < 40 40 < 30000 30,000

Acetone 50 100,000 < 49 49 21 50 6.9 41 < 50 50 < 44 44 < 50 50 < 3000 3,000 < 7000 7,000 < 50 50 < 50 50 < 60000 60,000

Acrolein < 20 20 < 22 22 < 16 16 < 22 22 < 17 17 < 23 23 < 1200 1,200 < 2800 2,800 < 24 24 < 32 32 < 24000 24,000

Acrylonitrile < 20 20 < 22 22 < 16 16 < 22 22 < 8.7 8.7 < 23 23 < 1200 1,200 < 1400 1,400 < 24 24 < 32 32 < 24000 24,000

Benzene 60 4,800 < 4.9 4.9 0.57 5.6 0.42 4.1 < 5.5 5.5 1 4.4 0.59 5.8 4,100 3,000 2,800 700 < 5.9 5.9 2.3 7.9 8,600 6,000

Bromobenzene < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 270 270 < 7.9 7.9 < 6000 6,000

Bromochloromethane < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

Bromodichloromethane < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

Bromoform < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

Bromomethane < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

Carbon Disulfide < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

Carbon tetrachloride 760 2,400 < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

Chlorobenzene 1,100 100,000 < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

Chloroethane < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

Chloroform 370 49,000 < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 250 250 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

Chloromethane < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

cis-1,2-Dichloroethene 250 100,000 < 4.9 4.9 87 250 5.2 4.1 < 5.5 5.5 62 250 6.4 5.8 870 300 7,600 700 0.73 5.9 570 240 730 6,000

cis-1,3-Dichloropropene < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

Dibromochloromethane < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

Dibromomethane < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

Dichlorodifluoromethane < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 0.88 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

Ethylbenzene 1,000 41,000 < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 7,000 300 640 700 < 5.9 5.9 < 7.9 7.9 21,000 6,000

Hexachlorobutadiene < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 270 270 < 7.9 7.9 < 6000 6,000

Isopropylbenzene < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 300 300 < 700 700 < 270 270 < 7.9 7.9 910 6,000

m&p-Xylenes 260 100,000 < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 17,000 3,000 820 700 < 5.9 5.9 < 7.9 7.9 62,000 6,000

Methyl Ethyl Ketone (2-Butanone) 120 100,000 < 30 30 < 34 34 < 24 24 < 33 33 < 26 26 < 35 35 < 1800 1,800 < 4200 4,200 < 35 35 < 48 48 < 36000 36,000

Methyl t-butyl ether (MTBE) 930 100,000 < 9.9 9.9 < 11 11 < 8.1 8.1 < 11 11 < 8.7 8.7 < 12 12 < 600 600 < 700 700 < 12 12 < 16 16 < 12000 12,000

Methylene chloride 50 100,000 < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

Naphthalene 12,000 100,000 < 4.9 4.9 < 5.6 5.6 0.9 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 300,000 30,000 6,500 700 61 270 52 240 620,000 85,000

n-Butylbenzene 12,000 100,000 < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 270 270 < 7.9 7.9 < 6000 6,000

n-Propylbenzene 3,900 100,000 < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 190 300 < 700 700 < 270 270 < 7.9 7.9 < 6000 6,000

o-Xylene 260 100,000 < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 9,200 3,000 230 700 < 5.9 5.9 < 7.9 7.9 21,000 6,000

p-Isopropyltoluene < 4.9 4.9 < 5.6 5.6 0.72 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 440 300 < 700 700 < 270 270 < 7.9 7.9 780 6,000

sec-Butylbenzene 11,000 100,000 < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 270 270 < 7.9 7.9 < 6000 6,000

Styrene < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 1,000 300 < 700 700 < 5.9 5.9 < 7.9 7.9 1,100 6,000

Tert-butyl alcohol < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 270 270 < 7.9 7.9 < 6000 6,000

tert-Butylbenzene 5,900 100,000 < 99 99 < 110 110 < 81 81 < 110 110 < 87 87 < 120 120 < 6000 6,000 < 14000 14,000 < 120 120 < 160 160 < 120000 ######

Tetrachloroethene 1,300 19,000 < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

Tetrahydrofuran (THF) < 9.9 9.9 < 11 11 < 8.1 8.1 < 11 11 < 8.7 8.7 < 12 12 < 600 600 < 1400 1,400 < 12 12 < 16 16 < 12000 12,000

Toluene 700 100,000 < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 8,600 3,000 290 700 0.72 5.9 < 7.9 7.9 22,000 6,000

trans-1,2-Dichloroethene 190 100,000 < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 2.6 4.4 < 5.8 5.8 33 150 160 150 < 5.9 5.9 3 7.9 < 6000 6,000

trans-1,3-Dichloropropene < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

trabs-1,4-dichloro-2-butene < 9.9 9.9 < 11 11 < 8.1 8.1 < 11 11 < 8.7 8.7 < 12 12 < 600 600 < 1400 1,400 < 540 540 < 16 16 < 12000 12,000

Trichloroethene 470 21,000 1.7 4.9 110 280 65 290 0.66 5.5 41 350 2.1 5.8 3,300 300 3,700 700 360 270 390 240 < 6000 6,000

Trichlorofluoromethane < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

Trichlorotrifluoroethane < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 < 4.4 4.4 < 5.8 5.8 < 300 300 < 700 700 < 5.9 5.9 < 7.9 7.9 < 6000 6,000

Vinyl Chloride 20 900 < 4.9 4.9 < 5.6 5.6 < 4.1 4.1 < 5.5 5.5 2.6 4.4 2.2 5.8 290 300 2,600 700 < 5.9 5.9 16 7.9 < 6000 6,000

Total BTEX Concentration

Total VOCs Concentration

Notes:* - 6 NYCRR Part 375-6 Remedial Program Soil Cleanup Objectives

RL - Reporting Limit

Bold/highlighted- Indicated exceedance of the NYSDEC UUSCO Guidance Value

Bold/highlighted- Indicated exceedance of the NYSDEC RRSCO Guidance Value

14B4

(0-5')

801120

µg/Kg

(20-21')

218.57 110.58 25669

µg/Kg

8/25/2015

(0-5') (10-15') (10-15') (10-15')

8/25/2015 8/25/2015

1.7 80.67 0.66 11.29 375923 422.45 1033.3

2.30 0.42 0 0.590.57 1 45900 0.724780 134600

µg/Kg µg/Kg µg/Kg µg/Kg µg/Kg µg/Kgµg/Kg µg/Kg µg/Kg

8/25/2015 8/25/2015 8/25/2015 8/25/2015

(15-18')

8/25/2015

(0-5') (20-25') (0-5')

8/25/20158/25/2015 8/25/2015COMPOUND

NYSDEC Part 375.6 Unrestricted Use Soil Cleanup Objectives*

NYDEC Part 375.6 Restricted Residential Soil Cleanup

Objectives*

14B314B214B1

(10-15')




1,1,1,2-Tetrachlorothane

1,1,1-Trichloroethane 680 100,000

1,1,2,2-Tetrachloroethane

1,1,2-Trichloroethane

1,1-Dichloroethane 270 26,000

1,1-Dichloroethene 330 100,000

1,1-Dichloropropene

1,2,3-Trichlorobenzene

1,2,3-Trichloropropane


1,2,4-Trimethylbenzene 3,600 52,000

1,2-Dibromo-3-chloropropane

1,2-Dibromomethane

1,2-Dichlorobenzene 1,100 100,000

1,2-Dichloroethane 20 3,100

1,2-Dichloropropane

1,3,5-Trimethylbenzene 8,400 52,000


1,3-Dichloropropane


1,4-dioxane

2,2-Dichloropropane

2-Chlorotoluene

2-Hexanone (Methyl Butyl Ketone)

2-Isopropyltoluene

4-Chlorotoluene

4-Methyl-2-Pentanone

Acetone 50 100,000

Acrolein

Acrylonitrile

Benzene 60 4,800

Bromobenzene

Bromochloromethane

Bromodichloromethane

Bromoform

Bromomethane

Carbon Disulfide

Carbon tetrachloride 760 2,400

Chlorobenzene 1,100 100,000

Chloroethane

Chloroform 370 49,000

Chloromethane

cis-1,2-Dichloroethene 250 100,000

cis-1,3-Dichloropropene

Dibromochloromethane

Dibromomethane

Dichlorodifluoromethane

Ethylbenzene 1,000 41,000

Hexachlorobutadiene

Isopropylbenzene

m&p-Xylenes 260 100,000

Methyl Ethyl Ketone (2-Butanone) 120 100,000

Methyl t-butyl ether (MTBE) 930 100,000

Methylene chloride 50 100,000

Naphthalene 12,000 100,000

n-Butylbenzene 12,000 100,000

n-Propylbenzene 3,900 100,000

o-Xylene 260 100,000

p-Isopropyltoluene

sec-Butylbenzene 11,000 100,000

Styrene

Tert-butyl alcohol

tert-Butylbenzene 5,900 100,000

Tetrachloroethene 1,300 19,000

Tetrahydrofuran (THF)

Toluene 700 100,000

trans-1,2-Dichloroethene 190 100,000

trans-1,3-Dichloropropene

trabs-1,4-dichloro-2-butene

Trichloroethene 470 21,000

Trichlorofluoromethane

Trichlorotrifluoroethane

Vinyl Chloride 20 900

Total BTEX Concentration

Total VOCs Concentration





COMPOUNDNYSDEC Part 375.6

Unrestricted Use Soil Cleanup Objectives*

NYDEC Part 375.6 Restricted Residential Soil Cleanup

Objectives*

Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL

< 4.8 4.8 < 17 17 < 20 20 < 21 21 < 17 17 < 1600 1,600 < 21 21 < 6.0 6.0 < 18 18 < 21 21 < 18 18 < 25 25

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 250 250 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 300 300 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 150 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 1 5.3 < 4.6 4.6 < 6.2 6.2

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 47 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 97 97 < 86 86 < 100 100 < 100 100 < 86 86 < 8000 8,000 < 100 100 < 100 100 < 90 90 < 100 100 < 91 91 < 100 100

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 24 24 < 21 21 < 25 25 < 26 26 < 22 22 < 2000 2,000 < 27 27 < 30 30 < 23 23 < 26 26 < 23 23 < 31 31

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 24 24 < 21 21 < 25 25 < 26 26 < 22 22 < 2000 2,000 < 27 27 < 30 30 < 23 23 < 26 26 < 23 23 < 31 31

11 48 6.4 43 8.7 50 7.6 50 < 43 43 < 4000 4,000 12 50 < 50 50 < 45 45 19 50 < 46 46 < 50 50

< 19 19 < 17 17 < 20 20 < 21 21 < 17 17 < 1600 1,600 < 21 21 < 24 24 < 18 18 < 21 21 < 18 18 < 25 25

< 9.7 9.7 < 17 17 < 20 20 < 21 21 < 17 17 < 1600 1,600 < 21 21 < 12 12 < 18 18 < 21 21 < 18 18 < 25 25

0.78 4.8 0.44 4.3 160 350 < 5.2 5.2 0.73 4.3 890 400 0.77 5.3 < 6.0 6.0 < 4.5 4.5 0.69 5.3 < 4.6 4.6 0.73 6.2

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 3.4 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 1.1 5.3 < 6.0 6.0 < 4.5 4.5 2.4 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 250 250 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

3.7 4.8 1.6 4.3 50 250 0.92 5.2 160 250 8,700 400 3.1 5.3 2.5 6.0 37 4.5 170 250 < 4.6 4.6 16 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 0.96 5.0 < 5.2 5.2 < 4.3 4.3 280 400 1.9 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 43 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 77 350 < 5.2 5.2 < 4.3 4.3 270 400 7.5 5.3 < 6.0 6.0 < 4.5 4.5 1.1 5.3 < 4.6 4.6 < 6.2 6.2

< 29 29 < 26 26 < 30 30 < 31 31 < 26 26 < 2400 2,400 < 32 32 < 36 36 < 27 27 < 32 32 < 27 27 < 37 37

< 9.7 9.7 < 8.6 8.6 < 10 10 < 10 10 < 8.6 8.6 < 800 800 < 11 11 < 12 12 < 9.0 9.0 < 11 11 < 9.1 9.1 < 12 12

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 570 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

210 230 50 250 1,100 350 140 270 5.2 8.0 2,700 400 260 400 < 6.0 6.0 < 4.5 4.5 2.6 5.3 < 4.6 4.6 < 6.2 6.2

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 63 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 130 400 2.5 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 170 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 230 230 < 250 250 < 5.0 5.0 < 270 270 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 97 97 < 86 86 < 100 100 < 100 100 < 86 86 < 8000 8,000 < 110 110 < 120 120 < 90 90 < 110 110 < 91 91 < 120 120

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 9.7 9.7 < 8.6 8.6 < 10 10 < 10 10 < 8.6 8.6 < 800 800 < 11 11 < 12 12 < 9.0 9.0 < 11 11 < 9.1 9.1 < 12 12

< 4.8 4.8 < 4.3 4.3 0.51 5.0 0.64 5.2 < 4.3 4.3 150 400 110 400 < 6.0 6.0 < 4.5 4.5 2.1 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 0.47 4.3 94 150 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 0.84 5.3 < 4.6 4.6 0.97 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 470 470 < 490 490 < 10 10 < 540 540 < 8.6 8.6 < 800 800 < 11 11 < 12 12 < 9.0 9.0 < 11 11 < 9.1 9.1 < 12 12

56 230 51 250 2.4 5.0 32 270 63 290 14,000 400 100 400 2.3 6.0 23 4.5 250 260 3.2 4.6 2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 < 4.3 4.3 < 5.0 5.0 < 5.2 5.2 < 4.3 4.3 < 400 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 < 5.3 5.3 < 4.6 4.6 < 6.2 6.2

< 4.8 4.8 0.48 4.3 2.2 5.0 < 5.2 5.2 7.6 4.3 1,100 400 < 5.3 5.3 < 6.0 6.0 < 4.5 4.5 0.58 5.3 < 4.6 4.6 0.72 6.2

1405.17

(0-5') (15-19.5')

8/25/2015

14B814B714B6

(0-5') (15-17')

20.42

µg/Kg µg/Kg

8/25/2015

0.73

60

0.78 0.44

14B5

29357

8/25/2015

µg/Kgµg/Kg µg/Kg

8/25/20158/25/2015 8/25/2015

µg/Kg µg/Kg

8/25/2015

(10-15') (10-15')

µg/Kg

3.2281.48 109.92 181.16 237 498.87 4.8

0

8/25/2015

0

450.31

3.89238.47 0

µg/Kg

0.64 0.73 122.671720

µg/Kg µg/Kg µg/Kg

8/25/2015

(0-5') (20-25')(0-5') (15-20')(10-15')

8/25/2015 8/25/20158/25/2015

(10-15')


510 Driggs Avenue, Brooklyn, New York Soil Analytical Results

Semi-Volatile Organic Compounds

Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL

1,2,4,5-Tetrachlorobenzene < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

1,2,4-Trichlorobenzene < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

1,2-Dichlorobenzene < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

1,2-Diphenylhydrazine < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

1,3-Dichlorobenzene < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

1,4-Dichlorobenzene 500 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

2,4,5-Trichlorophenol < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

2,4,6-Trichlorophenol < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

2,4-Dichlorophenol < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

2,4-Dimethylphenol < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

2,4-Dinitrophenol < 730 730 < 7300 7,300 < 740 740 < 770 770 < 780 780 < 710 710 < 730 730 < 8300 8,300

2,4-Dinitrotoluene < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

2,6-Dinitrotoluene < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

2-Chloronaphthalene < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

2-Chlorophenol < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

2-Methylnaphthalene < 250 250 2,300 2,600 130 260 < 270 270 < 270 270 < 250 250 < 260 260 19,000 2,900

2-Methylphenol (o-cresol) 330 100,000 < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

2-Nitroaniline < 730 730 < 7300 7,300 < 740 740 < 770 770 < 780 780 < 710 710 < 730 730 < 8300 8,300

2-Nitrophenol < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

3&4-Methylphenol (m&p-cresol) 330 100,000 < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

3,3'-Dichlorobenzidine < 730 730 < 7300 7,300 < 740 740 < 770 770 < 780 780 < 710 710 < 730 730 < 8300 8,300

3-Nitroaniline < 730 730 < 7300 7,300 < 740 740 < 770 770 < 780 780 < 710 710 < 730 730 < 8300 8,300

4,6-Dinitro-2-methylphenol < 1800 1,800 < 18000 18,000 < 1800 1,800 < 1900 1,900 < 1900 1,900 < 1800 1,800 < 1800 1,800 < 21000 21,000

4-Bromophenyl phenyl ether < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

4-Chloro-3-methylphenol < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

4-Chloroaniline < 290 290 < 2900 2,900 < 300 300 < 310 310 < 310 310 < 290 290 < 290 290 < 3300 3,300

4-Chlorophenyl phenyl ether < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

4-Nitroaniline < 730 730 < 7300 7,300 < 740 740 < 770 770 < 780 780 < 710 710 < 730 730 < 8300 8,300

4-Nitrophenol < 360 360 < 3700 3,700 < 370 370 < 380 380 < 390 390 < 360 360 < 370 370 < 4100 4,100

Acenaphthene 20,000 100,000 < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 2,900 2,900

Acenaphthylene 100,000 100,000 110 250 < 2600 2,600 120 260 < 270 270 < 270 270 < 250 250 < 260 260 8,400 2,900

Acetophenone < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

Aniline < 290 290 < 2900 2,900 < 300 300 < 310 310 < 310 310 < 290 290 < 290 290 < 3300 3,300

Anthracene 100,000 100,000 860 250 15,000 2,600 300 260 < 270 270 < 270 270 150 250 < 260 260 16,000 2,900

Benz(a)anthracene 1,000 1,000 3,500 250 16,000 2,600 820 260 < 270 270 < 270 270 750 250 490 260 14,000 2,900

Benzidine < 730 730 < 7300 7,300 < 740 740 < 770 770 < 780 780 < 710 710 < 730 730 < 8300 8,300

Benzo(a)pyrene 1,000 1,000 3,200 250 13,000 2,600 810 260 < 270 270 < 270 270 1,000 250 700 260 13,000 2,900

Benzo(b)fluoranthene 1,000 1,000 4,500 250 11,000 2,600 750 260 < 270 270 < 270 270 660 250 510 260 9,900 2,900

Benzo(ghi)perylene 100,000 100,000 3,000 250 6,200 2,600 500 260 < 270 270 < 270 270 530 250 370 260 5,000 2,900

Benzo(k)fluoranthene 800 3,900 3,400 250 10,000 2,600 620 260 < 270 270 < 270 270 850 250 520 260 10,000 2,900

Benzoic acid < 1800 1,800 < 18000 18,000 < 1800 1,800 < 1900 1,900 < 1900 1,900 < 1800 1,800 < 1800 1,800 < 21000 21,000

Benzyl butyl phthalate < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

Bis(2-chloroethoxy)methane < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

Bis(2-chloroethyl)ether < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

Bis(2-chloroisopropyl)ether < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

Bis(2-ethylhexyl)phthalate < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

Carbazole 350 1,800 7,300 18,000 < 1800 1,800 < 1900 1,900 < 1900 1,900 < 1800 1,800 < 1800 1,800 5,700 21,000

Chrysene 1,000 3,900 3,300 250 16,000 2,600 820 260 < 270 270 < 270 270 690 250 470 260 13,000 2,900

Dibenz(a,h)anthracene 330 330 1,400 250 1,300 2,600 170 260 < 270 270 < 270 270 180 250 < 260 260 2,000 2,900

Dibenzofuran 7,000 59,000 240 250 6,300 2,600 140 260 < 270 270 < 270 270 < 250 250 < 260 260 12,000 2,900

Diethyl phthalate < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

Dimethylphthalate < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

Di-n-butylphthalate < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

Di-n-octylphthalate < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

Fluoranthene 100,000 100,000 4,300 250 47,000 2,600 1,300 260 < 270 270 < 270 270 860 250 570 260 25,000 2,900

Fluorene 30,000 100,000 230 250 7,500 2,600 150 260 < 270 270 < 270 270 < 250 250 < 260 260 18,000 2,900

Hexachlorobenzene < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

Hexachlorobutadiene < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

Hexachlorocyclopentadiene < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

Hexachloroethane < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

Indeno(1,2,3-cd)pyrene 500 500 3,900 250 7,200 2,600 570 260 < 270 270 < 270 270 600 250 410 260 6,400 2,900

Isophorone < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

Naphthalene 12,000 100,000 240 250 5,000 2,600 230 260 < 270 270 < 270 270 < 250 250 < 260 260 43,000 2,900

Nitrobenzene < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

N-Nitrosodimethylamine < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

N-Nitrosodi-n-propylamine < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

N-Nitrosodiphenylamine < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

Pentachloronitrobenzene < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

Pentachlorophenol 800 6,700 < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

Phenanthrene 100,000 100,000 2,500 250 66,000 2,600 1,100 260 < 270 270 < 270 270 440 250 360 260 45,000 2,900

Phenol 330 100,000 < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900

Pyrene 100,000 100,000 4,100 250 41,000 2,600 1,200 260 < 270 270 < 270 270 780 250 540 260 20,000 2,900

Pyridine < 250 250 < 2600 2,600 < 260 260 < 270 270 < 270 270 < 250 250 < 260 260 < 2900 2,900





µg/Kg

14B1 14B2 14B3


8/25/2015

µg/Kg µg/Kg µg/Kg µg/Kg

(0-5') (10-15') (15-18')

8/25/20158/25/2015 8/25/2015 8/25/2015 8/25/2015

(20-25')COMPOUNDNYSDEC Part 375.6


NYDEC Part 375.6 Restricted Residential

Soil Cleanup Objectives*

(0-5') (10-15') (0-5') (10-15')

8/25/2015 8/25/2015




Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL

1,2,4,5-Tetrachlorobenzene < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

1,2,4-Trichlorobenzene < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

1,2-Dichlorobenzene < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

1,2-Diphenylhydrazine < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310



2,4,5-Trichlorophenol < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

2,4,6-Trichlorophenol < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

2,4-Dichlorophenol < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

2,4-Dimethylphenol < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

2,4-Dinitrophenol < 700 700 < 790 790 < 8200 8,200 < 720 720 < 730 730 < 840 840 < 700 700 < 760 760 < 900 900

2,4-Dinitrotoluene < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

2,6-Dinitrotoluene < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

2-Chloronaphthalene < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

2-Chlorophenol < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

2-Methylnaphthalene < 240 240 < 280 280 74,000 2,900 < 250 250 110 260 470 290 < 250 250 < 270 270 < 310 310

2-Methylphenol (o-cresol) 330 100,000 < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

2-Nitroaniline < 700 700 < 790 790 < 8200 8,200 < 720 720 < 730 730 < 840 840 < 700 700 < 760 760 < 900 900

2-Nitrophenol < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

3&4-Methylphenol (m&p-cresol) 330 100,000 < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

3,3'-Dichlorobenzidine < 700 700 < 790 790 < 8200 8,200 < 720 720 < 730 730 < 840 840 < 700 700 < 760 760 < 900 900

3-Nitroaniline < 700 700 < 790 790 < 8200 8,200 < 720 720 < 730 730 < 840 840 < 700 700 < 760 760 < 900 900

4,6-Dinitro-2-methylphenol < 1700 1,700 < 2000 2,000 < 21000 21,000 < 1800 1,800 < 1800 1,800 < 2100 2,100 < 1800 1,800 < 1900 1,900 < 2200 2,200

4-Bromophenyl phenyl ether < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

4-Chloro-3-methylphenol < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

4-Chloroaniline < 280 280 < 320 320 < 3300 3,300 < 290 290 < 290 290 < 340 340 < 280 280 < 310 310 < 360 360

4-Chlorophenyl phenyl ether < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

4-Nitroaniline < 700 700 < 790 790 < 8200 8,200 < 720 720 < 730 730 < 840 840 < 700 700 < 760 760 < 900 900

4-Nitrophenol < 350 350 < 400 400 < 4100 4,100 < 360 360 < 360 360 < 420 420 < 350 350 < 380 380 < 450 450

Acenaphthene 20,000 100,000 < 240 240 190 280 12,000 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 330 310

Acenaphthylene 100,000 100,000 < 240 240 < 280 280 20,000 2,900 120 250 460 260 330 290 < 250 250 < 270 270 620 310

Acetophenone < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

Aniline < 280 280 < 320 320 < 3300 3,300 < 290 290 < 290 290 < 340 340 < 280 280 < 310 310 < 360 360

Anthracene 100,000 100,000 120 240 240 280 50,000 2,900 210 250 1,400 260 2,700 290 < 250 250 < 270 270 3,900 310

Benz(a)anthracene 1,000 1,000 480 240 1,800 280 41,000 2,900 850 250 2,700 260 8,000 1,500 170 250 170 270 6,300 310

Benzidine < 700 700 < 790 790 < 8200 8,200 < 720 720 < 730 730 < 840 840 < 700 700 < 760 760 < 900 900

Benzo(a)pyrene 1,000 1,000 600 240 3,600 280 28,000 2,900 1,000 250 3,000 260 14,000 1,500 170 250 390 270 2,100 310

Benzo(b)fluoranthene 1,000 1,000 420 240 2,300 280 21,000 2,900 980 250 2,200 260 9,700 1,500 160 250 250 270 8,800 310

Benzo(ghi)perylene 100,000 100,000 430 240 2,900 280 9,700 2,900 660 250 1,300 260 6,200 1,500 150 250 290 270 5,100 310

Benzo(k)fluoranthene 800 3,900 490 240 2,900 280 26,000 2,900 870 250 2,700 260 6,500 290 160 250 270 270 4,600 310

Benzoic acid < 1700 1,700 < 2000 2,000 < 21000 21,000 < 1800 1,800 < 1800 1,800 < 2100 2,100 < 1800 1,800 < 1900 1,900 < 2200 2,200

Benzyl butyl phthalate < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

Bis(2-chloroethoxy)methane < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

Bis(2-chloroethyl)ether < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

Bis(2-chloroisopropyl)ether < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

Bis(2-ethylhexyl)phthalate < 240 240 < 280 280 < 2900 2,900 140 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

Carbazole < 1700 1,700 < 2000 2,000 20,000 21,000 < 1800 1,800 280 1,800 2,500 2,100 < 1800 1,800 < 1900 1,900 1,700 2,200

Chrysene 1,000 3,900 510 240 1,800 280 38,000 2,900 910 250 2,600 260 8,200 1,500 180 250 170 270 6,100 310

Dibenz(a,h)anthracene 330 330 150 240 500 280 3,800 2,900 250 250 440 260 4,200 290 < 250 250 < 270 270 1,900 310

Dibenzofuran 7,000 59,000 < 240 240 < 280 280 43,000 2,900 < 250 250 470 260 1,300 290 < 250 250 < 270 270 3,200 310

Diethyl phthalate < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

Dimethylphthalate < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

Di-n-butylphthalate < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

Di-n-octylphthalate < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

Fluoranthene 100,000 100,000 770 240 1,300 280 70,000 14,000 1,300 250 4,100 260 8,500 1,500 340 250 240 270 8,800 310

Fluorene 30,000 100,000 < 240 240 < 280 280 66,000 2,900 < 250 250 950 260 2,300 290 < 250 250 < 270 270 3,700 310

Hexachlorobenzene < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

Hexachlorobutadiene < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

Hexachlorocyclopentadiene < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

Hexachloroethane < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

Indeno(1,2,3-cd)pyrene 500 500 500 240 3,400 280 11,000 2,900 710 250 1,600 260 7,400 1,500 180 250 340 270 6,200 310

Isophorone < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

Naphthalene 12,000 100,000 < 240 240 410 280 190,000 14,000 < 250 250 230 260 2,300 290 < 250 250 < 270 270 4,300 310

Nitrobenzene < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

N-Nitrosodimethylamine < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

N-Nitrosodi-n-propylamine < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

N-Nitrosodiphenylamine < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

Pentachloronitrobenzene < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

Pentachlorophenol 800 6,700 < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

Phenanthrene 100,000 100,000 470 240 700 280 140,000 14,000 750 250 4,200 260 5,200 290 150 250 110 270 8,100 310

Phenol 330 100,000 < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310

Pyrene 100,000 100,000 690 240 1,100 280 73,000 2,900 1,100 250 3,500 260 8,100 1,500 300 250 220 270 7,200 310

Pyridine < 240 240 < 280 280 < 2900 2,900 < 250 250 < 260 260 < 290 290 < 250 250 < 270 270 < 310 310





(10-15') (15-19.5')COMPOUNDNYSDEC Part 375.6




8/25/2015

(0-5')(0-5') (10-15') (20-21')

8/25/2015 8/25/2015 8/25/2015

(15-17')

µg/Kg µg/Kgµg/Kg µg/Kg µg/Kg µg/Kg µg/Kg

8/25/2015 8/25/2015

14B4 14B5 14B6

µg/Kg µg/Kg

8/25/2015 8/25/2015 8/25/2015

(0-5') (10-15')




Result RL Result RL Result RL Result RL Result RL Result RL

1,2,4,5-Tetrachlorobenzene < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

1,2,4-Trichlorobenzene < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

1,2-Dichlorobenzene < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

1,2-Diphenylhydrazine < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290



2,4,5-Trichlorophenol < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

2,4,6-Trichlorophenol < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

2,4-Dichlorophenol < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

2,4-Dimethylphenol < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

2,4-Dinitrophenol < 820 820 < 730 730 < 810 810 < 730 730 < 800 800 < 840 840

2,4-Dinitrotoluene < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

2,6-Dinitrotoluene < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

2-Chloronaphthalene < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

2-Chlorophenol < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

2-Methylnaphthalene < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

2-Methylphenol (o-cresol) 330 100,000 < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

2-Nitroaniline < 820 820 < 730 730 < 810 810 < 730 730 < 800 800 < 840 840

2-Nitrophenol < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

3&4-Methylphenol (m&p-cresol) 330 100,000 < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

3,3'-Dichlorobenzidine < 820 820 < 730 730 < 810 810 < 730 730 < 800 800 < 840 840

3-Nitroaniline < 820 820 < 730 730 < 810 810 < 730 730 < 800 800 < 840 840

4,6-Dinitro-2-methylphenol < 2000 2,000 < 1800 1,800 < 2000 2,000 < 1800 1,800 < 2000 2,000 < 2100 2,100

4-Bromophenyl phenyl ether < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

4-Chloro-3-methylphenol < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

4-Chloroaniline < 330 330 < 290 290 < 320 320 < 290 290 < 320 320 < 340 340

4-Chlorophenyl phenyl ether < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

4-Nitroaniline < 820 820 < 730 730 < 810 810 < 730 730 < 800 800 < 840 840

4-Nitrophenol < 410 410 < 370 370 < 410 410 < 360 360 < 400 400 < 420 420

Acenaphthene 20,000 100,000 < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Acenaphthylene 100,000 100,000 < 290 290 < 260 260 < 280 280 130 260 < 280 280 < 290 290

Acetophenone < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Aniline < 330 330 < 290 290 < 320 320 < 290 290 < 320 320 < 340 340

Anthracene 100,000 100,000 260 290 < 260 260 < 280 280 200 260 < 280 280 < 290 290

Benz(a)anthracene 1,000 1,000 1,200 290 < 260 260 140 280 1,100 260 < 280 280 < 290 290

Benzidine < 820 820 < 730 730 < 810 810 < 730 730 < 800 800 < 840 840

Benzo(a)pyrene 1,000 1,000 940 290 < 260 260 920 280 970 260 < 280 280 < 290 290

Benzo(b)fluoranthene 1,000 1,000 1,100 290 < 260 260 560 280 820 260 < 280 280 < 290 290

Benzo(ghi)perylene 100,000 100,000 640 290 < 260 260 340 280 620 260 < 280 280 < 290 290

Benzo(k)fluoranthene 800 3,900 960 290 < 260 260 680 280 980 260 < 280 280 < 290 290

Benzoic acid < 2000 2,000 < 1800 1,800 < 2000 2,000 < 1800 1,800 < 2000 2,000 < 2100 2,100

Benzyl butyl phthalate < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Bis(2-chloroethoxy)methane < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Bis(2-chloroethyl)ether < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Bis(2-chloroisopropyl)ether < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Bis(2-ethylhexyl)phthalate < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Carbazole < 2000 2,000 < 1800 1,800 < 2000 2,000 < 1800 1,800 < 2000 2,000 < 2100 2,100

Chrysene 1,000 3,900 1,400 290 < 260 260 150 280 1,100 260 < 280 280 < 290 290

Dibenz(a,h)anthracene 330 330 160 290 < 260 260 < 280 280 200 260 < 280 280 < 290 290

Dibenzofuran 7,000 59,000 < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Diethyl phthalate < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Dimethylphthalate < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Di-n-butylphthalate < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Di-n-octylphthalate < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Fluoranthene 100,000 100,000 2,800 290 < 260 260 < 280 280 1,800 260 < 280 280 < 290 290

Fluorene 30,000 100,000 < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Hexachlorobenzene < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Hexachlorobutadiene < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Hexachlorocyclopentadiene < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Hexachloroethane < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Indeno(1,2,3-cd)pyrene 500 500 720 290 < 260 260 410 280 680 260 150 280 < 290 290

Isophorone < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Naphthalene 12,000 100,000 < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Nitrobenzene < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

N-Nitrosodimethylamine < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

N-Nitrosodi-n-propylamine < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

N-Nitrosodiphenylamine < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Pentachloronitrobenzene < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Pentachlorophenol 800 6,700 < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Phenanthrene 100,000 100,000 1,700 290 < 260 260 < 280 280 730 260 < 280 280 < 290 290

Phenol 330 100,000 < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290

Pyrene 100,000 100,000 2,200 290 < 260 260 < 280 280 1,500 260 < 280 280 < 290 290

Pyridine < 290 290 < 260 260 < 280 280 < 260 260 < 280 280 < 290 290





µg/Kg

14B7 14B8

8/25/2015

(0-5') (10-15') (15-20') (0-5') (10-15') (20-25')

8/25/2015 8/25/2015 8/25/2015




Soil Cleanup Objectives* 8/25/2015

µg/Kg µg/Kg

8/25/2015




Pesticides PCBs

Result RL Result RL Result RL Result RL Result RL Result RL Result RL

4,4' -DDD 3.3 13,000 < 9.1 9.1 < 5.0 5.0 < 2.3 2.3 < 60 60 < 20 20 4.3 3.3 < 60 60

4,4' -DDE 3.3 8,900 < 9.1 9.1 8.1 2.2 < 2.3 2.3 < 11 11 < 20 20 4 2.1 < 40 40

4,4' -DDT 3.3 7,900 < 9.1 9.1 7.1 2.2 < 2.3 2.3 < 11 11 < 25 25 < 2.1 2.1 < 30 30

a-BHC 20 480 < 18 18 < 7.4 7.4 < 7.7 7.7 < 36 36 < 41 41 < 6.9 6.9 < 41 41

a-Chlordane 94 4,200 68 18 110 3.7 < 3.9 3.9 130 18 < 41 41 22 3.4 170 41

Aldrin 5 97 < 5.5 5.5 < 3.7 3.7 < 3.9 3.9 < 18 18 < 12 12 < 3.4 3.4 < 12 12

b-BHC 36 360 < 18 18 < 7.4 7.4 < 7.7 7.7 < 36 36 < 41 41 < 6.9 6.9 < 41 41

Chlordane 94 4,200 510 180 970 180 < 39 39 1,300 180 < 410 410 120 34 650 410

d-BHC 40 100,000 < 37 37 < 7.4 7.4 < 7.7 7.7 < 36 36 < 41 41 < 6.9 6.9 < 41 41

Dieldrin 5 200 < 5.5 5.5 9.4 3.7 < 3.9 3.9 < 18 18 < 12 12 < 3.4 3.4 < 12 12

Endosulfan I 2,400 24,000 < 37 37 < 7.4 7.4 < 7.7 7.7 < 36 36 < 82 82 < 6.9 6.9 < 82 82

Endosulfan II 2,400 24,000 < 37 37 < 7.4 7.4 < 7.7 7.7 < 36 36 < 20 20 < 6.9 6.9 < 82 82

Endosulfan sulfate 2,400 24,000 < 37 37 < 7.4 7.4 < 7.7 7.7 < 36 36 < 82 82 < 6.9 6.9 < 82 82

Endrin 14 11,000 < 18 18 < 7.4 7.4 < 7.7 7.7 < 36 36 < 41 41 < 6.9 6.9 < 41 41

Endrin aldehyde < 37 37 < 7.4 7.4 < 7.7 7.7 < 36 36 < 82 82 < 6.9 6.9 < 82 82

Endrin ketone < 37 37 < 7.4 7.4 < 7.7 7.7 < 36 36 < 82 82 < 6.9 6.9 < 82 82

g-BHC < 7.3 7.3 < 2.0 2.0 < 1.5 1.5 < 7.2 7.2 < 16 16 < 1.4 1.4 < 30 30

g-Chlordane 52 18 130 3.7 < 3.9 3.9 160 18 < 41 41 19 3.4 99 41

Heptachlor 42 2,100 < 37 37 < 7.4 7.4 < 7.7 7.7 < 36 36 < 41 41 < 6.9 6.9 < 41 41

Heptachlor epoxide < 37 37 < 7.4 7.4 < 7.7 7.7 < 36 36 < 41 41 < 6.9 6.9 < 82 82

Methoxychlor < 180 180 < 37 37 < 39 39 < 180 180 < 410 410 < 34 34 < 410 410

Toxaphene < 730 730 < 150 150 < 150 150 < 720 720 < 1600 1,600 < 140 140 < 1600 1,600

PCB-1016 100 1,000 < 37 37 < 180 180 < 39 39 < 36 36 < 41 41 < 34 34 < 41 41

PCB-1221 100 1,000 < 37 37 < 180 180 < 39 39 < 36 36 < 41 41 < 34 34 < 41 41

PCB-1232 100 1,000 < 37 37 < 180 180 < 39 39 < 36 36 < 41 41 < 34 34 < 41 41

PCB-1242 100 1,000 < 37 37 < 180 180 < 39 39 < 36 36 < 41 41 < 34 34 < 41 41

PCB-1248 100 1,000 < 37 37 < 180 180 < 39 39 < 36 36 < 41 41 < 34 34 < 41 41

PCB-1254 100 1,000 < 37 37 < 180 180 < 39 39 < 36 36 < 41 41 < 34 34 < 41 41

PCB-1260 100 1,000 < 37 37 < 180 180 < 39 39 < 36 36 < 41 41 < 34 34 < 41 41

PCB-1262 100 1,000 < 37 37 < 180 180 < 39 39 < 36 36 < 41 41 < 34 34 < 41 41

PCB-1268 100 1,000 < 37 37 < 180 180 < 39 39 < 36 36 < 41 41 < 34 34 < 41 41


RL- Reporting Limit



14B2 14B3 14B4(0-5')

8/25/2015(20-21')

8/25/2015(0-5') (20-25') (0-5') (15-18')

8/25/2015 8/25/2015

Pes

tici

des

µg/Kgµg/Kgµg/Kg µg/Kg µg/Kg µg/Kg

PC

Bs

8/25/2015 8/25/2015 8/25/2015

14B1(0-5')

µg/Kg



NYDEC Part 375.6 Restricted Residential Soil

Cleanup Objectives*



Pesticides PCBs


4,4' -DDD 3.3 13,000 < 21 21 < 25 25 < 2.1 2.1 < 27 27 < 10 10 < 2.4 2.4 < 15 15 < 2.6 2.6

4,4' -DDE 3.3 8,900 < 21 21 < 25 25 < 2.1 2.1 < 27 27 < 10 10 < 2.4 2.4 < 9.2 9.2 < 2.6 2.6

4,4' -DDT 3.3 7,900 < 21 21 < 25 25 < 2.1 2.1 < 27 27 < 10 10 < 2.4 2.4 < 9.2 9.2 < 2.6 2.6

a-BHC 20 480 < 35 35 < 42 42 < 7.0 7.0 < 44 44 < 21 21 < 8.0 8.0 < 18 18 < 8.6 8.6

a-Chlordane 94 4,200 < 35 35 < 42 42 < 3.5 3.5 < 44 44 56 21 < 4.0 4.0 50 18 < 4.3 4.3

Aldrin 5 97 < 11 11 < 12 12 < 3.5 3.5 < 13 13 < 6.2 6.2 < 4.0 4.0 < 5.5 5.5 < 4.3 4.3

b-BHC 36 360 < 35 35 < 42 42 < 7.0 7.0 < 44 44 < 21 21 < 8.0 8.0 < 18 18 < 8.6 8.6

Chlordane 94 4,200 < 350 350 < 420 420 < 35 35 < 440 440 320 210 < 40 40 220 180 < 43 43

d-BHC 40 100,000 < 35 35 < 42 42 < 7.0 7.0 < 44 44 < 21 21 < 8.0 8.0 < 37 37 < 8.6 8.6

Dieldrin 5 200 < 11 11 < 15 15 < 3.5 3.5 < 44 44 13 6.2 < 4.0 4.0 < 5.5 5.5 < 4.3 4.3

Endosulfan I 2,400 24,000 < 70 70 < 83 83 < 7.0 7.0 < 89 89 < 41 41 < 8.0 8.0 < 37 37 < 8.6 8.6

Endosulfan II 2,400 24,000 < 70 70 < 83 83 < 7.0 7.0 < 89 89 < 41 41 < 8.0 8.0 < 37 37 < 8.6 8.6

Endosulfan sulfate 2,400 24,000 < 70 70 < 83 83 < 7.0 7.0 < 89 89 < 41 41 < 8.0 8.0 < 37 37 < 8.6 8.6

Endrin 14 11,000 < 35 35 < 42 42 < 7.0 7.0 < 89 89 < 21 21 < 8.0 8.0 < 18 18 < 8.6 8.6

Endrin aldehyde < 70 70 < 120 120 < 7.0 7.0 < 89 89 < 50 50 < 8.0 8.0 < 37 37 < 8.6 8.6

Endrin ketone < 70 70 < 83 83 < 7.0 7.0 < 89 89 < 41 41 < 8.0 8.0 < 37 37 < 8.6 8.6

g-BHC < 14 14 < 40 40 < 8.0 8.0 < 30 30 < 8.2 8.2 < 1.6 1.6 < 7.3 7.3 < 1.7 1.7

g-Chlordane < 35 35 < 180 180 < 3.5 3.5 < 44 44 66 21 < 4.0 4.0 39 18 < 4.3 4.3

Heptachlor 42 2,100 < 35 35 < 42 42 < 7.0 7.0 < 44 44 < 41 41 < 8.0 8.0 < 37 37 < 8.6 8.6

Heptachlor epoxide < 70 70 < 83 83 < 7.0 7.0 < 89 89 < 41 41 < 8.0 8.0 < 37 37 < 8.6 8.6

Methoxychlor < 350 350 < 420 420 < 35 35 < 440 440 < 210 210 < 40 40 < 180 180 < 43 43

Toxaphene < 1400 1,400 < 1700 1,700 < 140 140 < 1800 1,800 < 820 820 < 160 160 < 730 730 < 170 170

PCB-1016 100 1,000 < 35 35 < 42 42 < 35 35 < 44 44 < 41 41 < 40 40 < 37 37 < 43 43

PCB-1221 100 1,000 < 35 35 < 42 42 < 35 35 < 44 44 < 41 41 < 40 40 < 37 37 < 43 43

PCB-1232 100 1,000 < 35 35 < 42 42 < 35 35 < 44 44 < 41 41 < 40 40 < 37 37 < 43 43

PCB-1242 100 1,000 < 35 35 < 42 42 < 35 35 < 44 44 < 41 41 < 40 40 < 37 37 < 43 43

PCB-1248 100 1,000 < 35 35 < 42 42 < 35 35 < 44 44 < 41 41 < 40 40 < 37 37 < 43 43

PCB-1254 100 1,000 < 35 35 < 42 42 < 35 35 < 44 44 < 41 41 < 40 40 < 37 37 < 43 43

PCB-1260 100 1,000 < 35 35 < 42 42 < 35 35 < 44 44 < 41 41 < 40 40 < 37 37 < 43 43

PCB-1262 100 1,000 < 35 35 < 42 42 < 35 35 < 44 44 < 41 41 < 40 40 < 37 37 < 43 43

PCB-1268 100 1,000 < 35 35 < 42 42 < 35 35 < 44 44 < 41 41 < 40 40 < 37 37 < 43 43


RL- Reporting Limit



PC

Bs

(20-25')(15-20')(0-5') (0-5')COMPOUND

NYSDEC Part 375.6 Unrestricted Use Soil Cleanup Objectives*

NYDEC Part 375.6 Restricted Residential Soil

Cleanup Objectives*8/25/2015 8/25/2015

(15-17')

Pes

tici

des

µg/Kg µg/Kg µg/Kg µg/Kgµg/Kg8/25/2015

µg/Kg µg/Kg µg/Kg8/25/20158/25/2015

14B8

8/25/2015

14B5 14B6 14B7

8/25/20158/25/2015(0-5')(15-19.5')(0-5')



Metals

Result RL Result RL Result RL Result RL Result RL Result RL Result RL

Aluminum 8,460 33 8,770 33 9,510 37 8,780 34 7,200 42 8,810 33 9,810 40

Antimony < 1.7 1.7 < 1.6 1.6 < 1.9 1.9 < 1.7 1.7 < 2.1 2.1 < 1.7 1.7 < 2.0 2.0

Arsenic 13 16 3.6 0.7 3.7 0.7 1.5 0.7 2.4 0.7 2.8 0.8 2.6 0.7 3.3 0.8

Barium 350 350 72 0.7 63.8 0.7 81.4 0.7 54.2 0.7 72 0.8 80.9 0.7 69.7 0.8

Beryllium 7.2 14 0.45 0.26 0.4 0.26 0.61 0.30 0.39 0.27 0.44 0.33 0.35 0.27 0.49 0.32

Cadmium 2.5 2.5 0.59 0.33 < 0.33 0.33 < 0.37 0.37 < 0.34 0.34 0.21 0.42 < 0.33 0.33 < 0.40 0.40

Calcium 5,560 3.3 4,670 3.3 2,210 3.7 3,950 3.4 27,000 42 5,440 3.3 11,300 4.0

Chromium 30 180 31.3 0.33 17.4 0.33 22.7 0.37 17.5 0.34 14.1 0.42 17.1 0.33 15.7 0.40

Cobalt 8.27 0.33 7.04 0.33 10.3 0.37 6.29 0.34 6.86 0.42 6.24 0.33 5.4 0.40

Copper 50 270 25.1 0.33 20.6 0.33 21.5 0.37 21.5 0.34 20.5 0.42 22.2 0.33 15.7 0.40

Iron 17,900 33 15,800 33 24,100 37 13,900 34 19,600 42 15,000 33 16,700 40

Lead 63 400 102 0.7 56.1 0.7 7.2 0.7 29.9 0.7 121 0.8 79.2 0.7 50.8 0.8

Magnesium 2,530 3.3 2,410 3.3 4,020 3.7 2,230 3.4 3,490 4.2 3,210 3.3 10,100 40

Manganese 1,600 2,000 356 3.3 334 3.3 367 3.7 252 3.4 521 4.2 266 3.3 649 4.0

Mercury 0.18 0.81 0.58 0.03 0.19 0.03 < 0.03 0.03 0.09 0.03 0.41 0.03 0.05 0.03 0.06 0.03

Nickel 30 140 36.3 0.33 19.4 0.33 17.5 0.37 17.3 0.34 14.1 0.42 17 0.33 11.9 0.40

Potassium 1,420 7 1,220 7 2,830 7 1,120 7 1,670 8 1,310 7 1,150 8

Selenium 3.9 36 < 1.3 1.3 < 1.3 1.3 < 1.5 1.5 < 1.4 1.4 < 1.7 1.7 < 1.3 1.3 < 1.6 1.6

Silver 2 36 < 0.33 0.33 < 0.33 0.33 < 0.37 0.37 < 0.34 0.34 < 0.42 0.42 < 0.33 0.33 < 0.40 0.40

Sodium 290 7 248 7 368 7 157 7 548 8 374 7 1,100 8

Thallium < 1.3 1.3 < 1.3 1.3 < 1.5 1.5 < 1.4 1.4 < 1.7 1.7 < 1.3 1.3 < 1.6 1.6

Vanadium 25 0.3 26.2 0.3 34.7 0.4 23.9 0.3 24.3 0.4 29.5 0.3 30.3 0.4

Zinc 109 2,200 88.5 0.7 66.3 0.7 47.3 0.7 41.7 0.7 51.4 0.8 56.7 0.7 28.4 0.8


RL- Reporting Limit



14B1

8/25/2015mg/Kg mg/Kg mg/Kg

(0-5') (0-5') (15-18')

14B2(0-5')

mg/Kg8/25/2015 8/25/2015 8/25/2015

mg/Kg8/25/2015

(0-5') (20-21')COMPOUNDNYSDEC Part 375.6




14B3 14B4(20-25')

mg/Kg mg/Kg8/25/2015 8/25/2015



Metals

Aluminum

Antimony

Arsenic 13 16

Barium 350 350

Beryllium 7.2 14

Cadmium 2.5 2.5

Calcium

Chromium 30 180

Cobalt

Copper 50 270

Iron

Lead 63 400

Magnesium

Manganese 1,600 2,000

Mercury 0.18 0.81

Nickel 30 140

Potassium

Selenium 3.9 36

Silver 2 36

Sodium

Thallium

Vanadium

Zinc 109 2,200


RL- Reporting Limit








9,240 32 11,800 39 7,140 32 8,350 43 6,730 42 11,000 37 8,600 34 12,800 41

< 1.6 1.6 < 1.9 1.9 < 1.6 1.6 < 2.2 2.2 < 2.1 2.1 < 1.8 1.8 < 1.7 1.7 < 2.1 2.1

3.4 0.6 4.5 0.8 2 0.6 8.2 0.9 2.8 0.8 1.5 0.7 2.3 0.7 1.9 0.8

70.1 0.6 77.7 0.8 48.8 0.6 65.4 0.9 55.5 0.8 55.3 0.7 58 0.7 80 0.8

0.41 0.26 0.48 0.31 0.28 0.26 0.53 0.35 0.32 0.33 0.64 0.29 0.39 0.27 0.69 0.33

< 0.32 0.32 < 0.39 0.39 < 0.32 0.32 < 0.43 0.43 < 0.42 0.42 < 0.37 0.37 < 0.34 0.34 < 0.41 0.41

14,300 32 6,810 3.9 3,090 3.2 8,210 4.3 5,910 4.2 1,260 3.7 6,250 3.4 2,370 4.1

19.2 0.32 25.3 0.39 14 0.32 14.2 0.43 15 0.42 21.1 0.37 16.3 0.34 29.9 0.41

6.94 0.32 8.21 0.39 4.6 0.32 5.73 0.43 5.05 0.42 10.1 0.37 6.26 0.34 12.5 0.41

26 0.32 24.5 0.39 14.4 0.32 15.4 0.43 21.3 0.42 17.2 0.37 16.5 0.34 22.4 0.41

14,900 32 18,200 39 10,500 32 14,400 43 12,500 42 23,900 37 15,100 34 27,100 41

55.5 0.6 52.8 0.8 46.4 0.6 107 0.9 47.2 0.8 5.9 0.7 38.9 0.7 8.3 0.8

5,620 32 3,070 3.9 1,960 3.2 2,680 4.3 3,000 4.2 3,500 3.7 3,670 3.4 5,160 4.1

294 3.2 406 3.9 184 3.2 235 4.3 230 4.2 420 3.7 337 3.4 589 4.1

0.23 0.03 0.1 0.03 0.08 0.03 0.18 0.03 0.07 0.03 < 0.03 0.03 0.14 0.03 < 0.03 0.03

16.1 0.32 20.3 0.39 12.3 0.32 16.5 0.43 13.2 0.42 16.2 0.37 13.9 0.34 21.6 0.41

1,940 6 1,420 8 790 6 1,060 9 984 8 2,170 7 1,160 7 3,690 8

< 1.3 1.3 < 1.5 1.5 < 1.3 1.3 < 1.7 1.7 < 1.7 1.7 < 1.5 1.5 < 1.4 1.4 < 1.6 1.6

< 0.32 0.32 < 0.39 0.39 < 0.32 0.32 < 0.43 0.43 < 0.42 0.42 < 0.37 0.37 < 0.34 0.34 < 0.41 0.41

321 6 206 8 164 6 1,110 9 176 8 290 7 134 7 249 8

< 1.3 1.3 < 1.5 1.5 < 1.3 1.3 < 1.7 1.7 < 1.7 1.7 < 1.5 1.5 < 1.4 1.4 < 1.6 1.6

29.7 0.3 30.2 0.4 19.9 0.3 24.7 0.4 26.5 0.4 31.4 0.4 27.6 0.3 37.8 0.4

63.9 0.6 67.6 0.8 56.6 0.6 26.5 0.9 52.1 0.8 33.9 0.7 44.8 0.7 49.8 0.8

mg/Kgmg/Kg mg/Kg8/25/2015

(15-17')(0-5') (15-19.5') (0-5')

8/25/2015mg/Kg mg/Kg

14B5 14B6 14B7

8/25/2015 8/25/2015mg/Kg

(15-20')

mg/Kg

(0-5')(0-5')

8/25/2015

14B8

8/25/2015 8/25/20158/25/2015mg/Kg

(20-25')


510 Driggs Avenue, Brooklyn, New YorkGround Water Analytical Results


µg/L Results RL Results RL Results RL Results RL Results RL Results RL

1,1,1,2-Tetrachlorothane 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

1,1,1-Trichloroethane 5 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

1,1,2,2-Tetrachloroethane 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

1,1,2-Trichloroethane 1 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

1,1-Dichloroethane 5 0.67 5.0 0.85 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

1,1-Dichloroethene 5 0.29 1.0 5.8 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

1,1-Dichloropropene < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

1,2,3-Trichlorobenzene < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

1,2,3-Trichloropropane 0.04 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0


1,2,4-Trimethylbenzene 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

1,2-Dibromo-3-chloropropane 0.04 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

1,2-Dibromoethane < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

1,2-Dichlorobenzene 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

1,2-Dichloroethane 0.6 < 0.60 0.60 < 0.60 0.60 < 0.60 0.60 < 0.60 0.60 < 0.60 0.60 < 0.60 0.60

1,2-Dichloropropane 0.94 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

1,3,5-Trimethylbenzene 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

1,3-Dichlorobenzene < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

1,3-Dichloropropane 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0


2,2-Dichloropropane 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

2-Chlorotoluene 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

2-Hexanone (Methyl Butyl Ketone) < 2.5 2.5 < 2.5 2.5 < 2.5 2.5 < 2.5 2.5 < 2.5 2.5 < 2.5 2.5

2-Isopropyltoluene 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

4-Chlorotoluene 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

4-Methyl-2-Pentanone < 2.5 2.5 < 2.5 2.5 < 2.5 2.5 < 2.5 2.5 < 2.5 2.5 < 2.5 2.5

Acetone 6.8 5.0 3.4 5.0 < 5.0 5.0 2.7 5.0 5.1 5.0 3.9 5.0

Acrolein < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Acrylonitrile 5 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Benzene 1 18 0.70 23 0.70 0.33 0.70 < 0.70 0.70 2.1 0.70 0.28 0.70

Bromobenzene 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Bromochloromethane 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Bromodichloromethane < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Bromoform < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Bromomethane 5 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Carbon Disulfide 60 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Carbon tetrachloride 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Chlorobenzene 5 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Chloroethane 5 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 0.31 5.0 < 5.0 5.0

Chloroform 7 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Chloromethane 60 0.74 5.0 < 5.0 5.0 < 5.0 5.0 0.76 5.0 0.63 5.0 1.1 5.0

cis-1,2-Dichloroethene 5 70 5.0 1,200 100 51 5.0 8.4 1.0 16 1.0 14 1.0

cis-1,3-Dichloropropene < 0.40 0.40 < 0.40 0.40 < 0.40 0.40 < 0.40 0.40 < 0.40 0.40 < 0.40 0.40

Dibromochloromethane < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Dibromomethane 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Dichlorodifluoromethane 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Ethylbenzene 5 < 1.0 1.0 0.66 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Hexachlorobutadiene 0.5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 0.5 0.5 < 0.5 0.5 < 0.5 0.5

Isopropylbenzene 5 0.26 1.0 0.35 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

m&p-Xylenes 5 < 1.0 1.0 0.63 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Methyl Ethyl Ketone (2-Butanone) < 2.5 2.5 < 2.5 2.5 < 2.5 2.5 < 2.5 2.5 < 2.5 2.5 < 2.5 2.5

Methyl t-butyl ether (MTBE) 10 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Methylene chloride 5 < 3.0 3.0 < 3.0 3.0 < 3.0 3.0 < 3.0 3.0 < 3.0 3.0 < 3.0 3.0

Naphthalene 10 < 1.0 1.0 3.4 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

n-Butylbenzene 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

n-Propylbenzene 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

o-Xylene 5 < 1.0 1.0 0.67 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

p-Isopropyltoluene < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

sec-Butylbenzene 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Styrene 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

tert-Butylbenzene 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Tetrachloroethene 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Tetrahydrofuran (THF) < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Toluene 5 < 1.0 1.0 1.5 1.0 2.1 1.0 0.56 1.0 < 1.0 1.0 < 1.0 1.0

trans-1,2-Dichloroethene 5 6.3 5.0 12 5.0 0.82 5.0 < 5.0 5.0 0.4 5.0 0.67 5.0

trans-1,3-Dichloropropene 0.4 < 0.40 0.40 < 0.40 0.40 < 0.40 0.40 < 0.40 0.40 < 0.40 0.40 < 0.40 0.40

trans-1,4-dichloro-2-butene 5 < 2.5 2.5 < 2.5 2.5 < 2.5 2.5 < 2.5 2.5 < 2.5 2.5 < 2.5 2.5

Trichloroethene 5 6.3 1.0 12 1.0 2.4 1.0 4 1.0 1.4 1.0 2.6 1.0

Trichlorofluoromethane 5 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Trichlorotrifluoroethane < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Vinyl Chloride 2 36 5.0 470 100 0.75 1.0 0.96 1.0 0.28 1.0 0.63 1.0

Notes:RL- Reporting LimitBold/highlighted- Indicated exceedance of the NYSDEC Groundwater Standard

9/8/2015 9/8/2015Compound

NYSDEC Groundwater Quality Standards

µg/L

9/9/2015µg/L

9/9/2015

14MW314MW1

µg/L µg/Lµg/L

14MW4

9/9/2015

14MW5 14MW6

µg/L

14MW7

9/8/2015




µg/L

Results RL Results RL Results RL Results RL Results RL Results RL

1,2,4,5-Tetrachlorobenzene - - - - - - < 0.50 0.50 < 0.50 0.50 < 0.50 0.50



1,2-Diphenylhydrazine < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0



2,4,5-Trichlorophenol - - - - - - < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

2,4,6-Trichlorophenol - - - - - - < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

2,4-Dichlorophenol - - - - - - < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

2,4-Dimethylphenol - - - - - - < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

2,4-Dinitrophenol - - - - - - < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

2,4-Dinitrotoluene 5 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

2,6-Dinitrotoluene 5 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

2-Chloronaphthalene 10 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

2-Chlorophenol - - - - - - < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

2-Methylnaphthalene < 0.05 0.05 0.12 0.05 < 0.05 0.05 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

2-Methylphenol (o-cresol) - - - - - - < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

2-Nitroaniline 5 < 20 20 < 20 20 < 20 20 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

2-Nitrophenol - - - - - - < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

3&4-Methylphenol (m&p-cresol) - - - - - - < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

3,3'-Dichlorobenzidine 5 < 20 20 < 20 20 < 20 20 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

3-Nitroaniline 5 < 20 20 < 20 20 < 20 20 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

4,6-Dinitro-2-methylphenol < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

4-Bromophenyl phenyl ether < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

4-Chloro-3-methylphenol - - - - - - < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

4-Chloroaniline 5 < 20 20 < 20 20 < 20 20 < 3.5 3.5 < 3.5 3.5 < 3.5 3.5

4-Chlorophenyl phenyl ether < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

4-Nitroaniline 5 < 20 20 < 20 20 < 20 20 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

4-Nitrophenol - - - - - - < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Acetophenone - - - - - - < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Aniline - - - - - - < 3.5 3.5 < 3.5 3.5 < 3.5 3.5

Anthracene 50 0.65 0.05 2.3 0.05 0.1 0.05 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Benzidine 5 < 18 18 < 18 18 < 18 18 < 4.5 4.5 < 4.5 4.5 < 4.5 4.5

Benzoic acid < 20 20 < 20 20 < 20 20 < 25 25 < 25 25 < 25 25

Benzyl Alcohol < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 - - - - - -

Benzyl butyl phthalate 50 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Bis(2-chloroethoxy)methane 5 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Bis(2-chloroethyl)ether 1 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Bis(2-chloroisopropyl)ether < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Carbazole - - - - - - < 25 25 < 25 25 < 25 25

Dibenzofuran 4.1 5.0 7.6 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Diethyl phthalate 50 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Dimethylphthalate 50 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Di-n-butylphthalate 50 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Di-n-octylphthalate 50 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Fluoranthene 50 0.35 0.05 2.2 0.05 < 0.05 0.05 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Fluorene 50 1.5 0.05 1.3 0.05 < 0.05 0.05 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Hexachlorobutadiene 0.5 < 0.05 0.05 < 0.05 0.05 < 0.05 0.05 < 0.40 0.40 < 0.40 0.40 < 0.40 0.40

Hexachlorocyclopentadiene 5 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Isophorone 50 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Naphthalene 10 < 0.05 0.05 1.9 0.05 0.27 0.05 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Nitrobenzene 0.4 < 0.05 0.05 < 0.05 0.05 < 0.05 0.05 < 0.10 0.10 < 0.10 0.10 < 0.10 0.10

N-Nitrosodimethylamine < 0.05 0.05 < 0.05 0.05 < 0.05 0.05 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

N-Nitrosodi-n-propylamine < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

N-Nitrosodiphenylamine 50 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Phenol - - - - - - < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Pyrene 50 0.27 0.05 1.5 0.05 0.05 0.05 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Pyridine - - - - - - < 10 10 < 10 10 < 10 10

Acenaphthene 20 6 0.05 3.8 0.05 < 0.05 0.05 < 5.0 5.0 < 5.0 5.0 < 5.0 5.0

Acenaphthylene 1.8 0.05 4.3 0.05 < 0.05 0.05 < 0.10 0.10 < 0.10 0.10 < 0.10 0.10

Benz(a)anthracene 0.002* 0.06 0.05 0.35 0.05 < 0.05 0.05 0.03 0.02 < 0.02 0.02 0.02 0.02

Benzo(a)pyrene ND < 0.02 0.02 0.29 0.02 < 0.02 0.02 0.02 0.02 < 0.02 0.02 < 0.02 0.02

Benzo(b)fluoranthene 0.002* < 0.05 0.05 0.2 0.05 < 0.05 0.05 0.02 0.02 < 0.02 0.02 < 0.02 0.02

Benzo(ghi)perylene < 0.05 0.05 0.2 0.05 < 0.05 0.05 < 0.02 0.02 < 0.02 0.02 < 0.02 0.02

Benzo(k)fluoranthene 0.002* < 0.05 0.05 0.27 0.05 < 0.05 0.05 < 0.02 0.02 < 0.02 0.02 < 0.02 0.02

Bis(2-ethylhexyl)phthalate 5 0.11 0.05 0.12 0.05 0.11 0.05 < 1.0 1.0 < 1.0 1.0 < 1.0 1.0

Chrysene 0.002* < 0.05 0.05 0.31 0.05 < 0.05 0.05 0.02 0.02 < 0.02 0.02 0.02 0.02

Dibenz(a,h)anthracene < 0.05 0.05 0.07 0.05 < 0.05 0.05 < 0.02 0.02 < 0.02 0.02 < 0.02 0.02

Hexachlorobenzene 0.04 < 0.02 0.02 < 0.02 0.02 < 0.02 0.02 < 0.02 0.02 < 0.02 0.02 < 0.02 0.02

Hexachloroethane 5 < 0.05 0.05 < 0.05 0.05 < 0.05 0.05 < 0.50 0.50 < 0.50 0.50 < 0.50 0.50

Indeno(1,2,3-cd)pyrene 0.002* < 0.05 0.05 0.18 0.05 < 0.05 0.05 < 0.02 0.02 < 0.02 0.02 < 0.02 0.02

Phenanthrene 50 0.13 0.05 0.95 0.05 < 0.05 0.05 < 0.10 0.10 < 0.10 0.10 < 0.10 0.10

Pentachloronitrobenzene - - - - - - < 0.10 0.10 < 0.10 0.10 < 0.10 0.10

Pentachlorophenol - - - - - - < 1.0 1.0 < 0.80 0.80 < 0.80 0.80

Notes:RL- Reporting LimitBold/highlighted- Indicated exceedance of the NYSDEC Groundwater Standard

Bold/highlighted- Indicated exceedance of the NYSDEC Groundwater Guidance Value

* Guidance value

NYSDEC Ambient WaterQuality Standards

TOGS 1.1.1µg/L µg/L µg/L

9/8/2015 9/8/2015 9/8/2015

14MW4 14MW5 14MW6 14MW7

µg/L

Compound14MW3

µg/L

14MW1

µg/L

9/9/2015 9/9/2015 9/9/2015



Pesticides PCBs

µg/L


PCB-1016 0.09 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050

PCB-1221 0.09 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050

PCB-1232 0.09 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050

PCB-1242 0.09 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050

PCB-1248 0.09 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050

PCB-1254 0.09 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050

PCB-1260 0.09 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050

PCB-1262 0.09 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050

PCB-1268 0.09 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050 < 0.050 0.050

4,4-DDD 0.3 < 0.010 0.010 < 0.010 0.010 < 0.020 0.020 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010

4,4-DDE 0.2 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010

4,4-DDT 0.11 < 0.010 0.010 < 0.015 0.015 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010

a-BHC 0.94 < 0.005 0.005 < 0.005 0.005 < 0.005 0.005 < 0.005 0.005 < 0.005 0.005 < 0.005 0.005

a-Chlordane < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010

Alachlor < 0.075 0.075 < 0.075 0.075 < 0.075 0.075 < 0.075 0.075 < 0.075 0.075 < 0.075 0.075

Aldrin < 0.003 0.003 < 0.005 0.005 < 0.002 0.002 < 0.003 0.003 < 0.003 0.003 < 0.003 0.003

b-BHC 0.04 < 0.015 0.015 < 0.015 0.015 < 0.015 0.015 < 0.015 0.015 < 0.015 0.015 < 0.015 0.015

Chlordane 0.05 < 0.10 0.10 < 0.10 0.10 < 0.10 0.10 < 0.05 0.05 < 0.05 0.05 < 0.05 0.05

d-BHC 0.04 < 0.005 0.005 < 0.020 0.020 < 0.005 0.005 < 0.005 0.005 < 0.005 0.005 < 0.005 0.005

Dieldrin 0.004 < 0.015 0.015 < 0.015 0.015 < 0.008 0.008 < 0.004 0.004 < 0.004 0.004 < 0.004 0.004

Endosulfan I < 0.080 0.080 < 0.015 0.015 < 0.015 0.015 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010

Endosulfan II < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010

Endosulfan Sulfate < 0.010 0.010 < 0.010 0.010 < 0.015 0.015 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010

Endrin < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010

Endrin aldehyde 5 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010

Endrin ketone < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010

gamma-BHC 0.05 < 0.016 0.016 < 0.005 0.005 < 0.010 0.010 < 0.011 0.011 < 0.011 0.011 < 0.011 0.011

g-Chlordane < 0.010 0.010 < 0.015 0.015 < 0.015 0.015 < 0.016 0.016 < 0.016 0.016 < 0.016 0.016

Heptachlor 0.04 < 0.010 0.010 < 0.060 0.060 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010

Heptachlor epoxide 0.03 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010 < 0.010 0.010

Methoxychlor 35 < 0.10 0.10 < 0.10 0.10 < 0.10 0.10 < 0.10 0.10 < 0.10 0.10 < 0.10 0.10

Toxaphene < 0.25 0.25 < 0.25 0.25 < 0.25 0.25 < 0.25 0.25 < 0.25 0.25 < 0.25 0.25

Notes:

RL- Reporting limit

ND - Non-detect

Bold/highlighted- Indicated exceedance of the NYSDEC Groundwater Standard

µg/L

9/9/2015µg/L µg/L

14MW7

µg/L

9/8/2015 9/8/2015 9/8/2015

14MW5 14MW6

ND* - Due to matrix interference from non target compounds in the sample an elevated RL was reported.

Compound


14MW1 14MW3 14MW4

9/9/2015 9/9/2015µg/Lµg/L



Total Metals

mg/L


Aluminum NS 0.048 0.010 1.5 0.010 0.492 0.010 1.65 0.010 9.02 0.010 1.84 0.010

Antimony 0.003 < 0.002 0.002 < 0.002 0.002 < 0.002 0.002 < 0.002 0.002 < 0.002 0.002 < 0.002 0.002

Arsenic 0.025 0.01 0.004 0.005 0.004 0.003 0.004 0.004 0.004 0.007 0.004 0.001 0.004

Barium 1 0.087 0.010 0.084 0.010 0.021 0.010 0.02 0.010 0.071 0.010 0.025 0.010

Beryllium 0.003 < 0.001 0.001 < 0.001 0.001 < 0.001 0.001 < 0.001 0.001 < 0.001 0.001 < 0.001 0.001

Cadmium 0.005 < 0.004 0.004 < 0.004 0.004 < 0.004 0.004 < 0.004 0.004 < 0.004 0.004 < 0.004 0.004

Calcium NS 80.3 0.010 65 0.010 28 0.010 26.6 0.010 6.49 0.010 12.2 0.010

Chromium 0.05 0.004 0.001 0.003 0.001 < 0.001 0.001 0.005 0.001 0.021 0.001 0.004 0.001

Cobalt NS < 0.005 0.005 < 0.005 0.005 < 0.005 0.005 < 0.005 0.005 0.006 0.005 0.002 0.005

Copper 0.2 < 0.005 0.005 0.003 0.005 0.002 0.005 0.006 0.005 0.017 0.005 0.003 0.005

Iron 0.5 2.38 0.01 2.4 0.01 0.4 0.01 2.75 0.01 12.4 0.01 2.11 0.01

Lead 0.025 0.002 0.002 0.012 0.002 0.004 0.002 0.006 0.002 0.006 0.002 < 0.002 0.002

Magnesium 35 18.8 0.01 22 0.01 6.05 0.01 2.03 0.01 5.69 0.01 6.26 0.01

Manganese 0.3 0.38 0.005 0.285 0.005 0.152 0.005 0.358 0.005 0.468 0.005 0.496 0.005

Mercury 0.0007 < 0.0002 0.0002 < 0.0002 0.0002 < 0.0002 0.0002 < 0.0002 0.0002 < 0.0002 0.0002 < 0.0002 0.0002

Nickel 0.1 0.002 0.004 0.003 0.004 0.003 0.004 0.006 0.004 0.017 0.004 0.005 0.004

Potassium NS 10.9 0.1 11.1 0.1 6.1 0.1 3.5 0.1 6.7 0.1 8.1 0.1

Selenium 0.01 < 0.002 0.002 < 0.002 0.002 < 0.002 0.002 < 0.002 0.002 < 0.002 0.002 < 0.002 0.002

Silver 0.05 < 0.005 0.005 < 0.005 0.005 < 0.005 0.005 < 0.005 0.005 < 0.005 0.005 < 0.005 0.005

Sodium 2 110 1.0 84.1 1.0 58.7 1.0 9.2 0.1 75.5 1.0 68.6 1.0

Thallium 0.0005 < 0.001 0.001 < 0.001 0.001 < 0.001 0.001 < 0.0005 0.0005 < 0.0005 0.0005 < 0.0005 0.0005

Vanadium NS < 0.010 0.010 0.003 0.010 0.008 0.010 0.005 0.010 0.022 0.010 0.006 0.010

Zinc 2 < 0.010 0.010 0.006 0.010 < 0.010 0.010 0.006 0.010 0.025 0.010 0.003 0.010

Notes:

RL- Reporting limit

NS - No Standard


mg/L

9/9/2015 9/9/2015mg/L

9/8/2015mg/L mg/Lmg/L

Compound


14MW1 14MW4

mg/L

14MW3

9/9/2015 9/8/2015 9/8/2015

14MW5 14MW6 14MW7



Dissolved Metals

mg/L

Results RL Results RL Results RL

Aluminum NS < 0.011 0.011 0.007 0.011 0.14 0.011

Antimony 0.003 < 0.003 0.003 < 0.003 0.003 < 0.003 0.003

Arsenic 0.025 0.004 0.003 < 0.003 0.003 < 0.003 0.003

Barium 1 0.07 0.011 0.064 0.011 0.016 0.011

Beryllium 0.003 < 0.001 0.001 < 0.001 0.001 < 0.001 0.001

Cadmium 0.005 < 0.004 0.004 < 0.004 0.004 < 0.004 0.004

Calcium NS 72.4 0.01 56 0.01 25.4 0.01

Chromium 0.05 0.001 0.001 < 0.001 0.001 < 0.001 0.001

Cobalt NS < 0.005 0.005 < 0.005 0.005 < 0.005 0.005

Copper 0.2 < 0.005 0.005 < 0.005 0.005 < 0.005 0.005

Iron 0.5 0.04 0.01 0.05 0.01 0.02 0.01

Lead 0.025 0.003 0.002 0.002 0.002 0.001 0.002

Magnesium 35 16.8 0.01 19 0.01 5.37 0.01

Manganese 0.3 0.349 0.005 0.23 0.005 0.112 0.005

Mercury 0.0007 0.0002 0.0002 < 0.0002 0.0002 < 0.0002 0.0002

Nickel 0.1 < 0.004 0.004 < 0.004 0.004 < 0.004 0.004

Potassium NS 10.7 0.1 11.5 0.1 6 0.1

Selenium 0.01 < 0.004 0.004 < 0.004 0.004 < 0.004 0.004

Silver 0.05 < 0.005 0.005 < 0.005 0.005 < 0.005 0.005

Sodium 2 103 1.1 76.5 1.1 55.4 1.1

Thallium 0.0005 < 0.001 0.001 < 0.001 0.001 < 0.001 0.001

Vanadium NS < 0.011 0.011 < 0.011 0.011 0.005 0.011

Zinc 2 < 0.011 0.011 < 0.011 0.011 < 0.011 0.011

Notes:

RL- Reporting limit

NS - No Standard


mg/L

9/9/2015 9/9/2015 9/9/2015Compound


14MW1 14MW3 14MW4

mg/L mg/L


510 Driggs Avenue, Brooklyn, New YorkAnalytical Results

Soil Gas - Volatile Organic Compounds

(µg/m3) (a) (µg/m3) (b)Result RL Result RL Result RL Result RL Result RL Result RL Result RL

1,1,1,2-Tetrachloroethane < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

1,1,1-Trichloroethane 100 <2.0 - 2.8 13.8 1.00 86.2 1.00 7.36 1.00 1.07 1.00 2.02 1.00 2.74 1.00 2.21 1.00

1,1,2,2-Tetrachloroethane <1.5 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

1,1,2-Trichloroethane <1.0 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

1,1-Dichloroethane <1.0 < 1.00 1.00 4.77 1.00 2.51 1.00 58.2 1.00 54.6 1.00 < 1.00 1.00 25.2 1.00

1,1-Dichloroethene <1.0 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 44.4 1.00 1,100 74.9 < 1.00 1.00 586 74.9

1,2,4-Trichlorobenzene NA < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

1,2,4-Trimethylbenzene <1.0 2.05 1.00 2.67 1.00 2.52 1.00 1.46 1.00 1.72 1.00 2.23 1.00 1.89 1.00

1,2-Dibromoethane <1.5 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

1,2-Dichlorobenzene <2.0 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

1,2-Dichloroethane <1.0 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

1,2-Dichloropropane < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

1,2-Dichlorotetrafluoroethane < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

1,3,5-Trimethylbenzene <1.0 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

1,3-Butadiene NA < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

1,3-Dichlorobenzene <2.0 9.31 1.00 11 1.00 16.6 1.00 9.01 1.00 5.62 1.00 7.93 1.00 5.57 1.00

1,4-Dichlorobenzene NA < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

1,4-Dioxane < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

2-Hexanone 113 1.00 148 40.0 102 1.00 107 1.00 < 1.00 1.00 80.2 1.00 67.5 1.00

4-Ethyltoluene NA < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

4-Isopropyltoluene < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

4-Methyl-2-pentanone 10.4 1.00 10.4 1.00 9.13 1.00 6.1 1.00 < 1.00 1.00 13.8 1.00 9.62 1.00

Acetone NA 1,550 39.9 2,920 39.9 1,580 39.9 1,370 29.9 1,410 75.0 1,650 32.0 1,510 75.0

Acrylonitrile < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

Benzene <1.6 - 4.7 2.93 1.00 6.93 1.00 2.26 1.00 79.5 1.00 1,240 75.0 6.61 1.00 390 75.0

Benzyl Chloride NA < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

Bromodichloromethane <5.0 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

Bromoform <1.0 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

Bromomethane <1.0 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

Carbon Disulfide NA 1.02 1.00 1.75 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 1.1 1.00 < 1.00 1.00

Carbon Tetrachloride 5 <3.1 0.33 0.25 0.35 0.25 0.57 0.25 < 0.25 0.25 < 0.25 0.25 0.26 0.25 < 0.25 0.25

Chlorobenzene <2.0 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

Chloroethane NA < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 245 74.9 < 1.00 1.00 33.2 1.00

Chloroform <2.4 84.4 1.00 165 1.00 10.3 1.00 2.53 1.00 < 1.00 1.00 8.44 1.00 1.73 1.00

Chloromethane <1.0 - 1.4 < 1.00 1.00 2.33 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 1.4 1.00

cis-1,2-Dichloroethene <1.0 5.43 1.00 452 40.0 31.7 1.00 3,140 30.0 44,400 1,500 5.27 1.00 4,200 74.9

cis-1,3-Dichloropropene NA < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

Cyclohexane NA < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 8.6 1.00 396 75.0 < 1.00 1.00 172 75.0

Dibromochloromethane <5.0 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

Dichlorodifluromethane NA 75.1 1.00 32.8 1.00 152 1.00 140 1.00 90.9 1.00 25.8 1.00 47 1.00

Ethanol 138 1.00 215 1.00 169 1.00 104 1.00 97.9 1.00 178 1.00 84 1.00

Ethyl Acetate NA 2.3 1.00 7.02 1.00 1.82 1.00 < 1.00 1.00 2.36 1.00 < 1.00 1.00 < 1.00 1.00

Ethylbenzene <4.3 4.69 1.00 5.12 1.00 5.08 1.00 2.84 1.00 4.86 1.00 5.82 1.00 4.34 1.00

Heptane NA 5.98 1.00 13.9 1.00 4.26 1.00 7.09 1.00 9.71 1.00 7.04 1.00 < 1.00 1.00

Hexachlorobutadiene NA < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

Hexane <1.5 4.97 1.00 11.9 1.00 3.8 1.00 12.2 1.00 722 75.0 6.52 1.00 262 75.0

Isopropylalcohol NA 28.7 1.00 75.4 1.00 27 1.00 35.9 1.00 19.6 1.00 36.8 1.00 20.9 1.00

Isopropylbenzene < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 2.36 1.00 < 1.00 1.00 < 1.00 1.00

Xylene (m&p) <4.3 17 1.00 18.3 1.00 19.4 1.00 10.1 1.00 16.4 1.00 21.2 1.00 11.5 1.00

Methyl Ethyl Ketone 327 40.1 796 40.1 318 40.1 304 30.1 < 1.00 1.00 469 32.1 162 74.9

MTBE NA < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

Methylene Chloride <3.4 1.19 1.00 4.3 1.00 < 1.00 1.00 1.82 1.00 < 1.00 1.00 < 1.00 1.00 20 1.00

n-Butylbenzene < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

Xylene (o) <4.3 7.51 1.00 7.68 1.00 8.42 1.00 5.21 1.00 10.2 1.00 8.46 1.00 6.94 1.00

Propylene NA 71.9 40.1 104 40.1 83.8 40.1 390 29.9 3,780 75.0 79.8 32.0 5,610 150

sec-Butylbenzene < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

Styrene <1.0 < 1.00 1.00 1.08 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

Tetrachloroethene 100 30 0.25 113 0.25 25.6 0.25 7.25 0.25 8.74 0.25 4.74 0.25 23.4 0.25

Tetrahydrofuran NA < 1.00 1.00 1.69 1.00 4.13 1.00 2.63 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

Toluene 1.0 - 6.1 7.34 1.00 17.6 1.00 6.36 1.00 5.27 1.00 30.5 1.00 7.76 1.00 11.3 1.00

trans-1,2-Dichloroethene NA < 1.00 1.00 13.7 1.00 3.48 1.00 64.6 1.00 1,380 74.9 < 1.00 1.00 128 1.00

trans-1,3-Dichloropropene NA < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

Trichloroethene 5 <1.7 2,910 9.99 16,900 25.0 1,840 9.99 1,330 7.52 5,690 18.7 763 8.00 6,120 18.7

Trichlorofluoromethane NA 249 40.0 62.9 1.00 691 40.0 14.4 1.00 19.9 1.00 183 1.00 14.1 1.00

Trichlorotrifluoroethane < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00

Vinyl Chloride <1.0 0.82 0.25 < 0.25 0.25 < 0.25 0.25 3,240 18.8 116,000 376 < 0.25 0.25 10,800 37.6

BTEXTotal VOCs

Notes:NA No guidance value or standard available

7781.85 167478.74 773.01 21271.4

9/8/2015 9/8/2015NYSDOH Soil Outdoor Background Levels

14SG4 14SG59/8/2015 9/8/2015 9/8/2015 9/8/2015 9/8/2015

1301.96

(a) Final Guidance for Evaluating Soil Vapor Intrusion in the State of New York. October 2006. New York State Department of Health.

14SG6 14SG7

(µg/m3) (µg/m3) (µg/m3) (µg/m3) (µg/m3) (µg/m3)

(b) NYSDOH Guidance for Evaluating Soil Vapor Intrusion in the State of New York, February 2005, Summary of Background Levels for Selected Compounds

14SG2 14SG3

4982.462552.24 21583.86

2,946 17,479 1,901

2724.05 8194.563839.75 13160.0749.85 424.08

COMPOUNDS NYSDOH Maximum Sub-Slab Value

14SG1

(µg/m3)

39.47 55.63 41.52 102.92


510 Driggs Avenue, Brooklyn, New YorkParameters Detected Above Track 1 Soil Cleanup Objectives

14B2 14B6 14B7 14B8(0-5') (10-15') (0-5') (0-5') (10-15') (15-18') (0-5') (10-15') (20-21') (0-5') (10-15') (15-19.5') (15-17') (0-5') (0-5')

8/25/2015 8/25/2015 8/25/2015 8/25/2015 8/25/2015 8/25/2015 8/25/2015 8/25/2015 8/25/2015 8/25/2015 8/25/2015 8/25/2015 8/25/2015 8/25/2015 8/25/2015

Sample Results in ug/kg

1,2,4-Trimethylbenzene 14,000-27,000 2 - - - - 14,000 - - - 27,000 - - - - - -

1,3,5-Trimethylbenzene 9,600-16,000 2 - - - - 9,600 - - - 16,000 - - - - - -

Benzene 160-8,600 5 - - - - 4,100 2,800 - - 8,600 - - 160 890 - -

cis-1,2-Dichloroethene 570-8,700 5 - - - - 870 7,600 - 570 730 - - - 8,700 - -

Ethylbenzene 7,000-21,000 2 - - - - 7,000 - - - 21,000 - - - - - -

m&p-Xylenes 270-62,000 4 - - - - 17,000 820 - - 62,000 - - - 270 - -

Methylene chloride 570 1 - - - - - - - - - - - - 570 - -

Naphthalene 300,000-620,000 2 - - - - 300,000 - - - 620,000 - - - - - -

o-Xylene 9,200-21,000 2 - - - - 9,200 - - - 21,000 - - - - - -

Toluene 8,600-22,000 2 - - - - 8,600 - - - 22,000 - - - - - -

Trichloroethene 3,300-14,000 3 - - - - 3,300 3,700 - - - - - - 14,000 - -

Vinyl Chloride 290-2,600 3 - - - - 290 2,600 - - - - - - 1,100 - -


Benz(a)anthracene 1,100-41,000 10 3,500 16,000 - - - 14,000 - 1,800 41,000 - 2,700 8,000 6,300 1,200 1,100Benzo(a)pyrene 2,100-28,000 8 3,200 13,000 - - - 13,000 - 3,600 28,000 - 3,000 14,000 2,100 - -

Benzo(b)fluoranthene 1,100-21,000 9 4,500 11,000 - - - 9,900 - 2,300 21,000 - 2,200 9,700 8,800 1,100 -Benzo(k)fluoranthene 850-26,000 12 3,400 10,000 - 850 - 10,000 - 2,900 26,000 870 2,700 6,500 4,600 960 980Chrysene 1,100-38,000 10 3,300 16,000 - - - 13,000 - 1,800 38,000 - 2,600 8,200 6,100 1,400 1,100Dibenz(a,h)anthracene 440-3,800 8 1,400 1,300 - - - 2,000 - 500 3,800 - 440 4,200 1,900 - -

Dibenzofuran 12,000-43,000 2 - - - - - 12,000 - - 43,000 - - - - - -

Fluorene 66,000 1 - - - - - - - - 66,000 - - - - - -

Indeno(1,2,3-cd)pyrene 570-11,000 13 3,900 7,200 570 600 - 6,400 - 3,400 11,000 710 1,600 7,400 6,200 720 680Naphthalene 43,000-190,000 2 - - - - - 43,000 - - 190,000 - - - - - -

Phenanthrene 140,000 1 - - - - - - - - 140,000 - - - - - -


4,4' -DDD 4.3 1 - - - - - - 4.3 - - - - - - - -

4,4' -DDE 4-8.1 2 - - 8.1 - - - 4 - - - - - - - -

4,4' -DDT 7.1 1 - - 7.1 - - - - - - - - - - - -

a-Chlordane 110-170 3 - - 110 130 - - - - 170 - - - - - -

Chlordane 120-1,300 7 510 - 970 1,300 - - 120 - 650 - - - - 320 220Dieldrin 9.4-13 2 - - 9.4 - - - - - - - - - - 13 -

Sample Results in mg/kg

Chromium 31.3 1 31.3 - - - - - - - - - - - - - -

Lead 79.2-121 4 102 - - - - 121 79.2 - - - - - 107 - -

Mercury 0.19-0.58 4 0.58 - 0.19 - - 0.41 - - - 0.23 - - - - -

Nickel 36.3 1 36.3 - - - - - - - - - - - - - -


RL - Laboratory Reporting Limit



14B3 14B4 14B5COMPOUND

Range in Exceedances

Frequency of Detection

14B1


510 Driggs Avenue, Brooklyn, New YorkParameters Detected Above Ambient Groundwater Standards

14MW1 14MW3 14MW4 14MW5 14MW6 14MW7

9/29/2015 9/30/2015 9/30/2015 9/8/2015 9/8/2015 9/8/2015

Sample Results in ug/kL

1,1-Dichloroethene 5.8 1 - 5.8 - - - -

Benzene 2.1 - 23 3 18 23 - - 2.1 -

cis-1,2-Dichloroethene 8.4 - 1,200 7 70 1,200 51 8.4 16 14trans-1,2-Dichloroethene 6.3 - 12 2 6.3 12 - - - -

Trichloroethene 6.3 - 12 2 6.3 12 - - - -

Vinyl Chloride 36 - 470 2 36 470 - - - -

Sample Results in ug/L

Benz(a)anthracene 0.02 - 0.35 3 - 0.35 - 0.03 - 0.02Benzo(a)pyrene 0.02 1 - - - 0.02 - -

Benzo(b)fluoranthene 0.02 - 0.2 2 - 0.2 - 0.02 - -

Benzo(k)fluoranthene 0.27 1 - 0.27 - - - -

Chrysene 0.02 - 0.31 4 - 0.31 - 0.02 - 0.02Indeno(1,2,3-cd)pyrene 0.18 1 - 0.18 - - - -

Sample Results in mg/L

Iron 0.75 - 12.4 6 2.38 2.4 - 2.75 12.4 2.11Manganese 0.315 - 0.496 5 0.38 - - 0.358 0.468 0.496Sodium 58.7 - 110 5 110 84.1 58.7 - 75.5 68.6Manganese (dissolved) 0.349 1 0.349 - - - - -

Sodium (dissolved) 55.4-110 3 110 76.5 55.4 - - -


RL - Laboratory Reporting Limit


COMPOUNDRange in

ExceedancesFrequency of

Detection

FIGURES

SITE LOCATION

EEBBCCEnvironmental Business Consultants

Phone 631.504.6000Fax 631. 924 .2870

FORMER STERLING TRANSFORMER CORP.

FIGURE 1 Site Location Map

USGS Brooklyn Quadrangle 1995, Contour Interval = 10 feet

510 DRIGGS AVENUE, BROOKLYN, NY

KEY:

150BCP Property Boundary

SIDEWALK

Lot 1

DR

IGG

S A

VE

NU

E

SCALE:

30

Scale: 1 inch = 30 feet

N. 8th STREET

Lot 22

N. 9th STREET

Approx. Location of USTon 1942 Sanborn Map

Parking Lot Surface Drains

100'

175'

Lot 20

Lot 30

SIDEWALK


Phone 631.504.6000Fax 631. 924 .2870

Site Plan

Site Name:

Site Address:

Drawing Title:

FORMER STERLING TRANSFORMER CORP.Figure No.2 510 Driggs Avenue, Brooklyn, NY

KEY:


SIDEWALK

Lot 1

DR

IGG

S A

VE

NU

E

SCALE:

30


N. 8th STREET

Lot 22

N. 9th STREET

Lot 20

Lot 30

SIDEWALK

Sept 2014 Phase II Boring Location

B4

B3

B1

B2

Bx

14BxAug2015 Boring Location

14B4

14B8

14B2

14B1

14B3

14B7

14B614B5


Phone 631.504.6000Fax 631. 924 .2870

Soil Boring Locations

Site Name:

Site Address:

Drawing Title:


KEY:


SIDEWALK

Lot 1

DR

IGG

S A

VE

NU

E

SCALE:

30


N. 8th STREET

Lot 22

N. 9th STREET

Lot 20

Lot 30

SIDEWALK

GW4

GW3

GW1

14MW1

14MW6

14MW5

14MW2

14MW3

14MW7

14MW4

Sept 2014 Phase II GW Sampling LocationGWx

14MWxAug2015 MW Location


Phone 631.504.6000Fax 631. 924 .2870

Monitoring Well Locations

Site Name:

Site Address:

Drawing Title:


KEY:


SCALE:

25

Scale: 1 inch = 25 feetSept 2014 Phase II GW Sampling LocationGWx

14MWxMonitoring Well Location

SIDEWALK

Lot 1

DR

IGG

S A

VE

NU

E

N. 8th STREET

Lot 22

Lot 20

Lot 30

GW4

GW3

GW1

14MW1

14MW6

14MW5

14MW2

14MW3

14MW7

14MW4

83.75

83.73

83.37

83.07

83.27

83.36

83.73

83.383

.5

83.7

83 73


Phone 631.504.6000Fax 631. 924 .2870

Ground Water Elevation Map

Site Name:

Site Address:

Drawing Title:


KEY:


SIDEWALK

Lot 1

DR

IGG

S A

VE

NU

E

SCALE:

30


N. 8th STREET

Lot 22

N. 9th STREET

100'

175'

Lot 20

Lot 30

SIDEWALK

Soil Gas Location14SGx

14SG1 14SG2

14SG6

14SG3

14SG7

14SG5

14SG4


Phone 631.504.6000Fax 631. 924 .2870

Soil Gas Locations

Site Name:

Site Address:

Drawing Title:


KEY:


SIDEWALK

Lot 1 DR

IGG

S A

VE

NU

E

SCALE:

40


N. 8th STREET

Lot 22

Sept 2014 Phase II Boring Location

B4

B3

B1

B2

Bx

14BxAug2015 Boring Location

14B4

14B8

14B2

14SB1

14B3

14B7

14B614B5

1,2,4-Trimethylbenzene 21,000

Benz(a)anthracene 3,500


Indeno(1,2,3-cd)pyrene 5701,3,5-Trimethylbenzene 12,000

Benzo(a)pyrene 3,200


4,4' -DDE 8.1Benzene 43,000

Benzo(b)fluoranthene 4,500


Chromium* 31.3Ethylbenzene 9,200

Benzo(k)fluoranthene 3,400


Lead* 102m&p-Xylenes 82,000

Chrysene 3,300

Chrysene 16,000

Mercury* 0.58Methylene chloride 5,600

Dibenz(a,h)anthracene 1,400


Nickel* 36.3Naphthalene 880,000

Indeno(1,2,3-cd)pyrene 3,900


o-Xylene 18,000

Chlordane 510

Toluene 91,000

3&4-Methylphenol 53,000

Acenaphthene 49,000

Acenaphthylene 170,000

Anthracene 190,000





Chrysene 120,000

Dibenzofuran 170,000

Fluoranthene 330,000

Fluorene 240,000


Naphthalene 1,100,000

Phenanthrene 660,000

Pyrene 280,000

Lead* 84.7

B3 (18-20') 9/30/14

14B1

14B1

(0-5') 8/25/15

(10-15') 8/25/15

14B2 (0-5') 8/25/15

4,4' -DDT 7.1

a-Chlordane 110

Chlordane 970

Dieldrin 9.4

Mercury* 0.19

Benzo(k)fluoranthene 870


Benzene 160

Indeno(1,2,3-cd)pyrene 710



Mercury* 0.23



Chlordane 650



Chrysene 2,600


Dibenz(a,h)anthracene 440

Chrysene 8,200





Benzo(k)fluoranthene 980Chrysene 1,100

Indeno(1,2,3-cd)pyrene 680Chlordane 220

14B2 (20-25') 8/25/15

14B5 (0-5') 8/25/15

14B5 (10-15') 8/25/15

14B5 (15-19.5') 8/25/15

14B8 (0-5') 8/25/15



Benzene 2,800

4,4' -DDD 4.3



cis-1,2-Dichloroethene 7,600

Mercury* 0.41

a-Chlordane 130

Benzene 4,100

m&p-Xylenes 820

cis-1,2-Dichloroethene 870

Trichloroethene 3,700

Ethylbenzene 7,000

Vinyl Chloride 2,600

m&p-Xylenes 17,000


Naphthalene 300,000


Toluene 8,600




Vinyl Chloride 290

Chrysene 13,000


Dibenzofuran 12,000


Naphthalene 43,000

Lead* 121

Chlordane 1,300


Benz(a)anthracene 1,800Benzo(a)pyrene 3,600

Benzo(b)fluoranthene 2,300Benzo(k)fluoranthene 2,900

Chrysene 1,800

Dibenz(a,h)anthracene 500Indeno(1,2,3-cd)pyrene 3,400

o-Xylene 21,000




Chrysene 38,000


Dibenzofuran 43,000

Fluorene 66,000


Naphthalene 190,000

Phenanthrene 140,000

a-Chlordane 170

4,4' -DDE 4

Chlordane 120

Lead* 79.2

Benzene 890


Dieldrin 13



m&p-Xylenes 270


Methylene chloride 570

Chrysene 1,400




Chlordane 320


Benzo(b)fluoranthene 8,800Benzo(k)fluoranthene 4,600

Chrysene 6,100Dibenz(a,h)anthracene 1,900

Indeno(1,2,3-cd)pyrene 6,200Lead* 107

14B3 (0-5') 8/25/15

14B3 (10-15') 8/25/15

14B3 (15-18') 8/25/15

14B4 (0-5') 8/25/15

14B4 (10-15') 8/25/15

14B6 (15-17') 8/25/15

14B7 (0-5') 8/25/15

14B7 (15-20') 8/25/15

Lead* 89.1

Mercury* 0.19

B4 (23-25') 9/30/14

o-Xylene 9,200



Benzene 8,600


Ethylbenzene 21,000

m&p-Xylenes 62,000

Naphthalene 620,000

14B4 (20-21') 8/25/15

Toluene 22,000

Note: All parameters except metals are in ug/kg

*Metals are reported in mg/kg

Exceeds Unrestricted SCOs

Exceeds Restricted Residneital SCOs


Phone 631.504.6000Fax 631. 924 .2870

Soil Exceedences

Site Name:

Site Address:

Drawing Title:


Geologic Cross SectionEEBBCC

Environmental Business Consultants Phone: 631.504.6000 FIGURE 8

South

Existing Grade

Silty Clay

A A'

North

1 Inch = 20 Feet

0

SCALE

10 40None

Vertical

Exageration

Non-Native Fill

14B8 14B2

PID 350

14B6

5

10

15

20

25

30

35

Silty Sand

20

B3 14B3 14B4

PID 0.0

PID 0.0

PID 0.0

PID 0.0

PID 0.0

PID 0.0

PID 0.0

PID 0.0

PID 0.0

PID 0.0

PID 0.0

PID 5.0

PID 0.0

PID 0.0

PID 90

W / Strong Petro Odor3" Black Fine Sand

PID 0.0

PID 0.0

PID 15020" Black Fine SandW / Strong Petro OdorPID 30

PID 0.0

PID 0.0

PID 5520" Black Fine SandW / Petro OdorPID 2534" Black Fine SandW / Petro Odor

PID 0.0

PID 0.0

PID 31520" Black Fine Sand, StrongPetro Odor,Pockets of fuel oil sheen

PID 15038" Black Fine SandW / Petro Odor

PID 25Slight Petro Odor

Water Table

Planned Building Excavation Depth

1808 Middle Country Road. Ridge. NY 11961 Fax: 631.924.2780

Former Universal Transformer Corp.

510 Driggs Avenue, Brooklyn, NY

150

SIDEWALK

Lot 1

DR

IGG

S A

VE

NU

E

SCALE:

35


N. 8th STREET

Lot 22

N. 9th STREET

SIDEWALK

GW4

GW3

GW1

14MW1

14MW6

14MW5

14MW2

14MW3

14MW7

14MW4


1,2,4-Trimethylbenzene 380


Benzene 18

1,1-Dichloroethene 5.8

cis-1,2-Dichloroethene

Trichloroethene 18




Benzene 23

Sodium

Vinyl Chloride 2.5

Benzene 4,300

Benzene 730

6.3



Ethylbenzene 270

Trichloroethene 6.3

trans-1,2-Dichloroethene 12

Ethylbenzene 350

Isopropylbenzene 15

Vinyl Chloride 36

Trichloroethene 12

m&p-Xylenes 1,600

m&p-Xylenes 520Iron 2.38

Vinyl Chloride 470

Methylene chloride 16

Naphthalene 2,000Manganese 0.38

Benz(a)anthracene 0.35

Naphthalene 9,400

o-Xylene 230Sodium 110

Benzo(b)fluoranthene 0.2

o-Xylene 570

Styrene 13

Benzo(k)fluoranthene 0.27

Styrene 270

Toluene 630

Chrysene 0.31

Toluene 3,800

Vinyl Chloride 4.3

Indeno(1,2,3-cd)pyrene 0.18

Trichloroethene 27

Iron 2.4

Vinyl Chloride 530

Sodium 84.1

trans-1,2-Dichloroethene

51

58.7

VOCs (ug/L)

VOCs (ug/L)

VOCs (ug/L)

VOCs (ug/L)

VOCs (ug/L)

VOCs (ug/L)

SVOCs (ug/L)

Metals (mg/L)

Metals (mg/L)

Metals (mg/L)

GW1 9/30/14

GW3 9/30/14

GW4 9/30/14

14MW1 9/9/15

14MW3 9/9/15

14MW4 9/9/15

cis-1,2-Dichloroethene 8.4

Benzene 2.1





Benzo(a)pyrene 0.02

Aluminum 9.02

Chrysene 0.02

Benzo(b)fluoranthene 0.02

Iron 12.4

Chrysene 0.02

Manganese 0.468

Aluminum 1.84

Sodium 75.5

Iron 2.11

Aluminum 1.65

Manganese 0.496

Iron 2.75

Sodium 68.6

Manganese 0.358

14MW5 9/8/15

14MW6 9/8/15

14MW7 9/8/15

Metals (mg/L)

Metals (mg/L)

Metals (mg/L)

VOCs (ug/L)

VOCs (ug/L)

VOCs (ug/L)

SVOCs (ug/L)

SVOCs (ug/L)

KEY:

BCP Property Boundary

Sept 2014 Phase II GW Sampling LocationGWx

14MWxAug2015 MW Location

Anticipated Maximum Extent of NAPL(Apparent thickness < 6 inches)


Phone 631.504.6000Fax 631. 924 .2870

Groundwater Exceedences

Site Name:

Site Address:

Drawing Title:


KEY:


SIDEWALK

Lot 1

DR

IGG

S A

VE

NU

E

SCALE:

30


N. 8th STREET

Lot 22

N. 9th STREET

SIDEWALK

Soil Gas Location14SGx

14SG1 14SG2

14SG6

14SG3

14SG7

14SG5

14SG4

1,1,1-Trichloroethane 13.8




1,2,4-Trimethylbenzene 2.05

1,1-Dichloroethane 4.77



1,3-Dichlorobenzene 9.31



1,1-Dichloroethene 44.4

2-Hexanone 113

1,3-Dichlorobenzene 11



4-Methyl-2-pentanone 10.4

2-Hexanone 148

2-Hexanone 102


Acetone 1,550



2-Hexanone 107

Benzene 2.93

Acetone 2,920

Acetone 1,580


Carbon Disulfide 1.02

Benzene 6.93

Benzene 2.26

Acetone 1,370

Carbon Tetrachloride 0.33



Benzene 79.5

Chloroform 84.4


Chloroform 10.3

Chloroform 2.53


Chloroform 165



Dichlorodifluromethane 75.1

Chloromethane 2.33

Dichlorodifluromethane 152

Cyclohexane 8.6

Ethanol 138


Ethanol 169


Ethyl Acetate 2.3


Ethyl Acetate 1.82

Ethanol 104

Ethylbenzene 4.69

Ethanol 215

Ethylbenzene 5.08

Ethylbenzene 2.84

Heptane 5.98

Ethyl Acetate 7.02

Heptane 4.26

Heptane 7.09

Hexane 4.97

Ethylbenzene 5.12

Hexane 3.8

Hexane 12.2

Isopropylalcohol 28.7

Heptane 13.9

Isopropylalcohol 27


Xylene (m&p) 17

Hexane 11.9

Xylene (m&p) 19.4

Xylene (m&p) 10.1

Methyl Ethyl Ketone 327




Methylene Chloride 1.19

Xylene (m&p) 18.3

Xylene (o) 8.42


Xylene (o) 7.51


Propylene 83.8

Xylene (o) 5.21

Propylene 71.9


Tetrachloroethene 25.6

Propylene 390

Tetrachloroethene 30

Xylene (o) 7.68

Tetrahydrofuran 4.13


Toluene 7.34

Propylene 104

Toluene 6.36

Tetrahydrofuran 2.63


Styrene 1.08

trans-1,2-Dichloroethene 3.48

Toluene 5.27







1,1-Dichloroethene 1,100


1,1-Dichloroethene 586


2-Hexanone 80.2





Acetone 1,410

Acetone 1,650

2-Hexanone 67.5

Benzene 1,240

Benzene 6.61


Chloroethane 245


Acetone 1,510



Benzene 390

Cyclohexane 396

Chloroform 8.44

Chloroethane 33.2



Chloroform 1.73

Ethanol 97.9


Chloromethane 1.4

Ethyl Acetate 2.36

Ethanol 178


Ethylbenzene 4.86

Ethylbenzene 5.82

Cyclohexane 172

Heptane 9.71

Heptane 7.04


Hexane 722

Hexane 6.52

Ethanol 84



Ethylbenzene 4.34

Isopropylbenzene 2.36

Xylene (m&p) 21.2

Hexane 262

Xylene (m&p) 16.4



Xylene (o) 10.2

Xylene (o) 8.46

Xylene (m&p) 11.5

Propylene 3,780

Propylene 79.8




Methylene Chloride 20

Toluene 30.5

Toluene 7.76

Xylene (o) 6.94

trans-1,2-Dichloroethene 1,380

Trichloroethene 763

Propylene 5,610


Trichlorofluoromethane 183


Trichlorofluoromethane 19.9

Toluene 11.3

Trichlorofluoromethane 249Vinyl Chloride 0.82

Tetrachloroethene 113

Toluene1.69

trans-1,2-Dichloroethene17.6

Trichloroethene13.7

Trichlorofluoromethane16,900

Tetrahydrofuran

62.9

TrichloroetheneTrichlorofluoromethane

1,840691

trans-1,2-Dichloroethene 64.6TrichloroetheneTrichlorofluoromethane

1,33014.4



Trichloroethene 6,120Trichlorofluoromethane 14.1

trans-1,2-Dichloroethene 128


14SG2

14SG3

14SG4

14SG5

14SG6

14SG7

14SG1

*All Results in (ug/m )3


Phone 631.504.6000Fax 631. 924 .2870

Soil Gas Detections

Site Name:

Site Address:

Drawing Title:


Owner

Rectangle

Owner

Typewritten Text

10

APPENDIX – A Soil Boring Logs

Geologic Boring Log Details

Site Elevation Datum

Site Name: DTW Ground Elevation

Drilling Company: Method:C2 Environmental Geoprobe Well SpecificationsDate Started:

NACompletion Depth:15 Feet Rob Bennett

DEPTH SAMPLES(ft below Reco- Blow SOIL DESCRIPTIONgrade) very per PID

(in.) 6 in. (ppm)

0 NA

5

10

15

20

25

30

14B1 Boring LogLocation: Eastern side of the central portion of the Site Depth to Water

Address: Date

Former Sterling Transformer Corp.

510 Driggs Avenue, Brooklyn, NYGroundwater

depthApprox. 20 ft. amsl

Approx. 12 ft bgsDate Completed:

8/25/2015 8/25/2015Geologist

14B1 Boring Log

(NTS)

to40 0.0

40" FILL: Brown silty gravelly sand with asphalt and crushed rock, no odor

*Retained soil sample 14B1 (0-5')

to31 0.0

31" FILL: Brown silty gravelly sand with asphaltand red brick fragments, no odor

to38 0.0

38" FILL: Brown silty gravelly sand with asphalt

*Top 18" of recovery is dry

*Bottom 20" of recovery is saturated

*Refusal encountered at 15 ft bgs


to

to

4" Asphalt pavement

*Groundwater encountered at approximately 12 ft bgs

and red brick fragments, no odor

to

EB CEB C ENVIRONMENTAL BUSINESS CONSULTANTS







(in.) 6 in. (ppm)

0 NA

5

10

15

20

25

30

14B2 Boring LogLocation: Middle of the northern portion of the Site between two

storm drains.Depth to Water

Address: Date





8/25/2015 8/25/2015Geologist

14B2 Boring Log

(NTS)

to30 0.0

30" FILL: Brown silty gravelly sand with asphalt and red brick fragments, no odor


to38 0.0

to20 0.0

20" Brown sandy silt, no odor*Top 5" of recovery is dry





to31 0.0

31" Brown sandy silt, saturated, no odor

to36 0.0

36" Brown silt, trace fine sand, high plasticity, saturated, no odor

4" Asphalt pavement

38" FILL: Brown silty gravelly sand with asphalt and red brick fragments, no odor

to






NACompletion Depth:18.5 Feet Rob Bennett


(in.) 6 in. (ppm)

0 NA

5

10

15

20

25

30

14B3 Boring LogLocation: Slightly south of the center of the Site between two

storm drains.Depth to Water

Address: Date





8/25/2015 8/25/2015Geologist

14B3 Boring Log

(NTS)

to31 0.0

31" FILL: Brown silty gravelly sand with asphaltand red brick fragments, no odor


to36 0.0

36" FILL: Brown silty sand with asphalt andred brick fragments, no odor

to40

120 to

150

20" Brown silty gravelly sand, dry, no odor



to30

25 to 30 *Refusal at 18-18.5 ft bgs


to

4" Asphalt pavement

20" Black-stained brown silty gravelly sand, wet, strong petroleum odor

30" Black-stained brown silt/sand mixture, slight petroleum odor

to








(in.) 6 in. (ppm)

0 NA

5

10

15

20

25

30

14B4 Boring LogDepth to Water

Address: Date

Location: South side of the Site. Adjacent to the potential location of a UST and in the footprint of a former gas holder (circa 1850s).





8/25/2015 8/25/2015Geologist

14B4 Boring Log

(NTS)

to38 0.0

38" FILL: Light brown silty sand, little some gravel, asphalt and red brick fragments, no odor


to32 0.0

32" Tan sandy silt (all fines), no odor

to37

0 to

315

17" Tan sandy silt, dry, no odor20" Black-stained tan fine sandy silt, strong



*Refusal at 21 ft bgs*Retained soil sample 14B4 (20-21')

to38

120 to

150

38" Black-stained sand with some gravel, wetpetroleum odor

to12

18 to 25

12" Dark brown/tan sand, wet, slight petroleum saturated, no odor

4" Asphalt pavement

petroleum odor, pockets of separate phase fuel oil-like material, sheen, saturated

to






NACompletion Depth:19.5 Feet Rob Bennett


(in.) 6 in. (ppm)

0 NA

5

10

15

20

25

30

14B5 Boring LogLocation: Southwest corner of the Site Depth to Water

Address: Date





8/25/2015 8/25/2015Geologist

14B5 Boring Log

(NTS)

to31 0.0

31" FILL: Tan silty gravelly sand with asphalt andred brick fragments, no odor


to39 0.0

39" Tan silty fine sand, no odor

to36

0 to

270

16" Brown fine sand and silt, no odor, dry



to42

35 to 50 *Refusal at 19.5 ft bgs

*Retained soil sample 14B5 (15-19.5')

to

4" Asphalt pavement

20" Black-stained light brown fine sand and silt, saturated, petroleum odor

42" Black-stained light brown fine sand and silt, saturated, petroleum odor

to








(in.) 6 in. (ppm)

0 NA

5

10

15

20

25

30

14B6 Boring LogLocation: Southeast corner of the Site to the south of a storm

drain.Depth to Water

Address: Date





8/25/2015 8/25/2015Geologist

14B6 Boring Log

(NTS)

to28 0.0

28" FILL: Tan silty sand with asphalt and red brick fragments, no odor


to20 0.0

20" Tan silty fine sand, no odor

to38

50 to 55

18" Tan silty fine sand, dry, no odor



to34

18 to 25 *Refusal at 19 ft bgs


to

4" Asphalt pavement

20" Black-stained tan silty fine sand, petroleum odor, wet

34" Black-stained tan silty fine sand, petroleum odor

to








(in.) 6 in. (ppm)

0 NA

5

10

15

20

25

30

14B7 Boring LogLocation: East side of the central portion of the Site. Depth to Water

Address: Date





8/25/2015 8/25/2015Geologist

14B7 Boring Log

(NTS)

to32 0.0

32" FILL: Brown silty sand with asphalt and redbrick fragments, no odor


to38 0.0

38" Brown sand/silt mixture, no odor

to40 0.0

40" Brown sandy silt, no odor*Top 20" of recovery is dry




to46 0.0

*Refusal at 19.5-20' bgs


to

4" Asphalt pavement

46" Brown sandy silt with some gravel, saturated, no odor

to








(in.) 6 in. (ppm)

0 NA

5

10

15

20

25

30

14B8 Boring LogLocation: Northern corner of the Site Depth to Water

Address: Date

Approx. 20 ft. amsl

Date Completed:8/25/2015 8/25/2015



depth

Geologist

14B8 Boring Log

(NTS)

38 0.0

38" FILL: Brown silty sand with some gravel, asphalt and red brick fragments, no odor





to36 0.0

36" Brown sandy silt, no odor

42" Brown sandy silt, saturated, no odor

40 0.0

40" Brown sandy silt, little gravel, no odor*Top 20" of recovery is dry

27 0.0

27" Brown silt, trace sand, high plasticity, saturated, no odor


to

to

to

to

to

Approx. 12 ft bgs

4" Asphalt pavement

42 0.0


APPENDIX – B Monitoring Well Completion Reports

GROUNDWATER MONITORING WELL

CONSTRUCTION LOG

14MW1

Monitoring Well No.: 14MW1Protective Casing

X Flush Mount Pop-up

Project: 510 Driggs Avenue, Brooklyn NY

Bentonite Slurry

Gravel Pack Pellets Depth to Groundwater: 13.1' Date:

Gravel PackInstallation Depth: 20'

Grain Size # 00Survey Point Elevation: 97.64

Well Casing 0 - 10 ft bgsInstallation Date:

Material PVCInch Diam. 1 Drilling Contractor: C2 Environmental

Installation Method: Geoprobe10 ft

Water Removed During Development:

Well Screen 10 - 20 ft bgs

Material PVCInch Diam. 1Slot 15

x 20 ft

Note: Drawing is not to scale.Depths are given in feet below land surface.

8/26/2015

8/25/2015



CONSTRUCTION LOG

14MW2




Bentonite Slurry










x 19 ft Concrete


8/26/2015

8/25/2015



CONSTRUCTION LOG

14MW3




Bentonite Slurry










x 17 ft


8/26/2015

8/25/2015



CONSTRUCTION LOG

14MW4




Bentonite Slurry










x 20 ft


8/26/2015

8/25/2015



CONSTRUCTION LOG

14MW5




Bentonite Slurry










x 20 ft


8/26/2015

8/25/2015



CONSTRUCTION LOG

14MW6




Bentonite Slurry










x 20 ft


8/26/2015

8/25/2015



CONSTRUCTION LOG

14MW7




Bentonite Slurry










x 20 ft


8/26/2015

8/26/2015


APPENDIX - C Groundwater Sampling Logs

APPENDIX - D Soil Vapor Sampling Logs

APPENDIX - E Laboratory Reports (On Disk)

BJ89522 - BJ89528

Monday, November 02, 2015

Sample ID#s:

Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406

Project ID: 510 Driggs Avenue, Brooklyn, New York

Sincerely yours,

Laboratory DirectorPhyllis Shiller

Enclosed are revised Analysis Report pages. Please replace and discard the original pages. If you have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext. 200.

NELAC - #NY11301CT Lab Registration #PH-0618MA Lab Registration #MA-CT-007ME Lab Registration #CT-007NH Lab Registration #213693-A,B

NJ Lab Registration #CT-003NY Lab Registration #11301PA Lab Registration #68-03530RI Lab Registration #63VT Lab Registration #VT11301

This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.

This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.

A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.

587 East Middle Turnpike, P.O. Box 370, Manchester, CT 06040Telephone (860) 645-1102 Fax (860) 645-0823

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

NY ANALYTICAL SERVICES PROTOCOLDATA PACKAGE

Client: Environmental Business ConsultantsProject: 510 Driggs Avenue, Brooklyn, New York

Laboratory Project: GBJ89522

NY Analytical Services Protocol FormatNovember 02, 2015



SDG I.D.: GBJ89522

Environmental Business Consultants 510 Driggs Avenue, Brooklyn, New York

Methodology SummaryVolatiles in Air

Compendium of Methods for the Determination of Toxic Organic Compounds in Ambient Air: Method TO-15, Second Edition, U. S. Environmental Protection Agency, January 1999.

Sample Id Cross ReferenceClient Id Lab Id Matrix14SG5 BJ89522 AIR14SG7 BJ89523 AIR14SG6 BJ89524 AIR14SG1 BJ89525 AIR14SG3 BJ89526 AIR14SG4 BJ89527 AIR14SG2 BJ89528 AIR

SDG CommentsNovember 02, 2015



SDG I.D.: GBJ89522

Version 1: Analysis results minus QC and forms.

Version 3: Complete report with QC and forms.

Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

AIREBC72 Hour

09/08/15LBsee "By" below

PR

Laboratory Data

14SG5

Phoenix ID: BJ89522

09/09/1511:3717:33

Parameterppbv

ResultppbvRL

ug/m3Result Date/Time By Dilution

FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406

Analysis ReportNovember 02, 2015

Date Time



SDG ID: GBJ89522

Client ID:Project ID: 510 Driggs Avenue, Brooklyn, New York

LOD/MDL

ug/m3RL

LOD/MDL

Canister Id: 489

Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 09/12/15 K/P 1ND 10.146 1.00 1.00

0.3701,1,1-Trichloroethane 0.183 09/12/15 K/P 12.020.183 1.00 1.00ND1,1,2,2-Tetrachloroethane 0.146 09/12/15 K/P 1ND0.146 1.00 1.00ND1,1,2-Trichloroethane 0.183 09/12/15 K/P 1ND0.183 1.00 1.0013.51,1-Dichloroethane 0.247 09/12/15 K/P 154.60.247 1.00 1.002771,1-Dichloroethene 18.9 09/15/15 K/P 75110018.9 74.9 74.9DND1,2,4-Trichlorobenzene 0.135 09/12/15 K/P 1ND0.135 1.00 1.00

0.3501,2,4-Trimethylbenzene 0.204 09/12/15 K/P 11.720.204 1.00 1.00ND1,2-Dibromoethane(EDB) 0.130 09/12/15 K/P 1ND0.130 1.00 1.00ND1,2-Dichlorobenzene 0.166 09/12/15 K/P 1ND0.166 1.00 1.00ND1,2-Dichloroethane 0.247 09/12/15 K/P 1ND0.247 1.00 1.00ND1,2-dichloropropane 0.217 09/12/15 K/P 1ND0.217 1.00 1.00ND1,2-Dichlorotetrafluoroethane 0.143 09/12/15 K/P 1ND0.143 1.00 1.00ND1,3,5-Trimethylbenzene 0.204 09/12/15 K/P 1ND0.204 1.00 1.00ND1,3-Butadiene 0.452 09/12/15 K/P 1ND0.452 1.00 1.00

0.9351,3-Dichlorobenzene 0.166 09/12/15 K/P 15.620.166 1.00 1.00ND1,4-Dichlorobenzene 0.166 09/12/15 K/P 1ND0.166 1.00 1.00ND1,4-Dioxane 0.278 09/12/15 K/P 1ND0.278 1.00 1.00ND2-Hexanone(MBK) 0.244 09/12/15 K/P 1ND 10.244 1.00 1.00ND4-Ethyltoluene 0.204 09/12/15 K/P 1ND 10.204 1.00 1.00ND4-Isopropyltoluene 0.182 09/12/15 K/P 1ND 10.182 1.00 1.00ND4-Methyl-2-pentanone(MIBK) 0.244 09/12/15 K/P 1ND0.244 1.00 1.00595Acetone 31.6 09/15/15 K/P 75141031.6 75.0 75.0DSNDAcrylonitrile 0.461 09/12/15 K/P 1ND0.461 1.00 1.00387Benzene 23.5 09/15/15 K/P 75124023.5 75.0 75.0DNDBenzyl chloride 0.193 09/12/15 K/P 1ND0.193 1.00 1.00

Page 1 of 21 Ver 3

14SG5Phoenix I.D.: BJ89522

Client ID:510 Driggs Avenue, Brooklyn, New YorkProject ID:

Parameterppbv

ResultppbvRL


LOD/MDL

ug/m3RL

LOD/MDL

NDBromodichloromethane 0.149 09/12/15 K/P 1ND0.149 1.00 1.00NDBromoform 0.097 09/12/15 K/P 1ND0.097 1.00 1.00NDBromomethane 0.258 09/12/15 K/P 1ND0.258 1.00 1.00NDCarbon Disulfide 0.321 09/12/15 K/P 1ND0.321 1.00 1.00NDCarbon Tetrachloride 0.040 09/12/15 K/P 1ND0.040 0.25 0.25NDChlorobenzene 0.217 09/12/15 K/P 1ND0.217 1.00 1.0092.8Chloroethane 28.4 09/15/15 K/P 7524528.4 74.9 74.9DNDChloroform 0.205 09/12/15 K/P 1ND0.205 1.00 1.00NDChloromethane 0.485 09/12/15 K/P 1ND0.485 1.00 1.00

11200Cis-1,2-Dichloroethene 379 09/16/15 K/P 150044400379 1500 1500DNDcis-1,3-Dichloropropene 0.221 09/12/15 K/P 1ND0.221 1.00 1.00115Cyclohexane 21.8 09/15/15 K/P 7539621.8 75.0 75.0DNDDibromochloromethane 0.118 09/12/15 K/P 1ND0.118 1.00 1.0018.4Dichlorodifluoromethane 0.202 09/12/15 K/P 190.90.202 1.00 1.0052.0Ethanol 0.531 09/12/15 K/P 197.9 10.531 1.00 1.00SENDEthyl acetate 0.278 09/12/15 K/P 1ND 10.278 1.00 1.001.12Ethylbenzene 0.230 09/12/15 K/P 14.860.230 1.00 1.002.37Heptane 0.244 09/12/15 K/P 19.70.244 1.00 1.00NDHexachlorobutadiene 0.094 09/12/15 K/P 1ND0.094 1.00 1.00205Hexane 21.3 09/15/15 K/P 7572221.3 75.0 75.0DS7.99Isopropylalcohol 0.407 09/12/15 K/P 119.60.407 1.00 1.00S0.480Isopropylbenzene 0.204 09/12/15 K/P 12.360.204 1.00 1.003.78m,p-Xylene 0.230 09/12/15 K/P 116.40.230 1.00 1.00NDMethyl Ethyl Ketone 0.339 09/12/15 K/P 1ND0.339 1.00 1.00NDMethyl tert-butyl ether(MTBE) 0.278 09/12/15 K/P 1ND0.278 1.00 1.00NDMethylene Chloride 0.288 09/12/15 K/P 1ND0.288 1.00 1.00NDn-Butylbenzene 0.182 09/12/15 K/P 1ND 10.182 1.00 1.002.36o-Xylene 0.230 09/12/15 K/P 110.20.230 1.00 1.002200Propylene 43.6 09/15/15 K/P 753780 143.6 75.0 75.0DNDsec-Butylbenzene 0.182 09/12/15 K/P 1ND 10.182 1.00 1.00NDStyrene 0.235 09/12/15 K/P 1ND0.235 1.00 1.001.29Tetrachloroethene 0.037 09/12/15 K/P 18.740.037 0.25 0.25NDTetrahydrofuran 0.339 09/12/15 K/P 1ND 10.339 1.00 1.008.09Toluene 0.266 09/12/15 K/P 130.50.266 1.00 1.00349Trans-1,2-Dichloroethene 18.9 09/15/15 K/P 75138018.9 74.9 74.9DNDtrans-1,3-Dichloropropene 0.221 09/12/15 K/P 1ND0.221 1.00 1.00

1060Trichloroethene 3.49 09/15/15 K/P 7556903.49 18.7 18.7D3.54Trichlorofluoromethane 0.178 09/12/15 K/P 119.90.178 1.00 1.00NDTrichlorotrifluoroethane 0.131 09/12/15 K/P 1ND0.131 1.00 1.00

45600Vinyl Chloride 147 09/16/15 K/P 1500116000147 376 376D

QA/QC Surrogates108% Bromofluorobenzene % 09/12/15 K/P 1108% % %

Page 2 of 21 Ver 3



Parameterppbv

ResultppbvRL


LOD/MDL

ug/m3RL

LOD/MDL

Comments:

S - Laboratory solvent, contamination is possible.

Phyllis Shiller, Laboratory DirectorNovember 02, 2015

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.

Reviewed and Released by: Tina Covensky

RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection LimitQA/QC Surrogates: Surrogates are compounds (preceeded with a %) added by the lab to determine analysis efficiency. Surrogate results(%) listed in the report are not "detected" compounds.

Page 3 of 21 Ver 3



AIREBC72 Hour


PR

Laboratory Data

14SG7

Phoenix ID: BJ89523

09/09/1511:3017:33

Parameterppbv

ResultppbvRL




Date Time



SDG ID: GBJ89522


LOD/MDL

ug/m3RL

LOD/MDL

Canister Id: 13636

Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 09/12/15 KCA 1ND 10.146 1.00 1.00

0.4061,1,1-Trichloroethane 0.183 09/12/15 KCA 12.210.183 1.00 1.00ND1,1,2,2-Tetrachloroethane 0.146 09/12/15 KCA 1ND0.146 1.00 1.00ND1,1,2-Trichloroethane 0.183 09/12/15 KCA 1ND0.183 1.00 1.006.221,1-Dichloroethane 0.247 09/12/15 KCA 125.20.247 1.00 1.001481,1-Dichloroethene 18.9 09/15/15 KCA 7558618.9 74.9 74.9DND1,2,4-Trichlorobenzene 0.135 09/12/15 KCA 1ND0.135 1.00 1.00

0.3851,2,4-Trimethylbenzene 0.204 09/12/15 KCA 11.890.204 1.00 1.00ND1,2-Dibromoethane(EDB) 0.130 09/12/15 KCA 1ND0.130 1.00 1.00ND1,2-Dichlorobenzene 0.166 09/12/15 KCA 1ND0.166 1.00 1.00ND1,2-Dichloroethane 0.247 09/12/15 KCA 1ND0.247 1.00 1.00ND1,2-dichloropropane 0.217 09/12/15 KCA 1ND0.217 1.00 1.00ND1,2-Dichlorotetrafluoroethane 0.143 09/12/15 KCA 1ND0.143 1.00 1.00ND1,3,5-Trimethylbenzene 0.204 09/12/15 KCA 1ND0.204 1.00 1.00ND1,3-Butadiene 0.452 09/12/15 KCA 1ND0.452 1.00 1.00

0.9271,3-Dichlorobenzene 0.166 09/12/15 KCA 15.570.166 1.00 1.00ND1,4-Dichlorobenzene 0.166 09/12/15 KCA 1ND0.166 1.00 1.00ND1,4-Dioxane 0.278 09/12/15 KCA 1ND0.278 1.00 1.0016.52-Hexanone(MBK) 0.244 09/12/15 KCA 167.5 10.244 1.00 1.00ND4-Ethyltoluene 0.204 09/12/15 KCA 1ND 10.204 1.00 1.00ND4-Isopropyltoluene 0.182 09/12/15 KCA 1ND 10.182 1.00 1.002.354-Methyl-2-pentanone(MIBK) 0.244 09/12/15 KCA 19.60.244 1.00 1.00638Acetone 31.6 09/15/15 KCA 75151031.6 75.0 75.0DSNDAcrylonitrile 0.461 09/12/15 KCA 1ND0.461 1.00 1.00122Benzene 23.5 09/15/15 KCA 7539023.5 75.0 75.0DNDBenzyl chloride 0.193 09/12/15 KCA 1ND0.193 1.00 1.00

Page 4 of 21 Ver 3



Parameterppbv

ResultppbvRL


LOD/MDL

ug/m3RL

LOD/MDL

NDBromodichloromethane 0.149 09/12/15 KCA 1ND0.149 1.00 1.00NDBromoform 0.097 09/12/15 KCA 1ND0.097 1.00 1.00NDBromomethane 0.258 09/12/15 KCA 1ND0.258 1.00 1.00NDCarbon Disulfide 0.321 09/12/15 KCA 1ND0.321 1.00 1.00NDCarbon Tetrachloride 0.040 09/12/15 KCA 1ND0.040 0.25 0.25NDChlorobenzene 0.217 09/12/15 KCA 1ND0.217 1.00 1.0012.6Chloroethane 0.379 09/12/15 KCA 133.20.379 1.00 1.000.355Chloroform 0.205 09/12/15 KCA 11.730.205 1.00 1.000.680Chloromethane 0.485 09/12/15 KCA 11.400.485 1.00 1.001060Cis-1,2-Dichloroethene 18.9 09/15/15 KCA 75420018.9 74.9 74.9DNDcis-1,3-Dichloropropene 0.221 09/12/15 KCA 1ND0.221 1.00 1.0050.0Cyclohexane 21.8 09/15/15 KCA 7517221.8 75.0 75.0DNDDibromochloromethane 0.118 09/12/15 KCA 1ND0.118 1.00 1.009.52Dichlorodifluoromethane 0.202 09/12/15 KCA 147.00.202 1.00 1.0044.6Ethanol 0.531 09/12/15 KCA 184.0 10.531 1.00 1.00SENDEthyl acetate 0.278 09/12/15 KCA 1ND 10.278 1.00 1.001.00Ethylbenzene 0.230 09/12/15 KCA 14.340.230 1.00 1.00NDHeptane 0.244 09/12/15 KCA 1ND0.244 1.00 1.00NDHexachlorobutadiene 0.094 09/12/15 KCA 1ND0.094 1.00 1.0074.5Hexane 21.3 09/15/15 KCA 7526221.3 75.0 75.0DS8.49Isopropylalcohol 0.407 09/12/15 KCA 120.90.407 1.00 1.00SNDIsopropylbenzene 0.204 09/12/15 KCA 1ND0.204 1.00 1.002.66m,p-Xylene 0.230 09/12/15 KCA 111.50.230 1.00 1.0055.0Methyl Ethyl Ketone 25.4 09/15/15 KCA 7516225.4 74.9 74.9DNDMethyl tert-butyl ether(MTBE) 0.278 09/12/15 KCA 1ND0.278 1.00 1.005.75Methylene Chloride 0.288 09/12/15 KCA 120.00.288 1.00 1.00SNDn-Butylbenzene 0.182 09/12/15 KCA 1ND 10.182 1.00 1.001.60o-Xylene 0.230 09/12/15 KCA 16.940.230 1.00 1.003260Propylene 87.2 09/16/15 KCA 1505610 187.2 150 150DNDsec-Butylbenzene 0.182 09/12/15 KCA 1ND 10.182 1.00 1.00NDStyrene 0.235 09/12/15 KCA 1ND0.235 1.00 1.003.45Tetrachloroethene 0.037 09/12/15 KCA 123.40.037 0.25 0.25NDTetrahydrofuran 0.339 09/12/15 KCA 1ND 10.339 1.00 1.003.00Toluene 0.266 09/12/15 KCA 111.30.266 1.00 1.0032.2Trans-1,2-Dichloroethene 0.252 09/12/15 KCA 11280.252 1.00 1.00NDtrans-1,3-Dichloropropene 0.221 09/12/15 KCA 1ND0.221 1.00 1.00

1140Trichloroethene 3.49 09/15/15 KCA 7561203.49 18.7 18.7D2.52Trichlorofluoromethane 0.178 09/12/15 KCA 114.10.178 1.00 1.00NDTrichlorotrifluoroethane 0.131 09/12/15 KCA 1ND0.131 1.00 1.00

4240Vinyl Chloride 14.7 09/16/15 KCA 1501080014.7 37.6 37.6D

QA/QC Surrogates105% Bromofluorobenzene % 09/12/15 KCA 1105% % %

Page 5 of 21 Ver 3



Parameterppbv

ResultppbvRL


LOD/MDL

ug/m3RL

LOD/MDL

Comments:







Page 6 of 21 Ver 3



AIREBC72 Hour


PR

Laboratory Data

14SG6

Phoenix ID: BJ89524

09/09/1511:3217:33

Parameterppbv

ResultppbvRL




Date Time



SDG ID: GBJ89522


LOD/MDL

ug/m3RL

LOD/MDL

Canister Id: 494


0.5021,1,1-Trichloroethane 0.183 09/12/15 KCA 12.740.183 1.00 1.00ND1,1,2,2-Tetrachloroethane 0.146 09/12/15 KCA 1ND0.146 1.00 1.00ND1,1,2-Trichloroethane 0.183 09/12/15 KCA 1ND0.183 1.00 1.00ND1,1-Dichloroethane 0.247 09/12/15 KCA 1ND0.247 1.00 1.00ND1,1-Dichloroethene 0.252 09/12/15 KCA 1ND0.252 1.00 1.00ND1,2,4-Trichlorobenzene 0.135 09/12/15 KCA 1ND0.135 1.00 1.00

0.4541,2,4-Trimethylbenzene 0.204 09/12/15 KCA 12.230.204 1.00 1.00ND1,2-Dibromoethane(EDB) 0.130 09/12/15 KCA 1ND0.130 1.00 1.00ND1,2-Dichlorobenzene 0.166 09/12/15 KCA 1ND0.166 1.00 1.00ND1,2-Dichloroethane 0.247 09/12/15 KCA 1ND0.247 1.00 1.00ND1,2-dichloropropane 0.217 09/12/15 KCA 1ND0.217 1.00 1.00ND1,2-Dichlorotetrafluoroethane 0.143 09/12/15 KCA 1ND0.143 1.00 1.00ND1,3,5-Trimethylbenzene 0.204 09/12/15 KCA 1ND0.204 1.00 1.00ND1,3-Butadiene 0.452 09/12/15 KCA 1ND0.452 1.00 1.001.321,3-Dichlorobenzene 0.166 09/12/15 KCA 17.930.166 1.00 1.00ND1,4-Dichlorobenzene 0.166 09/12/15 KCA 1ND0.166 1.00 1.00ND1,4-Dioxane 0.278 09/12/15 KCA 1ND0.278 1.00 1.0019.62-Hexanone(MBK) 0.244 09/12/15 KCA 180.2 10.244 1.00 1.00ND4-Ethyltoluene 0.204 09/12/15 KCA 1ND 10.204 1.00 1.00ND4-Isopropyltoluene 0.182 09/12/15 KCA 1ND 10.182 1.00 1.003.364-Methyl-2-pentanone(MIBK) 0.244 09/12/15 KCA 113.80.244 1.00 1.00696Acetone 13.5 09/16/15 KCA 32165013.5 32.0 32.0DSNDAcrylonitrile 0.461 09/12/15 KCA 1ND0.461 1.00 1.002.07Benzene 0.313 09/12/15 KCA 16.610.313 1.00 1.00NDBenzyl chloride 0.193 09/12/15 KCA 1ND0.193 1.00 1.00

Page 7 of 21 Ver 3



Parameterppbv

ResultppbvRL


LOD/MDL

ug/m3RL

LOD/MDL

NDBromodichloromethane 0.149 09/12/15 KCA 1ND0.149 1.00 1.00NDBromoform 0.097 09/12/15 KCA 1ND0.097 1.00 1.00NDBromomethane 0.258 09/12/15 KCA 1ND0.258 1.00 1.00

0.353Carbon Disulfide 0.321 09/12/15 KCA 11.100.321 1.00 1.000.042Carbon Tetrachloride 0.040 09/12/15 KCA 10.260.040 0.25 0.25NDChlorobenzene 0.217 09/12/15 KCA 1ND0.217 1.00 1.00NDChloroethane 0.379 09/12/15 KCA 1ND0.379 1.00 1.001.73Chloroform 0.205 09/12/15 KCA 18.440.205 1.00 1.00NDChloromethane 0.485 09/12/15 KCA 1ND0.485 1.00 1.001.33Cis-1,2-Dichloroethene 0.252 09/12/15 KCA 15.270.252 1.00 1.00NDcis-1,3-Dichloropropene 0.221 09/12/15 KCA 1ND0.221 1.00 1.00NDCyclohexane 0.291 09/12/15 KCA 1ND0.291 1.00 1.00NDDibromochloromethane 0.118 09/12/15 KCA 1ND0.118 1.00 1.005.23Dichlorodifluoromethane 0.202 09/12/15 KCA 125.80.202 1.00 1.0094.3Ethanol 0.531 09/12/15 KCA 1178 10.531 1.00 1.00SENDEthyl acetate 0.278 09/12/15 KCA 1ND 10.278 1.00 1.001.34Ethylbenzene 0.230 09/12/15 KCA 15.820.230 1.00 1.001.72Heptane 0.244 09/12/15 KCA 17.040.244 1.00 1.00NDHexachlorobutadiene 0.094 09/12/15 KCA 1ND0.094 1.00 1.001.85Hexane 0.284 09/12/15 KCA 16.520.284 1.00 1.00S15.0Isopropylalcohol 0.407 09/12/15 KCA 136.80.407 1.00 1.00SNDIsopropylbenzene 0.204 09/12/15 KCA 1ND0.204 1.00 1.004.89m,p-Xylene 0.230 09/12/15 KCA 121.20.230 1.00 1.00159Methyl Ethyl Ketone 10.9 09/16/15 KCA 3246910.9 32.1 32.1DNDMethyl tert-butyl ether(MTBE) 0.278 09/12/15 KCA 1ND0.278 1.00 1.00NDMethylene Chloride 0.288 09/12/15 KCA 1ND0.288 1.00 1.00NDn-Butylbenzene 0.182 09/12/15 KCA 1ND 10.182 1.00 1.001.95o-Xylene 0.230 09/12/15 KCA 18.460.230 1.00 1.0046.4Propylene 18.6 09/16/15 KCA 3279.8 118.6 32.0 32.0DNDsec-Butylbenzene 0.182 09/12/15 KCA 1ND 10.182 1.00 1.00NDStyrene 0.235 09/12/15 KCA 1ND0.235 1.00 1.00

0.700Tetrachloroethene 0.037 09/12/15 KCA 14.740.037 0.25 0.25NDTetrahydrofuran 0.339 09/12/15 KCA 1ND 10.339 1.00 1.002.06Toluene 0.266 09/12/15 KCA 17.760.266 1.00 1.00NDTrans-1,2-Dichloroethene 0.252 09/12/15 KCA 1ND0.252 1.00 1.00NDtrans-1,3-Dichloropropene 0.221 09/12/15 KCA 1ND0.221 1.00 1.00142Trichloroethene 1.49 09/16/15 KCA 327631.49 8.00 8.00D32.6Trichlorofluoromethane 0.178 09/12/15 KCA 11830.178 1.00 1.00NDTrichlorotrifluoroethane 0.131 09/12/15 KCA 1ND0.131 1.00 1.00NDVinyl Chloride 0.098 09/12/15 KCA 1ND0.098 0.25 0.25


Page 8 of 21 Ver 3



Parameterppbv

ResultppbvRL


LOD/MDL

ug/m3RL

LOD/MDL

Comments:







Page 9 of 21 Ver 3



AIREBC72 Hour


PR

Laboratory Data

14SG1

Phoenix ID: BJ89525

09/09/1511:3617:33

Parameterppbv

ResultppbvRL




Date Time



SDG ID: GBJ89522


LOD/MDL

ug/m3RL

LOD/MDL

Canister Id: 480

Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 09/15/15 KCA 1ND 10.146 1.00 1.002.541,1,1-Trichloroethane 0.183 09/15/15 KCA 113.80.183 1.00 1.00ND1,1,2,2-Tetrachloroethane 0.146 09/15/15 KCA 1ND0.146 1.00 1.00ND1,1,2-Trichloroethane 0.183 09/15/15 KCA 1ND0.183 1.00 1.00ND1,1-Dichloroethane 0.247 09/15/15 KCA 1ND0.247 1.00 1.00ND1,1-Dichloroethene 0.252 09/15/15 KCA 1ND0.252 1.00 1.00ND1,2,4-Trichlorobenzene 0.135 09/15/15 KCA 1ND0.135 1.00 1.00

0.4181,2,4-Trimethylbenzene 0.204 09/15/15 KCA 12.050.204 1.00 1.00ND1,2-Dibromoethane(EDB) 0.130 09/15/15 KCA 1ND0.130 1.00 1.00ND1,2-Dichlorobenzene 0.166 09/15/15 KCA 1ND0.166 1.00 1.00ND1,2-Dichloroethane 0.247 09/15/15 KCA 1ND0.247 1.00 1.00ND1,2-dichloropropane 0.217 09/15/15 KCA 1ND0.217 1.00 1.00ND1,2-Dichlorotetrafluoroethane 0.143 09/15/15 KCA 1ND0.143 1.00 1.00ND1,3,5-Trimethylbenzene 0.204 09/15/15 KCA 1ND0.204 1.00 1.00ND1,3-Butadiene 0.452 09/15/15 KCA 1ND0.452 1.00 1.001.551,3-Dichlorobenzene 0.166 09/15/15 KCA 19.310.166 1.00 1.00ND1,4-Dichlorobenzene 0.166 09/15/15 KCA 1ND0.166 1.00 1.00ND1,4-Dioxane 0.278 09/15/15 KCA 1ND0.278 1.00 1.0027.72-Hexanone(MBK) 0.244 09/15/15 KCA 1113 10.244 1.00 1.00ND4-Ethyltoluene 0.204 09/15/15 KCA 1ND 10.204 1.00 1.00ND4-Isopropyltoluene 0.182 09/15/15 KCA 1ND 10.182 1.00 1.002.554-Methyl-2-pentanone(MIBK) 0.244 09/15/15 KCA 110.40.244 1.00 1.00654Acetone 16.8 09/16/15 KCA 40155016.8 39.9 39.9DSNDAcrylonitrile 0.461 09/15/15 KCA 1ND0.461 1.00 1.00

0.918Benzene 0.313 09/15/15 KCA 12.930.313 1.00 1.00NDBenzyl chloride 0.193 09/15/15 KCA 1ND0.193 1.00 1.00

Page 10 of 21 Ver 3



Parameterppbv

ResultppbvRL


LOD/MDL

ug/m3RL

LOD/MDL


0.327Carbon Disulfide 0.321 09/15/15 KCA 11.020.321 1.00 1.000.053Carbon Tetrachloride 0.040 09/15/15 KCA 10.330.040 0.25 0.25NDChlorobenzene 0.217 09/15/15 KCA 1ND0.217 1.00 1.00NDChloroethane 0.379 09/15/15 KCA 1ND0.379 1.00 1.0017.3Chloroform 0.205 09/15/15 KCA 184.40.205 1.00 1.00NDChloromethane 0.485 09/15/15 KCA 1ND0.485 1.00 1.001.37Cis-1,2-Dichloroethene 0.252 09/15/15 KCA 15.430.252 1.00 1.00NDcis-1,3-Dichloropropene 0.221 09/15/15 KCA 1ND0.221 1.00 1.00NDCyclohexane 0.291 09/15/15 KCA 1ND0.291 1.00 1.00NDDibromochloromethane 0.118 09/15/15 KCA 1ND0.118 1.00 1.0015.2Dichlorodifluoromethane 0.202 09/15/15 KCA 175.10.202 1.00 1.0073.1Ethanol 0.531 09/15/15 KCA 1138 10.531 1.00 1.00SE0.639Ethyl acetate 0.278 09/15/15 KCA 12.30 10.278 1.00 1.001.08Ethylbenzene 0.230 09/15/15 KCA 14.690.230 1.00 1.001.46Heptane 0.244 09/15/15 KCA 15.980.244 1.00 1.00NDHexachlorobutadiene 0.094 09/15/15 KCA 1ND0.094 1.00 1.001.41Hexane 0.284 09/15/15 KCA 14.970.284 1.00 1.00S11.7Isopropylalcohol 0.407 09/15/15 KCA 128.70.407 1.00 1.00SNDIsopropylbenzene 0.204 09/15/15 KCA 1ND0.204 1.00 1.003.92m,p-Xylene 0.230 09/15/15 KCA 117.00.230 1.00 1.00111Methyl Ethyl Ketone 13.6 09/16/15 KCA 4032713.6 40.1 40.1DNDMethyl tert-butyl ether(MTBE) 0.278 09/15/15 KCA 1ND0.278 1.00 1.00

0.344Methylene Chloride 0.288 09/15/15 KCA 11.190.288 1.00 1.00SNDn-Butylbenzene 0.182 09/15/15 KCA 1ND 10.182 1.00 1.001.73o-Xylene 0.230 09/15/15 KCA 17.510.230 1.00 1.0041.8Propylene 23.3 09/16/15 KCA 4071.9 123.3 40.1 40.1DNDsec-Butylbenzene 0.182 09/15/15 KCA 1ND 10.182 1.00 1.00NDStyrene 0.235 09/15/15 KCA 1ND0.235 1.00 1.004.42Tetrachloroethene 0.037 09/15/15 KCA 130.00.037 0.25 0.25NDTetrahydrofuran 0.339 09/15/15 KCA 1ND 10.339 1.00 1.001.95Toluene 0.266 09/15/15 KCA 17.340.266 1.00 1.00NDTrans-1,2-Dichloroethene 0.252 09/15/15 KCA 1ND0.252 1.00 1.00NDtrans-1,3-Dichloropropene 0.221 09/15/15 KCA 1ND0.221 1.00 1.00542Trichloroethene 1.86 09/16/15 KCA 4029101.86 10.0 10.0D44.4Trichlorofluoromethane 7.12 09/16/15 KCA 402497.12 40.0 40.0DNDTrichlorotrifluoroethane 0.131 09/15/15 KCA 1ND0.131 1.00 1.00

0.320Vinyl Chloride 0.098 09/15/15 KCA 10.820.098 0.25 0.25


Page 11 of 21 Ver 3



Parameterppbv

ResultppbvRL


LOD/MDL

ug/m3RL

LOD/MDL

Comments:







Page 12 of 21 Ver 3



AIREBC72 Hour


PR

Laboratory Data

14SG3

Phoenix ID: BJ89526

09/09/1512:3517:33

Parameterppbv

ResultppbvRL




Date Time



SDG ID: GBJ89522


LOD/MDL

ug/m3RL

LOD/MDL

Canister Id: 12862

Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 09/15/15 KCA 1ND 10.146 1.00 1.001.351,1,1-Trichloroethane 0.183 09/15/15 KCA 17.360.183 1.00 1.00ND1,1,2,2-Tetrachloroethane 0.146 09/15/15 KCA 1ND0.146 1.00 1.00ND1,1,2-Trichloroethane 0.183 09/15/15 KCA 1ND0.183 1.00 1.00

0.6201,1-Dichloroethane 0.247 09/15/15 KCA 12.510.247 1.00 1.00ND1,1-Dichloroethene 0.252 09/15/15 KCA 1ND0.252 1.00 1.00ND1,2,4-Trichlorobenzene 0.135 09/15/15 KCA 1ND0.135 1.00 1.00

0.5131,2,4-Trimethylbenzene 0.204 09/15/15 KCA 12.520.204 1.00 1.00ND1,2-Dibromoethane(EDB) 0.130 09/15/15 KCA 1ND0.130 1.00 1.00ND1,2-Dichlorobenzene 0.166 09/15/15 KCA 1ND0.166 1.00 1.00ND1,2-Dichloroethane 0.247 09/15/15 KCA 1ND0.247 1.00 1.00ND1,2-dichloropropane 0.217 09/15/15 KCA 1ND0.217 1.00 1.00ND1,2-Dichlorotetrafluoroethane 0.143 09/15/15 KCA 1ND0.143 1.00 1.00ND1,3,5-Trimethylbenzene 0.204 09/15/15 KCA 1ND0.204 1.00 1.00ND1,3-Butadiene 0.452 09/15/15 KCA 1ND0.452 1.00 1.002.761,3-Dichlorobenzene 0.166 09/15/15 KCA 116.60.166 1.00 1.00ND1,4-Dichlorobenzene 0.166 09/15/15 KCA 1ND0.166 1.00 1.00ND1,4-Dioxane 0.278 09/15/15 KCA 1ND0.278 1.00 1.0024.92-Hexanone(MBK) 0.244 09/15/15 KCA 1102 10.244 1.00 1.00ND4-Ethyltoluene 0.204 09/15/15 KCA 1ND 10.204 1.00 1.00ND4-Isopropyltoluene 0.182 09/15/15 KCA 1ND 10.182 1.00 1.002.234-Methyl-2-pentanone(MIBK) 0.244 09/15/15 KCA 19.130.244 1.00 1.00667Acetone 16.8 09/16/15 KCA 40158016.8 39.9 39.9DSNDAcrylonitrile 0.461 09/15/15 KCA 1ND0.461 1.00 1.00

0.708Benzene 0.313 09/15/15 KCA 12.260.313 1.00 1.00NDBenzyl chloride 0.193 09/15/15 KCA 1ND0.193 1.00 1.00

Page 13 of 21 Ver 3



Parameterppbv

ResultppbvRL


LOD/MDL

ug/m3RL

LOD/MDL

NDBromodichloromethane 0.149 09/15/15 KCA 1ND0.149 1.00 1.00NDBromoform 0.097 09/15/15 KCA 1ND0.097 1.00 1.00NDBromomethane 0.258 09/15/15 KCA 1ND0.258 1.00 1.00NDCarbon Disulfide 0.321 09/15/15 KCA 1ND0.321 1.00 1.00

0.091Carbon Tetrachloride 0.040 09/15/15 KCA 10.570.040 0.25 0.25NDChlorobenzene 0.217 09/15/15 KCA 1ND0.217 1.00 1.00NDChloroethane 0.379 09/15/15 KCA 1ND0.379 1.00 1.002.12Chloroform 0.205 09/15/15 KCA 110.30.205 1.00 1.00NDChloromethane 0.485 09/15/15 KCA 1ND0.485 1.00 1.008.01Cis-1,2-Dichloroethene 0.252 09/15/15 KCA 131.70.252 1.00 1.00NDcis-1,3-Dichloropropene 0.221 09/15/15 KCA 1ND0.221 1.00 1.00NDCyclohexane 0.291 09/15/15 KCA 1ND0.291 1.00 1.00NDDibromochloromethane 0.118 09/15/15 KCA 1ND0.118 1.00 1.0030.8Dichlorodifluoromethane 0.202 09/15/15 KCA 11520.202 1.00 1.0090.0Ethanol 0.531 09/15/15 KCA 1169 10.531 1.00 1.00SE0.504Ethyl acetate 0.278 09/15/15 KCA 11.82 10.278 1.00 1.001.17Ethylbenzene 0.230 09/15/15 KCA 15.080.230 1.00 1.001.04Heptane 0.244 09/15/15 KCA 14.260.244 1.00 1.00NDHexachlorobutadiene 0.094 09/15/15 KCA 1ND0.094 1.00 1.001.08Hexane 0.284 09/15/15 KCA 13.800.284 1.00 1.00S11.0Isopropylalcohol 0.407 09/15/15 KCA 127.00.407 1.00 1.00SNDIsopropylbenzene 0.204 09/15/15 KCA 1ND0.204 1.00 1.004.46m,p-Xylene 0.230 09/15/15 KCA 119.40.230 1.00 1.00108Methyl Ethyl Ketone 13.6 09/16/15 KCA 4031813.6 40.1 40.1DNDMethyl tert-butyl ether(MTBE) 0.278 09/15/15 KCA 1ND0.278 1.00 1.00NDMethylene Chloride 0.288 09/15/15 KCA 1ND0.288 1.00 1.00NDn-Butylbenzene 0.182 09/15/15 KCA 1ND 10.182 1.00 1.001.94o-Xylene 0.230 09/15/15 KCA 18.420.230 1.00 1.0048.7Propylene 23.3 09/16/15 KCA 4083.8 123.3 40.1 40.1DNDsec-Butylbenzene 0.182 09/15/15 KCA 1ND 10.182 1.00 1.00NDStyrene 0.235 09/15/15 KCA 1ND0.235 1.00 1.003.78Tetrachloroethene 0.037 09/15/15 KCA 125.60.037 0.25 0.251.40Tetrahydrofuran 0.339 09/15/15 KCA 14.13 10.339 1.00 1.001.69Toluene 0.266 09/15/15 KCA 16.360.266 1.00 1.000.879Trans-1,2-Dichloroethene 0.252 09/15/15 KCA 13.480.252 1.00 1.00NDtrans-1,3-Dichloropropene 0.221 09/15/15 KCA 1ND0.221 1.00 1.00343Trichloroethene 1.86 09/16/15 KCA 4018401.86 10.0 10.0D123Trichlorofluoromethane 7.12 09/16/15 KCA 406917.12 40.0 40.0DNDTrichlorotrifluoroethane 0.131 09/15/15 KCA 1ND0.131 1.00 1.00NDVinyl Chloride 0.098 09/15/15 KCA 1ND0.098 0.25 0.25


Page 14 of 21 Ver 3



Parameterppbv

ResultppbvRL


LOD/MDL

ug/m3RL

LOD/MDL

Comments:







Page 15 of 21 Ver 3



AIREBC72 Hour


PR

Laboratory Data

14SG4

Phoenix ID: BJ89527

09/09/1511:3417:33

Parameterppbv

ResultppbvRL




Date Time



SDG ID: GBJ89522


LOD/MDL

ug/m3RL

LOD/MDL

Canister Id: 11288


0.1971,1,1-Trichloroethane 0.183 09/15/15 KCA 11.070.183 1.00 1.00ND1,1,2,2-Tetrachloroethane 0.146 09/15/15 KCA 1ND0.146 1.00 1.00ND1,1,2-Trichloroethane 0.183 09/15/15 KCA 1ND0.183 1.00 1.0014.41,1-Dichloroethane 0.247 09/15/15 KCA 158.20.247 1.00 1.0011.21,1-Dichloroethene 0.252 09/15/15 KCA 144.40.252 1.00 1.00ND1,2,4-Trichlorobenzene 0.135 09/15/15 KCA 1ND0.135 1.00 1.00

0.2971,2,4-Trimethylbenzene 0.204 09/15/15 KCA 11.460.204 1.00 1.00ND1,2-Dibromoethane(EDB) 0.130 09/15/15 KCA 1ND0.130 1.00 1.00ND1,2-Dichlorobenzene 0.166 09/15/15 KCA 1ND0.166 1.00 1.00ND1,2-Dichloroethane 0.247 09/15/15 KCA 1ND0.247 1.00 1.00ND1,2-dichloropropane 0.217 09/15/15 KCA 1ND0.217 1.00 1.00ND1,2-Dichlorotetrafluoroethane 0.143 09/15/15 KCA 1ND0.143 1.00 1.00ND1,3,5-Trimethylbenzene 0.204 09/15/15 KCA 1ND0.204 1.00 1.00ND1,3-Butadiene 0.452 09/15/15 KCA 1ND0.452 1.00 1.001.501,3-Dichlorobenzene 0.166 09/15/15 KCA 19.010.166 1.00 1.00ND1,4-Dichlorobenzene 0.166 09/15/15 KCA 1ND0.166 1.00 1.00ND1,4-Dioxane 0.278 09/15/15 KCA 1ND0.278 1.00 1.0026.22-Hexanone(MBK) 0.244 09/15/15 KCA 1107 10.244 1.00 1.00ND4-Ethyltoluene 0.204 09/15/15 KCA 1ND 10.204 1.00 1.00ND4-Isopropyltoluene 0.182 09/15/15 KCA 1ND 10.182 1.00 1.001.494-Methyl-2-pentanone(MIBK) 0.244 09/15/15 KCA 16.100.244 1.00 1.00579Acetone 12.6 09/16/15 KCA 30137012.6 29.9 29.9DSNDAcrylonitrile 0.461 09/15/15 KCA 1ND0.461 1.00 1.0024.9Benzene 0.313 09/15/15 KCA 179.50.313 1.00 1.00NDBenzyl chloride 0.193 09/15/15 KCA 1ND0.193 1.00 1.00

Page 16 of 21 Ver 3



Parameterppbv

ResultppbvRL


LOD/MDL

ug/m3RL

LOD/MDL

NDBromodichloromethane 0.149 09/15/15 KCA 1ND0.149 1.00 1.00NDBromoform 0.097 09/15/15 KCA 1ND0.097 1.00 1.00NDBromomethane 0.258 09/15/15 KCA 1ND0.258 1.00 1.00NDCarbon Disulfide 0.321 09/15/15 KCA 1ND0.321 1.00 1.00NDCarbon Tetrachloride 0.040 09/15/15 KCA 1ND0.040 0.25 0.25NDChlorobenzene 0.217 09/15/15 KCA 1ND0.217 1.00 1.00NDChloroethane 0.379 09/15/15 KCA 1ND0.379 1.00 1.00

0.518Chloroform 0.205 09/15/15 KCA 12.530.205 1.00 1.00NDChloromethane 0.485 09/15/15 KCA 1ND0.485 1.00 1.00793Cis-1,2-Dichloroethene 7.57 09/16/15 KCA 3031407.57 30.0 30.0DNDcis-1,3-Dichloropropene 0.221 09/15/15 KCA 1ND0.221 1.00 1.002.50Cyclohexane 0.291 09/15/15 KCA 18.600.291 1.00 1.00NDDibromochloromethane 0.118 09/15/15 KCA 1ND0.118 1.00 1.0028.3Dichlorodifluoromethane 0.202 09/15/15 KCA 11400.202 1.00 1.0055.3Ethanol 0.531 09/15/15 KCA 1104 10.531 1.00 1.00SENDEthyl acetate 0.278 09/15/15 KCA 1ND 10.278 1.00 1.00

0.654Ethylbenzene 0.230 09/15/15 KCA 12.840.230 1.00 1.001.73Heptane 0.244 09/15/15 KCA 17.090.244 1.00 1.00NDHexachlorobutadiene 0.094 09/15/15 KCA 1ND0.094 1.00 1.003.47Hexane 0.284 09/15/15 KCA 112.20.284 1.00 1.00S14.6Isopropylalcohol 0.407 09/15/15 KCA 135.90.407 1.00 1.00SNDIsopropylbenzene 0.204 09/15/15 KCA 1ND0.204 1.00 1.002.32m,p-Xylene 0.230 09/15/15 KCA 110.10.230 1.00 1.00103Methyl Ethyl Ketone 10.2 09/16/15 KCA 3030410.2 30.1 30.1DNDMethyl tert-butyl ether(MTBE) 0.278 09/15/15 KCA 1ND0.278 1.00 1.00

0.523Methylene Chloride 0.288 09/15/15 KCA 11.820.288 1.00 1.00SNDn-Butylbenzene 0.182 09/15/15 KCA 1ND 10.182 1.00 1.001.20o-Xylene 0.230 09/15/15 KCA 15.210.230 1.00 1.00227Propylene 17.4 09/16/15 KCA 30390 117.4 29.9 29.9DNDsec-Butylbenzene 0.182 09/15/15 KCA 1ND 10.182 1.00 1.00NDStyrene 0.235 09/15/15 KCA 1ND0.235 1.00 1.001.07Tetrachloroethene 0.037 09/15/15 KCA 17.250.037 0.25 0.250.893Tetrahydrofuran 0.339 09/15/15 KCA 12.63 10.339 1.00 1.001.40Toluene 0.266 09/15/15 KCA 15.270.266 1.00 1.0016.3Trans-1,2-Dichloroethene 0.252 09/15/15 KCA 164.60.252 1.00 1.00NDtrans-1,3-Dichloropropene 0.221 09/15/15 KCA 1ND0.221 1.00 1.00248Trichloroethene 1.40 09/16/15 KCA 3013301.40 7.52 7.52D2.57Trichlorofluoromethane 0.178 09/15/15 KCA 114.40.178 1.00 1.00NDTrichlorotrifluoroethane 0.131 09/15/15 KCA 1ND0.131 1.00 1.00

1270Vinyl Chloride 7.34 09/16/15 KCA 7532407.34 18.8 18.8D


Page 17 of 21 Ver 3



Parameterppbv

ResultppbvRL


LOD/MDL

ug/m3RL

LOD/MDL

Comments:







Page 18 of 21 Ver 3



AIREBC72 Hour


PR

Laboratory Data

14SG2

Phoenix ID: BJ89528

09/09/1511:2417:33

Parameterppbv

ResultppbvRL




Date Time



SDG ID: GBJ89522


LOD/MDL

ug/m3RL

LOD/MDL

Canister Id: 487

Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 09/15/15 KCA 1ND 10.146 1.00 1.0015.81,1,1-Trichloroethane 0.183 09/15/15 KCA 186.20.183 1.00 1.00ND1,1,2,2-Tetrachloroethane 0.146 09/15/15 KCA 1ND0.146 1.00 1.00ND1,1,2-Trichloroethane 0.183 09/15/15 KCA 1ND0.183 1.00 1.001.181,1-Dichloroethane 0.247 09/15/15 KCA 14.770.247 1.00 1.00ND1,1-Dichloroethene 0.252 09/15/15 KCA 1ND0.252 1.00 1.00ND1,2,4-Trichlorobenzene 0.135 09/15/15 KCA 1ND0.135 1.00 1.00

0.5441,2,4-Trimethylbenzene 0.204 09/15/15 KCA 12.670.204 1.00 1.00ND1,2-Dibromoethane(EDB) 0.130 09/15/15 KCA 1ND0.130 1.00 1.00ND1,2-Dichlorobenzene 0.166 09/15/15 KCA 1ND0.166 1.00 1.00ND1,2-Dichloroethane 0.247 09/15/15 KCA 1ND0.247 1.00 1.00ND1,2-dichloropropane 0.217 09/15/15 KCA 1ND0.217 1.00 1.00ND1,2-Dichlorotetrafluoroethane 0.143 09/15/15 KCA 1ND0.143 1.00 1.00ND1,3,5-Trimethylbenzene 0.204 09/15/15 KCA 1ND0.204 1.00 1.00ND1,3-Butadiene 0.452 09/15/15 KCA 1ND0.452 1.00 1.001.831,3-Dichlorobenzene 0.166 09/15/15 KCA 111.00.166 1.00 1.00ND1,4-Dichlorobenzene 0.166 09/15/15 KCA 1ND0.166 1.00 1.00ND1,4-Dioxane 0.278 09/15/15 KCA 1ND0.278 1.00 1.0036.22-Hexanone(MBK) 9.77 09/16/15 KCA 40148 19.77 40.0 40.0DND4-Ethyltoluene 0.204 09/15/15 KCA 1ND 10.204 1.00 1.00ND4-Isopropyltoluene 0.182 09/15/15 KCA 1ND 10.182 1.00 1.002.534-Methyl-2-pentanone(MIBK) 0.244 09/15/15 KCA 110.40.244 1.00 1.001230Acetone 16.8 09/16/15 KCA 40292016.8 39.9 39.9DSNDAcrylonitrile 0.461 09/15/15 KCA 1ND0.461 1.00 1.002.17Benzene 0.313 09/15/15 KCA 16.930.313 1.00 1.00NDBenzyl chloride 0.193 09/15/15 KCA 1ND0.193 1.00 1.00

Page 19 of 21 Ver 3



Parameterppbv

ResultppbvRL


LOD/MDL

ug/m3RL

LOD/MDL


0.563Carbon Disulfide 0.321 09/15/15 KCA 11.750.321 1.00 1.000.056Carbon Tetrachloride 0.040 09/15/15 KCA 10.350.040 0.25 0.25NDChlorobenzene 0.217 09/15/15 KCA 1ND0.217 1.00 1.00NDChloroethane 0.379 09/15/15 KCA 1ND0.379 1.00 1.0033.9Chloroform 0.205 09/15/15 KCA 11650.205 1.00 1.001.13Chloromethane 0.485 09/15/15 KCA 12.330.485 1.00 1.00114Cis-1,2-Dichloroethene 10.1 09/16/15 KCA 4045210.1 40.0 40.0DNDcis-1,3-Dichloropropene 0.221 09/15/15 KCA 1ND0.221 1.00 1.00NDCyclohexane 0.291 09/15/15 KCA 1ND0.291 1.00 1.00NDDibromochloromethane 0.118 09/15/15 KCA 1ND0.118 1.00 1.006.64Dichlorodifluoromethane 0.202 09/15/15 KCA 132.80.202 1.00 1.00114Ethanol 0.531 09/15/15 KCA 1215 10.531 1.00 1.00SE1.95Ethyl acetate 0.278 09/15/15 KCA 17.02 10.278 1.00 1.001.18Ethylbenzene 0.230 09/15/15 KCA 15.120.230 1.00 1.003.39Heptane 0.244 09/15/15 KCA 113.90.244 1.00 1.00NDHexachlorobutadiene 0.094 09/15/15 KCA 1ND0.094 1.00 1.003.39Hexane 0.284 09/15/15 KCA 111.90.284 1.00 1.00S30.7Isopropylalcohol 0.407 09/15/15 KCA 175.40.407 1.00 1.00SNDIsopropylbenzene 0.204 09/15/15 KCA 1ND0.204 1.00 1.004.21m,p-Xylene 0.230 09/15/15 KCA 118.30.230 1.00 1.00270Methyl Ethyl Ketone 13.6 09/16/15 KCA 4079613.6 40.1 40.1DNDMethyl tert-butyl ether(MTBE) 0.278 09/15/15 KCA 1ND0.278 1.00 1.001.24Methylene Chloride 0.288 09/15/15 KCA 14.300.288 1.00 1.00SNDn-Butylbenzene 0.182 09/15/15 KCA 1ND 10.182 1.00 1.001.77o-Xylene 0.230 09/15/15 KCA 17.680.230 1.00 1.0060.5Propylene 23.3 09/16/15 KCA 40104 123.3 40.1 40.1DNDsec-Butylbenzene 0.182 09/15/15 KCA 1ND 10.182 1.00 1.00

0.254Styrene 0.235 09/15/15 KCA 11.080.235 1.00 1.0016.6Tetrachloroethene 0.037 09/15/15 KCA 11130.037 0.25 0.250.575Tetrahydrofuran 0.339 09/15/15 KCA 11.69 10.339 1.00 1.004.68Toluene 0.266 09/15/15 KCA 117.60.266 1.00 1.003.47Trans-1,2-Dichloroethene 0.252 09/15/15 KCA 113.70.252 1.00 1.00NDtrans-1,3-Dichloropropene 0.221 09/15/15 KCA 1ND0.221 1.00 1.00

3150Trichloroethene 4.66 09/16/15 KCA 100169004.66 25.0 25.0D11.2Trichlorofluoromethane 0.178 09/15/15 KCA 162.90.178 1.00 1.00NDTrichlorotrifluoroethane 0.131 09/15/15 KCA 1ND0.131 1.00 1.00NDVinyl Chloride 0.098 09/15/15 KCA 1ND0.098 0.25 0.25


Page 20 of 21 Ver 3



Parameterppbv

ResultppbvRL


LOD/MDL

ug/m3RL

LOD/MDL

Comments:







Page 21 of 21 Ver 3

QA/QC Data

Parameter

BlkBlk RLppbv ppbv

SampleResultppbv

SampleDupppbv

DUPRPD

QA/QC ReportNovember 02, 2015



SDG I.D.: GBJ89522

LCS%

SampleResultug/m3

SampleDup

ug/m3

%Rec

Limits

%RPD

LimitsBlk

ug/m3

BlkRL

ug/m3

QA/QC Batch 320174 (ppbv), QC Sample No: BJ89532 (BJ89522, BJ89523, BJ89524)

Volatiles1,1,1,2-Tetrachloroethane ND NDND NC103 ND ND 70 - 130 20ND 1.000.146

1,1,1-Trichloroethane ND NDND NC102 ND ND 70 - 130 20ND 1.000.183

1,1,2,2-Tetrachloroethane ND NDND NC102 ND ND 70 - 130 20ND 1.000.146

1,1,2-Trichloroethane ND NDND NC119 ND ND 70 - 130 20ND 1.000.183

1,1-Dichloroethane ND NDND NC98 ND ND 70 - 130 20ND 1.000.247

1,1-Dichloroethene ND NDND NC96 ND ND 70 - 130 20ND 1.000.252

1,2,4-Trichlorobenzene ND NDND NC112 ND ND 70 - 130 20ND 1.000.135

1,2,4-Trimethylbenzene 0.239 0.256ND 6.9111 1.17 1.26 70 - 130 20ND 1.000.204

1,2-Dibromoethane(EDB) ND NDND NC105 ND ND 70 - 130 20ND 1.000.130

1,2-Dichlorobenzene ND NDND NC106 ND ND 70 - 130 20ND 1.000.166


1,2-dichloropropane ND NDND NC103 ND ND 70 - 130 20ND 1.000.216

1,2-Dichlorotetrafluoroethane ND NDND NC98 ND ND 70 - 130 20ND 1.000.143

1,3,5-Trimethylbenzene ND NDND NC114 ND ND 70 - 130 20ND 1.000.204

1,3-Butadiene ND NDND NC130 ND ND 70 - 130 20ND 1.000.452



1,4-Dioxane ND NDND NC119 ND ND 70 - 130 20ND 1.000.278

2-Hexanone(MBK) ND NDND NC119 ND ND 70 - 130 20ND 1.000.244

4-Ethyltoluene ND NDND NC119 ND ND 70 - 130 20ND 1.000.204

4-Isopropyltoluene ND NDND NC106 ND ND 70 - 130 20ND 1.000.182

4-Methyl-2-pentanone(MIBK) ND NDND NC99 ND ND 70 - 130 20ND 1.000.244

Acrylonitrile ND NDND NC99 ND ND 70 - 130 20ND 1.000.461

Benzene ND NDND NC99 ND ND 70 - 130 20ND 1.000.313

Benzyl chloride ND NDND NC128 ND ND 70 - 130 20ND 1.000.193

Bromodichloromethane ND NDND NC106 ND ND 70 - 130 20ND 1.000.149

Bromoform ND NDND NC113 ND ND 70 - 130 20ND 1.000.097

Bromomethane ND NDND NC102 ND ND 70 - 130 20ND 1.000.257

Carbon Disulfide ND NDND NC101 ND ND 70 - 130 20ND 1.000.321

Carbon Tetrachloride 0.082 0.090ND 9.3104 0.52 0.57 70 - 130 20ND 0.250.040

Chlorobenzene ND NDND NC100 ND ND 70 - 130 20ND 1.000.217

Chloroethane ND NDND NC104 ND ND 70 - 130 20ND 1.000.379

Chloroform ND NDND NC97 ND ND 70 - 130 20ND 1.000.205

Chloromethane 0.650 0.742ND 13.2104 1.34 1.53 70 - 130 20ND 1.000.484

Cis-1,2-Dichloroethene ND NDND NC102 ND ND 70 - 130 20ND 1.010.256

cis-1,3-Dichloropropene ND NDND NC92 ND ND 70 - 130 20ND 1.000.220

Cyclohexane ND NDND NC103 ND ND 70 - 130 20ND 1.000.291

Dibromochloromethane ND NDND NC109 ND ND 70 - 130 20ND 1.000.117

Dichlorodifluoromethane 0.275 0.284ND 3.2102 1.36 1.40 70 - 130 20ND 1.000.202

Ethanol 87.3 98.4ND 12.0106 164 185 70 - 130 20ND 1.000.531

Ethyl acetate 0.323 0.342ND 5.7106 1.16 1.23 70 - 130 20ND 1.000.278

Page 1 of 4

QA/QC Data

Parameter

BlkBlk RLppbv ppbv

SampleResultppbv

SampleDupppbv

DUPRPD

SDG I.D.: GBJ89522

LCS%

SampleResultug/m3

SampleDup

ug/m3

%Rec

Limits

%RPD

LimitsBlk

ug/m3

BlkRL

ug/m3

Ethylbenzene ND NDND NC115 ND ND 70 - 130 20ND 1.000.230

Heptane ND NDND NC97 ND ND 70 - 130 20ND 1.000.244

Hexachlorobutadiene ND NDND NC92 ND ND 70 - 130 20ND 1.000.094

Hexane 0.324 0.327ND 0.9102 1.14 1.15 70 - 130 20ND 1.000.284

Isopropylalcohol 1.52 1.75ND 14.1107 3.73 4.30 70 - 130 20ND 1.000.407

Isopropylbenzene ND NDND NC114 ND ND 70 - 130 20ND 1.000.204

m,p-Xylene 0.235 0.258ND 9.3117 1.02 1.12 70 - 130 20ND 1.000.230

Methyl Ethyl Ketone 0.574 0.600ND 4.4110 1.69 1.77 70 - 130 20ND 1.000.339

Methyl tert-butyl ether(MTBE) ND NDND NC111 ND ND 70 - 130 20ND 1.000.277

Methylene Chloride 0.388 0.159ND 83.797 1.35 0.55 r70 - 130 20ND 1.000.288

n-Butylbenzene ND NDND NC101 ND ND 70 - 130 20ND 1.000.182

o-Xylene ND NDND NC111 ND ND 70 - 130 20ND 1.000.230

sec-Butylbenzene ND NDND NC110 ND ND 70 - 130 20ND 1.000.182

Styrene ND NDND NC138 ND ND l70 - 130 20ND 1.000.235

Tetrachloroethene 0.351 0.390ND 10.5102 2.38 2.64 70 - 130 20ND 0.250.037

Tetrahydrofuran ND NDND NC100 ND ND 70 - 130 20ND 1.000.339

Toluene 0.644 0.708ND 9.5110 2.43 2.67 70 - 130 20ND 1.000.266

Trans-1,2-Dichloroethene ND NDND NC102 ND ND 70 - 130 20ND 1.000.252

trans-1,3-Dichloropropene ND NDND NC87 ND ND 70 - 130 20ND 1.000.220

Trichlorofluoromethane 0.247 0.259ND 4.7104 1.39 1.45 70 - 130 20ND 1.000.178

Trichlorotrifluoroethane ND NDND NC97 ND ND 70 - 130 20ND 1.000.131

Vinyl Chloride ND NDND NC108 ND ND 70 - 130 20ND 0.250.098

% Bromofluorobenzene 103 10399 0.099 103 103 70 - 130 2099 %%

QA/QC Batch 320442 (ppbv), QC Sample No: BJ90968 (BJ89522 (75X, 1500X) , BJ89523 (75X, 150X) , BJ89524 (32X) , BJ89525 (40X) , BJ89526 (40X) , BJ89527 (30X, 75X) , BJ89528 (40X, 100X) )

Volatiles1,1-Dichloroethene ND NDND NC99 ND ND 70 - 130 20ND 1.000.252


Acetone 2.89 3.06ND 5.793 6.86 7.26 70 - 130 20ND 1.000.421





Hexane ND NDND NC102 ND ND 70 - 130 20ND 1.000.284

Methyl Ethyl Ketone 0.971 1.03ND 5.9100 2.86 3.04 70 - 130 20ND 1.000.339

Propylene ND NDND NC117 ND ND 70 - 130 20ND 1.000.581


Trichloroethene ND NDND NC99 ND ND 70 - 130 20ND 0.250.047


Vinyl Chloride ND NDND NC113 ND ND 70 - 130 20ND 0.250.098

QA/QC Batch 320322 (ppbv), QC Sample No: BJ90974 (BJ89525, BJ89526, BJ89527, BJ89528)

Volatiles1,1,1,2-Tetrachloroethane ND NDND NC100 ND ND 70 - 130 20ND 1.000.146

1,1,1-Trichloroethane 3.68 3.68ND 0.0102 20.1 20.1 70 - 130 20ND 1.000.183

1,1,2,2-Tetrachloroethane ND NDND NC100 ND ND 70 - 130 20ND 1.000.146

1,1,2-Trichloroethane ND NDND NC62 ND ND l70 - 130 20ND 1.000.183


1,1-Dichloroethene ND NDND NC99 ND ND 70 - 130 20ND 1.000.252

1,2,4-Trichlorobenzene ND NDND NC112 ND ND 70 - 130 20ND 1.000.135


1,2-Dibromoethane(EDB) ND NDND NC106 ND ND 70 - 130 20ND 1.000.130


Page 2 of 4

QA/QC Data

Parameter

BlkBlk RLppbv ppbv

SampleResultppbv

SampleDupppbv

DUPRPD

SDG I.D.: GBJ89522

LCS%

SampleResultug/m3

SampleDup

ug/m3

%Rec

Limits

%RPD

LimitsBlk

ug/m3

BlkRL

ug/m3


1,2-dichloropropane ND NDND NC105 ND ND 70 - 130 20ND 1.000.216

1,2-Dichlorotetrafluoroethane ND NDND NC101 ND ND 70 - 130 20ND 1.000.143


1,3-Butadiene ND NDND NC136 ND ND l70 - 130 20ND 1.000.452

1,3-Dichlorobenzene 0.204 0.217ND 6.2102 1.23 1.30 70 - 130 20ND 1.000.166


1,4-Dioxane ND NDND NC117 ND ND 70 - 130 20ND 1.000.278


4-Ethyltoluene ND NDND NC111 ND ND 70 - 130 20ND 1.000.204

4-Isopropyltoluene ND NDND NC99 ND ND 70 - 130 20ND 1.000.182

4-Methyl-2-pentanone(MIBK) 0.266 0.286ND 7.297 1.09 1.17 70 - 130 20ND 1.000.244

Acrylonitrile ND NDND NC104 ND ND 70 - 130 20ND 1.000.461


Benzyl chloride ND NDND NC117 ND ND 70 - 130 20ND 1.000.193

Bromodichloromethane ND NDND NC103 ND ND 70 - 130 20ND 1.000.149

Bromoform ND NDND NC109 ND ND 70 - 130 20ND 1.000.097

Bromomethane ND NDND NC104 ND ND 70 - 130 20ND 1.000.257

Carbon Disulfide ND NDND NC102 ND ND 70 - 130 20ND 1.000.321

Carbon Tetrachloride 0.670 0.658ND 1.8104 4.21 4.14 70 - 130 20ND 0.250.040

Chlorobenzene ND NDND NC100 ND ND 70 - 130 20ND 1.000.217


Chloroform 29.8 29.8ND 0.098 145 145 70 - 130 20ND 1.000.205

Chloromethane ND NDND NC113 ND ND 70 - 130 20ND 1.000.484


cis-1,3-Dichloropropene ND NDND NC87 ND ND 70 - 130 20ND 1.000.220


Dibromochloromethane ND NDND NC107 ND ND 70 - 130 20ND 1.000.117

Dichlorodifluoromethane 0.375 0.361ND 3.8106 1.85 1.78 70 - 130 20ND 1.000.202

Ethanol 62.0 S 66.7 SND 7.3102 117 S 126 S 70 - 130 20ND 1.000.531

Ethyl acetate ND NDND NC99 ND ND 70 - 130 20ND 1.000.278

Ethylbenzene 2.38 2.37ND 0.4113 10.3 10.3 70 - 130 20ND 1.000.230

Heptane ND NDND NC96 ND ND 70 - 130 20ND 1.000.244

Hexachlorobutadiene ND NDND NC95 ND ND 70 - 130 20ND 1.000.094

Hexane 0.376 S 0.400 SND 6.2102 1.32 S 1.41 S 70 - 130 20ND 1.000.284

Isopropylalcohol 1.33 S 1.45 SND 8.6102 3.27 S 3.56 S 70 - 130 20ND 1.000.407

Isopropylbenzene ND NDND NC106 ND ND 70 - 130 20ND 1.000.204

m,p-Xylene 9.8 9.79ND 0.1112 42.5 42.5 70 - 130 20ND 1.000.230

Methyl tert-butyl ether(MTBE) ND NDND NC107 ND ND 70 - 130 20ND 1.000.277

Methylene Chloride ND S 0.288 SND NC95 ND 1.00 S 70 - 130 20ND 1.000.288

n-Butylbenzene ND NDND NC96 ND ND 70 - 130 20ND 1.000.182

o-Xylene 3.95 4.09ND 3.5111 17.1 17.7 70 - 130 20ND 1.000.230

sec-Butylbenzene ND NDND NC102 ND ND 70 - 130 20ND 1.000.182

Styrene ND NDND NC133 ND ND l70 - 130 20ND 1.000.235

Tetrachloroethene 6.42 6.38ND 0.6105 43.5 43.2 70 - 130 20ND 0.250.037

Tetrahydrofuran ND NDND NC101 ND ND 70 - 130 20ND 1.000.339

Toluene 0.637 0.605ND 5.2115 2.40 2.28 70 - 130 20ND 1.000.266


trans-1,3-Dichloropropene ND NDND NC85 ND ND 70 - 130 20ND 1.000.220


Trichlorotrifluoroethane ND NDND NC97 ND ND 70 - 130 20ND 1.000.131

Vinyl Chloride 0.177 0.101ND 54.7111 0.45 0.26 r70 - 130 20ND 0.250.098

% Bromofluorobenzene 104 105100 1.098 104 105 70 - 130 20100 %%

Page 3 of 4

QA/QC Data

Parameter

BlkBlk RLppbv ppbv

SampleResultppbv

SampleDupppbv

DUPRPD

SDG I.D.: GBJ89522

LCS%

SampleResultug/m3

SampleDup

ug/m3

%Rec

Limits

%RPD

LimitsBlk

ug/m3

BlkRL

ug/m3

l = This parameter is outside laboratory LCS/LCSD specified recovery limits.r = This parameter is outside laboratory RPD specified recovery limits.

MS - Matrix SpikePhyllis Shiller, Laboratory Director

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.

November 02, 2015MS Dup - Matrix Spike Duplicate

RPD - Relative Percent Difference

LCS - Laboratory Control SampleLCSD - Laboratory Control Sample Duplicate

NC - No CriteriaIntf - Interference

Page 4 of 4

Sample Criteria Exceedences ReportMonday, November 02, 2015 Page 1 of 1

Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis

UnitsCriteria

GBJ89522 - EBCCriteria: None

RLCriteria

State: NY

#Error*** No Data to Display ***

Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.

1

Sarah - Phoenixlabs

From: Patrick Recio [[email protected]]Sent: Friday, October 02, 2015 5:04 PMTo: Sarah - PhoenixlabsSubject: GBJ89522 - Address Change

Hey Sarah,

For SDG GBJ89522 I need the Site Id added to the file. The address is 510 Driggs Avenue, Brooklyn, New York. Sorry for the inconvenience.

Thanks,

Patrick RecioEnvironmental ScientistEBC Environmental Business Consultants Ph: 631.504.6000 ext. 119 Fax: 631.924.2870 Cell: 516.220.2997 [email protected]

mailto:[email protected]

mailto:[email protected]

BJ89517 - BJ89520

Thursday, October 29, 2015

Sample ID#s:


Project ID: 510 DRIGGS AVE., BROOKLYN

Sincerely yours,












Client: Environmental Business ConsultantsProject: 510 DRIGGS AVE., BROOKLYN


NY Analytical Services Protocol FormatOctober 29, 2015



SDG I.D.: GBJ89517

Environmental Business Consultants 510 DRIGGS AVE., BROOKLYN

Methodology Summary Volatiles

USEPA SW-846 Test Methods for Evaluating Solid Waste Physical/Chemical Methods 3rd Ed. Update V, Method 8260C and Environmental Protection Agency, EPA-600/4-79-020, Revised March 1983 (Methods 624) as printed in 40CFR part 136.

MercuryMethods for Chemical Analyses of Water and Wastes, EPA, Environmental Monitoring Systems Laboratory Cincinnati (EMSL-CL), EPA-600/4-79-020, method 245.1USEPA SW-846 Test Methods for Evaluating Solid Waste Physical/Chemical Methods Update III, 7470A.

MetalsICP :USEPA SW-846 Test Methods for Evaluating Solid Waste Physical/Chemical Methods 3rd Ed. Update IV, Method 6010C. Mercury:USEPA SW-846 Test Methods for Evaluating Solid Waste Physical/Chemical Methods Update III, 7471

Pesticides:USEPA SW-846 Test Methods for Evaluating Solid Waste Physical/Chemical Methods 3rd Ed. Update IV, Method 8081B.

Polychlorinated Biphenyls (PCBs)/Pesticides:Environmental Protection Agency, EPA-600/4-79-020, Revised March 1983 (Methods 608) as printed in 40CFR part 136.

Semivolatile Organic CompoundsUSEPA SW-846 Test Methods for Evaluating Solid Waste Physical/Chemical Methods 3rd Ed. Update IV, Method 8270D.

Semi-volatiles analysisUSEPA SW-846 Test Methods for Evaluating Solid Waste Physical/Chemical Methods 3rd Ed. Update IV, Method 8270D (SIM - selective ion monitoring mode).




SDG I.D.: GBJ89517


Sample Id Cross ReferenceClient Id Lab Id Matrix14MW5 BJ89517 GROUND WATER14MW6 BJ89518 GROUND WATER14MW7 BJ89519 GROUND WATERDUPLICATE BJ89520 GROUND WATER




SDG I.D.: GBJ89517


Laboratory Chronicle

Sample AnalysisCollection

DateExtraction

DateAnalysis

Date AnalystHold Time

MetBJ89517 Aluminum 09/08/15 09/09/15 09/10/15 EK YBJ89517 Antimony 09/08/15 09/09/15 09/14/15 RS YBJ89517 Arsenic - LDL 09/08/15 09/09/15 09/10/15 EK YBJ89517 Barium 09/08/15 09/09/15 09/10/15 EK YBJ89517 Beryllium 09/08/15 09/09/15 09/10/15 EK YBJ89517 Cadmium 09/08/15 09/09/15 09/10/15 EK YBJ89517 Calcium 09/08/15 09/09/15 09/10/15 EK YBJ89517 Chromium 09/08/15 09/09/15 09/10/15 EK YBJ89517 Cobalt 09/08/15 09/09/15 09/10/15 EK YBJ89517 Copper 09/08/15 09/09/15 09/10/15 EK YBJ89517 Iron 09/08/15 09/09/15 09/10/15 EK YBJ89517 Lead 09/08/15 09/09/15 09/10/15 EK YBJ89517 Magnesium 09/08/15 09/09/15 09/10/15 EK YBJ89517 Manganese 09/08/15 09/09/15 09/10/15 EK YBJ89517 Mercury 09/08/15 09/10/15 09/10/15 MA YBJ89517 Nickel 09/08/15 09/09/15 09/12/15 LK YBJ89517 Pesticides 09/08/15 09/09/15 09/10/15 CE YBJ89517 Polychlorinated Biphenyls 09/08/15 09/09/15 09/10/15 AW YBJ89517 Potassium 09/08/15 09/09/15 09/10/15 EK YBJ89517 Selenium 09/08/15 09/09/15 09/11/15 RS YBJ89517 Semivolatiles 09/08/15 09/09/15 09/11/15 DD YBJ89517 Silver 09/08/15 09/09/15 09/10/15 EK YBJ89517 Sodium 09/08/15 09/09/15 09/10/15 EK YBJ89517 Thallium - LDL 09/08/15 09/09/15 09/15/15 RS YBJ89517 Vanadium 09/08/15 09/09/15 09/10/15 EK YBJ89517 Volatiles 09/08/15 09/10/15 09/10/15 MH YBJ89517 Zinc 09/08/15 09/09/15 09/10/15 EK YBJ89518 Aluminum 09/08/15 09/09/15 09/10/15 EK YBJ89518 Antimony 09/08/15 09/10/15 09/14/15 RS YBJ89518 Arsenic - LDL 09/08/15 09/09/15 09/10/15 EK YBJ89518 Barium 09/08/15 09/09/15 09/10/15 EK YBJ89518 Beryllium 09/08/15 09/09/15 09/10/15 EK Y




SDG I.D.: GBJ89517


BJ89518 Cadmium 09/08/15 09/09/15 09/10/15 EK YBJ89518 Calcium 09/08/15 09/09/15 09/10/15 EK YBJ89518 Chromium 09/08/15 09/09/15 09/10/15 EK YBJ89518 Cobalt 09/08/15 09/09/15 09/10/15 EK YBJ89518 Copper 09/08/15 09/09/15 09/10/15 EK YBJ89518 Iron 09/08/15 09/09/15 09/10/15 EK YBJ89518 Lead 09/08/15 09/09/15 09/10/15 EK YBJ89518 Magnesium 09/08/15 09/09/15 09/10/15 EK YBJ89518 Manganese 09/08/15 09/09/15 09/10/15 EK YBJ89518 Mercury 09/08/15 09/10/15 09/10/15 MA YBJ89518 Nickel 09/08/15 09/09/15 09/10/15 EK YBJ89518 Pesticides 09/08/15 09/09/15 09/10/15 CE YBJ89518 Polychlorinated Biphenyls 09/08/15 09/09/15 09/10/15 AW YBJ89518 Potassium 09/08/15 09/09/15 09/10/15 EK YBJ89518 Selenium 09/08/15 09/10/15 09/11/15 RS YBJ89518 Semivolatiles 09/08/15 09/09/15 09/11/15 DD YBJ89518 Silver 09/08/15 09/09/15 09/10/15 EK YBJ89518 Sodium 09/08/15 09/09/15 09/10/15 EK YBJ89518 Thallium - LDL 09/08/15 09/10/15 09/15/15 RS YBJ89518 Vanadium 09/08/15 09/09/15 09/10/15 EK YBJ89518 Volatiles 09/08/15 09/10/15 09/10/15 MH YBJ89518 Zinc 09/08/15 09/09/15 09/10/15 EK YBJ89519 Aluminum 09/08/15 09/09/15 09/10/15 EK YBJ89519 Antimony 09/08/15 09/09/15 09/14/15 RS YBJ89519 Arsenic - LDL 09/08/15 09/09/15 09/10/15 EK YBJ89519 Barium 09/08/15 09/09/15 09/10/15 EK YBJ89519 Beryllium 09/08/15 09/09/15 09/10/15 EK YBJ89519 Cadmium 09/08/15 09/09/15 09/10/15 EK YBJ89519 Calcium 09/08/15 09/09/15 09/10/15 EK YBJ89519 Chromium 09/08/15 09/09/15 09/10/15 EK YBJ89519 Cobalt 09/08/15 09/09/15 09/10/15 EK YBJ89519 Copper 09/08/15 09/09/15 09/10/15 EK YBJ89519 Iron 09/08/15 09/09/15 09/10/15 EK YBJ89519 Lead 09/08/15 09/09/15 09/10/15 EK YBJ89519 Magnesium 09/08/15 09/09/15 09/10/15 EK YBJ89519 Manganese 09/08/15 09/09/15 09/10/15 EK YBJ89519 Mercury 09/08/15 09/10/15 09/10/15 MA Y




SDG I.D.: GBJ89517


BJ89519 Nickel 09/08/15 09/09/15 09/12/15 LK YBJ89519 Pesticides 09/08/15 09/09/15 09/10/15 CE YBJ89519 Polychlorinated Biphenyls 09/08/15 09/09/15 09/10/15 AW YBJ89519 Potassium 09/08/15 09/09/15 09/10/15 EK YBJ89519 Selenium 09/08/15 09/09/15 09/11/15 RS YBJ89519 Semivolatiles 09/08/15 09/09/15 09/11/15 DD YBJ89519 Silver 09/08/15 09/09/15 09/10/15 EK YBJ89519 Sodium 09/08/15 09/09/15 09/10/15 EK YBJ89519 Thallium - LDL 09/08/15 09/09/15 09/15/15 RS YBJ89519 Vanadium 09/08/15 09/09/15 09/10/15 EK YBJ89519 Volatiles 09/08/15 09/10/15 09/10/15 MH YBJ89519 Zinc 09/08/15 09/09/15 09/10/15 EK YBJ89520 Aluminum 09/08/15 09/09/15 09/10/15 EK YBJ89520 Antimony 09/08/15 09/09/15 09/14/15 RS YBJ89520 Arsenic - LDL 09/08/15 09/09/15 09/10/15 EK YBJ89520 Barium 09/08/15 09/09/15 09/10/15 EK YBJ89520 Beryllium 09/08/15 09/09/15 09/10/15 EK YBJ89520 Cadmium 09/08/15 09/09/15 09/10/15 EK YBJ89520 Calcium 09/08/15 09/09/15 09/10/15 EK YBJ89520 Chromium 09/08/15 09/09/15 09/10/15 EK YBJ89520 Cobalt 09/08/15 09/09/15 09/10/15 EK YBJ89520 Copper 09/08/15 09/09/15 09/10/15 EK YBJ89520 Iron 09/08/15 09/09/15 09/10/15 EK YBJ89520 Lead 09/08/15 09/09/15 09/10/15 EK YBJ89520 Magnesium 09/08/15 09/09/15 09/10/15 EK YBJ89520 Manganese 09/08/15 09/09/15 09/10/15 EK YBJ89520 Mercury 09/08/15 09/10/15 09/10/15 MA YBJ89520 Nickel 09/08/15 09/09/15 09/12/15 LK YBJ89520 Pesticides 09/08/15 09/09/15 09/10/15 CE YBJ89520 Polychlorinated Biphenyls 09/08/15 09/09/15 09/10/15 AW YBJ89520 Potassium 09/08/15 09/09/15 09/10/15 EK YBJ89520 Selenium 09/08/15 09/09/15 09/11/15 RS YBJ89520 Semivolatiles 09/08/15 09/09/15 09/11/15 DD YBJ89520 Silver 09/08/15 09/09/15 09/10/15 EK YBJ89520 Sodium 09/08/15 09/09/15 09/10/15 EK YBJ89520 Thallium - LDL 09/08/15 09/09/15 09/15/15 RS YBJ89520 Vanadium 09/08/15 09/09/15 09/10/15 EK Y




SDG I.D.: GBJ89517


BJ89520 Volatiles 09/08/15 09/10/15 09/10/15 MH YBJ89520 Zinc 09/08/15 09/09/15 09/10/15 EK Y

SDG CommentsOctober 29, 2015



SDG I.D.: GBJ89517

8260 Volatile Organics:1,2-Dibromoethane, 1,2,3 Trichloropropane, and 1,2-Dibromo-3-chloropropane do not meet NY TOGS GA criteria, these compounds are analyzed by GC/FID method 504 or 8011 to achieve this criteria.

SIM Analysis:The lowest possible reporting limit under SIM conditions is 0.02 ug/L. The NY TOGS GA criteria for some PAHs is 0.002 ug/L. This level can not be achieved.

Toxaphene is reported to the lowest possible reporting level. The NY TOGS criteria for this compound can not be achieved.





GROUND WATEREBC72 Hour


PR

Laboratory Data

14MW5

Phoenix ID: BJ89517

09/09/15 17:33

Parameter ResultRL/PQL Units Date/Time By Reference


Analysis ReportOctober 29, 2015

Date Time



SDG ID: GBJ89517

Client ID:Project ID: 510 DRIGGS AVE., BROOKLYN

LOD/MDL Dilution

< 0.005Silver 0.005 09/10/15 EK SW6010Cmg/L0.001 11.65Aluminum 0.010 09/10/15 EK SW6010Cmg/L0.0024 10.004Arsenic - LDL 0.004 09/10/15 EK SW6010Cmg/L0.001 1B0.020Barium 0.010 09/10/15 EK SW6010Cmg/L0.001 1

< 0.001Beryllium 0.001 09/10/15 EK SW6010Cmg/L0.001 126.6Calcium 0.010 09/10/15 EK SW6010Cmg/L B0.003 1

< 0.004Cadmium 0.004 09/10/15 EK SW6010Cmg/L0.0005 1< 0.005Cobalt 0.005 09/10/15 EK SW6010Cmg/L0.001 10.005Chromium 0.001 09/10/15 EK SW6010Cmg/L0.001 10.006Copper 0.005 09/10/15 EK SW6010Cmg/L0.001 12.75Iron 0.01 09/10/15 EK SW6010Cmg/L0.01 1

< 0.0002Mercury 0.0002 09/10/15 MA SW7470Amg/L0.00015 13.5Potassium 0.1 09/10/15 EK SW6010Cmg/L0.1 1

2.03Magnesium 0.01 09/10/15 EK SW6010Cmg/L0.001 10.358Manganese 0.005 09/10/15 EK SW6010Cmg/L0.001 19.2Sodium 0.1 09/10/15 EK SW6010Cmg/L0.1 1

0.006Nickel 0.004 09/12/15 LK SW6010Cmg/L0.001 10.006Lead 0.002 09/10/15 EK SW6010Cmg/L0.001 1

< 0.002Antimony 0.002 09/14/15 RS SW7010mg/L0.002 1< 0.002Selenium 0.002 09/11/15 RS SW7010mg/L0.001 1

< 0.0005Thallium - LDL 0.0005 09/15/15 RS SW7010mg/L0.0005 10.005Vanadium 0.010 09/10/15 EK SW6010Cmg/L0.001 1B0.006Zinc 0.010 09/10/15 EK SW6010Cmg/L0.001 1B

CompletedMercury Digestion 09/10/15 I/I SW7470ACompletedPCB Extraction (2 Liter) 09/09/15 LT SW3510CCompletedExtraction for Pest (2 Liter) 09/09/15 LT SW3510CCompletedSemi-Volatile Extraction 09/09/15 E/D/D SW3520CCompletedTotal Metals Digestion 09/09/15 AG SW3050B

Page 1 of 24 Ver 2

14MW5Phoenix I.D.: BJ89517

Client ID:510 DRIGGS AVE., BROOKLYNProject ID:


LOD/MDL Dilution

PesticidesND4,4' -DDD 0.010 09/10/15 CE SW8081Bug/L0.010 1ND4,4' -DDE 0.010 09/10/15 CE SW8081Bug/L0.010 1ND4,4' -DDT 0.010 09/10/15 CE SW8081Bug/L0.010 1NDa-BHC 0.005 09/10/15 CE SW8081Bug/L0.005 1NDa-chlordane 0.010 09/10/15 CE SW8081Bug/L0.010 1NDAlachlor 0.075 09/10/15 CE SW8081Bug/L 10.075 1NDAldrin 0.003 09/10/15 CE SW8081Bug/L0.003 1NDb-BHC 0.015 09/10/15 CE SW8081Bug/L0.015 1NDChlordane 0.05 09/10/15 CE SW8081Bug/L0.05 1NDd-BHC 0.005 09/10/15 CE SW8081Bug/L0.005 1NDDieldrin 0.004 09/10/15 CE SW8081Bug/L0.004 1NDEndosulfan I 0.010 09/10/15 CE SW8081Bug/L0.010 1NDEndosulfan II 0.010 09/10/15 CE SW8081Bug/L0.010 1NDEndosulfan Sulfate 0.010 09/10/15 CE SW8081Bug/L0.010 1NDEndrin 0.010 09/10/15 CE SW8081Bug/L0.010 1NDEndrin Aldehyde 0.010 09/10/15 CE SW8081Bug/L0.010 1NDEndrin ketone 0.010 09/10/15 CE SW8081Bug/L0.010 1NDg-BHC (Lindane) 0.011 09/10/15 CE SW8081Bug/L0.011 1NDg-chlordane 0.016 09/10/15 CE SW8081Bug/L0.016 1NDHeptachlor 0.010 09/10/15 CE SW8081Bug/L0.010 1NDHeptachlor epoxide 0.010 09/10/15 CE SW8081Bug/L0.010 1NDMethoxychlor 0.10 09/10/15 CE SW8081Bug/L0.10 1NDToxaphene 0.25 09/10/15 CE SW8081Bug/L0.25 1

QA/QC Surrogates62%DCBP (Surrogate Rec) 09/10/15 CE SW8081B% 1103%TCMX (Surrogate Rec) 09/10/15 CE SW8081B% 1

Polychlorinated BiphenylsNDPCB-1016 0.050 09/10/15 AW E608/SW8082Aug/L0.050 1NDPCB-1221 0.050 09/10/15 AW E608/SW8082Aug/L0.050 1NDPCB-1232 0.050 09/10/15 AW E608/SW8082Aug/L0.050 1NDPCB-1242 0.050 09/10/15 AW E608/SW8082Aug/L0.050 1NDPCB-1248 0.050 09/10/15 AW E608/SW8082Aug/L0.050 1NDPCB-1254 0.050 09/10/15 AW E608/SW8082Aug/L0.050 1NDPCB-1260 0.050 09/10/15 AW E608/SW8082Aug/L0.050 1NDPCB-1262 0.050 09/10/15 AW E608/SW8082Aug/L0.050 1NDPCB-1268 0.050 09/10/15 AW E608/SW8082Aug/L0.050 1

QA/QC Surrogates71% DCBP 09/10/15 AW 30 - 150 %% 181% TCMX 09/10/15 AW 30 - 150 %% 1

VolatilesND1,1,1,2-Tetrachloroethane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,1,1-Trichloroethane 5.0 09/10/15 MH SW8260Cug/L0.25 1ND1,1,2,2-Tetrachloroethane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,1,2-Trichloroethane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,1-Dichloroethane 5.0 09/10/15 MH SW8260Cug/L0.25 1ND1,1-Dichloroethene 1.0 09/10/15 MH SW8260Cug/L0.25 1

Page 2 of 24 Ver 2




LOD/MDL Dilution

ND1,1-Dichloropropene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2,3-Trichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2,3-Trichloropropane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2,4-Trichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2,4-Trimethylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2-Dibromo-3-chloropropane 1.0 09/10/15 MH SW8260Cug/L0.50 1ND1,2-Dibromoethane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2-Dichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2-Dichloroethane 0.60 09/10/15 MH SW8260Cug/L0.25 1ND1,2-Dichloropropane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,3,5-Trimethylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,3-Dichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,3-Dichloropropane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,4-Dichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND2,2-Dichloropropane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND2-Chlorotoluene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND2-Hexanone 2.5 09/10/15 MH SW8260Cug/L2.5 1ND2-Isopropyltoluene 1.0 09/10/15 MH SW8260Cug/L 10.25 1ND4-Chlorotoluene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND4-Methyl-2-pentanone 2.5 09/10/15 MH SW8260Cug/L2.5 12.7Acetone 5.0 09/10/15 MH SW8260Cug/L2.5 1JSNDAcrolein 5.0 09/10/15 MH SW8260Cug/L2.5 1NDAcrylonitrile 5.0 09/10/15 MH SW8260Cug/L2.5 1NDBenzene 0.70 09/10/15 MH SW8260Cug/L0.25 1NDBromobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDBromochloromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDBromodichloromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDBromoform 5.0 09/10/15 MH SW8260Cug/L0.25 1NDBromomethane 5.0 09/10/15 MH SW8260Cug/L0.25 1NDCarbon Disulfide 1.0 09/10/15 MH SW8260Cug/L0.25 1NDCarbon tetrachloride 1.0 09/10/15 MH SW8260Cug/L0.25 1NDChlorobenzene 5.0 09/10/15 MH SW8260Cug/L0.25 1NDChloroethane 5.0 09/10/15 MH SW8260Cug/L0.25 1NDChloroform 5.0 09/10/15 MH SW8260Cug/L0.25 10.76Chloromethane 5.0 09/10/15 MH SW8260Cug/L0.25 1J8.4cis-1,2-Dichloroethene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDcis-1,3-Dichloropropene 0.40 09/10/15 MH SW8260Cug/L0.25 1NDDibromochloromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDDibromomethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDDichlorodifluoromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDEthylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDHexachlorobutadiene 0.5 09/10/15 MH SW8260Cug/L0.10 1NDIsopropylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDm&p-Xylene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDMethyl ethyl ketone 2.5 09/10/15 MH SW8260Cug/L2.5 1NDMethyl t-butyl ether (MTBE) 1.0 09/10/15 MH SW8260Cug/L0.25 1NDMethylene chloride 3.0 09/10/15 MH SW8260Cug/L1.0 1NDNaphthalene 1.0 09/10/15 MH SW8260Cug/L1.0 1NDn-Butylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1

Page 3 of 24 Ver 2




LOD/MDL Dilution

NDn-Propylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDo-Xylene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDp-Isopropyltoluene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDsec-Butylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDStyrene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDtert-Butylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDTetrachloroethene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDTetrahydrofuran (THF) 5.0 09/10/15 MH SW8260Cug/L 12.5 10.56Toluene 1.0 09/10/15 MH SW8260Cug/L0.25 1JNDtrans-1,2-Dichloroethene 5.0 09/10/15 MH SW8260Cug/L0.25 1NDtrans-1,3-Dichloropropene 0.40 09/10/15 MH SW8260Cug/L0.25 1NDtrans-1,4-dichloro-2-butene 2.5 09/10/15 MH SW8260Cug/L2.5 14.0Trichloroethene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDTrichlorofluoromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDTrichlorotrifluoroethane 1.0 09/10/15 MH SW8260Cug/L0.25 10.96Vinyl chloride 1.0 09/10/15 MH SW8260Cug/L0.25 1J

QA/QC Surrogates101% 1,2-dichlorobenzene-d4 09/10/15 MH 70 - 130 %% 199% Bromofluorobenzene 09/10/15 MH 70 - 130 %% 1101% Dibromofluoromethane 09/10/15 MH 70 - 130 %% 197% Toluene-d8 09/10/15 MH 70 - 130 %% 1

SemivolatilesND1,2,4-Trichlorobenzene 5.0 09/14/15 DD SW8270Dug/L1.5 1ND1,2-Dichlorobenzene 1.0 09/14/15 DD SW8270Dug/L1.0 1ND1,2-Diphenylhydrazine 5.0 09/14/15 DD SW8270Dug/L1.6 1ND1,3-Dichlorobenzene 1.0 09/14/15 DD SW8270Dug/L1.0 1ND1,4-Dichlorobenzene 1.0 09/14/15 DD SW8270Dug/L1.0 1ND2,4,5-Trichlorophenol 1.0 09/14/15 DD SW8270Dug/L1.0 1ND2,4,6-Trichlorophenol 1.0 09/14/15 DD SW8270Dug/L1.0 1ND2,4-Dichlorophenol 1.0 09/14/15 DD SW8270Dug/L1.0 1ND2,4-Dimethylphenol 1.0 09/14/15 DD SW8270Dug/L1.0 1ND2,4-Dinitrophenol 1.0 09/14/15 DD SW8270Dug/L1.0 1ND2,4-Dinitrotoluene 5.0 09/14/15 DD SW8270Dug/L2.0 1ND2,6-Dinitrotoluene 5.0 09/14/15 DD SW8270Dug/L1.6 1ND2-Chloronaphthalene 5.0 09/14/15 DD SW8270Dug/L1.4 1ND2-Chlorophenol 1.0 09/14/15 DD SW8270Dug/L1.0 1ND2-Methylnaphthalene 5.0 09/14/15 DD SW8270Dug/L1.5 1ND2-Methylphenol (o-cresol) 1.0 09/14/15 DD SW8270Dug/L1.0 1ND2-Nitroaniline 5.0 09/14/15 DD SW8270Dug/L5.0 1ND2-Nitrophenol 1.0 09/14/15 DD SW8270Dug/L1.0 1ND3&4-Methylphenol (m&p-cresol) 1.0 09/14/15 DD SW8270Dug/L1.0 1ND3,3'-Dichlorobenzidine 5.0 09/14/15 DD SW8270Dug/L2.4 1ND3-Nitroaniline 5.0 09/14/15 DD SW8270Dug/L5.0 1ND4,6-Dinitro-2-methylphenol 1.0 09/14/15 DD SW8270Dug/L1.0 1ND4-Bromophenyl phenyl ether 5.0 09/14/15 DD SW8270Dug/L1.5 1ND4-Chloro-3-methylphenol 1.0 09/14/15 DD SW8270Dug/L1.0 1ND4-Chloroaniline 3.5 09/14/15 DD SW8270Dug/L2.3 1ND4-Chlorophenyl phenyl ether 5.0 09/14/15 DD SW8270Dug/L1.7 1ND4-Nitroaniline 5.0 09/14/15 DD SW8270Dug/L1.7 1

Page 4 of 24 Ver 2




LOD/MDL Dilution

ND4-Nitrophenol 1.0 09/14/15 DD SW8270Dug/L1.0 1NDAcenaphthene 5.0 09/14/15 DD SW8270Dug/L1.5 1NDAcetophenone 5.0 09/14/15 DD SW8270Dug/L1.6 1NDAniline 3.5 09/14/15 DD SW8270Dug/L5.0 1NDAnthracene 5.0 09/14/15 DD SW8270Dug/L1.6 1NDBenzidine 4.5 09/14/15 DD SW8270Dug/L2.9 1NDBenzoic acid 25 09/14/15 DD SW8270Dug/L10 1NDBenzyl butyl phthalate 5.0 09/14/15 DD SW8270Dug/L1.3 1NDBis(2-chloroethoxy)methane 5.0 09/14/15 DD SW8270Dug/L1.4 1NDBis(2-chloroethyl)ether 1.0 09/14/15 DD SW8270Dug/L1.0 1NDBis(2-chloroisopropyl)ether 5.0 09/14/15 DD SW8270Dug/L1.4 1NDCarbazole 25 09/14/15 DD SW8270Dug/L3.8 1NDDibenzofuran 5.0 09/14/15 DD SW8270Dug/L1.5 1NDDiethyl phthalate 5.0 09/14/15 DD SW8270Dug/L1.6 1NDDimethylphthalate 5.0 09/14/15 DD SW8270Dug/L1.6 1NDDi-n-butylphthalate 5.0 09/14/15 DD SW8270Dug/L1.3 1NDDi-n-octylphthalate 5.0 09/14/15 DD SW8270Dug/L1.3 1NDFluoranthene 5.0 09/14/15 DD SW8270Dug/L1.6 1NDFluorene 5.0 09/14/15 DD SW8270Dug/L1.7 1NDHexachlorocyclopentadiene 5.0 09/14/15 DD SW8270Dug/L1.5 1NDIsophorone 5.0 09/14/15 DD SW8270Dug/L1.4 1NDNaphthalene 5.0 09/14/15 DD SW8270Dug/L1.4 1NDN-Nitrosodimethylamine 1.0 09/14/15 DD SW8270Dug/L1.0 1NDN-Nitrosodi-n-propylamine 5.0 09/14/15 DD SW8270Dug/L1.6 1NDN-Nitrosodiphenylamine 5.0 09/14/15 DD SW8270Dug/L1.9 1NDPhenol 1.0 09/14/15 DD SW8270Dug/L1.0 1NDPyrene 5.0 09/14/15 DD SW8270Dug/L1.7 1NDPyridine 10 09/14/15 DD SW8270Dug/L1.2 1

QA/QC Surrogates99% 2,4,6-Tribromophenol 09/14/15 DD 15 - 110 %% 176% 2-Fluorobiphenyl 09/14/15 DD 30 - 130 %% 147% 2-Fluorophenol 09/14/15 DD 15 - 110 %% 166% Nitrobenzene-d5 09/14/15 DD 30 - 130 %% 146% Phenol-d5 09/14/15 DD 15 - 110 %% 197% Terphenyl-d14 09/14/15 DD 30 - 130 %% 1

SemivolatilesND1,2,4,5-Tetrachlorobenzene 0.50 09/11/15 D/P SW8270D (SIM)ug/L0.50 1NDAcenaphthylene 0.10 09/11/15 D/P SW8270D (SIM)ug/L0.10 10.03Benz(a)anthracene 0.02 09/11/15 D/P SW8270D (SIM)ug/L0.02 10.02Benzo(a)pyrene 0.02 09/11/15 D/P SW8270D (SIM)ug/L0.02 10.02Benzo(b)fluoranthene 0.02 09/11/15 D/P SW8270D (SIM)ug/L0.02 1NDBenzo(ghi)perylene 0.02 09/11/15 D/P SW8270D (SIM)ug/L0.02 1NDBenzo(k)fluoranthene 0.02 09/11/15 D/P SW8270D (SIM)ug/L0.02 1NDBis(2-ethylhexyl)phthalate 1.0 09/11/15 D/P SW8270D (SIM)ug/L1.0 10.02Chrysene 0.02 09/11/15 D/P SW8270D (SIM)ug/L0.02 1NDDibenz(a,h)anthracene 0.02 09/11/15 D/P SW8270D (SIM)ug/L0.02 1NDHexachlorobenzene 0.02 09/11/15 D/P SW8270D (SIM)ug/L0.02 1NDHexachlorobutadiene 0.40 09/11/15 D/P SW8270D (SIM)ug/L0.40 1NDHexachloroethane 0.50 09/11/15 D/P SW8270D (SIM)ug/L0.50 1

Page 5 of 24 Ver 2




LOD/MDL Dilution

NDIndeno(1,2,3-cd)pyrene 0.02 09/11/15 D/P SW8270D (SIM)ug/L0.02 1NDNitrobenzene 0.10 09/11/15 D/P SW8270D (SIM)ug/L0.10 1NDPentachloronitrobenzene 0.10 09/11/15 D/P SW8270D (SIM)ug/L0.10 1NDPentachlorophenol 1.0 09/11/15 D/P SW8270D (SIM)ug/L1.0 1NDPhenanthrene 0.10 09/11/15 D/P SW8270D (SIM)ug/L0.10 1

QA/QC Surrogates95% 2,4,6-Tribromophenol 09/11/15 D/P 15 - 110 %% 169% 2-Fluorobiphenyl 09/11/15 D/P 30 - 130 %% 153% 2-Fluorophenol 09/11/15 D/P 15 - 110 %% 178% Nitrobenzene-d5 09/11/15 D/P 30 - 130 %% 154% Phenol-d5 09/11/15 D/P 15 - 110 %% 178% Terphenyl-d14 09/11/15 D/P 30 - 130 %% 1

Comments:

Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.

Pesticide Comment:Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, an elevated RL was reported.


Phyllis Shiller, Laboratory DirectorOctober 29, 2015

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.



RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level J=Estimated Below RL LOD=Limit of Detection MDL=Method Detection LimitQA/QC Surrogates: Surrogates are compounds (preceeded with a %) added by the lab to determine analysis efficiency. Surrogate results(%) listed in the report are not "detected" compounds.

Page 6 of 24 Ver 2





PR

Laboratory Data

14MW6

Phoenix ID: BJ89518

09/09/15 17:33




Date Time



SDG ID: GBJ89517


LOD/MDL Dilution

< 0.005Silver 0.005 09/10/15 EK SW6010Cmg/L0.001 19.02Aluminum 0.010 09/10/15 EK SW6010Cmg/L0.0024 10.007Arsenic - LDL 0.004 09/10/15 EK SW6010Cmg/L0.001 10.071Barium 0.010 09/10/15 EK SW6010Cmg/L0.001 1


< 0.004Cadmium 0.004 09/10/15 EK SW6010Cmg/L0.0005 10.006Cobalt 0.005 09/10/15 EK SW6010Cmg/L0.001 10.021Chromium 0.001 09/10/15 EK SW6010Cmg/L0.001 10.017Copper 0.005 09/10/15 EK SW6010Cmg/L0.001 112.4Iron 0.01 09/10/15 EK SW6010Cmg/L0.01 1


5.69Magnesium 0.01 09/10/15 EK SW6010Cmg/L0.001 10.468Manganese 0.005 09/10/15 EK SW6010Cmg/L0.001 175.5Sodium 1.0 09/10/15 EK SW6010Cmg/L1.0 100.017Nickel 0.004 09/10/15 EK SW6010Cmg/L0.001 10.006Lead 0.002 09/10/15 EK SW6010Cmg/L0.001 1


< 0.0005Thallium - LDL 0.0005 09/15/15 RS SW7010mg/L0.0005 10.022Vanadium 0.010 09/10/15 EK SW6010Cmg/L0.001 10.025Zinc 0.010 09/10/15 EK SW6010Cmg/L0.001 1


Page 7 of 24 Ver 2




LOD/MDL Dilution






Page 8 of 24 Ver 2




LOD/MDL Dilution

ND1,1-Dichloropropene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2,3-Trichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2,3-Trichloropropane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2,4-Trichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2,4-Trimethylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2-Dibromo-3-chloropropane 1.0 09/10/15 MH SW8260Cug/L0.50 1ND1,2-Dibromoethane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2-Dichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2-Dichloroethane 0.60 09/10/15 MH SW8260Cug/L0.25 1ND1,2-Dichloropropane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,3,5-Trimethylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,3-Dichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,3-Dichloropropane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,4-Dichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND2,2-Dichloropropane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND2-Chlorotoluene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND2-Hexanone 2.5 09/10/15 MH SW8260Cug/L2.5 1ND2-Isopropyltoluene 1.0 09/10/15 MH SW8260Cug/L 10.25 1ND4-Chlorotoluene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND4-Methyl-2-pentanone 2.5 09/10/15 MH SW8260Cug/L2.5 15.1Acetone 5.0 09/10/15 MH SW8260Cug/L2.5 1SNDAcrolein 5.0 09/10/15 MH SW8260Cug/L2.5 1NDAcrylonitrile 5.0 09/10/15 MH SW8260Cug/L2.5 12.1Benzene 0.70 09/10/15 MH SW8260Cug/L0.25 1NDBromobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDBromochloromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDBromodichloromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDBromoform 5.0 09/10/15 MH SW8260Cug/L0.25 1NDBromomethane 5.0 09/10/15 MH SW8260Cug/L0.25 1NDCarbon Disulfide 1.0 09/10/15 MH SW8260Cug/L0.25 1NDCarbon tetrachloride 1.0 09/10/15 MH SW8260Cug/L0.25 1NDChlorobenzene 5.0 09/10/15 MH SW8260Cug/L0.25 10.31Chloroethane 5.0 09/10/15 MH SW8260Cug/L0.25 1JNDChloroform 5.0 09/10/15 MH SW8260Cug/L0.25 10.63Chloromethane 5.0 09/10/15 MH SW8260Cug/L0.25 1J16cis-1,2-Dichloroethene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDcis-1,3-Dichloropropene 0.40 09/10/15 MH SW8260Cug/L0.25 1NDDibromochloromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDDibromomethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDDichlorodifluoromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDEthylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDHexachlorobutadiene 0.5 09/10/15 MH SW8260Cug/L0.10 1NDIsopropylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDm&p-Xylene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDMethyl ethyl ketone 2.5 09/10/15 MH SW8260Cug/L2.5 1NDMethyl t-butyl ether (MTBE) 1.0 09/10/15 MH SW8260Cug/L0.25 1NDMethylene chloride 3.0 09/10/15 MH SW8260Cug/L1.0 1NDNaphthalene 1.0 09/10/15 MH SW8260Cug/L1.0 1NDn-Butylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1

Page 9 of 24 Ver 2




LOD/MDL Dilution

NDn-Propylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDo-Xylene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDp-Isopropyltoluene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDsec-Butylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDStyrene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDtert-Butylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDTetrachloroethene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDTetrahydrofuran (THF) 5.0 09/10/15 MH SW8260Cug/L 12.5 1NDToluene 1.0 09/10/15 MH SW8260Cug/L0.25 10.40trans-1,2-Dichloroethene 5.0 09/10/15 MH SW8260Cug/L0.25 1JNDtrans-1,3-Dichloropropene 0.40 09/10/15 MH SW8260Cug/L0.25 1NDtrans-1,4-dichloro-2-butene 2.5 09/10/15 MH SW8260Cug/L2.5 11.4Trichloroethene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDTrichlorofluoromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDTrichlorotrifluoroethane 1.0 09/10/15 MH SW8260Cug/L0.25 10.28Vinyl chloride 1.0 09/10/15 MH SW8260Cug/L0.25 1J


CompletedClient MS/MSD 09/11/15

SemivolatilesND1,2,4-Trichlorobenzene 5.0 09/14/15 DD SW8270Dug/L1.5 1ND1,2-Dichlorobenzene 1.0 09/14/15 DD SW8270Dug/L1.0 1ND1,2-Diphenylhydrazine 5.0 09/14/15 DD SW8270Dug/L1.6 1ND1,3-Dichlorobenzene 1.0 09/14/15 DD SW8270Dug/L1.0 1ND1,4-Dichlorobenzene 1.0 09/14/15 DD SW8270Dug/L1.0 1ND2,4,5-Trichlorophenol 1.0 09/14/15 DD SW8270Dug/L1.0 1ND2,4,6-Trichlorophenol 1.0 09/14/15 DD SW8270Dug/L1.0 1ND2,4-Dichlorophenol 1.0 09/14/15 DD SW8270Dug/L1.0 1ND2,4-Dimethylphenol 1.0 09/14/15 DD SW8270Dug/L1.0 1ND2,4-Dinitrophenol 1.0 09/14/15 DD SW8270Dug/L1.0 1ND2,4-Dinitrotoluene 5.0 09/14/15 DD SW8270Dug/L2.0 1ND2,6-Dinitrotoluene 5.0 09/14/15 DD SW8270Dug/L1.6 1ND2-Chloronaphthalene 5.0 09/14/15 DD SW8270Dug/L1.4 1ND2-Chlorophenol 1.0 09/14/15 DD SW8270Dug/L1.0 1ND2-Methylnaphthalene 5.0 09/14/15 DD SW8270Dug/L1.5 1ND2-Methylphenol (o-cresol) 1.0 09/14/15 DD SW8270Dug/L1.0 1ND2-Nitroaniline 5.0 09/14/15 DD SW8270Dug/L5.0 1ND2-Nitrophenol 1.0 09/14/15 DD SW8270Dug/L1.0 1ND3&4-Methylphenol (m&p-cresol) 1.0 09/14/15 DD SW8270Dug/L1.0 1ND3,3'-Dichlorobenzidine 5.0 09/14/15 DD SW8270Dug/L2.4 1ND3-Nitroaniline 5.0 09/14/15 DD SW8270Dug/L5.0 1ND4,6-Dinitro-2-methylphenol 1.0 09/14/15 DD SW8270Dug/L1.0 1ND4-Bromophenyl phenyl ether 5.0 09/14/15 DD SW8270Dug/L1.5 1ND4-Chloro-3-methylphenol 1.0 09/14/15 DD SW8270Dug/L1.0 1ND4-Chloroaniline 3.5 09/14/15 DD SW8270Dug/L2.3 1ND4-Chlorophenyl phenyl ether 5.0 09/14/15 DD SW8270Dug/L1.7 1

Page 10 of 24 Ver 2




LOD/MDL Dilution

ND4-Nitroaniline 5.0 09/14/15 DD SW8270Dug/L1.7 1ND4-Nitrophenol 1.0 09/14/15 DD SW8270Dug/L1.0 1NDAcenaphthene 5.0 09/14/15 DD SW8270Dug/L1.5 1NDAcetophenone 5.0 09/14/15 DD SW8270Dug/L1.6 1NDAniline 3.5 09/14/15 DD SW8270Dug/L5.0 1NDAnthracene 5.0 09/14/15 DD SW8270Dug/L1.6 1NDBenzidine 4.5 09/14/15 DD SW8270Dug/L2.9 1NDBenzoic acid 25 09/14/15 DD SW8270Dug/L10 1NDBenzyl butyl phthalate 5.0 09/14/15 DD SW8270Dug/L1.3 1NDBis(2-chloroethoxy)methane 5.0 09/14/15 DD SW8270Dug/L1.4 1NDBis(2-chloroethyl)ether 1.0 09/14/15 DD SW8270Dug/L1.0 1NDBis(2-chloroisopropyl)ether 5.0 09/14/15 DD SW8270Dug/L1.4 1NDCarbazole 25 09/14/15 DD SW8270Dug/L3.8 1NDDibenzofuran 5.0 09/14/15 DD SW8270Dug/L1.5 1NDDiethyl phthalate 5.0 09/14/15 DD SW8270Dug/L1.6 1NDDimethylphthalate 5.0 09/14/15 DD SW8270Dug/L1.6 1NDDi-n-butylphthalate 5.0 09/14/15 DD SW8270Dug/L1.3 1NDDi-n-octylphthalate 5.0 09/14/15 DD SW8270Dug/L1.3 1NDFluoranthene 5.0 09/14/15 DD SW8270Dug/L1.6 1NDFluorene 5.0 09/14/15 DD SW8270Dug/L1.7 1NDHexachlorocyclopentadiene 5.0 09/14/15 DD SW8270Dug/L1.5 1NDIsophorone 5.0 09/14/15 DD SW8270Dug/L1.4 1NDNaphthalene 5.0 09/14/15 DD SW8270Dug/L1.4 1NDN-Nitrosodimethylamine 1.0 09/14/15 DD SW8270Dug/L1.0 1NDN-Nitrosodi-n-propylamine 5.0 09/14/15 DD SW8270Dug/L1.6 1NDN-Nitrosodiphenylamine 5.0 09/14/15 DD SW8270Dug/L1.9 1NDPhenol 1.0 09/14/15 DD SW8270Dug/L1.0 1NDPyrene 5.0 09/14/15 DD SW8270Dug/L1.7 1NDPyridine 10 09/14/15 DD SW8270Dug/L1.2 1


SemivolatilesND1,2,4,5-Tetrachlorobenzene 0.50 09/11/15 DD SW8270D (SIM)ug/L0.50 1NDAcenaphthylene 0.10 09/11/15 DD SW8270D (SIM)ug/L0.10 1NDBenz(a)anthracene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDBenzo(a)pyrene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDBenzo(b)fluoranthene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDBenzo(ghi)perylene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDBenzo(k)fluoranthene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDBis(2-ethylhexyl)phthalate 1.0 09/11/15 DD SW8270D (SIM)ug/L1.0 1NDChrysene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDDibenz(a,h)anthracene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDHexachlorobenzene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDHexachlorobutadiene 0.40 09/11/15 DD SW8270D (SIM)ug/L0.40 1

Page 11 of 24 Ver 2




LOD/MDL Dilution

NDHexachloroethane 0.50 09/11/15 DD SW8270D (SIM)ug/L0.50 1NDIndeno(1,2,3-cd)pyrene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDNitrobenzene 0.10 09/11/15 DD SW8270D (SIM)ug/L0.10 1NDPentachloronitrobenzene 0.10 09/11/15 DD SW8270D (SIM)ug/L0.10 1NDPentachlorophenol 0.80 09/11/15 DD SW8270D (SIM)ug/L0.80 1NDPhenanthrene 0.10 09/11/15 DD SW8270D (SIM)ug/L0.10 1


Comments:








Page 12 of 24 Ver 2





PR

Laboratory Data

14MW7

Phoenix ID: BJ89519

09/09/15 17:33




Date Time



SDG ID: GBJ89517


LOD/MDL Dilution



< 0.004Cadmium 0.004 09/10/15 EK SW6010Cmg/L0.0005 10.002Cobalt 0.005 09/10/15 EK SW6010Cmg/L0.001 1B0.004Chromium 0.001 09/10/15 EK SW6010Cmg/L0.001 10.003Copper 0.005 09/10/15 EK SW6010Cmg/L0.001 1B2.11Iron 0.01 09/10/15 EK SW6010Cmg/L0.01 1


6.26Magnesium 0.01 09/10/15 EK SW6010Cmg/L0.001 10.496Manganese 0.005 09/10/15 EK SW6010Cmg/L0.001 168.6Sodium 1.0 09/10/15 EK SW6010Cmg/L1.0 100.005Nickel 0.004 09/12/15 LK SW6010Cmg/L0.001 1

< 0.002Lead 0.002 09/10/15 EK SW6010Cmg/L0.001 1< 0.002Antimony 0.002 09/14/15 RS SW7010mg/L0.002 1< 0.002Selenium 0.002 09/11/15 RS SW7010mg/L0.001 1



Page 13 of 24 Ver 2




LOD/MDL Dilution






Page 14 of 24 Ver 2




LOD/MDL Dilution

ND1,1-Dichloropropene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2,3-Trichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2,3-Trichloropropane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2,4-Trichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2,4-Trimethylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2-Dibromo-3-chloropropane 1.0 09/10/15 MH SW8260Cug/L0.50 1ND1,2-Dibromoethane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2-Dichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2-Dichloroethane 0.60 09/10/15 MH SW8260Cug/L0.25 1ND1,2-Dichloropropane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,3,5-Trimethylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,3-Dichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,3-Dichloropropane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,4-Dichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND2,2-Dichloropropane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND2-Chlorotoluene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND2-Hexanone 2.5 09/10/15 MH SW8260Cug/L2.5 1ND2-Isopropyltoluene 1.0 09/10/15 MH SW8260Cug/L 10.25 1ND4-Chlorotoluene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND4-Methyl-2-pentanone 2.5 09/10/15 MH SW8260Cug/L2.5 13.9Acetone 5.0 09/10/15 MH SW8260Cug/L2.5 1JSNDAcrolein 5.0 09/10/15 MH SW8260Cug/L2.5 1NDAcrylonitrile 5.0 09/10/15 MH SW8260Cug/L2.5 10.28Benzene 0.70 09/10/15 MH SW8260Cug/L0.25 1JNDBromobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDBromochloromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDBromodichloromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDBromoform 5.0 09/10/15 MH SW8260Cug/L0.25 1NDBromomethane 5.0 09/10/15 MH SW8260Cug/L0.25 1NDCarbon Disulfide 1.0 09/10/15 MH SW8260Cug/L0.25 1NDCarbon tetrachloride 1.0 09/10/15 MH SW8260Cug/L0.25 1NDChlorobenzene 5.0 09/10/15 MH SW8260Cug/L0.25 1NDChloroethane 5.0 09/10/15 MH SW8260Cug/L0.25 1NDChloroform 5.0 09/10/15 MH SW8260Cug/L0.25 11.1Chloromethane 5.0 09/10/15 MH SW8260Cug/L0.25 1J14cis-1,2-Dichloroethene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDcis-1,3-Dichloropropene 0.40 09/10/15 MH SW8260Cug/L0.25 1NDDibromochloromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDDibromomethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDDichlorodifluoromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDEthylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDHexachlorobutadiene 0.5 09/10/15 MH SW8260Cug/L0.10 1NDIsopropylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDm&p-Xylene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDMethyl ethyl ketone 2.5 09/10/15 MH SW8260Cug/L2.5 1NDMethyl t-butyl ether (MTBE) 1.0 09/10/15 MH SW8260Cug/L0.25 1NDMethylene chloride 3.0 09/10/15 MH SW8260Cug/L1.0 1NDNaphthalene 1.0 09/10/15 MH SW8260Cug/L1.0 1NDn-Butylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1

Page 15 of 24 Ver 2




LOD/MDL Dilution

NDn-Propylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDo-Xylene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDp-Isopropyltoluene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDsec-Butylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDStyrene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDtert-Butylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDTetrachloroethene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDTetrahydrofuran (THF) 5.0 09/10/15 MH SW8260Cug/L 12.5 1NDToluene 1.0 09/10/15 MH SW8260Cug/L0.25 10.67trans-1,2-Dichloroethene 5.0 09/10/15 MH SW8260Cug/L0.25 1JNDtrans-1,3-Dichloropropene 0.40 09/10/15 MH SW8260Cug/L0.25 1NDtrans-1,4-dichloro-2-butene 2.5 09/10/15 MH SW8260Cug/L2.5 12.6Trichloroethene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDTrichlorofluoromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDTrichlorotrifluoroethane 1.0 09/10/15 MH SW8260Cug/L0.25 10.63Vinyl chloride 1.0 09/10/15 MH SW8260Cug/L0.25 1J



Page 16 of 24 Ver 2




LOD/MDL Dilution



SemivolatilesND1,2,4,5-Tetrachlorobenzene 0.50 09/11/15 DD SW8270D (SIM)ug/L0.50 1NDAcenaphthylene 0.10 09/11/15 DD SW8270D (SIM)ug/L0.10 10.02Benz(a)anthracene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDBenzo(a)pyrene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDBenzo(b)fluoranthene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDBenzo(ghi)perylene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDBenzo(k)fluoranthene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDBis(2-ethylhexyl)phthalate 1.0 09/11/15 DD SW8270D (SIM)ug/L1.0 10.02Chrysene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDDibenz(a,h)anthracene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDHexachlorobenzene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDHexachlorobutadiene 0.40 09/11/15 DD SW8270D (SIM)ug/L0.40 1NDHexachloroethane 0.50 09/11/15 DD SW8270D (SIM)ug/L0.50 1

Page 17 of 24 Ver 2




LOD/MDL Dilution

NDIndeno(1,2,3-cd)pyrene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDNitrobenzene 0.10 09/11/15 DD SW8270D (SIM)ug/L0.10 1NDPentachloronitrobenzene 0.10 09/11/15 DD SW8270D (SIM)ug/L0.10 1NDPentachlorophenol 0.80 09/11/15 DD SW8270D (SIM)ug/L0.80 1NDPhenanthrene 0.10 09/11/15 DD SW8270D (SIM)ug/L0.10 1


Comments:









Page 18 of 24 Ver 2





PR

Laboratory Data

DUPLICATE

Phoenix ID: BJ89520

09/09/15 17:33




Date Time



SDG ID: GBJ89517


LOD/MDL Dilution



< 0.004Cadmium 0.004 09/10/15 EK SW6010Cmg/L0.0005 1< 0.005Cobalt 0.005 09/10/15 EK SW6010Cmg/L0.001 10.001Chromium 0.001 09/10/15 EK SW6010Cmg/L0.001 10.002Copper 0.005 09/10/15 EK SW6010Cmg/L0.001 1B0.75Iron 0.01 09/10/15 EK SW6010Cmg/L0.01 1


1.65Magnesium 0.01 09/10/15 EK SW6010Cmg/L0.001 10.315Manganese 0.005 09/10/15 EK SW6010Cmg/L0.001 18.1Sodium 0.1 09/10/15 EK SW6010Cmg/L0.1 1

0.004Nickel 0.004 09/12/15 LK SW6010Cmg/L0.001 1B0.004Lead 0.002 09/10/15 EK SW6010Cmg/L0.001 1




Page 19 of 24 Ver 2

DUPLICATEPhoenix I.D.: BJ89520



LOD/MDL Dilution






Page 20 of 24 Ver 2




LOD/MDL Dilution

ND1,1-Dichloropropene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2,3-Trichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2,3-Trichloropropane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2,4-Trichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2,4-Trimethylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2-Dibromo-3-chloropropane 1.0 09/10/15 MH SW8260Cug/L0.50 1ND1,2-Dibromoethane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2-Dichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,2-Dichloroethane 0.60 09/10/15 MH SW8260Cug/L0.25 1ND1,2-Dichloropropane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,3,5-Trimethylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,3-Dichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,3-Dichloropropane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND1,4-Dichlorobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND2,2-Dichloropropane 1.0 09/10/15 MH SW8260Cug/L0.25 1ND2-Chlorotoluene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND2-Hexanone 2.5 09/10/15 MH SW8260Cug/L2.5 1ND2-Isopropyltoluene 1.0 09/10/15 MH SW8260Cug/L 10.25 1ND4-Chlorotoluene 1.0 09/10/15 MH SW8260Cug/L0.25 1ND4-Methyl-2-pentanone 2.5 09/10/15 MH SW8260Cug/L2.5 13.8Acetone 5.0 09/10/15 MH SW8260Cug/L2.5 1JSNDAcrolein 5.0 09/10/15 MH SW8260Cug/L2.5 1NDAcrylonitrile 5.0 09/10/15 MH SW8260Cug/L2.5 1NDBenzene 0.70 09/10/15 MH SW8260Cug/L0.25 1NDBromobenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDBromochloromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDBromodichloromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDBromoform 5.0 09/10/15 MH SW8260Cug/L0.25 1NDBromomethane 5.0 09/10/15 MH SW8260Cug/L0.25 1NDCarbon Disulfide 1.0 09/10/15 MH SW8260Cug/L0.25 1NDCarbon tetrachloride 1.0 09/10/15 MH SW8260Cug/L0.25 1NDChlorobenzene 5.0 09/10/15 MH SW8260Cug/L0.25 1NDChloroethane 5.0 09/10/15 MH SW8260Cug/L0.25 1NDChloroform 5.0 09/10/15 MH SW8260Cug/L0.25 11.7Chloromethane 5.0 09/10/15 MH SW8260Cug/L0.25 1J8.9cis-1,2-Dichloroethene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDcis-1,3-Dichloropropene 0.40 09/10/15 MH SW8260Cug/L0.25 1NDDibromochloromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDDibromomethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDDichlorodifluoromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDEthylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDHexachlorobutadiene 0.5 09/10/15 MH SW8260Cug/L0.10 1NDIsopropylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDm&p-Xylene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDMethyl ethyl ketone 2.5 09/10/15 MH SW8260Cug/L2.5 1NDMethyl t-butyl ether (MTBE) 1.0 09/10/15 MH SW8260Cug/L0.25 1NDMethylene chloride 3.0 09/10/15 MH SW8260Cug/L1.0 1NDNaphthalene 1.0 09/10/15 MH SW8260Cug/L1.0 1NDn-Butylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1

Page 21 of 24 Ver 2




LOD/MDL Dilution

NDn-Propylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDo-Xylene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDp-Isopropyltoluene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDsec-Butylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDStyrene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDtert-Butylbenzene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDTetrachloroethene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDTetrahydrofuran (THF) 5.0 09/10/15 MH SW8260Cug/L 12.5 10.64Toluene 1.0 09/10/15 MH SW8260Cug/L0.25 1JNDtrans-1,2-Dichloroethene 5.0 09/10/15 MH SW8260Cug/L0.25 1NDtrans-1,3-Dichloropropene 0.40 09/10/15 MH SW8260Cug/L0.25 1NDtrans-1,4-dichloro-2-butene 2.5 09/10/15 MH SW8260Cug/L2.5 13.3Trichloroethene 1.0 09/10/15 MH SW8260Cug/L0.25 1NDTrichlorofluoromethane 1.0 09/10/15 MH SW8260Cug/L0.25 1NDTrichlorotrifluoroethane 1.0 09/10/15 MH SW8260Cug/L0.25 11.3Vinyl chloride 1.0 09/10/15 MH SW8260Cug/L0.25 1



Page 22 of 24 Ver 2




LOD/MDL Dilution



SemivolatilesND1,2,4,5-Tetrachlorobenzene 0.50 09/11/15 DD SW8270D (SIM)ug/L0.50 1NDAcenaphthylene 0.10 09/11/15 DD SW8270D (SIM)ug/L0.10 1NDBenz(a)anthracene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDBenzo(a)pyrene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDBenzo(b)fluoranthene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDBenzo(ghi)perylene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDBenzo(k)fluoranthene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDBis(2-ethylhexyl)phthalate 1.0 09/11/15 DD SW8270D (SIM)ug/L1.0 10.03Chrysene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDDibenz(a,h)anthracene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDHexachlorobenzene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDHexachlorobutadiene 0.40 09/11/15 DD SW8270D (SIM)ug/L0.40 1NDHexachloroethane 0.50 09/11/15 DD SW8270D (SIM)ug/L0.50 1

Page 23 of 24 Ver 2




LOD/MDL Dilution

NDIndeno(1,2,3-cd)pyrene 0.02 09/11/15 DD SW8270D (SIM)ug/L0.02 1NDNitrobenzene 0.10 09/11/15 DD SW8270D (SIM)ug/L0.10 1NDPentachloronitrobenzene 0.10 09/11/15 DD SW8270D (SIM)ug/L0.10 1NDPentachlorophenol 0.80 09/11/15 DD SW8270D (SIM)ug/L0.80 1NDPhenanthrene 0.10 09/11/15 DD SW8270D (SIM)ug/L0.10 1


Comments:









Page 24 of 24 Ver 2

QA/QC Data

Parameter BlkBlank RL

MS%

MSD%

MSRPD

QA/QC ReportOctober 29, 2015



SDG I.D.: GBJ89517

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPD

LimitsSampleResult

DupResult

QA/QC Batch 319746 (mg/L), QC Sample No: BJ87737 (BJ89517, BJ89518, BJ89519, BJ89520)Antimony - Water 96.3 99.4BRL 3.2113NC 115 1.8 75 - 125 200.037 0.0350.003

Selenium - Water 93.1 96.2BRL 3.3105NC 108 2.8 75 - 125 20<0.020 <0.0500.005

Thallium - Water 86.7 85.9BRL 0.9108NC 111 2.7 75 - 125 20<0.010 <0.0100.001

QA/QC Batch 319775 (mg/L), QC Sample No: BJ89518 (BJ89517, BJ89518, BJ89519, BJ89520)

ICP Metals - AqueousAluminum NC NCBRL NC98.11.90 100 1.9 80 - 120 209.02 8.850.010

Arsenic 105 107BRL 1.998.7NC 101 2.3 80 - 120 200.007 0.0070.004

Barium 108 110BRL 1.81064.30 108 1.9 80 - 120 200.071 0.0680.002

Beryllium 107 108BRL 0.9102NC 103 1.0 80 - 120 20<0.001 <0.0010.001

Cadmium 104 106BRL 1.996.3NC 98.7 2.5 80 - 120 20<0.004 <0.0010.001

Calcium NC NC0.014 NC1002.50 103 3.0 80 - 120 206.49 6.330.010

Chromium 103 104BRL 1.097.29.10 99.6 2.4 80 - 120 200.021 0.0230.001

Cobalt 107 108BRL 0.9101NC 103 2.0 80 - 120 200.006 0.0060.002

Copper 106 106BRL 0.0102NC 105 2.9 80 - 120 200.017 0.0170.005

Iron NC NCBRL NC1021.60 104 1.9 80 - 120 2012.4 12.20.010

Lead 102 104BRL 1.997.1NC 98.7 1.6 80 - 120 200.006 0.0050.002

Magnesium NC NCBRL NC99.72.00 101 1.3 80 - 120 205.69 5.580.01

Manganese 106 107BRL 0.91002.20 103 3.0 80 - 120 200.468 0.4580.001

Nickel 103 104BRL 1.097.4NC 99.7 2.3 80 - 120 200.017 0.0170.001

Potassium 123 125BRL 1.61063.00 109 2.8 80 - 120 206.7 6.50.1

Silver 104 104BRL 0.099.5NC 102 2.5 70 - 130 30<0.005 <0.0010.001

Sodium NC NCBRL NC1071.60 111 3.7 80 - 120 2086.2 84.80.1

Vanadium 103 104BRL 1.098.9NC 101 2.1 80 - 120 200.022 0.0230.002

Zinc 104 105BRL 1.097.2NC 99.7 2.5 80 - 120 200.025 0.0260.002

QA/QC Batch 319801 (mg/L), QC Sample No: BJ89518 (BJ89517, BJ89518, BJ89519, BJ89520)Mercury - Water 95.5 108BRL 12.3107NC 108 0.9 75 - 125 20<0.0002 <0.00020.0002

QA/QC Batch 319890 (mg/L), QC Sample No: BJ89518 (BJ89518)Antimony - Water 90.6 92.5BRL 2.1107NC 106 0.9 75 - 125 20<0.002 <0.0030.003

Selenium - Water 81.5 81.9BRL 0.5104NC 107 2.8 75 - 125 20<0.002 <0.0050.005

Thallium - Water 79.7 80.8BRL 1.498.1NC 97.9 0.2 75 - 125 20<0.001 <0.0010.001

Page 1 of 6

QA/QC Data


MS%

MSD%

MSRPD




SDG I.D.: GBJ89517

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

QA/QC Batch 319780 (ug/L), QC Sample No: BJ89518 (BJ89517, BJ89518, BJ89519, BJ89520)

Pesticides - Ground Water4,4' -DDD 86 94ND 8.9100 103 3.0 30 - 150 200.003

4,4' -DDE 82 87ND 5.993 95 2.1 50 - 150 200.003

4,4' -DDT 94 103ND 9.198 102 4.0 30 - 150 270.003

a-BHC 93 95ND 2.196 99 3.1 30 - 150 200.005

a-Chlordane 87 90ND 3.499 102 3.0 30 - 150 200.005

Alachlor NA NAND NCNA NA NC 30 - 150 200.005

Aldrin 72 79ND 9.367 57 16.1 30 - 150 220.002

b-BHC 108 100ND 7.7103 107 3.8 30 - 150 200.005

Chlordane 87 89ND 2.395 98 3.1 30 - 150 200.050

d-BHC 78 74ND 5.388 90 2.2 30 - 150 200.005

Dieldrin 88 91ND 3.498 102 4.0 30 - 130 180.002

Endosulfan I 99 109ND 9.6106 108 1.9 30 - 150 200.005

Endosulfan II 91 96ND 5.3100 103 3.0 30 - 150 200.005

Endosulfan sulfate 85 86ND 1.290 94 4.3 50 - 120 200.005

Endrin 89 92ND 3.396 100 4.1 50 - 120 210.005

Endrin aldehyde 78 95ND 19.7106 112 5.5 30 - 150 200.005

Endrin ketone 91 92ND 1.198 103 5.0 30 - 150 200.005

g-BHC 96 97ND 1.098 101 3.0 50 - 120 150.002

g-Chlordane 87 89ND 2.395 98 3.1 30 - 130 200.005

Heptachlor 88 93ND 5.598 101 3.0 30 - 150 200.005

Heptachlor epoxide 84 88ND 4.798 102 4.0 50 - 150 200.005

Methoxychlor 80 76ND 5.192 97 5.3 30 - 150 200.005

Toxaphene NA NAND NCNA NA NC 30 - 150 200.20

% DCBP 70 7877 10.896 92 4.3 30 - 150 20%

% TCMX 110 11288 1.8105 104 1.0 30 - 150 20%


Polychlorinated Biphenyls - Ground WaterPCB-1016 90 92ND 2.278 80 2.5 30 - 120 200.050

PCB-1221 ND 30 - 150 200.050

PCB-1232 ND 30 - 150 200.050

PCB-1242 ND 30 - 150 200.050

PCB-1248 ND 30 - 150 200.050

PCB-1254 ND 30 - 150 200.050

PCB-1260 90 95ND 5.488 89 1.1 30 - 150 200.050

PCB-1262 ND 30 - 150 200.050

PCB-1268 ND 30 - 150 200.050

% DCBP (Surrogate Rec) 93 9687 3.2104 100 3.9 30 - 150 20%

% TCMX (Surrogate Rec) 98 9180 7.489 87 2.3 30 - 150 20%

Page 2 of 6

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ89517

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

QA/QC Batch 319982 (ug/L), QC Sample No: BJ89518 (BJ89518, BJ89519, BJ89520)

Volatiles - Ground Water1,1,1,2-Tetrachloroethane 106 98ND 7.895 102 7.1 70 - 130 301.0

1,1,1-Trichloroethane 108 98ND 9.795 97 2.1 70 - 130 301.0

1,1,2,2-Tetrachloroethane 113 107ND 5.595 107 11.9 70 - 130 300.50


1,1-Dichloroethane 108 101ND 6.796 100 4.1 70 - 130 301.0

1,1-Dichloroethene 110 101ND 8.599 100 1.0 70 - 130 301.0

1,1-Dichloropropene 105 97ND 7.994 95 1.1 70 - 130 301.0

1,2,3-Trichlorobenzene 106 107ND 0.993 103 10.2 70 - 130 301.0

1,2,3-Trichloropropane 106 101ND 4.893 104 11.2 70 - 130 301.0


1,2,4-Trimethylbenzene 98 91ND 7.498 96 2.1 70 - 130 301.0

1,2-Dibromo-3-chloropropane 108 106ND 1.989 105 16.5 70 - 130 301.0

1,2-Dibromoethane 109 102ND 6.693 103 10.2 70 - 130 301.0

1,2-Dichlorobenzene 104 98ND 5.995 100 5.1 70 - 130 301.0


1,2-Dichloropropane 105 98ND 6.993 100 7.3 70 - 130 301.0






2-Chlorotoluene 100 91ND 9.4102 99 3.0 70 - 130 301.0

2-Hexanone 107 104ND 2.879 99 22.5 70 - 130 305.0

2-Isopropyltoluene 105 98ND 6.9104 100 3.9 70 - 130 301.0


4-Methyl-2-pentanone 110 106ND 3.778 99 23.7 70 - 130 305.0

Acetone 94 93ND 1.179 96 19.4 70 - 130 305.0

Acrolein 109 106ND 2.892 112 19.6 70 - 130 305.0

Acrylonitrile 115 121ND 5.191 109 18.0 70 - 130 305.0

Benzene 98 95ND 3.196 98 2.1 70 - 130 300.70

Bromobenzene 102 94ND 8.297 99 2.0 70 - 130 301.0

Bromochloromethane 114 108ND 5.495 107 11.9 70 - 130 301.0

Bromodichloromethane 113 104ND 8.397 106 8.9 70 - 130 300.50

Bromoform 110 109ND 0.990 104 14.4 70 - 130 301.0

Bromomethane 77 89ND 14.592 105 13.2 70 - 130 301.0

Carbon Disulfide 108 98ND 9.7109 107 1.9 70 - 130 301.0

Carbon tetrachloride 109 98ND 10.693 95 2.1 70 - 130 301.0

Chlorobenzene 104 94ND 10.197 99 2.0 70 - 130 301.0

Chloroethane 100 92ND 8.3102 102 0.0 70 - 130 301.0

Chloroform 107 99ND 7.896 100 4.1 70 - 130 301.0

Chloromethane 83 86ND 3.685 90 5.7 70 - 130 301.0

cis-1,2-Dichloroethene NC NCND NC98 103 5.0 70 - 130 301.0

cis-1,3-Dichloropropene 107 98ND 8.893 104 11.2 70 - 130 300.40

Dibromochloromethane 113 104ND 8.398 108 9.7 70 - 130 300.50

Dibromomethane 112 101ND 10.392 103 11.3 70 - 130 301.0

Dichlorodifluoromethane 89 80ND 10.7112 114 1.8 70 - 130 301.0

Ethylbenzene 104 95ND 9.0100 99 1.0 70 - 130 301.0

Hexachlorobutadiene 117 109ND 7.1109 105 3.7 70 - 130 300.40

Isopropylbenzene 99 91ND 8.499 96 3.1 70 - 130 301.0

m&p-Xylene 101 93ND 8.298 97 1.0 70 - 130 301.0

Page 3 of 6

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ89517

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

Methyl ethyl ketone 114 120ND 5.181 106 26.7 70 - 130 305.0

Methyl t-butyl ether (MTBE) 113 109ND 3.687 106 19.7 70 - 130 301.0

Methylene chloride 103 97ND 6.089 95 6.5 70 - 130 301.0

Naphthalene 109 114ND 4.595 109 13.7 70 - 130 301.0

n-Butylbenzene 107 98ND 8.8103 101 2.0 70 - 130 301.0

n-Propylbenzene 94 85ND 10.196 92 4.3 70 - 130 301.0

o-Xylene 104 94ND 10.195 99 4.1 70 - 130 301.0

p-Isopropyltoluene 105 95ND 10.0103 99 4.0 70 - 130 301.0

sec-Butylbenzene 105 99ND 5.9103 99 4.0 70 - 130 301.0

Styrene 107 98ND 8.898 100 2.0 70 - 130 301.0

tert-Butylbenzene 102 94ND 8.2101 96 5.1 70 - 130 301.0

Tetrachloroethene 104 95ND 9.096 97 1.0 70 - 130 301.0

Tetrahydrofuran (THF) 114 119ND 4.383 104 22.5 70 - 130 302.5

Toluene 103 94ND 9.195 97 2.1 70 - 130 301.0

trans-1,2-Dichloroethene 109 103ND 5.7103 105 1.9 70 - 130 301.0

trans-1,3-Dichloropropene 111 103ND 7.593 105 12.1 70 - 130 300.40

trans-1,4-dichloro-2-butene 94 91ND 3.285 97 13.2 70 - 130 305.0

Trichloroethene 100 91ND 9.497 98 1.0 70 - 130 301.0

Trichlorofluoromethane 103 91ND 12.488 89 1.1 70 - 130 301.0

Trichlorotrifluoroethane 100 89ND 11.687 89 2.3 70 - 130 301.0

Vinyl chloride 105 94ND 11.1101 105 3.9 70 - 130 301.0

% 1,2-dichlorobenzene-d4 103 103101 0.0101 101 0.0 70 - 130 30%

% Bromofluorobenzene 103 10499 1.0100 101 1.0 70 - 130 30%

% Dibromofluoromethane 107 107102 0.099 104 4.9 70 - 130 30%

% Toluene-d8 100 9997 1.099 99 0.0 70 - 130 30%


Semivolatiles (SIM) - Ground Water1,2,4,5-Tetrachlorobenzene 69 61ND 12.370 71 1.4 30 - 130 200.50

Acenaphthylene 86 80ND 7.292 90 2.2 30 - 130 200.02

Benz(a)anthracene 55 54ND 1.891 91 0.0 30 - 130 200.05

Benzo(a)pyrene 46 45ND 2.290 86 4.5 30 - 130 200.02

Benzo(b)fluoranthene 54 51ND 5.797 103 6.0 30 - 130 200.02

Benzo(ghi)perylene 48 46ND 4.394 90 4.3 30 - 130 200.02

Benzo(k)fluoranthene 53 54ND 1.9103 104 1.0 30 - 130 200.02

Bis(2-ethylhexyl)phthalate 55 56ND 1.8104 110 5.6 30 - 130 200.1

Chrysene 53 50ND 5.891 91 0.0 30 - 130 200.02

Dibenz(a,h)anthracene 48 46ND 4.394 89 5.5 30 - 130 200.01

Hexachlorobenzene 66 59ND 11.2100 97 3.0 30 - 130 200.02


Hexachloroethane 56 62ND 10.255 67 19.7 30 - 130 200.05

Indeno(1,2,3-cd)pyrene 49 46ND 6.395 90 5.4 30 - 130 200.02

Nitrobenzene 70 71ND 1.471 76 6.8 30 - 130 200.05

Pentachloronitrobenzene 79 80ND 1.399 95 4.1 30 - 130 200.10

Pentachlorophenol 114 113ND 0.9106 101 4.8 30 - 130 200.20

Phenanthrene 86 90ND 4.591 91 0.0 30 - 130 200.02

% 2,4,6-Tribromophenol 99 9378 6.391 92 1.1 15 - 110 20%

% 2-Fluorobiphenyl 87 7472 16.184 85 1.2 30 - 130 20%

% 2-Fluorophenol 55 4655 17.841 51 21.7 r15 - 110 20%

% Nitrobenzene-d5 74 7665 2.770 78 10.8 30 - 130 20%

% Phenol-d5 64 4862 28.650 63 23.0 r15 - 110 20%

% Terphenyl-d14 52 4986 5.993 97 4.2 30 - 130 20%

Page 4 of 6

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ89517

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits


Semivolatiles - Ground Water1,2,4-Trichlorobenzene 72 67ND 7.277 77 0.0 30 - 130 203.5


1,2-Diphenylhydrazine 92 80ND 14.098 91 7.4 30 - 130 201.6



2,4,5-Trichlorophenol 97 91ND 6.495 96 1.0 30 - 130 201.0

2,4,6-Trichlorophenol 92 88ND 4.490 92 2.2 30 - 130 201.0

2,4-Dichlorophenol 78 75ND 3.984 81 3.6 30 - 130 201.0

2,4-Dimethylphenol 79 73ND 7.987 81 7.1 30 - 130 201.0

2,4-Dinitrophenol 90 92ND 2.284 89 5.8 30 - 130 201.0

2,4-Dinitrotoluene 98 93ND 5.299 98 1.0 m30 - 130 203.5

2,6-Dinitrotoluene 100 96ND 4.198 95 3.1 30 - 130 203.5

2-Chloronaphthalene 85 79ND 7.388 91 3.4 30 - 130 203.5

2-Chlorophenol 70 61ND 13.759 64 8.1 30 - 130 201.0

2-Methylnaphthalene 82 77ND 6.394 89 5.5 30 - 130 203.5

2-Methylphenol (o-cresol) 72 67ND 7.268 71 4.3 30 - 130 201.0

2-Nitroaniline 102 91ND 11.4103 101 2.0 30 - 130 203.5

2-Nitrophenol 80 66ND 19.278 73 6.6 30 - 130 201.0

3&4-Methylphenol (m&p-cresol) 84 79ND 6.182 85 3.6 30 - 130 201.0

3,3'-Dichlorobenzidine <10 <10ND NC61 65 6.3 m30 - 130 205.0

3-Nitroaniline 83 82ND 1.292 91 1.1 30 - 130 205.0

4,6-Dinitro-2-methylphenol 101 96ND 5.193 98 5.2 30 - 130 201.0

4-Bromophenyl phenyl ether 84 84ND 0.094 97 3.1 30 - 130 203.5

4-Chloro-3-methylphenol 95 89ND 6.5102 93 9.2 30 - 130 201.0

4-Chloroaniline 78 66ND 16.789 82 8.2 30 - 130 203.5

4-Chlorophenyl phenyl ether 88 87ND 1.198 96 2.1 30 - 130 201.0

4-Nitroaniline 99 91ND 8.499 97 2.0 30 - 130 205.0

4-Nitrophenol 115 102ND 12.0103 103 0.0 m30 - 130 201.0

Acenaphthene 80 73ND 9.286 86 0.0 30 - 130 201.5

Acetophenone 75 72ND 4.178 80 2.5 30 - 130 203.5

Aniline 71 43ND 49.160 69 14.0 r30 - 130 203.5

Anthracene 86 82ND 4.894 96 2.1 30 - 130 201.5

Benzidine <10 <10ND NC26 68 89.4 l,m,r30 - 130 204.5

Benzoic acid 122 107ND 13.1111 103 7.5 30 - 130 2010

Benzyl butyl phthalate 79 74ND 6.591 93 2.2 30 - 130 201.5

Bis(2-chloroethoxy)methane 80 73ND 9.291 84 8.0 30 - 130 203.5

Bis(2-chloroethyl)ether 60 61ND 1.758 69 17.3 30 - 130 201.0

Bis(2-chloroisopropyl)ether 74 67ND 9.967 70 4.4 30 - 130 201.0

Carbazole 100 94ND 6.297 99 2.0 30 - 130 205.0

Dibenzofuran 93 88ND 5.595 96 1.0 30 - 130 203.5

Diethyl phthalate 99 93ND 6.3100 97 3.0 30 - 130 201.5

Dimethylphthalate 96 90ND 6.597 96 1.0 30 - 130 201.5

Di-n-butylphthalate 90 84ND 6.998 103 5.0 30 - 130 201.5

Di-n-octylphthalate 54 49ND 9.796 99 3.1 30 - 130 201.5

Fluoranthene 83 77ND 7.596 101 5.1 30 - 130 201.5

Fluorene 94 90ND 4.398 100 2.0 30 - 130 201.5

Hexachlorocyclopentadiene 39 37ND 5.342 32 27.0 r30 - 130 203.5

Isophorone 79 72ND 9.396 85 12.2 30 - 130 203.5

Naphthalene 72 69ND 4.382 80 2.5 30 - 130 201.5

N-Nitrosodimethylamine 65 43ND 40.757 77 29.9 r30 - 130 201.0

Page 5 of 6

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ89517

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

N-Nitrosodi-n-propylamine 81 78ND 3.883 83 0.0 30 - 130 203.5

N-Nitrosodiphenylamine 64 59ND 8.188 84 4.7 30 - 130 203.5

Phenol 72 54ND 28.663 68 7.6 r30 - 130 201.0

Pyrene 81 75ND 7.797 101 4.0 30 - 130 201.5

Pyridine 42 22ND 62.539 58 39.2 m,r30 - 130 205.0

% 2,4,6-Tribromophenol 106 9371 13.1100 96 4.1 15 - 110 20%

% 2-Fluorobiphenyl 78 7278 8.085 84 1.2 30 - 130 20%

% 2-Fluorophenol 57 4548 23.545 52 14.4 r15 - 110 20%

% Nitrobenzene-d5 71 6466 10.471 71 0.0 30 - 130 20%

% Phenol-d5 66 5163 25.654 57 5.4 r15 - 110 20%

% Terphenyl-d14 55 53102 3.7101 106 4.8 30 - 130 20%

l = This parameter is outside laboratory LCS/LCSD specified recovery limits.m = This parameter is outside laboratory MS/MSD specified recovery limits.r = This parameter is outside laboratory RPD specified recovery limits.



October 29, 2015MS Dup - Matrix Spike Duplicate

RPD - Relative Percent Difference

LCS - Laboratory Control SampleLCSD - Laboratory Control Sample Duplicate

NC - No CriteriaIntf - Interference

Page 6 of 6

Sample Criteria Exceedences ReportThursday, October 29, 2015 Page 1 of 3


UnitsCriteria

GBJ89517 - EBCCriteria: NY: 375RRS, GW

RLCriteria

State: NY

$8260DP25R cis-1,2-Dichloroethene 58.4 1.0 ug/LBJ89517 NY / TOGS - Water Quality / GA Criteria 5$8260DP25R 1,2-Dibromoethane 0.0006ND 1.0 ug/LBJ89517 NY / TOGS - Water Quality / GA Criteria 0.0006$8260DP25R 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBJ89517 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBJ89517 NY / TOGS - Water Quality / GA Criteria 0.04$DP8270-SIMR Chrysene 0.0020.02 0.02 ug/LBJ89517 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benz(a)anthracene 0.0020.03 0.02 ug/LBJ89517 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(a)pyrene 0.0020.02 0.02 ug/LBJ89517 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.0020.02 0.02 ug/LBJ89517 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(k)fluoranthene 0.002ND 0.02 ug/LBJ89517 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.02 ug/LBJ89517 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.02 ug/LBJ89517 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(k)fluoranthene 0.002ND 0.02 ug/LBJ89517 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.0020.02 0.02 ug/LBJ89517 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benz(a)anthracene 0.0020.03 0.02 ug/LBJ89517 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Chrysene 0.0020.02 0.02 ug/LBJ89517 NY / TOGS - Water Quality / GA Criteria 0.002$DPPEST_GA Toxaphene 0.06ND 0.25 ug/LBJ89517 NY / TOGS - Water Quality / GA Criteria 0.06AL-WM Aluminum 0.11.65 0.010 mg/LBJ89517 NY / TOGS - Water Quality / GA Criteria 0.1FE-WMDP Iron 0.32.75 0.01 mg/LBJ89517 NY / TOGS - Water Quality / GA Criteria 0.3MN-WMDP Manganese 0.30.358 0.005 mg/LBJ89517 NY / TOGS - Water Quality / GA Criteria 0.3

$8260DP25R cis-1,2-Dichloroethene 516 1.0 ug/LBJ89518 NY / TOGS - Water Quality / GA Criteria 5$8260DP25R Benzene 0.72.1 0.70 ug/LBJ89518 NY / TAGM - Volatile Organics / Groundwater Standards 0.7$8260DP25R Benzene 12.1 0.70 ug/LBJ89518 NY / TOGS - Water Quality / GA Criteria 1$8260DP25R 1,2-Dibromoethane 0.0006ND 1.0 ug/LBJ89518 NY / TOGS - Water Quality / GA Criteria 0.0006$8260DP25R 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBJ89518 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBJ89518 NY / TOGS - Water Quality / GA Criteria 0.04$DP8270-SIMR Benzo(k)fluoranthene 0.002ND 0.02 ug/LBJ89518 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.02 ug/LBJ89518 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Chrysene 0.002ND 0.02 ug/LBJ89518 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.002ND 0.02 ug/LBJ89518 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(a)pyrene 0.002ND 0.02 ug/LBJ89518 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benz(a)anthracene 0.002ND 0.02 ug/LBJ89518 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.002ND 0.02 ug/LBJ89518 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benz(a)anthracene 0.002ND 0.02 ug/LBJ89518 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Chrysene 0.002ND 0.02 ug/LBJ89518 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.02 ug/LBJ89518 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(k)fluoranthene 0.002ND 0.02 ug/LBJ89518 NY / TOGS - Water Quality / GA Criteria 0.002$DPPEST_GA Toxaphene 0.06ND 0.25 ug/LBJ89518 NY / TOGS - Water Quality / GA Criteria 0.06AL-WM Aluminum 0.19.02 0.010 mg/LBJ89518 NY / TOGS - Water Quality / GA Criteria 0.1FE-WMDP Iron 0.312.4 0.01 mg/LBJ89518 NY / TOGS - Water Quality / GA Criteria 0.3MN-WMDP Manganese 0.30.468 0.005 mg/LBJ89518 NY / TOGS - Water Quality / GA Criteria 0.3NA-WM Sodium 2075.5 1.0 mg/LBJ89518 NY / TOGS - Water Quality / GA Criteria 20



UnitsCriteria


RLCriteria

State: NY

$8260DP25R cis-1,2-Dichloroethene 514 1.0 ug/LBJ89519 NY / TOGS - Water Quality / GA Criteria 5$8260DP25R 1,2-Dibromoethane 0.0006ND 1.0 ug/LBJ89519 NY / TOGS - Water Quality / GA Criteria 0.0006$8260DP25R 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBJ89519 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBJ89519 NY / TOGS - Water Quality / GA Criteria 0.04$DP8270-SIMR Benzo(k)fluoranthene 0.002ND 0.02 ug/LBJ89519 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benz(a)anthracene 0.0020.02 0.02 ug/LBJ89519 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(a)pyrene 0.002ND 0.02 ug/LBJ89519 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.002ND 0.02 ug/LBJ89519 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.02 ug/LBJ89519 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Chrysene 0.0020.02 0.02 ug/LBJ89519 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.02 ug/LBJ89519 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Chrysene 0.0020.02 0.02 ug/LBJ89519 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.002ND 0.02 ug/LBJ89519 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benz(a)anthracene 0.0020.02 0.02 ug/LBJ89519 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(k)fluoranthene 0.002ND 0.02 ug/LBJ89519 NY / TOGS - Water Quality / GA Criteria 0.002$DPPEST_GA Toxaphene 0.06ND 0.25 ug/LBJ89519 NY / TOGS - Water Quality / GA Criteria 0.06AL-WM Aluminum 0.11.84 0.010 mg/LBJ89519 NY / TOGS - Water Quality / GA Criteria 0.1FE-WMDP Iron 0.32.11 0.01 mg/LBJ89519 NY / TOGS - Water Quality / GA Criteria 0.3MN-WMDP Manganese 0.30.496 0.005 mg/LBJ89519 NY / TOGS - Water Quality / GA Criteria 0.3NA-WM Sodium 2068.6 1.0 mg/LBJ89519 NY / TOGS - Water Quality / GA Criteria 20

$8260DP25R cis-1,2-Dichloroethene 58.9 1.0 ug/LBJ89520 NY / TOGS - Water Quality / GA Criteria 5$8260DP25R 1,2-Dibromoethane 0.0006ND 1.0 ug/LBJ89520 NY / TOGS - Water Quality / GA Criteria 0.0006$8260DP25R 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBJ89520 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBJ89520 NY / TOGS - Water Quality / GA Criteria 0.04$DP8270-SIMR Benzo(k)fluoranthene 0.002ND 0.02 ug/LBJ89520 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benz(a)anthracene 0.002ND 0.02 ug/LBJ89520 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.02 ug/LBJ89520 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(a)pyrene 0.002ND 0.02 ug/LBJ89520 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.002ND 0.02 ug/LBJ89520 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Chrysene 0.0020.03 0.02 ug/LBJ89520 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.02 ug/LBJ89520 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Chrysene 0.0020.03 0.02 ug/LBJ89520 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.002ND 0.02 ug/LBJ89520 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benz(a)anthracene 0.002ND 0.02 ug/LBJ89520 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(k)fluoranthene 0.002ND 0.02 ug/LBJ89520 NY / TOGS - Water Quality / GA Criteria 0.002$DPPEST_GA Toxaphene 0.06ND 0.25 ug/LBJ89520 NY / TOGS - Water Quality / GA Criteria 0.06AL-WM Aluminum 0.10.569 0.010 mg/LBJ89520 NY / TOGS - Water Quality / GA Criteria 0.1FE-WMDP Iron 0.30.75 0.01 mg/LBJ89520 NY / TOGS - Water Quality / GA Criteria 0.3MN-WMDP Manganese 0.30.315 0.005 mg/LBJ89520 NY / TOGS - Water Quality / GA Criteria 0.3



UnitsCriteria


RLCriteria

State: NY


BJ90192 - BJ90195

Friday, October 23, 2015

Sample ID#s:


Project ID: 510 DRIGGS AVE., BROOKLYN

Sincerely yours,












Client: Environmental Business ConsultantsProject: 510 DRIGGS AVE., BROOKLYN





SDG I.D.: GBJ90192




MercuryMethods for Chemical Analyses of Water and Wastes, EPA, Environmental Monitoring Systems Laboratory Cincinnati (EMSL-CL), EPA-600/4-79-020, method 245.1USEPA SW-846 Test Methods for Evaluating Solid Waste Physical/Chemical Methods Update III, 7470A.



Polychlorinated Biphenyls (PCBs)/Pesticides:Environmental Protection Agency, EPA-600/4-79-020, Revised March 1983 (Methods 608) as printed in 40CFR part 136.


Semi-volatiles analysisUSEPA SW-846 Test Methods for Evaluating Solid Waste Physical/Chemical Methods 3rd Ed. Update IV, Method 8270D (SIM - selective ion monitoring mode).




SDG I.D.: GBJ90192


Sample Id Cross ReferenceClient Id Lab Id Matrix14MW1 BJ90192 GROUND WATER14MW3 BJ90193 GROUND WATER14MW4 BJ90194 GROUND WATERTRIP BLANK BJ90195 GROUND WATER




SDG I.D.: GBJ90192


Laboratory ChronicleThe samples in this delivery group were received at 4°C.


DateExtraction

DateAnalysis


MetBJ90192 Aluminum 09/09/15 09/10/15 09/12/15 LK YBJ90192 Aluminum (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90192 Antimony 09/09/15 09/10/15 09/14/15 RS YBJ90192 Antimony, (Dissolved) 09/09/15 09/11/15 09/14/15 RS YBJ90192 Arsenic - LDL 09/09/15 09/10/15 09/12/15 LK YBJ90192 Arsenic, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90192 Barium 09/09/15 09/10/15 09/12/15 LK YBJ90192 Barium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90192 Beryllium 09/09/15 09/10/15 09/12/15 LK YBJ90192 Beryllium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90192 Cadmium 09/09/15 09/10/15 09/12/15 LK YBJ90192 Cadmium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90192 Calcium 09/09/15 09/10/15 09/12/15 LK YBJ90192 Calcium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90192 Chromium 09/09/15 09/10/15 09/12/15 LK YBJ90192 Chromium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90192 Cobalt 09/09/15 09/10/15 09/12/15 LK YBJ90192 Cobalt, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90192 Copper 09/09/15 09/10/15 09/12/15 LK YBJ90192 Copper, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90192 Iron 09/09/15 09/10/15 09/12/15 LK YBJ90192 Iron, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90192 Lead 09/09/15 09/10/15 09/12/15 LK YBJ90192 Lead (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90192 Magnesium 09/09/15 09/10/15 09/12/15 LK YBJ90192 Magnesium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90192 Manganese 09/09/15 09/10/15 09/12/15 LK YBJ90192 Manganese, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90192 Mercury 09/09/15 09/11/15 09/11/15 RS YBJ90192 Mercury (Dissolved) 09/09/15 09/14/15 09/14/15 MA YBJ90192 Nickel 09/09/15 09/10/15 09/12/15 LK YBJ90192 Nickel, (Dissolved) 09/09/15 09/11/15 09/15/15 EK Y




SDG I.D.: GBJ90192


BJ90192 Pesticides 09/09/15 09/15/15 09/16/15 CE YBJ90192 Polychlorinated Biphenyls 09/09/15 09/10/15 09/11/15 AW YBJ90192 Potassium 09/09/15 09/10/15 09/12/15 LK YBJ90192 Potassium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90192 Selenium 09/09/15 09/10/15 09/11/15 RS YBJ90192 Selenium, (Dissolved) 09/09/15 09/11/15 09/16/15 RS YBJ90192 Semivolatiles 09/09/15 09/10/15 09/15/15 DD YBJ90192 Semivolatiles (SIM) 09/09/15 09/10/15 09/14/15 DD YBJ90192 Silver 09/09/15 09/10/15 09/12/15 LK YBJ90192 Silver (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90192 Sodium 09/09/15 09/10/15 09/11/15 LK YBJ90192 Sodium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90192 Thallium , (Dissolved) 09/09/15 09/11/15 09/15/15 RS YBJ90192 Thallium - LDL 09/09/15 09/10/15 09/15/15 RS YBJ90192 Vanadium 09/09/15 09/10/15 09/12/15 LK YBJ90192 Vanadium, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90192 Volatiles 09/09/15 09/15/15 09/15/15 MH YBJ90192 Zinc 09/09/15 09/10/15 09/12/15 LK YBJ90192 Zinc, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90193 Aluminum 09/09/15 09/10/15 09/12/15 LK YBJ90193 Aluminum (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90193 Antimony 09/09/15 09/10/15 09/14/15 RS YBJ90193 Antimony, (Dissolved) 09/09/15 09/11/15 09/14/15 RS YBJ90193 Arsenic - LDL 09/09/15 09/10/15 09/12/15 LK YBJ90193 Arsenic, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90193 Barium 09/09/15 09/10/15 09/12/15 LK YBJ90193 Barium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90193 Beryllium 09/09/15 09/10/15 09/12/15 LK YBJ90193 Beryllium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90193 Cadmium 09/09/15 09/10/15 09/12/15 LK YBJ90193 Cadmium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90193 Calcium 09/09/15 09/10/15 09/12/15 LK YBJ90193 Calcium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90193 Chromium 09/09/15 09/10/15 09/12/15 LK YBJ90193 Chromium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90193 Cobalt 09/09/15 09/10/15 09/12/15 LK YBJ90193 Cobalt, (Dissolved) 09/09/15 09/11/15 09/15/15 EK Y




SDG I.D.: GBJ90192


BJ90193 Copper 09/09/15 09/10/15 09/12/15 LK YBJ90193 Copper, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90193 Iron 09/09/15 09/10/15 09/12/15 LK YBJ90193 Iron, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90193 Lead 09/09/15 09/10/15 09/12/15 LK YBJ90193 Lead (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90193 Magnesium 09/09/15 09/10/15 09/12/15 LK YBJ90193 Magnesium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90193 Manganese 09/09/15 09/10/15 09/12/15 LK YBJ90193 Manganese, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90193 Mercury 09/09/15 09/11/15 09/11/15 RS YBJ90193 Mercury (Dissolved) 09/09/15 09/14/15 09/14/15 MA YBJ90193 Nickel 09/09/15 09/10/15 09/12/15 LK YBJ90193 Nickel, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90193 Pesticides 09/09/15 09/15/15 09/16/15 CE YBJ90193 Polychlorinated Biphenyls 09/09/15 09/10/15 09/11/15 AW YBJ90193 Potassium 09/09/15 09/10/15 09/12/15 LK YBJ90193 Potassium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90193 Selenium 09/09/15 09/10/15 09/11/15 RS YBJ90193 Selenium, (Dissolved) 09/09/15 09/11/15 09/16/15 RS YBJ90193 Semivolatiles 09/09/15 09/10/15 09/15/15 DD YBJ90193 Semivolatiles (SIM) 09/09/15 09/10/15 09/14/15 DD YBJ90193 Silver 09/09/15 09/10/15 09/12/15 LK YBJ90193 Silver (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90193 Sodium 09/09/15 09/10/15 09/11/15 LK YBJ90193 Sodium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90193 Thallium , (Dissolved) 09/09/15 09/11/15 09/15/15 RS YBJ90193 Thallium - LDL 09/09/15 09/10/15 09/15/15 RS YBJ90193 Vanadium 09/09/15 09/10/15 09/12/15 LK YBJ90193 Vanadium, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90193 Volatiles 09/09/15 09/14/15 09/14/15 MH YBJ90193 Zinc 09/09/15 09/10/15 09/12/15 LK YBJ90193 Zinc, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90194 Aluminum 09/09/15 09/10/15 09/12/15 LK YBJ90194 Aluminum (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90194 Antimony 09/09/15 09/10/15 09/14/15 RS YBJ90194 Antimony, (Dissolved) 09/09/15 09/11/15 09/14/15 RS Y




SDG I.D.: GBJ90192


BJ90194 Arsenic - LDL 09/09/15 09/10/15 09/12/15 LK YBJ90194 Arsenic, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90194 Barium 09/09/15 09/10/15 09/12/15 LK YBJ90194 Barium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90194 Beryllium 09/09/15 09/10/15 09/12/15 LK YBJ90194 Beryllium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90194 Cadmium 09/09/15 09/10/15 09/12/15 LK YBJ90194 Cadmium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90194 Calcium 09/09/15 09/10/15 09/12/15 LK YBJ90194 Calcium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90194 Chromium 09/09/15 09/10/15 09/12/15 LK YBJ90194 Chromium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90194 Cobalt 09/09/15 09/10/15 09/12/15 LK YBJ90194 Cobalt, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90194 Copper 09/09/15 09/10/15 09/12/15 LK YBJ90194 Copper, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90194 Iron 09/09/15 09/10/15 09/12/15 LK YBJ90194 Iron, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90194 Lead 09/09/15 09/10/15 09/12/15 LK YBJ90194 Lead (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90194 Magnesium 09/09/15 09/10/15 09/12/15 LK YBJ90194 Magnesium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90194 Manganese 09/09/15 09/10/15 09/12/15 LK YBJ90194 Manganese, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90194 Mercury 09/09/15 09/11/15 09/11/15 RS YBJ90194 Mercury (Dissolved) 09/09/15 09/14/15 09/14/15 MA YBJ90194 Nickel 09/09/15 09/10/15 09/12/15 LK YBJ90194 Nickel, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90194 Pesticides 09/09/15 09/15/15 09/16/15 CE YBJ90194 Polychlorinated Biphenyls 09/09/15 09/10/15 09/11/15 AW YBJ90194 Potassium 09/09/15 09/10/15 09/12/15 LK YBJ90194 Potassium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90194 Selenium 09/09/15 09/10/15 09/11/15 RS YBJ90194 Selenium, (Dissolved) 09/09/15 09/11/15 09/16/15 RS YBJ90194 Semivolatiles 09/09/15 09/10/15 09/15/15 DD YBJ90194 Semivolatiles (SIM) 09/09/15 09/10/15 09/14/15 DD YBJ90194 Silver 09/09/15 09/10/15 09/12/15 LK Y




SDG I.D.: GBJ90192


BJ90194 Silver (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90194 Sodium 09/09/15 09/10/15 09/11/15 LK YBJ90194 Sodium (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90194 Thallium , (Dissolved) 09/09/15 09/11/15 09/15/15 RS YBJ90194 Thallium - LDL 09/09/15 09/10/15 09/15/15 RS YBJ90194 Vanadium 09/09/15 09/10/15 09/12/15 LK YBJ90194 Vanadium, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90194 Volatiles 09/09/15 09/14/15 09/14/15 MH YBJ90194 Zinc 09/09/15 09/10/15 09/12/15 LK YBJ90194 Zinc, (Dissolved) 09/09/15 09/11/15 09/15/15 EK YBJ90195 Volatiles 09/09/15 09/11/15 09/11/15 MH Y




SDG I.D.: GBJ90192

8260 Volatile Organics:1,2-Dibromoethane, 1,2,3 Trichloropropane, and 1,2-Dibromo-3-chloropropane do not meet NY TOGS GA criteria, these compounds are analyzed by GC/FID method 504 or 8011 to achieve this criteria.

SIM Analysis:The lowest possible reporting limit under SIM conditions is 0.02 ug/L. The NY TOGS GA criteria for some PAHs is 0.002 ug/L. This level can not be achieved.

Toxaphene is reported to the lowest possible reporting level. The NY TOGS criteria for this compound can not be achieved.







TG

Laboratory Data

14MW1

Phoenix ID: BJ90192

09/10/1510:0017:04




Date Time



SDG ID: GBJ90192


LOD/MDL Dilution

< 0.005Silver 0.005 09/12/15 LK SW6010Cmg/L0.001 10.048Aluminum 0.010 09/12/15 LK SW6010Cmg/L0.0024 10.010Arsenic - LDL 0.004 09/12/15 LK SW6010Cmg/L0.001 10.087Barium 0.010 09/12/15 LK SW6010Cmg/L0.001 1

< 0.001Beryllium 0.001 09/12/15 LK SW6010Cmg/L0.001 180.3Calcium 0.010 09/12/15 LK SW6010Cmg/L0.003 1

< 0.004Cadmium 0.004 09/12/15 LK SW6010Cmg/L0.0005 1< 0.005Cobalt 0.005 09/12/15 LK SW6010Cmg/L0.001 10.004Chromium 0.001 09/12/15 LK SW6010Cmg/L0.001 1

< 0.005Copper 0.005 09/12/15 LK SW6010Cmg/L0.001 1< 0.005Silver (Dissolved) 0.005 09/15/15 EK SW6010Cmg/L0.001 1< 0.011Aluminum (Dissolved) 0.011 09/15/15 EK SW6010Cmg/L0.005 10.004Arsenic, (Dissolved) 0.003 09/15/15 EK SW6010Cmg/L0.004 10.070Barium (Dissolved) 0.011 09/15/15 EK SW6010Cmg/L0.001 1

< 0.001Beryllium (Dissolved) 0.001 09/15/15 EK SW6010Cmg/L0.001 172.4Calcium (Dissolved) 0.01 09/15/15 EK SW6010Cmg/L0.01 1

< 0.004Cadmium (Dissolved) 0.004 09/15/15 EK SW6010Cmg/L0.0005 1< 0.005Cobalt, (Dissolved) 0.005 09/15/15 EK SW6010Cmg/L0.001 10.001Chromium (Dissolved) 0.001 09/15/15 EK SW6010Cmg/L0.001 1

< 0.005Copper, (Dissolved) 0.005 09/15/15 EK SW6010Cmg/L0.001 10.04Iron, (Dissolved) 0.01 09/15/15 EK SW6010Cmg/L0.01 1

0.0002Mercury (Dissolved) 0.0002 09/14/15 MA SW7470Amg/L0.00015 110.7Potassium (Dissolved) 0.1 09/15/15 EK SW6010Cmg/L0.01 116.8Magnesium (Dissolved) 0.01 09/15/15 EK SW6010Cmg/L0.01 10.349Manganese, (Dissolved) 0.005 09/15/15 EK SW6010Cmg/L0.001 1103Sodium (Dissolved) 1.1 09/15/15 EK SW6010Cmg/L0.11 10

< 0.004Nickel, (Dissolved) 0.004 09/15/15 EK SW6010Cmg/L0.001 10.003Lead (Dissolved) 0.002 09/15/15 EK SW6010Cmg/L0.001 1

Page 1 of 21 Ver 2




LOD/MDL Dilution

< 0.003Antimony, (Dissolved) 0.003 09/14/15 RS SW7010mg/L0.003 1< 0.004Selenium, (Dissolved) 0.004 09/16/15 RS SW7010mg/L0.002 1< 0.001Thallium , (Dissolved) 0.001 09/15/15 RS SW7010mg/L0.001 1< 0.011Vanadium, (Dissolved) 0.011 09/15/15 EK SW6010Cmg/L0.001 1< 0.011Zinc, (Dissolved) 0.011 09/15/15 EK SW6010Cmg/L0.0012 1

2.38Iron 0.01 09/12/15 LK SW6010Cmg/L0.01 1< 0.0002Mercury 0.0002 09/11/15 RS SW7470Amg/L0.00015 1

10.9Potassium 0.1 09/12/15 LK SW6010Cmg/L0.1 118.8Magnesium 0.01 09/12/15 LK SW6010Cmg/L0.001 10.380Manganese 0.005 09/12/15 LK SW6010Cmg/L0.001 1110Sodium 1.0 09/11/15 LK SW6010Cmg/L1.0 10

0.002Nickel 0.004 09/12/15 LK SW6010Cmg/L0.001 1B0.002Lead 0.002 09/12/15 LK SW6010Cmg/L0.001 1B

< 0.002Antimony 0.002 09/14/15 RS SW7010mg/L0.002 1< 0.002Selenium 0.002 09/11/15 RS SW7010mg/L0.001 1< 0.001Thallium - LDL 0.001 09/15/15 RS SW7010mg/L0.001 1< 0.010Vanadium 0.010 09/12/15 LK SW6010Cmg/L0.001 1< 0.010Zinc 0.010 09/12/15 LK SW6010Cmg/L0.001 1

CompletedFiltration 09/11/15 AG 0.45um FilterCompletedDissolved Mercury Digestion 09/14/15 I/I SW7470ACompletedMercury Digestion 09/11/15 /I SW7470ACompletedPCB Extraction (2 Liter) 09/15/15 L SW3510CCompletedExtraction for Pest (2 Liter) 09/10/15 SW3510CCompletedSemi-Volatile Extraction 09/10/15 e/D/D SW3520CCompletedDissolved Metals Preparation 09/11/15 AGCompletedTotal Metals Digestion 09/10/15 AG SW3050B

PesticidesND4,4' -DDD 0.010 09/16/15 CE SW8081Bug/L0.010 1ND4,4' -DDE 0.010 09/16/15 CE SW8081Bug/L0.010 1ND4,4' -DDT 0.010 09/16/15 CE SW8081Bug/L0.010 1NDa-BHC 0.005 09/16/15 CE SW8081Bug/L0.005 1NDa-chlordane 0.010 09/16/15 CE SW8081Bug/L0.010 1NDAlachlor 0.075 09/16/15 CE SW8081Bug/L 10.075 1NDAldrin 0.003 09/16/15 CE SW8081Bug/L0.003 1NDb-BHC 0.015 09/16/15 CE SW8081Bug/L0.015 1NDChlordane 0.10 09/16/15 CE SW8081Bug/L0.10 1NDd-BHC 0.005 09/16/15 CE SW8081Bug/L0.005 1NDDieldrin 0.015 09/16/15 CE SW8081Bug/L0.015 1NDEndosulfan I 0.080 09/16/15 CE SW8081Bug/L0.080 1NDEndosulfan II 0.010 09/16/15 CE SW8081Bug/L0.010 1NDEndosulfan Sulfate 0.010 09/16/15 CE SW8081Bug/L0.010 1NDEndrin 0.010 09/16/15 CE SW8081Bug/L0.010 1NDEndrin Aldehyde 0.010 09/16/15 CE SW8081Bug/L0.010 1NDEndrin ketone 0.010 09/16/15 CE SW8081Bug/L0.010 1NDg-BHC (Lindane) 0.016 09/16/15 CE SW8081Bug/L0.016 1NDg-chlordane 0.010 09/16/15 CE SW8081Bug/L0.010 1NDHeptachlor 0.010 09/16/15 CE SW8081Bug/L0.010 1NDHeptachlor epoxide 0.010 09/16/15 CE SW8081Bug/L0.010 1NDMethoxychlor 0.10 09/16/15 CE SW8081Bug/L0.10 1

Page 2 of 21 Ver 2




LOD/MDL Dilution

NDToxaphene 0.25 09/16/15 CE SW8081Bug/L0.25 1




VolatilesND1,1,1,2-Tetrachloroethane 1.0 09/14/15 MH SW8260Cug/L0.25 1ND1,1,1-Trichloroethane 5.0 09/14/15 MH SW8260Cug/L0.25 1ND1,1,2,2-Tetrachloroethane 1.0 09/14/15 MH SW8260Cug/L0.25 1ND1,1,2-Trichloroethane 1.0 09/14/15 MH SW8260Cug/L0.25 10.671,1-Dichloroethane 5.0 09/14/15 MH SW8260Cug/L0.25 1J0.291,1-Dichloroethene 1.0 09/14/15 MH SW8260Cug/L0.25 1JND1,1-Dichloropropene 1.0 09/14/15 MH SW8260Cug/L0.25 1ND1,2,3-Trichlorobenzene 1.0 09/14/15 MH SW8260Cug/L0.25 1ND1,2,3-Trichloropropane 1.0 09/14/15 MH SW8260Cug/L0.25 1ND1,2,4-Trichlorobenzene 1.0 09/14/15 MH SW8260Cug/L0.25 1ND1,2,4-Trimethylbenzene 1.0 09/14/15 MH SW8260Cug/L0.25 1ND1,2-Dibromo-3-chloropropane 1.0 09/14/15 MH SW8260Cug/L0.50 1ND1,2-Dibromoethane 1.0 09/14/15 MH SW8260Cug/L0.25 1ND1,2-Dichlorobenzene 1.0 09/14/15 MH SW8260Cug/L0.25 1ND1,2-Dichloroethane 0.60 09/14/15 MH SW8260Cug/L0.25 1ND1,2-Dichloropropane 1.0 09/14/15 MH SW8260Cug/L0.25 1ND1,3,5-Trimethylbenzene 1.0 09/14/15 MH SW8260Cug/L0.25 1ND1,3-Dichlorobenzene 1.0 09/14/15 MH SW8260Cug/L0.25 1ND1,3-Dichloropropane 1.0 09/14/15 MH SW8260Cug/L0.25 1ND1,4-Dichlorobenzene 1.0 09/14/15 MH SW8260Cug/L0.25 1ND2,2-Dichloropropane 1.0 09/14/15 MH SW8260Cug/L0.25 1ND2-Chlorotoluene 1.0 09/14/15 MH SW8260Cug/L0.25 1ND2-Hexanone 2.5 09/14/15 MH SW8260Cug/L2.5 1ND2-Isopropyltoluene 1.0 09/14/15 MH SW8260Cug/L 10.25 1ND4-Chlorotoluene 1.0 09/14/15 MH SW8260Cug/L0.25 1ND4-Methyl-2-pentanone 2.5 09/14/15 MH SW8260Cug/L2.5 16.8Acetone 5.0 09/14/15 MH SW8260Cug/L2.5 1SNDAcrolein 5.0 09/14/15 MH SW8260Cug/L2.5 1NDAcrylonitrile 5.0 09/14/15 MH SW8260Cug/L2.5 118Benzene 0.70 09/14/15 MH SW8260Cug/L0.25 1

Page 3 of 21 Ver 2




LOD/MDL Dilution

NDBromobenzene 1.0 09/14/15 MH SW8260Cug/L0.25 1NDBromochloromethane 1.0 09/14/15 MH SW8260Cug/L0.25 1NDBromodichloromethane 1.0 09/14/15 MH SW8260Cug/L0.25 1NDBromoform 5.0 09/14/15 MH SW8260Cug/L0.25 1NDBromomethane 5.0 09/14/15 MH SW8260Cug/L0.25 1NDCarbon Disulfide 1.0 09/14/15 MH SW8260Cug/L0.25 1NDCarbon tetrachloride 1.0 09/14/15 MH SW8260Cug/L0.25 1NDChlorobenzene 5.0 09/14/15 MH SW8260Cug/L0.25 1NDChloroethane 5.0 09/14/15 MH SW8260Cug/L0.25 1NDChloroform 5.0 09/14/15 MH SW8260Cug/L0.25 10.74Chloromethane 5.0 09/14/15 MH SW8260Cug/L0.25 1J70cis-1,2-Dichloroethene 5.0 09/15/15 MH SW8260Cug/L1.3 5DNDcis-1,3-Dichloropropene 0.40 09/14/15 MH SW8260Cug/L0.25 1NDDibromochloromethane 1.0 09/14/15 MH SW8260Cug/L0.25 1NDDibromomethane 1.0 09/14/15 MH SW8260Cug/L0.25 1NDDichlorodifluoromethane 1.0 09/14/15 MH SW8260Cug/L0.25 1NDEthylbenzene 1.0 09/14/15 MH SW8260Cug/L0.25 1NDHexachlorobutadiene 1.0 09/14/15 MH SW8260Cug/L0.10 10.26Isopropylbenzene 1.0 09/14/15 MH SW8260Cug/L0.25 1JNDm&p-Xylene 1.0 09/14/15 MH SW8260Cug/L0.25 1NDMethyl ethyl ketone 2.5 09/14/15 MH SW8260Cug/L2.5 1NDMethyl t-butyl ether (MTBE) 1.0 09/14/15 MH SW8260Cug/L0.25 1NDMethylene chloride 3.0 09/14/15 MH SW8260Cug/L1.0 1NDNaphthalene 1.0 09/14/15 MH SW8260Cug/L1.0 1NDn-Butylbenzene 1.0 09/14/15 MH SW8260Cug/L0.25 1NDn-Propylbenzene 1.0 09/14/15 MH SW8260Cug/L0.25 1NDo-Xylene 1.0 09/14/15 MH SW8260Cug/L0.25 1NDp-Isopropyltoluene 1.0 09/14/15 MH SW8260Cug/L0.25 1NDsec-Butylbenzene 1.0 09/14/15 MH SW8260Cug/L0.25 1NDStyrene 1.0 09/14/15 MH SW8260Cug/L0.25 1NDtert-Butylbenzene 1.0 09/14/15 MH SW8260Cug/L0.25 1NDTetrachloroethene 1.0 09/14/15 MH SW8260Cug/L0.25 1NDTetrahydrofuran (THF) 5.0 09/14/15 MH SW8260Cug/L 12.5 1NDToluene 1.0 09/14/15 MH SW8260Cug/L0.25 16.3trans-1,2-Dichloroethene 5.0 09/14/15 MH SW8260Cug/L0.25 1NDtrans-1,3-Dichloropropene 0.40 09/14/15 MH SW8260Cug/L0.25 1NDtrans-1,4-dichloro-2-butene 2.5 09/14/15 MH SW8260Cug/L2.5 16.3Trichloroethene 1.0 09/14/15 MH SW8260Cug/L0.25 1NDTrichlorofluoromethane 1.0 09/14/15 MH SW8260Cug/L0.25 1NDTrichlorotrifluoroethane 1.0 09/14/15 MH SW8260Cug/L0.25 136Vinyl chloride 5.0 09/15/15 MH SW8260Cug/L1.3 5D


SemivolatilesND1,2,4-Trichlorobenzene 5.0 09/15/15 DD SW8270Dug/L1.5 1ND1,2-Dichlorobenzene 5.0 09/15/15 DD SW8270Dug/L1.4 1

Page 4 of 21 Ver 2




LOD/MDL Dilution

ND1,2-Diphenylhydrazine 5.0 09/15/15 DD SW8270Dug/L2.0 1ND1,3-Dichlorobenzene 5.0 09/15/15 DD SW8270Dug/L1.5 1ND1,4-Dichlorobenzene 5.0 09/15/15 DD SW8270Dug/L1.5 1ND2,4-Dinitrotoluene 5.0 09/15/15 DD SW8270Dug/L2.0 1ND2,6-Dinitrotoluene 5.0 09/15/15 DD SW8270Dug/L1.6 1ND2-Chloronaphthalene 5.0 09/15/15 DD SW8270Dug/L1.4 1ND2-Nitroaniline 20 09/15/15 DD SW8270Dug/L5.1 1ND3,3'-Dichlorobenzidine 20 09/15/15 DD SW8270Dug/L2.4 1ND3-Nitroaniline 20 09/15/15 DD SW8270Dug/L11 1ND4-Bromophenyl phenyl ether 5.0 09/15/15 DD SW8270Dug/L1.5 1ND4-Chloroaniline 20 09/15/15 DD SW8270Dug/L2.3 1ND4-Chlorophenyl phenyl ether 5.0 09/15/15 DD SW8270Dug/L1.7 1ND4-Nitroaniline 20 09/15/15 DD SW8270Dug/L1.7 1NDBenzidine 18 09/15/15 DD SW8270Dug/L2.9 1NDBenzoic acid 20 09/15/15 DD SW8270Dug/L10 1NDBenzyl Alcohol 5.0 09/15/15 DD SW8270Dug/L5.0 1NDBenzyl butyl phthalate 5.0 09/15/15 DD SW8270Dug/L1.3 1NDBis(2-chloroethoxy)methane 5.0 09/15/15 DD SW8270Dug/L1.4 1NDBis(2-chloroethyl)ether 5.0 09/15/15 DD SW8270Dug/L1.4 1NDBis(2-chloroisopropyl)ether 5.0 09/15/15 DD SW8270Dug/L 1,1O1.4 14.1Dibenzofuran 5.0 09/15/15 DD SW8270Dug/L1.5 1JNDDiethyl phthalate 5.0 09/15/15 DD SW8270Dug/L1.6 1NDDimethylphthalate 5.0 09/15/15 DD SW8270Dug/L1.6 1NDDi-n-butylphthalate 5.0 09/15/15 DD SW8270Dug/L1.3 1NDDi-n-octylphthalate 5.0 09/15/15 DD SW8270Dug/L1.3 1NDHexachlorocyclopentadiene 5.0 09/15/15 DD SW8270Dug/L1.5 1NDIsophorone 5.0 09/15/15 DD SW8270Dug/L1.4 1NDN-Nitrosodi-n-propylamine 5.0 09/15/15 DD SW8270Dug/L1.6 1NDN-Nitrosodiphenylamine 5.0 09/15/15 DD SW8270Dug/L1.9 1

QA/QC Surrogates71% 2-Fluorobiphenyl 09/15/15 DD 30 - 130 %% 170% Nitrobenzene-d5 09/15/15 DD 30 - 130 %% 1100% Terphenyl-d14 09/15/15 DD 30 - 130 %% 1

Semivolatiles (SIM)ND2-Methylnaphthalene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 16.0Acenaphthene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 11.8Acenaphthylene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1

0.65Anthracene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 10.06Benz(a)anthracene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDBenzo(a)pyrene 0.02 09/14/15 DD SW8270D (SIM)ug/L0.02 1NDBenzo(b)fluoranthene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDBenzo(ghi)perylene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDBenzo(k)fluoranthene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 10.11Bis(2-ethylhexyl)phthalate 0.05 09/14/15 DD SW8270D (SIM)ug/L B*0.05 1BNDChrysene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDDibenz(a,h)anthracene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 10.35Fluoranthene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 11.5Fluorene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDHexachlorobenzene 0.02 09/14/15 DD SW8270D (SIM)ug/L0.02 1

Page 5 of 21 Ver 2




LOD/MDL Dilution

NDHexachlorobutadiene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDHexachloroethane 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDIndeno(1,2,3-cd)pyrene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDNaphthalene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDNitrobenzene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDN-Nitrosodimethylamine 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 10.13Phenanthrene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 10.27Pyrene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1


Comments:





1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.1O = This parameter is not certified by NY NELAC for this matrix.B* = Present in blank, a bias is possible.




Page 6 of 21 Ver 2





TG

Laboratory Data

14MW3

Phoenix ID: BJ90193

09/10/158:30

17:04




Date Time



SDG ID: GBJ90192


LOD/MDL Dilution

< 0.005Silver 0.005 09/12/15 LK SW6010Cmg/L0.001 11.50Aluminum 0.010 09/12/15 LK SW6010Cmg/L0.0024 10.005Arsenic - LDL 0.004 09/12/15 LK SW6010Cmg/L0.001 10.084Barium 0.010 09/12/15 LK SW6010Cmg/L0.001 1


< 0.004Cadmium 0.004 09/12/15 LK SW6010Cmg/L0.0005 1< 0.005Cobalt 0.005 09/12/15 LK SW6010Cmg/L0.001 10.003Chromium 0.001 09/12/15 LK SW6010Cmg/L0.001 10.003Copper 0.005 09/12/15 LK SW6010Cmg/L0.001 1B

< 0.005Silver (Dissolved) 0.005 09/15/15 EK SW6010Cmg/L0.001 10.007Aluminum (Dissolved) 0.011 09/15/15 EK SW6010Cmg/L0.005 1B

< 0.003Arsenic, (Dissolved) 0.003 09/15/15 EK SW6010Cmg/L0.004 10.064Barium (Dissolved) 0.011 09/15/15 EK SW6010Cmg/L0.001 1


< 0.004Cadmium (Dissolved) 0.004 09/15/15 EK SW6010Cmg/L0.0005 1< 0.005Cobalt, (Dissolved) 0.005 09/15/15 EK SW6010Cmg/L0.001 1< 0.001Chromium (Dissolved) 0.001 09/15/15 EK SW6010Cmg/L0.001 1< 0.005Copper, (Dissolved) 0.005 09/15/15 EK SW6010Cmg/L0.001 1

0.05Iron, (Dissolved) 0.01 09/15/15 EK SW6010Cmg/L0.01 1< 0.0002Mercury (Dissolved) 0.0002 09/14/15 MA SW7470Amg/L0.00015 1

11.5Potassium (Dissolved) 0.1 09/15/15 EK SW6010Cmg/L0.01 119.0Magnesium (Dissolved) 0.01 09/15/15 EK SW6010Cmg/L0.01 10.230Manganese, (Dissolved) 0.005 09/15/15 EK SW6010Cmg/L0.001 176.5Sodium (Dissolved) 1.1 09/15/15 EK SW6010Cmg/L0.11 10

< 0.004Nickel, (Dissolved) 0.004 09/15/15 EK SW6010Cmg/L0.001 10.002Lead (Dissolved) 0.002 09/15/15 EK SW6010Cmg/L0.001 1

Page 7 of 21 Ver 2




LOD/MDL Dilution

< 0.003Antimony, (Dissolved) 0.003 09/14/15 RS SW7010mg/L0.003 1< 0.004Selenium, (Dissolved) 0.004 09/16/15 RS SW7010mg/L0.002 1< 0.001Thallium , (Dissolved) 0.001 09/15/15 RS SW7010mg/L0.001 1< 0.011Vanadium, (Dissolved) 0.011 09/15/15 EK SW6010Cmg/L0.001 1< 0.011Zinc, (Dissolved) 0.011 09/15/15 EK SW6010Cmg/L0.0012 1

2.40Iron 0.01 09/12/15 LK SW6010Cmg/L0.01 1< 0.0002Mercury 0.0002 09/11/15 RS SW7470Amg/L0.00015 1

11.1Potassium 0.1 09/12/15 LK SW6010Cmg/L0.1 122.0Magnesium 0.01 09/12/15 LK SW6010Cmg/L0.001 10.285Manganese 0.005 09/12/15 LK SW6010Cmg/L0.001 184.1Sodium 1.0 09/11/15 LK SW6010Cmg/L1.0 100.003Nickel 0.004 09/12/15 LK SW6010Cmg/L0.001 1B0.012Lead 0.002 09/12/15 LK SW6010Cmg/L0.001 1

< 0.002Antimony 0.002 09/14/15 RS SW7010mg/L0.002 1< 0.002Selenium 0.002 09/11/15 RS SW7010mg/L0.001 1< 0.001Thallium - LDL 0.001 09/15/15 RS SW7010mg/L0.001 10.003Vanadium 0.010 09/12/15 LK SW6010Cmg/L0.001 1B0.006Zinc 0.010 09/12/15 LK SW6010Cmg/L0.001 1B

CompletedFiltration 09/11/15 AG 0.45um FilterCompletedDissolved Mercury Digestion 09/14/15 I/I SW7470ACompletedMercury Digestion 09/11/15 /I SW7470ACompletedPCB Extraction (2 Liter) 09/15/15 L SW3510CCompletedExtraction for Pest (2 Liter) 09/10/15 SW3510CCompletedSemi-Volatile Extraction 09/10/15 E/D/D SW3520CCompletedDissolved Metals Preparation 09/11/15 AGCompletedTotal Metals Digestion 09/10/15 AG SW3050B


Page 8 of 21 Ver 2




LOD/MDL Dilution





VolatilesND1,1,1,2-Tetrachloroethane 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,1,1-Trichloroethane 5.0 09/12/15 MH SW8260Cug/L0.25 1ND1,1,2,2-Tetrachloroethane 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,1,2-Trichloroethane 1.0 09/12/15 MH SW8260Cug/L0.25 10.851,1-Dichloroethane 5.0 09/12/15 MH SW8260Cug/L0.25 1J5.81,1-Dichloroethene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,1-Dichloropropene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,2,3-Trichlorobenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,2,3-Trichloropropane 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,2,4-Trichlorobenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,2,4-Trimethylbenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,2-Dibromo-3-chloropropane 1.0 09/12/15 MH SW8260Cug/L0.50 1ND1,2-Dibromoethane 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,2-Dichlorobenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,2-Dichloroethane 0.60 09/12/15 MH SW8260Cug/L0.25 1ND1,2-Dichloropropane 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,3,5-Trimethylbenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,3-Dichlorobenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,3-Dichloropropane 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,4-Dichlorobenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND2,2-Dichloropropane 1.0 09/12/15 MH SW8260Cug/L0.25 1ND2-Chlorotoluene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND2-Hexanone 2.5 09/12/15 MH SW8260Cug/L2.5 1ND2-Isopropyltoluene 1.0 09/12/15 MH SW8260Cug/L 10.25 1ND4-Chlorotoluene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND4-Methyl-2-pentanone 2.5 09/12/15 MH SW8260Cug/L2.5 13.4Acetone 5.0 09/12/15 MH SW8260Cug/L2.5 1JSNDAcrolein 5.0 09/12/15 MH SW8260Cug/L2.5 1NDAcrylonitrile 5.0 09/12/15 MH SW8260Cug/L2.5 123Benzene 0.70 09/12/15 MH SW8260Cug/L0.25 1

Page 9 of 21 Ver 2




LOD/MDL Dilution

NDBromobenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDBromochloromethane 1.0 09/12/15 MH SW8260Cug/L0.25 1NDBromodichloromethane 1.0 09/12/15 MH SW8260Cug/L0.25 1NDBromoform 5.0 09/12/15 MH SW8260Cug/L0.25 1NDBromomethane 5.0 09/12/15 MH SW8260Cug/L0.25 1NDCarbon Disulfide 1.0 09/12/15 MH SW8260Cug/L0.25 1NDCarbon tetrachloride 1.0 09/12/15 MH SW8260Cug/L0.25 1NDChlorobenzene 5.0 09/12/15 MH SW8260Cug/L0.25 1NDChloroethane 5.0 09/12/15 MH SW8260Cug/L0.25 1NDChloroform 5.0 09/12/15 MH SW8260Cug/L0.25 1NDChloromethane 5.0 09/12/15 MH SW8260Cug/L0.25 1

1200cis-1,2-Dichloroethene 100 09/14/15 MH SW8260Cug/L25 100DNDcis-1,3-Dichloropropene 0.40 09/12/15 MH SW8260Cug/L0.25 1NDDibromochloromethane 1.0 09/12/15 MH SW8260Cug/L0.25 1NDDibromomethane 1.0 09/12/15 MH SW8260Cug/L0.25 1NDDichlorodifluoromethane 1.0 09/12/15 MH SW8260Cug/L0.25 10.66Ethylbenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1JNDHexachlorobutadiene 1.0 09/12/15 MH SW8260Cug/L0.10 10.35Isopropylbenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1J0.63m&p-Xylene 1.0 09/12/15 MH SW8260Cug/L0.25 1JNDMethyl ethyl ketone 2.5 09/12/15 MH SW8260Cug/L2.5 1NDMethyl t-butyl ether (MTBE) 1.0 09/12/15 MH SW8260Cug/L0.25 1NDMethylene chloride 3.0 09/12/15 MH SW8260Cug/L1.0 13.4Naphthalene 1.0 09/12/15 MH SW8260Cug/L1.0 1NDn-Butylbenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDn-Propylbenzene 1.0 09/12/15 MH SW8260Cug/L0.25 10.67o-Xylene 1.0 09/12/15 MH SW8260Cug/L0.25 1JNDp-Isopropyltoluene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDsec-Butylbenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDStyrene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDtert-Butylbenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDTetrachloroethene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDTetrahydrofuran (THF) 5.0 09/12/15 MH SW8260Cug/L 12.5 11.5Toluene 1.0 09/12/15 MH SW8260Cug/L0.25 112trans-1,2-Dichloroethene 5.0 09/12/15 MH SW8260Cug/L0.25 1NDtrans-1,3-Dichloropropene 0.40 09/12/15 MH SW8260Cug/L0.25 1NDtrans-1,4-dichloro-2-butene 2.5 09/12/15 MH SW8260Cug/L2.5 112Trichloroethene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDTrichlorofluoromethane 1.0 09/12/15 MH SW8260Cug/L0.25 1NDTrichlorotrifluoroethane 1.0 09/12/15 MH SW8260Cug/L0.25 1470Vinyl chloride 100 09/14/15 MH SW8260Cug/L25 100D



Page 10 of 21 Ver 2




LOD/MDL Dilution

ND1,2-Diphenylhydrazine 5.0 09/15/15 DD SW8270Dug/L2.0 1ND1,3-Dichlorobenzene 5.0 09/15/15 DD SW8270Dug/L1.5 1ND1,4-Dichlorobenzene 5.0 09/15/15 DD SW8270Dug/L1.5 1ND2,4-Dinitrotoluene 5.0 09/15/15 DD SW8270Dug/L2.0 1ND2,6-Dinitrotoluene 5.0 09/15/15 DD SW8270Dug/L1.6 1ND2-Chloronaphthalene 5.0 09/15/15 DD SW8270Dug/L1.4 1ND2-Nitroaniline 20 09/15/15 DD SW8270Dug/L5.1 1ND3,3'-Dichlorobenzidine 20 09/15/15 DD SW8270Dug/L2.4 1ND3-Nitroaniline 20 09/15/15 DD SW8270Dug/L11 1ND4-Bromophenyl phenyl ether 5.0 09/15/15 DD SW8270Dug/L1.5 1ND4-Chloroaniline 20 09/15/15 DD SW8270Dug/L2.3 1ND4-Chlorophenyl phenyl ether 5.0 09/15/15 DD SW8270Dug/L1.7 1ND4-Nitroaniline 20 09/15/15 DD SW8270Dug/L1.7 1NDBenzidine 18 09/15/15 DD SW8270Dug/L2.9 1NDBenzoic acid 20 09/15/15 DD SW8270Dug/L10 1NDBenzyl Alcohol 5.0 09/15/15 DD SW8270Dug/L5.0 1NDBenzyl butyl phthalate 5.0 09/15/15 DD SW8270Dug/L1.3 1NDBis(2-chloroethoxy)methane 5.0 09/15/15 DD SW8270Dug/L1.4 1NDBis(2-chloroethyl)ether 5.0 09/15/15 DD SW8270Dug/L1.4 1NDBis(2-chloroisopropyl)ether 5.0 09/15/15 DD SW8270Dug/L 1,1O1.4 17.6Dibenzofuran 5.0 09/15/15 DD SW8270Dug/L1.5 1NDDiethyl phthalate 5.0 09/15/15 DD SW8270Dug/L1.6 1NDDimethylphthalate 5.0 09/15/15 DD SW8270Dug/L1.6 1NDDi-n-butylphthalate 5.0 09/15/15 DD SW8270Dug/L1.3 1NDDi-n-octylphthalate 5.0 09/15/15 DD SW8270Dug/L1.3 1NDHexachlorocyclopentadiene 5.0 09/15/15 DD SW8270Dug/L1.5 1NDIsophorone 5.0 09/15/15 DD SW8270Dug/L1.4 1NDN-Nitrosodi-n-propylamine 5.0 09/15/15 DD SW8270Dug/L1.6 1NDN-Nitrosodiphenylamine 5.0 09/15/15 DD SW8270Dug/L1.9 1


Semivolatiles (SIM)0.122-Methylnaphthalene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 13.8Acenaphthene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 14.3Acenaphthylene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 12.3Anthracene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1

0.35Benz(a)anthracene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 10.29Benzo(a)pyrene 0.02 09/14/15 DD SW8270D (SIM)ug/L0.02 10.20Benzo(b)fluoranthene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 10.20Benzo(ghi)perylene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 10.27Benzo(k)fluoranthene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 10.12Bis(2-ethylhexyl)phthalate 0.05 09/14/15 DD SW8270D (SIM)ug/L B*0.05 1B0.31Chrysene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 10.07Dibenz(a,h)anthracene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 12.2Fluoranthene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 11.3Fluorene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDHexachlorobenzene 0.02 09/14/15 DD SW8270D (SIM)ug/L0.02 1

Page 11 of 21 Ver 2




LOD/MDL Dilution

NDHexachlorobutadiene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDHexachloroethane 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 10.18Indeno(1,2,3-cd)pyrene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 11.9Naphthalene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDNitrobenzene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDN-Nitrosodimethylamine 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 10.95Phenanthrene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 11.5Pyrene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1


Comments:








Page 12 of 21 Ver 2





TG

Laboratory Data

14MW4

Phoenix ID: BJ90194

09/10/1511:2017:04




Date Time



SDG ID: GBJ90192


LOD/MDL Dilution

< 0.005Silver 0.005 09/12/15 LK SW6010Cmg/L0.001 10.492Aluminum 0.010 09/12/15 LK SW6010Cmg/L0.0024 10.003Arsenic - LDL 0.004 09/12/15 LK SW6010Cmg/L0.001 1B0.021Barium 0.010 09/12/15 LK SW6010Cmg/L0.001 1


< 0.004Cadmium 0.004 09/12/15 LK SW6010Cmg/L0.0005 1< 0.005Cobalt 0.005 09/12/15 LK SW6010Cmg/L0.001 1< 0.001Chromium 0.001 09/12/15 LK SW6010Cmg/L0.001 10.002Copper 0.005 09/12/15 LK SW6010Cmg/L0.001 1B

< 0.005Silver (Dissolved) 0.005 09/15/15 EK SW6010Cmg/L0.001 10.140Aluminum (Dissolved) 0.011 09/15/15 EK SW6010Cmg/L0.005 1

< 0.003Arsenic, (Dissolved) 0.003 09/15/15 EK SW6010Cmg/L0.004 10.016Barium (Dissolved) 0.011 09/15/15 EK SW6010Cmg/L0.001 1


< 0.004Cadmium (Dissolved) 0.004 09/15/15 EK SW6010Cmg/L0.0005 1< 0.005Cobalt, (Dissolved) 0.005 09/15/15 EK SW6010Cmg/L0.001 1< 0.001Chromium (Dissolved) 0.001 09/15/15 EK SW6010Cmg/L0.001 1< 0.005Copper, (Dissolved) 0.005 09/15/15 EK SW6010Cmg/L0.001 1

0.02Iron, (Dissolved) 0.01 09/15/15 EK SW6010Cmg/L0.01 1< 0.0002Mercury (Dissolved) 0.0002 09/14/15 MA SW7470Amg/L0.00015 1

6.0Potassium (Dissolved) 0.1 09/15/15 EK SW6010Cmg/L0.01 15.37Magnesium (Dissolved) 0.01 09/15/15 EK SW6010Cmg/L0.01 10.112Manganese, (Dissolved) 0.005 09/15/15 EK SW6010Cmg/L0.001 155.4Sodium (Dissolved) 1.1 09/15/15 EK SW6010Cmg/L0.11 10

< 0.004Nickel, (Dissolved) 0.004 09/15/15 EK SW6010Cmg/L0.001 10.001Lead (Dissolved) 0.002 09/15/15 EK SW6010Cmg/L0.001 1B

Page 13 of 21 Ver 2




LOD/MDL Dilution

< 0.003Antimony, (Dissolved) 0.003 09/14/15 RS SW7010mg/L0.003 1< 0.004Selenium, (Dissolved) 0.004 09/16/15 RS SW7010mg/L0.002 1< 0.001Thallium , (Dissolved) 0.001 09/15/15 RS SW7010mg/L0.001 10.005Vanadium, (Dissolved) 0.011 09/15/15 EK SW6010Cmg/L0.001 1B

< 0.011Zinc, (Dissolved) 0.011 09/15/15 EK SW6010Cmg/L0.0012 10.40Iron 0.01 09/12/15 LK SW6010Cmg/L0.01 1

< 0.0002Mercury 0.0002 09/11/15 RS SW7470Amg/L0.00015 16.1Potassium 0.1 09/12/15 LK SW6010Cmg/L0.1 1

6.05Magnesium 0.01 09/12/15 LK SW6010Cmg/L0.001 10.152Manganese 0.005 09/12/15 LK SW6010Cmg/L0.001 158.7Sodium 1.0 09/11/15 LK SW6010Cmg/L1.0 100.003Nickel 0.004 09/12/15 LK SW6010Cmg/L0.001 1B0.004Lead 0.002 09/12/15 LK SW6010Cmg/L0.001 1

< 0.002Antimony 0.002 09/14/15 RS SW7010mg/L0.002 1< 0.002Selenium 0.002 09/11/15 RS SW7010mg/L0.001 1< 0.001Thallium - LDL 0.001 09/15/15 RS SW7010mg/L0.001 10.008Vanadium 0.010 09/12/15 LK SW6010Cmg/L0.001 1B

< 0.010Zinc 0.010 09/12/15 LK SW6010Cmg/L0.001 1CompletedFiltration 09/11/15 AG 0.45um FilterCompletedDissolved Mercury Digestion 09/14/15 I/I SW7470ACompletedMercury Digestion 09/11/15 /I SW7470ACompletedPCB Extraction (2 Liter) 09/15/15 L SW3510CCompletedExtraction for Pest (2 Liter) 09/10/15 SW3510CCompletedSemi-Volatile Extraction 09/10/15 E/D/D SW3520CCompletedDissolved Metals Preparation 09/11/15 AGCompletedTotal Metals Digestion 09/10/15 AG SW3050B


Page 14 of 21 Ver 2




LOD/MDL Dilution





VolatilesND1,1,1,2-Tetrachloroethane 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,1,1-Trichloroethane 5.0 09/12/15 MH SW8260Cug/L0.25 1ND1,1,2,2-Tetrachloroethane 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,1,2-Trichloroethane 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,1-Dichloroethane 5.0 09/12/15 MH SW8260Cug/L0.25 1ND1,1-Dichloroethene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,1-Dichloropropene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,2,3-Trichlorobenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,2,3-Trichloropropane 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,2,4-Trichlorobenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,2,4-Trimethylbenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,2-Dibromo-3-chloropropane 1.0 09/12/15 MH SW8260Cug/L0.50 1ND1,2-Dibromoethane 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,2-Dichlorobenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,2-Dichloroethane 0.60 09/12/15 MH SW8260Cug/L0.25 1ND1,2-Dichloropropane 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,3,5-Trimethylbenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,3-Dichlorobenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,3-Dichloropropane 1.0 09/12/15 MH SW8260Cug/L0.25 1ND1,4-Dichlorobenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND2,2-Dichloropropane 1.0 09/12/15 MH SW8260Cug/L0.25 1ND2-Chlorotoluene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND2-Hexanone 2.5 09/12/15 MH SW8260Cug/L2.5 1ND2-Isopropyltoluene 1.0 09/12/15 MH SW8260Cug/L 10.25 1ND4-Chlorotoluene 1.0 09/12/15 MH SW8260Cug/L0.25 1ND4-Methyl-2-pentanone 2.5 09/12/15 MH SW8260Cug/L2.5 1NDAcetone 5.0 09/12/15 MH SW8260Cug/L2.5 1NDAcrolein 5.0 09/12/15 MH SW8260Cug/L2.5 1NDAcrylonitrile 5.0 09/12/15 MH SW8260Cug/L2.5 10.33Benzene 0.70 09/12/15 MH SW8260Cug/L0.25 1J

Page 15 of 21 Ver 2




LOD/MDL Dilution

NDBromobenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDBromochloromethane 1.0 09/12/15 MH SW8260Cug/L0.25 1NDBromodichloromethane 1.0 09/12/15 MH SW8260Cug/L0.25 1NDBromoform 5.0 09/12/15 MH SW8260Cug/L0.25 1NDBromomethane 5.0 09/12/15 MH SW8260Cug/L0.25 1NDCarbon Disulfide 1.0 09/12/15 MH SW8260Cug/L0.25 1NDCarbon tetrachloride 1.0 09/12/15 MH SW8260Cug/L0.25 1NDChlorobenzene 5.0 09/12/15 MH SW8260Cug/L0.25 1NDChloroethane 5.0 09/12/15 MH SW8260Cug/L0.25 1NDChloroform 5.0 09/12/15 MH SW8260Cug/L0.25 1NDChloromethane 5.0 09/12/15 MH SW8260Cug/L0.25 151cis-1,2-Dichloroethene 5.0 09/14/15 MH SW8260Cug/L1.3 5DNDcis-1,3-Dichloropropene 0.40 09/12/15 MH SW8260Cug/L0.25 1NDDibromochloromethane 1.0 09/12/15 MH SW8260Cug/L0.25 1NDDibromomethane 1.0 09/12/15 MH SW8260Cug/L0.25 1NDDichlorodifluoromethane 1.0 09/12/15 MH SW8260Cug/L0.25 1NDEthylbenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDHexachlorobutadiene 1.0 09/12/15 MH SW8260Cug/L0.10 1NDIsopropylbenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDm&p-Xylene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDMethyl ethyl ketone 2.5 09/12/15 MH SW8260Cug/L2.5 1NDMethyl t-butyl ether (MTBE) 1.0 09/12/15 MH SW8260Cug/L0.25 1NDMethylene chloride 3.0 09/12/15 MH SW8260Cug/L1.0 1NDNaphthalene 1.0 09/12/15 MH SW8260Cug/L1.0 1NDn-Butylbenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDn-Propylbenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDo-Xylene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDp-Isopropyltoluene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDsec-Butylbenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDStyrene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDtert-Butylbenzene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDTetrachloroethene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDTetrahydrofuran (THF) 5.0 09/12/15 MH SW8260Cug/L 12.5 12.1Toluene 1.0 09/12/15 MH SW8260Cug/L0.25 1

0.82trans-1,2-Dichloroethene 5.0 09/12/15 MH SW8260Cug/L0.25 1JNDtrans-1,3-Dichloropropene 0.40 09/12/15 MH SW8260Cug/L0.25 1NDtrans-1,4-dichloro-2-butene 2.5 09/12/15 MH SW8260Cug/L2.5 12.4Trichloroethene 1.0 09/12/15 MH SW8260Cug/L0.25 1NDTrichlorofluoromethane 1.0 09/12/15 MH SW8260Cug/L0.25 1NDTrichlorotrifluoroethane 1.0 09/12/15 MH SW8260Cug/L0.25 10.75Vinyl chloride 1.0 09/12/15 MH SW8260Cug/L0.25 1J



Page 16 of 21 Ver 2




LOD/MDL Dilution

ND1,2-Diphenylhydrazine 5.0 09/15/15 DD SW8270Dug/L2.0 1ND1,3-Dichlorobenzene 5.0 09/15/15 DD SW8270Dug/L1.5 1ND1,4-Dichlorobenzene 5.0 09/15/15 DD SW8270Dug/L1.5 1ND2,4-Dinitrotoluene 5.0 09/15/15 DD SW8270Dug/L2.0 1ND2,6-Dinitrotoluene 5.0 09/15/15 DD SW8270Dug/L1.6 1ND2-Chloronaphthalene 5.0 09/15/15 DD SW8270Dug/L1.4 1ND2-Nitroaniline 20 09/15/15 DD SW8270Dug/L5.1 1ND3,3'-Dichlorobenzidine 20 09/15/15 DD SW8270Dug/L2.4 1ND3-Nitroaniline 20 09/15/15 DD SW8270Dug/L11 1ND4-Bromophenyl phenyl ether 5.0 09/15/15 DD SW8270Dug/L1.5 1ND4-Chloroaniline 20 09/15/15 DD SW8270Dug/L2.3 1ND4-Chlorophenyl phenyl ether 5.0 09/15/15 DD SW8270Dug/L1.7 1ND4-Nitroaniline 20 09/15/15 DD SW8270Dug/L1.7 1NDBenzidine 18 09/15/15 DD SW8270Dug/L2.9 1NDBenzoic acid 20 09/15/15 DD SW8270Dug/L10 1NDBenzyl Alcohol 5.0 09/15/15 DD SW8270Dug/L5.0 1NDBenzyl butyl phthalate 5.0 09/15/15 DD SW8270Dug/L1.3 1NDBis(2-chloroethoxy)methane 5.0 09/15/15 DD SW8270Dug/L1.4 1NDBis(2-chloroethyl)ether 5.0 09/15/15 DD SW8270Dug/L1.4 1NDBis(2-chloroisopropyl)ether 5.0 09/15/15 DD SW8270Dug/L 1,1O1.4 1NDDibenzofuran 5.0 09/15/15 DD SW8270Dug/L1.5 1NDDiethyl phthalate 5.0 09/15/15 DD SW8270Dug/L1.6 1NDDimethylphthalate 5.0 09/15/15 DD SW8270Dug/L1.6 1NDDi-n-butylphthalate 5.0 09/15/15 DD SW8270Dug/L1.3 1NDDi-n-octylphthalate 5.0 09/15/15 DD SW8270Dug/L1.3 1NDHexachlorocyclopentadiene 5.0 09/15/15 DD SW8270Dug/L1.5 1NDIsophorone 5.0 09/15/15 DD SW8270Dug/L1.4 1NDN-Nitrosodi-n-propylamine 5.0 09/15/15 DD SW8270Dug/L1.6 1NDN-Nitrosodiphenylamine 5.0 09/15/15 DD SW8270Dug/L1.9 1


Semivolatiles (SIM)ND2-Methylnaphthalene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDAcenaphthene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDAcenaphthylene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 10.10Anthracene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDBenz(a)anthracene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDBenzo(a)pyrene 0.02 09/14/15 DD SW8270D (SIM)ug/L0.02 1NDBenzo(b)fluoranthene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDBenzo(ghi)perylene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDBenzo(k)fluoranthene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 10.11Bis(2-ethylhexyl)phthalate 0.05 09/14/15 DD SW8270D (SIM)ug/L B*0.05 1BNDChrysene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDDibenz(a,h)anthracene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDFluoranthene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDFluorene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDHexachlorobenzene 0.02 09/14/15 DD SW8270D (SIM)ug/L0.02 1

Page 17 of 21 Ver 2




LOD/MDL Dilution

NDHexachlorobutadiene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDHexachloroethane 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDIndeno(1,2,3-cd)pyrene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 10.27Naphthalene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDNitrobenzene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDN-Nitrosodimethylamine 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1NDPhenanthrene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 10.05Pyrene 0.05 09/14/15 DD SW8270D (SIM)ug/L0.05 1


Comments:








Page 18 of 21 Ver 2





TG

Laboratory Data

TRIP BLANK

Phoenix ID: BJ90195

09/10/1511:2017:04




Date Time



SDG ID: GBJ90192


LOD/MDL Dilution

VolatilesND1,1,1,2-Tetrachloroethane 1.0 09/11/15 MH SW8260Cug/L0.25 1ND1,1,1-Trichloroethane 5.0 09/11/15 MH SW8260Cug/L0.25 1ND1,1,2,2-Tetrachloroethane 1.0 09/11/15 MH SW8260Cug/L0.25 1ND1,1,2-Trichloroethane 1.0 09/11/15 MH SW8260Cug/L0.25 1ND1,1-Dichloroethane 5.0 09/11/15 MH SW8260Cug/L0.25 1ND1,1-Dichloroethene 1.0 09/11/15 MH SW8260Cug/L0.25 1ND1,1-Dichloropropene 1.0 09/11/15 MH SW8260Cug/L0.25 1ND1,2,3-Trichlorobenzene 1.0 09/11/15 MH SW8260Cug/L0.25 1ND1,2,3-Trichloropropane 1.0 09/11/15 MH SW8260Cug/L0.25 1ND1,2,4-Trichlorobenzene 1.0 09/11/15 MH SW8260Cug/L0.25 1ND1,2,4-Trimethylbenzene 1.0 09/11/15 MH SW8260Cug/L0.25 1ND1,2-Dibromo-3-chloropropane 1.0 09/11/15 MH SW8260Cug/L0.50 1ND1,2-Dibromoethane 1.0 09/11/15 MH SW8260Cug/L0.25 1ND1,2-Dichlorobenzene 1.0 09/11/15 MH SW8260Cug/L0.25 1ND1,2-Dichloroethane 0.60 09/11/15 MH SW8260Cug/L0.25 1ND1,2-Dichloropropane 1.0 09/11/15 MH SW8260Cug/L0.25 1ND1,3,5-Trimethylbenzene 1.0 09/11/15 MH SW8260Cug/L0.25 1ND1,3-Dichlorobenzene 1.0 09/11/15 MH SW8260Cug/L0.25 1ND1,3-Dichloropropane 1.0 09/11/15 MH SW8260Cug/L0.25 1ND1,4-Dichlorobenzene 1.0 09/11/15 MH SW8260Cug/L0.25 1ND2,2-Dichloropropane 1.0 09/11/15 MH SW8260Cug/L0.25 1ND2-Chlorotoluene 1.0 09/11/15 MH SW8260Cug/L0.25 1ND2-Hexanone 2.5 09/11/15 MH SW8260Cug/L2.5 1ND2-Isopropyltoluene 1.0 09/11/15 MH SW8260Cug/L 10.25 1ND4-Chlorotoluene 1.0 09/11/15 MH SW8260Cug/L0.25 1ND4-Methyl-2-pentanone 2.5 09/11/15 MH SW8260Cug/L2.5 1

Page 19 of 21 Ver 2

TRIP BLANKPhoenix I.D.: BJ90195



LOD/MDL Dilution

NDAcetone 5.0 09/11/15 MH SW8260Cug/L2.5 1NDAcrolein 5.0 09/11/15 MH SW8260Cug/L2.5 1NDAcrylonitrile 5.0 09/11/15 MH SW8260Cug/L2.5 1NDBenzene 0.70 09/11/15 MH SW8260Cug/L0.25 1NDBromobenzene 1.0 09/11/15 MH SW8260Cug/L0.25 1NDBromochloromethane 1.0 09/11/15 MH SW8260Cug/L0.25 1NDBromodichloromethane 1.0 09/11/15 MH SW8260Cug/L0.25 1NDBromoform 5.0 09/11/15 MH SW8260Cug/L0.25 1NDBromomethane 5.0 09/11/15 MH SW8260Cug/L0.25 1NDCarbon Disulfide 1.0 09/11/15 MH SW8260Cug/L0.25 1NDCarbon tetrachloride 1.0 09/11/15 MH SW8260Cug/L0.25 1NDChlorobenzene 5.0 09/11/15 MH SW8260Cug/L0.25 1NDChloroethane 5.0 09/11/15 MH SW8260Cug/L0.25 1NDChloroform 5.0 09/11/15 MH SW8260Cug/L0.25 1NDChloromethane 5.0 09/11/15 MH SW8260Cug/L0.25 1NDcis-1,2-Dichloroethene 1.0 09/11/15 MH SW8260Cug/L0.25 1NDcis-1,3-Dichloropropene 0.40 09/11/15 MH SW8260Cug/L0.25 1NDDibromochloromethane 1.0 09/11/15 MH SW8260Cug/L0.25 1NDDibromomethane 1.0 09/11/15 MH SW8260Cug/L0.25 1NDDichlorodifluoromethane 1.0 09/11/15 MH SW8260Cug/L0.25 1NDEthylbenzene 1.0 09/11/15 MH SW8260Cug/L0.25 1NDHexachlorobutadiene 1.0 09/11/15 MH SW8260Cug/L0.10 1NDIsopropylbenzene 1.0 09/11/15 MH SW8260Cug/L0.25 1NDm&p-Xylene 1.0 09/11/15 MH SW8260Cug/L0.25 1NDMethyl ethyl ketone 2.5 09/11/15 MH SW8260Cug/L2.5 1NDMethyl t-butyl ether (MTBE) 1.0 09/11/15 MH SW8260Cug/L0.25 1NDMethylene chloride 3.0 09/11/15 MH SW8260Cug/L1.0 1NDNaphthalene 1.0 09/11/15 MH SW8260Cug/L1.0 1NDn-Butylbenzene 1.0 09/11/15 MH SW8260Cug/L0.25 1NDn-Propylbenzene 1.0 09/11/15 MH SW8260Cug/L0.25 1NDo-Xylene 1.0 09/11/15 MH SW8260Cug/L0.25 1NDp-Isopropyltoluene 1.0 09/11/15 MH SW8260Cug/L0.25 1NDsec-Butylbenzene 1.0 09/11/15 MH SW8260Cug/L0.25 1NDStyrene 1.0 09/11/15 MH SW8260Cug/L0.25 1NDtert-Butylbenzene 1.0 09/11/15 MH SW8260Cug/L0.25 1NDTetrachloroethene 1.0 09/11/15 MH SW8260Cug/L0.25 1NDTetrahydrofuran (THF) 5.0 09/11/15 MH SW8260Cug/L 12.5 1NDToluene 1.0 09/11/15 MH SW8260Cug/L0.25 1NDtrans-1,2-Dichloroethene 5.0 09/11/15 MH SW8260Cug/L0.25 1NDtrans-1,3-Dichloropropene 0.40 09/11/15 MH SW8260Cug/L0.25 1NDtrans-1,4-dichloro-2-butene 2.5 09/11/15 MH SW8260Cug/L2.5 1NDTrichloroethene 1.0 09/11/15 MH SW8260Cug/L0.25 1NDTrichlorofluoromethane 1.0 09/11/15 MH SW8260Cug/L0.25 1NDTrichlorotrifluoroethane 1.0 09/11/15 MH SW8260Cug/L0.25 1NDVinyl chloride 1.0 09/11/15 MH SW8260Cug/L0.25 1

QA/QC Surrogates101% 1,2-dichlorobenzene-d4 09/11/15 MH 70 - 130 %% 198% Bromofluorobenzene 09/11/15 MH 70 - 130 %% 199% Dibromofluoromethane 09/11/15 MH 70 - 130 %% 1

Page 20 of 21 Ver 2

TRIP BLANKPhoenix I.D.: BJ90195



LOD/MDL Dilution

98% Toluene-d8 09/11/15 MH 70 - 130 %% 1

Comments:

TRIP BLANK INCLUDED






Page 21 of 21 Ver 2

QA/QC Data


MS%

MSD%

MSRPD




SDG I.D.: GBJ90192

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPD

LimitsSampleResult

DupResult

QA/QC Batch 320153 (mg/L), QC Sample No: BJ89633 (BJ90192, BJ90193, BJ90194)Mercury (Dissolved) 102 96.3BRL 5.7101NC 91.8 9.5 75 - 125 20<0.0002 <0.00030.0003

QA/QC Batch 319957 (mg/L), QC Sample No: BJ89651 (BJ90192, BJ90193, BJ90194)Mercury - Water 84.7 78.9BRL 7.187.9NC 86.2 2.0 75 - 125 20<0.0002 <0.00020.0002

QA/QC Batch 319918 (mg/L), QC Sample No: BJ90192 (BJ90192, BJ90193, BJ90194)Antimony - Water 103 106BRL 2.9112NC 113 0.9 75 - 125 20<0.002 <0.0030.003

Selenium - Water 104 105BRL 1.0107NC 110 2.8 75 - 125 20<0.002 <0.0050.005

Thallium - Water 79.2 79.6BRL 0.591.9NC 93.0 1.2 75 - 125 20<0.001 <0.0010.001

QA/QC Batch 320098 (mg/L), QC Sample No: BJ90193 (BJ90192, BJ90193, BJ90194)

ICP Metals - DissolvedAluminum 86.7 88.3BRL 1.888.7NC 84.6 4.7 80 - 120 200.007 0.0060.011

Arsenic 89.8 90.8BRL 1.191.9NC 88.2 4.1 80 - 120 20<0.003 <0.0040.004

Barium 90.8 91.6BRL 0.994.68.10 90.4 4.5 80 - 120 200.064 0.0590.002

Beryllium 92.1 93.3BRL 1.396.0NC 91.8 4.5 80 - 120 20<0.001 <0.0010.001

Cadmium 87.3 89.0BRL 1.992.9NC 88.4 5.0 80 - 120 20<0.004 <0.0010.001

Calcium NC NCBRL NC94.96.80 90.2 5.1 80 - 120 2056.0 52.30.01

Chromium 90.7 91.7BRL 1.194.2NC 90.2 4.3 80 - 120 20<0.001 <0.0010.001

Cobalt 89.0 90.6BRL 1.893.5NC 89.0 4.9 80 - 120 20<0.005 <0.0010.001

Copper 93.0 95.3BRL 2.494.8NC 90.1 5.1 80 - 120 20<0.005 <0.0050.005

Iron 87.5 88.6BRL 1.293.9NC 89.0 5.4 80 - 120 200.05 0.0470.011

Lead 90.0 90.9BRL 1.093.2NC 89.4 4.2 80 - 120 200.002 0.0010.002

Magnesium NC NCBRL NC92.27.10 88.1 4.5 80 - 120 2019.0 17.70.01

Manganese 90.6 91.8BRL 1.394.96.70 90.4 4.9 80 - 120 200.230 0.2150.001

Nickel 88.8 90.6BRL 2.093.8NC 89.0 5.3 80 - 120 20<0.004 <0.0010.001

Potassium 109 111BRL 1.897.92.60 95.3 2.7 80 - 120 2011.5 11.20.1

Silver 92.4 93.2BRL 0.993.1NC 89.0 4.5 70 - 130 30<0.005 <0.0010.001

Sodium NC NCBRL NC97.23.60 94.9 2.4 80 - 120 2076.5 79.30.11

Vanadium 91.2 92.0BRL 0.994.1NC 89.9 4.6 80 - 120 20<0.011 <0.0020.002

Zinc 89.0 90.6BRL 1.892.7NC 87.7 5.5 80 - 120 20<0.011 <0.0020.002

QA/QC Batch 319926 (mg/L), QC Sample No: BJ90194 (BJ90192, BJ90193, BJ90194)

ICP Metals - AqueousAluminum 93.7 94.4BRL 0.796.12.50 87.3 9.6 80 - 120 200.404 0.3940.010

Arsenic 101 101BRL 0.098.9NC 97.4 1.5 80 - 120 20<0.004 <0.0040.004

Barium 101 101BRL 0.0101NC 94.4 6.8 80 - 120 200.019 0.0190.002

Beryllium 104 104BRL 0.0102NC 95.2 6.9 80 - 120 20<0.001 <0.0010.001

Cadmium 105 104BRL 1.0100NC 99.8 0.2 80 - 120 20<0.004 <0.0010.001

Calcium 111 109BRL 1.898.60.80 92.0 6.9 80 - 120 2025.9 26.10.010

Chromium 101 101BRL 0.099.1NC 97.8 1.3 80 - 120 20<0.001 <0.0010.001

Cobalt 105 105BRL 0.0102NC 101 1.0 80 - 120 20<0.005 <0.0020.002

Copper 100 100BRL 0.0101NC 90.3 11.2 80 - 120 200.001 <0.0050.005

Iron 104 104BRL 0.01020.30 100 2.0 80 - 120 200.37 0.3710.010

Lead 102 102BRL 0.099.3NC 97.8 1.5 80 - 120 200.001 0.0020.002

Page 1 of 8

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ90192

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPD

LimitsSampleResult

DupResult

Magnesium 102 101BRL 1.099.50.20 98.0 1.5 80 - 120 205.63 5.640.01

Manganese 103 103BRL 0.01010.70 99.6 1.4 80 - 120 200.143 0.1440.001

Nickel 103 103BRL 0.0101NC 99.1 1.9 80 - 120 20<0.004 <0.0010.001

Potassium 103 103BRL 0.01090 94.4 14.4 80 - 120 206.3 6.30.1

Silver 99.5 99.0BRL 0.598.7NC 85.8 14.0 70 - 130 30<0.005 <0.0010.001

Sodium NC NCBRL NC1105.60 95.1 14.5 80 - 120 2058.7 55.50.1

Vanadium 101 100BRL 1.098.4NC 89.9 9.0 80 - 120 200.005 0.0060.002

Zinc 100 99.9BRL 0.197.3NC 96.0 1.3 80 - 120 20<0.010 <0.0020.002

QA/QC Batch 320099 (mg/L), QC Sample No: BJ90194 (BJ90192, BJ90193, BJ90194)Antimony (Dissolved)-LDL 113 112BRL 0.9117NC 114 2.6 75 - 125 20<0.003 <0.0050.005

Selenium (Dissolved) 108 115BRL 6.3121NC 117 3.4 75 - 125 20<0.004 <0.0020.002

Thallium (Dissolved) 94.5 95.6BRL 1.299.9NC 101 1.1 75 - 125 20<0.001 <0.0020.002

Page 2 of 8

QA/QC Data


MS%

MSD%

MSRPD




SDG I.D.: GBJ90192

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits


Pesticides - Ground Water4,4' -DDD ND 82 81 1.2 30 - 150 200.003

4,4' -DDE ND 76 75 1.3 50 - 150 200.003

4,4' -DDT ND 90 89 1.1 30 - 150 270.003

a-BHC ND 90 89 1.1 30 - 150 200.005

a-Chlordane ND 88 88 0.0 30 - 150 200.005

Alachlor ND NA NA NC 30 - 150 200.005

Aldrin ND 78 78 0.0 30 - 150 220.002

b-BHC ND 90 90 0.0 30 - 150 200.005

Chlordane ND 84 83 1.2 30 - 150 200.050

d-BHC ND 90 89 1.1 30 - 150 200.005

Dieldrin ND 88 87 1.1 30 - 130 180.002

Endosulfan I ND 97 96 1.0 30 - 150 200.005

Endosulfan II ND 93 91 2.2 30 - 150 200.005

Endosulfan sulfate ND 86 84 2.4 50 - 120 200.005

Endrin ND 83 82 1.2 50 - 120 210.005

Endrin aldehyde ND 93 92 1.1 30 - 150 200.005

Endrin ketone ND 85 85 0.0 30 - 150 200.005

g-BHC ND 91 91 0.0 50 - 120 150.002

g-Chlordane ND 84 83 1.2 30 - 130 200.005

Heptachlor ND 88 88 0.0 30 - 150 200.005

Heptachlor epoxide ND 84 86 2.4 50 - 150 200.005

Methoxychlor ND 80 81 1.2 30 - 150 200.005

Toxaphene ND NA NA NC 30 - 150 200.20

% DCBP 89 67 54 21.5 r30 - 150 20%

% TCMX 87 98 102 4.0 30 - 150 20%

A LCS and LCS duplicate were performed instead of a MS and MSD. Alpha and gamma chlordane were spiked and analyzed instead of technical chlordane. Gamma chlordane recovery is reported as chlordane in the LCS and LCSD

Comment:


Polychlorinated Biphenyls - Ground WaterPCB-1016 ND 69 62 10.7 30 - 120 200.050

PCB-1221 ND 30 - 150 200.050

PCB-1232 ND 30 - 150 200.050

PCB-1242 ND 30 - 150 200.050

PCB-1248 ND 30 - 150 200.050

PCB-1254 ND 30 - 150 200.050

PCB-1260 ND 89 76 15.8 30 - 150 200.050

PCB-1262 ND 30 - 150 200.050

PCB-1268 ND 30 - 150 200.050

% DCBP (Surrogate Rec) 71 93 85 9.0 30 - 150 20%

% TCMX (Surrogate Rec) 70 100 85 16.2 30 - 150 20%

Page 3 of 8

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ90192

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

A LCS and LCS Duplicate were performed instead of a matrix spike and matrix spike duplicate.

Comment:


Semivolatiles (SIM) - Ground Water2-Methylnaphthalene ND 96 87 9.8 30 - 130 200.02

Acenaphthene ND 97 82 16.8 30 - 130 200.02

Acenaphthylene ND 113 101 11.2 30 - 130 200.02

Anthracene ND 102 92 10.3 30 - 130 200.02

Benz(a)anthracene ND 98 92 6.3 30 - 130 200.02

Benzo(a)pyrene ND 98 85 14.2 30 - 130 200.02

Benzo(b)fluoranthene ND 82 71 14.4 30 - 130 200.02

Benzo(ghi)perylene ND 106 92 14.1 30 - 130 200.02

Benzo(k)fluoranthene ND 80 79 1.3 30 - 130 200.02

Bis(2-ethylhexyl)phthalate 0.17 B 126 140 10.5 l30 - 130 200.05

Chrysene ND 96 90 6.5 30 - 130 200.02

Dibenz(a,h)anthracene ND 107 92 15.1 30 - 130 200.01

Fluoranthene ND 103 94 9.1 30 - 130 200.02

Fluorene ND 104 89 15.5 30 - 130 200.02

Hexachlorobenzene ND 95 93 2.1 30 - 130 200.02

Hexachlorobutadiene ND 66 56 16.4 30 - 130 200.05

Hexachloroethane ND 57 50 13.1 30 - 130 200.05

Indeno(1,2,3-cd)pyrene ND 109 94 14.8 30 - 130 200.02

Naphthalene ND 74 64 14.5 30 - 130 200.02

Nitrobenzene ND 73 64 13.1 30 - 130 200.05

N-Nitrosodimethylamine ND 55 55 0.0 30 - 130 200.05

Phenanthrene ND 96 89 7.6 30 - 130 200.02

Pyrene ND 99 91 8.4 30 - 130 200.02

% 2-Fluorobiphenyl 63 88 79 10.8 30 - 130 20%

% Nitrobenzene-d5 57 76 67 12.6 30 - 130 20%

% Terphenyl-d14 66 89 81 9.4 30 - 130 20%


Semivolatiles - Ground Water1,2,4-Trichlorobenzene ND 77 67 13.9 30 - 130 203.5

1,2-Dichlorobenzene ND 65 57 13.1 30 - 130 201.0

1,2-Diphenylhydrazine ND 98 97 1.0 30 - 130 201.6



2,4-Dinitrotoluene ND 105 98 6.9 30 - 130 203.5

2,6-Dinitrotoluene ND 103 99 4.0 30 - 130 203.5

2-Chloronaphthalene ND 95 85 11.1 30 - 130 203.5

2-Nitroaniline ND 111 108 2.7 30 - 130 203.5

3,3'-Dichlorobenzidine ND 69 69 0.0 30 - 130 205.0

3-Nitroaniline ND 98 90 8.5 30 - 130 205.0

4-Bromophenyl phenyl ether ND 103 94 9.1 30 - 130 203.5

4-Chloroaniline ND 81 79 2.5 30 - 130 203.5

4-Chlorophenyl phenyl ether ND 104 95 9.0 30 - 130 201.0

4-Nitroaniline ND 99 103 4.0 30 - 130 205.0

Benzidine ND 54 60 10.5 30 - 130 204.5

Benzoic acid ND 112 112 0.0 30 - 130 2010

Benzyl Alcohol ND 92 75 20.4 30 - 130 205.0

Benzyl butyl phthalate ND 98 97 1.0 30 - 130 201.5

Page 4 of 8

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ90192

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

Bis(2-chloroethoxy)methane ND 87 78 10.9 30 - 130 203.5

Bis(2-chloroethyl)ether ND 67 56 17.9 30 - 130 201.0

Bis(2-chloroisopropyl)ether ND 70 62 12.1 30 - 130 201.0

Dibenzofuran ND 101 96 5.1 30 - 130 203.5

Diethyl phthalate ND 101 100 1.0 30 - 130 201.5

Dimethylphthalate ND 102 95 7.1 30 - 130 201.5

Di-n-butylphthalate ND 107 103 3.8 30 - 130 201.5

Di-n-octylphthalate ND 104 105 1.0 30 - 130 201.5

Hexachlorocyclopentadiene ND 42 34 21.1 r30 - 130 203.5

Isophorone ND 85 80 6.1 30 - 130 203.5

N-Nitrosodi-n-propylamine ND 90 78 14.3 30 - 130 203.5

N-Nitrosodiphenylamine ND 93 85 9.0 30 - 130 203.5

% 2-Fluorobiphenyl 72 90 79 13.0 30 - 130 20%

% Nitrobenzene-d5 53 73 65 11.6 30 - 130 20%

% Terphenyl-d14 104 114 107 6.3 30 - 130 20%


Volatiles - Ground Water1,1,1,2-Tetrachloroethane ND 91 94 3.2 70 - 130 301.0

1,1,1-Trichloroethane ND 91 95 4.3 70 - 130 301.0

1,1,2,2-Tetrachloroethane ND 96 102 6.1 70 - 130 300.50


1,1-Dichloroethane ND 90 95 5.4 70 - 130 301.0

1,1-Dichloroethene ND 89 92 3.3 70 - 130 301.0

1,1-Dichloropropene ND 88 92 4.4 70 - 130 301.0

1,2,3-Trichlorobenzene ND 100 108 7.7 70 - 130 301.0

1,2,3-Trichloropropane ND 98 102 4.0 70 - 130 301.0


1,2,4-Trimethylbenzene ND 93 96 3.2 70 - 130 301.0

1,2-Dibromo-3-chloropropane ND 89 94 5.5 70 - 130 301.0

1,2-Dibromoethane ND 94 100 6.2 70 - 130 301.0



1,2-Dichloropropane ND 91 96 5.3 70 - 130 301.0






2-Chlorotoluene ND 100 104 3.9 70 - 130 301.0

2-Hexanone ND 90 93 3.3 70 - 130 305.0

2-Isopropyltoluene ND 93 95 2.1 70 - 130 301.0


4-Methyl-2-pentanone ND 88 95 7.7 70 - 130 305.0

Acetone ND 79 86 8.5 70 - 130 305.0

Acrolein ND 81 91 11.6 70 - 130 305.0

Acrylonitrile ND 86 90 4.5 70 - 130 305.0

Benzene ND 93 98 5.2 70 - 130 300.70

Bromobenzene ND 96 100 4.1 70 - 130 301.0

Bromochloromethane ND 90 95 5.4 70 - 130 301.0

Bromodichloromethane ND 93 99 6.3 70 - 130 300.50

Bromoform ND 83 88 5.8 70 - 130 301.0

Bromomethane ND 78 84 7.4 70 - 130 301.0

Page 5 of 8

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ90192

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

Carbon Disulfide ND 92 95 3.2 70 - 130 301.0

Carbon tetrachloride ND 81 85 4.8 70 - 130 301.0

Chlorobenzene ND 90 93 3.3 70 - 130 301.0

Chloroethane ND 87 90 3.4 70 - 130 301.0

Chloroform ND 94 101 7.2 70 - 130 301.0

Chloromethane ND 82 86 4.8 70 - 130 301.0

cis-1,2-Dichloroethene ND 92 101 9.3 70 - 130 301.0

cis-1,3-Dichloropropene ND 92 95 3.2 70 - 130 300.40

Dibromochloromethane ND 89 92 3.3 70 - 130 300.50

Dibromomethane ND 90 97 7.5 70 - 130 301.0

Dichlorodifluoromethane ND 81 86 6.0 70 - 130 301.0

Ethylbenzene ND 93 94 1.1 70 - 130 301.0


Isopropylbenzene ND 91 93 2.2 70 - 130 301.0

m&p-Xylene ND 91 94 3.2 70 - 130 301.0

Methyl ethyl ketone ND 93 106 13.1 70 - 130 305.0

Methyl t-butyl ether (MTBE) ND 98 105 6.9 70 - 130 301.0

Methylene chloride ND 88 94 6.6 70 - 130 301.0

Naphthalene ND 99 106 6.8 70 - 130 301.0

n-Butylbenzene ND 95 95 0.0 70 - 130 301.0

n-Propylbenzene ND 90 92 2.2 70 - 130 301.0

o-Xylene ND 90 94 4.3 70 - 130 301.0

p-Isopropyltoluene ND 93 93 0.0 70 - 130 301.0

sec-Butylbenzene ND 93 95 2.1 70 - 130 301.0

Styrene ND 92 95 3.2 70 - 130 301.0

tert-Butylbenzene ND 91 92 1.1 70 - 130 301.0

Tetrachloroethene ND 88 91 3.4 70 - 130 301.0

Tetrahydrofuran (THF) ND 82 89 8.2 70 - 130 302.5

Toluene ND 90 94 4.3 70 - 130 301.0

trans-1,2-Dichloroethene ND 98 103 5.0 70 - 130 301.0

trans-1,3-Dichloropropene ND 94 99 5.2 70 - 130 300.40

trans-1,4-dichloro-2-butene ND 77 83 7.5 70 - 130 305.0

Trichloroethene ND 88 93 5.5 70 - 130 301.0

Trichlorofluoromethane ND 72 75 4.1 70 - 130 301.0

Trichlorotrifluoroethane ND 71 74 4.1 70 - 130 301.0

Vinyl chloride ND 85 89 4.6 70 - 130 301.0

% 1,2-dichlorobenzene-d4 101 98 99 1.0 70 - 130 30%

% Bromofluorobenzene 98 100 100 0.0 70 - 130 30%

% Dibromofluoromethane 97 98 98 0.0 70 - 130 30%

% Toluene-d8 98 97 97 0.0 70 - 130 30%


Comment:

QA/QC Batch 320319 (ug/L), QC Sample No: BJ91084 (BJ90192, BJ90193 (100X) , BJ90194 (5X) )

Volatiles - Ground Water1,1,1,2-Tetrachloroethane ND 101 123 19.6 70 - 130 301.0


1,1,2,2-Tetrachloroethane ND 103 120 15.2 70 - 130 300.50



1,1-Dichloroethene ND 95 115 19.0 70 - 130 301.0

1,1-Dichloropropene ND 98 121 21.0 70 - 130 301.0


Page 6 of 8

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ90192

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

1,2,3-Trichloropropane ND 103 122 16.9 70 - 130 301.0



1,2-Dibromo-3-chloropropane ND 106 116 9.0 70 - 130 301.0

1,2-Dibromoethane ND 102 119 15.4 70 - 130 301.0










2-Hexanone ND 90 107 17.3 70 - 130 305.0

2-Isopropyltoluene ND 94 120 24.3 70 - 130 301.0


4-Methyl-2-pentanone ND 95 108 12.8 70 - 130 305.0

Acetone ND 107 111 3.7 70 - 130 305.0

Acrolein ND 107 118 9.8 70 - 130 305.0

Acrylonitrile ND 115 125 8.3 70 - 130 305.0

Benzene ND 97 120 21.2 70 - 130 300.70

Bromobenzene ND 97 117 18.7 70 - 130 301.0

Bromochloromethane ND 106 118 10.7 70 - 130 301.0

Bromodichloromethane ND 102 123 18.7 70 - 130 300.50

Bromoform ND 106 123 14.8 70 - 130 301.0

Bromomethane ND 116 160 31.9 l,r70 - 130 301.0

Carbon Disulfide ND 99 119 18.3 70 - 130 301.0

Carbon tetrachloride ND 100 121 19.0 70 - 130 301.0

Chlorobenzene ND 97 118 19.5 70 - 130 301.0

Chloroethane ND 96 116 18.9 70 - 130 301.0

Chloroform ND 98 116 16.8 70 - 130 301.0

Chloromethane ND 98 118 18.5 70 - 130 301.0

cis-1,2-Dichloroethene ND 96 113 16.3 70 - 130 301.0

cis-1,3-Dichloropropene ND 99 116 15.8 70 - 130 300.40

Dibromochloromethane ND 109 125 13.7 70 - 130 300.50

Dibromomethane ND 104 115 10.0 70 - 130 301.0

Dichlorodifluoromethane ND 99 119 18.3 70 - 130 301.0

Ethylbenzene ND 96 121 23.0 70 - 130 301.0


Isopropylbenzene ND 93 118 23.7 70 - 130 301.0

m&p-Xylene ND 95 120 23.3 70 - 130 301.0

Methyl ethyl ketone ND 105 116 10.0 70 - 130 305.0

Methyl t-butyl ether (MTBE) ND 107 120 11.5 70 - 130 301.0

Methylene chloride ND 91 105 14.3 70 - 130 301.0

Naphthalene ND 103 118 13.6 70 - 130 301.0

n-Butylbenzene ND 93 119 24.5 70 - 130 301.0

n-Propylbenzene ND 92 117 23.9 70 - 130 301.0

o-Xylene ND 95 118 21.6 70 - 130 301.0

p-Isopropyltoluene ND 96 120 22.2 70 - 130 301.0

sec-Butylbenzene ND 95 121 24.1 70 - 130 301.0

Styrene ND 98 120 20.2 70 - 130 301.0

tert-Butylbenzene ND 93 118 23.7 70 - 130 301.0

Page 7 of 8

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ90192

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

Tetrachloroethene ND 92 113 20.5 70 - 130 301.0

Tetrahydrofuran (THF) ND 109 120 9.6 70 - 130 302.5

Toluene ND 95 117 20.8 70 - 130 301.0

trans-1,2-Dichloroethene ND 100 119 17.4 70 - 130 301.0

trans-1,3-Dichloropropene ND 101 118 15.5 70 - 130 300.40

trans-1,4-dichloro-2-butene ND 104 121 15.1 70 - 130 305.0

Trichloroethene ND 94 117 21.8 70 - 130 301.0

Trichlorofluoromethane ND 95 113 17.3 70 - 130 301.0

Trichlorotrifluoroethane ND 100 117 15.7 70 - 130 301.0


% 1,2-dichlorobenzene-d4 100 100 100 0.0 70 - 130 30%

% Bromofluorobenzene 96 101 100 1.0 70 - 130 30%

% Dibromofluoromethane 96 103 98 5.0 70 - 130 30%

% Toluene-d8 101 100 100 0.0 70 - 130 30%


Comment:

QA/QC Batch 320436 (ug/L), QC Sample No: BJ91360 (BJ90192 (5X) )

Volatiles - Ground Watercis-1,2-Dichloroethene ND 100 97 3.0 70 - 130 301.0



Comment:

l = This parameter is outside laboratory lcs/lcsd specified recovery limits.r = This parameter is outside laboratory rpd specified recovery limits.




RPD - Relative Percent DifferenceLCS - Laboratory Control Sample

LCSD - Laboratory Control Sample Duplicate

NC - No Criteria

Intf - Interference

Page 8 of 8

Sample Criteria Exceedences ReportFriday, October 23, 2015 Page 1 of 1


UnitsCriteria

GBJ90192 - EBCCriteria: NY: 375GWP

RLCriteria

State: NY

#Error*** No Data to Display ***


NY Temperature NarrationOctober 23, 2015



SDG I.D.: GBJ90192

The samples in this delivery group were received at 4°C.(Note acceptance criteria is above freezing up to 6°C)

Page 1 of 1

BJ81780 - BJ81802, BJ81976 - BJ81977

Monday, October 05, 2015

Sample ID#s:


Project ID: 510 DRIGGS

Sincerely yours,







All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.






SDG I.D.: GBJ81780

Please be advised that the NY 375 soil criteria for chromium are based on hexavalent chromium and trivalent chromium.

BJ81790 - Client provided soil jar for volatile analysis. Phoenix prepared sample per method 5035.






Client: Environmental Business ConsultantsProject: 510 DRIGGS





SDG I.D.: GBJ81780

Environmental Business Consultants 510 DRIGGS



Accelerated Solvent Extraction (ASE)Soil Sample - USEPA SW-846 Test Methods for Evaluating Solid Waste Physical/Chemical Methods 3rd Ed.Update III, Method 3545A.

Mercury PrepSoil Sample - USEPA SW-846 Test Methods for Evaluating Solid Waste Physical/Chemical Methods 3rd Ed. Update IV, Method 7471B.



Polychlorinated Biphenyls (PCBs):USEPA SW-846 Test Methods for Evaluating Solid Waste Physical/Chemical Methods 3rd Ed. Update IV, Method 8082A.





SDG I.D.: GBJ81780


Sample Id Cross ReferenceClient Id Lab Id Matrix14B8 (0-5) BJ81780 SOLID14B8 (10-15) BJ81781 SOLID14B8 (20-25) BJ81782 SOLID14B7 (0-5) BJ81783 SOLID14B7 (10-15) BJ81784 SOLID14B7 (15-20) BJ81785 SOLID14B2 (0-5) BJ81786 SOLID14B2 (10-15) BJ81787 SOLID14B2 (20-25) BJ81788 SOLID14B1 (0-5) BJ81789 SOLID14B1 (10-15) BJ81790 SOLID14B3 (0-5) BJ81791 SOLID14B3 (10-15) BJ81792 SOLID14B3 (15-18) BJ81793 SOLID14B6 (0-5) BJ81794 SOLID14B6 (10-15) BJ81795 SOLID14B6 (15-17) BJ81796 SOLID14B4 (0-5) BJ81797 SOLID14B4 (10-15) BJ81798 SOLID14B4 (20-21) BJ81799 SOLID14B5 (0-5) BJ81800 SOLID14B5 (10-15) BJ81801 SOLID14B5 (15-19.5) BJ81802 SOLIDTRIP BLANK LL BJ81976 SOILTRIP BLANK HL BJ81977 SOIL




SDG I.D.: GBJ81780


Laboratory ChronicleThe samples in this delivery group were received at 2°C.


DateExtraction

DateAnalysis


MetBJ81780 1,4-dioxane 08/25/15 08/29/15 08/29/15 JLI YBJ81780 Aluminum 08/25/15 08/26/15 08/28/15 LK YBJ81780 Antimony 08/25/15 08/26/15 08/28/15 LK YBJ81780 Arsenic 08/25/15 08/26/15 08/28/15 LK YBJ81780 Barium 08/25/15 08/26/15 08/28/15 LK YBJ81780 Beryllium 08/25/15 08/26/15 08/28/15 LK YBJ81780 Cadmium 08/25/15 08/26/15 08/28/15 LK YBJ81780 Calcium 08/25/15 08/26/15 08/28/15 LK YBJ81780 Chromium 08/25/15 08/26/15 08/28/15 LK YBJ81780 Cobalt 08/25/15 08/26/15 08/28/15 LK YBJ81780 Copper 08/25/15 08/26/15 08/28/15 LK YBJ81780 Iron 08/25/15 08/26/15 08/28/15 LK YBJ81780 Lead 08/25/15 08/26/15 08/28/15 LK YBJ81780 Magnesium 08/25/15 08/26/15 08/28/15 LK YBJ81780 Manganese 08/25/15 08/26/15 08/28/15 LK YBJ81780 Mercury 08/25/15 08/27/15 08/27/15 RS YBJ81780 Nickel 08/25/15 08/26/15 08/28/15 LK YBJ81780 Pesticides - Soil 08/25/15 08/26/15 08/28/15 CE YBJ81780 Polychlorinated Biphenyls 08/25/15 08/26/15 08/29/15 AW YBJ81780 Potassium 08/25/15 08/26/15 08/28/15 LK YBJ81780 Selenium 08/25/15 08/26/15 08/28/15 LK YBJ81780 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81780 Silver 08/25/15 08/26/15 08/28/15 LK YBJ81780 Sodium 08/25/15 08/26/15 08/28/15 LK YBJ81780 Thallium 08/25/15 08/26/15 08/28/15 LK YBJ81780 Vanadium 08/25/15 08/26/15 08/28/15 LK YBJ81780 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81780 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81780 Zinc 08/25/15 08/26/15 08/28/15 LK YBJ81781 1,4-dioxane 08/25/15 08/29/15 08/29/15 JLI YBJ81781 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81781 Volatiles 08/25/15 08/29/15 08/29/15 JLI Y




SDG I.D.: GBJ81780


BJ81781 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81782 1,4-dioxane 08/25/15 08/29/15 08/29/15 JLI YBJ81782 Aluminum 08/25/15 08/26/15 08/28/15 LK YBJ81782 Antimony 08/25/15 08/26/15 08/28/15 LK YBJ81782 Arsenic 08/25/15 08/26/15 08/28/15 LK YBJ81782 Barium 08/25/15 08/26/15 08/28/15 LK YBJ81782 Beryllium 08/25/15 08/26/15 08/28/15 LK YBJ81782 Cadmium 08/25/15 08/26/15 08/28/15 LK YBJ81782 Calcium 08/25/15 08/26/15 08/28/15 LK YBJ81782 Chromium 08/25/15 08/26/15 08/28/15 LK YBJ81782 Cobalt 08/25/15 08/26/15 08/28/15 LK YBJ81782 Copper 08/25/15 08/26/15 08/28/15 LK YBJ81782 Iron 08/25/15 08/26/15 08/28/15 LK YBJ81782 Lead 08/25/15 08/26/15 08/28/15 LK YBJ81782 Magnesium 08/25/15 08/26/15 08/28/15 LK YBJ81782 Manganese 08/25/15 08/26/15 08/28/15 LK YBJ81782 Mercury 08/25/15 08/27/15 08/27/15 RS YBJ81782 Nickel 08/25/15 08/26/15 08/28/15 LK YBJ81782 Pesticides - Soil 08/25/15 08/26/15 08/28/15 F YBJ81782 Polychlorinated Biphenyls 08/25/15 08/26/15 08/29/15 AW YBJ81782 Potassium 08/25/15 08/26/15 08/28/15 LK YBJ81782 Selenium 08/25/15 08/26/15 08/28/15 LK YBJ81782 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81782 Silver 08/25/15 08/26/15 08/28/15 LK YBJ81782 Sodium 08/25/15 08/26/15 08/28/15 LK YBJ81782 Thallium 08/25/15 08/26/15 08/28/15 LK YBJ81782 Vanadium 08/25/15 08/26/15 08/28/15 LK YBJ81782 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81782 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81782 Zinc 08/25/15 08/26/15 08/28/15 LK YBJ81783 1,4-dioxane 08/25/15 08/29/15 08/29/15 JLI YBJ81783 Aluminum 08/25/15 08/26/15 08/28/15 LK YBJ81783 Antimony 08/25/15 08/26/15 08/28/15 LK YBJ81783 Arsenic 08/25/15 08/26/15 08/28/15 LK YBJ81783 Barium 08/25/15 08/26/15 08/28/15 LK YBJ81783 Beryllium 08/25/15 08/26/15 08/28/15 LK YBJ81783 Cadmium 08/25/15 08/26/15 08/28/15 LK Y




SDG I.D.: GBJ81780


BJ81783 Calcium 08/25/15 08/26/15 08/28/15 LK YBJ81783 Chromium 08/25/15 08/26/15 08/28/15 LK YBJ81783 Cobalt 08/25/15 08/26/15 08/28/15 LK YBJ81783 Copper 08/25/15 08/26/15 08/28/15 LK YBJ81783 Iron 08/25/15 08/26/15 08/28/15 LK YBJ81783 Lead 08/25/15 08/26/15 08/28/15 LK YBJ81783 Magnesium 08/25/15 08/26/15 08/28/15 LK YBJ81783 Manganese 08/25/15 08/26/15 08/28/15 LK YBJ81783 Mercury 08/25/15 08/27/15 08/27/15 RS YBJ81783 Nickel 08/25/15 08/26/15 08/28/15 LK YBJ81783 Pesticides - Soil 08/25/15 08/26/15 08/28/15 CE YBJ81783 Polychlorinated Biphenyls 08/25/15 08/26/15 08/29/15 AW YBJ81783 Potassium 08/25/15 08/26/15 08/28/15 LK YBJ81783 Selenium 08/25/15 08/26/15 08/28/15 LK YBJ81783 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81783 Silver 08/25/15 08/26/15 08/28/15 LK YBJ81783 Sodium 08/25/15 08/26/15 08/28/15 LK YBJ81783 Thallium 08/25/15 08/26/15 08/28/15 LK YBJ81783 Vanadium 08/25/15 08/26/15 08/28/15 LK YBJ81783 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81783 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81783 Zinc 08/25/15 08/26/15 08/28/15 LK YBJ81784 1,4-dioxane 08/25/15 08/29/15 08/29/15 JLI YBJ81784 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81784 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81784 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81785 1,4-dioxane 08/25/15 08/29/15 08/29/15 JLI YBJ81785 Aluminum 08/25/15 08/26/15 08/28/15 LK YBJ81785 Antimony 08/25/15 08/26/15 08/28/15 LK YBJ81785 Arsenic 08/25/15 08/26/15 08/28/15 LK YBJ81785 Barium 08/25/15 08/26/15 08/28/15 LK YBJ81785 Beryllium 08/25/15 08/26/15 08/28/15 LK YBJ81785 Cadmium 08/25/15 08/26/15 08/28/15 LK YBJ81785 Calcium 08/25/15 08/26/15 08/28/15 LK YBJ81785 Chromium 08/25/15 08/26/15 08/28/15 LK YBJ81785 Cobalt 08/25/15 08/26/15 08/28/15 LK YBJ81785 Copper 08/25/15 08/26/15 08/28/15 LK Y




SDG I.D.: GBJ81780


BJ81785 Iron 08/25/15 08/26/15 08/28/15 LK YBJ81785 Lead 08/25/15 08/26/15 08/28/15 LK YBJ81785 Magnesium 08/25/15 08/26/15 08/28/15 LK YBJ81785 Manganese 08/25/15 08/26/15 08/28/15 LK YBJ81785 Mercury 08/25/15 08/27/15 08/27/15 RS YBJ81785 Nickel 08/25/15 08/26/15 08/28/15 LK YBJ81785 Pesticides - Soil 08/25/15 08/26/15 08/28/15 CE YBJ81785 Polychlorinated Biphenyls 08/25/15 08/26/15 08/29/15 AW YBJ81785 Potassium 08/25/15 08/26/15 08/28/15 LK YBJ81785 Selenium 08/25/15 08/26/15 08/28/15 LK YBJ81785 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81785 Silver 08/25/15 08/26/15 08/28/15 LK YBJ81785 Sodium 08/25/15 08/26/15 08/28/15 LK YBJ81785 Thallium 08/25/15 08/26/15 08/28/15 LK YBJ81785 Vanadium 08/25/15 08/26/15 08/28/15 LK YBJ81785 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81785 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81785 Zinc 08/25/15 08/26/15 08/28/15 LK YBJ81786 1,4-dioxane 08/25/15 08/29/15 08/29/15 JLI YBJ81786 Aluminum 08/25/15 08/26/15 08/28/15 LK YBJ81786 Antimony 08/25/15 08/26/15 08/28/15 LK YBJ81786 Arsenic 08/25/15 08/26/15 08/28/15 LK YBJ81786 Barium 08/25/15 08/26/15 08/28/15 LK YBJ81786 Beryllium 08/25/15 08/26/15 08/28/15 LK YBJ81786 Cadmium 08/25/15 08/26/15 08/28/15 LK YBJ81786 Calcium 08/25/15 08/26/15 08/28/15 LK YBJ81786 Chromium 08/25/15 08/26/15 08/28/15 LK YBJ81786 Cobalt 08/25/15 08/26/15 08/28/15 LK YBJ81786 Copper 08/25/15 08/26/15 08/28/15 LK YBJ81786 Iron 08/25/15 08/26/15 08/28/15 LK YBJ81786 Lead 08/25/15 08/26/15 08/28/15 LK YBJ81786 Magnesium 08/25/15 08/26/15 08/28/15 LK YBJ81786 Manganese 08/25/15 08/26/15 08/28/15 LK YBJ81786 Mercury 08/25/15 08/27/15 08/27/15 RS YBJ81786 Nickel 08/25/15 08/26/15 08/28/15 LK YBJ81786 Pesticides - Soil 08/25/15 08/26/15 08/28/15 CE YBJ81786 Polychlorinated Biphenyls 08/25/15 08/26/15 08/31/15 AW Y




SDG I.D.: GBJ81780


BJ81786 Potassium 08/25/15 08/26/15 08/28/15 LK YBJ81786 Selenium 08/25/15 08/26/15 08/28/15 LK YBJ81786 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81786 Silver 08/25/15 08/26/15 08/28/15 LK YBJ81786 Sodium 08/25/15 08/26/15 08/28/15 LK YBJ81786 Thallium 08/25/15 08/26/15 08/28/15 LK YBJ81786 Vanadium 08/25/15 08/26/15 08/28/15 LK YBJ81786 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81786 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81786 Zinc 08/25/15 08/26/15 08/28/15 LK YBJ81787 1,4-dioxane 08/25/15 08/29/15 08/29/15 JLI YBJ81787 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81787 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81787 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81788 1,4-dioxane 08/25/15 08/29/15 08/29/15 JLI YBJ81788 Aluminum 08/25/15 08/26/15 08/28/15 LK YBJ81788 Antimony 08/25/15 08/26/15 08/28/15 LK YBJ81788 Arsenic 08/25/15 08/26/15 08/28/15 LK YBJ81788 Barium 08/25/15 08/26/15 08/28/15 LK YBJ81788 Beryllium 08/25/15 08/26/15 08/28/15 LK YBJ81788 Cadmium 08/25/15 08/26/15 08/28/15 LK YBJ81788 Calcium 08/25/15 08/26/15 08/28/15 LK YBJ81788 Chromium 08/25/15 08/26/15 08/28/15 LK YBJ81788 Cobalt 08/25/15 08/26/15 08/28/15 LK YBJ81788 Copper 08/25/15 08/26/15 08/28/15 LK YBJ81788 Iron 08/25/15 08/26/15 08/28/15 LK YBJ81788 Lead 08/25/15 08/26/15 08/28/15 LK YBJ81788 Magnesium 08/25/15 08/26/15 08/28/15 LK YBJ81788 Manganese 08/25/15 08/26/15 08/28/15 LK YBJ81788 Mercury 08/25/15 08/27/15 08/27/15 RS YBJ81788 Nickel 08/25/15 08/26/15 08/28/15 LK YBJ81788 Pesticides - Soil 08/25/15 08/26/15 08/28/15 CE YBJ81788 Polychlorinated Biphenyls 08/25/15 08/26/15 08/29/15 AW YBJ81788 Potassium 08/25/15 08/26/15 08/28/15 LK YBJ81788 Selenium 08/25/15 08/26/15 08/28/15 LK YBJ81788 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81788 Silver 08/25/15 08/26/15 08/28/15 LK Y




SDG I.D.: GBJ81780


BJ81788 Sodium 08/25/15 08/26/15 08/28/15 LK YBJ81788 Thallium 08/25/15 08/26/15 08/28/15 LK YBJ81788 Vanadium 08/25/15 08/26/15 08/28/15 LK YBJ81788 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81788 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81788 Zinc 08/25/15 08/26/15 08/28/15 LK YBJ81789 1,4-dioxane 08/25/15 08/29/15 08/29/15 JLI YBJ81789 Aluminum 08/25/15 08/26/15 08/28/15 LK YBJ81789 Antimony 08/25/15 08/26/15 08/28/15 LK YBJ81789 Arsenic 08/25/15 08/26/15 08/28/15 LK YBJ81789 Barium 08/25/15 08/26/15 08/28/15 LK YBJ81789 Beryllium 08/25/15 08/26/15 08/28/15 LK YBJ81789 Cadmium 08/25/15 08/26/15 08/28/15 LK YBJ81789 Calcium 08/25/15 08/26/15 08/28/15 LK YBJ81789 Chromium 08/25/15 08/26/15 08/28/15 LK YBJ81789 Cobalt 08/25/15 08/26/15 08/28/15 LK YBJ81789 Copper 08/25/15 08/26/15 08/28/15 LK YBJ81789 Iron 08/25/15 08/26/15 08/28/15 LK YBJ81789 Lead 08/25/15 08/26/15 08/28/15 LK YBJ81789 Magnesium 08/25/15 08/26/15 08/28/15 LK YBJ81789 Manganese 08/25/15 08/26/15 08/28/15 LK YBJ81789 Mercury 08/25/15 08/27/15 08/27/15 RS YBJ81789 Nickel 08/25/15 08/26/15 08/28/15 LK YBJ81789 Pesticides - Soil 08/25/15 08/26/15 08/28/15 CE YBJ81789 Polychlorinated Biphenyls 08/25/15 08/26/15 08/29/15 AW YBJ81789 Potassium 08/25/15 08/26/15 08/28/15 LK YBJ81789 Selenium 08/25/15 08/26/15 08/28/15 LK YBJ81789 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81789 Silver 08/25/15 08/26/15 08/28/15 LK YBJ81789 Sodium 08/25/15 08/26/15 08/28/15 LK YBJ81789 Thallium 08/25/15 08/26/15 08/28/15 LK YBJ81789 Vanadium 08/25/15 08/26/15 08/28/15 LK YBJ81789 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81789 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81789 Zinc 08/25/15 08/26/15 08/28/15 LK YBJ81790 1,4-dioxane 08/25/15 08/29/15 08/29/15 JLI YBJ81790 Semivolatiles 08/25/15 08/26/15 08/27/15 DD Y




SDG I.D.: GBJ81780


BJ81790 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81790 Volatiles 08/25/15 08/29/15 08/29/15 JLI YBJ81791 1,4-dioxane 08/25/15 08/31/15 08/31/15 JLI YBJ81791 Aluminum 08/25/15 08/26/15 08/28/15 LK YBJ81791 Antimony 08/25/15 08/26/15 08/28/15 LK YBJ81791 Arsenic 08/25/15 08/26/15 08/28/15 LK YBJ81791 Barium 08/25/15 08/26/15 08/28/15 LK YBJ81791 Beryllium 08/25/15 08/26/15 08/28/15 LK YBJ81791 Cadmium 08/25/15 08/26/15 08/28/15 LK YBJ81791 Calcium 08/25/15 08/26/15 08/28/15 LK YBJ81791 Chromium 08/25/15 08/26/15 08/28/15 LK YBJ81791 Cobalt 08/25/15 08/26/15 08/28/15 LK YBJ81791 Copper 08/25/15 08/26/15 08/28/15 LK YBJ81791 Iron 08/25/15 08/26/15 08/28/15 LK YBJ81791 Lead 08/25/15 08/26/15 08/28/15 LK YBJ81791 Magnesium 08/25/15 08/26/15 08/28/15 LK YBJ81791 Manganese 08/25/15 08/26/15 08/28/15 LK YBJ81791 Mercury 08/25/15 08/27/15 08/27/15 RS YBJ81791 Nickel 08/25/15 08/26/15 08/28/15 LK YBJ81791 Pesticides - Soil 08/25/15 08/26/15 08/28/15 CE YBJ81791 Polychlorinated Biphenyls 08/25/15 08/26/15 08/31/15 AW YBJ81791 Potassium 08/25/15 08/26/15 08/28/15 LK YBJ81791 Selenium 08/25/15 08/26/15 08/28/15 LK YBJ81791 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81791 Silver 08/25/15 08/26/15 08/28/15 LK YBJ81791 Sodium 08/25/15 08/26/15 08/28/15 LK YBJ81791 Thallium 08/25/15 08/26/15 08/28/15 LK YBJ81791 Vanadium 08/25/15 08/26/15 08/28/15 LK YBJ81791 Volatiles 08/25/15 08/31/15 08/31/15 JLI YBJ81791 Volatiles 08/25/15 08/31/15 08/31/15 JLI YBJ81791 Zinc 08/25/15 08/26/15 08/28/15 LK YBJ81792 1,4-dioxane 08/25/15 08/30/15 08/30/15 JLI YBJ81792 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81792 Volatiles 08/25/15 08/30/15 08/30/15 JLI YBJ81792 Volatiles 08/25/15 08/31/15 08/31/15 JLI YBJ81793 1,4-dioxane 08/25/15 08/31/15 08/31/15 JLI YBJ81793 Aluminum 08/25/15 08/26/15 08/28/15 LK Y




SDG I.D.: GBJ81780


BJ81793 Antimony 08/25/15 08/26/15 08/28/15 LK YBJ81793 Arsenic 08/25/15 08/26/15 08/28/15 LK YBJ81793 Barium 08/25/15 08/26/15 08/28/15 LK YBJ81793 Beryllium 08/25/15 08/26/15 08/28/15 LK YBJ81793 Cadmium 08/25/15 08/26/15 08/28/15 LK YBJ81793 Calcium 08/25/15 08/26/15 08/28/15 LK YBJ81793 Chromium 08/25/15 08/26/15 08/28/15 LK YBJ81793 Cobalt 08/25/15 08/26/15 08/28/15 LK YBJ81793 Copper 08/25/15 08/26/15 08/28/15 LK YBJ81793 Iron 08/25/15 08/26/15 08/28/15 LK YBJ81793 Lead 08/25/15 08/26/15 08/28/15 LK YBJ81793 Magnesium 08/25/15 08/26/15 08/28/15 LK YBJ81793 Manganese 08/25/15 08/26/15 08/28/15 LK YBJ81793 Mercury 08/25/15 08/27/15 08/27/15 RS YBJ81793 Nickel 08/25/15 08/26/15 08/28/15 LK YBJ81793 Pesticides - Soil 08/25/15 08/26/15 09/03/15 CE YBJ81793 Polychlorinated Biphenyls 08/25/15 08/26/15 08/29/15 AW YBJ81793 Potassium 08/25/15 08/26/15 08/28/15 LK YBJ81793 Selenium 08/25/15 08/26/15 08/28/15 LK YBJ81793 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81793 Silver 08/25/15 08/26/15 08/28/15 LK YBJ81793 Sodium 08/25/15 08/26/15 08/28/15 LK YBJ81793 Thallium 08/25/15 08/26/15 08/28/15 LK YBJ81793 Vanadium 08/25/15 08/26/15 08/28/15 LK YBJ81793 Volatiles 08/25/15 08/31/15 08/31/15 JLI YBJ81793 Volatiles 08/25/15 08/31/15 08/31/15 JLI YBJ81793 Zinc 08/25/15 08/26/15 08/28/15 LK YBJ81794 1,4-dioxane 08/25/15 08/31/15 08/31/15 JLI YBJ81794 Aluminum 08/25/15 08/26/15 08/28/15 LK YBJ81794 Antimony 08/25/15 08/26/15 08/28/15 LK YBJ81794 Arsenic 08/25/15 08/26/15 08/28/15 LK YBJ81794 Barium 08/25/15 08/26/15 08/28/15 LK YBJ81794 Beryllium 08/25/15 08/26/15 08/28/15 LK YBJ81794 Cadmium 08/25/15 08/26/15 08/28/15 LK YBJ81794 Calcium 08/25/15 08/26/15 08/28/15 LK YBJ81794 Chromium 08/25/15 08/26/15 08/28/15 LK YBJ81794 Cobalt 08/25/15 08/26/15 08/28/15 LK Y




SDG I.D.: GBJ81780


BJ81794 Copper 08/25/15 08/26/15 08/28/15 LK YBJ81794 Iron 08/25/15 08/26/15 08/28/15 LK YBJ81794 Lead 08/25/15 08/26/15 08/28/15 LK YBJ81794 Magnesium 08/25/15 08/26/15 08/28/15 LK YBJ81794 Manganese 08/25/15 08/26/15 08/28/15 LK YBJ81794 Mercury 08/25/15 08/27/15 08/27/15 RS YBJ81794 Nickel 08/25/15 08/26/15 08/28/15 LK YBJ81794 Pesticides - Soil 08/25/15 08/26/15 08/28/15 CE YBJ81794 Polychlorinated Biphenyls 08/25/15 08/26/15 08/29/15 AW YBJ81794 Potassium 08/25/15 08/26/15 08/28/15 LK YBJ81794 Selenium 08/25/15 08/26/15 08/28/15 LK YBJ81794 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81794 Silver 08/25/15 08/26/15 08/28/15 LK YBJ81794 Sodium 08/25/15 08/26/15 08/28/15 LK YBJ81794 Thallium 08/25/15 08/26/15 08/28/15 LK YBJ81794 Vanadium 08/25/15 08/26/15 08/28/15 LK YBJ81794 Volatiles 08/25/15 08/31/15 08/31/15 JLI YBJ81794 Volatiles 08/25/15 08/31/15 08/31/15 JLI YBJ81794 Zinc 08/25/15 08/26/15 08/28/15 LK YBJ81795 1,4-dioxane 08/25/15 08/30/15 08/30/15 JLI YBJ81795 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81795 Volatiles 08/25/15 08/30/15 08/30/15 JLI YBJ81795 Volatiles 08/25/15 08/31/15 08/31/15 JLI YBJ81796 1,4-dioxane 08/25/15 09/01/15 09/01/15 JLI YBJ81796 Aluminum 08/25/15 08/26/15 08/28/15 LK YBJ81796 Antimony 08/25/15 08/26/15 08/28/15 LK YBJ81796 Arsenic 08/25/15 08/26/15 08/28/15 LK YBJ81796 Barium 08/25/15 08/26/15 08/28/15 LK YBJ81796 Beryllium 08/25/15 08/26/15 08/28/15 LK YBJ81796 Cadmium 08/25/15 08/26/15 08/28/15 LK YBJ81796 Calcium 08/25/15 08/26/15 08/28/15 LK YBJ81796 Chromium 08/25/15 08/26/15 08/28/15 LK YBJ81796 Cobalt 08/25/15 08/26/15 08/28/15 LK YBJ81796 Copper 08/25/15 08/26/15 08/28/15 LK YBJ81796 Iron 08/25/15 08/26/15 08/28/15 LK YBJ81796 Lead 08/25/15 08/26/15 08/28/15 LK YBJ81796 Magnesium 08/25/15 08/26/15 08/28/15 LK Y




SDG I.D.: GBJ81780


BJ81796 Manganese 08/25/15 08/26/15 08/28/15 LK YBJ81796 Mercury 08/25/15 08/27/15 08/27/15 RS YBJ81796 Nickel 08/25/15 08/26/15 08/28/15 LK YBJ81796 Pesticides - Soil 08/25/15 08/26/15 08/29/15 CE YBJ81796 Polychlorinated Biphenyls 08/25/15 08/26/15 08/29/15 AW YBJ81796 Potassium 08/25/15 08/26/15 08/28/15 LK YBJ81796 Selenium 08/25/15 08/26/15 08/28/15 LK YBJ81796 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81796 Silver 08/25/15 08/26/15 08/28/15 LK YBJ81796 Sodium 08/25/15 08/26/15 08/28/15 LK YBJ81796 Thallium 08/25/15 08/26/15 08/28/15 LK YBJ81796 Vanadium 08/25/15 08/26/15 08/28/15 LK YBJ81796 Volatiles 08/25/15 09/01/15 09/01/15 JLI YBJ81796 Volatiles 08/25/15 09/01/15 09/01/15 JLI YBJ81796 Zinc 08/25/15 08/26/15 08/31/15 LK YBJ81797 1,4-dioxane 08/25/15 08/31/15 08/31/15 JLI YBJ81797 Aluminum 08/25/15 08/26/15 08/28/15 LK YBJ81797 Antimony 08/25/15 08/26/15 08/28/15 LK YBJ81797 Arsenic 08/25/15 08/26/15 08/28/15 LK YBJ81797 Barium 08/25/15 08/26/15 08/28/15 LK YBJ81797 Beryllium 08/25/15 08/26/15 08/28/15 LK YBJ81797 Cadmium 08/25/15 08/26/15 08/28/15 LK YBJ81797 Calcium 08/25/15 08/26/15 08/28/15 LK YBJ81797 Chromium 08/25/15 08/26/15 08/28/15 LK YBJ81797 Cobalt 08/25/15 08/26/15 08/28/15 LK YBJ81797 Copper 08/25/15 08/26/15 08/28/15 LK YBJ81797 Iron 08/25/15 08/26/15 08/28/15 LK YBJ81797 Lead 08/25/15 08/26/15 08/28/15 LK YBJ81797 Magnesium 08/25/15 08/26/15 08/28/15 LK YBJ81797 Manganese 08/25/15 08/26/15 08/28/15 LK YBJ81797 Mercury 08/25/15 08/27/15 08/27/15 RS YBJ81797 Nickel 08/25/15 08/26/15 08/28/15 LK YBJ81797 Pesticides - Soil 08/25/15 08/26/15 08/28/15 CE YBJ81797 Polychlorinated Biphenyls 08/25/15 08/26/15 08/29/15 AW YBJ81797 Potassium 08/25/15 08/26/15 08/28/15 LK YBJ81797 Selenium 08/25/15 08/26/15 08/28/15 LK YBJ81797 Semivolatiles 08/25/15 08/26/15 08/27/15 DD Y




SDG I.D.: GBJ81780


BJ81797 Silver 08/25/15 08/26/15 08/28/15 LK YBJ81797 Sodium 08/25/15 08/26/15 08/28/15 LK YBJ81797 Thallium 08/25/15 08/26/15 08/28/15 LK YBJ81797 Vanadium 08/25/15 08/26/15 08/28/15 LK YBJ81797 Volatiles 08/25/15 08/31/15 08/31/15 JLI YBJ81797 Volatiles 08/25/15 09/01/15 09/01/15 JLI YBJ81797 Zinc 08/25/15 08/26/15 08/28/15 LK YBJ81798 1,4-dioxane 08/25/15 08/30/15 08/30/15 JLI YBJ81798 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81798 Volatiles 08/25/15 08/30/15 08/30/15 JLI YBJ81798 Volatiles 08/25/15 08/31/15 08/31/15 JLI YBJ81799 1,4-dioxane 08/25/15 08/30/15 08/30/15 JLI YBJ81799 Aluminum 08/25/15 08/26/15 08/28/15 LK YBJ81799 Antimony 08/25/15 08/26/15 08/28/15 LK YBJ81799 Arsenic 08/25/15 08/26/15 08/28/15 LK YBJ81799 Barium 08/25/15 08/26/15 08/28/15 LK YBJ81799 Beryllium 08/25/15 08/26/15 08/28/15 LK YBJ81799 Cadmium 08/25/15 08/26/15 08/28/15 LK YBJ81799 Calcium 08/25/15 08/26/15 08/28/15 LK YBJ81799 Chromium 08/25/15 08/26/15 08/28/15 LK YBJ81799 Cobalt 08/25/15 08/26/15 08/28/15 LK YBJ81799 Copper 08/25/15 08/26/15 08/28/15 LK YBJ81799 Iron 08/25/15 08/26/15 08/28/15 LK YBJ81799 Lead 08/25/15 08/26/15 08/28/15 LK YBJ81799 Magnesium 08/25/15 08/26/15 08/28/15 LK YBJ81799 Manganese 08/25/15 08/26/15 08/28/15 LK YBJ81799 Mercury 08/25/15 08/27/15 08/27/15 RS YBJ81799 Nickel 08/25/15 08/26/15 08/28/15 LK YBJ81799 Pesticides - Soil 08/25/15 08/26/15 08/28/15 CE YBJ81799 Polychlorinated Biphenyls 08/25/15 08/26/15 08/29/15 AW YBJ81799 Potassium 08/25/15 08/26/15 08/28/15 LK YBJ81799 Selenium 08/25/15 08/26/15 08/28/15 LK YBJ81799 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81799 Silver 08/25/15 08/26/15 08/28/15 LK YBJ81799 Sodium 08/25/15 08/26/15 08/28/15 LK YBJ81799 Thallium 08/25/15 08/26/15 08/28/15 LK YBJ81799 Vanadium 08/25/15 08/26/15 08/28/15 LK Y




SDG I.D.: GBJ81780


BJ81799 Volatiles 08/25/15 08/30/15 08/30/15 JLI YBJ81799 Volatiles 08/25/15 08/31/15 08/31/15 JLI YBJ81799 Zinc 08/25/15 08/26/15 08/31/15 LK YBJ81800 1,4-dioxane 08/25/15 08/30/15 08/30/15 JLI YBJ81800 Aluminum 08/25/15 08/26/15 08/28/15 LK YBJ81800 Antimony 08/25/15 08/26/15 08/28/15 LK YBJ81800 Arsenic 08/25/15 08/26/15 08/28/15 LK YBJ81800 Barium 08/25/15 08/26/15 08/28/15 LK YBJ81800 Beryllium 08/25/15 08/26/15 08/28/15 LK YBJ81800 Cadmium 08/25/15 08/26/15 08/28/15 LK YBJ81800 Calcium 08/25/15 08/26/15 08/28/15 LK YBJ81800 Chromium 08/25/15 08/26/15 08/28/15 LK YBJ81800 Cobalt 08/25/15 08/26/15 08/28/15 LK YBJ81800 Copper 08/25/15 08/26/15 08/28/15 LK YBJ81800 Iron 08/25/15 08/26/15 08/28/15 LK YBJ81800 Lead 08/25/15 08/26/15 08/28/15 LK YBJ81800 Magnesium 08/25/15 08/26/15 08/28/15 LK YBJ81800 Manganese 08/25/15 08/26/15 08/28/15 LK YBJ81800 Mercury 08/25/15 08/27/15 08/27/15 RS YBJ81800 Nickel 08/25/15 08/26/15 08/28/15 LK YBJ81800 Pesticides - Soil 08/25/15 08/26/15 08/28/15 CE YBJ81800 Polychlorinated Biphenyls 08/25/15 08/26/15 08/31/15 AW YBJ81800 Potassium 08/25/15 08/26/15 08/28/15 LK YBJ81800 Selenium 08/25/15 08/26/15 08/28/15 LK YBJ81800 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81800 Silver 08/25/15 08/26/15 08/28/15 LK YBJ81800 Sodium 08/25/15 08/26/15 08/28/15 LK YBJ81800 Thallium 08/25/15 08/26/15 08/28/15 LK YBJ81800 Vanadium 08/25/15 08/26/15 08/28/15 LK YBJ81800 Volatiles 08/25/15 08/30/15 08/30/15 JLI YBJ81800 Volatiles 08/25/15 08/31/15 08/31/15 JLI YBJ81800 Zinc 08/25/15 08/26/15 08/28/15 LK YBJ81801 1,4-dioxane 08/25/15 08/31/15 08/31/15 JLI YBJ81801 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81801 Volatiles 08/25/15 08/31/15 08/31/15 JLI YBJ81801 Volatiles 08/25/15 09/01/15 09/01/15 JLI YBJ81802 1,4-dioxane 08/25/15 08/31/15 08/31/15 JLI Y




SDG I.D.: GBJ81780


BJ81802 Aluminum 08/25/15 08/26/15 08/28/15 LK YBJ81802 Antimony 08/25/15 08/26/15 08/28/15 LK YBJ81802 Arsenic 08/25/15 08/26/15 08/28/15 LK YBJ81802 Barium 08/25/15 08/26/15 08/28/15 LK YBJ81802 Beryllium 08/25/15 08/26/15 08/28/15 LK YBJ81802 Cadmium 08/25/15 08/26/15 08/28/15 LK YBJ81802 Calcium 08/25/15 08/26/15 08/28/15 LK YBJ81802 Chromium 08/25/15 08/26/15 08/28/15 LK YBJ81802 Cobalt 08/25/15 08/26/15 08/28/15 LK YBJ81802 Copper 08/25/15 08/26/15 08/28/15 LK YBJ81802 Iron 08/25/15 08/26/15 08/28/15 LK YBJ81802 Lead 08/25/15 08/26/15 08/28/15 LK YBJ81802 Magnesium 08/25/15 08/26/15 08/28/15 LK YBJ81802 Manganese 08/25/15 08/26/15 08/28/15 LK YBJ81802 Mercury 08/25/15 08/27/15 08/27/15 RS YBJ81802 Nickel 08/25/15 08/26/15 08/28/15 LK YBJ81802 Pesticides - Soil 08/25/15 08/26/15 08/28/15 CE YBJ81802 Polychlorinated Biphenyls 08/25/15 08/26/15 08/29/15 AW YBJ81802 Potassium 08/25/15 08/26/15 08/28/15 LK YBJ81802 Selenium 08/25/15 08/26/15 08/28/15 LK YBJ81802 Semivolatiles 08/25/15 08/26/15 08/27/15 DD YBJ81802 Silver 08/25/15 08/26/15 08/28/15 LK YBJ81802 Sodium 08/25/15 08/26/15 08/28/15 LK YBJ81802 Thallium 08/25/15 08/26/15 08/28/15 LK YBJ81802 Vanadium 08/25/15 08/26/15 08/28/15 LK YBJ81802 Volatiles 08/25/15 08/30/15 08/30/15 JLI YBJ81802 Volatiles 08/25/15 08/31/15 08/31/15 JLI YBJ81802 Zinc 08/25/15 08/26/15 08/28/15 LK YBJ81976 Volatiles 08/25/15 08/31/15 08/31/15 JLI YBJ81976 Volatiles 08/25/15 08/31/15 08/31/15 JLI YBJ81977 Volatiles 08/25/15 08/31/15 08/31/15 JLI YBJ81977 Volatiles 08/25/15 08/31/15 08/31/15 JLI Y



SOLIDEBC72 Hour

08/25/15SWsee "By" below

RB

Laboratory Data

14B8 (0-5)

Phoenix ID: BJ81780

08/26/158:00

17:00




Date Time



SDG ID: GBJ81780

Client ID:Project ID: 510 DRIGGS

LOD/MDL Dilution

< 0.34Silver 0.34 08/28/15 LK SW6010Cmg/Kg0.34 18600Aluminum 34 08/28/15 LK SW6010Cmg/Kg6.9 102.3Arsenic 0.7 08/28/15 LK SW6010Cmg/Kg0.69 1

58.0Barium 0.7 08/28/15 LK SW6010Cmg/Kg0.34 10.39Beryllium 0.27 08/28/15 LK SW6010Cmg/Kg0.14 16250Calcium 3.4 08/28/15 LK SW6010Cmg/Kg3.2 1

< 0.34Cadmium 0.34 08/28/15 LK SW6010Cmg/Kg0.14 16.26Cobalt 0.34 08/28/15 LK SW6010Cmg/Kg0.34 116.3Chromium 0.34 08/28/15 LK SW6010Cmg/Kg0.34 116.5Copper 0.34 08/28/15 LK SW6010Cmg/kg0.34 1

15100Iron 34 08/28/15 LK SW6010Cmg/Kg B34 100.14Mercury 0.03 08/27/15 RS SW7471Bmg/Kg0.02 11160Potassium 7 08/28/15 LK SW6010Cmg/Kg2.7 1N3670Magnesium 3.4 08/28/15 LK SW6010Cmg/Kg3.4 1337Manganese 3.4 08/28/15 LK SW6010Cmg/Kg3.4 10134Sodium 7 08/28/15 LK SW6010Cmg/Kg2.9 1N13.9Nickel 0.34 08/28/15 LK SW6010Cmg/Kg0.34 138.9Lead 0.7 08/28/15 LK SW6010Cmg/Kg0.34 1< 1.7Antimony 1.7 08/28/15 LK SW6010Cmg/Kg1.7 1N< 1.4Selenium 1.4 08/28/15 LK SW6010Cmg/Kg1.2 1< 1.4Thallium 1.4 08/28/15 LK SW6010Cmg/Kg1.4 127.6Vanadium 0.3 08/28/15 LK SW6010Cmg/Kg0.34 144.8Zinc 0.7 08/28/15 LK SW6010Cmg/Kg B0.34 190Percent Solid 08/26/15 I SW846-%Solid%

CompletedSoil Extraction for PCB 08/26/15 BC SW3545ACompletedSoil Extraction for Pesticide 08/26/15 BC/H SW3545ACompletedSoil Extraction for SVOA 08/26/15 BJ/VH SW3545ACompletedMercury Digestion 08/27/15 I/I SW7471B

Page 1 of 136 Ver 2

14B8 (0-5)Phoenix I.D.: BJ81780

Client ID:510 DRIGGSProject ID:


LOD/MDL Dilution

CompletedTotal Metals Digest 08/26/15 G/AG SW3050BCompletedField Extraction 08/25/15 SW5035A

Polychlorinated BiphenylsNDPCB-1016 37 08/29/15 AW SW8082Aug/Kg37 2NDPCB-1221 37 08/29/15 AW SW8082Aug/Kg37 2NDPCB-1232 37 08/29/15 AW SW8082Aug/Kg37 2NDPCB-1242 37 08/29/15 AW SW8082Aug/Kg37 2NDPCB-1248 37 08/29/15 AW SW8082Aug/Kg37 2NDPCB-1254 37 08/29/15 AW SW8082Aug/Kg37 2NDPCB-1260 37 08/29/15 AW SW8082Aug/Kg37 2NDPCB-1262 37 08/29/15 AW SW8082Aug/Kg37 2NDPCB-1268 37 08/29/15 AW SW8082Aug/Kg37 2


Pesticides - SoilND4,4' -DDD 15 08/28/15 CE SW8081Bug/Kg15 10ND4,4' -DDE 9.2 08/28/15 CE SW8081Bug/Kg9.2 10ND4,4' -DDT 9.2 08/28/15 CE SW8081Bug/Kg9.2 10NDa-BHC 18 08/28/15 CE SW8081Bug/Kg18 1050a-Chlordane 18 08/28/15 CE SW8081Bug/Kg18 10NDAldrin 5.5 08/28/15 CE SW8081Bug/Kg5.5 10NDb-BHC 18 08/28/15 CE SW8081Bug/Kg18 10NDd-BHC 37 08/28/15 CE SW8081Bug/Kg37 10NDDieldrin 5.5 08/28/15 CE SW8081Bug/Kg5.5 10NDEndosulfan I 37 08/28/15 CE SW8081Bug/Kg37 10NDEndosulfan II 37 08/28/15 CE SW8081Bug/Kg37 10NDEndosulfan sulfate 37 08/28/15 CE SW8081Bug/Kg37 10NDEndrin 18 08/28/15 CE SW8081Bug/Kg18 10NDEndrin aldehyde 37 08/28/15 CE SW8081Bug/Kg37 10NDEndrin ketone 37 08/28/15 CE SW8081Bug/Kg37 10NDg-BHC 7.3 08/28/15 CE SW8081Bug/Kg7.3 1039g-Chlordane 18 08/28/15 CE SW8081Bug/Kg18 10NDHeptachlor 37 08/28/15 CE SW8081Bug/Kg37 10NDHeptachlor epoxide 37 08/28/15 CE SW8081Bug/Kg37 10NDMethoxychlor 180 08/28/15 CE SW8081Bug/Kg180 10NDToxaphene 730 08/28/15 CE SW8081Bug/Kg730 10

QA/QC SurrogatesDiluted Out% DCBP 08/28/15 CE 30 - 150 %% 10Diluted Out% TCMX 08/28/15 CE 30 - 150 %% 10

VolatilesND1,1,1,2-Tetrachloroethane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1ND1,1,1-Trichloroethane 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND1,1,2,2-Tetrachloroethane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1ND1,1,2-Trichloroethane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1ND1,1-Dichloroethane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1ND1,1-Dichloroethene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1

Page 2 of 136 Ver 2

14B8 (0-5)Phoenix I.D.: BJ81780



LOD/MDL Dilution

ND1,1-Dichloropropene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND1,2,3-Trichlorobenzene 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1ND1,2,3-Trichloropropane 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND1,2,4-Trichlorobenzene 5.3 08/29/15 JLI SW8260Cug/Kg1.1 11.01,2,4-Trimethylbenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1JND1,2-Dibromo-3-chloropropane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1ND1,2-Dibromoethane 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND1,2-Dichlorobenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND1,2-Dichloroethane 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND1,2-Dichloropropane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1ND1,3,5-Trimethylbenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND1,3-Dichlorobenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND1,3-Dichloropropane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1ND1,4-Dichlorobenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND2,2-Dichloropropane 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND2-Chlorotoluene 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1ND2-Hexanone 26 08/29/15 JLI SW8260Cug/Kg5.3 1ND2-Isopropyltoluene 5.3 08/29/15 JLI SW8260Cug/Kg 10.53 1ND4-Chlorotoluene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND4-Methyl-2-pentanone 26 08/29/15 JLI SW8260Cug/Kg5.3 119Acetone 50 08/29/15 JLI SW8260Cug/Kg5.3 1JSNDAcrylonitrile 11 08/29/15 JLI SW8260Cug/Kg1.1 10.69Benzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1JNDBromobenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDBromochloromethane 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDBromodichloromethane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1NDBromoform 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1NDBromomethane 5.3 08/29/15 JLI SW8260Cug/Kg2.1 12.4Carbon Disulfide 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1JNDCarbon tetrachloride 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1NDChlorobenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDChloroethane 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDChloroform 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDChloromethane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1170cis-1,2-Dichloroethene 250 08/29/15 JLI SW8260Cug/Kg26 50JNDcis-1,3-Dichloropropene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDDibromochloromethane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1NDDibromomethane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1NDDichlorodifluoromethane 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDEthylbenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDHexachlorobutadiene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDIsopropylbenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 11.1m&p-Xylene 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1JNDMethyl Ethyl Ketone 32 08/29/15 JLI SW8260Cug/Kg5.3 1NDMethyl t-butyl ether (MTBE) 11 08/29/15 JLI SW8260Cug/Kg1.1 1NDMethylene chloride 5.3 08/29/15 JLI SW8260Cug/Kg5.3 12.6Naphthalene 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1JNDn-Butylbenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDn-Propylbenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.95 1

Page 3 of 136 Ver 2

14B8 (0-5)Phoenix I.D.: BJ81780



LOD/MDL Dilution

NDo-Xylene 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1NDp-Isopropyltoluene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDsec-Butylbenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDStyrene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDtert-Butylbenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDTetrachloroethene 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1NDTetrahydrofuran (THF) 11 08/29/15 JLI SW8260Cug/Kg 12.6 12.1Toluene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1J

0.84trans-1,2-Dichloroethene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1JNDtrans-1,3-Dichloropropene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDtrans-1,4-dichloro-2-butene 11 08/29/15 JLI SW8260Cug/Kg2.6 1250Trichloroethene 260 08/29/15 JLI SW8260Cug/Kg26 50JNDTrichlorofluoromethane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1NDTrichlorotrifluoroethane 5.3 08/29/15 JLI SW8260Cug/Kg0.53 10.58Vinyl chloride 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1J

QA/QC Surrogates103% 1,2-dichlorobenzene-d4 08/29/15 JLI 70 - 130 %% 187% Bromofluorobenzene 08/29/15 JLI 70 - 130 %% 1102% Dibromofluoromethane 08/29/15 JLI 70 - 130 %% 194% Toluene-d8 08/29/15 JLI 70 - 130 %% 1

1,4-dioxaneND1,4-dioxane 100 08/29/15 JLI SW8260Cug/kg42 1

QA/QC Surrogates103% 1,2-dichlorobenzene-d4 08/29/15 JLI 70 - 130 %% 187% Bromofluorobenzene 08/29/15 JLI 70 - 130 %% 194% Toluene-d8 08/29/15 JLI 70 - 130 %% 1

VolatilesND1,1,1,2-Tetrachloroethane 21 08/29/15 JLI SW8260Cug/Kg1.1 1NDAcrolein 21 08/29/15 JLI SW8260Cug/Kg2.6 1NDAcrylonitrile 21 08/29/15 JLI SW8260Cug/Kg0.53 1NDTert-butyl alcohol 110 08/29/15 JLI SW8260Cug/Kg21 1

SemivolatilesND1,2,4,5-Tetrachlorobenzene 260 08/27/15 DD SW8270Dug/Kg130 1ND1,2,4-Trichlorobenzene 260 08/27/15 DD SW8270Dug/Kg110 1ND1,2-Dichlorobenzene 260 08/27/15 DD SW8270Dug/Kg100 1ND1,2-Diphenylhydrazine 260 08/27/15 DD SW8270Dug/Kg120 1ND1,3-Dichlorobenzene 260 08/27/15 DD SW8270Dug/Kg110 1ND1,4-Dichlorobenzene 260 08/27/15 DD SW8270Dug/Kg110 1ND2,4,5-Trichlorophenol 260 08/27/15 DD SW8270Dug/Kg200 1ND2,4,6-Trichlorophenol 260 08/27/15 DD SW8270Dug/Kg120 1ND2,4-Dichlorophenol 260 08/27/15 DD SW8270Dug/Kg130 1ND2,4-Dimethylphenol 260 08/27/15 DD SW8270Dug/Kg90 1ND2,4-Dinitrophenol 730 08/27/15 DD SW8270Dug/Kg260 1ND2,4-Dinitrotoluene 260 08/27/15 DD SW8270Dug/Kg140 1ND2,6-Dinitrotoluene 260 08/27/15 DD SW8270Dug/Kg120 1ND2-Chloronaphthalene 260 08/27/15 DD SW8270Dug/Kg100 1ND2-Chlorophenol 260 08/27/15 DD SW8270Dug/Kg100 1

Page 4 of 136 Ver 2

14B8 (0-5)Phoenix I.D.: BJ81780



LOD/MDL Dilution

ND2-Methylnaphthalene 260 08/27/15 DD SW8270Dug/Kg110 1ND2-Methylphenol (o-cresol) 260 08/27/15 DD SW8270Dug/Kg170 1ND2-Nitroaniline 730 08/27/15 DD SW8270Dug/Kg370 1ND2-Nitrophenol 260 08/27/15 DD SW8270Dug/Kg230 1ND3&4-Methylphenol (m&p-cresol) 260 08/27/15 DD SW8270Dug/Kg 1140 1ND3,3'-Dichlorobenzidine 730 08/27/15 DD SW8270Dug/Kg170 1ND3-Nitroaniline 730 08/27/15 DD SW8270Dug/Kg730 1ND4,6-Dinitro-2-methylphenol 1800 08/27/15 DD SW8270Dug/Kg390 1ND4-Bromophenyl phenyl ether 260 08/27/15 DD SW8270Dug/Kg110 1ND4-Chloro-3-methylphenol 260 08/27/15 DD SW8270Dug/Kg130 1ND4-Chloroaniline 290 08/27/15 DD SW8270Dug/Kg170 1ND4-Chlorophenyl phenyl ether 260 08/27/15 DD SW8270Dug/Kg120 1ND4-Nitroaniline 730 08/27/15 DD SW8270Dug/Kg120 1ND4-Nitrophenol 360 08/27/15 DD SW8270Dug/Kg160 1NDAcenaphthene 260 08/27/15 DD SW8270Dug/Kg110 1130Acenaphthylene 260 08/27/15 DD SW8270Dug/Kg100 1JNDAcetophenone 260 08/27/15 DD SW8270Dug/Kg110 1NDAniline 290 08/27/15 DD SW8270Dug/Kg290 1200Anthracene 260 08/27/15 DD SW8270Dug/Kg120 1J

1100Benz(a)anthracene 260 08/27/15 DD SW8270Dug/Kg120 1NDBenzidine 730 08/27/15 DD SW8270Dug/Kg210 1970Benzo(a)pyrene 260 08/27/15 DD SW8270Dug/Kg120 1820Benzo(b)fluoranthene 260 08/27/15 DD SW8270Dug/Kg120 1620Benzo(ghi)perylene 260 08/27/15 DD SW8270Dug/Kg120 1980Benzo(k)fluoranthene 260 08/27/15 DD SW8270Dug/Kg120 1NDBenzoic acid 1800 08/27/15 DD SW8270Dug/Kg 1730 1NDBenzyl butyl phthalate 260 08/27/15 DD SW8270Dug/Kg94 1NDBis(2-chloroethoxy)methane 260 08/27/15 DD SW8270Dug/Kg100 1NDBis(2-chloroethyl)ether 260 08/27/15 DD SW8270Dug/Kg98 1NDBis(2-chloroisopropyl)ether 260 08/27/15 DD SW8270Dug/Kg 1100 1NDBis(2-ethylhexyl)phthalate 260 08/27/15 DD SW8270Dug/Kg100 1NDCarbazole 1800 08/27/15 DD SW8270Dug/Kg280 1

1100Chrysene 260 08/27/15 DD SW8270Dug/Kg120 1200Dibenz(a,h)anthracene 260 08/27/15 DD SW8270Dug/Kg120 1JNDDibenzofuran 260 08/27/15 DD SW8270Dug/Kg110 1NDDiethyl phthalate 260 08/27/15 DD SW8270Dug/Kg120 1NDDimethylphthalate 260 08/27/15 DD SW8270Dug/Kg110 1NDDi-n-butylphthalate 260 08/27/15 DD SW8270Dug/Kg97 1NDDi-n-octylphthalate 260 08/27/15 DD SW8270Dug/Kg94 1

1800Fluoranthene 260 08/27/15 DD SW8270Dug/Kg120 1NDFluorene 260 08/27/15 DD SW8270Dug/Kg120 1NDHexachlorobenzene 260 08/27/15 DD SW8270Dug/Kg110 1NDHexachlorobutadiene 260 08/27/15 DD SW8270Dug/Kg130 1NDHexachlorocyclopentadiene 260 08/27/15 DD SW8270Dug/Kg110 1NDHexachloroethane 260 08/27/15 DD SW8270Dug/Kg110 1680Indeno(1,2,3-cd)pyrene 260 08/27/15 DD SW8270Dug/Kg120 1NDIsophorone 260 08/27/15 DD SW8270Dug/Kg100 1NDNaphthalene 260 08/27/15 DD SW8270Dug/Kg100 1NDNitrobenzene 260 08/27/15 DD SW8270Dug/Kg130 1

Page 5 of 136 Ver 2

14B8 (0-5)Phoenix I.D.: BJ81780



LOD/MDL Dilution

NDN-Nitrosodimethylamine 260 08/27/15 DD SW8270Dug/Kg100 1NDN-Nitrosodi-n-propylamine 260 08/27/15 DD SW8270Dug/Kg120 1NDN-Nitrosodiphenylamine 260 08/27/15 DD SW8270Dug/Kg140 1NDPentachloronitrobenzene 260 08/27/15 DD SW8270Dug/Kg140 1NDPentachlorophenol 260 08/27/15 DD SW8270Dug/Kg140 1730Phenanthrene 260 08/27/15 DD SW8270Dug/Kg100 1NDPhenol 260 08/27/15 DD SW8270Dug/Kg120 1

1500Pyrene 260 08/27/15 DD SW8270Dug/Kg130 1NDPyridine 260 08/27/15 DD SW8270Dug/Kg90 1


Comments:










RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level J=Estimated Below RL LOD=Limit of Detection MDL=Method Detection Limit

Page 6 of 136 Ver 2



SOLIDEBC72 Hour


RB

Laboratory Data

14B8 (10-15)

Phoenix ID: BJ81781

08/26/158:15

17:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution

82Percent Solid 08/26/15 I SW846-%Solid%CompletedSoil Extraction for SVOA 08/26/15 BJ/VH SW3545ACompletedField Extraction 08/25/15 SW5035A

VolatilesND1,1,1,2-Tetrachloroethane 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1ND1,1,1-Trichloroethane 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1ND1,1,2,2-Tetrachloroethane 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1ND1,1,2-Trichloroethane 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1ND1,1-Dichloroethane 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1ND1,1-Dichloroethene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1ND1,1-Dichloropropene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1ND1,2,3-Trichlorobenzene 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1ND1,2,3-Trichloropropane 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1ND1,2,4-Trichlorobenzene 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1ND1,2,4-Trimethylbenzene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1ND1,2-Dibromo-3-chloropropane 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1ND1,2-Dibromoethane 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1ND1,2-Dichlorobenzene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1ND1,2-Dichloroethane 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1ND1,2-Dichloropropane 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1ND1,3,5-Trimethylbenzene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1ND1,3-Dichlorobenzene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1ND1,3-Dichloropropane 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1ND1,4-Dichlorobenzene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1ND2,2-Dichloropropane 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1ND2-Chlorotoluene 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1ND2-Hexanone 23 08/29/15 JLI SW8260Cug/Kg4.6 1

Page 7 of 136 Ver 2

14B8 (10-15)Phoenix I.D.: BJ81781



LOD/MDL Dilution

ND2-Isopropyltoluene 4.6 08/29/15 JLI SW8260Cug/Kg 10.46 1ND4-Chlorotoluene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1ND4-Methyl-2-pentanone 23 08/29/15 JLI SW8260Cug/Kg4.6 1NDAcetone 46 08/29/15 JLI SW8260Cug/Kg4.6 1NDAcrylonitrile 9.1 08/29/15 JLI SW8260Cug/Kg0.91 1NDBenzene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDBromobenzene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDBromochloromethane 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDBromodichloromethane 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1NDBromoform 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1NDBromomethane 4.6 08/29/15 JLI SW8260Cug/Kg1.8 1NDCarbon Disulfide 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1NDCarbon tetrachloride 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1NDChlorobenzene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDChloroethane 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDChloroform 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDChloromethane 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1NDcis-1,2-Dichloroethene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDcis-1,3-Dichloropropene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDDibromochloromethane 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1NDDibromomethane 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1NDDichlorodifluoromethane 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDEthylbenzene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDHexachlorobutadiene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDIsopropylbenzene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDm&p-Xylene 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1NDMethyl Ethyl Ketone 27 08/29/15 JLI SW8260Cug/Kg4.6 1NDMethyl t-butyl ether (MTBE) 9.1 08/29/15 JLI SW8260Cug/Kg0.91 1NDMethylene chloride 4.6 08/29/15 JLI SW8260Cug/Kg4.6 1NDNaphthalene 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1NDn-Butylbenzene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDn-Propylbenzene 4.6 08/29/15 JLI SW8260Cug/Kg0.82 1NDo-Xylene 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1NDp-Isopropyltoluene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDsec-Butylbenzene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDStyrene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDtert-Butylbenzene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDTetrachloroethene 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1NDTetrahydrofuran (THF) 9.1 08/29/15 JLI SW8260Cug/Kg 12.3 1NDToluene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDtrans-1,2-Dichloroethene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDtrans-1,3-Dichloropropene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDtrans-1,4-dichloro-2-butene 9.1 08/29/15 JLI SW8260Cug/Kg2.3 13.2Trichloroethene 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1JNDTrichlorofluoromethane 4.6 08/29/15 JLI SW8260Cug/Kg0.91 1NDTrichlorotrifluoroethane 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1NDVinyl chloride 4.6 08/29/15 JLI SW8260Cug/Kg0.46 1

QA/QC Surrogates100% 1,2-dichlorobenzene-d4 08/29/15 JLI 70 - 130 %% 1

Page 8 of 136 Ver 2

14B8 (10-15)Phoenix I.D.: BJ81781



LOD/MDL Dilution

98% Bromofluorobenzene 08/29/15 JLI 70 - 130 %% 1100% Dibromofluoromethane 08/29/15 JLI 70 - 130 %% 199% Toluene-d8 08/29/15 JLI 70 - 130 %% 1




SemivolatilesND1,2,4,5-Tetrachlorobenzene 280 08/27/15 DD SW8270Dug/Kg140 1ND1,2,4-Trichlorobenzene 280 08/27/15 DD SW8270Dug/Kg120 1ND1,2-Dichlorobenzene 280 08/27/15 DD SW8270Dug/Kg110 1ND1,2-Diphenylhydrazine 280 08/27/15 DD SW8270Dug/Kg130 1ND1,3-Dichlorobenzene 280 08/27/15 DD SW8270Dug/Kg120 1ND1,4-Dichlorobenzene 280 08/27/15 DD SW8270Dug/Kg120 1ND2,4,5-Trichlorophenol 280 08/27/15 DD SW8270Dug/Kg220 1ND2,4,6-Trichlorophenol 280 08/27/15 DD SW8270Dug/Kg130 1ND2,4-Dichlorophenol 280 08/27/15 DD SW8270Dug/Kg140 1ND2,4-Dimethylphenol 280 08/27/15 DD SW8270Dug/Kg99 1ND2,4-Dinitrophenol 800 08/27/15 DD SW8270Dug/Kg280 1ND2,4-Dinitrotoluene 280 08/27/15 DD SW8270Dug/Kg160 1ND2,6-Dinitrotoluene 280 08/27/15 DD SW8270Dug/Kg130 1ND2-Chloronaphthalene 280 08/27/15 DD SW8270Dug/Kg110 1ND2-Chlorophenol 280 08/27/15 DD SW8270Dug/Kg110 1ND2-Methylnaphthalene 280 08/27/15 DD SW8270Dug/Kg120 1ND2-Methylphenol (o-cresol) 280 08/27/15 DD SW8270Dug/Kg190 1ND2-Nitroaniline 800 08/27/15 DD SW8270Dug/Kg400 1ND2-Nitrophenol 280 08/27/15 DD SW8270Dug/Kg250 1ND3&4-Methylphenol (m&p-cresol) 280 08/27/15 DD SW8270Dug/Kg 1160 1ND3,3'-Dichlorobenzidine 800 08/27/15 DD SW8270Dug/Kg190 1ND3-Nitroaniline 800 08/27/15 DD SW8270Dug/Kg800 1ND4,6-Dinitro-2-methylphenol 2000 08/27/15 DD SW8270Dug/Kg430 1ND4-Bromophenyl phenyl ether 280 08/27/15 DD SW8270Dug/Kg120 1ND4-Chloro-3-methylphenol 280 08/27/15 DD SW8270Dug/Kg140 1ND4-Chloroaniline 320 08/27/15 DD SW8270Dug/Kg190 1ND4-Chlorophenyl phenyl ether 280 08/27/15 DD SW8270Dug/Kg130 1ND4-Nitroaniline 800 08/27/15 DD SW8270Dug/Kg130 1ND4-Nitrophenol 400 08/27/15 DD SW8270Dug/Kg180 1NDAcenaphthene 280 08/27/15 DD SW8270Dug/Kg120 1NDAcenaphthylene 280 08/27/15 DD SW8270Dug/Kg110 1NDAcetophenone 280 08/27/15 DD SW8270Dug/Kg120 1

Page 9 of 136 Ver 2

14B8 (10-15)Phoenix I.D.: BJ81781



LOD/MDL Dilution

NDAniline 320 08/27/15 DD SW8270Dug/Kg320 1NDAnthracene 280 08/27/15 DD SW8270Dug/Kg130 1NDBenz(a)anthracene 280 08/27/15 DD SW8270Dug/Kg130 1NDBenzidine 800 08/27/15 DD SW8270Dug/Kg240 1NDBenzo(a)pyrene 280 08/27/15 DD SW8270Dug/Kg130 1NDBenzo(b)fluoranthene 280 08/27/15 DD SW8270Dug/Kg140 1NDBenzo(ghi)perylene 280 08/27/15 DD SW8270Dug/Kg130 1NDBenzo(k)fluoranthene 280 08/27/15 DD SW8270Dug/Kg130 1NDBenzoic acid 2000 08/27/15 DD SW8270Dug/Kg 1800 1NDBenzyl butyl phthalate 280 08/27/15 DD SW8270Dug/Kg100 1NDBis(2-chloroethoxy)methane 280 08/27/15 DD SW8270Dug/Kg110 1NDBis(2-chloroethyl)ether 280 08/27/15 DD SW8270Dug/Kg110 1NDBis(2-chloroisopropyl)ether 280 08/27/15 DD SW8270Dug/Kg 1110 1NDBis(2-ethylhexyl)phthalate 280 08/27/15 DD SW8270Dug/Kg120 1NDCarbazole 2000 08/27/15 DD SW8270Dug/Kg300 1NDChrysene 280 08/27/15 DD SW8270Dug/Kg130 1NDDibenz(a,h)anthracene 280 08/27/15 DD SW8270Dug/Kg130 1NDDibenzofuran 280 08/27/15 DD SW8270Dug/Kg120 1NDDiethyl phthalate 280 08/27/15 DD SW8270Dug/Kg130 1NDDimethylphthalate 280 08/27/15 DD SW8270Dug/Kg120 1NDDi-n-butylphthalate 280 08/27/15 DD SW8270Dug/Kg110 1NDDi-n-octylphthalate 280 08/27/15 DD SW8270Dug/Kg100 1NDFluoranthene 280 08/27/15 DD SW8270Dug/Kg130 1NDFluorene 280 08/27/15 DD SW8270Dug/Kg130 1NDHexachlorobenzene 280 08/27/15 DD SW8270Dug/Kg120 1NDHexachlorobutadiene 280 08/27/15 DD SW8270Dug/Kg140 1NDHexachlorocyclopentadiene 280 08/27/15 DD SW8270Dug/Kg120 1NDHexachloroethane 280 08/27/15 DD SW8270Dug/Kg120 1150Indeno(1,2,3-cd)pyrene 280 08/27/15 DD SW8270Dug/Kg130 1JNDIsophorone 280 08/27/15 DD SW8270Dug/Kg110 1NDNaphthalene 280 08/27/15 DD SW8270Dug/Kg120 1NDNitrobenzene 280 08/27/15 DD SW8270Dug/Kg140 1NDN-Nitrosodimethylamine 280 08/27/15 DD SW8270Dug/Kg110 1NDN-Nitrosodi-n-propylamine 280 08/27/15 DD SW8270Dug/Kg130 1NDN-Nitrosodiphenylamine 280 08/27/15 DD SW8270Dug/Kg150 1NDPentachloronitrobenzene 280 08/27/15 DD SW8270Dug/Kg150 1NDPentachlorophenol 280 08/27/15 DD SW8270Dug/Kg150 1NDPhenanthrene 280 08/27/15 DD SW8270Dug/Kg110 1NDPhenol 280 08/27/15 DD SW8270Dug/Kg130 1NDPyrene 280 08/27/15 DD SW8270Dug/Kg140 1NDPyridine 280 08/27/15 DD SW8270Dug/Kg98 1


Page 10 of 136 Ver 2

14B8 (10-15)Phoenix I.D.: BJ81781



LOD/MDL Dilution

Comments:











SOLIDEBC72 Hour


RB

Laboratory Data

14B8 (20-25)

Phoenix ID: BJ81782

08/26/158:30

17:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution

< 0.41Silver 0.41 08/28/15 LK SW6010Cmg/Kg0.41 112800Aluminum 41 08/28/15 LK SW6010Cmg/Kg8.2 10

1.9Arsenic 0.8 08/28/15 LK SW6010Cmg/Kg0.82 180.0Barium 0.8 08/28/15 LK SW6010Cmg/Kg0.41 10.69Beryllium 0.33 08/28/15 LK SW6010Cmg/Kg0.16 12370Calcium 4.1 08/28/15 LK SW6010Cmg/Kg3.8 1


27100Iron 41 08/28/15 LK SW6010Cmg/Kg B41 10< 0.03Mercury 0.03 08/27/15 RS SW7471Bmg/Kg0.02 13690Potassium 8 08/28/15 LK SW6010Cmg/Kg3.2 1N5160Magnesium 4.1 08/28/15 LK SW6010Cmg/Kg4.1 1589Manganese 4.1 08/28/15 LK SW6010Cmg/Kg4.1 10249Sodium 8 08/28/15 LK SW6010Cmg/Kg3.5 1N21.6Nickel 0.41 08/28/15 LK SW6010Cmg/Kg0.41 18.3Lead 0.8 08/28/15 LK SW6010Cmg/Kg0.41 1

< 2.1Antimony 2.1 08/28/15 LK SW6010Cmg/Kg2.1 1N< 1.6Selenium 1.6 08/28/15 LK SW6010Cmg/Kg1.4 1< 1.6Thallium 1.6 08/28/15 LK SW6010Cmg/Kg1.6 137.8Vanadium 0.4 08/28/15 LK SW6010Cmg/Kg0.41 149.8Zinc 0.8 08/28/15 LK SW6010Cmg/Kg B0.41 177Percent Solid 08/26/15 I SW846-%Solid%



14B8 (20-25)Phoenix I.D.: BJ81782



LOD/MDL Dilution




Pesticides - SoilND4,4' -DDD 2.6 08/28/15 F SW8081Bug/Kg2.6 2ND4,4' -DDE 2.6 08/28/15 F SW8081Bug/Kg2.6 2ND4,4' -DDT 2.6 08/28/15 F SW8081Bug/Kg2.6 2NDa-BHC 8.6 08/28/15 F SW8081Bug/Kg8.6 2NDa-Chlordane 4.3 08/28/15 F SW8081Bug/Kg4.3 2NDAldrin 4.3 08/28/15 F SW8081Bug/Kg4.3 2NDb-BHC 8.6 08/28/15 F SW8081Bug/Kg8.6 2NDd-BHC 8.6 08/28/15 F SW8081Bug/Kg8.6 2NDDieldrin 4.3 08/28/15 F SW8081Bug/Kg4.3 2NDEndosulfan I 8.6 08/28/15 F SW8081Bug/Kg8.6 2NDEndosulfan II 8.6 08/28/15 F SW8081Bug/Kg8.6 2NDEndosulfan sulfate 8.6 08/28/15 F SW8081Bug/Kg8.6 2NDEndrin 8.6 08/28/15 F SW8081Bug/Kg8.6 2NDEndrin aldehyde 8.6 08/28/15 F SW8081Bug/Kg8.6 2NDEndrin ketone 8.6 08/28/15 F SW8081Bug/Kg8.6 2NDg-BHC 1.7 08/28/15 F SW8081Bug/Kg1.7 2NDg-Chlordane 4.3 08/28/15 F SW8081Bug/Kg4.3 2NDHeptachlor 8.6 08/28/15 F SW8081Bug/Kg8.6 2NDHeptachlor epoxide 8.6 08/28/15 F SW8081Bug/Kg8.6 2NDMethoxychlor 43 08/28/15 F SW8081Bug/Kg43 2NDToxaphene 170 08/28/15 F SW8081Bug/Kg170 2

QA/QC Surrogates96% DCBP 08/28/15 F 30 - 150 %% 285% TCMX 08/28/15 F 30 - 150 %% 2



14B8 (20-25)Phoenix I.D.: BJ81782



LOD/MDL Dilution

ND1,1-Dichloropropene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1ND1,2,3-Trichlorobenzene 6.2 08/29/15 JLI SW8260Cug/Kg1.2 1ND1,2,3-Trichloropropane 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1ND1,2,4-Trichlorobenzene 6.2 08/29/15 JLI SW8260Cug/Kg1.2 1ND1,2,4-Trimethylbenzene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1ND1,2-Dibromo-3-chloropropane 6.2 08/29/15 JLI SW8260Cug/Kg1.2 1ND1,2-Dibromoethane 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1ND1,2-Dichlorobenzene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1ND1,2-Dichloroethane 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1ND1,2-Dichloropropane 6.2 08/29/15 JLI SW8260Cug/Kg1.2 1ND1,3,5-Trimethylbenzene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1ND1,3-Dichlorobenzene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1ND1,3-Dichloropropane 6.2 08/29/15 JLI SW8260Cug/Kg1.2 1ND1,4-Dichlorobenzene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1ND2,2-Dichloropropane 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1ND2-Chlorotoluene 6.2 08/29/15 JLI SW8260Cug/Kg1.2 1ND2-Hexanone 31 08/29/15 JLI SW8260Cug/Kg6.2 1ND2-Isopropyltoluene 6.2 08/29/15 JLI SW8260Cug/Kg 10.62 1ND4-Chlorotoluene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1ND4-Methyl-2-pentanone 31 08/29/15 JLI SW8260Cug/Kg6.2 1NDAcetone 50 08/29/15 JLI SW8260Cug/Kg6.2 1NDAcrylonitrile 12 08/29/15 JLI SW8260Cug/Kg1.2 10.73Benzene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1JNDBromobenzene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1NDBromochloromethane 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1NDBromodichloromethane 6.2 08/29/15 JLI SW8260Cug/Kg1.2 1NDBromoform 6.2 08/29/15 JLI SW8260Cug/Kg1.2 1NDBromomethane 6.2 08/29/15 JLI SW8260Cug/Kg2.5 1NDCarbon Disulfide 6.2 08/29/15 JLI SW8260Cug/Kg1.2 1NDCarbon tetrachloride 6.2 08/29/15 JLI SW8260Cug/Kg1.2 1NDChlorobenzene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1NDChloroethane 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1NDChloroform 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1NDChloromethane 6.2 08/29/15 JLI SW8260Cug/Kg1.2 116cis-1,2-Dichloroethene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1NDcis-1,3-Dichloropropene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1NDDibromochloromethane 6.2 08/29/15 JLI SW8260Cug/Kg1.2 1NDDibromomethane 6.2 08/29/15 JLI SW8260Cug/Kg1.2 1NDDichlorodifluoromethane 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1NDEthylbenzene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1NDHexachlorobutadiene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1NDIsopropylbenzene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1NDm&p-Xylene 6.2 08/29/15 JLI SW8260Cug/Kg1.2 1NDMethyl Ethyl Ketone 37 08/29/15 JLI SW8260Cug/Kg6.2 1NDMethyl t-butyl ether (MTBE) 12 08/29/15 JLI SW8260Cug/Kg1.2 1NDMethylene chloride 6.2 08/29/15 JLI SW8260Cug/Kg6.2 1NDNaphthalene 6.2 08/29/15 JLI SW8260Cug/Kg1.2 1NDn-Butylbenzene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1NDn-Propylbenzene 6.2 08/29/15 JLI SW8260Cug/Kg1.1 1


14B8 (20-25)Phoenix I.D.: BJ81782



LOD/MDL Dilution

NDo-Xylene 6.2 08/29/15 JLI SW8260Cug/Kg1.2 1NDp-Isopropyltoluene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1NDsec-Butylbenzene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1NDStyrene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1NDtert-Butylbenzene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1NDTetrachloroethene 6.2 08/29/15 JLI SW8260Cug/Kg1.2 1NDTetrahydrofuran (THF) 12 08/29/15 JLI SW8260Cug/Kg 13.1 1NDToluene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 10.97trans-1,2-Dichloroethene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1JNDtrans-1,3-Dichloropropene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1NDtrans-1,4-dichloro-2-butene 12 08/29/15 JLI SW8260Cug/Kg3.1 12.0Trichloroethene 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1JNDTrichlorofluoromethane 6.2 08/29/15 JLI SW8260Cug/Kg1.2 1NDTrichlorotrifluoroethane 6.2 08/29/15 JLI SW8260Cug/Kg0.62 10.72Vinyl chloride 6.2 08/29/15 JLI SW8260Cug/Kg0.62 1J







14B8 (20-25)Phoenix I.D.: BJ81782



LOD/MDL Dilution

ND2-Methylnaphthalene 290 08/27/15 DD SW8270Dug/Kg130 1ND2-Methylphenol (o-cresol) 290 08/27/15 DD SW8270Dug/Kg200 1ND2-Nitroaniline 840 08/27/15 DD SW8270Dug/Kg420 1ND2-Nitrophenol 290 08/27/15 DD SW8270Dug/Kg270 1ND3&4-Methylphenol (m&p-cresol) 290 08/27/15 DD SW8270Dug/Kg 1170 1ND3,3'-Dichlorobenzidine 840 08/27/15 DD SW8270Dug/Kg200 1ND3-Nitroaniline 840 08/27/15 DD SW8270Dug/Kg840 1ND4,6-Dinitro-2-methylphenol 2100 08/27/15 DD SW8270Dug/Kg450 1ND4-Bromophenyl phenyl ether 290 08/27/15 DD SW8270Dug/Kg120 1ND4-Chloro-3-methylphenol 290 08/27/15 DD SW8270Dug/Kg150 1ND4-Chloroaniline 340 08/27/15 DD SW8270Dug/Kg200 1ND4-Chlorophenyl phenyl ether 290 08/27/15 DD SW8270Dug/Kg140 1ND4-Nitroaniline 840 08/27/15 DD SW8270Dug/Kg140 1ND4-Nitrophenol 420 08/27/15 DD SW8270Dug/Kg190 1NDAcenaphthene 290 08/27/15 DD SW8270Dug/Kg130 1NDAcenaphthylene 290 08/27/15 DD SW8270Dug/Kg120 1NDAcetophenone 290 08/27/15 DD SW8270Dug/Kg130 1NDAniline 340 08/27/15 DD SW8270Dug/Kg340 1NDAnthracene 290 08/27/15 DD SW8270Dug/Kg140 1NDBenz(a)anthracene 290 08/27/15 DD SW8270Dug/Kg140 1NDBenzidine 840 08/27/15 DD SW8270Dug/Kg250 1NDBenzo(a)pyrene 290 08/27/15 DD SW8270Dug/Kg140 1NDBenzo(b)fluoranthene 290 08/27/15 DD SW8270Dug/Kg140 1NDBenzo(ghi)perylene 290 08/27/15 DD SW8270Dug/Kg140 1NDBenzo(k)fluoranthene 290 08/27/15 DD SW8270Dug/Kg140 1NDBenzoic acid 2100 08/27/15 DD SW8270Dug/Kg 1840 1NDBenzyl butyl phthalate 290 08/27/15 DD SW8270Dug/Kg110 1NDBis(2-chloroethoxy)methane 290 08/27/15 DD SW8270Dug/Kg120 1NDBis(2-chloroethyl)ether 290 08/27/15 DD SW8270Dug/Kg110 1NDBis(2-chloroisopropyl)ether 290 08/27/15 DD SW8270Dug/Kg 1120 1NDBis(2-ethylhexyl)phthalate 290 08/27/15 DD SW8270Dug/Kg120 1NDCarbazole 2100 08/27/15 DD SW8270Dug/Kg320 1NDChrysene 290 08/27/15 DD SW8270Dug/Kg140 1NDDibenz(a,h)anthracene 290 08/27/15 DD SW8270Dug/Kg140 1NDDibenzofuran 290 08/27/15 DD SW8270Dug/Kg120 1NDDiethyl phthalate 290 08/27/15 DD SW8270Dug/Kg130 1NDDimethylphthalate 290 08/27/15 DD SW8270Dug/Kg130 1NDDi-n-butylphthalate 290 08/27/15 DD SW8270Dug/Kg110 1NDDi-n-octylphthalate 290 08/27/15 DD SW8270Dug/Kg110 1NDFluoranthene 290 08/27/15 DD SW8270Dug/Kg140 1NDFluorene 290 08/27/15 DD SW8270Dug/Kg140 1NDHexachlorobenzene 290 08/27/15 DD SW8270Dug/Kg120 1NDHexachlorobutadiene 290 08/27/15 DD SW8270Dug/Kg150 1NDHexachlorocyclopentadiene 290 08/27/15 DD SW8270Dug/Kg130 1NDHexachloroethane 290 08/27/15 DD SW8270Dug/Kg130 1NDIndeno(1,2,3-cd)pyrene 290 08/27/15 DD SW8270Dug/Kg140 1NDIsophorone 290 08/27/15 DD SW8270Dug/Kg120 1NDNaphthalene 290 08/27/15 DD SW8270Dug/Kg120 1NDNitrobenzene 290 08/27/15 DD SW8270Dug/Kg150 1


14B8 (20-25)Phoenix I.D.: BJ81782



LOD/MDL Dilution

NDN-Nitrosodimethylamine 290 08/27/15 DD SW8270Dug/Kg120 1NDN-Nitrosodi-n-propylamine 290 08/27/15 DD SW8270Dug/Kg140 1NDN-Nitrosodiphenylamine 290 08/27/15 DD SW8270Dug/Kg160 1NDPentachloronitrobenzene 290 08/27/15 DD SW8270Dug/Kg160 1NDPentachlorophenol 290 08/27/15 DD SW8270Dug/Kg160 1NDPhenanthrene 290 08/27/15 DD SW8270Dug/Kg120 1NDPhenol 290 08/27/15 DD SW8270Dug/Kg130 1NDPyrene 290 08/27/15 DD SW8270Dug/Kg140 1NDPyridine 290 08/27/15 DD SW8270Dug/Kg100 1


Comments:












SOLIDEBC72 Hour


RB

Laboratory Data

14B7 (0-5)

Phoenix ID: BJ81783

08/26/159:00

17:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution


55.5Barium 0.8 08/28/15 LK SW6010Cmg/Kg0.42 10.32Beryllium 0.33 08/28/15 LK SW6010Cmg/Kg0.17 1B5910Calcium 4.2 08/28/15 LK SW6010Cmg/Kg3.8 1


12500Iron 42 08/28/15 LK SW6010Cmg/Kg B42 100.07Mercury 0.03 08/27/15 RS SW7471Bmg/Kg0.02 1984Potassium 8 08/28/15 LK SW6010Cmg/Kg3.2 1N

3000Magnesium 4.2 08/28/15 LK SW6010Cmg/Kg4.2 1230Manganese 4.2 08/28/15 LK SW6010Cmg/Kg4.2 10176Sodium 8 08/28/15 LK SW6010Cmg/Kg3.6 1N13.2Nickel 0.42 08/28/15 LK SW6010Cmg/Kg0.42 147.2Lead 0.8 08/28/15 LK SW6010Cmg/Kg0.42 1< 2.1Antimony 2.1 08/28/15 LK SW6010Cmg/Kg2.1 1N< 1.7Selenium 1.7 08/28/15 LK SW6010Cmg/Kg1.4 1< 1.7Thallium 1.7 08/28/15 LK SW6010Cmg/Kg1.7 126.5Vanadium 0.4 08/28/15 LK SW6010Cmg/Kg0.42 152.1Zinc 0.8 08/28/15 LK SW6010Cmg/Kg B0.42 180Percent Solid 08/26/15 I SW846-%Solid%



14B7 (0-5)Phoenix I.D.: BJ81783



LOD/MDL Dilution




Pesticides - SoilND4,4' -DDD 10 08/28/15 CE SW8081Bug/Kg10 10ND4,4' -DDE 10 08/28/15 CE SW8081Bug/Kg10 10ND4,4' -DDT 10 08/28/15 CE SW8081Bug/Kg10 10NDa-BHC 21 08/28/15 CE SW8081Bug/Kg21 1056a-Chlordane 21 08/28/15 CE SW8081Bug/Kg21 10NDAldrin 6.2 08/28/15 CE SW8081Bug/Kg6.2 10NDb-BHC 21 08/28/15 CE SW8081Bug/Kg21 10NDd-BHC 21 08/28/15 CE SW8081Bug/Kg21 1013Dieldrin 6.2 08/28/15 CE SW8081Bug/Kg6.2 10NDEndosulfan I 41 08/28/15 CE SW8081Bug/Kg41 10NDEndosulfan II 41 08/28/15 CE SW8081Bug/Kg41 10NDEndosulfan sulfate 41 08/28/15 CE SW8081Bug/Kg41 10NDEndrin 21 08/28/15 CE SW8081Bug/Kg21 10NDEndrin aldehyde 50 08/28/15 CE SW8081Bug/Kg50 10NDEndrin ketone 41 08/28/15 CE SW8081Bug/Kg41 10NDg-BHC 8.2 08/28/15 CE SW8081Bug/Kg8.2 1066g-Chlordane 21 08/28/15 CE SW8081Bug/Kg21 10NDHeptachlor 41 08/28/15 CE SW8081Bug/Kg41 10NDHeptachlor epoxide 41 08/28/15 CE SW8081Bug/Kg41 10NDMethoxychlor 210 08/28/15 CE SW8081Bug/Kg210 10NDToxaphene 820 08/28/15 CE SW8081Bug/Kg820 10

QA/QC Surrogates93% DCBP 08/28/15 CE 30 - 150 %% 1087% TCMX 08/28/15 CE 30 - 150 %% 10



14B7 (0-5)Phoenix I.D.: BJ81783



LOD/MDL Dilution

ND1,1-Dichloropropene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND1,2,3-Trichlorobenzene 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1ND1,2,3-Trichloropropane 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND1,2,4-Trichlorobenzene 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1ND1,2,4-Trimethylbenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND1,2-Dibromo-3-chloropropane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1ND1,2-Dibromoethane 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND1,2-Dichlorobenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND1,2-Dichloroethane 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND1,2-Dichloropropane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1ND1,3,5-Trimethylbenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND1,3-Dichlorobenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND1,3-Dichloropropane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1ND1,4-Dichlorobenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND2,2-Dichloropropane 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND2-Chlorotoluene 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1ND2-Hexanone 27 08/29/15 JLI SW8260Cug/Kg5.3 1ND2-Isopropyltoluene 5.3 08/29/15 JLI SW8260Cug/Kg 10.53 1ND4-Chlorotoluene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1ND4-Methyl-2-pentanone 27 08/29/15 JLI SW8260Cug/Kg5.3 112Acetone 50 08/29/15 JLI SW8260Cug/Kg5.3 1JSNDAcrylonitrile 11 08/29/15 JLI SW8260Cug/Kg1.1 10.77Benzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1JNDBromobenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDBromochloromethane 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDBromodichloromethane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1NDBromoform 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1NDBromomethane 5.3 08/29/15 JLI SW8260Cug/Kg2.1 11.1Carbon Disulfide 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1JNDCarbon tetrachloride 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1NDChlorobenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDChloroethane 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDChloroform 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDChloromethane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 13.1cis-1,2-Dichloroethene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1JNDcis-1,3-Dichloropropene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDDibromochloromethane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1NDDibromomethane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1NDDichlorodifluoromethane 5.3 08/29/15 JLI SW8260Cug/Kg0.53 11.9Ethylbenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1JNDHexachlorobutadiene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDIsopropylbenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 17.5m&p-Xylene 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1NDMethyl Ethyl Ketone 32 08/29/15 JLI SW8260Cug/Kg5.3 1NDMethyl t-butyl ether (MTBE) 11 08/29/15 JLI SW8260Cug/Kg1.1 1NDMethylene chloride 5.3 08/29/15 JLI SW8260Cug/Kg5.3 1260Naphthalene 400 08/29/15 JLI SW8260Cug/Kg79 50JNDn-Butylbenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDn-Propylbenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.96 1


14B7 (0-5)Phoenix I.D.: BJ81783



LOD/MDL Dilution

2.5o-Xylene 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1JNDp-Isopropyltoluene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDsec-Butylbenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDStyrene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDtert-Butylbenzene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDTetrachloroethene 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1NDTetrahydrofuran (THF) 11 08/29/15 JLI SW8260Cug/Kg 12.7 1110Toluene 400 08/29/15 JLI SW8260Cug/Kg40 50JNDtrans-1,2-Dichloroethene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDtrans-1,3-Dichloropropene 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDtrans-1,4-dichloro-2-butene 11 08/29/15 JLI SW8260Cug/Kg2.7 1100Trichloroethene 400 08/29/15 JLI SW8260Cug/Kg40 50JNDTrichlorofluoromethane 5.3 08/29/15 JLI SW8260Cug/Kg1.1 1NDTrichlorotrifluoroethane 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1NDVinyl chloride 5.3 08/29/15 JLI SW8260Cug/Kg0.53 1







14B7 (0-5)Phoenix I.D.: BJ81783



LOD/MDL Dilution

ND2-Methylnaphthalene 290 08/27/15 DD SW8270Dug/Kg120 1ND2-Methylphenol (o-cresol) 290 08/27/15 DD SW8270Dug/Kg190 1ND2-Nitroaniline 820 08/27/15 DD SW8270Dug/Kg410 1ND2-Nitrophenol 290 08/27/15 DD SW8270Dug/Kg260 1ND3&4-Methylphenol (m&p-cresol) 290 08/27/15 DD SW8270Dug/Kg 1160 1ND3,3'-Dichlorobenzidine 820 08/27/15 DD SW8270Dug/Kg190 1ND3-Nitroaniline 820 08/27/15 DD SW8270Dug/Kg820 1ND4,6-Dinitro-2-methylphenol 2000 08/27/15 DD SW8270Dug/Kg440 1ND4-Bromophenyl phenyl ether 290 08/27/15 DD SW8270Dug/Kg120 1ND4-Chloro-3-methylphenol 290 08/27/15 DD SW8270Dug/Kg140 1ND4-Chloroaniline 330 08/27/15 DD SW8270Dug/Kg190 1ND4-Chlorophenyl phenyl ether 290 08/27/15 DD SW8270Dug/Kg140 1ND4-Nitroaniline 820 08/27/15 DD SW8270Dug/Kg140 1ND4-Nitrophenol 410 08/27/15 DD SW8270Dug/Kg190 1NDAcenaphthene 290 08/27/15 DD SW8270Dug/Kg120 1NDAcenaphthylene 290 08/27/15 DD SW8270Dug/Kg110 1NDAcetophenone 290 08/27/15 DD SW8270Dug/Kg130 1NDAniline 330 08/27/15 DD SW8270Dug/Kg330 1260Anthracene 290 08/27/15 DD SW8270Dug/Kg130 1J

1200Benz(a)anthracene 290 08/27/15 DD SW8270Dug/Kg140 1NDBenzidine 820 08/27/15 DD SW8270Dug/Kg240 1940Benzo(a)pyrene 290 08/27/15 DD SW8270Dug/Kg130 1

1100Benzo(b)fluoranthene 290 08/27/15 DD SW8270Dug/Kg140 1640Benzo(ghi)perylene 290 08/27/15 DD SW8270Dug/Kg130 1960Benzo(k)fluoranthene 290 08/27/15 DD SW8270Dug/Kg140 1NDBenzoic acid 2000 08/27/15 DD SW8270Dug/Kg 1820 1NDBenzyl butyl phthalate 290 08/27/15 DD SW8270Dug/Kg110 1NDBis(2-chloroethoxy)methane 290 08/27/15 DD SW8270Dug/Kg110 1NDBis(2-chloroethyl)ether 290 08/27/15 DD SW8270Dug/Kg110 1NDBis(2-chloroisopropyl)ether 290 08/27/15 DD SW8270Dug/Kg 1110 1NDBis(2-ethylhexyl)phthalate 290 08/27/15 DD SW8270Dug/Kg120 1NDCarbazole 2000 08/27/15 DD SW8270Dug/Kg310 1

1400Chrysene 290 08/27/15 DD SW8270Dug/Kg140 1160Dibenz(a,h)anthracene 290 08/27/15 DD SW8270Dug/Kg130 1JNDDibenzofuran 290 08/27/15 DD SW8270Dug/Kg120 1NDDiethyl phthalate 290 08/27/15 DD SW8270Dug/Kg130 1NDDimethylphthalate 290 08/27/15 DD SW8270Dug/Kg130 1NDDi-n-butylphthalate 290 08/27/15 DD SW8270Dug/Kg110 1NDDi-n-octylphthalate 290 08/27/15 DD SW8270Dug/Kg110 1



14B7 (0-5)Phoenix I.D.: BJ81783



LOD/MDL Dilution

NDN-Nitrosodimethylamine 290 08/27/15 DD SW8270Dug/Kg120 1NDN-Nitrosodi-n-propylamine 290 08/27/15 DD SW8270Dug/Kg130 1NDN-Nitrosodiphenylamine 290 08/27/15 DD SW8270Dug/Kg160 1NDPentachloronitrobenzene 290 08/27/15 DD SW8270Dug/Kg150 1NDPentachlorophenol 290 08/27/15 DD SW8270Dug/Kg150 1

1700Phenanthrene 290 08/27/15 DD SW8270Dug/Kg120 1NDPhenol 290 08/27/15 DD SW8270Dug/Kg130 1



Comments:














SOLIDEBC72 Hour


RB

Laboratory Data

14B7 (10-15)

Phoenix ID: BJ81784

08/26/159:15

17:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution




14B7 (10-15)Phoenix I.D.: BJ81784



LOD/MDL Dilution

ND2-Isopropyltoluene 6.0 08/29/15 JLI SW8260Cug/Kg 10.60 1ND4-Chlorotoluene 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1ND4-Methyl-2-pentanone 30 08/29/15 JLI SW8260Cug/Kg6.0 1NDAcetone 50 08/29/15 JLI SW8260Cug/Kg6.0 1NDAcrylonitrile 12 08/29/15 JLI SW8260Cug/Kg1.2 1NDBenzene 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDBromobenzene 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDBromochloromethane 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDBromodichloromethane 6.0 08/29/15 JLI SW8260Cug/Kg1.2 1NDBromoform 6.0 08/29/15 JLI SW8260Cug/Kg1.2 1NDBromomethane 6.0 08/29/15 JLI SW8260Cug/Kg2.4 1NDCarbon Disulfide 6.0 08/29/15 JLI SW8260Cug/Kg1.2 1NDCarbon tetrachloride 6.0 08/29/15 JLI SW8260Cug/Kg1.2 1NDChlorobenzene 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDChloroethane 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDChloroform 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDChloromethane 6.0 08/29/15 JLI SW8260Cug/Kg1.2 12.5cis-1,2-Dichloroethene 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1JNDcis-1,3-Dichloropropene 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDDibromochloromethane 6.0 08/29/15 JLI SW8260Cug/Kg1.2 1NDDibromomethane 6.0 08/29/15 JLI SW8260Cug/Kg1.2 1NDDichlorodifluoromethane 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDEthylbenzene 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDHexachlorobutadiene 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDIsopropylbenzene 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDm&p-Xylene 6.0 08/29/15 JLI SW8260Cug/Kg1.2 1NDMethyl Ethyl Ketone 36 08/29/15 JLI SW8260Cug/Kg6.0 1NDMethyl t-butyl ether (MTBE) 12 08/29/15 JLI SW8260Cug/Kg1.2 1NDMethylene chloride 6.0 08/29/15 JLI SW8260Cug/Kg6.0 1NDNaphthalene 6.0 08/29/15 JLI SW8260Cug/Kg1.2 1NDn-Butylbenzene 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDn-Propylbenzene 6.0 08/29/15 JLI SW8260Cug/Kg1.1 1NDo-Xylene 6.0 08/29/15 JLI SW8260Cug/Kg1.2 1NDp-Isopropyltoluene 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDsec-Butylbenzene 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDStyrene 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDtert-Butylbenzene 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDTetrachloroethene 6.0 08/29/15 JLI SW8260Cug/Kg1.2 1NDTetrahydrofuran (THF) 12 08/29/15 JLI SW8260Cug/Kg 13.0 1NDToluene 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDtrans-1,2-Dichloroethene 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDtrans-1,3-Dichloropropene 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDtrans-1,4-dichloro-2-butene 12 08/29/15 JLI SW8260Cug/Kg3.0 12.3Trichloroethene 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1JNDTrichlorofluoromethane 6.0 08/29/15 JLI SW8260Cug/Kg1.2 1NDTrichlorotrifluoroethane 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1NDVinyl chloride 6.0 08/29/15 JLI SW8260Cug/Kg0.60 1



14B7 (10-15)Phoenix I.D.: BJ81784



LOD/MDL Dilution







14B7 (10-15)Phoenix I.D.: BJ81784



LOD/MDL Dilution

NDAniline 290 08/27/15 DD SW8270Dug/Kg290 1NDAnthracene 260 08/27/15 DD SW8270Dug/Kg120 1NDBenz(a)anthracene 260 08/27/15 DD SW8270Dug/Kg120 1NDBenzidine 730 08/27/15 DD SW8270Dug/Kg220 1NDBenzo(a)pyrene 260 08/27/15 DD SW8270Dug/Kg120 1NDBenzo(b)fluoranthene 260 08/27/15 DD SW8270Dug/Kg130 1NDBenzo(ghi)perylene 260 08/27/15 DD SW8270Dug/Kg120 1NDBenzo(k)fluoranthene 260 08/27/15 DD SW8270Dug/Kg120 1NDBenzoic acid 1800 08/27/15 DD SW8270Dug/Kg 1730 1NDBenzyl butyl phthalate 260 08/27/15 DD SW8270Dug/Kg95 1NDBis(2-chloroethoxy)methane 260 08/27/15 DD SW8270Dug/Kg100 1NDBis(2-chloroethyl)ether 260 08/27/15 DD SW8270Dug/Kg99 1NDBis(2-chloroisopropyl)ether 260 08/27/15 DD SW8270Dug/Kg 1100 1NDBis(2-ethylhexyl)phthalate 260 08/27/15 DD SW8270Dug/Kg110 1NDCarbazole 1800 08/27/15 DD SW8270Dug/Kg280 1NDChrysene 260 08/27/15 DD SW8270Dug/Kg120 1NDDibenz(a,h)anthracene 260 08/27/15 DD SW8270Dug/Kg120 1NDDibenzofuran 260 08/27/15 DD SW8270Dug/Kg110 1NDDiethyl phthalate 260 08/27/15 DD SW8270Dug/Kg120 1NDDimethylphthalate 260 08/27/15 DD SW8270Dug/Kg110 1NDDi-n-butylphthalate 260 08/27/15 DD SW8270Dug/Kg98 1NDDi-n-octylphthalate 260 08/27/15 DD SW8270Dug/Kg95 1NDFluoranthene 260 08/27/15 DD SW8270Dug/Kg120 1NDFluorene 260 08/27/15 DD SW8270Dug/Kg120 1NDHexachlorobenzene 260 08/27/15 DD SW8270Dug/Kg110 1NDHexachlorobutadiene 260 08/27/15 DD SW8270Dug/Kg130 1NDHexachlorocyclopentadiene 260 08/27/15 DD SW8270Dug/Kg110 1NDHexachloroethane 260 08/27/15 DD SW8270Dug/Kg110 1NDIndeno(1,2,3-cd)pyrene 260 08/27/15 DD SW8270Dug/Kg120 1NDIsophorone 260 08/27/15 DD SW8270Dug/Kg100 1NDNaphthalene 260 08/27/15 DD SW8270Dug/Kg110 1NDNitrobenzene 260 08/27/15 DD SW8270Dug/Kg130 1NDN-Nitrosodimethylamine 260 08/27/15 DD SW8270Dug/Kg100 1NDN-Nitrosodi-n-propylamine 260 08/27/15 DD SW8270Dug/Kg120 1NDN-Nitrosodiphenylamine 260 08/27/15 DD SW8270Dug/Kg140 1NDPentachloronitrobenzene 260 08/27/15 DD SW8270Dug/Kg140 1NDPentachlorophenol 260 08/27/15 DD SW8270Dug/Kg140 1NDPhenanthrene 260 08/27/15 DD SW8270Dug/Kg110 1NDPhenol 260 08/27/15 DD SW8270Dug/Kg120 1NDPyrene 260 08/27/15 DD SW8270Dug/Kg130 1NDPyridine 260 08/27/15 DD SW8270Dug/Kg90 1



14B7 (10-15)Phoenix I.D.: BJ81784



LOD/MDL Dilution

Comments:











SOLIDEBC72 Hour


RB

Laboratory Data

14B7 (15-20)

Phoenix ID: BJ81785

08/26/159:30

17:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution








14B7 (15-20)Phoenix I.D.: BJ81785



LOD/MDL Dilution




Pesticides - SoilND4,4' -DDD 2.4 08/28/15 CE SW8081Bug/Kg2.4 2ND4,4' -DDE 2.4 08/28/15 CE SW8081Bug/Kg2.4 2ND4,4' -DDT 2.4 08/28/15 CE SW8081Bug/Kg2.4 2NDa-BHC 8.0 08/28/15 CE SW8081Bug/Kg8.0 2NDa-Chlordane 4.0 08/28/15 CE SW8081Bug/Kg4.0 2NDAldrin 4.0 08/28/15 CE SW8081Bug/Kg4.0 2NDb-BHC 8.0 08/28/15 CE SW8081Bug/Kg8.0 2NDd-BHC 8.0 08/28/15 CE SW8081Bug/Kg8.0 2NDDieldrin 4.0 08/28/15 CE SW8081Bug/Kg4.0 2NDEndosulfan I 8.0 08/28/15 CE SW8081Bug/Kg8.0 2NDEndosulfan II 8.0 08/28/15 CE SW8081Bug/Kg8.0 2NDEndosulfan sulfate 8.0 08/28/15 CE SW8081Bug/Kg8.0 2NDEndrin 8.0 08/28/15 CE SW8081Bug/Kg8.0 2NDEndrin aldehyde 8.0 08/28/15 CE SW8081Bug/Kg8.0 2NDEndrin ketone 8.0 08/28/15 CE SW8081Bug/Kg8.0 2NDg-BHC 1.6 08/28/15 CE SW8081Bug/Kg1.6 2NDg-Chlordane 4.0 08/28/15 CE SW8081Bug/Kg4.0 2NDHeptachlor 8.0 08/28/15 CE SW8081Bug/Kg8.0 2NDHeptachlor epoxide 8.0 08/28/15 CE SW8081Bug/Kg8.0 2NDMethoxychlor 40 08/28/15 CE SW8081Bug/Kg40 2NDToxaphene 160 08/28/15 CE SW8081Bug/Kg160 2




14B7 (15-20)Phoenix I.D.: BJ81785



LOD/MDL Dilution

ND1,1-Dichloropropene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1ND1,2,3-Trichlorobenzene 4.5 08/29/15 JLI SW8260Cug/Kg0.90 1ND1,2,3-Trichloropropane 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1ND1,2,4-Trichlorobenzene 4.5 08/29/15 JLI SW8260Cug/Kg0.90 1ND1,2,4-Trimethylbenzene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1ND1,2-Dibromo-3-chloropropane 4.5 08/29/15 JLI SW8260Cug/Kg0.90 1ND1,2-Dibromoethane 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1ND1,2-Dichlorobenzene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1ND1,2-Dichloroethane 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1ND1,2-Dichloropropane 4.5 08/29/15 JLI SW8260Cug/Kg0.90 1ND1,3,5-Trimethylbenzene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1ND1,3-Dichlorobenzene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1ND1,3-Dichloropropane 4.5 08/29/15 JLI SW8260Cug/Kg0.90 1ND1,4-Dichlorobenzene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1ND2,2-Dichloropropane 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1ND2-Chlorotoluene 4.5 08/29/15 JLI SW8260Cug/Kg0.90 1ND2-Hexanone 23 08/29/15 JLI SW8260Cug/Kg4.5 1ND2-Isopropyltoluene 4.5 08/29/15 JLI SW8260Cug/Kg 10.45 1ND4-Chlorotoluene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1ND4-Methyl-2-pentanone 23 08/29/15 JLI SW8260Cug/Kg4.5 1NDAcetone 45 08/29/15 JLI SW8260Cug/Kg4.5 1NDAcrylonitrile 9.0 08/29/15 JLI SW8260Cug/Kg0.90 1NDBenzene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDBromobenzene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDBromochloromethane 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDBromodichloromethane 4.5 08/29/15 JLI SW8260Cug/Kg0.90 1NDBromoform 4.5 08/29/15 JLI SW8260Cug/Kg0.90 1NDBromomethane 4.5 08/29/15 JLI SW8260Cug/Kg1.8 1NDCarbon Disulfide 4.5 08/29/15 JLI SW8260Cug/Kg0.90 1NDCarbon tetrachloride 4.5 08/29/15 JLI SW8260Cug/Kg0.90 1NDChlorobenzene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDChloroethane 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDChloroform 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDChloromethane 4.5 08/29/15 JLI SW8260Cug/Kg0.90 137cis-1,2-Dichloroethene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDcis-1,3-Dichloropropene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDDibromochloromethane 4.5 08/29/15 JLI SW8260Cug/Kg0.90 1NDDibromomethane 4.5 08/29/15 JLI SW8260Cug/Kg0.90 1NDDichlorodifluoromethane 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDEthylbenzene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDHexachlorobutadiene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDIsopropylbenzene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDm&p-Xylene 4.5 08/29/15 JLI SW8260Cug/Kg0.90 1NDMethyl Ethyl Ketone 27 08/29/15 JLI SW8260Cug/Kg4.5 1NDMethyl t-butyl ether (MTBE) 9.0 08/29/15 JLI SW8260Cug/Kg0.90 1NDMethylene chloride 4.5 08/29/15 JLI SW8260Cug/Kg4.5 1NDNaphthalene 4.5 08/29/15 JLI SW8260Cug/Kg0.90 1NDn-Butylbenzene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDn-Propylbenzene 4.5 08/29/15 JLI SW8260Cug/Kg0.81 1


14B7 (15-20)Phoenix I.D.: BJ81785



LOD/MDL Dilution

NDo-Xylene 4.5 08/29/15 JLI SW8260Cug/Kg0.90 1NDp-Isopropyltoluene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDsec-Butylbenzene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDStyrene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDtert-Butylbenzene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDTetrachloroethene 4.5 08/29/15 JLI SW8260Cug/Kg0.90 1NDTetrahydrofuran (THF) 9.0 08/29/15 JLI SW8260Cug/Kg 12.3 1NDToluene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDtrans-1,2-Dichloroethene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDtrans-1,3-Dichloropropene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDtrans-1,4-dichloro-2-butene 9.0 08/29/15 JLI SW8260Cug/Kg2.3 123Trichloroethene 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDTrichlorofluoromethane 4.5 08/29/15 JLI SW8260Cug/Kg0.90 1NDTrichlorotrifluoroethane 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1NDVinyl chloride 4.5 08/29/15 JLI SW8260Cug/Kg0.45 1







14B7 (15-20)Phoenix I.D.: BJ81785



LOD/MDL Dilution

ND2-Methylnaphthalene 280 08/27/15 DD SW8270Dug/Kg120 1ND2-Methylphenol (o-cresol) 280 08/27/15 DD SW8270Dug/Kg190 1ND2-Nitroaniline 810 08/27/15 DD SW8270Dug/Kg410 1ND2-Nitrophenol 280 08/27/15 DD SW8270Dug/Kg260 1ND3&4-Methylphenol (m&p-cresol) 280 08/27/15 DD SW8270Dug/Kg 1160 1ND3,3'-Dichlorobenzidine 810 08/27/15 DD SW8270Dug/Kg190 1ND3-Nitroaniline 810 08/27/15 DD SW8270Dug/Kg810 1ND4,6-Dinitro-2-methylphenol 2000 08/27/15 DD SW8270Dug/Kg440 1ND4-Bromophenyl phenyl ether 280 08/27/15 DD SW8270Dug/Kg120 1ND4-Chloro-3-methylphenol 280 08/27/15 DD SW8270Dug/Kg140 1ND4-Chloroaniline 320 08/27/15 DD SW8270Dug/Kg190 1ND4-Chlorophenyl phenyl ether 280 08/27/15 DD SW8270Dug/Kg140 1ND4-Nitroaniline 810 08/27/15 DD SW8270Dug/Kg140 1ND4-Nitrophenol 410 08/27/15 DD SW8270Dug/Kg180 1NDAcenaphthene 280 08/27/15 DD SW8270Dug/Kg120 1NDAcenaphthylene 280 08/27/15 DD SW8270Dug/Kg110 1NDAcetophenone 280 08/27/15 DD SW8270Dug/Kg130 1NDAniline 320 08/27/15 DD SW8270Dug/Kg320 1NDAnthracene 280 08/27/15 DD SW8270Dug/Kg130 1140Benz(a)anthracene 280 08/27/15 DD SW8270Dug/Kg140 1JNDBenzidine 810 08/27/15 DD SW8270Dug/Kg240 1920Benzo(a)pyrene 280 08/27/15 DD SW8270Dug/Kg130 1560Benzo(b)fluoranthene 280 08/27/15 DD SW8270Dug/Kg140 1340Benzo(ghi)perylene 280 08/27/15 DD SW8270Dug/Kg130 1680Benzo(k)fluoranthene 280 08/27/15 DD SW8270Dug/Kg130 1NDBenzoic acid 2000 08/27/15 DD SW8270Dug/Kg 1810 1NDBenzyl butyl phthalate 280 08/27/15 DD SW8270Dug/Kg100 1NDBis(2-chloroethoxy)methane 280 08/27/15 DD SW8270Dug/Kg110 1NDBis(2-chloroethyl)ether 280 08/27/15 DD SW8270Dug/Kg110 1NDBis(2-chloroisopropyl)ether 280 08/27/15 DD SW8270Dug/Kg 1110 1NDBis(2-ethylhexyl)phthalate 280 08/27/15 DD SW8270Dug/Kg120 1NDCarbazole 2000 08/27/15 DD SW8270Dug/Kg310 1150Chrysene 280 08/27/15 DD SW8270Dug/Kg140 1JNDDibenz(a,h)anthracene 280 08/27/15 DD SW8270Dug/Kg130 1NDDibenzofuran 280 08/27/15 DD SW8270Dug/Kg120 1NDDiethyl phthalate 280 08/27/15 DD SW8270Dug/Kg130 1NDDimethylphthalate 280 08/27/15 DD SW8270Dug/Kg130 1NDDi-n-butylphthalate 280 08/27/15 DD SW8270Dug/Kg110 1NDDi-n-octylphthalate 280 08/27/15 DD SW8270Dug/Kg100 1NDFluoranthene 280 08/27/15 DD SW8270Dug/Kg130 1NDFluorene 280 08/27/15 DD SW8270Dug/Kg130 1NDHexachlorobenzene 280 08/27/15 DD SW8270Dug/Kg120 1NDHexachlorobutadiene 280 08/27/15 DD SW8270Dug/Kg150 1NDHexachlorocyclopentadiene 280 08/27/15 DD SW8270Dug/Kg120 1NDHexachloroethane 280 08/27/15 DD SW8270Dug/Kg120 1410Indeno(1,2,3-cd)pyrene 280 08/27/15 DD SW8270Dug/Kg130 1NDIsophorone 280 08/27/15 DD SW8270Dug/Kg110 1NDNaphthalene 280 08/27/15 DD SW8270Dug/Kg120 1NDNitrobenzene 280 08/27/15 DD SW8270Dug/Kg140 1


14B7 (15-20)Phoenix I.D.: BJ81785



LOD/MDL Dilution



Comments:












SOLIDEBC72 Hour


RB

Laboratory Data

14B2 (0-5)

Phoenix ID: BJ81786

08/26/1510:0017:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution







14B2 (0-5)Phoenix I.D.: BJ81786



LOD/MDL Dilution




Pesticides - SoilND4,4' -DDD 5.0 08/28/15 CE SW8081Bug/Kg5.0 28.14,4' -DDE 2.2 08/28/15 CE SW8081Bug/Kg2.2 27.14,4' -DDT 2.2 08/28/15 CE SW8081Bug/Kg2.2 2NDa-BHC 7.4 08/28/15 CE SW8081Bug/Kg7.4 2110a-Chlordane 3.7 08/28/15 CE SW8081Bug/Kg3.7 2NDAldrin 3.7 08/28/15 CE SW8081Bug/Kg3.7 2NDb-BHC 7.4 08/28/15 CE SW8081Bug/Kg7.4 2NDd-BHC 7.4 08/28/15 CE SW8081Bug/Kg7.4 29.4Dieldrin 3.7 08/28/15 CE SW8081Bug/Kg3.7 2NDEndosulfan I 7.4 08/28/15 CE SW8081Bug/Kg7.4 2NDEndosulfan II 7.4 08/28/15 CE SW8081Bug/Kg7.4 2NDEndosulfan sulfate 7.4 08/28/15 CE SW8081Bug/Kg7.4 2NDEndrin 7.4 08/28/15 CE SW8081Bug/Kg7.4 2NDEndrin aldehyde 7.4 08/28/15 CE SW8081Bug/Kg7.4 2NDEndrin ketone 7.4 08/28/15 CE SW8081Bug/Kg7.4 2NDg-BHC 2.0 08/28/15 CE SW8081Bug/Kg2.0 2130g-Chlordane 3.7 08/28/15 CE SW8081Bug/Kg3.7 2NDHeptachlor 7.4 08/28/15 CE SW8081Bug/Kg7.4 2NDHeptachlor epoxide 7.4 08/28/15 CE SW8081Bug/Kg7.4 2NDMethoxychlor 37 08/28/15 CE SW8081Bug/Kg37 2NDToxaphene 150 08/28/15 CE SW8081Bug/Kg150 2




14B2 (0-5)Phoenix I.D.: BJ81786



LOD/MDL Dilution

ND1,1-Dichloropropene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1ND1,2,3-Trichlorobenzene 4.1 08/29/15 JLI SW8260Cug/Kg0.81 1ND1,2,3-Trichloropropane 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1ND1,2,4-Trichlorobenzene 4.1 08/29/15 JLI SW8260Cug/Kg0.81 10.431,2,4-Trimethylbenzene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1JND1,2-Dibromo-3-chloropropane 4.1 08/29/15 JLI SW8260Cug/Kg0.81 1ND1,2-Dibromoethane 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1ND1,2-Dichlorobenzene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1ND1,2-Dichloroethane 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1ND1,2-Dichloropropane 4.1 08/29/15 JLI SW8260Cug/Kg0.81 11.11,3,5-Trimethylbenzene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1JND1,3-Dichlorobenzene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1ND1,3-Dichloropropane 4.1 08/29/15 JLI SW8260Cug/Kg0.81 1ND1,4-Dichlorobenzene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1ND2,2-Dichloropropane 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1ND2-Chlorotoluene 4.1 08/29/15 JLI SW8260Cug/Kg0.81 1ND2-Hexanone 20 08/29/15 JLI SW8260Cug/Kg4.1 1ND2-Isopropyltoluene 4.1 08/29/15 JLI SW8260Cug/Kg 10.41 1ND4-Chlorotoluene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1ND4-Methyl-2-pentanone 20 08/29/15 JLI SW8260Cug/Kg4.1 16.9Acetone 41 08/29/15 JLI SW8260Cug/Kg4.1 1JSNDAcrylonitrile 8.1 08/29/15 JLI SW8260Cug/Kg0.81 10.42Benzene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1JNDBromobenzene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1NDBromochloromethane 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1NDBromodichloromethane 4.1 08/29/15 JLI SW8260Cug/Kg0.81 1NDBromoform 4.1 08/29/15 JLI SW8260Cug/Kg0.81 1NDBromomethane 4.1 08/29/15 JLI SW8260Cug/Kg1.6 1NDCarbon Disulfide 4.1 08/29/15 JLI SW8260Cug/Kg0.81 1NDCarbon tetrachloride 4.1 08/29/15 JLI SW8260Cug/Kg0.81 1NDChlorobenzene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1NDChloroethane 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1NDChloroform 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1NDChloromethane 4.1 08/29/15 JLI SW8260Cug/Kg0.81 15.2cis-1,2-Dichloroethene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1NDcis-1,3-Dichloropropene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1NDDibromochloromethane 4.1 08/29/15 JLI SW8260Cug/Kg0.81 1NDDibromomethane 4.1 08/29/15 JLI SW8260Cug/Kg0.81 1NDDichlorodifluoromethane 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1NDEthylbenzene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1NDHexachlorobutadiene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1NDIsopropylbenzene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1NDm&p-Xylene 4.1 08/29/15 JLI SW8260Cug/Kg0.81 1NDMethyl Ethyl Ketone 24 08/29/15 JLI SW8260Cug/Kg4.1 1NDMethyl t-butyl ether (MTBE) 8.1 08/29/15 JLI SW8260Cug/Kg0.81 1NDMethylene chloride 4.1 08/29/15 JLI SW8260Cug/Kg4.1 10.90Naphthalene 4.1 08/29/15 JLI SW8260Cug/Kg0.81 1JNDn-Butylbenzene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1NDn-Propylbenzene 4.1 08/29/15 JLI SW8260Cug/Kg0.73 1


14B2 (0-5)Phoenix I.D.: BJ81786



LOD/MDL Dilution

NDo-Xylene 4.1 08/29/15 JLI SW8260Cug/Kg0.81 10.72p-Isopropyltoluene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1JNDsec-Butylbenzene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1NDStyrene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1NDtert-Butylbenzene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1NDTetrachloroethene 4.1 08/29/15 JLI SW8260Cug/Kg0.81 1NDTetrahydrofuran (THF) 8.1 08/29/15 JLI SW8260Cug/Kg 12.0 1NDToluene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1NDtrans-1,2-Dichloroethene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1NDtrans-1,3-Dichloropropene 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1NDtrans-1,4-dichloro-2-butene 8.1 08/29/15 JLI SW8260Cug/Kg2.0 165Trichloroethene 290 08/29/15 JLI SW8260Cug/Kg29 50JNDTrichlorofluoromethane 4.1 08/29/15 JLI SW8260Cug/Kg0.81 1NDTrichlorotrifluoroethane 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1NDVinyl chloride 4.1 08/29/15 JLI SW8260Cug/Kg0.41 1







14B2 (0-5)Phoenix I.D.: BJ81786



LOD/MDL Dilution

1302-Methylnaphthalene 260 08/27/15 DD SW8270Dug/Kg110 1JND2-Methylphenol (o-cresol) 260 08/27/15 DD SW8270Dug/Kg170 1ND2-Nitroaniline 740 08/27/15 DD SW8270Dug/Kg370 1ND2-Nitrophenol 260 08/27/15 DD SW8270Dug/Kg230 1ND3&4-Methylphenol (m&p-cresol) 260 08/27/15 DD SW8270Dug/Kg 1150 1ND3,3'-Dichlorobenzidine 740 08/27/15 DD SW8270Dug/Kg170 1ND3-Nitroaniline 740 08/27/15 DD SW8270Dug/Kg740 1ND4,6-Dinitro-2-methylphenol 1800 08/27/15 DD SW8270Dug/Kg400 1ND4-Bromophenyl phenyl ether 260 08/27/15 DD SW8270Dug/Kg110 1ND4-Chloro-3-methylphenol 260 08/27/15 DD SW8270Dug/Kg130 1ND4-Chloroaniline 300 08/27/15 DD SW8270Dug/Kg170 1ND4-Chlorophenyl phenyl ether 260 08/27/15 DD SW8270Dug/Kg120 1ND4-Nitroaniline 740 08/27/15 DD SW8270Dug/Kg120 1ND4-Nitrophenol 370 08/27/15 DD SW8270Dug/Kg170 1NDAcenaphthene 260 08/27/15 DD SW8270Dug/Kg110 1120Acenaphthylene 260 08/27/15 DD SW8270Dug/Kg100 1JNDAcetophenone 260 08/27/15 DD SW8270Dug/Kg120 1NDAniline 300 08/27/15 DD SW8270Dug/Kg300 1300Anthracene 260 08/27/15 DD SW8270Dug/Kg120 1820Benz(a)anthracene 260 08/27/15 DD SW8270Dug/Kg120 1NDBenzidine 740 08/27/15 DD SW8270Dug/Kg220 1810Benzo(a)pyrene 260 08/27/15 DD SW8270Dug/Kg120 1750Benzo(b)fluoranthene 260 08/27/15 DD SW8270Dug/Kg130 1500Benzo(ghi)perylene 260 08/27/15 DD SW8270Dug/Kg120 1620Benzo(k)fluoranthene 260 08/27/15 DD SW8270Dug/Kg120 1NDBenzoic acid 1800 08/27/15 DD SW8270Dug/Kg 1740 1NDBenzyl butyl phthalate 260 08/27/15 DD SW8270Dug/Kg95 1NDBis(2-chloroethoxy)methane 260 08/27/15 DD SW8270Dug/Kg100 1NDBis(2-chloroethyl)ether 260 08/27/15 DD SW8270Dug/Kg100 1NDBis(2-chloroisopropyl)ether 260 08/27/15 DD SW8270Dug/Kg 1100 1NDBis(2-ethylhexyl)phthalate 260 08/27/15 DD SW8270Dug/Kg110 1NDCarbazole 1800 08/27/15 DD SW8270Dug/Kg280 1820Chrysene 260 08/27/15 DD SW8270Dug/Kg120 1170Dibenz(a,h)anthracene 260 08/27/15 DD SW8270Dug/Kg120 1J140Dibenzofuran 260 08/27/15 DD SW8270Dug/Kg110 1JNDDiethyl phthalate 260 08/27/15 DD SW8270Dug/Kg120 1NDDimethylphthalate 260 08/27/15 DD SW8270Dug/Kg110 1NDDi-n-butylphthalate 260 08/27/15 DD SW8270Dug/Kg98 1NDDi-n-octylphthalate 260 08/27/15 DD SW8270Dug/Kg95 1

1300Fluoranthene 260 08/27/15 DD SW8270Dug/Kg120 1150Fluorene 260 08/27/15 DD SW8270Dug/Kg120 1JNDHexachlorobenzene 260 08/27/15 DD SW8270Dug/Kg110 1NDHexachlorobutadiene 260 08/27/15 DD SW8270Dug/Kg130 1NDHexachlorocyclopentadiene 260 08/27/15 DD SW8270Dug/Kg110 1NDHexachloroethane 260 08/27/15 DD SW8270Dug/Kg110 1570Indeno(1,2,3-cd)pyrene 260 08/27/15 DD SW8270Dug/Kg120 1NDIsophorone 260 08/27/15 DD SW8270Dug/Kg100 1230Naphthalene 260 08/27/15 DD SW8270Dug/Kg110 1JNDNitrobenzene 260 08/27/15 DD SW8270Dug/Kg130 1


14B2 (0-5)Phoenix I.D.: BJ81786



LOD/MDL Dilution





Comments:



PCB Comment:Due to the presence of what appears to be Chlordane in the sample which co-elutes with the PCBs, an elevated RL was reported.

Pesticide Comment:Due to the presence of Chlordane in the sample, an elevated RL was reported.











SOLIDEBC72 Hour


RB

Laboratory Data

14B2 (10-15)

Phoenix ID: BJ81787

08/26/1510:1517:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution




14B2 (10-15)Phoenix I.D.: BJ81787



LOD/MDL Dilution

ND2-Isopropyltoluene 5.5 08/29/15 JLI SW8260Cug/Kg 10.55 1ND4-Chlorotoluene 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1ND4-Methyl-2-pentanone 28 08/29/15 JLI SW8260Cug/Kg5.5 1NDAcetone 50 08/29/15 JLI SW8260Cug/Kg5.5 1NDAcrylonitrile 11 08/29/15 JLI SW8260Cug/Kg1.1 1NDBenzene 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDBromobenzene 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDBromochloromethane 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDBromodichloromethane 5.5 08/29/15 JLI SW8260Cug/Kg1.1 1NDBromoform 5.5 08/29/15 JLI SW8260Cug/Kg1.1 1NDBromomethane 5.5 08/29/15 JLI SW8260Cug/Kg2.2 1NDCarbon Disulfide 5.5 08/29/15 JLI SW8260Cug/Kg1.1 1NDCarbon tetrachloride 5.5 08/29/15 JLI SW8260Cug/Kg1.1 1NDChlorobenzene 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDChloroethane 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDChloroform 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDChloromethane 5.5 08/29/15 JLI SW8260Cug/Kg1.1 1NDcis-1,2-Dichloroethene 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDcis-1,3-Dichloropropene 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDDibromochloromethane 5.5 08/29/15 JLI SW8260Cug/Kg1.1 1NDDibromomethane 5.5 08/29/15 JLI SW8260Cug/Kg1.1 1NDDichlorodifluoromethane 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDEthylbenzene 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDHexachlorobutadiene 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDIsopropylbenzene 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDm&p-Xylene 5.5 08/29/15 JLI SW8260Cug/Kg1.1 1NDMethyl Ethyl Ketone 33 08/29/15 JLI SW8260Cug/Kg5.5 1NDMethyl t-butyl ether (MTBE) 11 08/29/15 JLI SW8260Cug/Kg1.1 1NDMethylene chloride 5.5 08/29/15 JLI SW8260Cug/Kg5.5 1NDNaphthalene 5.5 08/29/15 JLI SW8260Cug/Kg1.1 1NDn-Butylbenzene 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDn-Propylbenzene 5.5 08/29/15 JLI SW8260Cug/Kg0.99 1NDo-Xylene 5.5 08/29/15 JLI SW8260Cug/Kg1.1 1NDp-Isopropyltoluene 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDsec-Butylbenzene 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDStyrene 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDtert-Butylbenzene 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDTetrachloroethene 5.5 08/29/15 JLI SW8260Cug/Kg1.1 1NDTetrahydrofuran (THF) 11 08/29/15 JLI SW8260Cug/Kg 12.8 1NDToluene 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDtrans-1,2-Dichloroethene 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDtrans-1,3-Dichloropropene 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDtrans-1,4-dichloro-2-butene 11 08/29/15 JLI SW8260Cug/Kg2.8 10.66Trichloroethene 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1JNDTrichlorofluoromethane 5.5 08/29/15 JLI SW8260Cug/Kg1.1 1NDTrichlorotrifluoroethane 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1NDVinyl chloride 5.5 08/29/15 JLI SW8260Cug/Kg0.55 1



14B2 (10-15)Phoenix I.D.: BJ81787



LOD/MDL Dilution







14B2 (10-15)Phoenix I.D.: BJ81787



LOD/MDL Dilution

NDAniline 310 08/27/15 DD SW8270Dug/Kg310 1NDAnthracene 270 08/27/15 DD SW8270Dug/Kg130 1NDBenz(a)anthracene 270 08/27/15 DD SW8270Dug/Kg130 1NDBenzidine 770 08/27/15 DD SW8270Dug/Kg230 1NDBenzo(a)pyrene 270 08/27/15 DD SW8270Dug/Kg120 1NDBenzo(b)fluoranthene 270 08/27/15 DD SW8270Dug/Kg130 1NDBenzo(ghi)perylene 270 08/27/15 DD SW8270Dug/Kg120 1NDBenzo(k)fluoranthene 270 08/27/15 DD SW8270Dug/Kg130 1NDBenzoic acid 1900 08/27/15 DD SW8270Dug/Kg 1770 1NDBenzyl butyl phthalate 270 08/27/15 DD SW8270Dug/Kg99 1NDBis(2-chloroethoxy)methane 270 08/27/15 DD SW8270Dug/Kg110 1NDBis(2-chloroethyl)ether 270 08/27/15 DD SW8270Dug/Kg100 1NDBis(2-chloroisopropyl)ether 270 08/27/15 DD SW8270Dug/Kg 1110 1NDBis(2-ethylhexyl)phthalate 270 08/27/15 DD SW8270Dug/Kg110 1NDCarbazole 1900 08/27/15 DD SW8270Dug/Kg290 1NDChrysene 270 08/27/15 DD SW8270Dug/Kg130 1NDDibenz(a,h)anthracene 270 08/27/15 DD SW8270Dug/Kg120 1NDDibenzofuran 270 08/27/15 DD SW8270Dug/Kg110 1NDDiethyl phthalate 270 08/27/15 DD SW8270Dug/Kg120 1NDDimethylphthalate 270 08/27/15 DD SW8270Dug/Kg120 1NDDi-n-butylphthalate 270 08/27/15 DD SW8270Dug/Kg100 1NDDi-n-octylphthalate 270 08/27/15 DD SW8270Dug/Kg99 1NDFluoranthene 270 08/27/15 DD SW8270Dug/Kg120 1NDFluorene 270 08/27/15 DD SW8270Dug/Kg130 1NDHexachlorobenzene 270 08/27/15 DD SW8270Dug/Kg110 1NDHexachlorobutadiene 270 08/27/15 DD SW8270Dug/Kg140 1NDHexachlorocyclopentadiene 270 08/27/15 DD SW8270Dug/Kg120 1NDHexachloroethane 270 08/27/15 DD SW8270Dug/Kg110 1NDIndeno(1,2,3-cd)pyrene 270 08/27/15 DD SW8270Dug/Kg130 1NDIsophorone 270 08/27/15 DD SW8270Dug/Kg110 1NDNaphthalene 270 08/27/15 DD SW8270Dug/Kg110 1NDNitrobenzene 270 08/27/15 DD SW8270Dug/Kg130 1NDN-Nitrosodimethylamine 270 08/27/15 DD SW8270Dug/Kg110 1NDN-Nitrosodi-n-propylamine 270 08/27/15 DD SW8270Dug/Kg120 1NDN-Nitrosodiphenylamine 270 08/27/15 DD SW8270Dug/Kg150 1NDPentachloronitrobenzene 270 08/27/15 DD SW8270Dug/Kg140 1NDPentachlorophenol 270 08/27/15 DD SW8270Dug/Kg140 1NDPhenanthrene 270 08/27/15 DD SW8270Dug/Kg110 1NDPhenol 270 08/27/15 DD SW8270Dug/Kg120 1NDPyrene 270 08/27/15 DD SW8270Dug/Kg130 1NDPyridine 270 08/27/15 DD SW8270Dug/Kg94 1



14B2 (10-15)Phoenix I.D.: BJ81787



LOD/MDL Dilution

Comments:











SOLIDEBC72 Hour


RB

Laboratory Data

14B2 (20-25)

Phoenix ID: BJ81788

08/26/1510:3017:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution








14B2 (20-25)Phoenix I.D.: BJ81788



LOD/MDL Dilution






VolatilesND1,1,1,2-Tetrachloroethane 4.4 08/29/15 JLI SW8260Cug/Kg0.87 1ND1,1,1-Trichloroethane 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1ND1,1,2,2-Tetrachloroethane 4.4 08/29/15 JLI SW8260Cug/Kg0.87 1ND1,1,2-Trichloroethane 4.4 08/29/15 JLI SW8260Cug/Kg0.87 1ND1,1-Dichloroethane 4.4 08/29/15 JLI SW8260Cug/Kg0.87 10.501,1-Dichloroethene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1J


14B2 (20-25)Phoenix I.D.: BJ81788



LOD/MDL Dilution

ND1,1-Dichloropropene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1ND1,2,3-Trichlorobenzene 4.4 08/29/15 JLI SW8260Cug/Kg0.87 1ND1,2,3-Trichloropropane 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1ND1,2,4-Trichlorobenzene 4.4 08/29/15 JLI SW8260Cug/Kg0.87 1ND1,2,4-Trimethylbenzene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1ND1,2-Dibromo-3-chloropropane 4.4 08/29/15 JLI SW8260Cug/Kg0.87 1ND1,2-Dibromoethane 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1ND1,2-Dichlorobenzene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1ND1,2-Dichloroethane 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1ND1,2-Dichloropropane 4.4 08/29/15 JLI SW8260Cug/Kg0.87 1ND1,3,5-Trimethylbenzene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1ND1,3-Dichlorobenzene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1ND1,3-Dichloropropane 4.4 08/29/15 JLI SW8260Cug/Kg0.87 1ND1,4-Dichlorobenzene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1ND2,2-Dichloropropane 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1ND2-Chlorotoluene 4.4 08/29/15 JLI SW8260Cug/Kg0.87 1ND2-Hexanone 22 08/29/15 JLI SW8260Cug/Kg4.4 1ND2-Isopropyltoluene 4.4 08/29/15 JLI SW8260Cug/Kg 10.44 1ND4-Chlorotoluene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1ND4-Methyl-2-pentanone 22 08/29/15 JLI SW8260Cug/Kg4.4 1NDAcetone 44 08/29/15 JLI SW8260Cug/Kg4.4 1NDAcrylonitrile 8.7 08/29/15 JLI SW8260Cug/Kg0.87 11.0Benzene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1JNDBromobenzene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1NDBromochloromethane 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1NDBromodichloromethane 4.4 08/29/15 JLI SW8260Cug/Kg0.87 1NDBromoform 4.4 08/29/15 JLI SW8260Cug/Kg0.87 1NDBromomethane 4.4 08/29/15 JLI SW8260Cug/Kg1.7 1NDCarbon Disulfide 4.4 08/29/15 JLI SW8260Cug/Kg0.87 1NDCarbon tetrachloride 4.4 08/29/15 JLI SW8260Cug/Kg0.87 1NDChlorobenzene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1NDChloroethane 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1NDChloroform 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1NDChloromethane 4.4 08/29/15 JLI SW8260Cug/Kg0.87 162cis-1,2-Dichloroethene 250 08/29/15 JLI SW8260Cug/Kg35 50JNDcis-1,3-Dichloropropene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1NDDibromochloromethane 4.4 08/29/15 JLI SW8260Cug/Kg0.87 1NDDibromomethane 4.4 08/29/15 JLI SW8260Cug/Kg0.87 10.88Dichlorodifluoromethane 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1JNDEthylbenzene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1NDHexachlorobutadiene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1NDIsopropylbenzene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1NDm&p-Xylene 4.4 08/29/15 JLI SW8260Cug/Kg0.87 1NDMethyl Ethyl Ketone 26 08/29/15 JLI SW8260Cug/Kg4.4 1NDMethyl t-butyl ether (MTBE) 8.7 08/29/15 JLI SW8260Cug/Kg0.87 1NDMethylene chloride 4.4 08/29/15 JLI SW8260Cug/Kg4.4 1NDNaphthalene 4.4 08/29/15 JLI SW8260Cug/Kg0.87 1NDn-Butylbenzene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1NDn-Propylbenzene 4.4 08/29/15 JLI SW8260Cug/Kg0.78 1


14B2 (20-25)Phoenix I.D.: BJ81788



LOD/MDL Dilution

NDo-Xylene 4.4 08/29/15 JLI SW8260Cug/Kg0.87 1NDp-Isopropyltoluene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1NDsec-Butylbenzene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1NDStyrene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1NDtert-Butylbenzene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1NDTetrachloroethene 4.4 08/29/15 JLI SW8260Cug/Kg0.87 1NDTetrahydrofuran (THF) 8.7 08/29/15 JLI SW8260Cug/Kg 12.2 1NDToluene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 12.6trans-1,2-Dichloroethene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1JNDtrans-1,3-Dichloropropene 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1NDtrans-1,4-dichloro-2-butene 8.7 08/29/15 JLI SW8260Cug/Kg2.2 141Trichloroethene 350 08/29/15 JLI SW8260Cug/Kg35 50JNDTrichlorofluoromethane 4.4 08/29/15 JLI SW8260Cug/Kg0.87 1NDTrichlorotrifluoroethane 4.4 08/29/15 JLI SW8260Cug/Kg0.44 12.6Vinyl chloride 4.4 08/29/15 JLI SW8260Cug/Kg0.44 1J







14B2 (20-25)Phoenix I.D.: BJ81788



LOD/MDL Dilution

ND2-Methylnaphthalene 270 08/27/15 DD SW8270Dug/Kg120 1ND2-Methylphenol (o-cresol) 270 08/27/15 DD SW8270Dug/Kg180 1ND2-Nitroaniline 780 08/27/15 DD SW8270Dug/Kg390 1ND2-Nitrophenol 270 08/27/15 DD SW8270Dug/Kg250 1ND3&4-Methylphenol (m&p-cresol) 270 08/27/15 DD SW8270Dug/Kg 1150 1ND3,3'-Dichlorobenzidine 780 08/27/15 DD SW8270Dug/Kg180 1ND3-Nitroaniline 780 08/27/15 DD SW8270Dug/Kg780 1ND4,6-Dinitro-2-methylphenol 1900 08/27/15 DD SW8270Dug/Kg420 1ND4-Bromophenyl phenyl ether 270 08/27/15 DD SW8270Dug/Kg110 1ND4-Chloro-3-methylphenol 270 08/27/15 DD SW8270Dug/Kg140 1ND4-Chloroaniline 310 08/27/15 DD SW8270Dug/Kg180 1ND4-Chlorophenyl phenyl ether 270 08/27/15 DD SW8270Dug/Kg130 1ND4-Nitroaniline 780 08/27/15 DD SW8270Dug/Kg130 1ND4-Nitrophenol 390 08/27/15 DD SW8270Dug/Kg180 1NDAcenaphthene 270 08/27/15 DD SW8270Dug/Kg120 1NDAcenaphthylene 270 08/27/15 DD SW8270Dug/Kg110 1NDAcetophenone 270 08/27/15 DD SW8270Dug/Kg120 1NDAniline 310 08/27/15 DD SW8270Dug/Kg310 1NDAnthracene 270 08/27/15 DD SW8270Dug/Kg130 1NDBenz(a)anthracene 270 08/27/15 DD SW8270Dug/Kg130 1NDBenzidine 780 08/27/15 DD SW8270Dug/Kg230 1NDBenzo(a)pyrene 270 08/27/15 DD SW8270Dug/Kg130 1NDBenzo(b)fluoranthene 270 08/27/15 DD SW8270Dug/Kg130 1NDBenzo(ghi)perylene 270 08/27/15 DD SW8270Dug/Kg130 1NDBenzo(k)fluoranthene 270 08/27/15 DD SW8270Dug/Kg130 1NDBenzoic acid 1900 08/27/15 DD SW8270Dug/Kg 1780 1NDBenzyl butyl phthalate 270 08/27/15 DD SW8270Dug/Kg100 1NDBis(2-chloroethoxy)methane 270 08/27/15 DD SW8270Dug/Kg110 1NDBis(2-chloroethyl)ether 270 08/27/15 DD SW8270Dug/Kg100 1NDBis(2-chloroisopropyl)ether 270 08/27/15 DD SW8270Dug/Kg 1110 1NDBis(2-ethylhexyl)phthalate 270 08/27/15 DD SW8270Dug/Kg110 1NDCarbazole 1900 08/27/15 DD SW8270Dug/Kg290 1NDChrysene 270 08/27/15 DD SW8270Dug/Kg130 1NDDibenz(a,h)anthracene 270 08/27/15 DD SW8270Dug/Kg130 1NDDibenzofuran 270 08/27/15 DD SW8270Dug/Kg110 1NDDiethyl phthalate 270 08/27/15 DD SW8270Dug/Kg120 1NDDimethylphthalate 270 08/27/15 DD SW8270Dug/Kg120 1NDDi-n-butylphthalate 270 08/27/15 DD SW8270Dug/Kg100 1NDDi-n-octylphthalate 270 08/27/15 DD SW8270Dug/Kg100 1NDFluoranthene 270 08/27/15 DD SW8270Dug/Kg130 1NDFluorene 270 08/27/15 DD SW8270Dug/Kg130 1NDHexachlorobenzene 270 08/27/15 DD SW8270Dug/Kg110 1NDHexachlorobutadiene 270 08/27/15 DD SW8270Dug/Kg140 1NDHexachlorocyclopentadiene 270 08/27/15 DD SW8270Dug/Kg120 1NDHexachloroethane 270 08/27/15 DD SW8270Dug/Kg120 1NDIndeno(1,2,3-cd)pyrene 270 08/27/15 DD SW8270Dug/Kg130 1NDIsophorone 270 08/27/15 DD SW8270Dug/Kg110 1NDNaphthalene 270 08/27/15 DD SW8270Dug/Kg110 1NDNitrobenzene 270 08/27/15 DD SW8270Dug/Kg140 1


14B2 (20-25)Phoenix I.D.: BJ81788



LOD/MDL Dilution



Comments:












SOLIDEBC72 Hour


RB

Laboratory Data

14B1 (0-5)

Phoenix ID: BJ81789

08/26/1511:0017:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution


72.0Barium 0.7 08/28/15 LK SW6010Cmg/Kg0.33 10.45Beryllium 0.26 08/28/15 LK SW6010Cmg/Kg0.13 15560Calcium 3.3 08/28/15 LK SW6010Cmg/Kg3.0 10.59Cadmium 0.33 08/28/15 LK SW6010Cmg/Kg0.13 18.27Cobalt 0.33 08/28/15 LK SW6010Cmg/Kg0.33 131.3Chromium 0.33 08/28/15 LK SW6010Cmg/Kg0.33 125.1Copper 0.33 08/28/15 LK SW6010Cmg/kg0.33 1

17900Iron 33 08/28/15 LK SW6010Cmg/Kg B33 100.58Mercury 0.03 08/27/15 RS SW7471Bmg/Kg0.02 11420Potassium 7 08/28/15 LK SW6010Cmg/Kg2.6 1N2530Magnesium 3.3 08/28/15 LK SW6010Cmg/Kg3.3 1356Manganese 3.3 08/28/15 LK SW6010Cmg/Kg3.3 10290Sodium 7 08/28/15 LK SW6010Cmg/Kg2.8 1N36.3Nickel 0.33 08/28/15 LK SW6010Cmg/Kg0.33 1102Lead 0.7 08/28/15 LK SW6010Cmg/Kg0.33 1




14B1 (0-5)Phoenix I.D.: BJ81789



LOD/MDL Dilution




Pesticides - SoilND4,4' -DDD 9.1 08/28/15 CE SW8081Bug/Kg9.1 10ND4,4' -DDE 9.1 08/28/15 CE SW8081Bug/Kg9.1 10ND4,4' -DDT 9.1 08/28/15 CE SW8081Bug/Kg9.1 10NDa-BHC 18 08/28/15 CE SW8081Bug/Kg18 1068a-Chlordane 18 08/28/15 CE SW8081Bug/Kg18 10NDAldrin 5.5 08/28/15 CE SW8081Bug/Kg5.5 10NDb-BHC 18 08/28/15 CE SW8081Bug/Kg18 10NDd-BHC 37 08/28/15 CE SW8081Bug/Kg37 10NDDieldrin 5.5 08/28/15 CE SW8081Bug/Kg5.5 10NDEndosulfan I 37 08/28/15 CE SW8081Bug/Kg37 10NDEndosulfan II 37 08/28/15 CE SW8081Bug/Kg37 10NDEndosulfan sulfate 37 08/28/15 CE SW8081Bug/Kg37 10NDEndrin 18 08/28/15 CE SW8081Bug/Kg18 10NDEndrin aldehyde 37 08/28/15 CE SW8081Bug/Kg37 10NDEndrin ketone 37 08/28/15 CE SW8081Bug/Kg37 10NDg-BHC 7.3 08/28/15 CE SW8081Bug/Kg7.3 1052g-Chlordane 18 08/28/15 CE SW8081Bug/Kg18 10NDHeptachlor 37 08/28/15 CE SW8081Bug/Kg37 10NDHeptachlor epoxide 37 08/28/15 CE SW8081Bug/Kg37 10NDMethoxychlor 180 08/28/15 CE SW8081Bug/Kg180 10NDToxaphene 730 08/28/15 CE SW8081Bug/Kg730 10




14B1 (0-5)Phoenix I.D.: BJ81789



LOD/MDL Dilution

ND1,1-Dichloropropene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1ND1,2,3-Trichlorobenzene 4.9 08/29/15 JLI SW8260Cug/Kg0.99 1ND1,2,3-Trichloropropane 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1ND1,2,4-Trichlorobenzene 4.9 08/29/15 JLI SW8260Cug/Kg0.99 1ND1,2,4-Trimethylbenzene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1ND1,2-Dibromo-3-chloropropane 4.9 08/29/15 JLI SW8260Cug/Kg0.99 1ND1,2-Dibromoethane 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1ND1,2-Dichlorobenzene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1ND1,2-Dichloroethane 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1ND1,2-Dichloropropane 4.9 08/29/15 JLI SW8260Cug/Kg0.99 1ND1,3,5-Trimethylbenzene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1ND1,3-Dichlorobenzene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1ND1,3-Dichloropropane 4.9 08/29/15 JLI SW8260Cug/Kg0.99 1ND1,4-Dichlorobenzene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1ND2,2-Dichloropropane 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1ND2-Chlorotoluene 4.9 08/29/15 JLI SW8260Cug/Kg0.99 1ND2-Hexanone 25 08/29/15 JLI SW8260Cug/Kg4.9 1ND2-Isopropyltoluene 4.9 08/29/15 JLI SW8260Cug/Kg 10.49 1ND4-Chlorotoluene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1ND4-Methyl-2-pentanone 25 08/29/15 JLI SW8260Cug/Kg4.9 1NDAcetone 49 08/29/15 JLI SW8260Cug/Kg4.9 1NDAcrylonitrile 9.9 08/29/15 JLI SW8260Cug/Kg0.99 1NDBenzene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDBromobenzene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDBromochloromethane 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDBromodichloromethane 4.9 08/29/15 JLI SW8260Cug/Kg0.99 1NDBromoform 4.9 08/29/15 JLI SW8260Cug/Kg0.99 1NDBromomethane 4.9 08/29/15 JLI SW8260Cug/Kg2.0 1NDCarbon Disulfide 4.9 08/29/15 JLI SW8260Cug/Kg0.99 1NDCarbon tetrachloride 4.9 08/29/15 JLI SW8260Cug/Kg0.99 1NDChlorobenzene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDChloroethane 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDChloroform 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDChloromethane 4.9 08/29/15 JLI SW8260Cug/Kg0.99 1NDcis-1,2-Dichloroethene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDcis-1,3-Dichloropropene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDDibromochloromethane 4.9 08/29/15 JLI SW8260Cug/Kg0.99 1NDDibromomethane 4.9 08/29/15 JLI SW8260Cug/Kg0.99 1NDDichlorodifluoromethane 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDEthylbenzene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDHexachlorobutadiene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDIsopropylbenzene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDm&p-Xylene 4.9 08/29/15 JLI SW8260Cug/Kg0.99 1NDMethyl Ethyl Ketone 30 08/29/15 JLI SW8260Cug/Kg4.9 1NDMethyl t-butyl ether (MTBE) 9.9 08/29/15 JLI SW8260Cug/Kg0.99 1NDMethylene chloride 4.9 08/29/15 JLI SW8260Cug/Kg4.9 1NDNaphthalene 4.9 08/29/15 JLI SW8260Cug/Kg0.99 1NDn-Butylbenzene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDn-Propylbenzene 4.9 08/29/15 JLI SW8260Cug/Kg0.89 1


14B1 (0-5)Phoenix I.D.: BJ81789



LOD/MDL Dilution

NDo-Xylene 4.9 08/29/15 JLI SW8260Cug/Kg0.99 1NDp-Isopropyltoluene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDsec-Butylbenzene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDStyrene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDtert-Butylbenzene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDTetrachloroethene 4.9 08/29/15 JLI SW8260Cug/Kg0.99 1NDTetrahydrofuran (THF) 9.9 08/29/15 JLI SW8260Cug/Kg 12.5 1NDToluene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDtrans-1,2-Dichloroethene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDtrans-1,3-Dichloropropene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDtrans-1,4-dichloro-2-butene 9.9 08/29/15 JLI SW8260Cug/Kg2.5 11.7Trichloroethene 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1JNDTrichlorofluoromethane 4.9 08/29/15 JLI SW8260Cug/Kg0.99 1NDTrichlorotrifluoroethane 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1NDVinyl chloride 4.9 08/29/15 JLI SW8260Cug/Kg0.49 1





SemivolatilesND1,2,4,5-Tetrachlorobenzene 250 08/27/15 DD SW8270Dug/Kg130 1ND1,2,4-Trichlorobenzene 250 08/27/15 DD SW8270Dug/Kg110 1ND1,2-Dichlorobenzene 250 08/27/15 DD SW8270Dug/Kg100 1ND1,2-Diphenylhydrazine 250 08/27/15 DD SW8270Dug/Kg120 1ND1,3-Dichlorobenzene 250 08/27/15 DD SW8270Dug/Kg110 15001,4-Dichlorobenzene 250 08/27/15 DD SW8270Dug/Kg110 1ND2,4,5-Trichlorophenol 250 08/27/15 DD SW8270Dug/Kg200 1ND2,4,6-Trichlorophenol 250 08/27/15 DD SW8270Dug/Kg120 1ND2,4-Dichlorophenol 250 08/27/15 DD SW8270Dug/Kg130 1ND2,4-Dimethylphenol 250 08/27/15 DD SW8270Dug/Kg90 1ND2,4-Dinitrophenol 730 08/27/15 DD SW8270Dug/Kg250 1ND2,4-Dinitrotoluene 250 08/27/15 DD SW8270Dug/Kg140 1ND2,6-Dinitrotoluene 250 08/27/15 DD SW8270Dug/Kg110 1ND2-Chloronaphthalene 250 08/27/15 DD SW8270Dug/Kg100 1ND2-Chlorophenol 250 08/27/15 DD SW8270Dug/Kg100 1


14B1 (0-5)Phoenix I.D.: BJ81789



LOD/MDL Dilution

ND2-Methylnaphthalene 250 08/27/15 DD SW8270Dug/Kg110 1ND2-Methylphenol (o-cresol) 250 08/27/15 DD SW8270Dug/Kg170 1ND2-Nitroaniline 730 08/27/15 DD SW8270Dug/Kg370 1ND2-Nitrophenol 250 08/27/15 DD SW8270Dug/Kg230 1ND3&4-Methylphenol (m&p-cresol) 250 08/27/15 DD SW8270Dug/Kg 1140 1ND3,3'-Dichlorobenzidine 730 08/27/15 DD SW8270Dug/Kg170 1ND3-Nitroaniline 730 08/27/15 DD SW8270Dug/Kg730 1ND4,6-Dinitro-2-methylphenol 1800 08/27/15 DD SW8270Dug/Kg390 1ND4-Bromophenyl phenyl ether 250 08/27/15 DD SW8270Dug/Kg110 1ND4-Chloro-3-methylphenol 250 08/27/15 DD SW8270Dug/Kg130 1ND4-Chloroaniline 290 08/27/15 DD SW8270Dug/Kg170 1ND4-Chlorophenyl phenyl ether 250 08/27/15 DD SW8270Dug/Kg120 1ND4-Nitroaniline 730 08/27/15 DD SW8270Dug/Kg120 1ND4-Nitrophenol 360 08/27/15 DD SW8270Dug/Kg160 1NDAcenaphthene 250 08/27/15 DD SW8270Dug/Kg110 1110Acenaphthylene 250 08/27/15 DD SW8270Dug/Kg100 1JNDAcetophenone 250 08/27/15 DD SW8270Dug/Kg110 1NDAniline 290 08/27/15 DD SW8270Dug/Kg290 1860Anthracene 250 08/27/15 DD SW8270Dug/Kg120 1

3500Benz(a)anthracene 250 08/27/15 DD SW8270Dug/Kg120 1NDBenzidine 730 08/27/15 DD SW8270Dug/Kg210 1

3200Benzo(a)pyrene 250 08/27/15 DD SW8270Dug/Kg120 14500Benzo(b)fluoranthene 250 08/27/15 DD SW8270Dug/Kg120 13000Benzo(ghi)perylene 250 08/27/15 DD SW8270Dug/Kg120 13400Benzo(k)fluoranthene 250 08/27/15 DD SW8270Dug/Kg120 1NDBenzoic acid 1800 08/27/15 DD SW8270Dug/Kg 1730 1NDBenzyl butyl phthalate 250 08/27/15 DD SW8270Dug/Kg94 1NDBis(2-chloroethoxy)methane 250 08/27/15 DD SW8270Dug/Kg100 1NDBis(2-chloroethyl)ether 250 08/27/15 DD SW8270Dug/Kg98 1NDBis(2-chloroisopropyl)ether 250 08/27/15 DD SW8270Dug/Kg 1100 1NDBis(2-ethylhexyl)phthalate 250 08/27/15 DD SW8270Dug/Kg100 1350Carbazole 1800 08/27/15 DD SW8270Dug/Kg280 1J

3300Chrysene 250 08/27/15 DD SW8270Dug/Kg120 11400Dibenz(a,h)anthracene 250 08/27/15 DD SW8270Dug/Kg120 1240Dibenzofuran 250 08/27/15 DD SW8270Dug/Kg110 1JNDDiethyl phthalate 250 08/27/15 DD SW8270Dug/Kg110 1NDDimethylphthalate 250 08/27/15 DD SW8270Dug/Kg110 1NDDi-n-butylphthalate 250 08/27/15 DD SW8270Dug/Kg97 1NDDi-n-octylphthalate 250 08/27/15 DD SW8270Dug/Kg94 1

4300Fluoranthene 250 08/27/15 DD SW8270Dug/Kg120 1230Fluorene 250 08/27/15 DD SW8270Dug/Kg120 1JNDHexachlorobenzene 250 08/27/15 DD SW8270Dug/Kg110 1NDHexachlorobutadiene 250 08/27/15 DD SW8270Dug/Kg130 1NDHexachlorocyclopentadiene 250 08/27/15 DD SW8270Dug/Kg110 1NDHexachloroethane 250 08/27/15 DD SW8270Dug/Kg110 1

3900Indeno(1,2,3-cd)pyrene 250 08/27/15 DD SW8270Dug/Kg120 1NDIsophorone 250 08/27/15 DD SW8270Dug/Kg100 1240Naphthalene 250 08/27/15 DD SW8270Dug/Kg100 1JNDNitrobenzene 250 08/27/15 DD SW8270Dug/Kg130 1


14B1 (0-5)Phoenix I.D.: BJ81789



LOD/MDL Dilution





Comments:













SOLIDEBC72 Hour


RB

Laboratory Data

14B1 (10-15)

Phoenix ID: BJ81790

08/26/1511:1517:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution




14B1 (10-15)Phoenix I.D.: BJ81790



LOD/MDL Dilution

ND2-Isopropyltoluene 5.6 08/29/15 JLI SW8260Cug/Kg 10.56 1ND4-Chlorotoluene 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1ND4-Methyl-2-pentanone 28 08/29/15 JLI SW8260Cug/Kg5.6 121Acetone 50 08/29/15 JLI SW8260Cug/Kg5.6 1JSNDAcrylonitrile 11 08/29/15 JLI SW8260Cug/Kg0.56 10.57Benzene 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1JNDBromobenzene 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1NDBromochloromethane 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1NDBromodichloromethane 5.6 08/29/15 JLI SW8260Cug/Kg1.1 1NDBromoform 5.6 08/29/15 JLI SW8260Cug/Kg1.1 1NDBromomethane 5.6 08/29/15 JLI SW8260Cug/Kg2.2 1NDCarbon Disulfide 5.6 08/29/15 JLI SW8260Cug/Kg1.1 1NDCarbon tetrachloride 5.6 08/29/15 JLI SW8260Cug/Kg1.1 1NDChlorobenzene 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1NDChloroethane 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1NDChloroform 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1NDChloromethane 5.6 08/29/15 JLI SW8260Cug/Kg1.1 187cis-1,2-Dichloroethene 250 08/29/15 JLI SW8260Cug/Kg28 50JNDcis-1,3-Dichloropropene 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1NDDibromochloromethane 5.6 08/29/15 JLI SW8260Cug/Kg1.1 1NDDibromomethane 5.6 08/29/15 JLI SW8260Cug/Kg1.1 1NDDichlorodifluoromethane 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1NDEthylbenzene 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1NDHexachlorobutadiene 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1NDIsopropylbenzene 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1NDm&p-Xylene 5.6 08/29/15 JLI SW8260Cug/Kg1.1 1NDMethyl Ethyl Ketone 34 08/29/15 JLI SW8260Cug/Kg5.6 1NDMethyl t-butyl ether (MTBE) 11 08/29/15 JLI SW8260Cug/Kg1.1 1NDMethylene chloride 5.6 08/29/15 JLI SW8260Cug/Kg5.6 1NDNaphthalene 5.6 08/29/15 JLI SW8260Cug/Kg1.1 1NDn-Butylbenzene 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1NDn-Propylbenzene 5.6 08/29/15 JLI SW8260Cug/Kg1.0 1NDo-Xylene 5.6 08/29/15 JLI SW8260Cug/Kg1.1 1NDp-Isopropyltoluene 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1NDsec-Butylbenzene 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1NDStyrene 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1NDtert-Butylbenzene 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1NDTetrachloroethene 5.6 08/29/15 JLI SW8260Cug/Kg1.1 1NDTetrahydrofuran (THF) 11 08/29/15 JLI SW8260Cug/Kg 12.8 1NDToluene 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1NDtrans-1,2-Dichloroethene 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1NDtrans-1,3-Dichloropropene 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1NDtrans-1,4-dichloro-2-butene 11 08/29/15 JLI SW8260Cug/Kg2.8 1110Trichloroethene 280 08/29/15 JLI SW8260Cug/Kg28 50JNDTrichlorofluoromethane 5.6 08/29/15 JLI SW8260Cug/Kg1.1 1NDTrichlorotrifluoroethane 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1NDVinyl chloride 5.6 08/29/15 JLI SW8260Cug/Kg0.56 1



14B1 (10-15)Phoenix I.D.: BJ81790



LOD/MDL Dilution






23002-Methylnaphthalene 2600 08/27/15 DD SW8270Dug/Kg1100 10JND2-Methylphenol (o-cresol) 2600 08/27/15 DD SW8270Dug/Kg1700 10ND2-Nitroaniline 7300 08/27/15 DD SW8270Dug/Kg3700 10ND2-Nitrophenol 2600 08/27/15 DD SW8270Dug/Kg2300 10ND3&4-Methylphenol (m&p-cresol) 2600 08/27/15 DD SW8270Dug/Kg 11400 10ND3,3'-Dichlorobenzidine 7300 08/27/15 DD SW8270Dug/Kg1700 10ND3-Nitroaniline 7300 08/27/15 DD SW8270Dug/Kg7300 10ND4,6-Dinitro-2-methylphenol 18000 08/27/15 DD SW8270Dug/Kg4000 10ND4-Bromophenyl phenyl ether 2600 08/27/15 DD SW8270Dug/Kg1100 10ND4-Chloro-3-methylphenol 2600 08/27/15 DD SW8270Dug/Kg1300 10ND4-Chloroaniline 2900 08/27/15 DD SW8270Dug/Kg1700 10ND4-Chlorophenyl phenyl ether 2600 08/27/15 DD SW8270Dug/Kg1200 10ND4-Nitroaniline 7300 08/27/15 DD SW8270Dug/Kg1200 10ND4-Nitrophenol 3700 08/27/15 DD SW8270Dug/Kg1700 10NDAcenaphthene 2600 08/27/15 DD SW8270Dug/Kg1100 10NDAcenaphthylene 2600 08/27/15 DD SW8270Dug/Kg1000 10NDAcetophenone 2600 08/27/15 DD SW8270Dug/Kg1100 10


14B1 (10-15)Phoenix I.D.: BJ81790



LOD/MDL Dilution

NDAniline 2900 08/27/15 DD SW8270Dug/Kg2900 1015000Anthracene 2600 08/27/15 DD SW8270Dug/Kg1200 1016000Benz(a)anthracene 2600 08/27/15 DD SW8270Dug/Kg1200 10

NDBenzidine 7300 08/27/15 DD SW8270Dug/Kg2200 1013000Benzo(a)pyrene 2600 08/27/15 DD SW8270Dug/Kg1200 1011000Benzo(b)fluoranthene 2600 08/27/15 DD SW8270Dug/Kg1300 106200Benzo(ghi)perylene 2600 08/27/15 DD SW8270Dug/Kg1200 1010000Benzo(k)fluoranthene 2600 08/27/15 DD SW8270Dug/Kg1200 10

NDBenzoic acid 18000 08/27/15 DD SW8270Dug/Kg 17300 10NDBenzyl butyl phthalate 2600 08/27/15 DD SW8270Dug/Kg950 10NDBis(2-chloroethoxy)methane 2600 08/27/15 DD SW8270Dug/Kg1000 10NDBis(2-chloroethyl)ether 2600 08/27/15 DD SW8270Dug/Kg990 10NDBis(2-chloroisopropyl)ether 2600 08/27/15 DD SW8270Dug/Kg 11000 10NDBis(2-ethylhexyl)phthalate 2600 08/27/15 DD SW8270Dug/Kg1100 10

7300Carbazole 18000 08/27/15 DD SW8270Dug/Kg2800 10J16000Chrysene 2600 08/27/15 DD SW8270Dug/Kg1200 101300Dibenz(a,h)anthracene 2600 08/27/15 DD SW8270Dug/Kg1200 10J6300Dibenzofuran 2600 08/27/15 DD SW8270Dug/Kg1100 10NDDiethyl phthalate 2600 08/27/15 DD SW8270Dug/Kg1200 10NDDimethylphthalate 2600 08/27/15 DD SW8270Dug/Kg1100 10NDDi-n-butylphthalate 2600 08/27/15 DD SW8270Dug/Kg980 10NDDi-n-octylphthalate 2600 08/27/15 DD SW8270Dug/Kg950 10

47000Fluoranthene 2600 08/27/15 DD SW8270Dug/Kg1200 107500Fluorene 2600 08/27/15 DD SW8270Dug/Kg1200 10NDHexachlorobenzene 2600 08/27/15 DD SW8270Dug/Kg1100 10NDHexachlorobutadiene 2600 08/27/15 DD SW8270Dug/Kg1300 10NDHexachlorocyclopentadiene 2600 08/27/15 DD SW8270Dug/Kg1100 10NDHexachloroethane 2600 08/27/15 DD SW8270Dug/Kg1100 10

7200Indeno(1,2,3-cd)pyrene 2600 08/27/15 DD SW8270Dug/Kg1200 10NDIsophorone 2600 08/27/15 DD SW8270Dug/Kg1000 10

5000Naphthalene 2600 08/27/15 DD SW8270Dug/Kg1100 10NDNitrobenzene 2600 08/27/15 DD SW8270Dug/Kg1300 10NDN-Nitrosodimethylamine 2600 08/27/15 DD SW8270Dug/Kg1000 10NDN-Nitrosodi-n-propylamine 2600 08/27/15 DD SW8270Dug/Kg1200 10NDN-Nitrosodiphenylamine 2600 08/27/15 DD SW8270Dug/Kg1400 10NDPentachloronitrobenzene 2600 08/27/15 DD SW8270Dug/Kg1400 10NDPentachlorophenol 2600 08/27/15 DD SW8270Dug/Kg1400 10



QA/QC SurrogatesDiluted Out% 2,4,6-Tribromophenol 08/27/15 DD 30 - 130 %% 10Diluted Out% 2-Fluorobiphenyl 08/27/15 DD 30 - 130 %% 10Diluted Out% 2-Fluorophenol 08/27/15 DD 30 - 130 %% 10Diluted Out% Nitrobenzene-d5 08/27/15 DD 30 - 130 %% 10Diluted Out% Phenol-d5 08/27/15 DD 30 - 130 %% 10Diluted Out% Terphenyl-d14 08/27/15 DD 30 - 130 %% 10


14B1 (10-15)Phoenix I.D.: BJ81790



LOD/MDL Dilution

Comments:


This sample was not collected in accordance with EPA method 5035. NELAC requires the laboratory to qualify the volatile soil data as biased low.

Semi-Volatile Comment:Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, a dilution was required resulting in an elevated RL for the semivolatile analysis.











SOLIDEBC72 Hour


RB

Laboratory Data

14B3 (0-5)

Phoenix ID: BJ81791

08/26/1512:0017:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution







14B3 (0-5)Phoenix I.D.: BJ81791



LOD/MDL Dilution




Pesticides - SoilND4,4' -DDD 60 08/28/15 CE SW8081Bug/Kg60 10ND4,4' -DDE 11 08/28/15 CE SW8081Bug/Kg11 10ND4,4' -DDT 11 08/28/15 CE SW8081Bug/Kg11 10NDa-BHC 36 08/28/15 CE SW8081Bug/Kg36 10130a-Chlordane 18 08/28/15 CE SW8081Bug/Kg18 10NDAldrin 18 08/28/15 CE SW8081Bug/Kg18 10NDb-BHC 36 08/28/15 CE SW8081Bug/Kg36 10NRChlordane 180 08/28/15 CE SW8081Bug/Kg180 10NDd-BHC 36 08/28/15 CE SW8081Bug/Kg36 10NDDieldrin 18 08/28/15 CE SW8081Bug/Kg18 10NDEndosulfan I 36 08/28/15 CE SW8081Bug/Kg36 10NDEndosulfan II 36 08/28/15 CE SW8081Bug/Kg36 10NDEndosulfan sulfate 36 08/28/15 CE SW8081Bug/Kg36 10NDEndrin 36 08/28/15 CE SW8081Bug/Kg36 10NDEndrin aldehyde 36 08/28/15 CE SW8081Bug/Kg36 10NDEndrin ketone 36 08/28/15 CE SW8081Bug/Kg36 10NDg-BHC 7.2 08/28/15 CE SW8081Bug/Kg7.2 10160g-Chlordane 18 08/28/15 CE SW8081Bug/Kg18 10NDHeptachlor 36 08/28/15 CE SW8081Bug/Kg36 10NDHeptachlor epoxide 36 08/28/15 CE SW8081Bug/Kg36 10NDMethoxychlor 180 08/28/15 CE SW8081Bug/Kg180 10NDToxaphene 720 08/28/15 CE SW8081Bug/Kg720 10


VolatilesND1,1,1,2-Tetrachloroethane 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1ND1,1,1-Trichloroethane 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1ND1,1,2,2-Tetrachloroethane 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1ND1,1,2-Trichloroethane 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1ND1,1-Dichloroethane 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1


14B3 (0-5)Phoenix I.D.: BJ81791



LOD/MDL Dilution

ND1,1-Dichloroethene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1ND1,1-Dichloropropene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1ND1,2,3-Trichlorobenzene 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1ND1,2,3-Trichloropropane 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1ND1,2,4-Trichlorobenzene 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1ND1,2,4-Trimethylbenzene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1ND1,2-Dibromo-3-chloropropane 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1ND1,2-Dibromoethane 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1ND1,2-Dichlorobenzene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1ND1,2-Dichloroethane 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1ND1,2-Dichloropropane 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1ND1,3,5-Trimethylbenzene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1ND1,3-Dichlorobenzene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1ND1,3-Dichloropropane 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1ND1,4-Dichlorobenzene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1ND2,2-Dichloropropane 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1ND2-Chlorotoluene 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1ND2-Hexanone 29 08/31/15 JLI SW8260Cug/Kg5.8 1ND2-Isopropyltoluene 5.8 08/31/15 JLI SW8260Cug/Kg 10.58 1ND4-Chlorotoluene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1ND4-Methyl-2-pentanone 29 08/31/15 JLI SW8260Cug/Kg5.8 1NDAcetone 50 08/31/15 JLI SW8260Cug/Kg5.8 1NDAcrylonitrile 12 08/31/15 JLI SW8260Cug/Kg1.2 10.59Benzene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1JNDBromobenzene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1NDBromochloromethane 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1NDBromodichloromethane 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1NDBromoform 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1NDBromomethane 5.8 08/31/15 JLI SW8260Cug/Kg2.3 1NDCarbon Disulfide 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1NDCarbon tetrachloride 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1NDChlorobenzene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1NDChloroethane 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1NDChloroform 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1NDChloromethane 5.8 08/31/15 JLI SW8260Cug/Kg1.2 16.4cis-1,2-Dichloroethene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1NDcis-1,3-Dichloropropene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1NDDibromochloromethane 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1NDDibromomethane 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1NDDichlorodifluoromethane 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1NDEthylbenzene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1NDHexachlorobutadiene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1NDIsopropylbenzene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1NDm&p-Xylene 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1NDMethyl Ethyl Ketone 35 08/31/15 JLI SW8260Cug/Kg5.8 1NDMethyl t-butyl ether (MTBE) 12 08/31/15 JLI SW8260Cug/Kg1.2 1NDMethylene chloride 5.8 08/31/15 JLI SW8260Cug/Kg5.8 1NDNaphthalene 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1NDn-Butylbenzene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1


14B3 (0-5)Phoenix I.D.: BJ81791



LOD/MDL Dilution

NDn-Propylbenzene 5.8 08/31/15 JLI SW8260Cug/Kg1.0 1NDo-Xylene 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1NDp-Isopropyltoluene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1NDsec-Butylbenzene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1NDStyrene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1NDtert-Butylbenzene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1NDTetrachloroethene 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1NDTetrahydrofuran (THF) 12 08/31/15 JLI SW8260Cug/Kg 12.9 1NDToluene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1NDtrans-1,2-Dichloroethene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1NDtrans-1,3-Dichloropropene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1NDtrans-1,4-dichloro-2-butene 12 08/31/15 JLI SW8260Cug/Kg2.9 12.1Trichloroethene 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1JNDTrichlorofluoromethane 5.8 08/31/15 JLI SW8260Cug/Kg1.2 1NDTrichlorotrifluoroethane 5.8 08/31/15 JLI SW8260Cug/Kg0.58 12.2Vinyl chloride 5.8 08/31/15 JLI SW8260Cug/Kg0.58 1J





SemivolatilesND1,2,4,5-Tetrachlorobenzene 250 08/27/15 DD SW8270Dug/Kg130 1ND1,2,4-Trichlorobenzene 250 08/27/15 DD SW8270Dug/Kg110 1ND1,2-Dichlorobenzene 250 08/27/15 DD SW8270Dug/Kg100 1ND1,2-Diphenylhydrazine 250 08/27/15 DD SW8270Dug/Kg120 1ND1,3-Dichlorobenzene 250 08/27/15 DD SW8270Dug/Kg110 1ND1,4-Dichlorobenzene 250 08/27/15 DD SW8270Dug/Kg110 1ND2,4,5-Trichlorophenol 250 08/27/15 DD SW8270Dug/Kg200 1ND2,4,6-Trichlorophenol 250 08/27/15 DD SW8270Dug/Kg110 1ND2,4-Dichlorophenol 250 08/27/15 DD SW8270Dug/Kg130 1ND2,4-Dimethylphenol 250 08/27/15 DD SW8270Dug/Kg89 1ND2,4-Dinitrophenol 710 08/27/15 DD SW8270Dug/Kg250 1ND2,4-Dinitrotoluene 250 08/27/15 DD SW8270Dug/Kg140 1ND2,6-Dinitrotoluene 250 08/27/15 DD SW8270Dug/Kg110 1ND2-Chloronaphthalene 250 08/27/15 DD SW8270Dug/Kg100 1


14B3 (0-5)Phoenix I.D.: BJ81791



LOD/MDL Dilution

ND2-Chlorophenol 250 08/27/15 DD SW8270Dug/Kg100 1ND2-Methylnaphthalene 250 08/27/15 DD SW8270Dug/Kg110 1ND2-Methylphenol (o-cresol) 250 08/27/15 DD SW8270Dug/Kg170 1ND2-Nitroaniline 710 08/27/15 DD SW8270Dug/Kg360 1ND2-Nitrophenol 250 08/27/15 DD SW8270Dug/Kg230 1ND3&4-Methylphenol (m&p-cresol) 250 08/27/15 DD SW8270Dug/Kg 1140 1ND3,3'-Dichlorobenzidine 710 08/27/15 DD SW8270Dug/Kg170 1ND3-Nitroaniline 710 08/27/15 DD SW8270Dug/Kg710 1ND4,6-Dinitro-2-methylphenol 1800 08/27/15 DD SW8270Dug/Kg380 1ND4-Bromophenyl phenyl ether 250 08/27/15 DD SW8270Dug/Kg110 1ND4-Chloro-3-methylphenol 250 08/27/15 DD SW8270Dug/Kg130 1ND4-Chloroaniline 290 08/27/15 DD SW8270Dug/Kg170 1ND4-Chlorophenyl phenyl ether 250 08/27/15 DD SW8270Dug/Kg120 1ND4-Nitroaniline 710 08/27/15 DD SW8270Dug/Kg120 1ND4-Nitrophenol 360 08/27/15 DD SW8270Dug/Kg160 1NDAcenaphthene 250 08/27/15 DD SW8270Dug/Kg110 1NDAcenaphthylene 250 08/27/15 DD SW8270Dug/Kg100 1NDAcetophenone 250 08/27/15 DD SW8270Dug/Kg110 1NDAniline 290 08/27/15 DD SW8270Dug/Kg290 1150Anthracene 250 08/27/15 DD SW8270Dug/Kg120 1J750Benz(a)anthracene 250 08/27/15 DD SW8270Dug/Kg120 1NDBenzidine 710 08/27/15 DD SW8270Dug/Kg210 1

1000Benzo(a)pyrene 250 08/27/15 DD SW8270Dug/Kg120 1660Benzo(b)fluoranthene 250 08/27/15 DD SW8270Dug/Kg120 1530Benzo(ghi)perylene 250 08/27/15 DD SW8270Dug/Kg120 1850Benzo(k)fluoranthene 250 08/27/15 DD SW8270Dug/Kg120 1NDBenzoic acid 1800 08/27/15 DD SW8270Dug/Kg 1710 1NDBenzyl butyl phthalate 250 08/27/15 DD SW8270Dug/Kg92 1NDBis(2-chloroethoxy)methane 250 08/27/15 DD SW8270Dug/Kg99 1NDBis(2-chloroethyl)ether 250 08/27/15 DD SW8270Dug/Kg96 1NDBis(2-chloroisopropyl)ether 250 08/27/15 DD SW8270Dug/Kg 199 1NDBis(2-ethylhexyl)phthalate 250 08/27/15 DD SW8270Dug/Kg100 1NDCarbazole 1800 08/27/15 DD SW8270Dug/Kg270 1690Chrysene 250 08/27/15 DD SW8270Dug/Kg120 1180Dibenz(a,h)anthracene 250 08/27/15 DD SW8270Dug/Kg120 1JNDDibenzofuran 250 08/27/15 DD SW8270Dug/Kg100 1NDDiethyl phthalate 250 08/27/15 DD SW8270Dug/Kg110 1NDDimethylphthalate 250 08/27/15 DD SW8270Dug/Kg110 1NDDi-n-butylphthalate 250 08/27/15 DD SW8270Dug/Kg95 1NDDi-n-octylphthalate 250 08/27/15 DD SW8270Dug/Kg92 1860Fluoranthene 250 08/27/15 DD SW8270Dug/Kg120 1NDFluorene 250 08/27/15 DD SW8270Dug/Kg120 1NDHexachlorobenzene 250 08/27/15 DD SW8270Dug/Kg100 1NDHexachlorobutadiene 250 08/27/15 DD SW8270Dug/Kg130 1NDHexachlorocyclopentadiene 250 08/27/15 DD SW8270Dug/Kg110 1NDHexachloroethane 250 08/27/15 DD SW8270Dug/Kg110 1600Indeno(1,2,3-cd)pyrene 250 08/27/15 DD SW8270Dug/Kg120 1NDIsophorone 250 08/27/15 DD SW8270Dug/Kg100 1NDNaphthalene 250 08/27/15 DD SW8270Dug/Kg100 1


14B3 (0-5)Phoenix I.D.: BJ81791



LOD/MDL Dilution

NDNitrobenzene 250 08/27/15 DD SW8270Dug/Kg130 1NDN-Nitrosodimethylamine 250 08/27/15 DD SW8270Dug/Kg100 1NDN-Nitrosodi-n-propylamine 250 08/27/15 DD SW8270Dug/Kg120 1NDN-Nitrosodiphenylamine 250 08/27/15 DD SW8270Dug/Kg140 1NDPentachloronitrobenzene 250 08/27/15 DD SW8270Dug/Kg130 1NDPentachlorophenol 250 08/27/15 DD SW8270Dug/Kg140 1440Phenanthrene 250 08/27/15 DD SW8270Dug/Kg100 1NDPhenol 250 08/27/15 DD SW8270Dug/Kg110 1780Pyrene 250 08/27/15 DD SW8270Dug/Kg120 1NDPyridine 250 08/27/15 DD SW8270Dug/Kg88 1


Comments:



Pesticide Comment:Sample was evaluated against an external standard.Due to the presence of Chlordane in the sample, an elevated RL was reported.










SOLIDEBC72 Hour


RB

Laboratory Data

14B3 (10-15)

Phoenix ID: BJ81792

08/26/1512:1517:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution


VolatilesND1,1,1,2-Tetrachloroethane 300 08/30/15 JLI SW8260Cug/Kg60 50ND1,1,1-Trichloroethane 300 08/30/15 JLI SW8260Cug/Kg30 50ND1,1,2,2-Tetrachloroethane 300 08/30/15 JLI SW8260Cug/Kg60 50ND1,1,2-Trichloroethane 300 08/30/15 JLI SW8260Cug/Kg60 50ND1,1-Dichloroethane 250 08/30/15 JLI SW8260Cug/Kg60 50ND1,1-Dichloroethene 300 08/30/15 JLI SW8260Cug/Kg30 50ND1,1-Dichloropropene 300 08/30/15 JLI SW8260Cug/Kg30 50ND1,2,3-Trichlorobenzene 300 08/30/15 JLI SW8260Cug/Kg60 50ND1,2,3-Trichloropropane 300 08/30/15 JLI SW8260Cug/Kg30 50ND1,2,4-Trichlorobenzene 300 08/30/15 JLI SW8260Cug/Kg60 50

140001,2,4-Trimethylbenzene 3000 08/31/15 JLI SW8260Cug/Kg300 500DND1,2-Dibromo-3-chloropropane 300 08/30/15 JLI SW8260Cug/Kg60 50ND1,2-Dibromoethane 300 08/30/15 JLI SW8260Cug/Kg30 50ND1,2-Dichlorobenzene 300 08/30/15 JLI SW8260Cug/Kg30 50ND1,2-Dichloroethane 300 08/30/15 JLI SW8260Cug/Kg30 50ND1,2-Dichloropropane 300 08/30/15 JLI SW8260Cug/Kg60 50

96001,3,5-Trimethylbenzene 300 08/30/15 JLI SW8260Cug/Kg30 50ND1,3-Dichlorobenzene 300 08/30/15 JLI SW8260Cug/Kg30 50ND1,3-Dichloropropane 300 08/30/15 JLI SW8260Cug/Kg60 50ND1,4-Dichlorobenzene 300 08/30/15 JLI SW8260Cug/Kg30 50ND2,2-Dichloropropane 300 08/30/15 JLI SW8260Cug/Kg30 50ND2-Chlorotoluene 300 08/30/15 JLI SW8260Cug/Kg60 50ND2-Hexanone 1500 08/30/15 JLI SW8260Cug/Kg300 50


14B3 (10-15)Phoenix I.D.: BJ81792



LOD/MDL Dilution

ND2-Isopropyltoluene 300 08/30/15 JLI SW8260Cug/Kg 130 50ND4-Chlorotoluene 300 08/30/15 JLI SW8260Cug/Kg30 50ND4-Methyl-2-pentanone 1500 08/30/15 JLI SW8260Cug/Kg300 50NDAcetone 3000 08/30/15 JLI SW8260Cug/Kg300 50NDAcrylonitrile 600 08/30/15 JLI SW8260Cug/Kg60 50

4100Benzene 3000 08/31/15 JLI SW8260Cug/Kg300 500DNDBromobenzene 300 08/30/15 JLI SW8260Cug/Kg30 50NDBromochloromethane 300 08/30/15 JLI SW8260Cug/Kg30 50NDBromodichloromethane 300 08/30/15 JLI SW8260Cug/Kg60 50NDBromoform 300 08/30/15 JLI SW8260Cug/Kg60 50NDBromomethane 300 08/30/15 JLI SW8260Cug/Kg120 50NDCarbon Disulfide 300 08/30/15 JLI SW8260Cug/Kg60 50NDCarbon tetrachloride 300 08/30/15 JLI SW8260Cug/Kg60 50NDChlorobenzene 300 08/30/15 JLI SW8260Cug/Kg30 50NDChloroethane 300 08/30/15 JLI SW8260Cug/Kg30 50NDChloroform 300 08/30/15 JLI SW8260Cug/Kg30 50NDChloromethane 300 08/30/15 JLI SW8260Cug/Kg60 50870cis-1,2-Dichloroethene 300 08/30/15 JLI SW8260Cug/Kg30 50NDcis-1,3-Dichloropropene 300 08/30/15 JLI SW8260Cug/Kg30 50NDDibromochloromethane 300 08/30/15 JLI SW8260Cug/Kg60 50NDDibromomethane 300 08/30/15 JLI SW8260Cug/Kg60 50NDDichlorodifluoromethane 300 08/30/15 JLI SW8260Cug/Kg30 50

7000Ethylbenzene 300 08/30/15 JLI SW8260Cug/Kg30 50NDHexachlorobutadiene 300 08/30/15 JLI SW8260Cug/Kg30 50300Isopropylbenzene 300 08/30/15 JLI SW8260Cug/Kg30 50J

17000m&p-Xylene 3000 08/31/15 JLI SW8260Cug/Kg600 500DNDMethyl Ethyl Ketone 1800 08/30/15 JLI SW8260Cug/Kg300 50NDMethyl t-butyl ether (MTBE) 600 08/30/15 JLI SW8260Cug/Kg60 50NDMethylene chloride 300 08/30/15 JLI SW8260Cug/Kg300 50

300000Naphthalene 30000 08/31/15 JLI SW8260Cug/Kg6000 5000DNDn-Butylbenzene 300 08/30/15 JLI SW8260Cug/Kg30 50190n-Propylbenzene 300 08/30/15 JLI SW8260Cug/Kg54 50J

9200o-Xylene 3000 08/31/15 JLI SW8260Cug/Kg600 500D440p-Isopropyltoluene 300 08/30/15 JLI SW8260Cug/Kg30 50NDsec-Butylbenzene 300 08/30/15 JLI SW8260Cug/Kg30 50

1000Styrene 300 08/30/15 JLI SW8260Cug/Kg30 50NDtert-Butylbenzene 300 08/30/15 JLI SW8260Cug/Kg30 50NDTetrachloroethene 300 08/30/15 JLI SW8260Cug/Kg60 50NDTetrahydrofuran (THF) 600 08/30/15 JLI SW8260Cug/Kg 1150 50

8600Toluene 3000 08/31/15 JLI SW8260Cug/Kg300 500D33trans-1,2-Dichloroethene 150 08/30/15 JLI SW8260Cug/Kg30 50JNDtrans-1,3-Dichloropropene 300 08/30/15 JLI SW8260Cug/Kg30 50NDtrans-1,4-dichloro-2-butene 600 08/30/15 JLI SW8260Cug/Kg150 50

3300Trichloroethene 300 08/30/15 JLI SW8260Cug/Kg30 50NDTrichlorofluoromethane 300 08/30/15 JLI SW8260Cug/Kg60 50NDTrichlorotrifluoroethane 300 08/30/15 JLI SW8260Cug/Kg30 50290Vinyl chloride 250 08/30/15 JLI SW8260Cug/Kg30 50



14B3 (10-15)Phoenix I.D.: BJ81792



LOD/MDL Dilution




VolatilesND1,1,1,2-Tetrachloroethane 1200 08/30/15 JLI SW8260Cug/Kg60 50NDAcrolein 1200 08/30/15 JLI SW8260Cug/Kg150 50NDAcrylonitrile 1200 08/30/15 JLI SW8260Cug/Kg30 50NDTert-butyl alcohol 6000 08/30/15 JLI SW8260Cug/Kg1200 50



14B3 (10-15)Phoenix I.D.: BJ81792



LOD/MDL Dilution

NDAniline 290 08/27/15 DD SW8270Dug/Kg290 1NDAnthracene 260 08/27/15 DD SW8270Dug/Kg120 1490Benz(a)anthracene 260 08/27/15 DD SW8270Dug/Kg120 1NDBenzidine 730 08/27/15 DD SW8270Dug/Kg220 1700Benzo(a)pyrene 260 08/27/15 DD SW8270Dug/Kg120 1510Benzo(b)fluoranthene 260 08/27/15 DD SW8270Dug/Kg130 1370Benzo(ghi)perylene 260 08/27/15 DD SW8270Dug/Kg120 1520Benzo(k)fluoranthene 260 08/27/15 DD SW8270Dug/Kg120 1NDBenzoic acid 1800 08/27/15 DD SW8270Dug/Kg 1730 1NDBenzyl butyl phthalate 260 08/27/15 DD SW8270Dug/Kg95 1NDBis(2-chloroethoxy)methane 260 08/27/15 DD SW8270Dug/Kg100 1NDBis(2-chloroethyl)ether 260 08/27/15 DD SW8270Dug/Kg99 1NDBis(2-chloroisopropyl)ether 260 08/27/15 DD SW8270Dug/Kg 1100 1NDBis(2-ethylhexyl)phthalate 260 08/27/15 DD SW8270Dug/Kg110 1NDCarbazole 1800 08/27/15 DD SW8270Dug/Kg280 1470Chrysene 260 08/27/15 DD SW8270Dug/Kg120 1NDDibenz(a,h)anthracene 260 08/27/15 DD SW8270Dug/Kg120 1NDDibenzofuran 260 08/27/15 DD SW8270Dug/Kg110 1NDDiethyl phthalate 260 08/27/15 DD SW8270Dug/Kg120 1NDDimethylphthalate 260 08/27/15 DD SW8270Dug/Kg110 1NDDi-n-butylphthalate 260 08/27/15 DD SW8270Dug/Kg98 1NDDi-n-octylphthalate 260 08/27/15 DD SW8270Dug/Kg95 1570Fluoranthene 260 08/27/15 DD SW8270Dug/Kg120 1NDFluorene 260 08/27/15 DD SW8270Dug/Kg120 1NDHexachlorobenzene 260 08/27/15 DD SW8270Dug/Kg110 1NDHexachlorobutadiene 260 08/27/15 DD SW8270Dug/Kg130 1NDHexachlorocyclopentadiene 260 08/27/15 DD SW8270Dug/Kg110 1NDHexachloroethane 260 08/27/15 DD SW8270Dug/Kg110 1410Indeno(1,2,3-cd)pyrene 260 08/27/15 DD SW8270Dug/Kg120 1NDIsophorone 260 08/27/15 DD SW8270Dug/Kg100 1NDNaphthalene 260 08/27/15 DD SW8270Dug/Kg110 1NDNitrobenzene 260 08/27/15 DD SW8270Dug/Kg130 1NDN-Nitrosodimethylamine 260 08/27/15 DD SW8270Dug/Kg100 1NDN-Nitrosodi-n-propylamine 260 08/27/15 DD SW8270Dug/Kg120 1NDN-Nitrosodiphenylamine 260 08/27/15 DD SW8270Dug/Kg140 1NDPentachloronitrobenzene 260 08/27/15 DD SW8270Dug/Kg140 1NDPentachlorophenol 260 08/27/15 DD SW8270Dug/Kg140 1360Phenanthrene 260 08/27/15 DD SW8270Dug/Kg100 1NDPhenol 260 08/27/15 DD SW8270Dug/Kg120 1540Pyrene 260 08/27/15 DD SW8270Dug/Kg130 1NDPyridine 260 08/27/15 DD SW8270Dug/Kg90 1



14B3 (10-15)Phoenix I.D.: BJ81792



LOD/MDL Dilution

Comments:


Volatile Comment:Elevated reporting limits for volatiles due to the presence of target and/or non-target compounds.










SOLIDEBC72 Hour


RB

Laboratory Data

14B3 (15-18)

Phoenix ID: BJ81793

08/26/1512:3017:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution


72.0Barium 0.8 08/28/15 LK SW6010Cmg/Kg0.42 10.44Beryllium 0.33 08/28/15 LK SW6010Cmg/Kg0.17 1

27000Calcium 42 08/28/15 LK SW6010Cmg/Kg38 100.21Cadmium 0.42 08/28/15 LK SW6010Cmg/Kg0.17 1B6.86Cobalt 0.42 08/28/15 LK SW6010Cmg/Kg0.42 114.1Chromium 0.42 08/28/15 LK SW6010Cmg/Kg0.42 120.5Copper 0.42 08/28/15 LK SW6010Cmg/kg0.42 1

19600Iron 42 08/28/15 LK SW6010Cmg/Kg B42 100.41Mercury 0.03 08/27/15 RS SW7471Bmg/Kg0.02 11670Potassium 8 08/28/15 LK SW6010Cmg/Kg3.2 1N3490Magnesium 4.2 08/28/15 LK SW6010Cmg/Kg4.2 1521Manganese 4.2 08/28/15 LK SW6010Cmg/Kg4.2 10548Sodium 8 08/28/15 LK SW6010Cmg/Kg3.6 1N14.1Nickel 0.42 08/28/15 LK SW6010Cmg/Kg0.42 1121Lead 0.8 08/28/15 LK SW6010Cmg/Kg0.42 1




14B3 (15-18)Phoenix I.D.: BJ81793



LOD/MDL Dilution




Pesticides - SoilND4,4' -DDD 20 09/03/15 CE SW8081Bug/Kg20 20ND4,4' -DDE 20 09/03/15 CE SW8081Bug/Kg20 20ND4,4' -DDT 25 09/03/15 CE SW8081Bug/Kg25 20NDa-BHC 41 09/03/15 CE SW8081Bug/Kg41 20NDa-Chlordane 41 09/03/15 CE SW8081Bug/Kg41 20NDAldrin 12 09/03/15 CE SW8081Bug/Kg12 20NDb-BHC 41 09/03/15 CE SW8081Bug/Kg41 20NDd-BHC 41 09/03/15 CE SW8081Bug/Kg41 20NDDieldrin 12 09/03/15 CE SW8081Bug/Kg12 20NDEndosulfan I 82 09/03/15 CE SW8081Bug/Kg82 20NDEndosulfan II 20 09/03/15 CE SW8081Bug/Kg20 20NDEndosulfan sulfate 82 09/03/15 CE SW8081Bug/Kg82 20NDEndrin 41 09/03/15 CE SW8081Bug/Kg41 20NDEndrin aldehyde 82 09/03/15 CE SW8081Bug/Kg82 20NDEndrin ketone 82 09/03/15 CE SW8081Bug/Kg82 20NDg-BHC 16 09/03/15 CE SW8081Bug/Kg16 20NDg-Chlordane 41 09/03/15 CE SW8081Bug/Kg41 20NDHeptachlor 41 09/03/15 CE SW8081Bug/Kg41 20NDHeptachlor epoxide 41 09/03/15 CE SW8081Bug/Kg41 20NDMethoxychlor 410 09/03/15 CE SW8081Bug/Kg410 20NDToxaphene 1600 09/03/15 CE SW8081Bug/Kg1600 20


VolatilesND1,1,1,2-Tetrachloroethane 700 08/31/15 JLI SW8260Cug/Kg140 50ND1,1,1-Trichloroethane 700 08/31/15 JLI SW8260Cug/Kg70 50ND1,1,2,2-Tetrachloroethane 700 08/31/15 JLI SW8260Cug/Kg140 50ND1,1,2-Trichloroethane 700 08/31/15 JLI SW8260Cug/Kg140 50ND1,1-Dichloroethane 250 08/31/15 JLI SW8260Cug/Kg140 50ND1,1-Dichloroethene 250 08/31/15 JLI SW8260Cug/Kg70 50


14B3 (15-18)Phoenix I.D.: BJ81793



LOD/MDL Dilution

ND1,1-Dichloropropene 700 08/31/15 JLI SW8260Cug/Kg70 50ND1,2,3-Trichlorobenzene 700 08/31/15 JLI SW8260Cug/Kg140 50ND1,2,3-Trichloropropane 700 08/31/15 JLI SW8260Cug/Kg70 50ND1,2,4-Trichlorobenzene 700 08/31/15 JLI SW8260Cug/Kg140 502401,2,4-Trimethylbenzene 700 08/31/15 JLI SW8260Cug/Kg70 50JND1,2-Dibromo-3-chloropropane 700 08/31/15 JLI SW8260Cug/Kg140 50ND1,2-Dibromoethane 700 08/31/15 JLI SW8260Cug/Kg70 50ND1,2-Dichlorobenzene 700 08/31/15 JLI SW8260Cug/Kg70 50ND1,2-Dichloroethane 700 08/31/15 JLI SW8260Cug/Kg70 50ND1,2-Dichloropropane 700 08/31/15 JLI SW8260Cug/Kg140 50891,3,5-Trimethylbenzene 700 08/31/15 JLI SW8260Cug/Kg70 50JND1,3-Dichlorobenzene 700 08/31/15 JLI SW8260Cug/Kg70 50ND1,3-Dichloropropane 700 08/31/15 JLI SW8260Cug/Kg140 50ND1,4-Dichlorobenzene 700 08/31/15 JLI SW8260Cug/Kg70 50ND2,2-Dichloropropane 700 08/31/15 JLI SW8260Cug/Kg70 50ND2-Chlorotoluene 700 08/31/15 JLI SW8260Cug/Kg140 50ND2-Hexanone 3500 08/31/15 JLI SW8260Cug/Kg700 50ND2-Isopropyltoluene 700 08/31/15 JLI SW8260Cug/Kg 170 50ND4-Chlorotoluene 700 08/31/15 JLI SW8260Cug/Kg70 50ND4-Methyl-2-pentanone 3500 08/31/15 JLI SW8260Cug/Kg700 50NDAcetone 7000 08/31/15 JLI SW8260Cug/Kg700 50NDAcrylonitrile 1400 08/31/15 JLI SW8260Cug/Kg140 50

2800Benzene 700 08/31/15 JLI SW8260Cug/Kg70 50NDBromobenzene 700 08/31/15 JLI SW8260Cug/Kg70 50NDBromochloromethane 700 08/31/15 JLI SW8260Cug/Kg70 50NDBromodichloromethane 700 08/31/15 JLI SW8260Cug/Kg140 50NDBromoform 700 08/31/15 JLI SW8260Cug/Kg140 50NDBromomethane 700 08/31/15 JLI SW8260Cug/Kg280 50NDCarbon Disulfide 700 08/31/15 JLI SW8260Cug/Kg140 50NDCarbon tetrachloride 700 08/31/15 JLI SW8260Cug/Kg140 50NDChlorobenzene 700 08/31/15 JLI SW8260Cug/Kg70 50NDChloroethane 700 08/31/15 JLI SW8260Cug/Kg70 50NDChloroform 250 08/31/15 JLI SW8260Cug/Kg70 50NDChloromethane 700 08/31/15 JLI SW8260Cug/Kg140 50

7600cis-1,2-Dichloroethene 700 08/31/15 JLI SW8260Cug/Kg70 50NDcis-1,3-Dichloropropene 700 08/31/15 JLI SW8260Cug/Kg70 50NDDibromochloromethane 700 08/31/15 JLI SW8260Cug/Kg140 50NDDibromomethane 700 08/31/15 JLI SW8260Cug/Kg140 50NDDichlorodifluoromethane 700 08/31/15 JLI SW8260Cug/Kg70 50640Ethylbenzene 700 08/31/15 JLI SW8260Cug/Kg70 50JNDHexachlorobutadiene 700 08/31/15 JLI SW8260Cug/Kg70 50NDIsopropylbenzene 700 08/31/15 JLI SW8260Cug/Kg70 50820m&p-Xylene 700 08/31/15 JLI SW8260Cug/Kg140 50NDMethyl Ethyl Ketone 4200 08/31/15 JLI SW8260Cug/Kg700 50NDMethyl t-butyl ether (MTBE) 700 08/31/15 JLI SW8260Cug/Kg140 50NDMethylene chloride 700 08/31/15 JLI SW8260Cug/Kg700 50

6500Naphthalene 700 08/31/15 JLI SW8260Cug/Kg140 50NDn-Butylbenzene 700 08/31/15 JLI SW8260Cug/Kg70 50NDn-Propylbenzene 700 08/31/15 JLI SW8260Cug/Kg130 50


14B3 (15-18)Phoenix I.D.: BJ81793



LOD/MDL Dilution

230o-Xylene 700 08/31/15 JLI SW8260Cug/Kg140 50JNDp-Isopropyltoluene 700 08/31/15 JLI SW8260Cug/Kg70 50NDsec-Butylbenzene 700 08/31/15 JLI SW8260Cug/Kg70 50NDStyrene 700 08/31/15 JLI SW8260Cug/Kg70 50NDtert-Butylbenzene 700 08/31/15 JLI SW8260Cug/Kg70 50NDTetrachloroethene 700 08/31/15 JLI SW8260Cug/Kg140 50NDTetrahydrofuran (THF) 1400 08/31/15 JLI SW8260Cug/Kg 1350 50290Toluene 700 08/31/15 JLI SW8260Cug/Kg70 50J160trans-1,2-Dichloroethene 150 08/31/15 JLI SW8260Cug/Kg70 50JNDtrans-1,3-Dichloropropene 700 08/31/15 JLI SW8260Cug/Kg70 50NDtrans-1,4-dichloro-2-butene 1400 08/31/15 JLI SW8260Cug/Kg350 50

3700Trichloroethene 700 08/31/15 JLI SW8260Cug/Kg70 50NDTrichlorofluoromethane 700 08/31/15 JLI SW8260Cug/Kg140 50NDTrichlorotrifluoroethane 700 08/31/15 JLI SW8260Cug/Kg70 50

2600Vinyl chloride 700 08/31/15 JLI SW8260Cug/Kg70 50







14B3 (15-18)Phoenix I.D.: BJ81793



LOD/MDL Dilution

190002-Methylnaphthalene 2900 08/27/15 DD SW8270Dug/Kg1200 10ND2-Methylphenol (o-cresol) 2900 08/27/15 DD SW8270Dug/Kg1900 10ND2-Nitroaniline 8300 08/27/15 DD SW8270Dug/Kg4200 10ND2-Nitrophenol 2900 08/27/15 DD SW8270Dug/Kg2600 10ND3&4-Methylphenol (m&p-cresol) 2900 08/27/15 DD SW8270Dug/Kg 11600 10ND3,3'-Dichlorobenzidine 8300 08/27/15 DD SW8270Dug/Kg2000 10ND3-Nitroaniline 8300 08/27/15 DD SW8270Dug/Kg8300 10ND4,6-Dinitro-2-methylphenol 21000 08/27/15 DD SW8270Dug/Kg4500 10ND4-Bromophenyl phenyl ether 2900 08/27/15 DD SW8270Dug/Kg1200 10ND4-Chloro-3-methylphenol 2900 08/27/15 DD SW8270Dug/Kg1500 10ND4-Chloroaniline 3300 08/27/15 DD SW8270Dug/Kg1900 10ND4-Chlorophenyl phenyl ether 2900 08/27/15 DD SW8270Dug/Kg1400 10ND4-Nitroaniline 8300 08/27/15 DD SW8270Dug/Kg1400 10ND4-Nitrophenol 4100 08/27/15 DD SW8270Dug/Kg1900 10

2900Acenaphthene 2900 08/27/15 DD SW8270Dug/Kg1300 108400Acenaphthylene 2900 08/27/15 DD SW8270Dug/Kg1200 10NDAcetophenone 2900 08/27/15 DD SW8270Dug/Kg1300 10NDAniline 3300 08/27/15 DD SW8270Dug/Kg3300 10

16000Anthracene 2900 08/27/15 DD SW8270Dug/Kg1400 1014000Benz(a)anthracene 2900 08/27/15 DD SW8270Dug/Kg1400 10



5700Carbazole 21000 08/27/15 DD SW8270Dug/Kg3100 10J13000Chrysene 2900 08/27/15 DD SW8270Dug/Kg1400 102000Dibenz(a,h)anthracene 2900 08/27/15 DD SW8270Dug/Kg1300 10J12000Dibenzofuran 2900 08/27/15 DD SW8270Dug/Kg1200 10

NDDiethyl phthalate 2900 08/27/15 DD SW8270Dug/Kg1300 10NDDimethylphthalate 2900 08/27/15 DD SW8270Dug/Kg1300 10NDDi-n-butylphthalate 2900 08/27/15 DD SW8270Dug/Kg1100 10NDDi-n-octylphthalate 2900 08/27/15 DD SW8270Dug/Kg1100 10

25000Fluoranthene 2900 08/27/15 DD SW8270Dug/Kg1300 1018000Fluorene 2900 08/27/15 DD SW8270Dug/Kg1400 10

NDHexachlorobenzene 2900 08/27/15 DD SW8270Dug/Kg1200 10NDHexachlorobutadiene 2900 08/27/15 DD SW8270Dug/Kg1500 10NDHexachlorocyclopentadiene 2900 08/27/15 DD SW8270Dug/Kg1300 10NDHexachloroethane 2900 08/27/15 DD SW8270Dug/Kg1200 10


43000Naphthalene 2900 08/27/15 DD SW8270Dug/Kg1200 10NDNitrobenzene 2900 08/27/15 DD SW8270Dug/Kg1400 10


14B3 (15-18)Phoenix I.D.: BJ81793



LOD/MDL Dilution





Comments:















SOLIDEBC72 Hour


RB

Laboratory Data

14B6 (0-5)

Phoenix ID: BJ81794

08/26/1512:4517:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution




10500Iron 32 08/28/15 LK SW6010Cmg/Kg B32 100.08Mercury 0.03 08/27/15 RS SW7471Bmg/Kg0.02 1790Potassium 6 08/28/15 LK SW6010Cmg/Kg2.5 1N

1960Magnesium 3.2 08/28/15 LK SW6010Cmg/Kg3.2 1184Manganese 3.2 08/28/15 LK SW6010Cmg/Kg3.2 10164Sodium 6 08/28/15 LK SW6010Cmg/Kg2.8 1N12.3Nickel 0.32 08/28/15 LK SW6010Cmg/Kg0.32 146.4Lead 0.6 08/28/15 LK SW6010Cmg/Kg0.32 1< 1.6Antimony 1.6 08/28/15 LK SW6010Cmg/Kg1.6 1N< 1.3Selenium 1.3 08/28/15 LK SW6010Cmg/Kg1.1 1< 1.3Thallium 1.3 08/28/15 LK SW6010Cmg/Kg1.3 119.9Vanadium 0.3 08/28/15 LK SW6010Cmg/Kg0.32 156.6Zinc 0.6 08/28/15 LK SW6010Cmg/Kg B0.32 193Percent Solid 08/26/15 I SW846-%Solid%



14B6 (0-5)Phoenix I.D.: BJ81794



LOD/MDL Dilution








14B6 (0-5)Phoenix I.D.: BJ81794



LOD/MDL Dilution

ND1,1-Dichloropropene 5.2 08/31/15 JLI SW8260Cug/Kg0.52 1ND1,2,3-Trichlorobenzene 270 08/31/15 JLI SW8260Cug/Kg54 50ND1,2,3-Trichloropropane 270 08/31/15 JLI SW8260Cug/Kg27 50ND1,2,4-Trichlorobenzene 270 08/31/15 JLI SW8260Cug/Kg54 50ND1,2,4-Trimethylbenzene 270 08/31/15 JLI SW8260Cug/Kg27 50ND1,2-Dibromo-3-chloropropane 270 08/31/15 JLI SW8260Cug/Kg54 50ND1,2-Dibromoethane 5.2 08/31/15 JLI SW8260Cug/Kg0.52 1ND1,2-Dichlorobenzene 270 08/31/15 JLI SW8260Cug/Kg27 50ND1,2-Dichloroethane 5.2 08/31/15 JLI SW8260Cug/Kg0.52 1ND1,2-Dichloropropane 5.2 08/31/15 JLI SW8260Cug/Kg1.0 1ND1,3,5-Trimethylbenzene 270 08/31/15 JLI SW8260Cug/Kg27 50ND1,3-Dichlorobenzene 270 08/31/15 JLI SW8260Cug/Kg27 50ND1,3-Dichloropropane 5.2 08/31/15 JLI SW8260Cug/Kg1.0 1ND1,4-Dichlorobenzene 270 08/31/15 JLI SW8260Cug/Kg27 50ND2,2-Dichloropropane 5.2 08/31/15 JLI SW8260Cug/Kg0.52 1ND2-Chlorotoluene 270 08/31/15 JLI SW8260Cug/Kg54 50ND2-Hexanone 26 08/31/15 JLI SW8260Cug/Kg5.2 1ND2-Isopropyltoluene 270 08/31/15 JLI SW8260Cug/Kg 127 50ND4-Chlorotoluene 270 08/31/15 JLI SW8260Cug/Kg27 50ND4-Methyl-2-pentanone 26 08/31/15 JLI SW8260Cug/Kg5.2 17.6Acetone 50 08/31/15 JLI SW8260Cug/Kg5.2 1JSNDAcrylonitrile 10 08/31/15 JLI SW8260Cug/Kg1.0 1NDBenzene 5.2 08/31/15 JLI SW8260Cug/Kg0.52 1NDBromobenzene 270 08/31/15 JLI SW8260Cug/Kg27 50NDBromochloromethane 5.2 08/31/15 JLI SW8260Cug/Kg0.52 1NDBromodichloromethane 5.2 08/31/15 JLI SW8260Cug/Kg1.0 1NDBromoform 5.2 08/31/15 JLI SW8260Cug/Kg1.0 1NDBromomethane 5.2 08/31/15 JLI SW8260Cug/Kg2.1 1NDCarbon Disulfide 5.2 08/31/15 JLI SW8260Cug/Kg1.0 1NDCarbon tetrachloride 5.2 08/31/15 JLI SW8260Cug/Kg1.0 1NDChlorobenzene 5.2 08/31/15 JLI SW8260Cug/Kg0.52 1NDChloroethane 5.2 08/31/15 JLI SW8260Cug/Kg0.52 1NDChloroform 5.2 08/31/15 JLI SW8260Cug/Kg0.52 1NDChloromethane 5.2 08/31/15 JLI SW8260Cug/Kg1.0 10.92cis-1,2-Dichloroethene 5.2 08/31/15 JLI SW8260Cug/Kg0.52 1JNDcis-1,3-Dichloropropene 5.2 08/31/15 JLI SW8260Cug/Kg0.52 1NDDibromochloromethane 5.2 08/31/15 JLI SW8260Cug/Kg1.0 1NDDibromomethane 5.2 08/31/15 JLI SW8260Cug/Kg1.0 1NDDichlorodifluoromethane 5.2 08/31/15 JLI SW8260Cug/Kg0.52 1NDEthylbenzene 5.2 08/31/15 JLI SW8260Cug/Kg0.52 1NDHexachlorobutadiene 270 08/31/15 JLI SW8260Cug/Kg27 50NDIsopropylbenzene 270 08/31/15 JLI SW8260Cug/Kg27 50NDm&p-Xylene 5.2 08/31/15 JLI SW8260Cug/Kg1.0 1NDMethyl Ethyl Ketone 31 08/31/15 JLI SW8260Cug/Kg5.2 1NDMethyl t-butyl ether (MTBE) 10 08/31/15 JLI SW8260Cug/Kg1.0 1NDMethylene chloride 5.2 08/31/15 JLI SW8260Cug/Kg5.2 1140Naphthalene 270 08/31/15 JLI SW8260Cug/Kg54 50JNDn-Butylbenzene 270 08/31/15 JLI SW8260Cug/Kg27 50NDn-Propylbenzene 270 08/31/15 JLI SW8260Cug/Kg48 50


14B6 (0-5)Phoenix I.D.: BJ81794



LOD/MDL Dilution

NDo-Xylene 5.2 08/31/15 JLI SW8260Cug/Kg1.0 1NDp-Isopropyltoluene 270 08/31/15 JLI SW8260Cug/Kg27 50NDsec-Butylbenzene 270 08/31/15 JLI SW8260Cug/Kg27 50NDStyrene 5.2 08/31/15 JLI SW8260Cug/Kg0.52 1NDtert-Butylbenzene 270 08/31/15 JLI SW8260Cug/Kg27 50NDTetrachloroethene 5.2 08/31/15 JLI SW8260Cug/Kg1.0 1NDTetrahydrofuran (THF) 10 08/31/15 JLI SW8260Cug/Kg 12.6 10.64Toluene 5.2 08/31/15 JLI SW8260Cug/Kg0.52 1JNDtrans-1,2-Dichloroethene 5.2 08/31/15 JLI SW8260Cug/Kg0.52 1NDtrans-1,3-Dichloropropene 5.2 08/31/15 JLI SW8260Cug/Kg0.52 1NDtrans-1,4-dichloro-2-butene 540 08/31/15 JLI SW8260Cug/Kg130 5032Trichloroethene 270 08/31/15 JLI SW8260Cug/Kg27 50JNDTrichlorofluoromethane 5.2 08/31/15 JLI SW8260Cug/Kg1.0 1NDTrichlorotrifluoroethane 5.2 08/31/15 JLI SW8260Cug/Kg0.52 1NDVinyl chloride 5.2 08/31/15 JLI SW8260Cug/Kg0.52 1







14B6 (0-5)Phoenix I.D.: BJ81794



LOD/MDL Dilution

ND2-Methylnaphthalene 250 08/27/15 DD SW8270Dug/Kg100 1ND2-Methylphenol (o-cresol) 250 08/27/15 DD SW8270Dug/Kg160 1ND2-Nitroaniline 700 08/27/15 DD SW8270Dug/Kg350 1ND2-Nitrophenol 250 08/27/15 DD SW8270Dug/Kg220 1ND3&4-Methylphenol (m&p-cresol) 250 08/27/15 DD SW8270Dug/Kg 1140 1ND3,3'-Dichlorobenzidine 700 08/27/15 DD SW8270Dug/Kg170 1ND3-Nitroaniline 700 08/27/15 DD SW8270Dug/Kg700 1ND4,6-Dinitro-2-methylphenol 1800 08/27/15 DD SW8270Dug/Kg380 1ND4-Bromophenyl phenyl ether 250 08/27/15 DD SW8270Dug/Kg100 1ND4-Chloro-3-methylphenol 250 08/27/15 DD SW8270Dug/Kg120 1ND4-Chloroaniline 280 08/27/15 DD SW8270Dug/Kg160 1ND4-Chlorophenyl phenyl ether 250 08/27/15 DD SW8270Dug/Kg120 1ND4-Nitroaniline 700 08/27/15 DD SW8270Dug/Kg120 1ND4-Nitrophenol 350 08/27/15 DD SW8270Dug/Kg160 1NDAcenaphthene 250 08/27/15 DD SW8270Dug/Kg110 1NDAcenaphthylene 250 08/27/15 DD SW8270Dug/Kg98 1NDAcetophenone 250 08/27/15 DD SW8270Dug/Kg110 1NDAniline 280 08/27/15 DD SW8270Dug/Kg280 1NDAnthracene 250 08/27/15 DD SW8270Dug/Kg120 1170Benz(a)anthracene 250 08/27/15 DD SW8270Dug/Kg120 1JNDBenzidine 700 08/27/15 DD SW8270Dug/Kg210 1170Benzo(a)pyrene 250 08/27/15 DD SW8270Dug/Kg110 1J160Benzo(b)fluoranthene 250 08/27/15 DD SW8270Dug/Kg120 1J150Benzo(ghi)perylene 250 08/27/15 DD SW8270Dug/Kg110 1J160Benzo(k)fluoranthene 250 08/27/15 DD SW8270Dug/Kg120 1JNDBenzoic acid 1800 08/27/15 DD SW8270Dug/Kg 1700 1NDBenzyl butyl phthalate 250 08/27/15 DD SW8270Dug/Kg91 1NDBis(2-chloroethoxy)methane 250 08/27/15 DD SW8270Dug/Kg97 1NDBis(2-chloroethyl)ether 250 08/27/15 DD SW8270Dug/Kg95 1NDBis(2-chloroisopropyl)ether 250 08/27/15 DD SW8270Dug/Kg 198 1NDBis(2-ethylhexyl)phthalate 250 08/27/15 DD SW8270Dug/Kg100 1NDCarbazole 1800 08/27/15 DD SW8270Dug/Kg270 1180Chrysene 250 08/27/15 DD SW8270Dug/Kg120 1JNDDibenz(a,h)anthracene 250 08/27/15 DD SW8270Dug/Kg110 1NDDibenzofuran 250 08/27/15 DD SW8270Dug/Kg100 1NDDiethyl phthalate 250 08/27/15 DD SW8270Dug/Kg110 1NDDimethylphthalate 250 08/27/15 DD SW8270Dug/Kg110 1NDDi-n-butylphthalate 250 08/27/15 DD SW8270Dug/Kg93 1NDDi-n-octylphthalate 250 08/27/15 DD SW8270Dug/Kg91 1340Fluoranthene 250 08/27/15 DD SW8270Dug/Kg110 1NDFluorene 250 08/27/15 DD SW8270Dug/Kg120 1NDHexachlorobenzene 250 08/27/15 DD SW8270Dug/Kg100 1NDHexachlorobutadiene 250 08/27/15 DD SW8270Dug/Kg130 1NDHexachlorocyclopentadiene 250 08/27/15 DD SW8270Dug/Kg110 1NDHexachloroethane 250 08/27/15 DD SW8270Dug/Kg110 1180Indeno(1,2,3-cd)pyrene 250 08/27/15 DD SW8270Dug/Kg120 1JNDIsophorone 250 08/27/15 DD SW8270Dug/Kg98 1NDNaphthalene 250 08/27/15 DD SW8270Dug/Kg100 1NDNitrobenzene 250 08/27/15 DD SW8270Dug/Kg120 1


14B6 (0-5)Phoenix I.D.: BJ81794



LOD/MDL Dilution

NDN-Nitrosodimethylamine 250 08/27/15 DD SW8270Dug/Kg99 1NDN-Nitrosodi-n-propylamine 250 08/27/15 DD SW8270Dug/Kg110 1NDN-Nitrosodiphenylamine 250 08/27/15 DD SW8270Dug/Kg130 1NDPentachloronitrobenzene 250 08/27/15 DD SW8270Dug/Kg130 1NDPentachlorophenol 250 08/27/15 DD SW8270Dug/Kg130 1150Phenanthrene 250 08/27/15 DD SW8270Dug/Kg100 1JNDPhenol 250 08/27/15 DD SW8270Dug/Kg110 1300Pyrene 250 08/27/15 DD SW8270Dug/Kg120 1NDPyridine 250 08/27/15 DD SW8270Dug/Kg86 1


Comments:



Volatile Comment:There was a suppression of the last internal standard in the low level analysis, all affected compounds are reported from the methanol preserved high level analysis which did not exhibit this interference.












SOLIDEBC72 Hour


RB

Laboratory Data

14B6 (10-15)

Phoenix ID: BJ81795

08/26/1513:0017:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution




14B6 (10-15)Phoenix I.D.: BJ81795



LOD/MDL Dilution

ND2-Isopropyltoluene 4.3 08/30/15 JLI SW8260Cug/Kg 10.43 1ND4-Chlorotoluene 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1ND4-Methyl-2-pentanone 22 08/30/15 JLI SW8260Cug/Kg4.3 1NDAcetone 43 08/30/15 JLI SW8260Cug/Kg4.3 1NDAcrylonitrile 8.6 08/30/15 JLI SW8260Cug/Kg0.86 10.73Benzene 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1JNDBromobenzene 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1NDBromochloromethane 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1NDBromodichloromethane 4.3 08/30/15 JLI SW8260Cug/Kg0.86 1NDBromoform 4.3 08/30/15 JLI SW8260Cug/Kg0.86 1NDBromomethane 4.3 08/30/15 JLI SW8260Cug/Kg1.7 1NDCarbon Disulfide 4.3 08/30/15 JLI SW8260Cug/Kg0.86 1NDCarbon tetrachloride 4.3 08/30/15 JLI SW8260Cug/Kg0.86 1NDChlorobenzene 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1NDChloroethane 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1NDChloroform 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1NDChloromethane 4.3 08/30/15 JLI SW8260Cug/Kg0.86 1160cis-1,2-Dichloroethene 250 08/31/15 JLI SW8260Cug/Kg29 50JNDcis-1,3-Dichloropropene 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1NDDibromochloromethane 4.3 08/30/15 JLI SW8260Cug/Kg0.86 1NDDibromomethane 4.3 08/30/15 JLI SW8260Cug/Kg0.86 1NDDichlorodifluoromethane 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1NDEthylbenzene 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1NDHexachlorobutadiene 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1NDIsopropylbenzene 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1NDm&p-Xylene 4.3 08/30/15 JLI SW8260Cug/Kg0.86 1NDMethyl Ethyl Ketone 26 08/30/15 JLI SW8260Cug/Kg4.3 1NDMethyl t-butyl ether (MTBE) 8.6 08/30/15 JLI SW8260Cug/Kg0.86 1NDMethylene chloride 4.3 08/30/15 JLI SW8260Cug/Kg4.3 15.2Naphthalene 8.0 08/30/15 JLI SW8260Cug/Kg0.86 1JNDn-Butylbenzene 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1NDn-Propylbenzene 4.3 08/30/15 JLI SW8260Cug/Kg0.77 1NDo-Xylene 4.3 08/30/15 JLI SW8260Cug/Kg0.86 1NDp-Isopropyltoluene 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1NDsec-Butylbenzene 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1NDStyrene 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1NDtert-Butylbenzene 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1NDTetrachloroethene 4.3 08/30/15 JLI SW8260Cug/Kg0.86 1NDTetrahydrofuran (THF) 8.6 08/30/15 JLI SW8260Cug/Kg 12.2 1NDToluene 4.3 08/30/15 JLI SW8260Cug/Kg0.43 10.47trans-1,2-Dichloroethene 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1JNDtrans-1,3-Dichloropropene 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1NDtrans-1,4-dichloro-2-butene 8.6 08/30/15 JLI SW8260Cug/Kg2.2 163Trichloroethene 290 08/31/15 JLI SW8260Cug/Kg29 50JNDTrichlorofluoromethane 4.3 08/30/15 JLI SW8260Cug/Kg0.86 1NDTrichlorotrifluoroethane 4.3 08/30/15 JLI SW8260Cug/Kg0.43 17.6Vinyl chloride 4.3 08/30/15 JLI SW8260Cug/Kg0.43 1



14B6 (10-15)Phoenix I.D.: BJ81795



LOD/MDL Dilution







14B6 (10-15)Phoenix I.D.: BJ81795



LOD/MDL Dilution

NDAniline 310 08/27/15 DD SW8270Dug/Kg310 1NDAnthracene 270 08/27/15 DD SW8270Dug/Kg130 1170Benz(a)anthracene 270 08/27/15 DD SW8270Dug/Kg130 1JNDBenzidine 760 08/27/15 DD SW8270Dug/Kg220 1390Benzo(a)pyrene 270 08/27/15 DD SW8270Dug/Kg120 1250Benzo(b)fluoranthene 270 08/27/15 DD SW8270Dug/Kg130 1J290Benzo(ghi)perylene 270 08/27/15 DD SW8270Dug/Kg120 1270Benzo(k)fluoranthene 270 08/27/15 DD SW8270Dug/Kg130 1NDBenzoic acid 1900 08/27/15 DD SW8270Dug/Kg 1760 1NDBenzyl butyl phthalate 270 08/27/15 DD SW8270Dug/Kg99 1NDBis(2-chloroethoxy)methane 270 08/27/15 DD SW8270Dug/Kg110 1NDBis(2-chloroethyl)ether 270 08/27/15 DD SW8270Dug/Kg100 1NDBis(2-chloroisopropyl)ether 270 08/27/15 DD SW8270Dug/Kg 1110 1NDBis(2-ethylhexyl)phthalate 270 08/27/15 DD SW8270Dug/Kg110 1NDCarbazole 1900 08/27/15 DD SW8270Dug/Kg290 1170Chrysene 270 08/27/15 DD SW8270Dug/Kg130 1JNDDibenz(a,h)anthracene 270 08/27/15 DD SW8270Dug/Kg120 1NDDibenzofuran 270 08/27/15 DD SW8270Dug/Kg110 1NDDiethyl phthalate 270 08/27/15 DD SW8270Dug/Kg120 1NDDimethylphthalate 270 08/27/15 DD SW8270Dug/Kg120 1NDDi-n-butylphthalate 270 08/27/15 DD SW8270Dug/Kg100 1NDDi-n-octylphthalate 270 08/27/15 DD SW8270Dug/Kg99 1240Fluoranthene 270 08/27/15 DD SW8270Dug/Kg120 1JNDFluorene 270 08/27/15 DD SW8270Dug/Kg130 1NDHexachlorobenzene 270 08/27/15 DD SW8270Dug/Kg110 1NDHexachlorobutadiene 270 08/27/15 DD SW8270Dug/Kg140 1NDHexachlorocyclopentadiene 270 08/27/15 DD SW8270Dug/Kg120 1NDHexachloroethane 270 08/27/15 DD SW8270Dug/Kg110 1340Indeno(1,2,3-cd)pyrene 270 08/27/15 DD SW8270Dug/Kg130 1NDIsophorone 270 08/27/15 DD SW8270Dug/Kg110 1NDNaphthalene 270 08/27/15 DD SW8270Dug/Kg110 1NDNitrobenzene 270 08/27/15 DD SW8270Dug/Kg130 1NDN-Nitrosodimethylamine 270 08/27/15 DD SW8270Dug/Kg110 1NDN-Nitrosodi-n-propylamine 270 08/27/15 DD SW8270Dug/Kg120 1NDN-Nitrosodiphenylamine 270 08/27/15 DD SW8270Dug/Kg150 1NDPentachloronitrobenzene 270 08/27/15 DD SW8270Dug/Kg140 1NDPentachlorophenol 270 08/27/15 DD SW8270Dug/Kg140 1110Phenanthrene 270 08/27/15 DD SW8270Dug/Kg110 1JNDPhenol 270 08/27/15 DD SW8270Dug/Kg120 1220Pyrene 270 08/27/15 DD SW8270Dug/Kg130 1JNDPyridine 270 08/27/15 DD SW8270Dug/Kg94 1



14B6 (10-15)Phoenix I.D.: BJ81795



LOD/MDL Dilution

Comments:











SOLIDEBC72 Hour


RB

Laboratory Data

14B6 (15-17)

Phoenix ID: BJ81796

08/26/1513:1517:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution




14400Iron 43 08/28/15 LK SW6010Cmg/Kg B43 100.18Mercury 0.03 08/27/15 RS SW7471Bmg/Kg0.02 11060Potassium 9 08/28/15 LK SW6010Cmg/Kg3.4 1N2680Magnesium 4.3 08/28/15 LK SW6010Cmg/Kg4.3 1235Manganese 4.3 08/28/15 LK SW6010Cmg/Kg4.3 10

1110Sodium 9 08/28/15 LK SW6010Cmg/Kg3.7 1N16.5Nickel 0.43 08/28/15 LK SW6010Cmg/Kg0.43 1107Lead 0.9 08/28/15 LK SW6010Cmg/Kg0.43 1




14B6 (15-17)Phoenix I.D.: BJ81796



LOD/MDL Dilution








14B6 (15-17)Phoenix I.D.: BJ81796



LOD/MDL Dilution

ND1,1-Dichloropropene 400 09/01/15 JLI SW8260Cug/Kg40 50ND1,2,3-Trichlorobenzene 400 09/01/15 JLI SW8260Cug/Kg80 50ND1,2,3-Trichloropropane 400 09/01/15 JLI SW8260Cug/Kg40 50ND1,2,4-Trichlorobenzene 400 09/01/15 JLI SW8260Cug/Kg80 501501,2,4-Trimethylbenzene 400 09/01/15 JLI SW8260Cug/Kg40 50JND1,2-Dibromo-3-chloropropane 400 09/01/15 JLI SW8260Cug/Kg80 50ND1,2-Dibromoethane 400 09/01/15 JLI SW8260Cug/Kg40 50ND1,2-Dichlorobenzene 400 09/01/15 JLI SW8260Cug/Kg40 50ND1,2-Dichloroethane 400 09/01/15 JLI SW8260Cug/Kg40 50ND1,2-Dichloropropane 400 09/01/15 JLI SW8260Cug/Kg80 50471,3,5-Trimethylbenzene 400 09/01/15 JLI SW8260Cug/Kg40 50JND1,3-Dichlorobenzene 400 09/01/15 JLI SW8260Cug/Kg40 50ND1,3-Dichloropropane 400 09/01/15 JLI SW8260Cug/Kg80 50ND1,4-Dichlorobenzene 400 09/01/15 JLI SW8260Cug/Kg40 50ND2,2-Dichloropropane 400 09/01/15 JLI SW8260Cug/Kg40 50ND2-Chlorotoluene 400 09/01/15 JLI SW8260Cug/Kg80 50ND2-Hexanone 2000 09/01/15 JLI SW8260Cug/Kg400 50ND2-Isopropyltoluene 400 09/01/15 JLI SW8260Cug/Kg 140 50ND4-Chlorotoluene 400 09/01/15 JLI SW8260Cug/Kg40 50ND4-Methyl-2-pentanone 2000 09/01/15 JLI SW8260Cug/Kg400 50NDAcetone 4000 09/01/15 JLI SW8260Cug/Kg400 50NDAcrylonitrile 800 09/01/15 JLI SW8260Cug/Kg80 50890Benzene 400 09/01/15 JLI SW8260Cug/Kg40 50NDBromobenzene 400 09/01/15 JLI SW8260Cug/Kg40 50NDBromochloromethane 400 09/01/15 JLI SW8260Cug/Kg40 50NDBromodichloromethane 400 09/01/15 JLI SW8260Cug/Kg80 50NDBromoform 400 09/01/15 JLI SW8260Cug/Kg80 50NDBromomethane 400 09/01/15 JLI SW8260Cug/Kg160 50NDCarbon Disulfide 400 09/01/15 JLI SW8260Cug/Kg80 50NDCarbon tetrachloride 400 09/01/15 JLI SW8260Cug/Kg80 50NDChlorobenzene 400 09/01/15 JLI SW8260Cug/Kg40 50NDChloroethane 400 09/01/15 JLI SW8260Cug/Kg40 50NDChloroform 250 09/01/15 JLI SW8260Cug/Kg40 50NDChloromethane 400 09/01/15 JLI SW8260Cug/Kg80 50

8700cis-1,2-Dichloroethene 400 09/01/15 JLI SW8260Cug/Kg40 50NDcis-1,3-Dichloropropene 400 09/01/15 JLI SW8260Cug/Kg40 50NDDibromochloromethane 400 09/01/15 JLI SW8260Cug/Kg80 50NDDibromomethane 400 09/01/15 JLI SW8260Cug/Kg80 50NDDichlorodifluoromethane 400 09/01/15 JLI SW8260Cug/Kg40 50280Ethylbenzene 400 09/01/15 JLI SW8260Cug/Kg40 50JNDHexachlorobutadiene 400 09/01/15 JLI SW8260Cug/Kg40 5043Isopropylbenzene 400 09/01/15 JLI SW8260Cug/Kg40 50J270m&p-Xylene 400 09/01/15 JLI SW8260Cug/Kg80 50JNDMethyl Ethyl Ketone 2400 09/01/15 JLI SW8260Cug/Kg400 50NDMethyl t-butyl ether (MTBE) 800 09/01/15 JLI SW8260Cug/Kg80 50570Methylene chloride 400 09/01/15 JLI SW8260Cug/Kg400 50S

2700Naphthalene 400 09/01/15 JLI SW8260Cug/Kg80 5063n-Butylbenzene 400 09/01/15 JLI SW8260Cug/Kg40 50JNDn-Propylbenzene 400 09/01/15 JLI SW8260Cug/Kg72 50


14B6 (15-17)Phoenix I.D.: BJ81796



LOD/MDL Dilution

130o-Xylene 400 09/01/15 JLI SW8260Cug/Kg80 50J170p-Isopropyltoluene 400 09/01/15 JLI SW8260Cug/Kg40 50JNDsec-Butylbenzene 400 09/01/15 JLI SW8260Cug/Kg40 50NDStyrene 400 09/01/15 JLI SW8260Cug/Kg40 50NDtert-Butylbenzene 400 09/01/15 JLI SW8260Cug/Kg40 50NDTetrachloroethene 400 09/01/15 JLI SW8260Cug/Kg80 50NDTetrahydrofuran (THF) 800 09/01/15 JLI SW8260Cug/Kg 1200 50150Toluene 400 09/01/15 JLI SW8260Cug/Kg40 50J94trans-1,2-Dichloroethene 150 09/01/15 JLI SW8260Cug/Kg40 50JNDtrans-1,3-Dichloropropene 400 09/01/15 JLI SW8260Cug/Kg40 50NDtrans-1,4-dichloro-2-butene 800 09/01/15 JLI SW8260Cug/Kg200 50

14000Trichloroethene 400 09/01/15 JLI SW8260Cug/Kg40 50NDTrichlorofluoromethane 400 09/01/15 JLI SW8260Cug/Kg80 50NDTrichlorotrifluoroethane 400 09/01/15 JLI SW8260Cug/Kg40 50

1100Vinyl chloride 400 09/01/15 JLI SW8260Cug/Kg40 50







14B6 (15-17)Phoenix I.D.: BJ81796



LOD/MDL Dilution

ND2-Methylnaphthalene 310 08/27/15 DD SW8270Dug/Kg130 1ND2-Methylphenol (o-cresol) 310 08/27/15 DD SW8270Dug/Kg210 1ND2-Nitroaniline 900 08/27/15 DD SW8270Dug/Kg450 1ND2-Nitrophenol 310 08/27/15 DD SW8270Dug/Kg290 1ND3&4-Methylphenol (m&p-cresol) 310 08/27/15 DD SW8270Dug/Kg 1180 1ND3,3'-Dichlorobenzidine 900 08/27/15 DD SW8270Dug/Kg210 1ND3-Nitroaniline 900 08/27/15 DD SW8270Dug/Kg900 1ND4,6-Dinitro-2-methylphenol 2200 08/27/15 DD SW8270Dug/Kg480 1ND4-Bromophenyl phenyl ether 310 08/27/15 DD SW8270Dug/Kg130 1ND4-Chloro-3-methylphenol 310 08/27/15 DD SW8270Dug/Kg160 1ND4-Chloroaniline 360 08/27/15 DD SW8270Dug/Kg210 1ND4-Chlorophenyl phenyl ether 310 08/27/15 DD SW8270Dug/Kg150 1ND4-Nitroaniline 900 08/27/15 DD SW8270Dug/Kg150 1ND4-Nitrophenol 450 08/27/15 DD SW8270Dug/Kg200 1330Acenaphthene 310 08/27/15 DD SW8270Dug/Kg140 1620Acenaphthylene 310 08/27/15 DD SW8270Dug/Kg130 1NDAcetophenone 310 08/27/15 DD SW8270Dug/Kg140 1NDAniline 360 08/27/15 DD SW8270Dug/Kg360 1

3900Anthracene 310 08/27/15 DD SW8270Dug/Kg150 16300Benz(a)anthracene 310 08/27/15 DD SW8270Dug/Kg150 1NDBenzidine 900 08/27/15 DD SW8270Dug/Kg260 1

2100Benzo(a)pyrene 310 08/27/15 DD SW8270Dug/Kg150 18800Benzo(b)fluoranthene 310 08/27/15 DD SW8270Dug/Kg150 15100Benzo(ghi)perylene 310 08/27/15 DD SW8270Dug/Kg150 14600Benzo(k)fluoranthene 310 08/27/15 DD SW8270Dug/Kg150 1NDBenzoic acid 2200 08/27/15 DD SW8270Dug/Kg 1900 1NDBenzyl butyl phthalate 310 08/27/15 DD SW8270Dug/Kg120 1NDBis(2-chloroethoxy)methane 310 08/27/15 DD SW8270Dug/Kg120 1NDBis(2-chloroethyl)ether 310 08/27/15 DD SW8270Dug/Kg120 1NDBis(2-chloroisopropyl)ether 310 08/27/15 DD SW8270Dug/Kg 1120 1NDBis(2-ethylhexyl)phthalate 310 08/27/15 DD SW8270Dug/Kg130 1

1700Carbazole 2200 08/27/15 DD SW8270Dug/Kg340 1J6100Chrysene 310 08/27/15 DD SW8270Dug/Kg150 11900Dibenz(a,h)anthracene 310 08/27/15 DD SW8270Dug/Kg150 13200Dibenzofuran 310 08/27/15 DD SW8270Dug/Kg130 1NDDiethyl phthalate 310 08/27/15 DD SW8270Dug/Kg140 1NDDimethylphthalate 310 08/27/15 DD SW8270Dug/Kg140 1NDDi-n-butylphthalate 310 08/27/15 DD SW8270Dug/Kg120 1NDDi-n-octylphthalate 310 08/27/15 DD SW8270Dug/Kg120 1





14B6 (15-17)Phoenix I.D.: BJ81796



LOD/MDL Dilution





Comments:















SOLIDEBC72 Hour


RB

Laboratory Data

14B4 (0-5)

Phoenix ID: BJ81797

08/26/1513:3017:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution







14B4 (0-5)Phoenix I.D.: BJ81797



LOD/MDL Dilution




Pesticides - Soil4.34,4' -DDD 3.3 08/28/15 C/P SW8081Bug/Kg3.3 24.04,4' -DDE 2.1 08/28/15 C/P SW8081Bug/Kg2.1 2ND4,4' -DDT 2.1 08/28/15 C/P SW8081Bug/Kg2.1 2NDa-BHC 6.9 08/28/15 C/P SW8081Bug/Kg6.9 222a-Chlordane 3.4 08/28/15 C/P SW8081Bug/Kg3.4 2NDAldrin 3.4 08/28/15 C/P SW8081Bug/Kg3.4 2NDb-BHC 6.9 08/28/15 C/P SW8081Bug/Kg6.9 2NDd-BHC 6.9 08/28/15 C/P SW8081Bug/Kg6.9 2NDDieldrin 3.4 08/28/15 C/P SW8081Bug/Kg3.4 2NDEndosulfan I 6.9 08/28/15 C/P SW8081Bug/Kg6.9 2NDEndosulfan II 6.9 08/28/15 C/P SW8081Bug/Kg6.9 2NDEndosulfan sulfate 6.9 08/28/15 C/P SW8081Bug/Kg6.9 2NDEndrin 6.9 08/28/15 C/P SW8081Bug/Kg6.9 2NDEndrin aldehyde 6.9 08/28/15 C/P SW8081Bug/Kg6.9 2NDEndrin ketone 6.9 08/28/15 C/P SW8081Bug/Kg6.9 2NDg-BHC 1.4 08/28/15 C/P SW8081Bug/Kg1.4 219g-Chlordane 3.4 08/28/15 C/P SW8081Bug/Kg3.4 2NDHeptachlor 6.9 08/28/15 C/P SW8081Bug/Kg6.9 2NDHeptachlor epoxide 6.9 08/28/15 C/P SW8081Bug/Kg6.9 2NDMethoxychlor 34 08/28/15 C/P SW8081Bug/Kg34 2NDToxaphene 140 08/28/15 C/P SW8081Bug/Kg140 2

QA/QC Surrogates77% DCBP 08/28/15 C/P 30 - 150 %% 283% TCMX 08/28/15 C/P 30 - 150 %% 2



14B4 (0-5)Phoenix I.D.: BJ81797



LOD/MDL Dilution

ND1,1-Dichloropropene 5.9 08/31/15 JLI SW8260Cug/Kg0.59 1ND1,2,3-Trichlorobenzene 270 09/01/15 JLI SW8260Cug/Kg54 50ND1,2,3-Trichloropropane 270 09/01/15 JLI SW8260Cug/Kg27 50ND1,2,4-Trichlorobenzene 270 09/01/15 JLI SW8260Cug/Kg54 50ND1,2,4-Trimethylbenzene 270 09/01/15 JLI SW8260Cug/Kg27 50ND1,2-Dibromo-3-chloropropane 270 09/01/15 JLI SW8260Cug/Kg54 50ND1,2-Dibromoethane 5.9 08/31/15 JLI SW8260Cug/Kg0.59 1ND1,2-Dichlorobenzene 270 09/01/15 JLI SW8260Cug/Kg27 50ND1,2-Dichloroethane 5.9 08/31/15 JLI SW8260Cug/Kg0.59 1ND1,2-Dichloropropane 5.9 08/31/15 JLI SW8260Cug/Kg1.2 1ND1,3,5-Trimethylbenzene 270 09/01/15 JLI SW8260Cug/Kg27 50ND1,3-Dichlorobenzene 270 09/01/15 JLI SW8260Cug/Kg27 50ND1,3-Dichloropropane 5.9 08/31/15 JLI SW8260Cug/Kg1.2 1ND1,4-Dichlorobenzene 270 09/01/15 JLI SW8260Cug/Kg27 50ND2,2-Dichloropropane 5.9 08/31/15 JLI SW8260Cug/Kg0.59 1ND2-Chlorotoluene 270 09/01/15 JLI SW8260Cug/Kg54 50ND2-Hexanone 30 08/31/15 JLI SW8260Cug/Kg5.9 1ND2-Isopropyltoluene 270 09/01/15 JLI SW8260Cug/Kg 127 50ND4-Chlorotoluene 270 09/01/15 JLI SW8260Cug/Kg27 50ND4-Methyl-2-pentanone 30 08/31/15 JLI SW8260Cug/Kg5.9 1NDAcetone 50 08/31/15 JLI SW8260Cug/Kg5.9 1NDAcrylonitrile 12 08/31/15 JLI SW8260Cug/Kg1.2 1NDBenzene 5.9 08/31/15 JLI SW8260Cug/Kg0.59 1NDBromobenzene 270 09/01/15 JLI SW8260Cug/Kg27 50NDBromochloromethane 5.9 08/31/15 JLI SW8260Cug/Kg0.59 1NDBromodichloromethane 5.9 08/31/15 JLI SW8260Cug/Kg1.2 1NDBromoform 5.9 08/31/15 JLI SW8260Cug/Kg1.2 1NDBromomethane 5.9 08/31/15 JLI SW8260Cug/Kg2.4 1NDCarbon Disulfide 5.9 08/31/15 JLI SW8260Cug/Kg1.2 1NDCarbon tetrachloride 5.9 08/31/15 JLI SW8260Cug/Kg1.2 1NDChlorobenzene 5.9 08/31/15 JLI SW8260Cug/Kg0.59 1NDChloroethane 5.9 08/31/15 JLI SW8260Cug/Kg0.59 1NDChloroform 5.9 08/31/15 JLI SW8260Cug/Kg0.59 1NDChloromethane 5.9 08/31/15 JLI SW8260Cug/Kg1.2 10.73cis-1,2-Dichloroethene 5.9 08/31/15 JLI SW8260Cug/Kg0.59 1JNDcis-1,3-Dichloropropene 5.9 08/31/15 JLI SW8260Cug/Kg0.59 1NDDibromochloromethane 5.9 08/31/15 JLI SW8260Cug/Kg1.2 1NDDibromomethane 5.9 08/31/15 JLI SW8260Cug/Kg1.2 1NDDichlorodifluoromethane 5.9 08/31/15 JLI SW8260Cug/Kg0.59 1NDEthylbenzene 5.9 08/31/15 JLI SW8260Cug/Kg0.59 1NDHexachlorobutadiene 270 09/01/15 JLI SW8260Cug/Kg27 50NDIsopropylbenzene 270 09/01/15 JLI SW8260Cug/Kg27 50NDm&p-Xylene 5.9 08/31/15 JLI SW8260Cug/Kg1.2 1NDMethyl Ethyl Ketone 35 08/31/15 JLI SW8260Cug/Kg5.9 1NDMethyl t-butyl ether (MTBE) 12 08/31/15 JLI SW8260Cug/Kg1.2 1NDMethylene chloride 5.9 08/31/15 JLI SW8260Cug/Kg5.9 161Naphthalene 270 09/01/15 JLI SW8260Cug/Kg54 50JNDn-Butylbenzene 270 09/01/15 JLI SW8260Cug/Kg27 50NDn-Propylbenzene 270 09/01/15 JLI SW8260Cug/Kg48 50


14B4 (0-5)Phoenix I.D.: BJ81797



LOD/MDL Dilution

NDo-Xylene 5.9 08/31/15 JLI SW8260Cug/Kg1.2 1NDp-Isopropyltoluene 270 09/01/15 JLI SW8260Cug/Kg27 50NDsec-Butylbenzene 270 09/01/15 JLI SW8260Cug/Kg27 50NDStyrene 5.9 08/31/15 JLI SW8260Cug/Kg0.59 1NDtert-Butylbenzene 270 09/01/15 JLI SW8260Cug/Kg27 50NDTetrachloroethene 5.9 08/31/15 JLI SW8260Cug/Kg1.2 1NDTetrahydrofuran (THF) 12 08/31/15 JLI SW8260Cug/Kg 13.0 10.72Toluene 5.9 08/31/15 JLI SW8260Cug/Kg0.59 1JNDtrans-1,2-Dichloroethene 5.9 08/31/15 JLI SW8260Cug/Kg0.59 1NDtrans-1,3-Dichloropropene 5.9 08/31/15 JLI SW8260Cug/Kg0.59 1NDtrans-1,4-dichloro-2-butene 540 09/01/15 JLI SW8260Cug/Kg130 50360Trichloroethene 270 09/01/15 JLI SW8260Cug/Kg27 50NDTrichlorofluoromethane 5.9 08/31/15 JLI SW8260Cug/Kg1.2 1NDTrichlorotrifluoroethane 5.9 08/31/15 JLI SW8260Cug/Kg0.59 1NDVinyl chloride 5.9 08/31/15 JLI SW8260Cug/Kg0.59 1







14B4 (0-5)Phoenix I.D.: BJ81797



LOD/MDL Dilution

ND2-Methylnaphthalene 240 08/27/15 DD SW8270Dug/Kg100 1ND2-Methylphenol (o-cresol) 240 08/27/15 DD SW8270Dug/Kg160 1ND2-Nitroaniline 700 08/27/15 DD SW8270Dug/Kg350 1ND2-Nitrophenol 240 08/27/15 DD SW8270Dug/Kg220 1ND3&4-Methylphenol (m&p-cresol) 240 08/27/15 DD SW8270Dug/Kg 1140 1ND3,3'-Dichlorobenzidine 700 08/27/15 DD SW8270Dug/Kg160 1ND3-Nitroaniline 700 08/27/15 DD SW8270Dug/Kg700 1ND4,6-Dinitro-2-methylphenol 1700 08/27/15 DD SW8270Dug/Kg380 1ND4-Bromophenyl phenyl ether 240 08/27/15 DD SW8270Dug/Kg100 1ND4-Chloro-3-methylphenol 240 08/27/15 DD SW8270Dug/Kg120 1ND4-Chloroaniline 280 08/27/15 DD SW8270Dug/Kg160 1ND4-Chlorophenyl phenyl ether 240 08/27/15 DD SW8270Dug/Kg120 1ND4-Nitroaniline 700 08/27/15 DD SW8270Dug/Kg120 1ND4-Nitrophenol 350 08/27/15 DD SW8270Dug/Kg160 1NDAcenaphthene 240 08/27/15 DD SW8270Dug/Kg110 1NDAcenaphthylene 240 08/27/15 DD SW8270Dug/Kg98 1NDAcetophenone 240 08/27/15 DD SW8270Dug/Kg110 1NDAniline 280 08/27/15 DD SW8270Dug/Kg280 1120Anthracene 240 08/27/15 DD SW8270Dug/Kg110 1J480Benz(a)anthracene 240 08/27/15 DD SW8270Dug/Kg120 1NDBenzidine 700 08/27/15 DD SW8270Dug/Kg200 1600Benzo(a)pyrene 240 08/27/15 DD SW8270Dug/Kg110 1420Benzo(b)fluoranthene 240 08/27/15 DD SW8270Dug/Kg120 1430Benzo(ghi)perylene 240 08/27/15 DD SW8270Dug/Kg110 1490Benzo(k)fluoranthene 240 08/27/15 DD SW8270Dug/Kg120 1NDBenzoic acid 1700 08/27/15 DD SW8270Dug/Kg 1700 1NDBenzyl butyl phthalate 240 08/27/15 DD SW8270Dug/Kg90 1NDBis(2-chloroethoxy)methane 240 08/27/15 DD SW8270Dug/Kg96 1NDBis(2-chloroethyl)ether 240 08/27/15 DD SW8270Dug/Kg94 1NDBis(2-chloroisopropyl)ether 240 08/27/15 DD SW8270Dug/Kg 197 1NDBis(2-ethylhexyl)phthalate 240 08/27/15 DD SW8270Dug/Kg100 1NDCarbazole 1700 08/27/15 DD SW8270Dug/Kg260 1510Chrysene 240 08/27/15 DD SW8270Dug/Kg120 1150Dibenz(a,h)anthracene 240 08/27/15 DD SW8270Dug/Kg110 1JNDDibenzofuran 240 08/27/15 DD SW8270Dug/Kg100 1NDDiethyl phthalate 240 08/27/15 DD SW8270Dug/Kg110 1NDDimethylphthalate 240 08/27/15 DD SW8270Dug/Kg110 1NDDi-n-butylphthalate 240 08/27/15 DD SW8270Dug/Kg93 1NDDi-n-octylphthalate 240 08/27/15 DD SW8270Dug/Kg90 1770Fluoranthene 240 08/27/15 DD SW8270Dug/Kg110 1NDFluorene 240 08/27/15 DD SW8270Dug/Kg120 1NDHexachlorobenzene 240 08/27/15 DD SW8270Dug/Kg100 1NDHexachlorobutadiene 240 08/27/15 DD SW8270Dug/Kg130 1NDHexachlorocyclopentadiene 240 08/27/15 DD SW8270Dug/Kg110 1NDHexachloroethane 240 08/27/15 DD SW8270Dug/Kg100 1500Indeno(1,2,3-cd)pyrene 240 08/27/15 DD SW8270Dug/Kg120 1NDIsophorone 240 08/27/15 DD SW8270Dug/Kg98 1NDNaphthalene 240 08/27/15 DD SW8270Dug/Kg100 1NDNitrobenzene 240 08/27/15 DD SW8270Dug/Kg120 1


14B4 (0-5)Phoenix I.D.: BJ81797



LOD/MDL Dilution

NDN-Nitrosodimethylamine 240 08/27/15 DD SW8270Dug/Kg98 1NDN-Nitrosodi-n-propylamine 240 08/27/15 DD SW8270Dug/Kg110 1NDN-Nitrosodiphenylamine 240 08/27/15 DD SW8270Dug/Kg130 1NDPentachloronitrobenzene 240 08/27/15 DD SW8270Dug/Kg130 1NDPentachlorophenol 240 08/27/15 DD SW8270Dug/Kg130 1470Phenanthrene 240 08/27/15 DD SW8270Dug/Kg100 1NDPhenol 240 08/27/15 DD SW8270Dug/Kg110 1690Pyrene 240 08/27/15 DD SW8270Dug/Kg120 1NDPyridine 240 08/27/15 DD SW8270Dug/Kg86 1


Comments:




Pesticide Comment:Due to the presence of Chlordane in the sample, an elevated RL was reported.










SOLIDEBC72 Hour


RB

Laboratory Data

14B4 (10-15)

Phoenix ID: BJ81798

08/26/1513:4517:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution




14B4 (10-15)Phoenix I.D.: BJ81798



LOD/MDL Dilution

ND2-Isopropyltoluene 7.9 08/30/15 JLI SW8260Cug/Kg 10.79 1ND4-Chlorotoluene 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1ND4-Methyl-2-pentanone 40 08/30/15 JLI SW8260Cug/Kg7.9 1NDAcetone 50 08/30/15 JLI SW8260Cug/Kg7.9 1NDAcrylonitrile 16 08/30/15 JLI SW8260Cug/Kg1.6 12.3Benzene 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1JNDBromobenzene 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1NDBromochloromethane 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1NDBromodichloromethane 7.9 08/30/15 JLI SW8260Cug/Kg1.6 1NDBromoform 7.9 08/30/15 JLI SW8260Cug/Kg1.6 1NDBromomethane 7.9 08/30/15 JLI SW8260Cug/Kg3.2 1NDCarbon Disulfide 7.9 08/30/15 JLI SW8260Cug/Kg1.6 1NDCarbon tetrachloride 7.9 08/30/15 JLI SW8260Cug/Kg1.6 1NDChlorobenzene 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1NDChloroethane 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1NDChloroform 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1NDChloromethane 7.9 08/30/15 JLI SW8260Cug/Kg1.6 1570cis-1,2-Dichloroethene 240 08/31/15 JLI SW8260Cug/Kg24 50NDcis-1,3-Dichloropropene 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1NDDibromochloromethane 7.9 08/30/15 JLI SW8260Cug/Kg1.6 1NDDibromomethane 7.9 08/30/15 JLI SW8260Cug/Kg1.6 1NDDichlorodifluoromethane 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1NDEthylbenzene 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1NDHexachlorobutadiene 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1NDIsopropylbenzene 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1NDm&p-Xylene 7.9 08/30/15 JLI SW8260Cug/Kg1.6 1NDMethyl Ethyl Ketone 48 08/30/15 JLI SW8260Cug/Kg7.9 1NDMethyl t-butyl ether (MTBE) 16 08/30/15 JLI SW8260Cug/Kg1.6 1NDMethylene chloride 7.9 08/30/15 JLI SW8260Cug/Kg7.9 152Naphthalene 240 08/31/15 JLI SW8260Cug/Kg48 50JNDn-Butylbenzene 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1NDn-Propylbenzene 7.9 08/30/15 JLI SW8260Cug/Kg1.4 1NDo-Xylene 7.9 08/30/15 JLI SW8260Cug/Kg1.6 1NDp-Isopropyltoluene 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1NDsec-Butylbenzene 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1NDStyrene 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1NDtert-Butylbenzene 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1NDTetrachloroethene 7.9 08/30/15 JLI SW8260Cug/Kg1.6 1NDTetrahydrofuran (THF) 16 08/30/15 JLI SW8260Cug/Kg 14.0 1NDToluene 7.9 08/30/15 JLI SW8260Cug/Kg0.79 13.0trans-1,2-Dichloroethene 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1JNDtrans-1,3-Dichloropropene 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1NDtrans-1,4-dichloro-2-butene 16 08/30/15 JLI SW8260Cug/Kg4.0 1390Trichloroethene 240 08/31/15 JLI SW8260Cug/Kg24 50NDTrichlorofluoromethane 7.9 08/30/15 JLI SW8260Cug/Kg1.6 1NDTrichlorotrifluoroethane 7.9 08/30/15 JLI SW8260Cug/Kg0.79 116Vinyl chloride 7.9 08/30/15 JLI SW8260Cug/Kg0.79 1



14B4 (10-15)Phoenix I.D.: BJ81798



LOD/MDL Dilution





SemivolatilesND1,2,4,5-Tetrachlorobenzene 280 08/27/15 DD SW8270Dug/Kg140 1ND1,2,4-Trichlorobenzene 280 08/27/15 DD SW8270Dug/Kg120 1ND1,2-Dichlorobenzene 280 08/27/15 DD SW8270Dug/Kg110 1ND1,2-Diphenylhydrazine 280 08/27/15 DD SW8270Dug/Kg130 1ND1,3-Dichlorobenzene 280 08/27/15 DD SW8270Dug/Kg120 1ND1,4-Dichlorobenzene 280 08/27/15 DD SW8270Dug/Kg120 1ND2,4,5-Trichlorophenol 280 08/27/15 DD SW8270Dug/Kg220 1ND2,4,6-Trichlorophenol 280 08/27/15 DD SW8270Dug/Kg130 1ND2,4-Dichlorophenol 280 08/27/15 DD SW8270Dug/Kg140 1ND2,4-Dimethylphenol 280 08/27/15 DD SW8270Dug/Kg99 1ND2,4-Dinitrophenol 790 08/27/15 DD SW8270Dug/Kg280 1ND2,4-Dinitrotoluene 280 08/27/15 DD SW8270Dug/Kg160 1ND2,6-Dinitrotoluene 280 08/27/15 DD SW8270Dug/Kg130 1ND2-Chloronaphthalene 280 08/27/15 DD SW8270Dug/Kg110 1ND2-Chlorophenol 280 08/27/15 DD SW8270Dug/Kg110 1ND2-Methylnaphthalene 280 08/27/15 DD SW8270Dug/Kg120 1ND2-Methylphenol (o-cresol) 280 08/27/15 DD SW8270Dug/Kg190 1ND2-Nitroaniline 790 08/27/15 DD SW8270Dug/Kg400 1ND2-Nitrophenol 280 08/27/15 DD SW8270Dug/Kg250 1ND3&4-Methylphenol (m&p-cresol) 280 08/27/15 DD SW8270Dug/Kg 1160 1ND3,3'-Dichlorobenzidine 790 08/27/15 DD SW8270Dug/Kg190 1ND3-Nitroaniline 790 08/27/15 DD SW8270Dug/Kg790 1ND4,6-Dinitro-2-methylphenol 2000 08/27/15 DD SW8270Dug/Kg430 1ND4-Bromophenyl phenyl ether 280 08/27/15 DD SW8270Dug/Kg120 1ND4-Chloro-3-methylphenol 280 08/27/15 DD SW8270Dug/Kg140 1ND4-Chloroaniline 320 08/27/15 DD SW8270Dug/Kg190 1ND4-Chlorophenyl phenyl ether 280 08/27/15 DD SW8270Dug/Kg130 1ND4-Nitroaniline 790 08/27/15 DD SW8270Dug/Kg130 1ND4-Nitrophenol 400 08/27/15 DD SW8270Dug/Kg180 1190Acenaphthene 280 08/27/15 DD SW8270Dug/Kg120 1JNDAcenaphthylene 280 08/27/15 DD SW8270Dug/Kg110 1NDAcetophenone 280 08/27/15 DD SW8270Dug/Kg120 1


14B4 (10-15)Phoenix I.D.: BJ81798



LOD/MDL Dilution

NDAniline 320 08/27/15 DD SW8270Dug/Kg320 1240Anthracene 280 08/27/15 DD SW8270Dug/Kg130 1J

1800Benz(a)anthracene 280 08/27/15 DD SW8270Dug/Kg130 1NDBenzidine 790 08/27/15 DD SW8270Dug/Kg230 1

3600Benzo(a)pyrene 280 08/27/15 DD SW8270Dug/Kg130 12300Benzo(b)fluoranthene 280 08/27/15 DD SW8270Dug/Kg140 12900Benzo(ghi)perylene 280 08/27/15 DD SW8270Dug/Kg130 12900Benzo(k)fluoranthene 280 08/27/15 DD SW8270Dug/Kg130 1NDBenzoic acid 2000 08/27/15 DD SW8270Dug/Kg 1790 1NDBenzyl butyl phthalate 280 08/27/15 DD SW8270Dug/Kg100 1NDBis(2-chloroethoxy)methane 280 08/27/15 DD SW8270Dug/Kg110 1NDBis(2-chloroethyl)ether 280 08/27/15 DD SW8270Dug/Kg110 1NDBis(2-chloroisopropyl)ether 280 08/27/15 DD SW8270Dug/Kg 1110 1NDBis(2-ethylhexyl)phthalate 280 08/27/15 DD SW8270Dug/Kg110 1NDCarbazole 2000 08/27/15 DD SW8270Dug/Kg300 1

1800Chrysene 280 08/27/15 DD SW8270Dug/Kg130 1500Dibenz(a,h)anthracene 280 08/27/15 DD SW8270Dug/Kg130 1NDDibenzofuran 280 08/27/15 DD SW8270Dug/Kg120 1NDDiethyl phthalate 280 08/27/15 DD SW8270Dug/Kg130 1NDDimethylphthalate 280 08/27/15 DD SW8270Dug/Kg120 1NDDi-n-butylphthalate 280 08/27/15 DD SW8270Dug/Kg110 1NDDi-n-octylphthalate 280 08/27/15 DD SW8270Dug/Kg100 1

1300Fluoranthene 280 08/27/15 DD SW8270Dug/Kg130 1NDFluorene 280 08/27/15 DD SW8270Dug/Kg130 1NDHexachlorobenzene 280 08/27/15 DD SW8270Dug/Kg120 1NDHexachlorobutadiene 280 08/27/15 DD SW8270Dug/Kg140 1NDHexachlorocyclopentadiene 280 08/27/15 DD SW8270Dug/Kg120 1NDHexachloroethane 280 08/27/15 DD SW8270Dug/Kg120 1

3400Indeno(1,2,3-cd)pyrene 280 08/27/15 DD SW8270Dug/Kg130 1NDIsophorone 280 08/27/15 DD SW8270Dug/Kg110 1410Naphthalene 280 08/27/15 DD SW8270Dug/Kg110 1NDNitrobenzene 280 08/27/15 DD SW8270Dug/Kg140 1NDN-Nitrosodimethylamine 280 08/27/15 DD SW8270Dug/Kg110 1NDN-Nitrosodi-n-propylamine 280 08/27/15 DD SW8270Dug/Kg130 1NDN-Nitrosodiphenylamine 280 08/27/15 DD SW8270Dug/Kg150 1NDPentachloronitrobenzene 280 08/27/15 DD SW8270Dug/Kg150 1NDPentachlorophenol 280 08/27/15 DD SW8270Dug/Kg150 1700Phenanthrene 280 08/27/15 DD SW8270Dug/Kg110 1NDPhenol 280 08/27/15 DD SW8270Dug/Kg130 1




14B4 (10-15)Phoenix I.D.: BJ81798



LOD/MDL Dilution

Comments:











SOLIDEBC72 Hour


RB

Laboratory Data

14B4 (20-21)

Phoenix ID: BJ81799

08/26/1514:0017:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution



11300Calcium 4.0 08/28/15 LK SW6010Cmg/Kg3.6 1< 0.40Cadmium 0.40 08/28/15 LK SW6010Cmg/Kg0.16 15.40Cobalt 0.40 08/28/15 LK SW6010Cmg/Kg0.40 115.7Chromium 0.40 08/28/15 LK SW6010Cmg/Kg0.40 115.7Copper 0.40 08/28/15 LK SW6010Cmg/kg0.40 1

16700Iron 40 08/28/15 LK SW6010Cmg/Kg B40 100.06Mercury 0.03 08/27/15 RS SW7471Bmg/Kg0.02 11150Potassium 8 08/28/15 LK SW6010Cmg/Kg3.1 1N10100Magnesium 40 08/28/15 LK SW6010Cmg/Kg40 10649Manganese 4.0 08/28/15 LK SW6010Cmg/Kg4.0 10

1100Sodium 8 08/28/15 LK SW6010Cmg/Kg3.4 1N11.9Nickel 0.40 08/28/15 LK SW6010Cmg/Kg0.40 150.8Lead 0.8 08/28/15 LK SW6010Cmg/Kg0.40 1< 2.0Antimony 2.0 08/28/15 LK SW6010Cmg/Kg2.0 1N< 1.6Selenium 1.6 08/28/15 LK SW6010Cmg/Kg1.3 1< 1.6Thallium 1.6 08/28/15 LK SW6010Cmg/Kg1.6 130.3Vanadium 0.4 08/28/15 LK SW6010Cmg/Kg0.40 128.4Zinc 0.8 08/31/15 LK SW6010Cmg/Kg B0.40 179Percent Solid 08/26/15 I SW846-%Solid%



14B4 (20-21)Phoenix I.D.: BJ81799



LOD/MDL Dilution




Pesticides - SoilND4,4' -DDD 60 08/28/15 CE SW8081Bug/Kg60 20ND4,4' -DDE 40 08/28/15 CE SW8081Bug/Kg40 20ND4,4' -DDT 30 08/28/15 CE SW8081Bug/Kg30 20NDa-BHC 41 08/28/15 CE SW8081Bug/Kg41 20170a-Chlordane 41 08/28/15 CE SW8081Bug/Kg41 20NDAldrin 12 08/28/15 CE SW8081Bug/Kg12 20NDb-BHC 41 08/28/15 CE SW8081Bug/Kg41 20NDd-BHC 41 08/28/15 CE SW8081Bug/Kg41 20NDDieldrin 12 08/28/15 CE SW8081Bug/Kg12 20NDEndosulfan I 82 08/28/15 CE SW8081Bug/Kg82 20NDEndosulfan II 82 08/28/15 CE SW8081Bug/Kg82 20NDEndosulfan sulfate 82 08/28/15 CE SW8081Bug/Kg82 20NDEndrin 41 08/28/15 CE SW8081Bug/Kg41 20NDEndrin aldehyde 82 08/28/15 CE SW8081Bug/Kg82 20NDEndrin ketone 82 08/28/15 CE SW8081Bug/Kg82 20NDg-BHC 30 08/28/15 CE SW8081Bug/Kg30 2099g-Chlordane 41 08/28/15 CE SW8081Bug/Kg41 20NDHeptachlor 41 08/28/15 CE SW8081Bug/Kg41 20NDHeptachlor epoxide 82 08/28/15 CE SW8081Bug/Kg82 20NDMethoxychlor 410 08/28/15 CE SW8081Bug/Kg410 20NDToxaphene 1600 08/28/15 CE SW8081Bug/Kg1600 20




14B4 (20-21)Phoenix I.D.: BJ81799



LOD/MDL Dilution

ND1,1-Dichloropropene 6000 08/30/15 JLI SW8260Cug/Kg600 714ND1,2,3-Trichlorobenzene 6000 08/30/15 JLI SW8260Cug/Kg1200 714ND1,2,3-Trichloropropane 6000 08/30/15 JLI SW8260Cug/Kg600 714ND1,2,4-Trichlorobenzene 6000 08/30/15 JLI SW8260Cug/Kg1200 714

270001,2,4-Trimethylbenzene 6000 08/30/15 JLI SW8260Cug/Kg600 714ND1,2-Dibromo-3-chloropropane 6000 08/30/15 JLI SW8260Cug/Kg1200 714ND1,2-Dibromoethane 6000 08/30/15 JLI SW8260Cug/Kg600 714ND1,2-Dichlorobenzene 6000 08/30/15 JLI SW8260Cug/Kg600 714ND1,2-Dichloroethane 6000 08/30/15 JLI SW8260Cug/Kg600 714ND1,2-Dichloropropane 6000 08/30/15 JLI SW8260Cug/Kg1200 714

160001,3,5-Trimethylbenzene 6000 08/30/15 JLI SW8260Cug/Kg600 714ND1,3-Dichlorobenzene 6000 08/30/15 JLI SW8260Cug/Kg600 714ND1,3-Dichloropropane 6000 08/30/15 JLI SW8260Cug/Kg1200 714ND1,4-Dichlorobenzene 6000 08/30/15 JLI SW8260Cug/Kg600 714ND2,2-Dichloropropane 6000 08/30/15 JLI SW8260Cug/Kg600 714ND2-Chlorotoluene 6000 08/30/15 JLI SW8260Cug/Kg1200 714ND2-Hexanone 30000 08/30/15 JLI SW8260Cug/Kg6000 714ND2-Isopropyltoluene 6000 08/30/15 JLI SW8260Cug/Kg 1600 714ND4-Chlorotoluene 6000 08/30/15 JLI SW8260Cug/Kg600 714ND4-Methyl-2-pentanone 30000 08/30/15 JLI SW8260Cug/Kg6000 714NDAcetone 60000 08/30/15 JLI SW8260Cug/Kg6000 714NDAcrylonitrile 12000 08/30/15 JLI SW8260Cug/Kg1200 714

8600Benzene 6000 08/30/15 JLI SW8260Cug/Kg600 714NDBromobenzene 6000 08/30/15 JLI SW8260Cug/Kg600 714NDBromochloromethane 6000 08/30/15 JLI SW8260Cug/Kg600 714NDBromodichloromethane 6000 08/30/15 JLI SW8260Cug/Kg1200 714NDBromoform 6000 08/30/15 JLI SW8260Cug/Kg1200 714NDBromomethane 6000 08/30/15 JLI SW8260Cug/Kg2400 714NDCarbon Disulfide 6000 08/30/15 JLI SW8260Cug/Kg1200 714NDCarbon tetrachloride 6000 08/30/15 JLI SW8260Cug/Kg1200 714NDChlorobenzene 6000 08/30/15 JLI SW8260Cug/Kg600 714NDChloroethane 6000 08/30/15 JLI SW8260Cug/Kg600 714NDChloroform 6000 08/30/15 JLI SW8260Cug/Kg600 714NDChloromethane 6000 08/30/15 JLI SW8260Cug/Kg1200 714730cis-1,2-Dichloroethene 6000 08/30/15 JLI SW8260Cug/Kg600 714JNDcis-1,3-Dichloropropene 6000 08/30/15 JLI SW8260Cug/Kg600 714NDDibromochloromethane 6000 08/30/15 JLI SW8260Cug/Kg1200 714NDDibromomethane 6000 08/30/15 JLI SW8260Cug/Kg1200 714NDDichlorodifluoromethane 6000 08/30/15 JLI SW8260Cug/Kg600 714

21000Ethylbenzene 6000 08/30/15 JLI SW8260Cug/Kg600 714NDHexachlorobutadiene 6000 08/30/15 JLI SW8260Cug/Kg600 714910Isopropylbenzene 6000 08/30/15 JLI SW8260Cug/Kg600 714J

62000m&p-Xylene 6000 08/30/15 JLI SW8260Cug/Kg1200 714NDMethyl Ethyl Ketone 36000 08/30/15 JLI SW8260Cug/Kg6000 714NDMethyl t-butyl ether (MTBE) 12000 08/30/15 JLI SW8260Cug/Kg1200 714NDMethylene chloride 6000 08/30/15 JLI SW8260Cug/Kg6000 714

620000Naphthalene 85000 08/31/15 JLI SW8260Cug/Kg17000 10000DNDn-Butylbenzene 6000 08/30/15 JLI SW8260Cug/Kg600 714NDn-Propylbenzene 6000 08/30/15 JLI SW8260Cug/Kg1100 714


14B4 (20-21)Phoenix I.D.: BJ81799



LOD/MDL Dilution

21000o-Xylene 6000 08/30/15 JLI SW8260Cug/Kg1200 714780p-Isopropyltoluene 6000 08/30/15 JLI SW8260Cug/Kg600 714JNDsec-Butylbenzene 6000 08/30/15 JLI SW8260Cug/Kg600 714

1100Styrene 6000 08/30/15 JLI SW8260Cug/Kg600 714JNDtert-Butylbenzene 6000 08/30/15 JLI SW8260Cug/Kg600 714NDTetrachloroethene 6000 08/30/15 JLI SW8260Cug/Kg1200 714NDTetrahydrofuran (THF) 12000 08/30/15 JLI SW8260Cug/Kg 13000 714

22000Toluene 6000 08/30/15 JLI SW8260Cug/Kg600 714NDtrans-1,2-Dichloroethene 6000 08/30/15 JLI SW8260Cug/Kg600 714NDtrans-1,3-Dichloropropene 6000 08/30/15 JLI SW8260Cug/Kg600 714NDtrans-1,4-dichloro-2-butene 12000 08/30/15 JLI SW8260Cug/Kg3000 714NDTrichloroethene 6000 08/30/15 JLI SW8260Cug/Kg600 714NDTrichlorofluoromethane 6000 08/30/15 JLI SW8260Cug/Kg1200 714NDTrichlorotrifluoroethane 6000 08/30/15 JLI SW8260Cug/Kg600 714NDVinyl chloride 6000 08/30/15 JLI SW8260Cug/Kg600 714







14B4 (20-21)Phoenix I.D.: BJ81799



LOD/MDL Dilution

740002-Methylnaphthalene 2900 08/27/15 DD SW8270Dug/Kg1200 10ND2-Methylphenol (o-cresol) 2900 08/27/15 DD SW8270Dug/Kg1900 10ND2-Nitroaniline 8200 08/27/15 DD SW8270Dug/Kg4200 10ND2-Nitrophenol 2900 08/27/15 DD SW8270Dug/Kg2600 10ND3&4-Methylphenol (m&p-cresol) 2900 08/27/15 DD SW8270Dug/Kg 11600 10ND3,3'-Dichlorobenzidine 8200 08/27/15 DD SW8270Dug/Kg1900 10ND3-Nitroaniline 8200 08/27/15 DD SW8270Dug/Kg8200 10ND4,6-Dinitro-2-methylphenol 21000 08/27/15 DD SW8270Dug/Kg4400 10ND4-Bromophenyl phenyl ether 2900 08/27/15 DD SW8270Dug/Kg1200 10ND4-Chloro-3-methylphenol 2900 08/27/15 DD SW8270Dug/Kg1400 10ND4-Chloroaniline 3300 08/27/15 DD SW8270Dug/Kg1900 10ND4-Chlorophenyl phenyl ether 2900 08/27/15 DD SW8270Dug/Kg1400 10ND4-Nitroaniline 8200 08/27/15 DD SW8270Dug/Kg1400 10ND4-Nitrophenol 4100 08/27/15 DD SW8270Dug/Kg1900 10

12000Acenaphthene 2900 08/27/15 DD SW8270Dug/Kg1300 1020000Acenaphthylene 2900 08/27/15 DD SW8270Dug/Kg1200 10

NDAcetophenone 2900 08/27/15 DD SW8270Dug/Kg1300 10NDAniline 3300 08/27/15 DD SW8270Dug/Kg3300 10

50000Anthracene 2900 08/27/15 DD SW8270Dug/Kg1300 1041000Benz(a)anthracene 2900 08/27/15 DD SW8270Dug/Kg1400 10



20000Carbazole 21000 08/27/15 DD SW8270Dug/Kg3100 10J38000Chrysene 2900 08/27/15 DD SW8270Dug/Kg1400 103800Dibenz(a,h)anthracene 2900 08/27/15 DD SW8270Dug/Kg1300 1043000Dibenzofuran 2900 08/27/15 DD SW8270Dug/Kg1200 10

NDDiethyl phthalate 2900 08/27/15 DD SW8270Dug/Kg1300 10NDDimethylphthalate 2900 08/27/15 DD SW8270Dug/Kg1300 10NDDi-n-butylphthalate 2900 08/27/15 DD SW8270Dug/Kg1100 10NDDi-n-octylphthalate 2900 08/27/15 DD SW8270Dug/Kg1100 10

70000Fluoranthene 14000 08/27/15 DD SW8270Dug/Kg6700 50D66000Fluorene 2900 08/27/15 DD SW8270Dug/Kg1400 10

NDHexachlorobenzene 2900 08/27/15 DD SW8270Dug/Kg1200 10NDHexachlorobutadiene 2900 08/27/15 DD SW8270Dug/Kg1500 10NDHexachlorocyclopentadiene 2900 08/27/15 DD SW8270Dug/Kg1300 10NDHexachloroethane 2900 08/27/15 DD SW8270Dug/Kg1200 10


190000Naphthalene 14000 08/27/15 DD SW8270Dug/Kg5900 50DNDNitrobenzene 2900 08/27/15 DD SW8270Dug/Kg1400 10


14B4 (20-21)Phoenix I.D.: BJ81799



LOD/MDL Dilution


140000Phenanthrene 14000 08/27/15 DD SW8270Dug/Kg5900 50DNDPhenol 2900 08/27/15 DD SW8270Dug/Kg1300 10



Comments:














SOLIDEBC72 Hour


RB

Laboratory Data

14B5 (0-5)

Phoenix ID: BJ81800

08/26/1514:1517:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution



14300Calcium 32 08/28/15 LK SW6010Cmg/Kg30 10< 0.32Cadmium 0.32 08/28/15 LK SW6010Cmg/Kg0.13 16.94Cobalt 0.32 08/28/15 LK SW6010Cmg/Kg0.32 119.2Chromium 0.32 08/28/15 LK SW6010Cmg/Kg0.32 126.0Copper 0.32 08/28/15 LK SW6010Cmg/kg0.32 1

14900Iron 32 08/28/15 LK SW6010Cmg/Kg B32 100.23Mercury 0.03 08/27/15 RS SW7471Bmg/Kg0.02 11940Potassium 6 08/28/15 LK SW6010Cmg/Kg2.5 1N5620Magnesium 32 08/28/15 LK SW6010Cmg/Kg32 10294Manganese 3.2 08/28/15 LK SW6010Cmg/Kg3.2 10321Sodium 6 08/28/15 LK SW6010Cmg/Kg2.8 1N16.1Nickel 0.32 08/28/15 LK SW6010Cmg/Kg0.32 155.5Lead 0.6 08/28/15 LK SW6010Cmg/Kg0.32 1< 1.6Antimony 1.6 08/28/15 LK SW6010Cmg/Kg1.6 1N< 1.3Selenium 1.3 08/28/15 LK SW6010Cmg/Kg1.1 1< 1.3Thallium 1.3 08/28/15 LK SW6010Cmg/Kg1.3 129.7Vanadium 0.3 08/28/15 LK SW6010Cmg/Kg0.32 163.9Zinc 0.6 08/28/15 LK SW6010Cmg/Kg B0.32 192Percent Solid 08/26/15 I SW846-%Solid%



14B5 (0-5)Phoenix I.D.: BJ81800



LOD/MDL Dilution








14B5 (0-5)Phoenix I.D.: BJ81800



LOD/MDL Dilution

ND1,1-Dichloropropene 4.8 08/30/15 JLI SW8260Cug/Kg0.48 1ND1,2,3-Trichlorobenzene 230 08/31/15 JLI SW8260Cug/Kg47 50ND1,2,3-Trichloropropane 230 08/31/15 JLI SW8260Cug/Kg23 50ND1,2,4-Trichlorobenzene 230 08/31/15 JLI SW8260Cug/Kg47 50ND1,2,4-Trimethylbenzene 230 08/31/15 JLI SW8260Cug/Kg23 50ND1,2-Dibromo-3-chloropropane 230 08/31/15 JLI SW8260Cug/Kg47 50ND1,2-Dibromoethane 4.8 08/30/15 JLI SW8260Cug/Kg0.48 1ND1,2-Dichlorobenzene 230 08/31/15 JLI SW8260Cug/Kg23 50ND1,2-Dichloroethane 4.8 08/30/15 JLI SW8260Cug/Kg0.48 1ND1,2-Dichloropropane 4.8 08/30/15 JLI SW8260Cug/Kg0.97 1ND1,3,5-Trimethylbenzene 230 08/31/15 JLI SW8260Cug/Kg23 50ND1,3-Dichlorobenzene 230 08/31/15 JLI SW8260Cug/Kg23 50ND1,3-Dichloropropane 4.8 08/30/15 JLI SW8260Cug/Kg0.97 1ND1,4-Dichlorobenzene 230 08/31/15 JLI SW8260Cug/Kg23 50ND2,2-Dichloropropane 4.8 08/30/15 JLI SW8260Cug/Kg0.48 1ND2-Chlorotoluene 230 08/31/15 JLI SW8260Cug/Kg47 50ND2-Hexanone 24 08/30/15 JLI SW8260Cug/Kg4.8 1ND2-Isopropyltoluene 230 08/31/15 JLI SW8260Cug/Kg 123 50ND4-Chlorotoluene 230 08/31/15 JLI SW8260Cug/Kg23 50ND4-Methyl-2-pentanone 24 08/30/15 JLI SW8260Cug/Kg4.8 111Acetone 48 08/30/15 JLI SW8260Cug/Kg4.8 1JSNDAcrylonitrile 9.7 08/30/15 JLI SW8260Cug/Kg0.97 10.78Benzene 4.8 08/30/15 JLI SW8260Cug/Kg0.48 1JNDBromobenzene 230 08/31/15 JLI SW8260Cug/Kg23 50NDBromochloromethane 4.8 08/30/15 JLI SW8260Cug/Kg0.48 1NDBromodichloromethane 4.8 08/30/15 JLI SW8260Cug/Kg0.97 1NDBromoform 4.8 08/30/15 JLI SW8260Cug/Kg0.97 1NDBromomethane 4.8 08/30/15 JLI SW8260Cug/Kg1.9 1NDCarbon Disulfide 4.8 08/30/15 JLI SW8260Cug/Kg0.97 1NDCarbon tetrachloride 4.8 08/30/15 JLI SW8260Cug/Kg0.97 1NDChlorobenzene 4.8 08/30/15 JLI SW8260Cug/Kg0.48 1NDChloroethane 4.8 08/30/15 JLI SW8260Cug/Kg0.48 1NDChloroform 4.8 08/30/15 JLI SW8260Cug/Kg0.48 1NDChloromethane 4.8 08/30/15 JLI SW8260Cug/Kg0.97 13.7cis-1,2-Dichloroethene 4.8 08/30/15 JLI SW8260Cug/Kg0.48 1JNDcis-1,3-Dichloropropene 4.8 08/30/15 JLI SW8260Cug/Kg0.48 1NDDibromochloromethane 4.8 08/30/15 JLI SW8260Cug/Kg0.97 1NDDibromomethane 4.8 08/30/15 JLI SW8260Cug/Kg0.97 1NDDichlorodifluoromethane 4.8 08/30/15 JLI SW8260Cug/Kg0.48 1NDEthylbenzene 4.8 08/30/15 JLI SW8260Cug/Kg0.48 1NDHexachlorobutadiene 230 08/31/15 JLI SW8260Cug/Kg23 50NDIsopropylbenzene 230 08/31/15 JLI SW8260Cug/Kg23 50NDm&p-Xylene 4.8 08/30/15 JLI SW8260Cug/Kg0.97 1NDMethyl Ethyl Ketone 29 08/30/15 JLI SW8260Cug/Kg4.8 1NDMethyl t-butyl ether (MTBE) 9.7 08/30/15 JLI SW8260Cug/Kg0.97 1NDMethylene chloride 4.8 08/30/15 JLI SW8260Cug/Kg4.8 1210Naphthalene 230 08/31/15 JLI SW8260Cug/Kg47 50JNDn-Butylbenzene 230 08/31/15 JLI SW8260Cug/Kg23 50NDn-Propylbenzene 230 08/31/15 JLI SW8260Cug/Kg42 50


14B5 (0-5)Phoenix I.D.: BJ81800



LOD/MDL Dilution

NDo-Xylene 4.8 08/30/15 JLI SW8260Cug/Kg0.97 1NDp-Isopropyltoluene 230 08/31/15 JLI SW8260Cug/Kg23 50NDsec-Butylbenzene 230 08/31/15 JLI SW8260Cug/Kg23 50NDStyrene 4.8 08/30/15 JLI SW8260Cug/Kg0.48 1NDtert-Butylbenzene 230 08/31/15 JLI SW8260Cug/Kg23 50NDTetrachloroethene 4.8 08/30/15 JLI SW8260Cug/Kg0.97 1NDTetrahydrofuran (THF) 9.7 08/30/15 JLI SW8260Cug/Kg 12.4 1NDToluene 4.8 08/30/15 JLI SW8260Cug/Kg0.48 1NDtrans-1,2-Dichloroethene 4.8 08/30/15 JLI SW8260Cug/Kg0.48 1NDtrans-1,3-Dichloropropene 4.8 08/30/15 JLI SW8260Cug/Kg0.48 1NDtrans-1,4-dichloro-2-butene 470 08/31/15 JLI SW8260Cug/Kg120 5056Trichloroethene 230 08/31/15 JLI SW8260Cug/Kg23 50JNDTrichlorofluoromethane 4.8 08/30/15 JLI SW8260Cug/Kg0.97 1NDTrichlorotrifluoroethane 4.8 08/30/15 JLI SW8260Cug/Kg0.48 1NDVinyl chloride 4.8 08/30/15 JLI SW8260Cug/Kg0.48 1







14B5 (0-5)Phoenix I.D.: BJ81800



LOD/MDL Dilution

ND2-Methylnaphthalene 250 08/27/15 DD SW8270Dug/Kg110 1ND2-Methylphenol (o-cresol) 250 08/27/15 DD SW8270Dug/Kg170 1ND2-Nitroaniline 720 08/27/15 DD SW8270Dug/Kg360 1ND2-Nitrophenol 250 08/27/15 DD SW8270Dug/Kg230 1ND3&4-Methylphenol (m&p-cresol) 250 08/27/15 DD SW8270Dug/Kg 1140 1ND3,3'-Dichlorobenzidine 720 08/27/15 DD SW8270Dug/Kg170 1ND3-Nitroaniline 720 08/27/15 DD SW8270Dug/Kg720 1ND4,6-Dinitro-2-methylphenol 1800 08/27/15 DD SW8270Dug/Kg390 1ND4-Bromophenyl phenyl ether 250 08/27/15 DD SW8270Dug/Kg110 1ND4-Chloro-3-methylphenol 250 08/27/15 DD SW8270Dug/Kg130 1ND4-Chloroaniline 290 08/27/15 DD SW8270Dug/Kg170 1ND4-Chlorophenyl phenyl ether 250 08/27/15 DD SW8270Dug/Kg120 1ND4-Nitroaniline 720 08/27/15 DD SW8270Dug/Kg120 1ND4-Nitrophenol 360 08/27/15 DD SW8270Dug/Kg160 1NDAcenaphthene 250 08/27/15 DD SW8270Dug/Kg110 1120Acenaphthylene 250 08/27/15 DD SW8270Dug/Kg100 1JNDAcetophenone 250 08/27/15 DD SW8270Dug/Kg110 1NDAniline 290 08/27/15 DD SW8270Dug/Kg290 1210Anthracene 250 08/27/15 DD SW8270Dug/Kg120 1J850Benz(a)anthracene 250 08/27/15 DD SW8270Dug/Kg120 1NDBenzidine 720 08/27/15 DD SW8270Dug/Kg210 1

1000Benzo(a)pyrene 250 08/27/15 DD SW8270Dug/Kg120 1980Benzo(b)fluoranthene 250 08/27/15 DD SW8270Dug/Kg120 1660Benzo(ghi)perylene 250 08/27/15 DD SW8270Dug/Kg120 1870Benzo(k)fluoranthene 250 08/27/15 DD SW8270Dug/Kg120 1NDBenzoic acid 1800 08/27/15 DD SW8270Dug/Kg 1720 1NDBenzyl butyl phthalate 250 08/27/15 DD SW8270Dug/Kg93 1NDBis(2-chloroethoxy)methane 250 08/27/15 DD SW8270Dug/Kg100 1NDBis(2-chloroethyl)ether 250 08/27/15 DD SW8270Dug/Kg97 1NDBis(2-chloroisopropyl)ether 250 08/27/15 DD SW8270Dug/Kg 1100 1140Bis(2-ethylhexyl)phthalate 250 08/27/15 DD SW8270Dug/Kg100 1JNDCarbazole 1800 08/27/15 DD SW8270Dug/Kg270 1910Chrysene 250 08/27/15 DD SW8270Dug/Kg120 1250Dibenz(a,h)anthracene 250 08/27/15 DD SW8270Dug/Kg120 1NDDibenzofuran 250 08/27/15 DD SW8270Dug/Kg110 1NDDiethyl phthalate 250 08/27/15 DD SW8270Dug/Kg110 1NDDimethylphthalate 250 08/27/15 DD SW8270Dug/Kg110 1NDDi-n-butylphthalate 250 08/27/15 DD SW8270Dug/Kg96 1NDDi-n-octylphthalate 250 08/27/15 DD SW8270Dug/Kg93 1



14B5 (0-5)Phoenix I.D.: BJ81800



LOD/MDL Dilution

NDN-Nitrosodimethylamine 250 08/27/15 DD SW8270Dug/Kg100 1NDN-Nitrosodi-n-propylamine 250 08/27/15 DD SW8270Dug/Kg120 1NDN-Nitrosodiphenylamine 250 08/27/15 DD SW8270Dug/Kg140 1NDPentachloronitrobenzene 250 08/27/15 DD SW8270Dug/Kg130 1NDPentachlorophenol 250 08/27/15 DD SW8270Dug/Kg140 1750Phenanthrene 250 08/27/15 DD SW8270Dug/Kg100 1NDPhenol 250 08/27/15 DD SW8270Dug/Kg120 1



Comments:




Pesticide Comment:Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, an elevated RL was reported.Sample was evaluated against an external standard.











SOLIDEBC72 Hour


RB

Laboratory Data

14B5 (10-15)

Phoenix ID: BJ81801

08/26/1514:3017:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution


VolatilesND1,1,1,2-Tetrachloroethane 4.3 08/31/15 JLI SW8260Cug/Kg0.86 1ND1,1,1-Trichloroethane 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1ND1,1,2,2-Tetrachloroethane 4.3 08/31/15 JLI SW8260Cug/Kg0.86 1ND1,1,2-Trichloroethane 4.3 08/31/15 JLI SW8260Cug/Kg0.86 1ND1,1-Dichloroethane 4.3 08/31/15 JLI SW8260Cug/Kg0.86 1ND1,1-Dichloroethene 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1ND1,1-Dichloropropene 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1ND1,2,3-Trichlorobenzene 250 09/01/15 JLI SW8260Cug/Kg49 50ND1,2,3-Trichloropropane 250 09/01/15 JLI SW8260Cug/Kg25 50ND1,2,4-Trichlorobenzene 250 09/01/15 JLI SW8260Cug/Kg49 50ND1,2,4-Trimethylbenzene 250 09/01/15 JLI SW8260Cug/Kg25 50ND1,2-Dibromo-3-chloropropane 250 09/01/15 JLI SW8260Cug/Kg49 50ND1,2-Dibromoethane 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1ND1,2-Dichlorobenzene 250 09/01/15 JLI SW8260Cug/Kg25 50ND1,2-Dichloroethane 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1ND1,2-Dichloropropane 4.3 08/31/15 JLI SW8260Cug/Kg0.86 1ND1,3,5-Trimethylbenzene 250 09/01/15 JLI SW8260Cug/Kg25 50ND1,3-Dichlorobenzene 250 09/01/15 JLI SW8260Cug/Kg25 50ND1,3-Dichloropropane 4.3 08/31/15 JLI SW8260Cug/Kg0.86 1ND1,4-Dichlorobenzene 250 09/01/15 JLI SW8260Cug/Kg25 50ND2,2-Dichloropropane 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1ND2-Chlorotoluene 250 09/01/15 JLI SW8260Cug/Kg49 50ND2-Hexanone 21 08/31/15 JLI SW8260Cug/Kg4.3 1


14B5 (10-15)Phoenix I.D.: BJ81801



LOD/MDL Dilution

ND2-Isopropyltoluene 250 09/01/15 JLI SW8260Cug/Kg 125 50ND4-Chlorotoluene 250 09/01/15 JLI SW8260Cug/Kg25 50ND4-Methyl-2-pentanone 21 08/31/15 JLI SW8260Cug/Kg4.3 16.4Acetone 43 08/31/15 JLI SW8260Cug/Kg4.3 1JSNDAcrylonitrile 8.6 08/31/15 JLI SW8260Cug/Kg0.86 10.44Benzene 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1JNDBromobenzene 250 09/01/15 JLI SW8260Cug/Kg25 50NDBromochloromethane 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1NDBromodichloromethane 4.3 08/31/15 JLI SW8260Cug/Kg0.86 1NDBromoform 4.3 08/31/15 JLI SW8260Cug/Kg0.86 1NDBromomethane 4.3 08/31/15 JLI SW8260Cug/Kg1.7 1NDCarbon Disulfide 4.3 08/31/15 JLI SW8260Cug/Kg0.86 1NDCarbon tetrachloride 4.3 08/31/15 JLI SW8260Cug/Kg0.86 1NDChlorobenzene 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1NDChloroethane 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1NDChloroform 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1NDChloromethane 4.3 08/31/15 JLI SW8260Cug/Kg0.86 11.6cis-1,2-Dichloroethene 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1JNDcis-1,3-Dichloropropene 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1NDDibromochloromethane 4.3 08/31/15 JLI SW8260Cug/Kg0.86 1NDDibromomethane 4.3 08/31/15 JLI SW8260Cug/Kg0.86 1NDDichlorodifluoromethane 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1NDEthylbenzene 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1NDHexachlorobutadiene 250 09/01/15 JLI SW8260Cug/Kg25 50NDIsopropylbenzene 250 09/01/15 JLI SW8260Cug/Kg25 50NDm&p-Xylene 4.3 08/31/15 JLI SW8260Cug/Kg0.86 1NDMethyl Ethyl Ketone 26 08/31/15 JLI SW8260Cug/Kg4.3 1NDMethyl t-butyl ether (MTBE) 8.6 08/31/15 JLI SW8260Cug/Kg0.86 1NDMethylene chloride 4.3 08/31/15 JLI SW8260Cug/Kg4.3 150Naphthalene 250 09/01/15 JLI SW8260Cug/Kg49 50JNDn-Butylbenzene 250 09/01/15 JLI SW8260Cug/Kg25 50NDn-Propylbenzene 250 09/01/15 JLI SW8260Cug/Kg44 50NDo-Xylene 4.3 08/31/15 JLI SW8260Cug/Kg0.86 1NDp-Isopropyltoluene 250 09/01/15 JLI SW8260Cug/Kg25 50NDsec-Butylbenzene 250 09/01/15 JLI SW8260Cug/Kg25 50NDStyrene 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1NDtert-Butylbenzene 250 09/01/15 JLI SW8260Cug/Kg25 50NDTetrachloroethene 4.3 08/31/15 JLI SW8260Cug/Kg0.86 1NDTetrahydrofuran (THF) 8.6 08/31/15 JLI SW8260Cug/Kg 12.1 1NDToluene 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1NDtrans-1,2-Dichloroethene 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1NDtrans-1,3-Dichloropropene 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1NDtrans-1,4-dichloro-2-butene 490 09/01/15 JLI SW8260Cug/Kg120 5051Trichloroethene 250 09/01/15 JLI SW8260Cug/Kg25 50JNDTrichlorofluoromethane 4.3 08/31/15 JLI SW8260Cug/Kg0.86 1NDTrichlorotrifluoroethane 4.3 08/31/15 JLI SW8260Cug/Kg0.43 10.48Vinyl chloride 4.3 08/31/15 JLI SW8260Cug/Kg0.43 1J



14B5 (10-15)Phoenix I.D.: BJ81801



LOD/MDL Dilution





SemivolatilesND1,2,4,5-Tetrachlorobenzene 260 08/27/15 DD SW8270Dug/Kg130 1ND1,2,4-Trichlorobenzene 260 08/27/15 DD SW8270Dug/Kg110 1ND1,2-Dichlorobenzene 260 08/27/15 DD SW8270Dug/Kg100 1ND1,2-Diphenylhydrazine 260 08/27/15 DD SW8270Dug/Kg120 1ND1,3-Dichlorobenzene 260 08/27/15 DD SW8270Dug/Kg110 1ND1,4-Dichlorobenzene 260 08/27/15 DD SW8270Dug/Kg110 1ND2,4,5-Trichlorophenol 260 08/27/15 DD SW8270Dug/Kg200 1ND2,4,6-Trichlorophenol 260 08/27/15 DD SW8270Dug/Kg120 1ND2,4-Dichlorophenol 260 08/27/15 DD SW8270Dug/Kg130 1ND2,4-Dimethylphenol 260 08/27/15 DD SW8270Dug/Kg90 1ND2,4-Dinitrophenol 730 08/27/15 DD SW8270Dug/Kg260 1ND2,4-Dinitrotoluene 260 08/27/15 DD SW8270Dug/Kg140 1ND2,6-Dinitrotoluene 260 08/27/15 DD SW8270Dug/Kg120 1ND2-Chloronaphthalene 260 08/27/15 DD SW8270Dug/Kg100 1ND2-Chlorophenol 260 08/27/15 DD SW8270Dug/Kg100 11102-Methylnaphthalene 260 08/27/15 DD SW8270Dug/Kg110 1JND2-Methylphenol (o-cresol) 260 08/27/15 DD SW8270Dug/Kg170 1ND2-Nitroaniline 730 08/27/15 DD SW8270Dug/Kg370 1ND2-Nitrophenol 260 08/27/15 DD SW8270Dug/Kg230 1ND3&4-Methylphenol (m&p-cresol) 260 08/27/15 DD SW8270Dug/Kg 1140 1ND3,3'-Dichlorobenzidine 730 08/27/15 DD SW8270Dug/Kg170 1ND3-Nitroaniline 730 08/27/15 DD SW8270Dug/Kg730 1ND4,6-Dinitro-2-methylphenol 1800 08/27/15 DD SW8270Dug/Kg390 1ND4-Bromophenyl phenyl ether 260 08/27/15 DD SW8270Dug/Kg110 1ND4-Chloro-3-methylphenol 260 08/27/15 DD SW8270Dug/Kg130 1ND4-Chloroaniline 290 08/27/15 DD SW8270Dug/Kg170 1ND4-Chlorophenyl phenyl ether 260 08/27/15 DD SW8270Dug/Kg120 1ND4-Nitroaniline 730 08/27/15 DD SW8270Dug/Kg120 1ND4-Nitrophenol 360 08/27/15 DD SW8270Dug/Kg160 1NDAcenaphthene 260 08/27/15 DD SW8270Dug/Kg110 1460Acenaphthylene 260 08/27/15 DD SW8270Dug/Kg100 1NDAcetophenone 260 08/27/15 DD SW8270Dug/Kg110 1


14B5 (10-15)Phoenix I.D.: BJ81801



LOD/MDL Dilution

NDAniline 290 08/27/15 DD SW8270Dug/Kg290 11400Anthracene 260 08/27/15 DD SW8270Dug/Kg120 12700Benz(a)anthracene 260 08/27/15 DD SW8270Dug/Kg120 1NDBenzidine 730 08/27/15 DD SW8270Dug/Kg210 1

3000Benzo(a)pyrene 260 08/27/15 DD SW8270Dug/Kg120 12200Benzo(b)fluoranthene 260 08/27/15 DD SW8270Dug/Kg120 11300Benzo(ghi)perylene 260 08/27/15 DD SW8270Dug/Kg120 12700Benzo(k)fluoranthene 260 08/27/15 DD SW8270Dug/Kg120 1NDBenzoic acid 1800 08/27/15 DD SW8270Dug/Kg 1730 1NDBenzyl butyl phthalate 260 08/27/15 DD SW8270Dug/Kg94 1NDBis(2-chloroethoxy)methane 260 08/27/15 DD SW8270Dug/Kg100 1NDBis(2-chloroethyl)ether 260 08/27/15 DD SW8270Dug/Kg98 1NDBis(2-chloroisopropyl)ether 260 08/27/15 DD SW8270Dug/Kg 1100 1NDBis(2-ethylhexyl)phthalate 260 08/27/15 DD SW8270Dug/Kg100 1280Carbazole 1800 08/27/15 DD SW8270Dug/Kg280 1J

2600Chrysene 260 08/27/15 DD SW8270Dug/Kg120 1440Dibenz(a,h)anthracene 260 08/27/15 DD SW8270Dug/Kg120 1470Dibenzofuran 260 08/27/15 DD SW8270Dug/Kg110 1NDDiethyl phthalate 260 08/27/15 DD SW8270Dug/Kg120 1NDDimethylphthalate 260 08/27/15 DD SW8270Dug/Kg110 1NDDi-n-butylphthalate 260 08/27/15 DD SW8270Dug/Kg97 1NDDi-n-octylphthalate 260 08/27/15 DD SW8270Dug/Kg94 1


1600Indeno(1,2,3-cd)pyrene 260 08/27/15 DD SW8270Dug/Kg120 1NDIsophorone 260 08/27/15 DD SW8270Dug/Kg100 1230Naphthalene 260 08/27/15 DD SW8270Dug/Kg100 1JNDNitrobenzene 260 08/27/15 DD SW8270Dug/Kg130 1NDN-Nitrosodimethylamine 260 08/27/15 DD SW8270Dug/Kg100 1NDN-Nitrosodi-n-propylamine 260 08/27/15 DD SW8270Dug/Kg120 1NDN-Nitrosodiphenylamine 260 08/27/15 DD SW8270Dug/Kg140 1NDPentachloronitrobenzene 260 08/27/15 DD SW8270Dug/Kg140 1NDPentachlorophenol 260 08/27/15 DD SW8270Dug/Kg140 1





14B5 (10-15)Phoenix I.D.: BJ81801



LOD/MDL Dilution

Comments:













SOLIDEBC72 Hour


RB

Laboratory Data

14B5 (15-19.5)

Phoenix ID: BJ81802

08/26/1514:4517:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution







14B5 (15-19.5)Phoenix I.D.: BJ81802



LOD/MDL Dilution








14B5 (15-19.5)Phoenix I.D.: BJ81802



LOD/MDL Dilution

ND1,1-Dichloropropene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND1,2,3-Trichlorobenzene 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1ND1,2,3-Trichloropropane 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND1,2,4-Trichlorobenzene 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1ND1,2,4-Trimethylbenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND1,2-Dibromo-3-chloropropane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1ND1,2-Dibromoethane 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND1,2-Dichlorobenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND1,2-Dichloroethane 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND1,2-Dichloropropane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1ND1,3,5-Trimethylbenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND1,3-Dichlorobenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND1,3-Dichloropropane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1ND1,4-Dichlorobenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND2,2-Dichloropropane 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND2-Chlorotoluene 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1ND2-Hexanone 25 08/31/15 JLI SW8260Cug/Kg5.0 1ND2-Isopropyltoluene 5.0 08/31/15 JLI SW8260Cug/Kg 10.50 1ND4-Chlorotoluene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND4-Methyl-2-pentanone 25 08/31/15 JLI SW8260Cug/Kg5.0 18.7Acetone 50 08/31/15 JLI SW8260Cug/Kg5.0 1JSNDAcrylonitrile 10 08/31/15 JLI SW8260Cug/Kg1.0 1160Benzene 60 08/30/15 JLI SW8260Cug/Kg35 50NDBromobenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDBromochloromethane 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDBromodichloromethane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDBromoform 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDBromomethane 5.0 08/31/15 JLI SW8260Cug/Kg2.0 13.4Carbon Disulfide 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1JNDCarbon tetrachloride 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDChlorobenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDChloroethane 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDChloroform 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDChloromethane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 150cis-1,2-Dichloroethene 250 08/30/15 JLI SW8260Cug/Kg35 50JNDcis-1,3-Dichloropropene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDDibromochloromethane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDDibromomethane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDDichlorodifluoromethane 5.0 08/31/15 JLI SW8260Cug/Kg0.50 10.96Ethylbenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1JNDHexachlorobutadiene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDIsopropylbenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 177m&p-Xylene 350 08/30/15 JLI SW8260Cug/Kg70 50JNDMethyl Ethyl Ketone 30 08/31/15 JLI SW8260Cug/Kg5.0 1NDMethyl t-butyl ether (MTBE) 10 08/31/15 JLI SW8260Cug/Kg1.0 1NDMethylene chloride 5.0 08/31/15 JLI SW8260Cug/Kg5.0 1

1100Naphthalene 350 08/30/15 JLI SW8260Cug/Kg70 50NDn-Butylbenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDn-Propylbenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.90 1


14B5 (15-19.5)Phoenix I.D.: BJ81802



LOD/MDL Dilution

NDo-Xylene 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDp-Isopropyltoluene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDsec-Butylbenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDStyrene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDtert-Butylbenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDTetrachloroethene 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDTetrahydrofuran (THF) 10 08/31/15 JLI SW8260Cug/Kg 12.5 10.51Toluene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1JNDtrans-1,2-Dichloroethene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDtrans-1,3-Dichloropropene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDtrans-1,4-dichloro-2-butene 10 08/31/15 JLI SW8260Cug/Kg2.5 12.4Trichloroethene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1JNDTrichlorofluoromethane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDTrichlorotrifluoroethane 5.0 08/31/15 JLI SW8260Cug/Kg0.50 12.2Vinyl chloride 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1J







14B5 (15-19.5)Phoenix I.D.: BJ81802



LOD/MDL Dilution

4702-Methylnaphthalene 290 08/27/15 DD SW8270Dug/Kg130 1ND2-Methylphenol (o-cresol) 290 08/27/15 DD SW8270Dug/Kg200 1ND2-Nitroaniline 840 08/27/15 DD SW8270Dug/Kg430 1ND2-Nitrophenol 290 08/27/15 DD SW8270Dug/Kg270 1ND3&4-Methylphenol (m&p-cresol) 290 08/27/15 DD SW8270Dug/Kg 1170 1ND3,3'-Dichlorobenzidine 840 08/27/15 DD SW8270Dug/Kg200 1ND3-Nitroaniline 840 08/27/15 DD SW8270Dug/Kg840 1ND4,6-Dinitro-2-methylphenol 2100 08/27/15 DD SW8270Dug/Kg450 1ND4-Bromophenyl phenyl ether 290 08/27/15 DD SW8270Dug/Kg120 1ND4-Chloro-3-methylphenol 290 08/27/15 DD SW8270Dug/Kg150 1ND4-Chloroaniline 340 08/27/15 DD SW8270Dug/Kg200 1ND4-Chlorophenyl phenyl ether 290 08/27/15 DD SW8270Dug/Kg140 1ND4-Nitroaniline 840 08/27/15 DD SW8270Dug/Kg140 1ND4-Nitrophenol 420 08/27/15 DD SW8270Dug/Kg190 1NDAcenaphthene 290 08/27/15 DD SW8270Dug/Kg130 1330Acenaphthylene 290 08/27/15 DD SW8270Dug/Kg120 1NDAcetophenone 290 08/27/15 DD SW8270Dug/Kg130 1NDAniline 340 08/27/15 DD SW8270Dug/Kg340 1

2700Anthracene 290 08/27/15 DD SW8270Dug/Kg140 18000Benz(a)anthracene 1500 08/27/15 DD SW8270Dug/Kg710 5DNDBenzidine 840 08/27/15 DD SW8270Dug/Kg250 1

14000Benzo(a)pyrene 1500 08/27/15 DD SW8270Dug/Kg690 5D9700Benzo(b)fluoranthene 1500 08/27/15 DD SW8270Dug/Kg720 5D6200Benzo(ghi)perylene 1500 08/27/15 DD SW8270Dug/Kg680 5D6500Benzo(k)fluoranthene 290 08/27/15 DD SW8270Dug/Kg140 1NDBenzoic acid 2100 08/27/15 DD SW8270Dug/Kg 1840 1NDBenzyl butyl phthalate 290 08/27/15 DD SW8270Dug/Kg110 1NDBis(2-chloroethoxy)methane 290 08/27/15 DD SW8270Dug/Kg120 1NDBis(2-chloroethyl)ether 290 08/27/15 DD SW8270Dug/Kg110 1NDBis(2-chloroisopropyl)ether 290 08/27/15 DD SW8270Dug/Kg 1120 1NDBis(2-ethylhexyl)phthalate 290 08/27/15 DD SW8270Dug/Kg120 1

2500Carbazole 2100 08/27/15 DD SW8270Dug/Kg320 18200Chrysene 1500 08/27/15 DD SW8270Dug/Kg710 5D4200Dibenz(a,h)anthracene 290 08/27/15 DD SW8270Dug/Kg140 11300Dibenzofuran 290 08/27/15 DD SW8270Dug/Kg120 1NDDiethyl phthalate 290 08/27/15 DD SW8270Dug/Kg130 1NDDimethylphthalate 290 08/27/15 DD SW8270Dug/Kg130 1NDDi-n-butylphthalate 290 08/27/15 DD SW8270Dug/Kg110 1NDDi-n-octylphthalate 290 08/27/15 DD SW8270Dug/Kg110 1

8500Fluoranthene 1500 08/27/15 DD SW8270Dug/Kg680 5D2300Fluorene 290 08/27/15 DD SW8270Dug/Kg140 1NDHexachlorobenzene 290 08/27/15 DD SW8270Dug/Kg120 1NDHexachlorobutadiene 290 08/27/15 DD SW8270Dug/Kg150 1NDHexachlorocyclopentadiene 290 08/27/15 DD SW8270Dug/Kg130 1NDHexachloroethane 290 08/27/15 DD SW8270Dug/Kg130 1

7400Indeno(1,2,3-cd)pyrene 1500 08/27/15 DD SW8270Dug/Kg700 5DNDIsophorone 290 08/27/15 DD SW8270Dug/Kg120 1



14B5 (15-19.5)Phoenix I.D.: BJ81802



LOD/MDL Dilution



8100Pyrene 1500 08/27/15 DD SW8270Dug/Kg720 5DNDPyridine 290 08/27/15 DD SW8270Dug/Kg100 1


Comments:














SOILEBC72 Hour

08/25/15LPBsee "By" below

RB

Laboratory Data

TRIP BLANK LL

Phoenix ID: BJ81976

08/26/15 17:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution

VolatilesND1,1,1,2-Tetrachloroethane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1ND1,1,1-Trichloroethane 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND1,1,2,2-Tetrachloroethane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1ND1,1,2-Trichloroethane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1ND1,1-Dichloroethane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1ND1,1-Dichloroethene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND1,1-Dichloropropene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND1,2,3-Trichlorobenzene 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1ND1,2,3-Trichloropropane 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND1,2,4-Trichlorobenzene 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1ND1,2,4-Trimethylbenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND1,2-Dibromo-3-chloropropane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1ND1,2-Dibromoethane 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND1,2-Dichlorobenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND1,2-Dichloroethane 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND1,2-Dichloropropane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1ND1,3,5-Trimethylbenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND1,3-Dichlorobenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND1,3-Dichloropropane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1ND1,4-Dichlorobenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND2,2-Dichloropropane 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND2-Chlorotoluene 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1ND2-Hexanone 25 08/31/15 JLI SW8260Cug/Kg5.0 1ND2-Isopropyltoluene 5.0 08/31/15 JLI SW8260Cug/Kg 10.50 1ND4-Chlorotoluene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1ND4-Methyl-2-pentanone 25 08/31/15 JLI SW8260Cug/Kg5.0 1


TRIP BLANK LLPhoenix I.D.: BJ81976



LOD/MDL Dilution

NDAcetone 50 08/31/15 JLI SW8260Cug/Kg5.0 1NDAcrylonitrile 10 08/31/15 JLI SW8260Cug/Kg1.0 1NDBenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDBromobenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDBromochloromethane 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDBromodichloromethane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDBromoform 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDBromomethane 5.0 08/31/15 JLI SW8260Cug/Kg2.0 1NDCarbon Disulfide 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDCarbon tetrachloride 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDChlorobenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDChloroethane 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDChloroform 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDChloromethane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDcis-1,2-Dichloroethene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDcis-1,3-Dichloropropene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDDibromochloromethane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDDibromomethane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDDichlorodifluoromethane 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDEthylbenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDHexachlorobutadiene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDIsopropylbenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDm&p-Xylene 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDMethyl Ethyl Ketone 30 08/31/15 JLI SW8260Cug/Kg5.0 1NDMethyl t-butyl ether (MTBE) 10 08/31/15 JLI SW8260Cug/Kg1.0 1NDMethylene chloride 5.0 08/31/15 JLI SW8260Cug/Kg5.0 1NDNaphthalene 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDn-Butylbenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDn-Propylbenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.90 1NDo-Xylene 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDp-Isopropyltoluene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDsec-Butylbenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDStyrene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDtert-Butylbenzene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDTetrachloroethene 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDTetrahydrofuran (THF) 10 08/31/15 JLI SW8260Cug/Kg 12.5 1NDToluene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDtrans-1,2-Dichloroethene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDtrans-1,3-Dichloropropene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDtrans-1,4-dichloro-2-butene 10 08/31/15 JLI SW8260Cug/Kg2.5 1NDTrichloroethene 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDTrichlorofluoromethane 5.0 08/31/15 JLI SW8260Cug/Kg1.0 1NDTrichlorotrifluoroethane 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1NDVinyl chloride 5.0 08/31/15 JLI SW8260Cug/Kg0.50 1



TRIP BLANK LLPhoenix I.D.: BJ81976



LOD/MDL Dilution




Comments:

Results are reported on an ``as received`` basis, and are not corrected for dry weight.






RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit




SOILEBC72 Hour

08/25/15LPBsee "By" below

RB

Laboratory Data

TRIP BLANK HL

Phoenix ID: BJ81977

08/26/15 17:00




Date Time



SDG ID: GBJ81780


LOD/MDL Dilution

CompletedField Extraction 08/25/15 SW5035A

VolatilesND1,1,1,2-Tetrachloroethane 250 08/31/15 JLI SW8260Cug/Kg50 50ND1,1,1-Trichloroethane 250 08/31/15 JLI SW8260Cug/Kg25 50ND1,1,2,2-Tetrachloroethane 250 08/31/15 JLI SW8260Cug/Kg50 50ND1,1,2-Trichloroethane 250 08/31/15 JLI SW8260Cug/Kg50 50ND1,1-Dichloroethane 250 08/31/15 JLI SW8260Cug/Kg50 50ND1,1-Dichloroethene 250 08/31/15 JLI SW8260Cug/Kg25 50ND1,1-Dichloropropene 250 08/31/15 JLI SW8260Cug/Kg25 50ND1,2,3-Trichlorobenzene 250 08/31/15 JLI SW8260Cug/Kg50 50ND1,2,3-Trichloropropane 250 08/31/15 JLI SW8260Cug/Kg25 50ND1,2,4-Trichlorobenzene 250 08/31/15 JLI SW8260Cug/Kg50 50ND1,2,4-Trimethylbenzene 250 08/31/15 JLI SW8260Cug/Kg25 50ND1,2-Dibromo-3-chloropropane 250 08/31/15 JLI SW8260Cug/Kg50 50ND1,2-Dibromoethane 250 08/31/15 JLI SW8260Cug/Kg25 50ND1,2-Dichlorobenzene 250 08/31/15 JLI SW8260Cug/Kg25 50ND1,2-Dichloroethane 250 08/31/15 JLI SW8260Cug/Kg25 50ND1,2-Dichloropropane 250 08/31/15 JLI SW8260Cug/Kg50 50ND1,3,5-Trimethylbenzene 250 08/31/15 JLI SW8260Cug/Kg25 50ND1,3-Dichlorobenzene 250 08/31/15 JLI SW8260Cug/Kg25 50ND1,3-Dichloropropane 250 08/31/15 JLI SW8260Cug/Kg50 50ND1,4-Dichlorobenzene 250 08/31/15 JLI SW8260Cug/Kg25 50ND2,2-Dichloropropane 250 08/31/15 JLI SW8260Cug/Kg25 50ND2-Chlorotoluene 250 08/31/15 JLI SW8260Cug/Kg50 50ND2-Hexanone 1300 08/31/15 JLI SW8260Cug/Kg250 50ND2-Isopropyltoluene 250 08/31/15 JLI SW8260Cug/Kg 125 50ND4-Chlorotoluene 250 08/31/15 JLI SW8260Cug/Kg25 50


TRIP BLANK HLPhoenix I.D.: BJ81977



LOD/MDL Dilution

ND4-Methyl-2-pentanone 1300 08/31/15 JLI SW8260Cug/Kg250 50NDAcetone 2500 08/31/15 JLI SW8260Cug/Kg250 50NDAcrylonitrile 500 08/31/15 JLI SW8260Cug/Kg25 50NDBenzene 250 08/31/15 JLI SW8260Cug/Kg25 50NDBromobenzene 250 08/31/15 JLI SW8260Cug/Kg25 50NDBromochloromethane 250 08/31/15 JLI SW8260Cug/Kg25 50NDBromodichloromethane 250 08/31/15 JLI SW8260Cug/Kg50 50NDBromoform 250 08/31/15 JLI SW8260Cug/Kg50 50NDBromomethane 250 08/31/15 JLI SW8260Cug/Kg100 50NDCarbon Disulfide 250 08/31/15 JLI SW8260Cug/Kg50 50NDCarbon tetrachloride 250 08/31/15 JLI SW8260Cug/Kg50 50NDChlorobenzene 250 08/31/15 JLI SW8260Cug/Kg25 50NDChloroethane 250 08/31/15 JLI SW8260Cug/Kg25 50NDChloroform 250 08/31/15 JLI SW8260Cug/Kg25 50NDChloromethane 250 08/31/15 JLI SW8260Cug/Kg50 50NDcis-1,2-Dichloroethene 250 08/31/15 JLI SW8260Cug/Kg25 50NDcis-1,3-Dichloropropene 250 08/31/15 JLI SW8260Cug/Kg25 50NDDibromochloromethane 250 08/31/15 JLI SW8260Cug/Kg50 50NDDibromomethane 250 08/31/15 JLI SW8260Cug/Kg50 50NDDichlorodifluoromethane 250 08/31/15 JLI SW8260Cug/Kg25 50NDEthylbenzene 250 08/31/15 JLI SW8260Cug/Kg25 50NDHexachlorobutadiene 250 08/31/15 JLI SW8260Cug/Kg25 50NDIsopropylbenzene 250 08/31/15 JLI SW8260Cug/Kg25 50NDm&p-Xylene 250 08/31/15 JLI SW8260Cug/Kg50 50NDMethyl Ethyl Ketone 1500 08/31/15 JLI SW8260Cug/Kg250 50NDMethyl t-butyl ether (MTBE) 500 08/31/15 JLI SW8260Cug/Kg50 50NDMethylene chloride 250 08/31/15 JLI SW8260Cug/Kg250 50NDNaphthalene 250 08/31/15 JLI SW8260Cug/Kg50 50NDn-Butylbenzene 250 08/31/15 JLI SW8260Cug/Kg25 50NDn-Propylbenzene 250 08/31/15 JLI SW8260Cug/Kg45 50NDo-Xylene 250 08/31/15 JLI SW8260Cug/Kg50 50NDp-Isopropyltoluene 250 08/31/15 JLI SW8260Cug/Kg25 50NDsec-Butylbenzene 250 08/31/15 JLI SW8260Cug/Kg25 50NDStyrene 250 08/31/15 JLI SW8260Cug/Kg25 50NDtert-Butylbenzene 250 08/31/15 JLI SW8260Cug/Kg25 50NDTetrachloroethene 250 08/31/15 JLI SW8260Cug/Kg50 50NDTetrahydrofuran (THF) 500 08/31/15 JLI SW8260Cug/Kg 1130 50NDToluene 250 08/31/15 JLI SW8260Cug/Kg25 50NDtrans-1,2-Dichloroethene 250 08/31/15 JLI SW8260Cug/Kg25 50NDtrans-1,3-Dichloropropene 250 08/31/15 JLI SW8260Cug/Kg25 50NDtrans-1,4-dichloro-2-butene 500 08/31/15 JLI SW8260Cug/Kg130 50NDTrichloroethene 250 08/31/15 JLI SW8260Cug/Kg25 50NDTrichlorofluoromethane 250 08/31/15 JLI SW8260Cug/Kg50 50NDTrichlorotrifluoroethane 250 08/31/15 JLI SW8260Cug/Kg25 50NDVinyl chloride 250 08/31/15 JLI SW8260Cug/Kg25 50

QA/QC Surrogates101% 1,2-dichlorobenzene-d4 08/31/15 JLI 70 - 130 %% 5092% Bromofluorobenzene 08/31/15 JLI 70 - 130 %% 5098% Dibromofluoromethane 08/31/15 JLI 70 - 130 %% 50


TRIP BLANK HLPhoenix I.D.: BJ81977



LOD/MDL Dilution

100% Toluene-d8 08/31/15 JLI 70 - 130 %% 50




Comments:

Results are reported on an ``as received`` basis, and are not corrected for dry weight.






RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit


QA/QC Data


MS%

MSD%

MSRPD




SDG I.D.: GBJ81780

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPD

LimitsSampleResult

DupResult

QA/QC Batch 318455 (mg/kg), QC Sample No: BJ81785 (BJ81780, BJ81782, BJ81783, BJ81785, BJ81786, BJ81788, BJ81789, BJ81791, BJ81793, BJ81794, BJ81796, BJ81797, BJ81799, BJ81800, BJ81802)

ICP Metals - SoilAluminum NC NCBRL NC94.80.90 97.4 2.7 80 - 120 3011000 111005.0

Antimony 67.9 66.9BRL 1.576.8NC 78.6 2.3 m70 - 130 30<1.8 <3.63.3

Arsenic 89.3 87.1BRL 2.594.1NC 96.6 2.6 80 - 120 301.5 1.450.67

Barium 104 108BRL 3.898.11.80 103 4.9 80 - 120 3055.3 56.30.33

Beryllium 95.1 93.3BRL 1.996.4NC 98.9 2.6 80 - 120 300.64 0.600.27

Cadmium 88.3 86.7BRL 1.889.4NC 92.9 3.8 80 - 120 30<0.37 <0.360.33

Calcium NC NCBRL NC94.43.90 95.9 1.6 80 - 120 301260 13105.0

Chromium 96.2 95.7BRL 0.593.24.90 95.5 2.4 80 - 120 3021.1 20.10.33

Cobalt 93.7 92.7BRL 1.194.58.50 97.4 3.0 80 - 120 3010.1 11.00.33

Copper 103 103BRL 0.096.14.20 98.1 2.1 80 - 120 3017.2 16.50.33

Iron NC NC16.3 NC93.317.3 93.6 0.3 80 - 120 3023900 201005.0

Lead 89.7 88.3BRL 1.695.44.20 98.6 3.3 80 - 120 305.9 5.660.33

Magnesium NC NCBRL NC94.91.70 95.5 0.6 80 - 120 303500 35605.0

Manganese 89.4 96.8BRL 7.995.50.90 98.6 3.2 80 - 120 30420 4240.33

Nickel 92.7 91.6BRL 1.295.62.50 97.6 2.1 80 - 120 3016.2 15.80.33

Potassium >130 >130BRL NC1062.30 106 0.0 m80 - 120 302170 22205.0

Selenium 82.0 79.6BRL 3.099.1NC 100 0.9 80 - 120 30<1.5 <1.51.3

Silver 95.3 94.2BRL 1.298.3NC 101 2.7 70 - 130 30<0.37 <0.360.33

Sodium >130 >130BRL NC1003.10 101 1.0 m80 - 120 30290 2995.0

Thallium 92.0 91.1BRL 1.092.1NC 93.9 1.9 80 - 120 30<1.5 <3.33.0

Vanadium 96.9 96.4BRL 0.591.61.00 95.4 4.1 80 - 120 3031.4 31.10.33

Zinc 95.5 94.02.26 1.697.15.50 98.7 1.6 80 - 120 3033.9 32.10.33

QA/QC Batch 318498 (mg/kg), QC Sample No: BJ81791 (BJ81780, BJ81782, BJ81783, BJ81785, BJ81786, BJ81788, BJ81789, BJ81791, BJ81793, BJ81794, BJ81796, BJ81797, BJ81799, BJ81800, BJ81802)Mercury - Soil 110 110BRL 0.0104NC 95.4 8.6 75 - 125 300.09 0.080.06

m = This parameter is outside laboratory ms/msd specified recovery limits.

Page 1 of 14

QA/QC Data


MS%

MSD%

MSRPD




SDG I.D.: GBJ81780

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

QA/QC Batch 318459 (ug/Kg), QC Sample No: BJ81785 2X (BJ81780, BJ81782, BJ81783, BJ81785, BJ81786, BJ81788, BJ81789, BJ81791, BJ81793, BJ81794, BJ81796, BJ81797, BJ81799, BJ81800, BJ81802)

Pesticides - Solid4,4' -DDD 82 79ND 3.777 85 9.9 30 - 150 301.7

4,4' -DDE 82 84ND 2.479 82 3.7 50 - 150 301.7

4,4' -DDT 84 79ND 6.176 84 10.0 30 - 150 501.7

a-BHC 84 79ND 6.175 82 8.9 30 - 150 303.3

a-Chlordane 100 89ND 11.687 108 21.5 30 - 150 303.3

Aldrin 70 62ND 12.162 71 13.5 30 - 150 431.0

b-BHC 78 77ND 1.371 78 9.4 30 - 150 303.3

Chlordane 60 57ND 5.152 59 12.6 30 - 150 3033

d-BHC 95 88ND 7.785 97 13.2 30 - 150 303.3

Dieldrin 87 81ND 7.179 89 11.9 30 - 130 381.0

Endosulfan I 92 90ND 2.284 91 8.0 30 - 150 303.3

Endosulfan II 84 82ND 2.479 86 8.5 30 - 150 303.3

Endosulfan sulfate 72 72ND 0.070 75 6.9 50 - 120 303.3

Endrin 92 86ND 6.783 91 9.2 50 - 120 453.3

Endrin aldehyde 62 76ND 20.375 80 6.5 30 - 150 303.3

Endrin ketone 78 77ND 1.375 81 7.7 30 - 150 303.3

g-BHC 86 86ND 0.080 87 8.4 50 - 120 501.0

g-Chlordane 60 57ND 5.152 59 12.6 30 - 130 303.3

Heptachlor 89 81ND 9.479 92 15.2 30 - 150 313.3

Heptachlor epoxide 83 82ND 1.276 80 5.1 50 - 150 303.3

Methoxychlor 82 88ND 7.181 84 3.6 30 - 150 303.3

Toxaphene NA NAND NCNA NA NC 30 - 150 30130

% DCBP 84 8479 0.084 93 10.2 30 - 150 30%

% TCMX 92 9687 4.389 94 5.5 30 - 150 30%

QA/QC Batch 318456 (ug/Kg), QC Sample No: BJ81785 2X (BJ81780, BJ81782, BJ81783, BJ81785, BJ81786, BJ81788, BJ81789, BJ81791, BJ81793, BJ81794, BJ81796, BJ81797, BJ81799, BJ81800, BJ81802)

Polychlorinated Biphenyls - SolidPCB-1016 84 91ND 8.085 88 3.5 30 - 120 1533

PCB-1221 ND 30 - 150 3033

PCB-1232 ND 30 - 150 3033

PCB-1242 ND 30 - 150 3033

PCB-1248 ND 30 - 150 3033

PCB-1254 ND 30 - 150 3033

PCB-1260 87 97ND 10.986 93 7.8 30 - 150 2033

PCB-1262 ND 30 - 150 3033

PCB-1268 ND 30 - 150 3033

% DCBP (Surrogate Rec) 101 11296 10.3100 107 6.8 30 - 150 20%

% TCMX (Surrogate Rec) 94 10390 9.195 97 2.1 30 - 150 20%

Page 2 of 14

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ81780

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

QA/QC Batch 318452 (ug/kg), QC Sample No: BJ81785 (BJ81780, BJ81781, BJ81782, BJ81783, BJ81784, BJ81785, BJ81786, BJ81787, BJ81788, BJ81789, BJ81790, BJ81791, BJ81792, BJ81793, BJ81794, BJ81795, BJ81796, BJ81797, BJ81798)

Semivolatiles - Solid1,2,4,5-Tetrachlorobenzene 56ND 65 66 1.5 30 - 130 30230

1,2,4-Trichlorobenzene 54ND 64 67 4.6 30 - 130 30230

1,2-Dichlorobenzene 45ND 55 60 8.7 30 - 130 30180

1,2-Diphenylhydrazine 64ND 69 73 5.6 30 - 130 30230



2,4,5-Trichlorophenol 62ND 73 70 4.2 30 - 130 30230

2,4,6-Trichlorophenol 60ND 70 68 2.9 30 - 130 30130

2,4-Dichlorophenol 64ND 73 75 2.7 30 - 130 30130

2,4-Dimethylphenol 63ND 73 75 2.7 30 - 130 30230

2,4-Dinitrophenol 53ND 36 12 100.0 l,r30 - 130 30230

2,4-Dinitrotoluene 65ND 75 73 2.7 30 - 130 30130

2,6-Dinitrotoluene 64ND 71 72 1.4 30 - 130 30130

2-Chloronaphthalene 59ND 67 67 0.0 30 - 130 30230

2-Chlorophenol 59ND 66 68 3.0 30 - 130 30230

2-Methylnaphthalene 64ND 72 75 4.1 30 - 130 30230

2-Methylphenol (o-cresol) 60ND 67 70 4.4 30 - 130 30230

2-Nitroaniline 72ND 83 79 4.9 30 - 130 30330

2-Nitrophenol 68ND 74 78 5.3 30 - 130 30230

3&4-Methylphenol (m&p-cresol) 64ND 73 74 1.4 30 - 130 30230

3,3'-Dichlorobenzidine 56ND 67 61 9.4 30 - 130 30130

3-Nitroaniline 58ND 68 67 1.5 30 - 130 30330

4,6-Dinitro-2-methylphenol 68ND 66 30 75.0 r30 - 130 30230

4-Bromophenyl phenyl ether 61ND 71 68 4.3 30 - 130 30230

4-Chloro-3-methylphenol 70ND 81 82 1.2 30 - 130 30230

4-Chloroaniline 64ND 70 74 5.6 30 - 130 30230

4-Chlorophenyl phenyl ether 59ND 69 67 2.9 30 - 130 30230

4-Nitroaniline 71ND 83 80 3.7 30 - 130 30230

4-Nitrophenol 63ND 74 66 11.4 30 - 130 30230

Acenaphthene 59ND 68 67 1.5 30 - 130 30230

Acenaphthylene 57ND 65 64 1.6 30 - 130 30130

Acetophenone 59ND 65 69 6.0 30 - 130 30230

Aniline 54ND 58 59 1.7 30 - 130 30330

Anthracene 63ND 74 71 4.1 30 - 130 30230

Benz(a)anthracene 65ND 76 70 8.2 30 - 130 30230

Benzidine 56ND 67 50 29.1 30 - 130 30330

Benzo(a)pyrene 39ND 77 70 9.5 30 - 130 30130

Benzo(b)fluoranthene 50ND 76 72 5.4 30 - 130 30160

Benzo(ghi)perylene 54ND 77 69 11.0 30 - 130 30230

Benzo(k)fluoranthene 47ND 76 71 6.8 30 - 130 30230

Benzoic Acid 13ND <10 <10 NC l,m30 - 130 30330

Benzyl butyl phthalate 67ND 79 76 3.9 30 - 130 30230

Bis(2-chloroethoxy)methane 67ND 74 77 4.0 30 - 130 30230

Bis(2-chloroethyl)ether 52ND 58 64 9.8 30 - 130 30130

Bis(2-chloroisopropyl)ether 57ND 66 68 3.0 30 - 130 30230

Bis(2-ethylhexyl)phthalate 68ND 81 75 7.7 30 - 130 30230

Carbazole 65ND 76 72 5.4 30 - 130 30330

Chrysene 62ND 77 71 8.1 30 - 130 30230

Dibenz(a,h)anthracene 62ND 75 67 11.3 30 - 130 30130

Page 3 of 14

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ81780

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

Dibenzofuran 61ND 71 70 1.4 30 - 130 30230

Diethyl phthalate 61ND 72 69 4.3 30 - 130 30230

Dimethylphthalate 61ND 70 69 1.4 30 - 130 30230

Di-n-butylphthalate 66ND 77 74 4.0 30 - 130 30230

Di-n-octylphthalate 68ND 79 74 6.5 30 - 130 30230

Fluoranthene 63ND 72 69 4.3 30 - 130 30230

Fluorene 60ND 69 68 1.5 30 - 130 30230

Hexachlorobenzene 64ND 74 72 2.7 30 - 130 30130

Hexachlorobutadiene 48ND 61 64 4.8 30 - 130 30230

Hexachlorocyclopentadiene 56ND 64 67 4.6 30 - 130 30230

Hexachloroethane 40ND 54 59 8.8 30 - 130 30130

Indeno(1,2,3-cd)pyrene 54ND 78 71 9.4 30 - 130 30230

Isophorone 63ND 69 72 4.3 30 - 130 30130

Naphthalene 60ND 68 71 4.3 30 - 130 30230

Nitrobenzene 63ND 69 72 4.3 30 - 130 30130

N-Nitrosodimethylamine 52ND 51 61 17.9 30 - 130 30230

N-Nitrosodi-n-propylamine 66ND 72 75 4.1 30 - 130 30130

N-Nitrosodiphenylamine 61ND 72 69 4.3 30 - 130 30130

Pentachloronitrobenzene 63ND 73 69 5.6 30 - 130 30230

Pentachlorophenol 63ND 74 51 36.8 r30 - 130 30230

Phenanthrene 63ND 72 69 4.3 30 - 130 30130

Phenol 63ND 69 71 2.9 30 - 130 30230

Pyrene 62ND 72 69 4.3 30 - 130 30230

Pyridine 31ND 33 41 21.6 30 - 130 30230

% 2,4,6-Tribromophenol 6765 77 75 2.6 30 - 130 30%

% 2-Fluorobiphenyl 5558 64 63 1.6 30 - 130 30%

% 2-Fluorophenol 5148 57 60 5.1 30 - 130 30%

% Nitrobenzene-d5 6157 67 70 4.4 30 - 130 30%

% Phenol-d5 5854 66 67 1.5 30 - 130 30%

% Terphenyl-d14 5964 69 65 6.0 30 - 130 30%

QA/QC Batch 318847 (ug/kg), QC Sample No: BJ81787 (BJ81780 (50X) , BJ81783 (50X) , BJ81786 (50X) , BJ81787, BJ81788 (50X) , BJ81790 (50X) )

Volatiles - Solid1,1,1,2-Tetrachloroethane 118 115ND 2.6102 103 1.0 70 - 130 305.0



















Page 4 of 14

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ81780

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits


1,4-dioxane 108 102ND 5.7100 92 8.3 70 - 130 30100



2-Hexanone 93 91ND 2.275 77 2.6 70 - 130 3025



4-Methyl-2-pentanone 102 104ND 1.987 91 4.5 70 - 130 3025

Acetone 124 122ND 1.660 63 4.9 l70 - 130 3010

Acrolein 106 110ND 3.793 99 6.3 70 - 130 3025


Benzene 107 106ND 0.991 92 1.1 70 - 130 301.0

Bromobenzene 103 102ND 1.089 88 1.1 70 - 130 305.0



Bromoform 121 117ND 3.4111 111 0.0 70 - 130 305.0

Bromomethane 154 157ND 1.9124 122 1.6 m70 - 130 305.0


Carbon tetrachloride 129 135ND 4.5111 117 5.3 m70 - 130 305.0


Chloroethane 145 150ND 3.4118 121 2.5 m70 - 130 305.0

Chloroform 111 115ND 3.596 100 4.1 70 - 130 305.0


cis-1,2-Dichloroethene 102 106ND 3.889 86 3.4 70 - 130 305.0




Dichlorodifluoromethane 142 147ND 3.5127 132 3.9 l,m70 - 130 305.0

Ethylbenzene 109 107ND 1.992 93 1.1 70 - 130 301.0



m&p-Xylene 110 108ND 1.892 93 1.1 70 - 130 302.0

Methyl ethyl ketone 78 79ND 1.366 69 4.4 l70 - 130 305.0



Naphthalene 130 123ND 5.596 98 2.1 70 - 130 305.0



o-Xylene 112 108ND 3.695 94 1.1 70 - 130 302.0



Styrene 111 108ND 2.792 95 3.2 70 - 130 305.0

tert-butyl alcohol 120 112ND 6.991 80 12.9 70 - 130 30100




Toluene 109 108ND 0.992 93 1.1 70 - 130 301.0





Trichlorofluoromethane 153 157ND 2.6125 128 2.4 m70 - 130 305.0

Trichlorotrifluoroethane 135 138ND 2.2118 119 0.8 m70 - 130 305.0

Page 5 of 14

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ81780

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits





% Toluene-d8 100 10097 0.099 100 1.0 70 - 130 30%

QA/QC Batch 318971 (ug/kg), QC Sample No: BJ81794 (BJ81791, BJ81792 (500X, 5000X) , BJ81793 (50X) , BJ81794 (1X, 50X) , BJ81795 (50X) , BJ81797, BJ81798 (50X) , BJ81799 (10000X) , BJ81800 (50X) , BJ81801, BJ81802, BJ81976, BJ81977 (50X) )

Volatiles - Solid, Soil1,1,1,2-Tetrachloroethane 81 89ND 9.494 81 14.9 70 - 130 305.0







1,2,3-Trichlorobenzene 69 78ND 12.299 83 17.6 m70 - 130 305.0













1,4-dioxane 87 90ND 3.496 92 4.3 70 - 130 30100



2-Hexanone 73 80ND 9.289 78 13.2 70 - 130 3025




Acetone 50 51ND 2.068 59 14.2 l,m70 - 130 3010

Acrolein 45 42ND 6.987 80 8.4 m70 - 130 3025


Benzene 80 86ND 7.293 83 11.4 70 - 130 301.0

Bromobenzene 78 85ND 8.694 85 10.1 70 - 130 305.0



Bromoform 81 89ND 9.498 86 13.0 70 - 130 305.0

Bromomethane 42 54ND 25.082 69 17.2 l,m70 - 130 305.0





Chloroform 75 79ND 5.291 82 10.4 70 - 130 305.0




Page 6 of 14

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ81780

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits




Ethylbenzene 82 89ND 8.295 82 14.7 70 - 130 301.0



m&p-Xylene 81 89ND 9.494 81 14.9 70 - 130 302.0

Methyl ethyl ketone 62 66ND 6.376 66 14.1 l,m70 - 130 305.0



Naphthalene 81 86ND 6.0112 90 21.8 70 - 130 305.0



o-Xylene 85 92ND 7.999 86 14.1 70 - 130 302.0



Styrene 83 90ND 8.198 86 13.0 70 - 130 305.0





Toluene 81 86ND 6.092 82 11.5 70 - 130 301.0











% Toluene-d8 100 98101 2.0101 99 2.0 70 - 130 30%

QA/QC Batch 318457 (ug/Kg), QC Sample No: BJ81800 (BJ81799, BJ81800, BJ81801, BJ81802)

Semivolatiles - Solid1,2,4,5-Tetrachlorobenzene 66 62ND 6.363 72 13.3 30 - 130 30230

1,2,4-Trichlorobenzene 67 61ND 9.460 69 14.0 30 - 130 30230

1,2-Dichlorobenzene 61 57ND 6.850 61 19.8 30 - 130 30180

1,2-Diphenylhydrazine 76 63ND 18.769 71 2.9 30 - 130 30230



2,4,5-Trichlorophenol 70 63ND 10.570 78 10.8 30 - 130 30230

2,4,6-Trichlorophenol 65 58ND 11.470 79 12.1 30 - 130 30130

2,4-Dichlorophenol 75 70ND 6.970 78 10.8 30 - 130 30130

2,4-Dimethylphenol 80 71ND 11.966 71 7.3 30 - 130 30230

2,4-Dinitrophenol 45 44ND 2.214 22 44.4 l,r30 - 130 30230

2,4-Dinitrotoluene 81 70ND 14.673 79 7.9 30 - 130 30130

2,6-Dinitrotoluene 79 69ND 13.571 76 6.8 30 - 130 30130

2-Chloronaphthalene 71 61ND 15.267 74 9.9 30 - 130 30230

2-Chlorophenol 75 65ND 14.362 71 13.5 30 - 130 30230

2-Methylnaphthalene 78 78ND 0.069 79 13.5 30 - 130 30230

2-Methylphenol (o-cresol) 77 66ND 15.461 71 15.2 30 - 130 30230

Page 7 of 14

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ81780

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

2-Nitroaniline 91 80ND 12.986 88 2.3 30 - 130 30330

2-Nitrophenol 67 57ND 16.172 77 6.7 30 - 130 30230

3&4-Methylphenol (m&p-cresol) 79 72ND 9.364 76 17.1 30 - 130 30230

3,3'-Dichlorobenzidine 60 50ND 18.258 66 12.9 30 - 130 30130

3-Nitroaniline 77 64ND 18.468 72 5.7 30 - 130 30330

4,6-Dinitro-2-methylphenol 51 48ND 6.132 42 27.0 30 - 130 30230

4-Bromophenyl phenyl ether 70 62ND 12.169 78 12.2 30 - 130 30230

4-Chloro-3-methylphenol 89 83ND 7.076 84 10.0 30 - 130 30230

4-Chloroaniline 73 61ND 17.971 74 4.1 30 - 130 30230

4-Chlorophenyl phenyl ether 73 65ND 11.666 75 12.8 30 - 130 30230

4-Nitroaniline 87 72ND 18.975 77 2.6 30 - 130 30230

4-Nitrophenol 81 66ND 20.480 82 2.5 30 - 130 30230

Acenaphthene 68 61ND 10.965 71 8.8 30 - 130 30230

Acenaphthylene 68 63ND 7.664 68 6.1 30 - 130 30130

Acetophenone 71 62ND 13.558 66 12.9 30 - 130 30230

Aniline 51 46ND 10.353 63 17.2 30 - 130 30330

Anthracene 69 75ND 8.371 76 6.8 30 - 130 30230

Benz(a)anthracene 69 105ND 41.472 75 4.1 r30 - 130 30230

Benzidine 17 11ND 42.947 53 12.0 m,r30 - 130 30330

Benzo(a)pyrene 60 88ND 37.871 76 6.8 r30 - 130 30130

Benzo(b)fluoranthene 67 110ND 48.674 74 0.0 r30 - 130 30160

Benzo(ghi)perylene 44 55ND 22.272 78 8.0 30 - 130 30230

Benzo(k)fluoranthene 78 92ND 16.570 80 13.3 30 - 130 30230

Benzoic Acid 21 <10ND NC<10 <10 NC l,m30 - 130 30330

Benzyl butyl phthalate 86 65ND 27.874 73 1.4 30 - 130 30230

Bis(2-chloroethoxy)methane 75 66ND 12.867 70 4.4 30 - 130 30230

Bis(2-chloroethyl)ether 57 52ND 9.249 55 11.5 30 - 130 30130

Bis(2-chloroisopropyl)ether 67 54ND 21.555 61 10.3 30 - 130 30230

Bis(2-ethylhexyl)phthalate 66 56ND 16.473 72 1.4 30 - 130 30230

Carbazole 76 82ND 7.670 76 8.2 30 - 130 30330

Chrysene 76 124ND 48.076 78 2.6 r30 - 130 30230

Dibenz(a,h)anthracene 57 61ND 6.872 80 10.5 30 - 130 30130

Dibenzofuran 75 81ND 7.768 75 9.8 30 - 130 30230

Diethyl phthalate 85 73ND 15.276 83 8.8 30 - 130 30230

Dimethylphthalate 77 69ND 11.069 77 11.0 30 - 130 30230

Di-n-butylphthalate 75 63ND 17.476 79 3.9 30 - 130 30230

Di-n-octylphthalate 53 49ND 7.875 75 0.0 30 - 130 30230

Fluoranthene 79 >200ND NC74 79 6.5 m30 - 130 30230

Fluorene 77 73ND 5.369 77 11.0 30 - 130 30230

Hexachlorobenzene 63 51ND 21.176 77 1.3 30 - 130 30130

Hexachlorobutadiene 63 60ND 4.959 70 17.1 30 - 130 30230

Hexachlorocyclopentadiene <10 <10ND NC59 71 18.5 m30 - 130 30230

Hexachloroethane 56 53ND 5.550 57 13.1 30 - 130 30130

Indeno(1,2,3-cd)pyrene 47 60ND 24.372 79 9.3 30 - 130 30230

Isophorone 71 62ND 13.563 67 6.2 30 - 130 30130

Naphthalene 72 78ND 8.061 70 13.7 30 - 130 30230

Nitrobenzene 76 66ND 14.161 69 12.3 30 - 130 30130

N-Nitrosodimethylamine 50 31ND 46.936 44 20.0 r30 - 130 30230

N-Nitrosodi-n-propylamine 72 64ND 11.864 72 11.8 30 - 130 30130

N-Nitrosodiphenylamine 81 72ND 11.870 79 12.1 30 - 130 30130

Pentachloronitrobenzene 72 61ND 16.575 81 7.7 30 - 130 30230

Pentachlorophenol 74 69ND 7.077 89 14.5 30 - 130 30230

Phenanthrene 78 >200ND NC71 76 6.8 m30 - 130 30130

Page 8 of 14

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ81780

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

Phenol 76 67ND 12.664 74 14.5 30 - 130 30230

Pyrene 76 195ND 87.872 78 8.0 m,r30 - 130 30230

Pyridine 37 24ND 42.626 26 0.0 l,m,r30 - 130 30230

% 2,4,6-Tribromophenol 65 5366 20.380 79 1.3 30 - 130 30%

% 2-Fluorobiphenyl 68 5961 14.263 69 9.1 30 - 130 30%

% 2-Fluorophenol 61 4755 25.955 64 15.1 30 - 130 30%

% Nitrobenzene-d5 72 6558 10.260 67 11.0 30 - 130 30%

% Phenol-d5 73 6558 11.663 72 13.3 30 - 130 30%

% Terphenyl-d14 62 5373 15.769 78 12.2 30 - 130 30%

QA/QC Batch 318851 (ug/kg), QC Sample No: BJ82933 (BJ81792 (50X) , BJ81795, BJ81798, BJ81799 (714X) , BJ81800, BJ81802 (50X) )





















1,4-dioxane 104 103ND 1.095 95 0.0 70 - 130 30100



2-Hexanone 96 104ND 8.072 69 4.3 l70 - 130 3025




Acetone 61 68ND 10.956 58 3.5 l,m70 - 130 3010

Acrolein 50 53ND 5.885 93 9.0 m70 - 130 3025


Benzene 101 98ND 3.082 83 1.2 70 - 130 301.0

Bromobenzene 108 115ND 6.393 93 0.0 70 - 130 305.0



Bromoform 124 128ND 3.2101 102 1.0 70 - 130 305.0

Bromomethane 78 92ND 16.5107 106 0.9 70 - 130 305.0





Page 9 of 14

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ81780

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

Chloroform 102 109ND 6.687 90 3.4 70 - 130 305.0






Dichlorodifluoromethane 130 143ND 9.5113 111 1.8 m70 - 130 305.0

Ethylbenzene 111 111ND 0.088 83 5.8 70 - 130 301.0

Hexachlorobutadiene 133 152ND 13.3113 115 1.8 m70 - 130 305.0


m&p-Xylene 113 113ND 0.088 86 2.3 70 - 130 302.0

Methyl ethyl ketone 78 87ND 10.959 60 1.7 l70 - 130 305.0



Naphthalene 110 122ND 10.3100 100 0.0 70 - 130 305.0



o-Xylene 115 116ND 0.990 87 3.4 70 - 130 302.0



Styrene 113 115ND 1.890 87 3.4 70 - 130 305.0





Toluene 95 97ND 2.184 84 0.0 70 - 130 301.0











% Toluene-d8 102 9698 6.198 100 2.0 70 - 130 30%

QA/QC Batch 318835 (ug/kg), QC Sample No: BJ83283 (BJ81780, BJ81781, BJ81782, BJ81783, BJ81784, BJ81785, BJ81786, BJ81788, BJ81789, BJ81790)













Page 10 of 14

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ81780

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits









1,4-dioxane 107 101ND 5.8106 111 4.6 70 - 130 30100



2-Hexanone 83 78ND 6.281 85 4.8 70 - 130 3025




Acetone 68 67ND 1.565 67 3.0 l,m70 - 130 3010

Acrolein 116 93ND 22.0104 97 7.0 70 - 130 3025


Benzene 103 99ND 4.0104 108 3.8 70 - 130 301.0

Bromobenzene 99 95ND 4.1104 105 1.0 70 - 130 305.0


Bromodichloromethane 128 122ND 4.8126 131 3.9 l70 - 130 305.0

Bromoform 127 118ND 7.3122 121 0.8 70 - 130 305.0

Bromomethane 141 137ND 2.9129 134 3.8 l,m70 - 130 305.0




Chloroethane 135 134ND 0.7134 135 0.7 l,m70 - 130 305.0

Chloroform 117 110ND 6.2112 110 1.8 70 - 130 305.0






Dichlorodifluoromethane 115 112ND 2.6130 133 2.3 l70 - 130 305.0

Ethylbenzene 104 96ND 8.0107 105 1.9 70 - 130 301.0



m&p-Xylene 105 99ND 5.9107 108 0.9 70 - 130 302.0

Methyl ethyl ketone 72 69ND 4.375 77 2.6 m70 - 130 305.0



Naphthalene 105 102ND 2.9104 109 4.7 70 - 130 305.0



o-Xylene 106 99ND 6.8107 108 0.9 70 - 130 302.0



Styrene 107 100ND 6.8109 111 1.8 70 - 130 305.0





Page 11 of 14

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ81780

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

Toluene 104 98ND 5.9104 111 6.5 70 - 130 301.0


trans-1,3-Dichloropropene 125 119ND 4.9124 133 7.0 l70 - 130 305.0



Trichlorofluoromethane 147 142ND 3.5142 147 3.5 l,m70 - 130 305.0

Trichlorotrifluoroethane 135 132ND 2.2133 137 3.0 l,m70 - 130 305.0





% Toluene-d8 100 10197 1.099 98 1.0 70 - 130 30%

A blank MS/MSD was analyzed with this batch.

Comment:

QA/QC Batch 319095 (ug/kg), QC Sample No: BJ83508 (BJ81796 (50X) , BJ81797 (50X) )





















1,4-dioxane 100 103ND 3.097 116 17.8 70 - 130 30100



2-Hexanone 85 86ND 1.288 94 6.6 70 - 130 3025




Acetone 60 59ND 1.771 76 6.8 m70 - 130 3010

Acrolein 51 50ND 2.092 98 6.3 m70 - 130 3025


Benzene 90 93ND 3.385 94 10.1 70 - 130 301.0

Bromobenzene 85 88ND 3.587 95 8.8 70 - 130 305.0



Bromoform 99 104ND 4.999 109 9.6 70 - 130 305.0

Bromomethane 57 69ND 19.091 98 7.4 m70 - 130 305.0

Page 12 of 14

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ81780

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits





Chloroform 86 94ND 8.990 98 8.5 70 - 130 305.0







Ethylbenzene 95 99ND 4.190 98 8.5 70 - 130 301.0



m&p-Xylene 95 99ND 4.190 97 7.5 70 - 130 302.0

Methyl ethyl ketone 75 73ND 2.772 81 11.8 70 - 130 305.0



Naphthalene 82 89ND 8.290 100 10.5 70 - 130 305.0



o-Xylene 96 102ND 6.193 102 9.2 70 - 130 302.0



Styrene 96 102ND 6.193 101 8.2 70 - 130 305.0





Toluene 91 93ND 2.287 95 8.8 70 - 130 301.0











% Toluene-d8 98 9999 1.099 99 0.0 70 - 130 30%

QA/QC Batch 318978 (ug/kg), QC Sample No: BJ84181 (BJ81801 (50X) )

Volatiles - Solid1,2,3-Trichlorobenzene 78 89ND 13.295 87 8.8 70 - 130 305.0









Page 13 of 14

QA/QC Data


MS%

MSD%

MSRPD

SDG I.D.: GBJ81780

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits




Bromobenzene 90 93ND 3.399 95 4.1 70 - 130 305.0



Naphthalene 83 92ND 10.3106 96 9.9 70 - 130 305.0










l = This parameter is outside laboratory lcs/lcsd specified recovery limits.m = This parameter is outside laboratory ms/msd specified recovery limits.r = This parameter is outside laboratory rpd specified recovery limits.




RPD - Relative Percent DifferenceLCS - Laboratory Control Sample

LCSD - Laboratory Control Sample Duplicate

NC - No Criteria

Intf - Interference

Page 14 of 14

Sample Criteria Exceedences ReportMonday, October 05, 2015 Page 1 of 13


UnitsCriteria

GBJ81780 - EBCCriteria: NY: 375, 375GWP, 375RRS, 375RS

RLCriteria

State: NY

$8270SMRDP Chrysene 10001100 260 ug/KgBJ81780 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP Benz(a)anthracene 10001100 260 ug/KgBJ81780 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP Benz(a)anthracene 10001100 260 ug/KgBJ81780 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Chrysene 10001100 260 ug/KgBJ81780 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 500680 260 ug/KgBJ81780 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Benz(a)anthracene 10001100 260 ug/KgBJ81780 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 500680 260 ug/KgBJ81780 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Benz(a)anthracene 10001100 260 ug/KgBJ81780 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(k)fluoranthene 800980 260 ug/KgBJ81780 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Chrysene 10001100 260 ug/KgBJ81780 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 500680 260 ug/KgBJ81780 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$PESTSMDPR Aldrin 5ND 5.5 ug/KgBJ81780 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 5$PESTSMDPR 4,4' -DDE 3.3ND 9.2 ug/KgBJ81780 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR Dieldrin 5ND 5.5 ug/KgBJ81780 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 5$PESTSMDPR Endrin 14ND 18 ug/KgBJ81780 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 14$PESTSMDPR 4,4' -DDD 3.3ND 15 ug/KgBJ81780 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR 4,4' -DDT 3.3ND 9.2 ug/KgBJ81780 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3

$8270SMRDP Chrysene 10001400 290 ug/KgBJ81783 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP Benz(a)anthracene 10001200 290 ug/KgBJ81783 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP Benz(a)anthracene 10001200 290 ug/KgBJ81783 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(b)fluoranthene 10001100 290 ug/KgBJ81783 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 500720 290 ug/KgBJ81783 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Chrysene 10001400 290 ug/KgBJ81783 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 10001200 290 ug/KgBJ81783 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(b)fluoranthene 10001100 290 ug/KgBJ81783 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 500720 290 ug/KgBJ81783 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Indeno(1,2,3-cd)pyrene 500720 290 ug/KgBJ81783 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$8270SMRDP Chrysene 10001400 290 ug/KgBJ81783 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(b)fluoranthene 10001100 290 ug/KgBJ81783 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benz(a)anthracene 10001200 290 ug/KgBJ81783 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(k)fluoranthene 800960 290 ug/KgBJ81783 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$PESTSMDPR a-BHC 20ND 21 ug/KgBJ81783 NY / 375-6.8 PCBs/Pesticides / Ground Water Protection 20$PESTSMDPR a-BHC 20ND 21 ug/KgBJ81783 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 20$PESTSMDPR Aldrin 5ND 6.2 ug/KgBJ81783 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 5$PESTSMDPR 4,4' -DDE 3.3ND 10 ug/KgBJ81783 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR Dieldrin 513 6.2 ug/KgBJ81783 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 5$PESTSMDPR Endrin 14ND 21 ug/KgBJ81783 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 14$PESTSMDPR 4,4' -DDD 3.3ND 10 ug/KgBJ81783 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR 4,4' -DDT 3.3ND 10 ug/KgBJ81783 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3

$8270SMRDP Indeno(1,2,3-cd)pyrene 500570 260 ug/KgBJ81786 NY / 375-6.8 Semivolatiles / Residential 500



UnitsCriteria


RLCriteria

State: NY

$8270SMRDP Indeno(1,2,3-cd)pyrene 500570 260 ug/KgBJ81786 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Indeno(1,2,3-cd)pyrene 500570 260 ug/KgBJ81786 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$PCB_SMRDP PCB-1260 100ND 180 ug/KgBJ81786 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 100$PCB_SMRDP PCB-1254 100ND 180 ug/KgBJ81786 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 100$PCB_SMRDP PCB-1248 100ND 180 ug/KgBJ81786 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 100$PCB_SMRDP PCB-1242 100ND 180 ug/KgBJ81786 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 100$PCB_SMRDP PCB-1232 100ND 180 ug/KgBJ81786 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 100$PCB_SMRDP PCB-1016 100ND 180 ug/KgBJ81786 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 100$PCB_SMRDP PCB-1221 100ND 180 ug/KgBJ81786 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 100$PESTSMDPR a-Chlordane 94110 3.7 ug/KgBJ81786 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 94$PESTSMDPR 4,4' -DDE 3.38.1 2.2 ug/KgBJ81786 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR Dieldrin 59.4 3.7 ug/KgBJ81786 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 5$PESTSMDPR 4,4' -DDD 3.3ND 5.0 ug/KgBJ81786 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR 4,4' -DDT 3.37.1 2.2 ug/KgBJ81786 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3HG-SM Mercury 0.180.19 0.03 mg/KgBJ81786 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18

$8270SMRDP Benzo(k)fluoranthene 17003400 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Ground Water Protection 1700$8270SMRDP Benz(a)anthracene 10003500 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP Chrysene 10003300 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP Benzo(b)fluoranthene 17004500 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Ground Water Protection 1700$8270SMRDP Benzo(a)pyrene 10003200 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Chrysene 10003300 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Dibenz(a,h)anthracene 3301400 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Residential 330$8270SMRDP Benzo(b)fluoranthene 10004500 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 5003900 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Benzo(k)fluoranthene 10003400 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 10003500 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 5003900 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Dibenz(a,h)anthracene 3301400 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Residential Restricted 330$8270SMRDP Benz(a)anthracene 10003500 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(b)fluoranthene 10004500 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 10003200 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benz(a)anthracene 10003500 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(k)fluoranthene 8003400 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Indeno(1,2,3-cd)pyrene 5003900 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$8270SMRDP Dibenz(a,h)anthracene 3301400 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP Benzo(a)pyrene 10003200 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(b)fluoranthene 10004500 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Chrysene 10003300 250 ug/KgBJ81789 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$PESTSMDPR Aldrin 5ND 5.5 ug/KgBJ81789 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 5$PESTSMDPR 4,4' -DDE 3.3ND 9.1 ug/KgBJ81789 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR Dieldrin 5ND 5.5 ug/KgBJ81789 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 5



UnitsCriteria


RLCriteria

State: NY

$PESTSMDPR Endrin 14ND 18 ug/KgBJ81789 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 14$PESTSMDPR 4,4' -DDD 3.3ND 9.1 ug/KgBJ81789 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR 4,4' -DDT 3.3ND 9.1 ug/KgBJ81789 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3CR-SM Chromium 3031.3 0.33 mg/KgBJ81789 NY / 375-6.8 Metals / Unrestricted Use SoilHG-SM Mercury 0.180.58 0.03 mg/KgBJ81789 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18NI-SM Nickel 3036.3 0.33 mg/KgBJ81789 NY / 375-6.8 Metals / Unrestricted Use Soil 30PB-SMDP Lead 63102 0.7 mg/KgBJ81789 NY / 375-6.8 Metals / Unrestricted Use Soil 63

$8270SMRDP Benzo(b)fluoranthene 170011000 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Ground Water Protection 1700$8270SMRDP Chrysene 100016000 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP Benz(a)anthracene 100016000 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP Pentachlorophenol 800ND 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Ground Water Protection 800$8270SMRDP Benzo(k)fluoranthene 170010000 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Ground Water Protection 1700$8270SMRDP Phenol 330ND 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Ground Water Protection 330$8270SMRDP 2-Methylphenol (o-cresol) 330ND 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Ground Water Protection 330$8270SMRDP Chrysene 100016000 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(k)fluoranthene 100010000 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Dibenz(a,h)anthracene 3301300 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Residential 330$8270SMRDP Benzo(b)fluoranthene 100011000 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 5007200 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Benzo(a)pyrene 100013000 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 100016000 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Pentachlorophenol 2400ND 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Residential 2400$8270SMRDP Indeno(1,2,3-cd)pyrene 5007200 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Chrysene 390016000 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Residential Restricted 3900$8270SMRDP Dibenz(a,h)anthracene 3301300 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Residential Restricted 330$8270SMRDP Benzo(k)fluoranthene 390010000 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Residential Restricted 3900$8270SMRDP Benzo(b)fluoranthene 100011000 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 100013000 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benz(a)anthracene 100016000 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Pentachlorophenol 800ND 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benzo(b)fluoranthene 100011000 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Phenol 330ND 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP Benzo(k)fluoranthene 80010000 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP 2-Methylphenol (o-cresol) 330ND 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP Indeno(1,2,3-cd)pyrene 5007200 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$8270SMRDP Benz(a)anthracene 100016000 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Dibenz(a,h)anthracene 3301300 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP Benzo(a)pyrene 100013000 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Chrysene 100016000 2600 ug/KgBJ81790 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000

$8270SMRDP Indeno(1,2,3-cd)pyrene 500600 250 ug/KgBJ81791 NY / 375-6.8 Semivolatiles / Residential 500



UnitsCriteria


RLCriteria

State: NY

$8270SMRDP Indeno(1,2,3-cd)pyrene 500600 250 ug/KgBJ81791 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Benzo(k)fluoranthene 800850 250 ug/KgBJ81791 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Indeno(1,2,3-cd)pyrene 500600 250 ug/KgBJ81791 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$PESTSMDPR a-BHC 20ND 36 ug/KgBJ81791 NY / 375-6.8 PCBs/Pesticides / Ground Water Protection 20$PESTSMDPR a-BHC 20ND 36 ug/KgBJ81791 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 20$PESTSMDPR Aldrin 5ND 18 ug/KgBJ81791 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 5$PESTSMDPR a-Chlordane 94130 18 ug/KgBJ81791 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 94$PESTSMDPR 4,4' -DDE 3.3ND 11 ug/KgBJ81791 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR Dieldrin 5ND 18 ug/KgBJ81791 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 5$PESTSMDPR Endrin 14ND 36 ug/KgBJ81791 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 14$PESTSMDPR 4,4' -DDD 3.3ND 60 ug/KgBJ81791 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR 4,4' -DDT 3.3ND 11 ug/KgBJ81791 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3

$8260MADPR Vinyl chloride 20290 250 ug/KgBJ81792 NY / 375-6.8 Volatiles / Ground Water Protection 20$8260MADPR Vinyl chloride 210290 250 ug/KgBJ81792 NY / 375-6.8 Volatiles / Residential 210$8260MADPR Vinyl chloride 20290 250 ug/KgBJ81792 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260MADPR Acetone 50ND 3000 ug/KgBJ81792 NY / 375-6.8 Volatiles / Ground Water Protection 50$8260MADPR Acetone 50ND 3000 ug/KgBJ81792 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260MADPR Methylene chloride 50ND 300 ug/KgBJ81792 NY / 375-6.8 Volatiles / Ground Water Protection 50$8260MADPR Methylene chloride 50ND 300 ug/KgBJ81792 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260MADPR cis-1,2-Dichloroethene 250870 300 ug/KgBJ81792 NY / 375-6.8 Volatiles / Ground Water Protection 250$8260MADPR cis-1,2-Dichloroethene 250870 300 ug/KgBJ81792 NY / 375-6.8 Volatiles / Unrestricted Use Soil 250$8260MADPR Methyl Ethyl Ketone 120ND 1800 ug/KgBJ81792 NY / 375-6.8 Volatiles / Ground Water Protection 120$8260MADPR Methyl Ethyl Ketone 120ND 1800 ug/KgBJ81792 NY / 375-6.8 Volatiles / Unrestricted Use Soil 120$8260MADPR Benzene 604100 3000 ug/KgBJ81792 NY / 375-6.8 Volatiles / Ground Water Protection 60$8260MADPR Benzene 29004100 3000 ug/KgBJ81792 NY / 375-6.8 Volatiles / Residential 2900$8260MADPR Benzene 604100 3000 ug/KgBJ81792 NY / 375-6.8 Volatiles / Unrestricted Use Soil 60$8260MADPR 1,2-Dichloroethane 20ND 300 ug/KgBJ81792 NY / 375-6.8 Volatiles / Ground Water Protection 20$8260MADPR 1,2-Dichloroethane 20ND 300 ug/KgBJ81792 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260MADPR Trichloroethene 4703300 300 ug/KgBJ81792 NY / 375-6.8 Volatiles / Ground Water Protection 470$8260MADPR Trichloroethene 4703300 300 ug/KgBJ81792 NY / 375-6.8 Volatiles / Unrestricted Use Soil 470$8260MADPR Toluene 7008600 3000 ug/KgBJ81792 NY / 375-6.8 Volatiles / Ground Water Protection 700$8260MADPR Toluene 7008600 3000 ug/KgBJ81792 NY / 375-6.8 Volatiles / Unrestricted Use Soil 700$8260MADPR Ethylbenzene 10007000 300 ug/KgBJ81792 NY / 375-6.8 Volatiles / Ground Water Protection 1000$8260MADPR Ethylbenzene 10007000 300 ug/KgBJ81792 NY / 375-6.8 Volatiles / Unrestricted Use Soil 1000$8260MADPR 1,3,5-Trimethylbenzene 84009600 300 ug/KgBJ81792 NY / 375-6.8 Volatiles / Ground Water Protection 8400$8260MADPR 1,3,5-Trimethylbenzene 84009600 300 ug/KgBJ81792 NY / 375-6.8 Volatiles / Unrestricted Use Soil 8400$8260MADPR 1,2,4-Trimethylbenzene 360014000 3000 ug/KgBJ81792 NY / 375-6.8 Volatiles / Ground Water Protection 3600$8260MADPR 1,2,4-Trimethylbenzene 360014000 3000 ug/KgBJ81792 NY / 375-6.8 Volatiles / Unrestricted Use Soil 3600$DIOX_SMR 1,4-dioxane 100ND 6000 ug/kgBJ81792 NY / 375-6.8 Volatiles / Ground Water Protection 100$DIOX_SMR 1,4-dioxane 100ND 6000 ug/kgBJ81792 NY / 375-6.8 Volatiles / Unrestricted Use Soil 100



UnitsCriteria


RLCriteria

State: NY

$8260MADPR Vinyl chloride 202600 700 ug/KgBJ81793 NY / 375-6.8 Volatiles / Ground Water Protection 20$8260MADPR Vinyl chloride 2102600 700 ug/KgBJ81793 NY / 375-6.8 Volatiles / Residential 210$8260MADPR Vinyl chloride 9002600 700 ug/KgBJ81793 NY / 375-6.8 Volatiles / Residential Restricted 900$8260MADPR Vinyl chloride 202600 700 ug/KgBJ81793 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260MADPR Acetone 50ND 7000 ug/KgBJ81793 NY / 375-6.8 Volatiles / Ground Water Protection 50$8260MADPR Acetone 50ND 7000 ug/KgBJ81793 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260MADPR Methylene chloride 50ND 700 ug/KgBJ81793 NY / 375-6.8 Volatiles / Ground Water Protection 50$8260MADPR Methylene chloride 50ND 700 ug/KgBJ81793 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260MADPR cis-1,2-Dichloroethene 2507600 700 ug/KgBJ81793 NY / 375-6.8 Volatiles / Ground Water Protection 250$8260MADPR cis-1,2-Dichloroethene 2507600 700 ug/KgBJ81793 NY / 375-6.8 Volatiles / Unrestricted Use Soil 250$8260MADPR Methyl Ethyl Ketone 120ND 4200 ug/KgBJ81793 NY / 375-6.8 Volatiles / Ground Water Protection 120$8260MADPR Methyl Ethyl Ketone 120ND 4200 ug/KgBJ81793 NY / 375-6.8 Volatiles / Unrestricted Use Soil 120$8260MADPR 1,1,1-Trichloroethane 680ND 700 ug/KgBJ81793 NY / 375-6.8 Volatiles / Ground Water Protection 680$8260MADPR 1,1,1-Trichloroethane 680ND 700 ug/KgBJ81793 NY / 375-6.8 Volatiles / Unrestricted Use Soil 680$8260MADPR Benzene 602800 700 ug/KgBJ81793 NY / 375-6.8 Volatiles / Ground Water Protection 60$8260MADPR Benzene 602800 700 ug/KgBJ81793 NY / 375-6.8 Volatiles / Unrestricted Use Soil 60$8260MADPR 1,2-Dichloroethane 20ND 700 ug/KgBJ81793 NY / 375-6.8 Volatiles / Ground Water Protection 20$8260MADPR 1,2-Dichloroethane 20ND 700 ug/KgBJ81793 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260MADPR Trichloroethene 4703700 700 ug/KgBJ81793 NY / 375-6.8 Volatiles / Ground Water Protection 470$8260MADPR Trichloroethene 4703700 700 ug/KgBJ81793 NY / 375-6.8 Volatiles / Unrestricted Use Soil 470$8270SMRDP Dibenzofuran 700012000 2900 ug/KgBJ81793 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 7000$8270SMRDP Chrysene 100013000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP Naphthalene 1200043000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Ground Water Protection 12000$8270SMRDP Benzo(k)fluoranthene 170010000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Ground Water Protection 1700$8270SMRDP Phenol 330ND 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Ground Water Protection 330$8270SMRDP Benzo(b)fluoranthene 17009900 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Ground Water Protection 1700$8270SMRDP Pentachlorophenol 800ND 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Ground Water Protection 800$8270SMRDP Benz(a)anthracene 100014000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP 2-Methylphenol (o-cresol) 330ND 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Ground Water Protection 330$8270SMRDP Benzo(a)pyrene 100013000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Pentachlorophenol 2400ND 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Residential 2400$8270SMRDP Benzo(b)fluoranthene 10009900 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 5006400 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Chrysene 100013000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Dibenz(a,h)anthracene 3302000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Residential 330$8270SMRDP Benzo(k)fluoranthene 100010000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 100014000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 5006400 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Dibenz(a,h)anthracene 3302000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Residential Restricted 330$8270SMRDP Chrysene 390013000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Residential Restricted 3900$8270SMRDP Benzo(k)fluoranthene 390010000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Residential Restricted 3900$8270SMRDP Benz(a)anthracene 100014000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Residential Restricted 1000



UnitsCriteria


RLCriteria

State: NY

$8270SMRDP Benzo(b)fluoranthene 10009900 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 100013000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP 2-Methylphenol (o-cresol) 330ND 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP Phenol 330ND 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP Pentachlorophenol 800ND 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benz(a)anthracene 100014000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Naphthalene 1200043000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 12000$8270SMRDP Benzo(a)pyrene 100013000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(b)fluoranthene 10009900 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Dibenz(a,h)anthracene 3302000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP Benzo(k)fluoranthene 80010000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Chrysene 100013000 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 5006400 2900 ug/KgBJ81793 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$DIOX_SMR 1,4-dioxane 100ND 14000 ug/kgBJ81793 NY / 375-6.8 Volatiles / Ground Water Protection 100$DIOX_SMR 1,4-dioxane 9800ND 14000 ug/kgBJ81793 NY / 375-6.8 Volatiles / Residential 9800$DIOX_SMR 1,4-dioxane 13000ND 14000 ug/kgBJ81793 NY / 375-6.8 Volatiles / Residential Restricted 13000$DIOX_SMR 1,4-dioxane 100ND 14000 ug/kgBJ81793 NY / 375-6.8 Volatiles / Unrestricted Use Soil 100$PESTSMDPR a-BHC 20ND 41 ug/KgBJ81793 NY / 375-6.8 PCBs/Pesticides / Ground Water Protection 20$PESTSMDPR a-BHC 20ND 41 ug/KgBJ81793 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 20$PESTSMDPR b-BHC 36ND 41 ug/KgBJ81793 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 36$PESTSMDPR d-BHC 40ND 41 ug/KgBJ81793 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 40$PESTSMDPR Aldrin 5ND 12 ug/KgBJ81793 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 5$PESTSMDPR 4,4' -DDE 3.3ND 20 ug/KgBJ81793 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR Dieldrin 5ND 12 ug/KgBJ81793 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 5$PESTSMDPR Endrin 14ND 41 ug/KgBJ81793 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 14$PESTSMDPR 4,4' -DDD 3.3ND 20 ug/KgBJ81793 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR 4,4' -DDT 3.3ND 25 ug/KgBJ81793 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3HG-SM Mercury 0.180.41 0.03 mg/KgBJ81793 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18PB-SMDP Lead 63121 0.8 mg/KgBJ81793 NY / 375-6.8 Metals / Unrestricted Use Soil 63

$8260MADPR Vinyl chloride 201100 400 ug/KgBJ81796 NY / 375-6.8 Volatiles / Ground Water Protection 20$8260MADPR Vinyl chloride 2101100 400 ug/KgBJ81796 NY / 375-6.8 Volatiles / Residential 210$8260MADPR Vinyl chloride 9001100 400 ug/KgBJ81796 NY / 375-6.8 Volatiles / Residential Restricted 900$8260MADPR Vinyl chloride 201100 400 ug/KgBJ81796 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260MADPR Acetone 50ND 4000 ug/KgBJ81796 NY / 375-6.8 Volatiles / Ground Water Protection 50$8260MADPR Acetone 50ND 4000 ug/KgBJ81796 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260MADPR Methylene chloride 50570 400 ug/KgBJ81796 NY / 375-6.8 Volatiles / Ground Water Protection 50$8260MADPR Methylene chloride 50570 400 ug/KgBJ81796 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260MADPR cis-1,2-Dichloroethene 2508700 400 ug/KgBJ81796 NY / 375-6.8 Volatiles / Ground Water Protection 250$8260MADPR cis-1,2-Dichloroethene 2508700 400 ug/KgBJ81796 NY / 375-6.8 Volatiles / Unrestricted Use Soil 250$8260MADPR Methyl Ethyl Ketone 120ND 2400 ug/KgBJ81796 NY / 375-6.8 Volatiles / Ground Water Protection 120$8260MADPR Methyl Ethyl Ketone 120ND 2400 ug/KgBJ81796 NY / 375-6.8 Volatiles / Unrestricted Use Soil 120



UnitsCriteria


RLCriteria

State: NY

$8260MADPR Benzene 60890 400 ug/KgBJ81796 NY / 375-6.8 Volatiles / Ground Water Protection 60$8260MADPR Benzene 60890 400 ug/KgBJ81796 NY / 375-6.8 Volatiles / Unrestricted Use Soil 60$8260MADPR 1,2-Dichloroethane 20ND 400 ug/KgBJ81796 NY / 375-6.8 Volatiles / Ground Water Protection 20$8260MADPR 1,2-Dichloroethane 20ND 400 ug/KgBJ81796 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260MADPR Trichloroethene 47014000 400 ug/KgBJ81796 NY / 375-6.8 Volatiles / Ground Water Protection 470$8260MADPR Trichloroethene 1000014000 400 ug/KgBJ81796 NY / 375-6.8 Volatiles / Residential 10000$8260MADPR Trichloroethene 47014000 400 ug/KgBJ81796 NY / 375-6.8 Volatiles / Unrestricted Use Soil 470$8270SMRDP Benzo(k)fluoranthene 17004600 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Ground Water Protection 1700$8270SMRDP Chrysene 10006100 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP Benzo(b)fluoranthene 17008800 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Ground Water Protection 1700$8270SMRDP Benz(a)anthracene 10006300 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP Benzo(k)fluoranthene 10004600 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 5006200 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Chrysene 10006100 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Dibenz(a,h)anthracene 3301900 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Residential 330$8270SMRDP Benzo(a)pyrene 10002100 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 10006300 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(b)fluoranthene 10008800 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 5006200 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Benzo(a)pyrene 10002100 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benz(a)anthracene 10006300 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(b)fluoranthene 10008800 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(k)fluoranthene 39004600 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Residential Restricted 3900$8270SMRDP Dibenz(a,h)anthracene 3301900 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Residential Restricted 330$8270SMRDP Chrysene 39006100 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Residential Restricted 3900$8270SMRDP Indeno(1,2,3-cd)pyrene 5006200 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$8270SMRDP Dibenz(a,h)anthracene 3301900 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP Benz(a)anthracene 10006300 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(k)fluoranthene 8004600 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benzo(b)fluoranthene 10008800 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(a)pyrene 10002100 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Chrysene 10006100 310 ug/KgBJ81796 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$DIOX_SMR 1,4-dioxane 100ND 8000 ug/kgBJ81796 NY / 375-6.8 Volatiles / Ground Water Protection 100$DIOX_SMR 1,4-dioxane 100ND 8000 ug/kgBJ81796 NY / 375-6.8 Volatiles / Unrestricted Use Soil 100$PESTSMDPR a-BHC 20ND 44 ug/KgBJ81796 NY / 375-6.8 PCBs/Pesticides / Ground Water Protection 20$PESTSMDPR a-BHC 20ND 44 ug/KgBJ81796 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 20$PESTSMDPR b-BHC 36ND 44 ug/KgBJ81796 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 36$PESTSMDPR Heptachlor 42ND 44 ug/KgBJ81796 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 42$PESTSMDPR d-BHC 40ND 44 ug/KgBJ81796 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 40$PESTSMDPR Aldrin 5ND 13 ug/KgBJ81796 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 5$PESTSMDPR 4,4' -DDE 3.3ND 27 ug/KgBJ81796 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR Dieldrin 39ND 44 ug/KgBJ81796 NY / 375-6.8 PCBs/Pesticides / Residential 39



UnitsCriteria


RLCriteria

State: NY

$PESTSMDPR Dieldrin 5ND 44 ug/KgBJ81796 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 5$PESTSMDPR Endrin 60ND 89 ug/KgBJ81796 NY / 375-6.8 PCBs/Pesticides / Ground Water Protection 60$PESTSMDPR Endrin 14ND 89 ug/KgBJ81796 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 14$PESTSMDPR 4,4' -DDD 3.3ND 27 ug/KgBJ81796 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR 4,4' -DDT 3.3ND 27 ug/KgBJ81796 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3PB-SMDP Lead 63107 0.9 mg/KgBJ81796 NY / 375-6.8 Metals / Unrestricted Use Soil 63

$PESTSMDPR 4,4' -DDE 3.34.0 2.1 ug/KgBJ81797 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR 4,4' -DDD 3.34.3 3.3 ug/KgBJ81797 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3PB-SMDP Lead 6379.2 0.7 mg/KgBJ81797 NY / 375-6.8 Metals / Unrestricted Use Soil 63

$8260MADPR cis-1,2-Dichloroethene 250570 240 ug/KgBJ81798 NY / 375-6.8 Volatiles / Ground Water Protection 250$8260MADPR cis-1,2-Dichloroethene 250570 240 ug/KgBJ81798 NY / 375-6.8 Volatiles / Unrestricted Use Soil 250$8270SMRDP Benzo(b)fluoranthene 17002300 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Ground Water Protection 1700$8270SMRDP Chrysene 10001800 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP Benzo(k)fluoranthene 17002900 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Ground Water Protection 1700$8270SMRDP Benz(a)anthracene 10001800 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP Benzo(k)fluoranthene 10002900 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 5003400 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Chrysene 10001800 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(b)fluoranthene 10002300 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(a)pyrene 10003600 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 10001800 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Dibenz(a,h)anthracene 330500 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Residential 330$8270SMRDP Benzo(b)fluoranthene 10002300 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 5003400 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Benz(a)anthracene 10001800 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Dibenz(a,h)anthracene 330500 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Residential Restricted 330$8270SMRDP Benzo(a)pyrene 10003600 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 5003400 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$8270SMRDP Dibenz(a,h)anthracene 330500 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP Benzo(k)fluoranthene 8002900 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benzo(b)fluoranthene 10002300 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(a)pyrene 10003600 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Chrysene 10001800 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benz(a)anthracene 10001800 280 ug/KgBJ81798 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000

$8260MADPR Vinyl chloride 20ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 20$8260MADPR Vinyl chloride 210ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Residential 210$8260MADPR Vinyl chloride 900ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Residential Restricted 900$8260MADPR Vinyl chloride 20ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260MADPR 1,1-Dichloroethene 330ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 330$8260MADPR 1,1-Dichloroethene 330ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 330



UnitsCriteria


RLCriteria

State: NY

$8260MADPR Acetone 50ND 60000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 50$8260MADPR Acetone 50ND 60000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260MADPR Methylene chloride 50ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 50$8260MADPR Methylene chloride 50ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260MADPR trans-1,2-Dichloroethene 190ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 190$8260MADPR trans-1,2-Dichloroethene 190ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 190$8260MADPR 1,1-Dichloroethane 270ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 270$8260MADPR 1,1-Dichloroethane 270ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 270$8260MADPR cis-1,2-Dichloroethene 250730 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 250$8260MADPR cis-1,2-Dichloroethene 250730 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 250$8260MADPR Methyl Ethyl Ketone 120ND 36000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 120$8260MADPR Methyl Ethyl Ketone 120ND 36000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 120$8260MADPR Chloroform 370ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 370$8260MADPR Chloroform 370ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 370$8260MADPR 1,1,1-Trichloroethane 680ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 680$8260MADPR 1,1,1-Trichloroethane 680ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 680$8260MADPR Methyl t-butyl ether (MTBE) 930ND 12000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 930$8260MADPR Methyl t-butyl ether (MTBE) 930ND 12000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 930$8260MADPR Carbon tetrachloride 760ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 760$8260MADPR Carbon tetrachloride 1400ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Residential 1400$8260MADPR Carbon tetrachloride 2400ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Residential Restricted 2400$8260MADPR Carbon tetrachloride 760ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 760$8260MADPR Benzene 608600 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 60$8260MADPR Benzene 29008600 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Residential 2900$8260MADPR Benzene 48008600 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Residential Restricted 4800$8260MADPR Benzene 608600 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 60$8260MADPR 1,2-Dichloroethane 20ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 20$8260MADPR 1,2-Dichloroethane 2300ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Residential 2300$8260MADPR 1,2-Dichloroethane 3100ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Residential Restricted 3100$8260MADPR 1,2-Dichloroethane 20ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260MADPR Trichloroethene 470ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 470$8260MADPR Trichloroethene 470ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 470$8260MADPR Toluene 70022000 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 700$8260MADPR Toluene 70022000 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 700$8260MADPR Tetrachloroethene 1300ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 1300$8260MADPR Tetrachloroethene 5500ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Residential 5500$8260MADPR Tetrachloroethene 1300ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 1300$8260MADPR Chlorobenzene 1100ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 1100$8260MADPR Chlorobenzene 1100ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 1100$8260MADPR Ethylbenzene 100021000 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 1000$8260MADPR Ethylbenzene 100021000 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 1000$8260MADPR n-Propylbenzene 3900ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 3900



UnitsCriteria


RLCriteria

State: NY

$8260MADPR n-Propylbenzene 3900ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 3900$8260MADPR 1,3,5-Trimethylbenzene 840016000 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 8400$8260MADPR 1,3,5-Trimethylbenzene 840016000 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 8400$8260MADPR tert-Butylbenzene 5900ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 5900$8260MADPR tert-Butylbenzene 5900ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 5900$8260MADPR 1,2,4-Trimethylbenzene 360027000 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 3600$8260MADPR 1,2,4-Trimethylbenzene 360027000 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 3600$8260MADPR 1,3-Dichlorobenzene 2400ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 2400$8260MADPR 1,3-Dichlorobenzene 2400ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 2400$8260MADPR 1,4-Dichlorobenzene 1800ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 1800$8260MADPR 1,4-Dichlorobenzene 1800ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 1800$8260MADPR 1,2-Dichlorobenzene 1100ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 1100$8260MADPR 1,2-Dichlorobenzene 1100ND 6000 ug/KgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 1100$8270SMRDP Phenol 330ND 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Ground Water Protection 330$8270SMRDP Phenol 330ND 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP 2-Methylphenol (o-cresol) 330ND 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Ground Water Protection 330$8270SMRDP 2-Methylphenol (o-cresol) 330ND 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP Naphthalene 12000190000 14000 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Ground Water Protection 12000$8270SMRDP Naphthalene 100000190000 14000 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Residential 100000$8270SMRDP Naphthalene 100000190000 14000 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Residential Restricted 100000$8270SMRDP Naphthalene 12000190000 14000 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 12000$8270SMRDP Dibenzofuran 700043000 2900 ug/KgBJ81799 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 7000$8270SMRDP Fluorene 3000066000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 30000$8270SMRDP Pentachlorophenol 800ND 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Ground Water Protection 800$8270SMRDP Pentachlorophenol 2400ND 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Residential 2400$8270SMRDP Pentachlorophenol 800ND 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Phenanthrene 100000140000 14000 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Residential 100000$8270SMRDP Phenanthrene 100000140000 14000 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Residential Restricted 100000$8270SMRDP Phenanthrene 100000140000 14000 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 100000$8270SMRDP Benz(a)anthracene 100041000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP Benz(a)anthracene 100041000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 100041000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benz(a)anthracene 100041000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Chrysene 100038000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP Chrysene 100038000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Chrysene 390038000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Residential Restricted 3900$8270SMRDP Chrysene 100038000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(b)fluoranthene 170021000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Ground Water Protection 1700$8270SMRDP Benzo(b)fluoranthene 100021000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(b)fluoranthene 100021000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(b)fluoranthene 100021000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(k)fluoranthene 170026000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Ground Water Protection 1700



UnitsCriteria


RLCriteria

State: NY

$8270SMRDP Benzo(k)fluoranthene 100026000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(k)fluoranthene 390026000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Residential Restricted 3900$8270SMRDP Benzo(k)fluoranthene 80026000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benzo(a)pyrene 2200028000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Ground Water Protection 22000$8270SMRDP Benzo(a)pyrene 100028000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(a)pyrene 100028000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 100028000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 820011000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Ground Water Protection 8200$8270SMRDP Indeno(1,2,3-cd)pyrene 50011000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Indeno(1,2,3-cd)pyrene 50011000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Indeno(1,2,3-cd)pyrene 50011000 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$8270SMRDP Dibenz(a,h)anthracene 3303800 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Residential 330$8270SMRDP Dibenz(a,h)anthracene 3303800 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Residential Restricted 330$8270SMRDP Dibenz(a,h)anthracene 3303800 2900 ug/KgBJ81799 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$DIOX_SMR 1,4-dioxane 100ND 120000 ug/kgBJ81799 NY / 375-6.8 Volatiles / Ground Water Protection 100$DIOX_SMR 1,4-dioxane 9800ND 120000 ug/kgBJ81799 NY / 375-6.8 Volatiles / Residential 9800$DIOX_SMR 1,4-dioxane 13000ND 120000 ug/kgBJ81799 NY / 375-6.8 Volatiles / Residential Restricted 13000$DIOX_SMR 1,4-dioxane 100ND 120000 ug/kgBJ81799 NY / 375-6.8 Volatiles / Unrestricted Use Soil 100$PESTSMDPR a-BHC 20ND 41 ug/KgBJ81799 NY / 375-6.8 PCBs/Pesticides / Ground Water Protection 20$PESTSMDPR a-BHC 20ND 41 ug/KgBJ81799 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 20$PESTSMDPR b-BHC 36ND 41 ug/KgBJ81799 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 36$PESTSMDPR d-BHC 40ND 41 ug/KgBJ81799 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 40$PESTSMDPR Aldrin 5ND 12 ug/KgBJ81799 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 5$PESTSMDPR a-Chlordane 94170 41 ug/KgBJ81799 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 94$PESTSMDPR 4,4' -DDE 3.3ND 40 ug/KgBJ81799 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR Dieldrin 5ND 12 ug/KgBJ81799 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 5$PESTSMDPR Endrin 14ND 41 ug/KgBJ81799 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 14$PESTSMDPR 4,4' -DDD 3.3ND 60 ug/KgBJ81799 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR 4,4' -DDT 3.3ND 30 ug/KgBJ81799 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3

$8270SMRDP Indeno(1,2,3-cd)pyrene 500710 250 ug/KgBJ81800 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Indeno(1,2,3-cd)pyrene 500710 250 ug/KgBJ81800 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Benzo(k)fluoranthene 800870 250 ug/KgBJ81800 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Indeno(1,2,3-cd)pyrene 500710 250 ug/KgBJ81800 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$PESTSMDPR a-BHC 20ND 35 ug/KgBJ81800 NY / 375-6.8 PCBs/Pesticides / Ground Water Protection 20$PESTSMDPR a-BHC 20ND 35 ug/KgBJ81800 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 20$PESTSMDPR Aldrin 5ND 11 ug/KgBJ81800 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 5$PESTSMDPR 4,4' -DDE 3.3ND 21 ug/KgBJ81800 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR Dieldrin 5ND 11 ug/KgBJ81800 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 5$PESTSMDPR Endrin 14ND 35 ug/KgBJ81800 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 14$PESTSMDPR 4,4' -DDD 3.3ND 21 ug/KgBJ81800 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR 4,4' -DDT 3.3ND 21 ug/KgBJ81800 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3



UnitsCriteria


RLCriteria

State: NY

HG-SM Mercury 0.180.23 0.03 mg/KgBJ81800 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18

$8270SMRDP Benzo(b)fluoranthene 17002200 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Ground Water Protection 1700$8270SMRDP Benzo(k)fluoranthene 17002700 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Ground Water Protection 1700$8270SMRDP Chrysene 10002600 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP Benz(a)anthracene 10002700 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP Benzo(a)pyrene 10003000 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Dibenz(a,h)anthracene 330440 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Residential 330$8270SMRDP Chrysene 10002600 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 5001600 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Benzo(b)fluoranthene 10002200 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(k)fluoranthene 10002700 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 10002700 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Dibenz(a,h)anthracene 330440 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Residential Restricted 330$8270SMRDP Indeno(1,2,3-cd)pyrene 5001600 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Benzo(b)fluoranthene 10002200 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 10003000 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benz(a)anthracene 10002700 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 10003000 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Chrysene 10002600 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benz(a)anthracene 10002700 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Dibenz(a,h)anthracene 330440 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP Benzo(k)fluoranthene 8002700 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Indeno(1,2,3-cd)pyrene 5001600 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$8270SMRDP Benzo(b)fluoranthene 10002200 260 ug/KgBJ81801 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000

$8260MADPR Benzene 60160 60 ug/KgBJ81802 NY / 375-6.8 Volatiles / Ground Water Protection 60$8260MADPR Benzene 60160 60 ug/KgBJ81802 NY / 375-6.8 Volatiles / Unrestricted Use Soil 60$8270SMRDP Benz(a)anthracene 10008000 1500 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP Benz(a)anthracene 10008000 1500 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 10008000 1500 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benz(a)anthracene 10008000 1500 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Chrysene 10008200 1500 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Ground Water Protection 1000$8270SMRDP Chrysene 10008200 1500 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Chrysene 39008200 1500 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Residential Restricted 3900$8270SMRDP Chrysene 10008200 1500 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(b)fluoranthene 17009700 1500 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Ground Water Protection 1700$8270SMRDP Benzo(b)fluoranthene 10009700 1500 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(b)fluoranthene 10009700 1500 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(b)fluoranthene 10009700 1500 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(k)fluoranthene 17006500 290 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Ground Water Protection 1700$8270SMRDP Benzo(k)fluoranthene 10006500 290 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Residential 1000



UnitsCriteria


RLCriteria

State: NY

$8270SMRDP Benzo(k)fluoranthene 39006500 290 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Residential Restricted 3900$8270SMRDP Benzo(k)fluoranthene 8006500 290 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benzo(a)pyrene 100014000 1500 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(a)pyrene 100014000 1500 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 100014000 1500 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 5007400 1500 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Indeno(1,2,3-cd)pyrene 5007400 1500 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Indeno(1,2,3-cd)pyrene 5007400 1500 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$8270SMRDP Dibenz(a,h)anthracene 3304200 290 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Residential 330$8270SMRDP Dibenz(a,h)anthracene 3304200 290 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Residential Restricted 330$8270SMRDP Dibenz(a,h)anthracene 3304200 290 ug/KgBJ81802 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$PESTSMDPR a-BHC 20ND 42 ug/KgBJ81802 NY / 375-6.8 PCBs/Pesticides / Ground Water Protection 20$PESTSMDPR a-BHC 20ND 42 ug/KgBJ81802 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 20$PESTSMDPR b-BHC 36ND 42 ug/KgBJ81802 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 36$PESTSMDPR d-BHC 40ND 42 ug/KgBJ81802 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 40$PESTSMDPR Aldrin 5ND 12 ug/KgBJ81802 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 5$PESTSMDPR 4,4' -DDE 3.3ND 25 ug/KgBJ81802 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR Dieldrin 5ND 15 ug/KgBJ81802 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 5$PESTSMDPR Endrin 14ND 42 ug/KgBJ81802 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 14$PESTSMDPR 4,4' -DDD 3.3ND 25 ug/KgBJ81802 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR 4,4' -DDT 3.3ND 25 ug/KgBJ81802 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3


NY Temperature NarrationOctober 05, 2015



SDG I.D.: GBJ81780

The samples in this delivery group were received at 2°C.(Note acceptance criteria is above freezing up to 6°C)

Page 1 of 1

APPENDIX - F DUSRs

Page 1 of 12 Environmental Business Consultants SDG #: GBJ81780

DATA USABILITY SUMMARY REPORT (DUSR) SEMI-VOLATILE ORGANIC COMPOUNDS

USEPA Region II –Data Validation Project Name: 510 Driggs Avenue Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBJ81780 Client: Environmental Business Consultants Date: 12/31/2015 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for twenty-three (23) soil samples analyzed

for Semi-volatiles by SW-846 Method 8270D in accordance with the NYSDEC, Analytical Services Protocol (ASP) Format.

2. The samples were collected on 08/25/2015. The samples were submitted to Phoenix

Environmental Laboratories, Inc., Manchester, CT on 08/26/2015 for analysis. 3. The USEPA Region-II SOP HW-35, Revision 2, March 2013, Validating Semivolatile

Organic Compounds by Gas Chromatography/Mass Spectrometry, SW-846 Method 8270D was used in evaluating the Semi-volatiles data in this summary report.

4. In general, the data are valid as reported and may be used for decision making purposes.

Selected data points were qualified due to nonconformance of certain Quality Control criteria (see discussion below).


Samples: The samples included in this review are listed below:

Client Sample ID Laboratory Sample ID

Collection Date

Analysis Matrix Sample Status

14B8(0-5) BJ81780 8/25/15 SVO Soil 14B8(10-15) BJ81781 8/25/15 SVO Soil 14B8(20-25) BJ81782 8/25/15 SVO Soil 14B7(0-5) BJ81783 8/25/15 SVO Soil

14B7(10-15) BJ81784 8/25/15 SVO Soil 14B7(15-20) BJ81785 8/25/15 SVO Soil 14B2(0-5) BJ81786 8/25/15 SVO Soil


14B1(10-15) BJ81790 8/25/15 SVO Soil 14B3(0-5) BJ81791 8/25/15 SVO Soil




14B5(10-15) BJ81801 8/25/15 SVO Soil 14B5(15-19.5) BJ81802 8/25/15 SVO Soil

Sample Conditions/Problems: 1. The Traffic Reports/Chain-of-Custody Records, Sampling Report and/or Laboratory Case

Narrative did not indicate any problems with sample receipt, condition of samples, analytical problems or special circumstances affecting the quality of the data. No qualifications were required.

Holding Times: 1. All soil samples were extracted within 14 days from sample collection and analyzed

within 40 days following sample extraction. No qualifications were required.


GC/MS Tuning: 1. All of the DFTPP tunes in the initial and continuing calibrations met the percent relative

abundance criteria. No qualifications were required. Initial Calibration:

1. Initial calibration curve analyzed on 08/24/2015 (CHEM05) exhibited acceptable %RSDs (0.0%) for CCC compounds and average RRF values for SPCC compounds. Also, %RSDs for all other compounds were 20.0% and average RRF (>0.050) with the following exception(s):

Compound %RSD Pentachlorophenol 22.6

Client Sample ID Laboratory

Sample ID Compound Action

14B8(20-25) BJ81782 Pentachlorophenol UJ 14B7(0-5) BJ81783 Pentachlorophenol UJ

14B7(10-15) BJ81784 Pentachlorophenol UJ 14B7(15-20) BJ81785 Pentachlorophenol UJ 14B2(0-5) BJ81786 Pentachlorophenol UJ

14B2(10-15) BJ81787 Pentachlorophenol UJ 14B2(20-25) BJ81788 Pentachlorophenol UJ 14B1(0-5) BJ81789 Pentachlorophenol UJ 14B3(0-5) BJ81791 Pentachlorophenol UJ

14B3(10-15) BJ81792 Pentachlorophenol UJ 14B6(10-15) BJ81795 Pentachlorophenol UJ 14B6(15-17) BJ81796 Pentachlorophenol UJ 14B4(0-5) BJ81797 Pentachlorophenol UJ

14B5(10-15) BJ81801 Pentachlorophenol UJ 14B5(15-19.5) BJ81802 Pentachlorophenol UJ

14B8(0-5) BJ81780 Pentachlorophenol UJ 14B8(10-15) BJ81781 Pentachlorophenol UJ 14B1(10-15)

DL10 BJ81790 Pentachlorophenol UJ

14B3(15-18) DL10

BJ81793 Pentachlorophenol UJ

14B6(0-5) BJ81794 Pentachlorophenol UJ 14B4(20-21)

DL10 BJ81799 Pentachlorophenol UJ

14B4(20-21) BJ81799 Pentachlorophenol UJ



Compound Action

DL50 14B5(0-5) BJ81800 Pentachlorophenol UJ

14B5(15-19.5) DL5

BJ81802 Pentachlorophenol UJ

2. Initial calibration curve analyzed on 08/24/2015 (CHEM25) exhibited acceptable %RSDs

(0.0%) for CCC compounds and average RRF values for SPCC compounds. Also, %RSDs for all other compounds were 20.0% and average RRF (>0.050). No qualifications were required.

Continuing Calibration Verification (CCV): 1. CCV analyzed on 08/26/2015 @ 19:56 (CHEM05) exhibited acceptable %Ds (0.0%)

for CCC compounds and RRF values for SPCC compounds. Also, %Ds for all other compounds were .0% with the following exception(s):

Compound %D Benzidine -29.8



14B8(20-25) BJ81782 Benzidine UJ 14B7(0-5) BJ81783 Benzidine UJ

14B7(10-15) BJ81784 Benzidine UJ 14B7(15-20) BJ81785 Benzidine UJ 14B2(0-5) BJ81786 Benzidine UJ

14B2(10-15) BJ81787 Benzidine UJ 14B2(20-25) BJ81788 Benzidine UJ 14B1(0-5) BJ81789 Benzidine UJ 14B3(0-5) BJ81791 Benzidine UJ

14B3(10-15) BJ81792 Benzidine UJ 14B6(10-15) BJ81795 Benzidine UJ 14B6(15-17) BJ81796 Benzidine UJ 14B4(0-5) BJ81797 Benzidine UJ

14B5(10-15) BJ81801 Benzidine UJ 14B5(15-19.5) BJ81802 Benzidine UJ

2. CCV analyzed on 8/27/2015 @ 07:07 (CHEM05) exhibited acceptable %Ds (0.0%)

for CCC compounds and RRF values for SPCC compounds. Also, %Ds for all other compounds were 0.0% with the following exception(s):


Compound %D Hexachlorocyclopentadiene 79.0

2,4-Dinitrophenol 59.8 4,6-Dinitro-2-methylphenol 51.5



14B8(20-25) BJ81782 Hexachlorocyclopentadiene, 2,4-Dinitrophenol, 4,6-Dinitro-2-methylphenol

UJ


UJ


UJ


UJ


UJ


UJ


UJ


UJ


UJ


UJ


UJ


UJ


UJ


UJ

14B5(15-19.5) BJ81802 Hexachlorocyclopentadiene, 2,4-Dinitrophenol, 4,6-Dinitro-2-methylphenol

UJ


for CCC compounds and RRF values for SPCC compounds. Also, %Ds for all other compounds were .0% with the following exception(s):


Compound %D Benzidine(1) -27.3

(1) Results for this compound were previously qualified due to ICV criteria.


Compound Action

14B8(0-5) BJ81780 Benzidine UJ 14B8(10-15) BJ81781 Benzidine UJ 14B1(10-15)

DL10 BJ81790 Benzidine UJ

14B3(15-18) DL10

BJ81793 Benzidine UJ

14B6(0-5) BJ81794 Benzidine UJ 14B4(20-21)


14B4(20-21) DL50

BJ81799 Benzidine UJ

14B5(0-5) BJ81800 Benzidine UJ 14B5(15-19.5)




Compound %D

Hexachlorocyclopentadiene 89.9 2,4-Dinitrophenol 72.6

4,6-Dinitro-2-methylphenol 61.4


Compound Action


UJ


UJ

14B1(10-15) DL10

BJ81790 Hexachlorocyclopentadiene, 2,4-Dinitrophenol, 4,6-Dinitro-2-methylphenol

UJ

14B3(15-18) DL10


UJ


UJ

14B4(20-21) BJ81799 Hexachlorocyclopentadiene, 2,4-Dinitrophenol, UJ



Compound Action

DL10 4,6-Dinitro-2-methylphenol 14B4(20-21)

DL50 BJ81799 Hexachlorocyclopentadiene, 2,4-Dinitrophenol,

4,6-Dinitro-2-methylphenol UJ

14B5(0-5) BJ81800 Hexachlorocyclopentadiene 2,4-Dinitrophenol

4,6-Dinitro-2-methylphenol

R(1) UJ UJ

14B5(15-19.5) DL5


None

(1) Result for this compound was qualified due to low MS/MSD criteria. 5. CCV analyzed on 08/27/2015 @ 08:26 (CHEM25) exhibited acceptable %Ds (0.0%)

for CCC compounds and RRF values for SPCC compounds. Also, %Ds for all other compounds were .0%. No qualifications were required.



Compound %D

Hexachlorocyclopentadiene 59.4 2,4-Dinitrophenol 84.5

4,6-Dinitro-2-Methylphenol 66.2


Compound Action

14B4(10-15) BJ81798 Hexachlorocyclopentadiene, 2,4-Dinitrophenol, 4,6-Dinitro-2-Methylphenol

UJ

Surrogates: 1. Surrogate %REC values were within the QC acceptance limits. No qualifications were

required. Note: Due to high dilutions the following samples could not be evaluated based on surrogate recovery QC: 14B1(10-15), 14B3(15-18), and 14B4(20-21).

Internal Standard (IS) Area Performance: 1. All samples exhibited acceptable area count for all six internal standards with the

following exception(s):


Client Sample ID

Laboratory Sample ID

IS Compound Action

14B8(10-15) BJ81781 1,4-Dichlorobenzene-d4 (low)

N-Nitrosodimethylamine, pyridine, Phenol, Bis(2-chloroethyl)ether, Aniline, 2-Chlorophenol,

1,3-Dichlorobenzene, 1,4-Dichlorobenzene, 1,2-Dichlorobenzene, 2-Methylphenol,

N-Nitrosodi-n-propylamine, 3&4-methylphenol, acetophenone, hexachloroethane, nitrobenzene

UJ

14B5(0-5) BJ81800 Chrysene-d-12 (low) Perylene-d12 (low)

benz(a)anthracene, chrysene, benzo(b)fluoranthene, benzo(k)fluoranthene,

benzo(a)pyrene, indeno(1,2,3-cd)pyrene, dibenz(a,h)anthracene, benzo(ghi)perylene

bis(2-ethylhexyl)phthalate di-n-octylphthalate,

Benzyl butyl phthalate, 3,3’-dichlorobenzidine,

J J J J J

UJ UJ


benz(a)anthracene, chrysene, benzo(b)fluoranthene, benzo(k)fluoranthene,

benzo(a)pyrene, indeno(1,2,3-cd)pyrene, dibenz(a,h)anthracene, benzo(ghi)perylene

bis(2-ethylhexyl)phthalate di-n-octylphthalate, Benzyl butyl phthalate, 3,3’-dichlorobenzidine,

J J J J

UJ UJ


indeno(1,2,3-cd)pyrene, benz(a)anthracene, chrysene, benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthene, benzo(ghi)perylene dibenz(a,h)anthracene,

bis(2-ethylhexyl)phthalate, di-n-octylphthalate, Benzyl butyl phthalate, 3,3’-dichlorobenzidine,

J UJ UJ UJ UJ UJ


benz(a)anthracene, chrysene, benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthene, indeno(1,2,3-cd)pyrene, benzo(ghi)perylene

bis(2-ethylhexyl)phthalate, di-n-octylphthalate, dibenz(a,h)anthracene, Benzyl butyl phthalate,

3,3’-dichlorobenzidine,

J J J

UJ UJ UJ

14B4(20-21) BJ81799 Perylene-d12 (low) benzo(b)fluoranthene, benzo(k)fluoranthene, benzo(a)pyrene,

indeno(1,2,3-cd)pyrene, dibenz(a,h)anthracene, benzo(ghi)perylene

J

Method Blank (MB), Storage Blank (SB), Trip Blank (TB), Field Blank (FB), Rinsate Blank (RB) and Equipment Blank (EB): 1. Method Blank (BJ81785 BLANK) associated with the soil samples extracted on

8/26/2015 and analyzed on 8/27/2015 was free of contamination. No qualifications were required.

2. Method Blank (BJ81800 BLANK) associated with the soil samples extracted on



Laboratory Control Sample (LCS)/ Laboratory Control Sample Duplicate (LCSD): 1. Laboratory Control Sample (LCS)/Laboratory Control Sample Duplicate (LCSD)

associated with Batch ID: BJ81785 were analyzed on 08/27/2015. All %RECs/RPDs were within the laboratory control limits with the following exception(s):

Compound %R/%R/RPD Sample

Affected Action

Benzoic Acid 8/6/35.5 14B8(20-25), 14B7(0-5), 14B7(10-15), 14B7(15-20), 14B2(0-5), 14B2(10-15),

14B2(20-25), 14B1(0-5), 14B3(0-5), 14B3(10-15), 14B6(10-15), 14B6(15-17), 14B4(0-5),

14B5(10-15), 14B5(15-19.5), 14B8(0-5), 14B8(10-15), 14B1(10-15) DL10, 14B3(15-18)

DL10, 14B6(0-5), 14B4(20-21) DL10, 14B4(20-21) DL50, 14B5(0-5),

14B5(15-19.5) DL5

R

2,4-Dinitrophenol A/12/100 14B8(20-25), 14B7(0-5), 14B7(10-15), 14B7(15-20), 14B2(0-5), 14B2(10-15),

14B2(20-25), 14B1(0-5), 14B3(0-5), 14B3(10-15), 14B6(10-15), 14B6(15-17), 14B4(0-5),

14B5(10-15), 14B5(15-19.5), 14B8(0-5), 14B8(10-15), 14B1(10-15) DL10, 14B3(15-18)

DL10, 14B6(0-5), 14B4(20-21) DL10, 14B4(20-21) DL50, 14B5(0-5),

14B5(15-19.5) DL5

UJ(1)

4,6-Dinitro-2-methyphenol A/A/75.0 14B8(20-25), 14B7(0-5), 14B7(10-15), 14B7(15-20), 14B2(0-5), 14B2(10-15),

14B2(20-25), 14B1(0-5), 14B3(0-5), 14B3(10-15), 14B6(10-15), 14B6(15-17), 14B4(0-5),

14B5(10-15), 14B5(15-19.5), 14B8(0-5), 14B8(10-15), 14B1(10-15) DL10, 14B3(15-18)

DL10, 14B6(0-5), 14B4(20-21) DL10, 14B4(20-21) DL50, 14B5(0-5),

14B5(15-19.5) DL5

UJ(1)

Pentachlorophenol A/A/36.8 14B8(20-25), 14B7(0-5), 14B7(10-15), 14B7(15-20), 14B2(0-5), 14B2(10-15),

14B2(20-25), 14B1(0-5), 14B3(0-5), 14B3(10-15), 14B6(10-15), 14B6(15-17), 14B4(0-5),

14B5(10-15), 14B5(15-19.5), 14B8(0-5), 14B8(10-15), 14B1(10-15) DL10, 14B3(15-18)

DL10, 14B6(0-5), 14B4(20-21) DL10, 14B4(20-21) DL50, 14B5(0-5),

14B5(15-19.5) DL5

UJ(1)

A= Acceptable


(1) Results were previously qualified due to ICV/CCV criteria. 2. Laboratory Control Sample (LCS)/Laboratory Control Sample Duplicate (LCSD)

associated with Batch ID: BJ81800 were analyzed on 08/26/2015. All %RECs/RPDs were within the laboratory control limits with the following exception(s):


Affected Action

Pyridine 26/26/A 14B4(10-15) UJ Benzoic Acid 3/4/46.6 14B4(10-15) R

2,4-Dinitrophenol 14/22/44.4 14B4(10-15) UJ A= Acceptable Field Duplicate: 1. A field duplicate pair was not submitted with this SDG. Matrix Spike (MS)/Matrix Spike Duplicate (MSD): 1. Matrix Spike (MS) was performed on sample 14B7(15-20) (BJ81785). All %RECs were

within the laboratory control limits with the following exception(s):

Compound %R Action Benzoic Acid(1) 13 R(1)

(1) Result was previously qualified due to low LCS recovery. 2. Matrix Spike (MS)/Matrix Spike Duplicate (MSD) were performed on sample 14B5(0-5)

(BJ81800). All %RECs/RPDs were within the laboratory control limits with the following exception(s):

Compound %R/%R/RPD Action

N-Nitrosodimethylamine A/A/46.9 UJ Pyridine A/24/42.6 UJ

Benzoic Acid 21/5/123.1 R(2) Hexachlorocyclopentadiene 0/0/NC R

Phenanthrene A/249/104.6 J Fluoranthene 17/229/96.4 J

Benzidine A/11/42.9 UJ(1) Pyrene A/196/87.2 J

Benz(a)anthracene A/A/41.4 J(1) Chrysene A/A/48.8 J(1)

Benzo(b)fluoranthene A/A/48.6 J(1) Benzo(a)pyrene A/A/37.3 J(1)


(1) Results for these compounds were qualified due to ICV/CCV criteria. (2) Result was previously qualified due to low LCS recovery.

Target Compound Identification: 1. All Relative Retention Times (RRTs) of the reported compounds were within 0.06

RRT units of the standard (opening CCV).

2. Sample compound spectra were compared against the laboratory standard spectra. 3. No QC deviations were observed. Compound Quantitation and Reported Detection Limits: 1. All sample results were reported within the linear calibration range. 2. %Solids for all soil samples in this SDG were >50%. No qualifications were required. 3. Manual Calculation:

Cx = (Ax)(IS)(VE)(DF) (Ais)(RRF)(Volume injected, L)(V)(%Solids)

Cx = concentration of analyte as ug/kg Ax = Area of the characteristic ion for the compound to be measured, counts. Ais = Area of the characteristic ion for the specific internal standard, counts. IS = Concentration of the internal standard spiking mixture, ng RRF= Mean relative response factor from the initial calibration. DF = Dilution factor calculated. If no dilution is performed, DF= 1 V= Volume for liquids in ml, weight for soils/solids in grams. VE= final volume of concentrated extract Sample: BJ81785 LCS

N-Nitrosodimethylamine Sample weight= 15g

Volume purged=1.0ml DF = 1 %Solids=NA Concentration (g/kg) (dry) = 66783 x 40 x 1 x 1000 = 1709.3g/kg

138177 x 0.754 x 15


Compound Laboratory

(g/kg) Validation

(g/kg) %D

N-Nitrosodimethylamine 1709 1709 0.0 Comments: 1. Semivolatile data package meet requirement for New York State Department of

Environmental Conservation (NYSDEC) Analytical Services Protocol (ASP) Category B Deliverables.

2. Validation qualifiers (if required) were entered into the EDD for SDG: GBJ81780. 3. Summary of the qualified data is listed in the Data Summary Table for SDG: GBJ81780.


DATA USABILITY SUMMARY REPORT (DUSR) VOLATILE ORGANIC COMPOUNDS

USEPA Region II –Data Validation Project Name: 510 Driggs Avenue Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBJ81780 Client: Environmental Business Consultants Date: 1/04/2016 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for twenty-three (23) soil samples and two (2)

trip blanks analyzed for Volatiles by SW-846 Method 8260C in accordance to NYSDEC, Analytical Services Protocol (ASP) Format.


Environmental Laboratories, Inc., Manchester, CT on 08/26/2015 for analysis.

3. The USEPA Region-II SOP HW-24, Revision 4, October 2014, Validating Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry, SW-846 Method 8260C was used in evaluating the Volatiles data in this summary report.






Collection Date


14B8(0-5) BJ81780 8/25/15 VOA Soil 14B8(10-15) BJ81781 8/25/15 VOA Soil 14B8(20-25) BJ81782 8/25/15 VOA Soil 14B7(0-5) BJ81783 8/25/15 VOA Soil

14B7(10-15) BJ81784 8/25/15 VOA Soil 14B7(15-20) BJ81785 8/25/15 VOA Soil 14B2(0-5) BJ81786 8/25/15 VOA Soil


14B1(10-15) BJ81790 8/25/15 VOA Soil 14B3(0-5) BJ81791 8/25/15 VOA Soil




14B5(10-15) BJ81801 8/25/15 VOA Soil 14B5(15-19.5) BJ81802 8/25/15 VOA Soil Hi Trip Blank BJ81977 8/25/15 VOA Soil Trip Blank Lo Trip Blank BJ81976 8/25/15 VOA Soil Trip Blank



Holding Times: 1. All soil samples were analyzed within 14 days from sample collection. No qualifications

were required.


GC/MS Tuning: 1. All of the BFB tunes in the initial and continuing calibrations met the percent relative

abundance criteria. No qualifications were required. Initial Calibration:

1. Initial calibration curve analyzed on 08/22/2015 (Chem03) exhibited acceptable %RSDs (20.0%) for CCC compounds and average RRF values for SPCC compounds. Also, %RSDs for all other compounds were 20.0% and average RRF (>0.050) with the following exception(s):

Compound %RSD Chloroethane 27.5

Acetone 29.3


Compound Action

14B8(0-5) BJ81780 Chloroethane Acetone

UJ J

14B8(10-15) BJ81781 Chloroethane, Acetone UJ 14B8(20-25) BJ81782 Chloroethane, Acetone UJ 14B7(0-5) BJ81783 Chloroethane

Acetone UJ J

14B7(10-15) BJ81784 Chloroethane, Acetone UJ 14B7(15-20) BJ81785 Chloroethane, Acetone UJ 14B2(0-5) BJ81786 Chloroethane

Acetone UJ J

14B2(20-25) BJ81788 Chloroethane, Acetone UJ 14B1(0-5) BJ81789 Chloroethane, Acetone UJ

14B1(10-15) BJ81790 Chloroethane Acetone

UJ J

14B8(0-5) D50 BJ81780 Chloroethane, Acetone None 14B7(0-5) D50 BJ81783 Chloroethane, Acetone None 14B2(0-5) D50 BJ81786 Chloroethane, Acetone None 14B2(10-15) BJ81787 Chloroethane, Acetone UJ

14B2(20-25) D50 BJ81788 Chloroethane, Acetone None 14B1(10-15) D50 BJ81790 Chloroethane, Acetone None 14B3(10-15) D50 BJ81792 Chloroethane, Acetone UJ

14B6(10-15) BJ81795 Chloroethane, Acetone UJ 14B4(10-15) BJ81798 Chloroethane, Acetone UJ

14B4(20-21) D714 BJ81799 Chloroethane, Acetone UJ 14B5(0-5) BJ81800 Chloroethane UJ



Compound Action

Acetone J 14B5(15-19.5) D50 BJ81802 Chloroethane, Acetone None

2. Initial calibration curve analyzed on 08/31/2015 (Chem03) exhibited acceptable %RSDs

(20.0%) for CCC compounds and average RRF values for SPCC compounds. Also, %RSDs for all other compounds were 20.0% and average RRF (>0.050) with the following exception(s):

Compound %RSD Methylene Chloride 21.1



Hi Trip Blank BJ81977 Methylene Chloride UJ Lo Trip Blank BJ81976 Methylene Chloride UJ

14B3(0-5) BJ81791 Methylene Chloride UJ 14B3(15-18) D50 BJ81793 Methylene Chloride UJ 14B6(0-5) D50 BJ81794 Methylene Chloride None

14B6(0-5) BJ81794 Methylene Chloride UJ 14B6(10-15) D50 BJ81795 Methylene Chloride None

14B4(0-5) BJ81797 Methylene Chloride UJ 14B4(10-15) D50 BJ81798 Methylene Chloride None

14B4(20-21) D10000

BJ81799 Methylene Chloride None

14B5(0-5) D50 BJ81800 Methylene Chloride None 14B5(10-15) BJ81801 Methylene Chloride UJ

14B5(15-19.5) BJ81802 Methylene Chloride UJ 14B3(10-15) D5000 BJ81792 Methylene Chloride None 14B3(10-15) D500 BJ81792 Methylene Chloride None 14B5(10-15) D50 BJ81801 Methylene Chloride None 14B6(15-17) D50 BJ81796 Methylene Chloride J 14B4(0-5) D50 BJ81797 Methylene Chloride None




Compound %D Trichlorofluoromethane -33.7



14B8(0-5) BJ81780 Trichlorofluoromethane UJ 14B8(10-15) BJ81781 Trichlorofluoromethane UJ 14B8(20-25) BJ81782 Trichlorofluoromethane UJ 14B7(0-5) BJ81783 Trichlorofluoromethane UJ

14B7(10-15) BJ81784 Trichlorofluoromethane UJ 14B7(15-20) BJ81785 Trichlorofluoromethane UJ 14B2(0-5) BJ81786 Trichlorofluoromethane UJ

14B2(20-25) BJ81788 Trichlorofluoromethane UJ 14B1(0-5) BJ81789 Trichlorofluoromethane UJ

14B1(10-15) BJ81790 Trichlorofluoromethane UJ

2. CCV analyzed on 08/29/2015 @ 11:27 (CHEM03) exhibited acceptable %Ds (30.0%) for CCC compounds and RRF values for SPCC compounds. Also, %Ds for all other compounds were 30.0%. No qualifications were required.

3. CCV analyzed on 08/29/2015 @ 20:55 (CHEM03) exhibited acceptable %Ds (0.0%) for CCC compounds and RRF values for SPCC compounds. Also, %Ds for all other compounds were 20.0% with the following exception(s):

Compound %D Dichlorodifluoromethane -44.8

Bromomethane -41.5 Chloroethane -40.5

Trichlorofluoromethane -52.3 1,1-Dichloroethene -25.7 Carbon Disulfide -22.6

Acrolein -20.2 Trans-1,2-Dichloroethene -25.3

Methyl t-Butyl Ether -21.0 2,2-Dichloropropane -28.4 Carbon tetrachloride -32.8 1,1,1-Trichloroethane -27.7 1,1-Dichloropropene -22.2 1,2-Dichloroethane -29.5

Bromodichloromethane -28.6 Tetrachloroethene -21.2

Trans-1,3-Dichloropropene -26.3


Dibromochloromethane -22.0 Bromoform -24.8

Hexachlorobutadiene -20.9 Naphthalene -24.4



14B8(0-5) D50 BJ81780 Dichlorodifluoromethane, Bromomethane, Chloroethane, Trichlorofluoromethane, 1,1-Dichloroethene,

Carbon Disulfide, Acrolein, Trans-1,2-Dichloroethene, Methyl t-Butyl Ether,

2,2-Dichloropropane, Carbon tetrachloride, 1,1,1-Trichloroethane, 1,1-Dichloropropene, 1,2-Dichloroethane, Bromodichloromethane,

Tetrachloroethene, Trans-1,3-Dichloropropene, Dibromochloromethane, Bromoform, Hexachlorobutadiene,

Naphthalene

None





Naphthalene

UJ UJ UJ UJ UJ UJ UJ UJ UJ J





Naphthalene

UJ

14B2(10-15) BJ81787 Dichlorodifluoromethane, Bromomethane, Chloroethane, Trichlorofluoromethane, 1,1-Dichloroethene,



None



Compound Action


Naphthalene 14B2(20-25) D50 BJ81788 Dichlorodifluoromethane, Bromomethane, Chloroethane,

Trichlorofluoromethane, 1,1-Dichloroethene, Carbon Disulfide, Acrolein,

Trans-1,2-Dichloroethene, Methyl t-Butyl Ether, 2,2-Dichloropropane, Carbon tetrachloride, 1,1,1-Trichloroethane, 1,1-Dichloropropene, 1,2-Dichloroethane, Bromodichloromethane,


Naphthalene

None





Naphthalene

None



Compound %D Trichlorofluoromethane -36.6



14B3(10-15) D50 BJ81792 Trichlorofluoromethane UJ 14B6(10-15) BJ81795 Trichlorofluoromethane UJ 14B4(10-15) BJ81798 Trichlorofluoromethane UJ

14B4(20-21) D714 BJ81799 Trichlorofluoromethane UJ 14B5(0-5) BJ81800 Trichlorofluoromethane UJ

14B5(15-19.5) D50 BJ81802 Trichlorofluoromethane None



Compound %D Dichlorodifluoromethane -34.9

Bromomethane -44.9 Chloroethane -41.7

Trichlorofluoromethane -49.7 Carbon Tetrachloride -25.1 1,1,1-Trichloroethane -23.5 1,2-Dichloroethane -24.0

Bromodichloromethane -20.1 Dibromochloromethane -25.2

1,1,1,2-Tetrachloroethane -21.2 Bromoform -32.5

Hexachlorobutadiene -22.9 Tert-butyl alcohol -22.9



14B3(10-15) D50 BJ81792 Dichlorodifluoromethane, Bromomethane, Chloroethane, Trichlorofluoromethane, Carbon Tetrachloride,

1,1,1-Trichloroethane, 1,2-Dichloroethane, Bromodichloromethane, Dibromochloromethane,

1,1,1,2-Tetrachloroethane, Bromoform, Hexachlorobutadiene, Tert-butyl alcohol

UJ

14B6(10-15) BJ81795 Dichlorodifluoromethane, Bromomethane, Chloroethane, Trichlorofluoromethane, Carbon Tetrachloride,



UJ

14B4(10-15) BJ81798 Dichlorodifluoromethane, Bromomethane, Chloroethane, Trichlorofluoromethane, Carbon Tetrachloride,



UJ

14B4(20-21) D714 BJ81799 Dichlorodifluoromethane, Bromomethane, Chloroethane, Trichlorofluoromethane, Carbon Tetrachloride,


1,1,1,2-Tetrachloroethane, Bromoform, Hexachlorobutadiene,

UJ



Compound Action

Tert-butyl alcohol 14B5(0-5) BJ81800 Dichlorodifluoromethane, Bromomethane, Chloroethane,

Trichlorofluoromethane, Carbon Tetrachloride, 1,1,1-Trichloroethane, 1,2-Dichloroethane,

Bromodichloromethane, Dibromochloromethane, 1,1,1,2-Tetrachloroethane, Bromoform, Tert-butyl alcohol

Hexachlorobutadiene

UJ UJ UJ UJ UJ

None 14B5(15-19.5) D50 BJ81802 Dichlorodifluoromethane, Bromomethane, Chloroethane,

Trichlorofluoromethane, Carbon Tetrachloride, 1,1,1-Trichloroethane, 1,2-Dichloroethane,

Bromodichloromethane, Dibromochloromethane, 1,1,1,2-Tetrachloroethane, Bromoform, Hexachlorobutadiene,

Tert-butyl alcohol

UJ


for CCC compounds and RRF values for SPCC compounds. Also, %Ds for all other compounds were 30.0%. No qualifications were required.


Compound %D Dichlorodifluoromethane -28.8 Trichlorofluoromethane -20.5

Methyl Ethyl Ketone -23.1 Dibromochloromethane -20.2

2-Hexanone -31.9 o-Xylene -21.5

Bromoform -23.6 Trans-1,4-Dichloro-2-butene -20.1

1,4-Dioxane -21.9


Compound Action

Hi Trip Blank BJ81977 Dichlorodifluoromethane, Trichlorofluoromethane, Methyl Ethyl Ketone, Dibromochloromethane, 2-Hexanone,

o-Xylene, Bromoform, 1,4-Dioxane Trans-1,4-Dichloro-2-butene,

UJ

Lo Trip Blank BJ81976 Dichlorodifluoromethane, Trichlorofluoromethane, Methyl Ethyl Ketone, Dibromochloromethane, 2-Hexanone,

UJ



Compound Action


14B3(0-5) BJ81791 Dichlorodifluoromethane, Trichlorofluoromethane, Methyl Ethyl Ketone, Dibromochloromethane, 2-Hexanone,


UJ

14B3(15-18) D50 BJ81793 Dichlorodifluoromethane, Trichlorofluoromethane, Methyl Ethyl Ketone, Dibromochloromethane, 2-Hexanone,

Bromoform, 1,4-Dioxane, Trans-1,4-Dichloro-2-butene o-Xylene,

UJ UJ UJ J



None None None

UJ 14B6(0-5) BJ81794 Dichlorodifluoromethane, Trichlorofluoromethane,

Methyl Ethyl Ketone, Dibromochloromethane, 2-Hexanone, o-Xylene, Bromoform, 1,4-Dioxane

Trans-1,4-Dichloro-2-butene

UJ UJ UJ

None 14B6(10-15) D50 BJ81795 Dichlorodifluoromethane, Trichlorofluoromethane,



None

14B4(0-5) BJ81797 Dichlorodifluoromethane, Trichlorofluoromethane, Methyl Ethyl Ketone, Dibromochloromethane, 2-Hexanone,

o-Xylene, Bromoform, 1,4-Dioxane Trans-1,4-Dichloro-2-butene

UJ UJ UJ

None 14B4(10-15) D50 BJ81798 Dichlorodifluoromethane, Trichlorofluoromethane,



None

14B4(20-21) D10000

BJ81799 Dichlorodifluoromethane, Trichlorofluoromethane, Methyl Ethyl Ketone, Dibromochloromethane, 2-Hexanone,


None



None None None

UJ 14B5(10-15) BJ81801 Dichlorodifluoromethane, Trichlorofluoromethane,



UJ UJ UJ

None



Compound Action

14B5(15-19.5) BJ81802 Dichlorodifluoromethane, Trichlorofluoromethane, Methyl Ethyl Ketone, Dibromochloromethane, 2-Hexanone,


UJ



None


Bromoform, 1,4-Dioxane, Trans-1,4-Dichloro-2-butene o-Xylene

None None None

UJ



Surrogates: 1. All surrogates %RECs values for all soil samples with the following exception(s):

Client Sample ID


IS Compound Action

14B5(0-5) BJ81800 1,4-Dichlorobenzene-d4 All detects –J All non-detects - UJ

J/UJ(1)


J/UJ(1)


J/UJ(1)


J/UJ(1)

(1) Only results that were not diluted were qualified Internal Standard (IS) Area Performance: 1. All samples exhibited acceptable area count for all three internal standards within the QC

limits. No qualifications were required.


Method Blank (MB), Storage Blank (SB), Trip Blank (TB), Field Blank (FB), Rinsate Blank (RB) and Equipment Blank (EB): 1. Method Blank (BJ81787 Blank) analyzed on 8/29/2015 was free of contamination. No

qualifications were required. 2. Method Blank (BJ81794 Blank) analyzed on 8/31/2015 was free of contamination. No





qualifications were required. 7. Trip Blank Hi (BJ81977) analyzed on 08/31/2015 was free of contamination. No

qualifications were required. 8. Trip Blank Lo (BJ81976) analyzed on 08/31/2015 was free of contamination. No

qualifications were required. Laboratory Control Sample (LCS)/ Laboratory Control Sample Duplicate (LCSD): 1. Laboratory Control Sample and Laboratory Control Sample Duplicate associated with

BJ81787 LCS were analyzed on 08/29/2015. All %RECs and RPDs were within the laboratory control limits with the following exception(s):


Affected Action

Acetone 60/63/A 14B2(10-15) 14B8(0-5), 14B7(0-5), 14B2(0-5), 14B2(20-25)

14B1(10-15)

UJ(1) None None

Dichlorodifluoromethane 132/A/A 14B2(10-15), 14B8(0-5), 14B7(0-5), 14B2(0-5), 14B2(20-25) 14B1(10-15)

None

Methyl Ethyl Ketone 66/69/A 14B2(10-15) 14B8(0-5), 14B7(0-5), 14B2(0-5), 14B2(20-25)

14B1(10-15)

UJ None None

A= Acceptable


(1) Results for this compound were qualified due to ICV/CCV criteria. 2. Laboratory Control Sample and Laboratory Control Sample Duplicate associated with



Affected Action

Bromomethane A/69/A 14B3(10-15), 14B4(20-21), 14B4(0-5) 14B3(15-18), Hi Trip Blank Lo Trip Blank, 14B3(0-5),

14B6(0-5), 14B5(10-15), 14B5(15-19.5), 14B6(0-5)D, 14B6(10-15)D, 14B4(10-15)D,

14B5(0-5)D, 14B3(10-15)D

UJ(1) UJ UJ

UJ(1) None None

Acetone 68/60A 14B3(10-15), 14B4(20-21), Hi Trip Blank, 14B3(15-18), Lo Trip Blank, 14B3(0-5),

14B4(0-5) 14B6(0-5), 14B5(10-15), 14B5(15-19.5),

14B6(0-5)D, 14B6(10-15)D, 14B4(10-15)D, 14B5(0-5)D, 14B3(10-15)D

UJ(1) UJ UJ

UJ(1) J

None None

Methyl Ethyl Ketone A/66/A 14B3(10-15)D, 14B3(15-18)D, 14B4(20-21)D, Hi Trip Blank

Lo Trip Blank, 14B3(0-5), 14B4(0-5)

14B6(0-5), 14B5(10-15), 14B5(15-19.5), 14B6(0-5)D, 14B6(10-15)D, 14B4(10-15)D,

14B5(0-5)D, 14B3(10-15)D

UJ UJ UJ

UJ(1) UJ(1) None None

A= Acceptable (1) Results for this compound were qualified due to ICV/CCV criteria.

3. Laboratory Control Sample and Laboratory Control Sample Duplicate associated with



Affected Action

Acetone 56/58/A 14B3(10-15)D, 14B6(10-15), 14B4(10-15) 14B4(20-21) 14B5(0-5)

14B5(15-19.5)D

UJ(1) UJ(1) J(1)

None Methyl Ethyl Ketone 59/60/A 14B3(10-15)D, 14B4(20-21), 14B5(0-5)

14B4(10-15), 14B6(10-15), 14B5(15-19.5)D

UJ(1) UJ

None 2-Hexanone A/69/A 14B5(0-5) UJ(1)


Compound %R/%R/RPD Sample Affected

Action

14B4(10-15), 14B6(10-15), 14B3(10-15)D, 14B4(20-21),

14B5(15-19.5)D

UJ UJ

None A= Acceptable

(1) Results for this compound were qualified due to ICV/CCV criteria. 4. Laboratory Control Sample and Laboratory Control Sample Duplicate associated with



Affected Action

Dichlorodifluoromethane A/133/A 14B8(0-5), 14B8(10-15), 14B8(20-25), 14B7(0-5), 14B7(10-15), 14B7(15-20), 14B2(0-5), 14B2(20-25), 14B1(0-5), 14B1(10-15)

None

Bromomethane A/134/A 14B8(0-5), 14B8(10-15), 14B8(20-25), 14B7(0-5), 14B7(10-15), 14B7(15-20), 14B2(0-5), 14B2(20-25), 14B1(0-5), 14B1(10-15)

None

Chloroethane 134/135/A 14B8(0-5), 14B8(10-15), 14B8(20-25), 14B7(0-5), 14B7(10-15), 14B7(15-20), 14B2(0-5), 14B2(20-25), 14B1(0-5), 14B1(10-15)

None

Trichlorofluoromethane 133/137/A 14B8(0-5), 14B8(10-15), 14B8(20-25), 14B7(0-5), 14B7(10-15), 14B7(15-20), 14B2(0-5), 14B2(20-25), 14B1(0-5), 14B1(10-15)

None

Acetone 65/67/A 14B8(0-5), 14B7(0-5), 14B2(0-5) 14B1(10-15)

14B8(10-15), 14B8(20-25), 14B7(10-15) 14B7(15-20), 14B2(20-25), 14B1(0-5)

J(1) J(1)

UJ(1)

UJ(1) Carbon Tetrachloride 130/A/A 14B8(0-5), 14B8(10-15), 14B8(20-25), 14B7(0-5),

14B7(10-15), 14B7(15-20), 14B2(0-5), 14B2(20-25), 14B1(0-5), 14B1(10-15)

None

Bomodichloromethane A/131/A 14B8(0-5), 14B8(10-15), 14B8(20-25), 14B7(0-5), 14B7(10-15), 14B7(15-20), 14B2(0-5), 14B2(20-25), 14B1(0-5), 14B1(10-15)

None

Trans-1,3-Dichloropropene A/133/A 14B8(0-5), 14B8(10-15), 14B8(20-25), 14B7(0-5), 14B7(10-15), 14B7(15-20), 14B2(0-5), 14B2(20-25), 14B1(0-5), 14B1(10-15)

None

A= Acceptable (1) Results for this compound were qualified due to ICV/CCV criteria.


5. Laboratory Control Sample and Laboratory Control Sample Duplicate associated with BJ83508 LCS were analyzed on 09/01/2015. All %RECs and RPDs were within the laboratory control limits. No qualifications were required.




Affected Action

Acetone 69/62/A 14B5(10-15) D None A= Acceptable Field Duplicate: 1. A field duplicate pair was not submitted with this SDG. Matrix Spike (MS)/ Matrix Spike Duplicate (MSD):

1. Matrix Spike (MS)/Matrix Spike Duplicate (MSD) were performed on sample 14B2(10-15) (BJ81787). All %RECs/RPDs were within the laboratory control limits with the following exception(s):


Affected Action

Dichlorodifluoromethane 142/147/A 14B2(10-15) None Bromomethane 154/157/A 14B2(10-15) None Chloroethane 145/150/A 14B2(10-15) None

Trichlorofluoromethane 153/157/A 14B2(10-15) None Carbon Tetrachloride A/135/A 14B2(10-15) None

A= Acceptable

2. Matrix Spike (MS)/Matrix Spike Duplicate (MSD) were performed on sample 14B6(0-5) (BJ81794). All %RECs/RPDs were within the laboratory control limits with the following exception(s):


Affected Action

Bromomethane 42/54/A 14B6(0-5) UJ(1) Chloroethane 31/33/A 14B6(0-5) UJ(1)

Trichlorofluoromethane 21/23/A 14B6(0-5) UJ(1) Acrolein 45/42/A 14B6(0-5) UJ(1)



Action

Acetone 50/51/A 14B6(0-5) J(1) Methyl Ethyl Ketone 62/66/A 14B6(0-5) UJ(1)

1,2,3-Trichlorobenzene 69/A/A 14B6(0-5) UJ A= Acceptable

(1) Results for this compound were qualified due to ICV/CCV criteria.



2. Sample compound spectra were compared against the laboratory standard spectra. 3. No QC deviations were observed. Compound Quantitation and Reported Detection Limits: 1. All sample results were reported within the linear calibration range. No qualifications

were required. 2. %Solids for all soil samples in this SDG were >50%. No qualifications were required. 3. Manual Calculation: Cx = (Ax)(IS)(DF)

(Ais)(RRF)(V)(%Solids)

Cx = concentration of analyte as ug/kg Ax = Area of the characteristic ion for the compound to be measured, counts. Ais = Area of the characteristic ion for the specific internal standard, counts. IS = Concentration of the internal standard spiking mixture, ng RRF= Mean relative response factor from the initial calibration. DF = Dilution factor calculated. If no dilution is performed, DF= 1 V= Volume for liquids in ml, weight for soils/solids in grams.

LCS BJ81787 Dichlorodifluoromethane Sample weight= 5.0g Volume purged=5.0ml DF = 1 %Solids=100%


Concentration (g/kg) (dry) = 86939 x50 x1x 5.0 = 63.716g/kg 182415 x 0.374 x 5.0 x 1

Compound Laboratory

(g/kg) Validation

(g/kg) %D

Dichlorofluoromethane 64 64 0.0 Comments: 1. Volatile data package meet requirement for New York State Department of




DATA USABILITY SUMMARY REPORT (DUSR)

PESTICIDES USEPA Region II –Data Validation

Project Name: 510 Driggs Avenue Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBJ81780 Client: Environmental Business Consultants Date: 01/04/2016 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for fifteen (15) soil sample analyzed for

Pesticides by SW-846 Method 8081B in accordance with NYSDEC, Analytical Services Protocol (ASP) Format.


Environmental Laboratories, Inc., Manchester, CT on 08/26/2015 for analysis. 3. The USEPA Region-II SOP HW-36, Revision 4, May 2013, Validating Pesticide

compounds by Gas Chromatography, SW-846 Method 8081B was used in evaluating the Pesticides data in this summary report.


Selected data points were qualified due to nonconformance of certain Quality Control criteria (See discussion below).




Collection Date


14B8(0-5) BJ81780 8/25/15 Pesticides Soil 14B8(20-25) BJ81782 8/25/15 Pesticides Soil 14B7(0-5) BJ81783 8/25/15 Pesticides Soil

14B7(15-20) BJ81785 8/25/15 Pesticides Soil 14B2(0-5) BJ81786 8/25/15 Pesticides Soil

14B2(20-25) BJ81788 8/25/15 Pesticides Soil 14B1(0-5) BJ81789 8/25/15 Pesticides Soil 14B3(0-5) BJ81791 8/25/15 Pesticides Soil




14B5(15-19.5) BJ81802 8/25/15 Pesticides Soil Sample Conditions/Problems: 1. The Traffic Reports/Chain-of-Custody Records, Sampling Report and/or Laboratory Case



within 40 days following sample extraction. No qualifications were required. GC/ECD Instrument Performance Check: 1. 4,4’-DDT and Endrin breakdown exhibited acceptable results (20%). No qualifications

were required. Initial Calibration:


1. Initial calibration curve analyzed on 08/22/2015 (ECD13) exhibited acceptable %RSD (20%, [25% for alpha-BHC and delta-BHC, 30% for Toxaphene and surrogates]). No qualifications were required.

2. Initial calibration curve analyzed on 08/28/2015 (ECD35) exhibited acceptable %RSD (20%, [25% for alpha-BHC and delta-BHC, 30% for Toxaphene and surrogates]). No qualifications were required.

3. Initial calibration curve analyzed on 08/27/2015 (ECD4) exhibited acceptable %RSD

(20%, [25% for alpha-BHC and delta-BHC, 30% for Toxaphene and surrogates]). No qualifications were required.

Continuing Calibration Verification (CCV): 1. All CCVs analyzed on 8/28-29/2015 exhibited acceptable %Ds (20.0%) for all

compounds. No qualifications were required. 2. All CCVs analyzed on 9/03/2015 exhibited acceptable %Ds (20.0%) for all compounds

with the following exception(s): 9/03/2015 @ 15:35:

Compound Column %D Endosulfan II B 24.0

Note: Results were reported from the A column. No qualifications were required. Surrogates: 1. All surrogate %RECs values for all soil samples were within the laboratory control limits

(30%-150%). Note there were numerous surrogate recoveries that were diluted out or were not reported due to interference. No qualifications were required.

Internal Standard (IS) Area Performance: 1. All samples exhibited acceptable area count for the internal standard. No qualifications

were required. Method Blank (MB), Storage Blank (SB), Trip Blank (TB), Field Blank (FB), Rinsate Blank (RB) and Equipment Blank (EB):


1. Method Blank (BJ81785 BL) associated with the soil samples extracted on 08/26/2015

and analyzed on 08/28/2015 was free of contamination. No qualifications were required. Laboratory Control Sample (LCS)/ Laboratory Control Sample Duplicate (LCSD):

1. Laboratory Control Sample associated with ID: BJ81785 LCS was analyzed on 08/28/2015. All %RECs were within the laboratory control limits. No qualifications were required.

Field Duplicate: 1. A field duplicate pair was not submitted with this SDG. Matrix Spike (MS)/ Matrix Spike Duplicate (MSD): 1. Matrix Spike (MS) was performed on sample 14B7(15-20) (BJ81785). All %RECs were

within the laboratory control limits. No qualifications were required. Compound Quantitation, Compound Identification and Reported Detection Limits: 1. All sample results were reported within the linear calibration range. 2. %Solids for all soil samples in this SDG were >50%. No qualifications were required. 3. Manual Calculation:

BJ81785 LCS

4,4’-DDT

On Column concentration (A) = 38.1946ng Sample Weight= 15.0g DF = 2 Vi= 5ml %Solids= 100% Concentration (g/kg)(dry) = 38.1946ng x 5ml x 2 = 25.46g/kg 15.0g


Compound Laboratory

(g/kg) Validation

(g/kg) %D

4,4’-DDT 25.5 25.5 0.0 Comments: 1. Pesticides data package meet requirement for New York State Department of


2. Validation qualifiers (if required) were entered into the EDD for SDG: GBJ81780. 3. Summary of the qualified data is listed in the Data Summary Table for SDG GBJ81780.



POLYCHLORINATED BIPHENYLIS (PCBs) USEPA Region II –Data Validation

Project Name: 510 Driggs Avenue Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBJ81780 Client: Environmental Business Consultants Date: 1/04/2016 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for fifteen (15) soil samples analyzed for

PCBs by SW-846 Method 8082A in accordance with NYSDEC, Analytical Services Protocol (ASP) Format.


Environmental Laboratories, Inc., Manchester, CT on 08/26/2015 for analysis. 3. The USEPA Region-II SOP HW-37, Revision 3, May 2013, Validating PCBs compounds

by Gas Chromatography, SW-846 Method 8082A was used in evaluating the PCBs data in this summary report.






Collection Date


14B8(0-5) BJ81780 8/25/15 PCBs Soil 14B8(20-25) BJ81782 8/25/15 PCBs Soil 14B7(0-5) BJ81783 8/25/15 PCBs Soil

14B7(15-20) BJ81785 8/25/15 PCBs Soil 14B2(0-5) BJ81786 8/25/15 PCBs Soil

14B2(20-25) BJ81788 8/25/15 PCBs Soil 14B1(0-5) BJ81789 8/25/15 PCBs Soil 14B3(0-5) BJ81791 8/25/15 PCBs Soil




14B5(15-19.5) BJ81802 8/25/15 PCBs Soil Sample Conditions/Problems: 1. The Traffic Reports/Chain-of-Custody Records, Sampling Report and/or Laboratory Case



within 40 days following sample extraction. No qualifications were required. Initial Calibration: 1. Initial calibration curve analyzed on 08/24/2015 (ECD5) exhibited acceptable %RSD

(20.0%) on both columns. No qualifications were required. Continuing Calibration Verification (CCV):


1. All CCVs analyzed on 08/28-29 & 31/2015 exhibited acceptable %D averages (15.0%

for opening and 50% for closing) for all compounds. No qualifications were required. Surrogates: 1. All surrogates %RECs values for all soil samples and associated QC were within the

laboratory control limits (30% - 150%). No qualifications were required. Method Blank (MB), Storage Blank (SB), Trip Blank (TB), Field Blank (FB), Rinsate Blank (RB) and Equipment Blank (EB): 1. Method Blank (BJ81785 BL) associated with the soil samples extracted on 08/26/2015

and analyzed on 08/28/2015 was free of contamination. No qualifications were required. Laboratory Control Sample (LCS)/ Laboratory Control Sample Duplicate (LCSD): 1. Laboratory Control Sample and Laboratory Control Sample Duplicate associated with

ID: BJ81785 were analyzed on 08/28/2015. All %RECs and RPDs were within the laboratory control limits (50% - 150% [30%-150% for surrogates]). No qualifications were required.

Field Duplicate: 1. A field duplicate pair was not submitted with this SDG. Matrix Spike (MS)/ Matrix Spike Duplicate (MSD): 1. Matrix Spike (MS) was performed on sample 14B7(15-20) (BJ81785). All %RECs were

within the laboratory control limits. No qualifications were required. Compound Quantitation, Compound Identification and Reported Detection Limits: 1. All sample results were reported within the linear calibration range. 2. %Solids for all soil samples in this SDG were >50%. No qualifications were required. 3. Manual Calculation:


BJ81785 LCS

Aroclor-1016

On Column concentration (B)= 425.971ng Sample weight= 15.0g DF= 10 Vi= 5ml %Solids= 100% Concentration (g/kg) (dry) = 425.971ng x 5ml x10 = 1420.903g/kg 15.0g

Compound Laboratory

(g/kg) Validation

(g/kg) %D

Aroclor-1016 1420 1420 0.0 Comments: 1. PCBs data package meet requirement for New York State Department of Environmental

Conservation (NYSDEC) Analytical Services Protocol (ASP) Category B Deliverables. 2. Validation qualifiers (if required) were entered into the EDD for SDG: GBJ81780. 3. Summary of the qualified data is listed in the Data Summary Table for SDG: GBJ81780.


DATA USABILITY SUMMARY REPORT (DUSR) TRACE METALS

USEPA Region II –Data Validation Project Name: 510 Driggs Avenue Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBJ81780 Client: Environmental Business Consultants Date: 12/31/2015 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for fifteen (15) soil samples analyzed for the

following analyses:

1.1 Trace Metals-ICP-MS by SW-846 Method 6010C. 1.2 Mercury by SW-846 Method 7471A.


Environmental Laboratories, Inc., Manchester, CT on 8/26/2015 for analysis. 3. The USEPA Region-II SOP No. HW-2a, Revision 15, December 2012, Validation of

ICP-AES was used in evaluating the Trace Metals data and USEPA Region-II SOP No. HW-2c, Revision 15, December 2012, Validation of Mercury and Cyanide was used in evaluating the mercury data in this summary report.






Collection Date


14B8(0-5) BJ81780 8/25/15 ICP and CVAA Soil 14B8(20-25) BJ81782 8/25/15 ICP and CVAA Soil 14B7(0-5) BJ81783 8/25/15 ICP and CVAA Soil

14B7(15-20) BJ81785 8/25/15 ICP and CVAA Soil 14B2(0-5) BJ81786 8/25/15 ICP and CVAA Soil

14B2(20-25) BJ81788 8/25/15 ICP and CVAA Soil 14B1(0-5) BJ81789 8/25/15 ICP and CVAA Soil 14B3(0-5) BJ81791 8/25/15 ICP and CVAA Soil




14B5(15-19.5) BJ81802 8/25/15 ICP and CVAA Soil Sample Conditions/Problems: 1. The Traffic Reports/Chain-of-Custody Records, Sampling Report and/or Laboratory Case


Holding Times: 1. All soil samples were analyzed within the 6 months holding times for Trace Metals

analysis by ICP-AES. No qualifications were required. 2. All soil samples were digested and analyzed within the 28 days holding times for

Mercury analysis. No qualifications were required.


Initial and Continuing Calibration Verification (ICV and CCV): ICP-AES: 1. All %RECs in the ICV and CCVs were within QC limits (90-110) with the following

exception(s): Analyte Date

Analyzed %R Sample Affected Action

Potassium 8/28/15: 2:46 110.8 14B8(0-5), 14B8(20-25), 14B7(0-5), 14B2(0-5), J+ 8/28/15: 4:13 111.3 14B2(20-25), 14B1(0-5), 14B3(0-5),

14B3(15-18), 14B6(0-5)

Mercury: 1 All correlation coefficient for Mercury calibration curve analyzed were 0.995. No

qualifications were required. 2. All ICVs and CCVs %REC values were within the QC limits (85-115%). No

qualifications were required. CRQL Check Standard (CRI): 1. All CRI analyzed %RECs were within the control limits (70-130%) with the following

exception(s): Analyte Date


Zinc 8/28/15: 03:36 64.0 14B7(15-20), 14B8(0-5), 14B8(20-25), 14B7(0-5), 14B2(0-5), 14B2(20-25), 14B1(0-5), 14B3(0-5), 14B3(15-18), 14B6(0-5), 14B4(0-5),

14B5(0-5), 14B5(15-19.5)

J+

ICP-AES Interference Check Sample: 1. All %REC values were within the QC limits (80-120%) for ICSA and ICSAB with the



Analyte Date


Potassium 8/27/15: 11:51 125.7 14B8(0-5), 14B8(20-25), 14B7(0-5), 14B7(15-20), J+ 8/28/15: 1:45 127.8 14B2(0-5), 14B2(20-25), 14B1(0-5), 14B3(0-5), 8/28/15: 3:40 133.2 14B3(15-18), 14B6(0-5), 14B6(15-17), 14B4(0-5),

14B4(20-21), 14B5(0-5), 14B5(15-19.5)

Blanks (Method Blank, ICB and CCB): ICP-AES: 1. Method Blank-Soil (BJ81785) digested on 08/26/2015.

Element Concentration (mg/Kg)

CRQL* (mg/Kg)

Sample Affected Action

Iron 16.3 5.0 14B8(0-5), 14B8(20-25), 14B7(0-5), 14B7(15-20), 14B2(0-5), 14B2(20-25), 14B1(0-5), 14B3(0-5),

14B3(15-18), 14B6(0-5), 14B6(15-17), 14B4(0-5), 14B4(20-21), 14B5(0-5), 14B5(15-19.5)

None

Zinc 2.26 0.33 14B8(0-5), 14B8(20-25), 14B7(0-5), 14B7(15-20), 14B2(0-5), 14B2(20-25), 14B1(0-5), 14B3(0-5),

14B3(15-18), 14B6(0-5), 14B6(15-17), 14B4(0-5), 14B4(20-21), 14B5(0-5), 14B5(15-19.5)

None

*= If sample concentration >MDL but < Reporting limit, then sample result qualified as non-detect (U). If sample concentration greater than CRQL but less than10x the blank result, then qualify estimated (J). If sample concentration greater than 10x the blank results or sample was not detected then no qualifications or action is required.

2. All ICB and CCBs were free of contamination. No qualifications were required. Mercury: 1. All ICB and CCBs were free of contamination. No qualifications were required. 2. Method Blank (BJ81791) digested on 08/27/2015 was free of contamination. No

qualifications were required. Field Blank (FB) and Equipment Blank (EB): 1. Field Blanks were not submitted with this SDG.


Laboratory Control Sample (LCS)/ Laboratory Control Sample Duplicate (LCSD): ICP-AES and Mercury: 1. Laboratory Control Sample %RECs were within the laboratory control limits (70% -

130% for Metals, 75%-125% for Hg). No qualifications were required. Field Duplicate: 1. A field duplicate pair was not submitted with this SDG. Matrix Spike (MS)/ Matrix Spike Duplicate (MSD): ICP-AES and Mercury: 1. Matrix Spike (MS) was performed on sample 14B3(0-5) (BJ81791). All %RECs were

within the laboratory control limits for mercury. No qualifications were required. 2. Matrix Spike (MS) was performed on sample 14B7(15-20) (BJ81785). All %RECs were

within the laboratory control limits with the following exception(s):

Compound %R/Post %R Action Potassium 269/134 J+ Sodium 173/144 J+

Antimony 67.9/A UJ A=Acceptable

Sample Duplicate: ICP-AES and Mercury:

1. Sample Duplicate was performed on sample 14B3(0-5) (BJ81791). All RPDs were within the laboratory control limits for mercury. No qualifications were required.

2. Sample Duplicate was performed on sample 14B7(15-20) (BJ81785). All RPDs were

within the laboratory control limits for mercury. No qualifications were required.


ICP-AES Serial Dilution: 1. ICP serial dilution was performed on sample 14B7(15-20) (BJ81785). For all results for

which the concentration in the original sample is ≥ 50x the Method Detection Limits (MDL), the serial dilution analysis (a five-fold dilution) was within the acceptable limit (%D 10%). No qualifications were required.

Verification of Instrumental Parameters: 1. The following Forms were present in the data package:

1.1 Method Detection Limits, Form- X. 1.2 ICP-AES Interelement Correction Factors, Form -XIA and Form-XIB. 1.3 ICP-AES Linear Ranges, Form XII.

Compound Quantitation and Reported Detection Limits: 1. All sample results were reported within the linear calibration range. 2. %Solids for all soil samples in this SDG were >50%. No qualifications were required. 3. Manual calculation: Sample: 14B8(0-5) (BJ81780) Barium Concentration (mg/Kg) (dry wt.)= C x V x DF x 1Lx 1000gx 1mg W x S x 1000ml x 1 kg x 1000ug

V= 50ml W= 0.81g %Solids =90.0 DF=1.0 Concentration (mg/Kg) (dry wt.)= 855.4086ug/L x 50 x 1.0 x 1Lx 1000gx 1mg = 58.67 mg/kg 0.81 x 0.90 x 1000ml x 1 kg x 1000ug

Compound Laboratory

(mg/kg) Validation

(mg/kg) %D

Barium 58.0 58.0 0.0


Comments: 1. Trace Metals data package meet requirement for New York State Department of



510 DRIGGS AVENUEBROOKLYN, NY

DATA SUMMARY TABLESOIL

SDG: GBJ81780

Sample Name Lab IDAnalytical

Method Analysis DateDilution Factor Analyte Result Unit Qualifier MDL RL

14B8 (0-5) BJ81780 SW6010 8/28/15 1 Potassium 1160 mg/kg J+ 2.7 714B8 (0-5) BJ81780 SW8260 8/29/15 1 Acetone 19 ug/kg J 5.3 5014B8 (0-5) BJ81780 SW8260 8/29/15 1 Methylene Chloride ug/kg U 5.3 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Bromodichloromethane ug/kg U 1.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Bromomethane ug/kg U 2.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Carbon Tetrachloride ug/kg U 1.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Chloroethane ug/kg UJ 0.53 5.314B8 (0-5) BJ81780 SW6010 8/28/15 10 Iron 15100 mg/kg 34 3414B8 (0-5) BJ81780 SW8260 8/29/15 1 Methyl Ethyl Ketone (2-Butanone) ug/kg U 5.3 3214B8 (0-5) BJ81780 SW8270 8/27/15 1 Bis(2-Ethylhexyl) Phthalate ug/kg UJ 100 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Di-N-Octylphthalate ug/kg UJ 94 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Benzo(G,H,I)Perylene 620 ug/kg J 120 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Indeno(1,2,3-C,D)Pyrene 680 ug/kg J 120 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Benzo(B)Fluoranthene 820 ug/kg J 120 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Benzo(K)Fluoranthene 980 ug/kg J 120 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Chrysene 1100 ug/kg J 120 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Benzo(A)Pyrene 970 ug/kg J 120 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Dibenz(A,H)Anthracene 200 ug/kg J 120 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Benzo(A)Anthracene 1100 ug/kg J 120 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Benzyl Butyl Phthalate ug/kg UJ 94 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 3,3'-Dichlorobenzidine ug/kg UJ 170 73014B8 (0-5) BJ81780 SW8260 8/29/15 1 Dichlorodifluoromethane ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Trans-1,3-Dichloropropene ug/kg U 0.53 5.314B8 (0-5) BJ81780 E160.3 8/26/15 1 Solids, Percent 90 %14B8 (0-5) BJ81780 SW6010 8/28/15 10 Aluminum 8600 mg/kg 6.9 3414B8 (0-5) BJ81780 SW6010 8/28/15 10 Manganese 337 mg/kg 3.4 3.414B8 (0-5) BJ81780 SW6010 8/28/15 1 Lead 38.9 mg/kg 0.34 0.714B8 (0-5) BJ81780 SW6010 8/28/15 1 Magnesium 3670 mg/kg 3.4 3.414B8 (0-5) BJ81780 SW6010 8/28/15 1 Nickel 13.9 mg/kg 0.34 0.3414B8 (0-5) BJ81780 SW6010 8/28/15 1 Silver mg/kg U 0.34 0.3414B8 (0-5) BJ81780 SW6010 8/28/15 1 Sodium 134 mg/kg 2.9 714B8 (0-5) BJ81780 SW6010 8/28/15 1 Thallium mg/kg U 1.4 1.414B8 (0-5) BJ81780 SW6010 8/28/15 1 Antimony mg/kg U 1.7 1.714B8 (0-5) BJ81780 SW6010 8/28/15 1 Arsenic 2.3 mg/kg 0.69 0.714B8 (0-5) BJ81780 SW6010 8/28/15 1 Barium 58.0 mg/kg 0.34 0.714B8 (0-5) BJ81780 SW6010 8/28/15 1 Beryllium 0.39 mg/kg 0.14 0.2714B8 (0-5) BJ81780 SW6010 8/28/15 1 Cadmium mg/kg U 0.14 0.3414B8 (0-5) BJ81780 SW6010 8/28/15 1 Chromium, Total 16.3 mg/kg 0.34 0.34

Page 1 of 82



SDG: GBJ81780



14B8 (0-5) BJ81780 SW6010 8/28/15 1 Cobalt 6.26 mg/kg 0.34 0.3414B8 (0-5) BJ81780 SW6010 8/28/15 1 Copper 16.5 mg/kg 0.34 0.3414B8 (0-5) BJ81780 SW6010 8/28/15 1 Vanadium 27.6 mg/kg 0.34 0.314B8 (0-5) BJ81780 SW6010 8/28/15 1 Calcium 6250 mg/kg 3.2 3.414B8 (0-5) BJ81780 SW6010 8/28/15 1 Selenium mg/kg U 1.2 1.414B8 (0-5) BJ81780 SW7471 8/27/15 1 Mercury 0.14 mg/kg 0.02 0.0314B8 (0-5) BJ81780 SW8081 8/28/15 10 Heptachlor Epoxide ug/kg U 37 3714B8 (0-5) BJ81780 SW8081 8/28/15 10 Endosulfan Sulfate ug/kg U 37 3714B8 (0-5) BJ81780 SW8081 8/28/15 10 Aldrin ug/kg U 5.5 5.514B8 (0-5) BJ81780 SW8081 8/28/15 10 Alpha Bhc (Alpha Hexachlorocyclohexane) ug/kg U 18 1814B8 (0-5) BJ81780 SW8081 8/28/15 10 Beta Bhc (Beta Hexachlorocyclohexane) ug/kg U 18 1814B8 (0-5) BJ81780 SW8081 8/28/15 10 Delta BHC (Delta Hexachlorocyclohexane) ug/kg U 37 3714B8 (0-5) BJ81780 SW8081 8/28/15 10 Beta Endosulfan ug/kg U 37 3714B8 (0-5) BJ81780 SW8081 8/28/15 10 P,P'-DDT ug/kg U 9.2 9.214B8 (0-5) BJ81780 SW8081 8/28/15 10 cis-Chlordane 50 ug/kg 18 1814B8 (0-5) BJ81780 SW8081 8/28/15 10 trans-Chlordane 39 ug/kg 18 1814B8 (0-5) BJ81780 SW8081 8/28/15 10 Endrin Ketone ug/kg U 37 3714B8 (0-5) BJ81780 SW8081 8/28/15 10 Gamma Bhc (Lindane) ug/kg U 7.3 7.314B8 (0-5) BJ81780 SW8081 8/28/15 10 Dieldrin ug/kg U 5.5 5.514B8 (0-5) BJ81780 SW8081 8/28/15 10 Endrin ug/kg U 18 1814B8 (0-5) BJ81780 SW8081 8/28/15 10 Methoxychlor ug/kg U 180 18014B8 (0-5) BJ81780 SW8081 8/28/15 10 P,P'-DDD ug/kg U 15 1514B8 (0-5) BJ81780 SW8081 8/28/15 10 P,P'-DDE ug/kg U 9.2 9.214B8 (0-5) BJ81780 SW8081 8/28/15 10 Endrin Aldehyde ug/kg U 37 3714B8 (0-5) BJ81780 SW8081 8/28/15 10 Heptachlor ug/kg U 37 3714B8 (0-5) BJ81780 SW8081 8/28/15 10 Toxaphene ug/kg U 730 73014B8 (0-5) BJ81780 SW8081 8/28/15 10 Alpha Endosulfan ug/kg U 37 3714B8 (0-5) BJ81780 SW8082 8/29/15 2 PCB-1260 (Aroclor 1260) ug/kg U 37 3714B8 (0-5) BJ81780 SW8082 8/29/15 2 PCB-1254 (Aroclor 1254) ug/kg U 37 3714B8 (0-5) BJ81780 SW8082 8/29/15 2 PCB-1268 (Aroclor 1268) ug/kg U 37 3714B8 (0-5) BJ81780 SW8082 8/29/15 2 PCB-1221 (Aroclor 1221) ug/kg U 37 3714B8 (0-5) BJ81780 SW8082 8/29/15 2 PCB-1232 (Aroclor 1232) ug/kg U 37 3714B8 (0-5) BJ81780 SW8082 8/29/15 2 PCB-1248 (Aroclor 1248) ug/kg U 37 3714B8 (0-5) BJ81780 SW8082 8/29/15 2 PCB-1016 (Aroclor 1016) ug/kg U 37 3714B8 (0-5) BJ81780 SW8082 8/29/15 2 PCB-1262 (Aroclor 1262) ug/kg U 37 3714B8 (0-5) BJ81780 SW8082 8/29/15 2 PCB-1242 (Aroclor 1242) ug/kg U 37 3714B8 (0-5) BJ81780 SW8260 8/29/15 1 Ethylbenzene ug/kg U 0.53 5.3

Page 2 of 82



SDG: GBJ81780



14B8 (0-5) BJ81780 SW8260 8/29/15 1 Styrene ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Cis-1,3-Dichloropropene ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 N-Propylbenzene ug/kg U 0.95 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 N-Butylbenzene ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 4-Chlorotoluene ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 1,4-Dichlorobenzene ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 1,2-Dibromoethane (Ethylene Dibromide) ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Acrolein ug/kg U 2.6 2114B8 (0-5) BJ81780 SW8260 8/29/15 1 1,2-Dichloroethane ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Acrylonitrile ug/kg U 0.53 2114B8 (0-5) BJ81780 SW8260 8/29/15 1 Methyl Isobutyl Ketone (4-Methyl-2-Pentanone) ug/kg U 5.3 2614B8 (0-5) BJ81780 SW8260 8/29/15 1 1,3,5-Trimethylbenzene (Mesitylene) ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Bromobenzene ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Toluene 2.1 ug/kg J 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Chlorobenzene ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Tetrahydrofuran ug/kg U 2.6 1114B8 (0-5) BJ81780 SW8260 8/29/15 1 Trans-1,4-Dichloro-2-Butene ug/kg U 2.6 1114B8 (0-5) BJ81780 SW8260 8/29/15 1 1,2,4-Trichlorobenzene ug/kg U 1.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 1,4-Dioxane (P-Dioxane) ug/kg U 42 10014B8 (0-5) BJ81780 SW8260 8/29/15 1 Dibromochloromethane ug/kg U 1.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Tetrachloroethylene (PCE) ug/kg U 1.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Sec-Butylbenzene ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 1,3-Dichloropropane ug/kg U 1.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Trans-1,2-Dichloroethene 0.84 ug/kg J 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Tert-Butyl Methyl Ether ug/kg U 1.1 1114B8 (0-5) BJ81780 SW8260 8/29/15 1 m,p-Xylene 1.1 ug/kg J 1.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 O-Cymene (O-Isopropyltoluene) ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 1,3-Dichlorobenzene ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 1,1-Dichloropropene ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 2-Hexanone ug/kg U 5.3 2614B8 (0-5) BJ81780 SW8260 8/29/15 1 2,2-Dichloropropane ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 1,1,1,2-Tetrachloroethane ug/kg U 1.1 2114B8 (0-5) BJ81780 SW8260 8/29/15 1 Chloroform ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Benzene 0.69 ug/kg J 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 1,1,1-Trichloroethane ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Chloromethane ug/kg U 1.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Dibromomethane ug/kg U 1.1 5.3

Page 3 of 82



SDG: GBJ81780



14B8 (0-5) BJ81780 SW8260 8/29/15 1 Bromochloromethane ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Vinyl Chloride 0.58 ug/kg J 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Carbon Disulfide 2.4 ug/kg J 1.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Bromoform ug/kg U 1.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 1,1-Dichloroethane ug/kg U 1.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 1,1-Dichloroethene ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Tert-Butyl Alcohol ug/kg U 21 11014B8 (0-5) BJ81780 SW8260 8/29/15 1 1,1,2-Trichloro-1,2,2-Trifluoroethane ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 1,2-Dichloropropane ug/kg U 1.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 1,1,2-Trichloroethane ug/kg U 1.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 1,1,2,2-Tetrachloroethane ug/kg U 1.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 1,2,3-Trichlorobenzene ug/kg U 1.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Hexachlorobutadiene ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Naphthalene 2.6 ug/kg J 1.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 O-Xylene (1,2-Dimethylbenzene) ug/kg U 1.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 2-Chlorotoluene ug/kg U 1.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 1,2-Dichlorobenzene ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 1,2,4-Trimethylbenzene 1.0 ug/kg J 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 1,2-Dibromo-3-Chloropropane ug/kg U 1.1 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 1,2,3-Trichloropropane ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 T-Butylbenzene ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Isopropylbenzene (Cumene) ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 1 Cymene ug/kg U 0.53 5.314B8 (0-5) BJ81780 SW8260 8/29/15 50 Cis-1,2-Dichloroethylene 170 ug/kg J 26 25014B8 (0-5) BJ81780 SW8260 8/29/15 50 Trichloroethylene (TCE) 250 ug/kg J 26 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 4-Nitroaniline ug/kg U 120 73014B8 (0-5) BJ81780 SW8270 8/27/15 1 4-Nitrophenol ug/kg U 160 36014B8 (0-5) BJ81780 SW8270 8/27/15 1 4-Bromophenyl Phenyl Ether ug/kg U 110 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 2,4-Dimethylphenol ug/kg U 90 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 1,4-Dichlorobenzene ug/kg U 110 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 4-Chloroaniline ug/kg U 170 29014B8 (0-5) BJ81780 SW8270 8/27/15 1 Phenol ug/kg U 120 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Pyridine ug/kg U 90 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Bis(2-Chloroethyl) Ether (2-Chloroethyl Ether) ug/kg U 98 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Bis(2-Chloroethoxy) Methane ug/kg U 100 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Hexachlorobenzene ug/kg U 110 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Anthracene 200 ug/kg J 120 260

Page 4 of 82



SDG: GBJ81780



14B8 (0-5) BJ81780 SW8270 8/27/15 1 1,2,4-Trichlorobenzene ug/kg U 110 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 2,4-Dichlorophenol ug/kg U 130 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 2,4-Dinitrotoluene ug/kg U 140 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 1,2-Diphenylhydrazine ug/kg U 120 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Pyrene 1500 ug/kg 130 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Dimethyl Phthalate ug/kg U 110 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Dibenzofuran ug/kg U 110 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Fluoranthene 1800 ug/kg 120 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Acenaphthylene 130 ug/kg J 100 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 2,2-Oxybis(2-Chloropropane) ug/kg U 100 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 2,4-Dinitrophenol ug/kg UJ 260 73014B8 (0-5) BJ81780 SW8270 8/27/15 1 4,6-Dinitro-2-Methylphenol ug/kg UJ 390 180014B8 (0-5) BJ81780 SW8270 8/27/15 1 1,3-Dichlorobenzene ug/kg U 110 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 4-Chloro-3-Methylphenol ug/kg U 130 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 2,6-Dinitrotoluene ug/kg U 120 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 N-Nitrosodi-N-Propylamine ug/kg U 120 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Aniline ug/kg U 290 29014B8 (0-5) BJ81780 SW8270 8/27/15 1 N-Nitrosodimethylamine ug/kg U 100 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Benzoic Acid ug/kg R 730 180014B8 (0-5) BJ81780 SW8270 8/27/15 1 Hexachloroethane ug/kg U 110 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 4-Chlorophenyl Phenyl Ether ug/kg U 120 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Hexachlorocyclopentadiene ug/kg UJ 110 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Isophorone ug/kg U 100 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Pentachloronitrobenzene ug/kg U 140 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Acenaphthene ug/kg U 110 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Diethyl Phthalate ug/kg U 120 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Di-N-Butyl Phthalate ug/kg U 97 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Phenanthrene 730 ug/kg 100 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 N-Nitrosodiphenylamine ug/kg U 140 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Fluorene ug/kg U 120 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Carbazole ug/kg U 280 180014B8 (0-5) BJ81780 SW8270 8/27/15 1 Hexachlorobutadiene ug/kg U 130 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Pentachlorophenol ug/kg UJ 140 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 2,4,6-Trichlorophenol ug/kg U 120 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 2-Nitroaniline ug/kg U 370 73014B8 (0-5) BJ81780 SW8270 8/27/15 1 2-Nitrophenol ug/kg U 230 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Naphthalene ug/kg U 100 260

Page 5 of 82



SDG: GBJ81780



14B8 (0-5) BJ81780 SW8270 8/27/15 1 2-Methylnaphthalene ug/kg U 110 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 2-Chloronaphthalene ug/kg U 100 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Benzidine ug/kg U 210 73014B8 (0-5) BJ81780 SW8270 8/27/15 1 2-Methylphenol (O-Cresol) ug/kg U 170 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 1,2-Dichlorobenzene ug/kg U 100 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 2-Chlorophenol ug/kg U 100 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 1,2,4,5-Tetrachlorobenzene ug/kg U 130 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 2,4,5-Trichlorophenol ug/kg U 200 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Acetophenone ug/kg U 110 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 Nitrobenzene ug/kg U 130 26014B8 (0-5) BJ81780 SW8270 8/27/15 1 3-Nitroaniline ug/kg U 730 73014B8 (0-5) BJ81780 SW8270 8/27/15 1 3- And 4- Methylphenol (Total) ug/kg U 140 26014B8 (0-5) BJ81780 SW8260 8/29/15 1 Trichlorofluoromethane ug/kg UJ 1.1 5.314B8 (0-5) BJ81780 SW6010 8/28/15 1 Zinc 44.8 mg/kg J+ 0.34 0.714B8 (20-25) BJ81782 SW8260 8/29/15 1 Acetone ug/kg UJ 6.2 5014B8 (20-25) BJ81782 SW8270 8/27/15 1 Benzidine ug/kg UJ 250 84014B8 (20-25) BJ81782 SW8260 8/29/15 1 Bromodichloromethane ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW6010 8/28/15 1 Potassium 3690 mg/kg J+ 3.2 814B8 (20-25) BJ81782 SW8260 8/29/15 1 Methylene Chloride ug/kg U 6.2 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Bromomethane ug/kg U 2.5 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Carbon Tetrachloride ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW6010 8/28/15 10 Iron 27100 mg/kg 41 4114B8 (20-25) BJ81782 SW8260 8/29/15 1 Chloroethane ug/kg UJ 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Dichlorodifluoromethane ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Trans-1,3-Dichloropropene ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Trichlorofluoromethane ug/kg UJ 1.2 6.214B8 (20-25) BJ81782 E160.3 8/26/15 1 Solids, Percent 77 %14B8 (20-25) BJ81782 SW6010 8/28/15 10 Aluminum 12800 mg/kg 8.2 4114B8 (20-25) BJ81782 SW6010 8/28/15 10 Manganese 589 mg/kg 4.1 4.114B8 (20-25) BJ81782 SW6010 8/28/15 1 Lead 8.3 mg/kg 0.41 0.814B8 (20-25) BJ81782 SW6010 8/28/15 1 Magnesium 5160 mg/kg 4.1 4.114B8 (20-25) BJ81782 SW6010 8/28/15 1 Nickel 21.6 mg/kg 0.41 0.4114B8 (20-25) BJ81782 SW6010 8/28/15 1 Silver mg/kg U 0.41 0.4114B8 (20-25) BJ81782 SW6010 8/28/15 1 Sodium 249 mg/kg 3.5 814B8 (20-25) BJ81782 SW6010 8/28/15 1 Thallium mg/kg U 1.6 1.614B8 (20-25) BJ81782 SW6010 8/28/15 1 Antimony mg/kg U 2.1 2.114B8 (20-25) BJ81782 SW6010 8/28/15 1 Arsenic 1.9 mg/kg 0.82 0.8

Page 6 of 82



SDG: GBJ81780



14B8 (20-25) BJ81782 SW6010 8/28/15 1 Barium 80.0 mg/kg 0.41 0.814B8 (20-25) BJ81782 SW6010 8/28/15 1 Beryllium 0.69 mg/kg 0.16 0.3314B8 (20-25) BJ81782 SW6010 8/28/15 1 Cadmium mg/kg U 0.16 0.4114B8 (20-25) BJ81782 SW6010 8/28/15 1 Chromium, Total 29.9 mg/kg 0.41 0.4114B8 (20-25) BJ81782 SW6010 8/28/15 1 Cobalt 12.5 mg/kg 0.41 0.4114B8 (20-25) BJ81782 SW6010 8/28/15 1 Copper 22.4 mg/kg 0.41 0.4114B8 (20-25) BJ81782 SW6010 8/28/15 1 Vanadium 37.8 mg/kg 0.41 0.414B8 (20-25) BJ81782 SW6010 8/28/15 1 Zinc 49.8 mg/kg J+ 0.41 0.814B8 (20-25) BJ81782 SW6010 8/28/15 1 Calcium 2370 mg/kg 3.8 4.114B8 (20-25) BJ81782 SW6010 8/28/15 1 Selenium mg/kg U 1.4 1.614B8 (20-25) BJ81782 SW7471 8/27/15 1 Mercury mg/kg U 0.02 0.0314B8 (20-25) BJ81782 SW8081 8/28/15 2 Heptachlor Epoxide ug/kg U 8.6 8.614B8 (20-25) BJ81782 SW8081 8/28/15 2 Endosulfan Sulfate ug/kg U 8.6 8.614B8 (20-25) BJ81782 SW8081 8/28/15 2 Aldrin ug/kg U 4.3 4.314B8 (20-25) BJ81782 SW8081 8/28/15 2 Alpha Bhc (Alpha Hexachlorocyclohexane) ug/kg U 8.6 8.614B8 (20-25) BJ81782 SW8081 8/28/15 2 Beta Bhc (Beta Hexachlorocyclohexane) ug/kg U 8.6 8.614B8 (20-25) BJ81782 SW8081 8/28/15 2 Delta BHC (Delta Hexachlorocyclohexane) ug/kg U 8.6 8.614B8 (20-25) BJ81782 SW8081 8/28/15 2 Beta Endosulfan ug/kg U 8.6 8.614B8 (20-25) BJ81782 SW8081 8/28/15 2 P,P'-DDT ug/kg U 2.6 2.614B8 (20-25) BJ81782 SW8081 8/28/15 2 cis-Chlordane ug/kg U 4.3 4.314B8 (20-25) BJ81782 SW8081 8/28/15 2 trans-Chlordane ug/kg U 4.3 4.314B8 (20-25) BJ81782 SW8081 8/28/15 2 Endrin Ketone ug/kg U 8.6 8.614B8 (20-25) BJ81782 SW8081 8/28/15 2 Gamma Bhc (Lindane) ug/kg U 1.7 1.714B8 (20-25) BJ81782 SW8081 8/28/15 2 Dieldrin ug/kg U 4.3 4.314B8 (20-25) BJ81782 SW8081 8/28/15 2 Endrin ug/kg U 8.6 8.614B8 (20-25) BJ81782 SW8081 8/28/15 2 Methoxychlor ug/kg U 43 4314B8 (20-25) BJ81782 SW8081 8/28/15 2 P,P'-DDD ug/kg U 2.6 2.614B8 (20-25) BJ81782 SW8081 8/28/15 2 P,P'-DDE ug/kg U 2.6 2.614B8 (20-25) BJ81782 SW8081 8/28/15 2 Endrin Aldehyde ug/kg U 8.6 8.614B8 (20-25) BJ81782 SW8081 8/28/15 2 Heptachlor ug/kg U 8.6 8.614B8 (20-25) BJ81782 SW8081 8/28/15 2 Toxaphene ug/kg U 170 17014B8 (20-25) BJ81782 SW8081 8/28/15 2 Alpha Endosulfan ug/kg U 8.6 8.614B8 (20-25) BJ81782 SW8082 8/29/15 2 PCB-1260 (Aroclor 1260) ug/kg U 43 4314B8 (20-25) BJ81782 SW8082 8/29/15 2 PCB-1254 (Aroclor 1254) ug/kg U 43 4314B8 (20-25) BJ81782 SW8082 8/29/15 2 PCB-1268 (Aroclor 1268) ug/kg U 43 4314B8 (20-25) BJ81782 SW8082 8/29/15 2 PCB-1221 (Aroclor 1221) ug/kg U 43 4314B8 (20-25) BJ81782 SW8082 8/29/15 2 PCB-1232 (Aroclor 1232) ug/kg U 43 43

Page 7 of 82



SDG: GBJ81780



14B8 (20-25) BJ81782 SW8082 8/29/15 2 PCB-1248 (Aroclor 1248) ug/kg U 43 4314B8 (20-25) BJ81782 SW8082 8/29/15 2 PCB-1016 (Aroclor 1016) ug/kg U 43 4314B8 (20-25) BJ81782 SW8082 8/29/15 2 PCB-1262 (Aroclor 1262) ug/kg U 43 4314B8 (20-25) BJ81782 SW8082 8/29/15 2 PCB-1242 (Aroclor 1242) ug/kg U 43 4314B8 (20-25) BJ81782 SW8260 8/29/15 1 Ethylbenzene ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Styrene ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Cis-1,3-Dichloropropene ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 N-Propylbenzene ug/kg U 1.1 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 N-Butylbenzene ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 4-Chlorotoluene ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 1,4-Dichlorobenzene ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 1,2-Dibromoethane (Ethylene Dibromide) ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Acrolein ug/kg U 3.1 2514B8 (20-25) BJ81782 SW8260 8/29/15 1 1,2-Dichloroethane ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Acrylonitrile ug/kg U 0.62 2514B8 (20-25) BJ81782 SW8260 8/29/15 1 Methyl Isobutyl Ketone (4-Methyl-2-Pentanone) ug/kg U 6.2 3114B8 (20-25) BJ81782 SW8260 8/29/15 1 1,3,5-Trimethylbenzene (Mesitylene) ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Bromobenzene ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Toluene ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Chlorobenzene ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Tetrahydrofuran ug/kg U 3.1 1214B8 (20-25) BJ81782 SW8260 8/29/15 1 Trans-1,4-Dichloro-2-Butene ug/kg U 3.1 1214B8 (20-25) BJ81782 SW8260 8/29/15 1 1,2,4-Trichlorobenzene ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 1,4-Dioxane (P-Dioxane) ug/kg U 49 10014B8 (20-25) BJ81782 SW8260 8/29/15 1 Dibromochloromethane ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Tetrachloroethylene (PCE) ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Sec-Butylbenzene ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 1,3-Dichloropropane ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Cis-1,2-Dichloroethylene 16 ug/kg 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Trans-1,2-Dichloroethene 0.97 ug/kg J 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Tert-Butyl Methyl Ether ug/kg U 1.2 1214B8 (20-25) BJ81782 SW8260 8/29/15 1 m,p-Xylene ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 O-Cymene (O-Isopropyltoluene) ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 1,3-Dichlorobenzene ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 1,1-Dichloropropene ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 2-Hexanone ug/kg U 6.2 3114B8 (20-25) BJ81782 SW8260 8/29/15 1 2,2-Dichloropropane ug/kg U 0.62 6.2

Page 8 of 82



SDG: GBJ81780



14B8 (20-25) BJ81782 SW8260 8/29/15 1 1,1,1,2-Tetrachloroethane ug/kg U 1.2 2514B8 (20-25) BJ81782 SW8260 8/29/15 1 Chloroform ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Benzene 0.73 ug/kg J 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 1,1,1-Trichloroethane ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Chloromethane ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Dibromomethane ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Bromochloromethane ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Vinyl Chloride 0.72 ug/kg J 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Carbon Disulfide ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Bromoform ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 1,1-Dichloroethane ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 1,1-Dichloroethene ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Tert-Butyl Alcohol ug/kg U 25 12014B8 (20-25) BJ81782 SW8260 8/29/15 1 1,1,2-Trichloro-1,2,2-Trifluoroethane ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 1,2-Dichloropropane ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Methyl Ethyl Ketone (2-Butanone) ug/kg U 6.2 3714B8 (20-25) BJ81782 SW8260 8/29/15 1 1,1,2-Trichloroethane ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Trichloroethylene (TCE) 2.0 ug/kg J 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 1,1,2,2-Tetrachloroethane ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 1,2,3-Trichlorobenzene ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Hexachlorobutadiene ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Naphthalene ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 O-Xylene (1,2-Dimethylbenzene) ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 2-Chlorotoluene ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 1,2-Dichlorobenzene ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 1,2,4-Trimethylbenzene ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 1,2-Dibromo-3-Chloropropane ug/kg U 1.2 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 1,2,3-Trichloropropane ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 T-Butylbenzene ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Isopropylbenzene (Cumene) ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8260 8/29/15 1 Cymene ug/kg U 0.62 6.214B8 (20-25) BJ81782 SW8270 8/27/15 1 4-Nitroaniline ug/kg U 140 84014B8 (20-25) BJ81782 SW8270 8/27/15 1 4-Nitrophenol ug/kg U 190 42014B8 (20-25) BJ81782 SW8270 8/27/15 1 4-Bromophenyl Phenyl Ether ug/kg U 120 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 2,4-Dimethylphenol ug/kg U 100 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 1,4-Dichlorobenzene ug/kg U 120 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 4-Chloroaniline ug/kg U 200 340

Page 9 of 82



SDG: GBJ81780



14B8 (20-25) BJ81782 SW8270 8/27/15 1 Phenol ug/kg U 130 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Pyridine ug/kg U 100 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Bis(2-Chloroethyl) Ether (2-Chloroethyl Ether) ug/kg U 110 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Bis(2-Chloroethoxy) Methane ug/kg U 120 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Bis(2-Ethylhexyl) Phthalate ug/kg U 120 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Di-N-Octylphthalate ug/kg U 110 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Hexachlorobenzene ug/kg U 120 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Anthracene ug/kg U 140 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 1,2,4-Trichlorobenzene ug/kg U 130 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 2,4-Dichlorophenol ug/kg U 150 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 2,4-Dinitrotoluene ug/kg U 170 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 1,2-Diphenylhydrazine ug/kg U 140 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Pyrene ug/kg U 140 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Dimethyl Phthalate ug/kg U 130 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Dibenzofuran ug/kg U 120 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Benzo(G,H,I)Perylene ug/kg U 140 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Indeno(1,2,3-C,D)Pyrene ug/kg U 140 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Benzo(B)Fluoranthene ug/kg U 140 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Fluoranthene ug/kg U 140 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Benzo(K)Fluoranthene ug/kg U 140 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Acenaphthylene ug/kg U 120 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Chrysene ug/kg U 140 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 2,2-Oxybis(2-Chloropropane) ug/kg U 120 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Benzo(A)Pyrene ug/kg U 140 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 2,4-Dinitrophenol ug/kg UJ 290 84014B8 (20-25) BJ81782 SW8270 8/27/15 1 4,6-Dinitro-2-Methylphenol ug/kg UJ 450 210014B8 (20-25) BJ81782 SW8270 8/27/15 1 Dibenz(A,H)Anthracene ug/kg U 140 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 1,3-Dichlorobenzene ug/kg U 120 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Benzo(A)Anthracene ug/kg U 140 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 4-Chloro-3-Methylphenol ug/kg U 150 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 2,6-Dinitrotoluene ug/kg U 130 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 N-Nitrosodi-N-Propylamine ug/kg U 140 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Aniline ug/kg U 340 34014B8 (20-25) BJ81782 SW8270 8/27/15 1 N-Nitrosodimethylamine ug/kg U 120 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Benzoic Acid ug/kg R 840 210014B8 (20-25) BJ81782 SW8270 8/27/15 1 Hexachloroethane ug/kg U 130 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 4-Chlorophenyl Phenyl Ether ug/kg U 140 290

Page 10 of 82



SDG: GBJ81780



14B8 (20-25) BJ81782 SW8270 8/27/15 1 Hexachlorocyclopentadiene ug/kg UJ 130 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Isophorone ug/kg U 120 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Pentachloronitrobenzene ug/kg U 160 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Acenaphthene ug/kg U 130 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Diethyl Phthalate ug/kg U 130 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Di-N-Butyl Phthalate ug/kg U 110 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Phenanthrene ug/kg U 120 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Benzyl Butyl Phthalate ug/kg U 110 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 N-Nitrosodiphenylamine ug/kg U 160 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Fluorene ug/kg U 140 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Carbazole ug/kg U 320 210014B8 (20-25) BJ81782 SW8270 8/27/15 1 Hexachlorobutadiene ug/kg U 150 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Pentachlorophenol ug/kg UJ 160 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 2,4,6-Trichlorophenol ug/kg U 130 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 2-Nitroaniline ug/kg U 420 84014B8 (20-25) BJ81782 SW8270 8/27/15 1 2-Nitrophenol ug/kg U 270 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Naphthalene ug/kg U 120 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 2-Methylnaphthalene ug/kg U 130 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 2-Chloronaphthalene ug/kg U 120 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 3,3'-Dichlorobenzidine ug/kg U 200 84014B8 (20-25) BJ81782 SW8270 8/27/15 1 2-Methylphenol (O-Cresol) ug/kg U 200 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 1,2-Dichlorobenzene ug/kg U 120 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 2-Chlorophenol ug/kg U 120 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 1,2,4,5-Tetrachlorobenzene ug/kg U 150 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 2,4,5-Trichlorophenol ug/kg U 230 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Acetophenone ug/kg U 130 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 Nitrobenzene ug/kg U 150 29014B8 (20-25) BJ81782 SW8270 8/27/15 1 3-Nitroaniline ug/kg U 840 84014B8 (20-25) BJ81782 SW8270 8/27/15 1 3- And 4- Methylphenol (Total) ug/kg U 170 29014B7 (0-5) BJ81783 SW8260 8/29/15 1 Acetone 12 ug/kg J 5.3 5014B7 (0-5) BJ81783 SW8260 8/29/15 1 Bromodichloromethane ug/kg U 1.1 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Bromomethane ug/kg U 2.1 5.314B7 (0-5) BJ81783 SW8270 8/27/15 1 Benzidine ug/kg UJ 240 82014B7 (0-5) BJ81783 SW8260 8/29/15 1 Methylene Chloride ug/kg U 5.3 5.314B7 (0-5) BJ81783 SW6010 8/28/15 1 Potassium 984 mg/kg J+ 3.2 814B7 (0-5) BJ81783 SW8260 8/29/15 1 Carbon Tetrachloride ug/kg U 1.1 5.314B7 (0-5) BJ81783 SW6010 8/28/15 10 Iron 12500 mg/kg 42 42

Page 11 of 82



SDG: GBJ81780



14B7 (0-5) BJ81783 SW8260 8/29/15 1 Chloroethane ug/kg UJ 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Methyl Ethyl Ketone (2-Butanone) ug/kg U 5.3 3214B7 (0-5) BJ81783 E160.3 8/26/15 1 Solids, Percent 80 %14B7 (0-5) BJ81783 SW6010 8/28/15 10 Aluminum 6730 mg/kg 8.3 4214B7 (0-5) BJ81783 SW6010 8/28/15 10 Manganese 230 mg/kg 4.2 4.214B7 (0-5) BJ81783 SW6010 8/28/15 1 Lead 47.2 mg/kg 0.42 0.814B7 (0-5) BJ81783 SW6010 8/28/15 1 Magnesium 3000 mg/kg 4.2 4.214B7 (0-5) BJ81783 SW6010 8/28/15 1 Nickel 13.2 mg/kg 0.42 0.4214B7 (0-5) BJ81783 SW6010 8/28/15 1 Silver mg/kg U 0.42 0.4214B7 (0-5) BJ81783 SW6010 8/28/15 1 Sodium 176 mg/kg 3.6 814B7 (0-5) BJ81783 SW6010 8/28/15 1 Thallium mg/kg U 1.7 1.714B7 (0-5) BJ81783 SW6010 8/28/15 1 Antimony mg/kg U 2.1 2.114B7 (0-5) BJ81783 SW6010 8/28/15 1 Arsenic 2.8 mg/kg 0.83 0.814B7 (0-5) BJ81783 SW6010 8/28/15 1 Barium 55.5 mg/kg 0.42 0.814B7 (0-5) BJ81783 SW6010 8/28/15 1 Beryllium 0.32 mg/kg J 0.17 0.3314B7 (0-5) BJ81783 SW6010 8/28/15 1 Cadmium mg/kg U 0.17 0.4214B7 (0-5) BJ81783 SW6010 8/28/15 1 Chromium, Total 15.0 mg/kg 0.42 0.4214B7 (0-5) BJ81783 SW6010 8/28/15 1 Cobalt 5.05 mg/kg 0.42 0.4214B7 (0-5) BJ81783 SW6010 8/28/15 1 Copper 21.3 mg/kg 0.42 0.4214B7 (0-5) BJ81783 SW6010 8/28/15 1 Vanadium 26.5 mg/kg 0.42 0.414B7 (0-5) BJ81783 SW6010 8/28/15 1 Calcium 5910 mg/kg 3.8 4.214B7 (0-5) BJ81783 SW6010 8/28/15 1 Selenium mg/kg U 1.4 1.714B7 (0-5) BJ81783 SW7471 8/27/15 1 Mercury 0.07 mg/kg 0.02 0.0314B7 (0-5) BJ81783 SW8081 8/28/15 10 Heptachlor Epoxide ug/kg U 41 4114B7 (0-5) BJ81783 SW8081 8/28/15 10 Endosulfan Sulfate ug/kg U 41 4114B7 (0-5) BJ81783 SW8081 8/28/15 10 Aldrin ug/kg U 6.2 6.214B7 (0-5) BJ81783 SW8081 8/28/15 10 Alpha Bhc (Alpha Hexachlorocyclohexane) ug/kg U 21 2114B7 (0-5) BJ81783 SW8081 8/28/15 10 Beta Bhc (Beta Hexachlorocyclohexane) ug/kg U 21 2114B7 (0-5) BJ81783 SW8081 8/28/15 10 Delta BHC (Delta Hexachlorocyclohexane) ug/kg U 21 2114B7 (0-5) BJ81783 SW8081 8/28/15 10 Beta Endosulfan ug/kg U 41 4114B7 (0-5) BJ81783 SW8081 8/28/15 10 P,P'-DDT ug/kg U 10 1014B7 (0-5) BJ81783 SW8081 8/28/15 10 cis-Chlordane 56 ug/kg 21 2114B7 (0-5) BJ81783 SW8081 8/28/15 10 trans-Chlordane 66 ug/kg 21 2114B7 (0-5) BJ81783 SW8081 8/28/15 10 Endrin Ketone ug/kg U 41 4114B7 (0-5) BJ81783 SW8081 8/28/15 10 Gamma Bhc (Lindane) ug/kg U 8.2 8.214B7 (0-5) BJ81783 SW8081 8/28/15 10 Dieldrin 13 ug/kg 6.2 6.214B7 (0-5) BJ81783 SW8081 8/28/15 10 Endrin ug/kg U 21 21

Page 12 of 82



SDG: GBJ81780



14B7 (0-5) BJ81783 SW8081 8/28/15 10 Methoxychlor ug/kg U 210 21014B7 (0-5) BJ81783 SW8081 8/28/15 10 P,P'-DDD ug/kg U 10 1014B7 (0-5) BJ81783 SW8081 8/28/15 10 P,P'-DDE ug/kg U 10 1014B7 (0-5) BJ81783 SW8081 8/28/15 10 Endrin Aldehyde ug/kg U 50 5014B7 (0-5) BJ81783 SW8081 8/28/15 10 Heptachlor ug/kg U 41 4114B7 (0-5) BJ81783 SW8081 8/28/15 10 Toxaphene ug/kg U 820 82014B7 (0-5) BJ81783 SW8081 8/28/15 10 Alpha Endosulfan ug/kg U 41 4114B7 (0-5) BJ81783 SW8082 8/29/15 2 PCB-1260 (Aroclor 1260) ug/kg U 41 4114B7 (0-5) BJ81783 SW8082 8/29/15 2 PCB-1254 (Aroclor 1254) ug/kg U 41 4114B7 (0-5) BJ81783 SW8082 8/29/15 2 PCB-1268 (Aroclor 1268) ug/kg U 41 4114B7 (0-5) BJ81783 SW8082 8/29/15 2 PCB-1221 (Aroclor 1221) ug/kg U 41 4114B7 (0-5) BJ81783 SW8082 8/29/15 2 PCB-1232 (Aroclor 1232) ug/kg U 41 4114B7 (0-5) BJ81783 SW8082 8/29/15 2 PCB-1248 (Aroclor 1248) ug/kg U 41 4114B7 (0-5) BJ81783 SW8082 8/29/15 2 PCB-1016 (Aroclor 1016) ug/kg U 41 4114B7 (0-5) BJ81783 SW8082 8/29/15 2 PCB-1262 (Aroclor 1262) ug/kg U 41 4114B7 (0-5) BJ81783 SW8082 8/29/15 2 PCB-1242 (Aroclor 1242) ug/kg U 41 4114B7 (0-5) BJ81783 SW8260 8/29/15 1 Ethylbenzene 1.9 ug/kg J 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Styrene ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Cis-1,3-Dichloropropene ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 N-Propylbenzene ug/kg U 0.96 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 N-Butylbenzene ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 4-Chlorotoluene ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 1,4-Dichlorobenzene ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 1,2-Dibromoethane (Ethylene Dibromide) ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Acrolein ug/kg U 2.7 2114B7 (0-5) BJ81783 SW8260 8/29/15 1 1,2-Dichloroethane ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Acrylonitrile ug/kg U 0.53 2114B7 (0-5) BJ81783 SW8260 8/29/15 1 Methyl Isobutyl Ketone (4-Methyl-2-Pentanone) ug/kg U 5.3 2714B7 (0-5) BJ81783 SW8260 8/29/15 1 1,3,5-Trimethylbenzene (Mesitylene) ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Bromobenzene ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Chlorobenzene ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Tetrahydrofuran ug/kg U 2.7 1114B7 (0-5) BJ81783 SW8260 8/29/15 1 Trans-1,4-Dichloro-2-Butene ug/kg U 2.7 1114B7 (0-5) BJ81783 SW8260 8/29/15 1 1,2,4-Trichlorobenzene ug/kg U 1.1 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 1,4-Dioxane (P-Dioxane) ug/kg U 43 10014B7 (0-5) BJ81783 SW8260 8/29/15 1 Dibromochloromethane ug/kg U 1.1 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Tetrachloroethylene (PCE) ug/kg U 1.1 5.3

Page 13 of 82



SDG: GBJ81780



14B7 (0-5) BJ81783 SW8260 8/29/15 1 Sec-Butylbenzene ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 1,3-Dichloropropane ug/kg U 1.1 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Cis-1,2-Dichloroethylene 3.1 ug/kg J 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Trans-1,2-Dichloroethene ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Tert-Butyl Methyl Ether ug/kg U 1.1 1114B7 (0-5) BJ81783 SW8260 8/29/15 1 m,p-Xylene 7.5 ug/kg 1.1 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 O-Cymene (O-Isopropyltoluene) ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 1,3-Dichlorobenzene ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 1,1-Dichloropropene ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 2-Hexanone ug/kg U 5.3 2714B7 (0-5) BJ81783 SW8260 8/29/15 1 2,2-Dichloropropane ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 1,1,1,2-Tetrachloroethane ug/kg U 1.1 2114B7 (0-5) BJ81783 SW8260 8/29/15 1 Chloroform ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Benzene 0.77 ug/kg J 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 1,1,1-Trichloroethane ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Chloromethane ug/kg U 1.1 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Dibromomethane ug/kg U 1.1 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Bromochloromethane ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Vinyl Chloride ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Carbon Disulfide 1.1 ug/kg J 1.1 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Bromoform ug/kg U 1.1 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 1,1-Dichloroethane ug/kg U 1.1 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 1,1-Dichloroethene ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Tert-Butyl Alcohol ug/kg U 21 11014B7 (0-5) BJ81783 SW8260 8/29/15 1 1,1,2-Trichloro-1,2,2-Trifluoroethane ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 1,2-Dichloropropane ug/kg U 1.1 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 1,1,2-Trichloroethane ug/kg U 1.1 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 1,1,2,2-Tetrachloroethane ug/kg U 1.1 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 1,2,3-Trichlorobenzene ug/kg U 1.1 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Hexachlorobutadiene ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 O-Xylene (1,2-Dimethylbenzene) 2.5 ug/kg J 1.1 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 2-Chlorotoluene ug/kg U 1.1 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 1,2-Dichlorobenzene ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 1,2,4-Trimethylbenzene ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 1,2-Dibromo-3-Chloropropane ug/kg U 1.1 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 1,2,3-Trichloropropane ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 T-Butylbenzene ug/kg U 0.53 5.3

Page 14 of 82



SDG: GBJ81780



14B7 (0-5) BJ81783 SW8260 8/29/15 1 Isopropylbenzene (Cumene) ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Cymene ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 50 Toluene 110 ug/kg J 40 40014B7 (0-5) BJ81783 SW8260 8/29/15 50 Trichloroethylene (TCE) 100 ug/kg J 40 40014B7 (0-5) BJ81783 SW8260 8/29/15 50 Naphthalene 260 ug/kg J 79 40014B7 (0-5) BJ81783 SW8270 8/27/15 1 4-Nitroaniline ug/kg U 140 82014B7 (0-5) BJ81783 SW8270 8/27/15 1 4-Nitrophenol ug/kg U 190 41014B7 (0-5) BJ81783 SW8270 8/27/15 1 4-Bromophenyl Phenyl Ether ug/kg U 120 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 2,4-Dimethylphenol ug/kg U 100 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 1,4-Dichlorobenzene ug/kg U 120 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 4-Chloroaniline ug/kg U 190 33014B7 (0-5) BJ81783 SW8270 8/27/15 1 Phenol ug/kg U 130 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Pyridine ug/kg U 100 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Bis(2-Chloroethyl) Ether (2-Chloroethyl Ether) ug/kg U 110 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Bis(2-Chloroethoxy) Methane ug/kg U 110 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Bis(2-Ethylhexyl) Phthalate ug/kg U 120 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Di-N-Octylphthalate ug/kg U 110 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Hexachlorobenzene ug/kg U 120 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Anthracene 260 ug/kg J 130 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 1,2,4-Trichlorobenzene ug/kg U 120 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 2,4-Dichlorophenol ug/kg U 140 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 2,4-Dinitrotoluene ug/kg U 160 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 1,2-Diphenylhydrazine ug/kg U 130 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Pyrene 2200 ug/kg 140 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Dimethyl Phthalate ug/kg U 130 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Dibenzofuran ug/kg U 120 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Benzo(G,H,I)Perylene 640 ug/kg 130 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Indeno(1,2,3-C,D)Pyrene 720 ug/kg 140 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Benzo(B)Fluoranthene 1100 ug/kg 140 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Fluoranthene 2800 ug/kg 130 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Benzo(K)Fluoranthene 960 ug/kg 140 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Acenaphthylene ug/kg U 110 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Chrysene 1400 ug/kg 140 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 2,2-Oxybis(2-Chloropropane) ug/kg U 110 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Benzo(A)Pyrene 940 ug/kg 130 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 2,4-Dinitrophenol ug/kg UJ 290 82014B7 (0-5) BJ81783 SW8270 8/27/15 1 4,6-Dinitro-2-Methylphenol ug/kg UJ 440 2000

Page 15 of 82



SDG: GBJ81780



14B7 (0-5) BJ81783 SW8270 8/27/15 1 Dibenz(A,H)Anthracene 160 ug/kg J 130 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 1,3-Dichlorobenzene ug/kg U 120 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Benzo(A)Anthracene 1200 ug/kg 140 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 4-Chloro-3-Methylphenol ug/kg U 140 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 2,6-Dinitrotoluene ug/kg U 130 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 N-Nitrosodi-N-Propylamine ug/kg U 130 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Aniline ug/kg U 330 33014B7 (0-5) BJ81783 SW8270 8/27/15 1 N-Nitrosodimethylamine ug/kg U 120 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Benzoic Acid ug/kg R 820 200014B7 (0-5) BJ81783 SW8270 8/27/15 1 Hexachloroethane ug/kg U 120 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 4-Chlorophenyl Phenyl Ether ug/kg U 140 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Hexachlorocyclopentadiene ug/kg UJ 130 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Isophorone ug/kg U 110 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Pentachloronitrobenzene ug/kg U 150 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Acenaphthene ug/kg U 120 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Diethyl Phthalate ug/kg U 130 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Di-N-Butyl Phthalate ug/kg U 110 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Phenanthrene 1700 ug/kg 120 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Benzyl Butyl Phthalate ug/kg U 110 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 N-Nitrosodiphenylamine ug/kg U 160 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Fluorene ug/kg U 140 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Carbazole ug/kg U 310 200014B7 (0-5) BJ81783 SW8270 8/27/15 1 Hexachlorobutadiene ug/kg U 150 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Pentachlorophenol ug/kg UJ 150 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 2,4,6-Trichlorophenol ug/kg U 130 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 2-Nitroaniline ug/kg U 410 82014B7 (0-5) BJ81783 SW8270 8/27/15 1 2-Nitrophenol ug/kg U 260 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Naphthalene ug/kg U 120 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 2-Methylnaphthalene ug/kg U 120 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 2-Chloronaphthalene ug/kg U 120 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 3,3'-Dichlorobenzidine ug/kg U 190 82014B7 (0-5) BJ81783 SW8270 8/27/15 1 2-Methylphenol (O-Cresol) ug/kg U 190 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 1,2-Dichlorobenzene ug/kg U 120 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 2-Chlorophenol ug/kg U 120 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 1,2,4,5-Tetrachlorobenzene ug/kg U 140 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 2,4,5-Trichlorophenol ug/kg U 220 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 Acetophenone ug/kg U 130 290

Page 16 of 82



SDG: GBJ81780



14B7 (0-5) BJ81783 SW8270 8/27/15 1 Nitrobenzene ug/kg U 140 29014B7 (0-5) BJ81783 SW8270 8/27/15 1 3-Nitroaniline ug/kg U 820 82014B7 (0-5) BJ81783 SW8270 8/27/15 1 3- And 4- Methylphenol (Total) ug/kg U 160 29014B7 (0-5) BJ81783 SW8260 8/29/15 1 Dichlorodifluoromethane ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW6010 8/28/15 1 Zinc 52.1 mg/kg J+ 0.42 0.814B7 (0-5) BJ81783 SW8260 8/29/15 1 Trans-1,3-Dichloropropene ug/kg U 0.53 5.314B7 (0-5) BJ81783 SW8260 8/29/15 1 Trichlorofluoromethane ug/kg UJ 1.1 5.314B7 (15-20) BJ81785 SW8260 8/29/15 1 Acetone ug/kg UJ 4.5 4514B7 (15-20) BJ81785 SW8260 8/29/15 1 Bromodichloromethane ug/kg U 0.90 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Bromomethane ug/kg U 1.8 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Carbon Tetrachloride ug/kg U 0.90 4.514B7 (15-20) BJ81785 SW8270 8/27/15 1 Benzidine ug/kg UJ 240 81014B7 (15-20) BJ81785 SW6010 8/28/15 1 Potassium 2170 mg/kg J+ 2.9 714B7 (15-20) BJ81785 SW8260 8/29/15 1 Methylene Chloride ug/kg U 4.5 4.514B7 (15-20) BJ81785 SW6010 8/28/15 10 Iron 23900 mg/kg 37 3714B7 (15-20) BJ81785 SW8260 8/29/15 1 Chloroethane ug/kg UJ 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Dichlorodifluoromethane ug/kg U 0.45 4.514B7 (15-20) BJ81785 E160.3 8/26/15 1 Solids, Percent 82 %14B7 (15-20) BJ81785 SW6010 8/28/15 10 Aluminum 11000 mg/kg 7.3 3714B7 (15-20) BJ81785 SW6010 8/28/15 10 Manganese 420 mg/kg 3.7 3.714B7 (15-20) BJ81785 SW6010 8/28/15 1 Lead 5.9 mg/kg 0.37 0.714B7 (15-20) BJ81785 SW6010 8/28/15 1 Magnesium 3500 mg/kg 3.7 3.714B7 (15-20) BJ81785 SW6010 8/28/15 1 Nickel 16.2 mg/kg 0.37 0.3714B7 (15-20) BJ81785 SW6010 8/28/15 1 Silver mg/kg U 0.37 0.3714B7 (15-20) BJ81785 SW6010 8/28/15 1 Sodium 290 mg/kg J+ 3.2 714B7 (15-20) BJ81785 SW6010 8/28/15 1 Thallium mg/kg U 1.5 1.514B7 (15-20) BJ81785 SW6010 8/28/15 1 Antimony mg/kg UJ 1.8 1.814B7 (15-20) BJ81785 SW6010 8/28/15 1 Arsenic 1.5 mg/kg 0.73 0.714B7 (15-20) BJ81785 SW6010 8/28/15 1 Barium 55.3 mg/kg 0.37 0.714B7 (15-20) BJ81785 SW6010 8/28/15 1 Beryllium 0.64 mg/kg 0.15 0.2914B7 (15-20) BJ81785 SW6010 8/28/15 1 Cadmium mg/kg U 0.15 0.3714B7 (15-20) BJ81785 SW6010 8/28/15 1 Chromium, Total 21.1 mg/kg 0.37 0.3714B7 (15-20) BJ81785 SW6010 8/28/15 1 Cobalt 10.1 mg/kg 0.37 0.3714B7 (15-20) BJ81785 SW6010 8/28/15 1 Copper 17.2 mg/kg 0.37 0.3714B7 (15-20) BJ81785 SW6010 8/28/15 1 Vanadium 31.4 mg/kg 0.37 0.414B7 (15-20) BJ81785 SW6010 8/28/15 1 Calcium 1260 mg/kg 3.4 3.714B7 (15-20) BJ81785 SW6010 8/28/15 1 Selenium mg/kg U 1.2 1.5

Page 17 of 82



SDG: GBJ81780



14B7 (15-20) BJ81785 SW7471 8/27/15 1 Mercury mg/kg U 0.02 0.0314B7 (15-20) BJ81785 SW8081 8/28/15 2 Heptachlor Epoxide ug/kg U 8.0 8.014B7 (15-20) BJ81785 SW8081 8/28/15 2 Endosulfan Sulfate ug/kg U 8.0 8.014B7 (15-20) BJ81785 SW8081 8/28/15 2 Aldrin ug/kg U 4.0 4.014B7 (15-20) BJ81785 SW8081 8/28/15 2 Alpha Bhc (Alpha Hexachlorocyclohexane) ug/kg U 8.0 8.014B7 (15-20) BJ81785 SW8081 8/28/15 2 Beta Bhc (Beta Hexachlorocyclohexane) ug/kg U 8.0 8.014B7 (15-20) BJ81785 SW8081 8/28/15 2 Delta BHC (Delta Hexachlorocyclohexane) ug/kg U 8.0 8.014B7 (15-20) BJ81785 SW8081 8/28/15 2 Beta Endosulfan ug/kg U 8.0 8.014B7 (15-20) BJ81785 SW8081 8/28/15 2 P,P'-DDT ug/kg U 2.4 2.414B7 (15-20) BJ81785 SW8081 8/28/15 2 cis-Chlordane ug/kg U 4.0 4.014B7 (15-20) BJ81785 SW8081 8/28/15 2 trans-Chlordane ug/kg U 4.0 4.014B7 (15-20) BJ81785 SW8081 8/28/15 2 Endrin Ketone ug/kg U 8.0 8.014B7 (15-20) BJ81785 SW8081 8/28/15 2 Gamma Bhc (Lindane) ug/kg U 1.6 1.614B7 (15-20) BJ81785 SW8081 8/28/15 2 Dieldrin ug/kg U 4.0 4.014B7 (15-20) BJ81785 SW8081 8/28/15 2 Endrin ug/kg U 8.0 8.014B7 (15-20) BJ81785 SW8081 8/28/15 2 Methoxychlor ug/kg U 40 4014B7 (15-20) BJ81785 SW8081 8/28/15 2 P,P'-DDD ug/kg U 2.4 2.414B7 (15-20) BJ81785 SW8081 8/28/15 2 P,P'-DDE ug/kg U 2.4 2.414B7 (15-20) BJ81785 SW8081 8/28/15 2 Endrin Aldehyde ug/kg U 8.0 8.014B7 (15-20) BJ81785 SW8081 8/28/15 2 Heptachlor ug/kg U 8.0 8.014B7 (15-20) BJ81785 SW8081 8/28/15 2 Toxaphene ug/kg U 160 16014B7 (15-20) BJ81785 SW8081 8/28/15 2 Alpha Endosulfan ug/kg U 8.0 8.014B7 (15-20) BJ81785 SW8082 8/29/15 2 PCB-1260 (Aroclor 1260) ug/kg U 40 4014B7 (15-20) BJ81785 SW8082 8/29/15 2 PCB-1254 (Aroclor 1254) ug/kg U 40 4014B7 (15-20) BJ81785 SW8082 8/29/15 2 PCB-1268 (Aroclor 1268) ug/kg U 40 4014B7 (15-20) BJ81785 SW8082 8/29/15 2 PCB-1221 (Aroclor 1221) ug/kg U 40 4014B7 (15-20) BJ81785 SW8082 8/29/15 2 PCB-1232 (Aroclor 1232) ug/kg U 40 4014B7 (15-20) BJ81785 SW8082 8/29/15 2 PCB-1248 (Aroclor 1248) ug/kg U 40 4014B7 (15-20) BJ81785 SW8082 8/29/15 2 PCB-1016 (Aroclor 1016) ug/kg U 40 4014B7 (15-20) BJ81785 SW8082 8/29/15 2 PCB-1262 (Aroclor 1262) ug/kg U 40 4014B7 (15-20) BJ81785 SW8082 8/29/15 2 PCB-1242 (Aroclor 1242) ug/kg U 40 4014B7 (15-20) BJ81785 SW8260 8/29/15 1 Ethylbenzene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Styrene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Cis-1,3-Dichloropropene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 N-Propylbenzene ug/kg U 0.81 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 N-Butylbenzene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 4-Chlorotoluene ug/kg U 0.45 4.5

Page 18 of 82



SDG: GBJ81780



14B7 (15-20) BJ81785 SW8260 8/29/15 1 1,4-Dichlorobenzene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 1,2-Dibromoethane (Ethylene Dibromide) ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Acrolein ug/kg U 2.3 1814B7 (15-20) BJ81785 SW8260 8/29/15 1 1,2-Dichloroethane ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Acrylonitrile ug/kg U 0.45 1814B7 (15-20) BJ81785 SW8260 8/29/15 1 Methyl Isobutyl Ketone (4-Methyl-2-Pentanone) ug/kg U 4.5 2314B7 (15-20) BJ81785 SW8260 8/29/15 1 1,3,5-Trimethylbenzene (Mesitylene) ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Bromobenzene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Toluene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Chlorobenzene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Tetrahydrofuran ug/kg U 2.3 9.014B7 (15-20) BJ81785 SW8260 8/29/15 1 Trans-1,4-Dichloro-2-Butene ug/kg U 2.3 9.014B7 (15-20) BJ81785 SW8260 8/29/15 1 1,2,4-Trichlorobenzene ug/kg U 0.90 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 1,4-Dioxane (P-Dioxane) ug/kg U 36 9014B7 (15-20) BJ81785 SW8260 8/29/15 1 Dibromochloromethane ug/kg U 0.90 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Tetrachloroethylene (PCE) ug/kg U 0.90 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Sec-Butylbenzene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 1,3-Dichloropropane ug/kg U 0.90 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Cis-1,2-Dichloroethylene 37 ug/kg 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Trans-1,2-Dichloroethene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Tert-Butyl Methyl Ether ug/kg U 0.90 9.014B7 (15-20) BJ81785 SW8260 8/29/15 1 m,p-Xylene ug/kg U 0.90 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 O-Cymene (O-Isopropyltoluene) ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 1,3-Dichlorobenzene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 1,1-Dichloropropene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 2-Hexanone ug/kg U 4.5 2314B7 (15-20) BJ81785 SW8260 8/29/15 1 2,2-Dichloropropane ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 1,1,1,2-Tetrachloroethane ug/kg U 0.90 1814B7 (15-20) BJ81785 SW8260 8/29/15 1 Chloroform ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Benzene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 1,1,1-Trichloroethane ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Chloromethane ug/kg U 0.90 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Dibromomethane ug/kg U 0.90 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Bromochloromethane ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Vinyl Chloride ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Carbon Disulfide ug/kg U 0.90 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Bromoform ug/kg U 0.90 4.5

Page 19 of 82



SDG: GBJ81780



14B7 (15-20) BJ81785 SW8260 8/29/15 1 1,1-Dichloroethane ug/kg U 0.90 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 1,1-Dichloroethene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Tert-Butyl Alcohol ug/kg U 18 9014B7 (15-20) BJ81785 SW8260 8/29/15 1 1,1,2-Trichloro-1,2,2-Trifluoroethane ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 1,2-Dichloropropane ug/kg U 0.90 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Methyl Ethyl Ketone (2-Butanone) ug/kg U 4.5 2714B7 (15-20) BJ81785 SW8260 8/29/15 1 1,1,2-Trichloroethane ug/kg U 0.90 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Trichloroethylene (TCE) 23 ug/kg 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 1,1,2,2-Tetrachloroethane ug/kg U 0.90 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 1,2,3-Trichlorobenzene ug/kg U 0.90 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Hexachlorobutadiene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Naphthalene ug/kg U 0.90 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 O-Xylene (1,2-Dimethylbenzene) ug/kg U 0.90 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 2-Chlorotoluene ug/kg U 0.90 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 1,2-Dichlorobenzene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 1,2,4-Trimethylbenzene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 1,2-Dibromo-3-Chloropropane ug/kg U 0.90 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 1,2,3-Trichloropropane ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 T-Butylbenzene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Isopropylbenzene (Cumene) ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Cymene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8270 8/27/15 1 4-Nitroaniline ug/kg U 140 81014B7 (15-20) BJ81785 SW8270 8/27/15 1 4-Nitrophenol ug/kg U 180 41014B7 (15-20) BJ81785 SW8270 8/27/15 1 4-Bromophenyl Phenyl Ether ug/kg U 120 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 2,4-Dimethylphenol ug/kg U 100 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 1,4-Dichlorobenzene ug/kg U 120 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 4-Chloroaniline ug/kg U 190 32014B7 (15-20) BJ81785 SW8270 8/27/15 1 Phenol ug/kg U 130 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Pyridine ug/kg U 100 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Bis(2-Chloroethyl) Ether (2-Chloroethyl Ether) ug/kg U 110 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Bis(2-Chloroethoxy) Methane ug/kg U 110 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Bis(2-Ethylhexyl) Phthalate ug/kg U 120 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Di-N-Octylphthalate ug/kg U 100 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Hexachlorobenzene ug/kg U 120 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Anthracene ug/kg U 130 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 1,2,4-Trichlorobenzene ug/kg U 120 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 2,4-Dichlorophenol ug/kg U 140 280

Page 20 of 82



SDG: GBJ81780



14B7 (15-20) BJ81785 SW8270 8/27/15 1 2,4-Dinitrotoluene ug/kg U 160 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 1,2-Diphenylhydrazine ug/kg U 130 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Pyrene ug/kg U 140 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Dimethyl Phthalate ug/kg U 130 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Dibenzofuran ug/kg U 120 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Benzo(G,H,I)Perylene 340 ug/kg 130 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Indeno(1,2,3-C,D)Pyrene 410 ug/kg 130 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Benzo(B)Fluoranthene 560 ug/kg 140 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Fluoranthene ug/kg U 130 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Benzo(K)Fluoranthene 680 ug/kg 130 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Acenaphthylene ug/kg U 110 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Chrysene 150 ug/kg J 140 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 2,2-Oxybis(2-Chloropropane) ug/kg U 110 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Benzo(A)Pyrene 920 ug/kg 130 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 2,4-Dinitrophenol ug/kg UJ 280 81014B7 (15-20) BJ81785 SW8270 8/27/15 1 4,6-Dinitro-2-Methylphenol ug/kg UJ 440 200014B7 (15-20) BJ81785 SW8270 8/27/15 1 Dibenz(A,H)Anthracene ug/kg U 130 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 1,3-Dichlorobenzene ug/kg U 120 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Benzo(A)Anthracene 140 ug/kg J 140 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 4-Chloro-3-Methylphenol ug/kg U 140 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 2,6-Dinitrotoluene ug/kg U 130 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 N-Nitrosodi-N-Propylamine ug/kg U 130 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Aniline ug/kg U 320 32014B7 (15-20) BJ81785 SW8270 8/27/15 1 N-Nitrosodimethylamine ug/kg U 110 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Benzoic Acid ug/kg R 810 200014B7 (15-20) BJ81785 SW8270 8/27/15 1 Hexachloroethane ug/kg U 120 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 4-Chlorophenyl Phenyl Ether ug/kg U 140 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Hexachlorocyclopentadiene ug/kg UJ 120 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Isophorone ug/kg U 110 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Pentachloronitrobenzene ug/kg U 150 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Acenaphthene ug/kg U 120 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Diethyl Phthalate ug/kg U 130 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Di-N-Butyl Phthalate ug/kg U 110 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Phenanthrene ug/kg U 120 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Benzyl Butyl Phthalate ug/kg U 100 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 N-Nitrosodiphenylamine ug/kg U 160 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Fluorene ug/kg U 130 280

Page 21 of 82



SDG: GBJ81780



14B7 (15-20) BJ81785 SW8270 8/27/15 1 Carbazole ug/kg U 310 200014B7 (15-20) BJ81785 SW8270 8/27/15 1 Hexachlorobutadiene ug/kg U 150 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Pentachlorophenol ug/kg UJ 150 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 2,4,6-Trichlorophenol ug/kg U 130 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 2-Nitroaniline ug/kg U 410 81014B7 (15-20) BJ81785 SW8270 8/27/15 1 2-Nitrophenol ug/kg U 260 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Naphthalene ug/kg U 120 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 2-Methylnaphthalene ug/kg U 120 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 2-Chloronaphthalene ug/kg U 120 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 3,3'-Dichlorobenzidine ug/kg U 190 81014B7 (15-20) BJ81785 SW8270 8/27/15 1 2-Methylphenol (O-Cresol) ug/kg U 190 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 1,2-Dichlorobenzene ug/kg U 110 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 2-Chlorophenol ug/kg U 120 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 1,2,4,5-Tetrachlorobenzene ug/kg U 140 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 2,4,5-Trichlorophenol ug/kg U 220 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Acetophenone ug/kg U 130 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 Nitrobenzene ug/kg U 140 28014B7 (15-20) BJ81785 SW8270 8/27/15 1 3-Nitroaniline ug/kg U 810 81014B7 (15-20) BJ81785 SW8270 8/27/15 1 3- And 4- Methylphenol (Total) ug/kg U 160 28014B7 (15-20) BJ81785 SW6010 8/28/15 1 Zinc 33.9 mg/kg J+ 0.37 0.714B7 (15-20) BJ81785 SW8260 8/29/15 1 Trans-1,3-Dichloropropene ug/kg U 0.45 4.514B7 (15-20) BJ81785 SW8260 8/29/15 1 Trichlorofluoromethane ug/kg UJ 0.90 4.514B2 (0-5) BJ81786 SW6010 8/28/15 10 Iron 15800 mg/kg 33 3314B2 (0-5) BJ81786 SW8260 8/29/15 1 Acetone 6.9 ug/kg J 4.1 4114B2 (0-5) BJ81786 SW8260 8/29/15 1 Bromodichloromethane ug/kg U 0.81 4.114B2 (0-5) BJ81786 E160.3 8/26/15 1 Solids, Percent 90 %14B2 (0-5) BJ81786 SW6010 8/28/15 10 Aluminum 8770 mg/kg 6.5 3314B2 (0-5) BJ81786 SW6010 8/28/15 10 Manganese 334 mg/kg 3.3 3.314B2 (0-5) BJ81786 SW6010 8/28/15 1 Lead 56.1 mg/kg 0.33 0.714B2 (0-5) BJ81786 SW6010 8/28/15 1 Magnesium 2410 mg/kg 3.3 3.314B2 (0-5) BJ81786 SW6010 8/28/15 1 Nickel 19.4 mg/kg 0.33 0.3314B2 (0-5) BJ81786 SW6010 8/28/15 1 Silver mg/kg U 0.33 0.3314B2 (0-5) BJ81786 SW6010 8/28/15 1 Sodium 248 mg/kg 2.8 714B2 (0-5) BJ81786 SW6010 8/28/15 1 Thallium mg/kg U 1.3 1.314B2 (0-5) BJ81786 SW6010 8/28/15 1 Antimony mg/kg U 1.6 1.614B2 (0-5) BJ81786 SW6010 8/28/15 1 Arsenic 3.7 mg/kg 0.65 0.714B2 (0-5) BJ81786 SW6010 8/28/15 1 Barium 63.8 mg/kg 0.33 0.7

Page 22 of 82



SDG: GBJ81780



14B2 (0-5) BJ81786 SW6010 8/28/15 1 Beryllium 0.40 mg/kg 0.13 0.2614B2 (0-5) BJ81786 SW6010 8/28/15 1 Cadmium mg/kg U 0.13 0.3314B2 (0-5) BJ81786 SW6010 8/28/15 1 Chromium, Total 17.4 mg/kg 0.33 0.3314B2 (0-5) BJ81786 SW6010 8/28/15 1 Cobalt 7.04 mg/kg 0.33 0.3314B2 (0-5) BJ81786 SW6010 8/28/15 1 Copper 20.6 mg/kg 0.33 0.3314B2 (0-5) BJ81786 SW6010 8/28/15 1 Vanadium 26.2 mg/kg 0.33 0.314B2 (0-5) BJ81786 SW6010 8/28/15 1 Calcium 4670 mg/kg 3.0 3.314B2 (0-5) BJ81786 SW6010 8/28/15 1 Selenium mg/kg U 1.1 1.314B2 (0-5) BJ81786 SW7471 8/27/15 1 Mercury 0.19 mg/kg 0.02 0.0314B2 (0-5) BJ81786 SW8081 8/28/15 2 Heptachlor Epoxide ug/kg U 7.4 7.414B2 (0-5) BJ81786 SW8081 8/28/15 2 Endosulfan Sulfate ug/kg U 7.4 7.414B2 (0-5) BJ81786 SW8081 8/28/15 2 Aldrin ug/kg U 3.7 3.714B2 (0-5) BJ81786 SW8081 8/28/15 2 Alpha Bhc (Alpha Hexachlorocyclohexane) ug/kg U 7.4 7.414B2 (0-5) BJ81786 SW8081 8/28/15 2 Beta Bhc (Beta Hexachlorocyclohexane) ug/kg U 7.4 7.414B2 (0-5) BJ81786 SW8081 8/28/15 2 Delta BHC (Delta Hexachlorocyclohexane) ug/kg U 7.4 7.414B2 (0-5) BJ81786 SW8081 8/28/15 2 Beta Endosulfan ug/kg U 7.4 7.414B2 (0-5) BJ81786 SW8081 8/28/15 2 P,P'-DDT 7.1 ug/kg 2.2 2.214B2 (0-5) BJ81786 SW8081 8/28/15 2 cis-Chlordane 110 ug/kg 3.7 3.714B2 (0-5) BJ81786 SW8081 8/28/15 2 trans-Chlordane 130 ug/kg 3.7 3.714B2 (0-5) BJ81786 SW8081 8/28/15 2 Endrin Ketone ug/kg U 7.4 7.414B2 (0-5) BJ81786 SW8081 8/28/15 2 Gamma Bhc (Lindane) ug/kg U 2.0 2.014B2 (0-5) BJ81786 SW8081 8/28/15 2 Dieldrin 9.4 ug/kg 3.7 3.714B2 (0-5) BJ81786 SW8081 8/28/15 2 Endrin ug/kg U 7.4 7.414B2 (0-5) BJ81786 SW8081 8/28/15 2 Methoxychlor ug/kg U 37 3714B2 (0-5) BJ81786 SW8081 8/28/15 2 P,P'-DDD ug/kg U 5.0 5.014B2 (0-5) BJ81786 SW8081 8/28/15 2 P,P'-DDE 8.1 ug/kg 2.2 2.214B2 (0-5) BJ81786 SW8081 8/28/15 2 Endrin Aldehyde ug/kg U 7.4 7.414B2 (0-5) BJ81786 SW8081 8/28/15 2 Heptachlor ug/kg U 7.4 7.414B2 (0-5) BJ81786 SW8081 8/28/15 2 Toxaphene ug/kg U 150 15014B2 (0-5) BJ81786 SW8081 8/28/15 2 Alpha Endosulfan ug/kg U 7.4 7.414B2 (0-5) BJ81786 SW8082 8/31/15 10 PCB-1260 (Aroclor 1260) ug/kg U 180 18014B2 (0-5) BJ81786 SW8082 8/31/15 10 PCB-1254 (Aroclor 1254) ug/kg U 180 18014B2 (0-5) BJ81786 SW8082 8/31/15 10 PCB-1268 (Aroclor 1268) ug/kg U 180 18014B2 (0-5) BJ81786 SW8082 8/31/15 10 PCB-1221 (Aroclor 1221) ug/kg U 180 18014B2 (0-5) BJ81786 SW8082 8/31/15 10 PCB-1232 (Aroclor 1232) ug/kg U 180 18014B2 (0-5) BJ81786 SW8082 8/31/15 10 PCB-1248 (Aroclor 1248) ug/kg U 180 18014B2 (0-5) BJ81786 SW8082 8/31/15 10 PCB-1016 (Aroclor 1016) ug/kg U 180 180

Page 23 of 82



SDG: GBJ81780



14B2 (0-5) BJ81786 SW8082 8/31/15 10 PCB-1262 (Aroclor 1262) ug/kg U 180 18014B2 (0-5) BJ81786 SW8082 8/31/15 10 PCB-1242 (Aroclor 1242) ug/kg U 180 18014B2 (0-5) BJ81786 SW8260 8/29/15 1 Ethylbenzene ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Styrene ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Cis-1,3-Dichloropropene ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 N-Propylbenzene ug/kg U 0.73 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 N-Butylbenzene ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 4-Chlorotoluene ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,4-Dichlorobenzene ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,2-Dibromoethane (Ethylene Dibromide) ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Acrolein ug/kg U 2.0 1614B2 (0-5) BJ81786 SW8260 8/29/15 1 1,2-Dichloroethane ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Acrylonitrile ug/kg U 0.41 1614B2 (0-5) BJ81786 SW8260 8/29/15 1 Methyl Isobutyl Ketone (4-Methyl-2-Pentanone) ug/kg U 4.1 2014B2 (0-5) BJ81786 SW8260 8/29/15 1 1,3,5-Trimethylbenzene (Mesitylene) 1.1 ug/kg J 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Bromobenzene ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Toluene ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Chlorobenzene ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Tetrahydrofuran ug/kg U 2.0 8.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Trans-1,4-Dichloro-2-Butene ug/kg U 2.0 8.114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,2,4-Trichlorobenzene ug/kg U 0.81 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,4-Dioxane (P-Dioxane) ug/kg U 32 8114B2 (0-5) BJ81786 SW8260 8/29/15 1 Dibromochloromethane ug/kg U 0.81 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Tetrachloroethylene (PCE) ug/kg U 0.81 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Sec-Butylbenzene ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,3-Dichloropropane ug/kg U 0.81 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Cis-1,2-Dichloroethylene 5.2 ug/kg 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Trans-1,2-Dichloroethene ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Tert-Butyl Methyl Ether ug/kg U 0.81 8.114B2 (0-5) BJ81786 SW8260 8/29/15 1 m,p-Xylene ug/kg U 0.81 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 O-Cymene (O-Isopropyltoluene) ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,3-Dichlorobenzene ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,1-Dichloropropene ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 2-Hexanone ug/kg U 4.1 2014B2 (0-5) BJ81786 SW8260 8/29/15 1 2,2-Dichloropropane ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,1,1,2-Tetrachloroethane ug/kg U 0.81 1614B2 (0-5) BJ81786 SW8260 8/29/15 1 Chloroform ug/kg U 0.41 4.1

Page 24 of 82



SDG: GBJ81780



14B2 (0-5) BJ81786 SW8260 8/29/15 1 Benzene 0.42 ug/kg J 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,1,1-Trichloroethane ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Chloromethane ug/kg U 0.81 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Dibromomethane ug/kg U 0.81 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Bromochloromethane ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Vinyl Chloride ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Carbon Disulfide ug/kg U 0.81 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Bromoform ug/kg U 0.81 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,1-Dichloroethane ug/kg U 0.81 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,1-Dichloroethene ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Tert-Butyl Alcohol ug/kg U 16 8114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,1,2-Trichloro-1,2,2-Trifluoroethane ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,2-Dichloropropane ug/kg U 0.81 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,1,2-Trichloroethane ug/kg U 0.81 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,1,2,2-Tetrachloroethane ug/kg U 0.81 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,2,3-Trichlorobenzene ug/kg U 0.81 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Hexachlorobutadiene ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Naphthalene 0.90 ug/kg J 0.81 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 O-Xylene (1,2-Dimethylbenzene) ug/kg U 0.81 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 2-Chlorotoluene ug/kg U 0.81 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,2-Dichlorobenzene ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,2,4-Trimethylbenzene 0.43 ug/kg J 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,2-Dibromo-3-Chloropropane ug/kg U 0.81 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 1,2,3-Trichloropropane ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 T-Butylbenzene ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Isopropylbenzene (Cumene) ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Cymene 0.72 ug/kg J 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 50 Trichloroethylene (TCE) 65 ug/kg J 29 29014B2 (0-5) BJ81786 SW8270 8/27/15 1 4-Nitroaniline ug/kg U 120 74014B2 (0-5) BJ81786 SW8270 8/27/15 1 4-Nitrophenol ug/kg U 170 37014B2 (0-5) BJ81786 SW8270 8/27/15 1 4-Bromophenyl Phenyl Ether ug/kg U 110 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 2,4-Dimethylphenol ug/kg U 91 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 1,4-Dichlorobenzene ug/kg U 110 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 4-Chloroaniline ug/kg U 170 30014B2 (0-5) BJ81786 SW8270 8/27/15 1 Phenol ug/kg U 120 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Pyridine ug/kg U 91 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Bis(2-Chloroethyl) Ether (2-Chloroethyl Ether) ug/kg U 100 260

Page 25 of 82



SDG: GBJ81780



14B2 (0-5) BJ81786 SW8270 8/27/15 1 Bis(2-Chloroethoxy) Methane ug/kg U 100 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Bis(2-Ethylhexyl) Phthalate ug/kg U 110 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Di-N-Octylphthalate ug/kg U 95 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Hexachlorobenzene ug/kg U 110 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Anthracene 300 ug/kg 120 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 1,2,4-Trichlorobenzene ug/kg U 110 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 2,4-Dichlorophenol ug/kg U 130 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 2,4-Dinitrotoluene ug/kg U 150 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 1,2-Diphenylhydrazine ug/kg U 120 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Pyrene 1200 ug/kg 130 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Dimethyl Phthalate ug/kg U 110 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Dibenzofuran 140 ug/kg J 110 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Benzo(G,H,I)Perylene 500 ug/kg 120 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Indeno(1,2,3-C,D)Pyrene 570 ug/kg 120 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Benzo(B)Fluoranthene 750 ug/kg 130 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Fluoranthene 1300 ug/kg 120 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Benzo(K)Fluoranthene 620 ug/kg 120 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Acenaphthylene 120 ug/kg J 100 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Chrysene 820 ug/kg 120 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 2,2-Oxybis(2-Chloropropane) ug/kg U 100 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Benzo(A)Pyrene 810 ug/kg 120 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 2,4-Dinitrophenol ug/kg UJ 260 74014B2 (0-5) BJ81786 SW8270 8/27/15 1 4,6-Dinitro-2-Methylphenol ug/kg UJ 400 180014B2 (0-5) BJ81786 SW8270 8/27/15 1 Dibenz(A,H)Anthracene 170 ug/kg J 120 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 1,3-Dichlorobenzene ug/kg U 110 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Benzo(A)Anthracene 820 ug/kg 120 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 4-Chloro-3-Methylphenol ug/kg U 130 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 2,6-Dinitrotoluene ug/kg U 120 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 N-Nitrosodi-N-Propylamine ug/kg U 120 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Aniline ug/kg U 300 30014B2 (0-5) BJ81786 SW8270 8/27/15 1 N-Nitrosodimethylamine ug/kg U 100 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Benzoic Acid ug/kg R 740 180014B2 (0-5) BJ81786 SW8270 8/27/15 1 Hexachloroethane ug/kg U 110 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 4-Chlorophenyl Phenyl Ether ug/kg U 120 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Hexachlorocyclopentadiene ug/kg UJ 110 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Isophorone ug/kg U 100 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Pentachloronitrobenzene ug/kg U 140 260

Page 26 of 82



SDG: GBJ81780



14B2 (0-5) BJ81786 SW8270 8/27/15 1 Acenaphthene ug/kg U 110 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Diethyl Phthalate ug/kg U 120 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Di-N-Butyl Phthalate ug/kg U 98 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Phenanthrene 1100 ug/kg 110 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Benzyl Butyl Phthalate ug/kg U 95 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 N-Nitrosodiphenylamine ug/kg U 140 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Fluorene 150 ug/kg J 120 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Carbazole ug/kg U 280 180014B2 (0-5) BJ81786 SW8270 8/27/15 1 Hexachlorobutadiene ug/kg U 130 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Pentachlorophenol ug/kg UJ 140 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 2,4,6-Trichlorophenol ug/kg U 120 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 2-Nitroaniline ug/kg U 370 74014B2 (0-5) BJ81786 SW8270 8/27/15 1 2-Nitrophenol ug/kg U 230 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Naphthalene 230 ug/kg J 110 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 2-Methylnaphthalene 130 ug/kg J 110 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 2-Chloronaphthalene ug/kg U 100 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 3,3'-Dichlorobenzidine ug/kg U 170 74014B2 (0-5) BJ81786 SW8270 8/27/15 1 2-Methylphenol (O-Cresol) ug/kg U 170 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 1,2-Dichlorobenzene ug/kg U 100 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 2-Chlorophenol ug/kg U 100 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 1,2,4,5-Tetrachlorobenzene ug/kg U 130 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 2,4,5-Trichlorophenol ug/kg U 200 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Acetophenone ug/kg U 120 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 Nitrobenzene ug/kg U 130 26014B2 (0-5) BJ81786 SW8270 8/27/15 1 3-Nitroaniline ug/kg U 740 74014B2 (0-5) BJ81786 SW8270 8/27/15 1 3- And 4- Methylphenol (Total) ug/kg U 150 26014B2 (0-5) BJ81786 SW8260 8/29/15 1 Bromomethane ug/kg U 1.6 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Carbon Tetrachloride ug/kg U 0.81 4.114B2 (0-5) BJ81786 SW8270 8/27/15 1 Benzidine ug/kg UJ 220 74014B2 (0-5) BJ81786 SW8260 8/29/15 1 Methylene Chloride ug/kg U 4.1 4.114B2 (0-5) BJ81786 SW6010 8/28/15 1 Potassium 1220 mg/kg J+ 2.5 714B2 (0-5) BJ81786 SW6010 8/28/15 1 Zinc 66.3 mg/kg J+ 0.33 0.714B2 (0-5) BJ81786 SW8260 8/29/15 1 Chloroethane ug/kg UJ 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Methyl Ethyl Ketone (2-Butanone) ug/kg U 4.1 2414B2 (0-5) BJ81786 SW8260 8/29/15 1 Dichlorodifluoromethane ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Trans-1,3-Dichloropropene ug/kg U 0.41 4.114B2 (0-5) BJ81786 SW8260 8/29/15 1 Trichlorofluoromethane ug/kg UJ 0.81 4.1

Page 27 of 82



SDG: GBJ81780



14B2 (20-25) BJ81788 SW8260 8/29/15 1 Acetone ug/kg UJ 4.4 4414B2 (20-25) BJ81788 SW6010 8/28/15 10 Iron 24100 mg/kg 37 3714B2 (20-25) BJ81788 SW8260 8/29/15 1 Bromodichloromethane ug/kg U 0.87 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Bromomethane ug/kg U 1.7 4.414B2 (20-25) BJ81788 E160.3 8/26/15 1 Solids, Percent 85 %14B2 (20-25) BJ81788 SW6010 8/28/15 10 Aluminum 9510 mg/kg 7.4 3714B2 (20-25) BJ81788 SW6010 8/28/15 10 Manganese 367 mg/kg 3.7 3.714B2 (20-25) BJ81788 SW6010 8/28/15 1 Lead 7.2 mg/kg 0.37 0.714B2 (20-25) BJ81788 SW6010 8/28/15 1 Magnesium 4020 mg/kg 3.7 3.714B2 (20-25) BJ81788 SW6010 8/28/15 1 Nickel 17.5 mg/kg 0.37 0.3714B2 (20-25) BJ81788 SW6010 8/28/15 1 Silver mg/kg U 0.37 0.3714B2 (20-25) BJ81788 SW6010 8/28/15 1 Sodium 368 mg/kg 3.2 714B2 (20-25) BJ81788 SW6010 8/28/15 1 Thallium mg/kg U 1.5 1.514B2 (20-25) BJ81788 SW6010 8/28/15 1 Antimony mg/kg U 1.9 1.914B2 (20-25) BJ81788 SW6010 8/28/15 1 Arsenic 1.5 mg/kg 0.74 0.714B2 (20-25) BJ81788 SW6010 8/28/15 1 Barium 81.4 mg/kg 0.37 0.714B2 (20-25) BJ81788 SW6010 8/28/15 1 Beryllium 0.61 mg/kg 0.15 0.3014B2 (20-25) BJ81788 SW6010 8/28/15 1 Cadmium mg/kg U 0.15 0.3714B2 (20-25) BJ81788 SW6010 8/28/15 1 Chromium, Total 22.7 mg/kg 0.37 0.3714B2 (20-25) BJ81788 SW6010 8/28/15 1 Cobalt 10.3 mg/kg 0.37 0.3714B2 (20-25) BJ81788 SW6010 8/28/15 1 Copper 21.5 mg/kg 0.37 0.3714B2 (20-25) BJ81788 SW6010 8/28/15 1 Vanadium 34.7 mg/kg 0.37 0.414B2 (20-25) BJ81788 SW6010 8/28/15 1 Calcium 2210 mg/kg 3.4 3.714B2 (20-25) BJ81788 SW6010 8/28/15 1 Selenium mg/kg U 1.3 1.514B2 (20-25) BJ81788 SW7471 8/27/15 1 Mercury mg/kg U 0.02 0.0314B2 (20-25) BJ81788 SW8081 8/28/15 2 Heptachlor Epoxide ug/kg U 7.7 7.714B2 (20-25) BJ81788 SW8081 8/28/15 2 Endosulfan Sulfate ug/kg U 7.7 7.714B2 (20-25) BJ81788 SW8081 8/28/15 2 Aldrin ug/kg U 3.9 3.914B2 (20-25) BJ81788 SW8081 8/28/15 2 Alpha Bhc (Alpha Hexachlorocyclohexane) ug/kg U 7.7 7.714B2 (20-25) BJ81788 SW8081 8/28/15 2 Beta Bhc (Beta Hexachlorocyclohexane) ug/kg U 7.7 7.714B2 (20-25) BJ81788 SW8081 8/28/15 2 Delta BHC (Delta Hexachlorocyclohexane) ug/kg U 7.7 7.714B2 (20-25) BJ81788 SW8081 8/28/15 2 Beta Endosulfan ug/kg U 7.7 7.714B2 (20-25) BJ81788 SW8081 8/28/15 2 P,P'-DDT ug/kg U 2.3 2.314B2 (20-25) BJ81788 SW8081 8/28/15 2 cis-Chlordane ug/kg U 3.9 3.914B2 (20-25) BJ81788 SW8081 8/28/15 2 trans-Chlordane ug/kg U 3.9 3.914B2 (20-25) BJ81788 SW8081 8/28/15 2 Endrin Ketone ug/kg U 7.7 7.714B2 (20-25) BJ81788 SW8081 8/28/15 2 Gamma Bhc (Lindane) ug/kg U 1.5 1.5

Page 28 of 82



SDG: GBJ81780



14B2 (20-25) BJ81788 SW8081 8/28/15 2 Dieldrin ug/kg U 3.9 3.914B2 (20-25) BJ81788 SW8081 8/28/15 2 Endrin ug/kg U 7.7 7.714B2 (20-25) BJ81788 SW8081 8/28/15 2 Methoxychlor ug/kg U 39 3914B2 (20-25) BJ81788 SW8081 8/28/15 2 P,P'-DDD ug/kg U 2.3 2.314B2 (20-25) BJ81788 SW8081 8/28/15 2 P,P'-DDE ug/kg U 2.3 2.314B2 (20-25) BJ81788 SW8081 8/28/15 2 Endrin Aldehyde ug/kg U 7.7 7.714B2 (20-25) BJ81788 SW8081 8/28/15 2 Heptachlor ug/kg U 7.7 7.714B2 (20-25) BJ81788 SW8081 8/28/15 2 Toxaphene ug/kg U 150 15014B2 (20-25) BJ81788 SW8081 8/28/15 2 Alpha Endosulfan ug/kg U 7.7 7.714B2 (20-25) BJ81788 SW8082 8/29/15 2 PCB-1260 (Aroclor 1260) ug/kg U 39 3914B2 (20-25) BJ81788 SW8082 8/29/15 2 PCB-1254 (Aroclor 1254) ug/kg U 39 3914B2 (20-25) BJ81788 SW8082 8/29/15 2 PCB-1268 (Aroclor 1268) ug/kg U 39 3914B2 (20-25) BJ81788 SW8082 8/29/15 2 PCB-1221 (Aroclor 1221) ug/kg U 39 3914B2 (20-25) BJ81788 SW8082 8/29/15 2 PCB-1232 (Aroclor 1232) ug/kg U 39 3914B2 (20-25) BJ81788 SW8082 8/29/15 2 PCB-1248 (Aroclor 1248) ug/kg U 39 3914B2 (20-25) BJ81788 SW8082 8/29/15 2 PCB-1016 (Aroclor 1016) ug/kg U 39 3914B2 (20-25) BJ81788 SW8082 8/29/15 2 PCB-1262 (Aroclor 1262) ug/kg U 39 3914B2 (20-25) BJ81788 SW8082 8/29/15 2 PCB-1242 (Aroclor 1242) ug/kg U 39 3914B2 (20-25) BJ81788 SW8260 8/29/15 1 Ethylbenzene ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Styrene ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Cis-1,3-Dichloropropene ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 N-Propylbenzene ug/kg U 0.78 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 N-Butylbenzene ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 4-Chlorotoluene ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 1,4-Dichlorobenzene ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 1,2-Dibromoethane (Ethylene Dibromide) ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Acrolein ug/kg U 2.2 1714B2 (20-25) BJ81788 SW8260 8/29/15 1 1,2-Dichloroethane ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Acrylonitrile ug/kg U 0.44 1714B2 (20-25) BJ81788 SW8260 8/29/15 1 Methyl Isobutyl Ketone (4-Methyl-2-Pentanone) ug/kg U 4.4 2214B2 (20-25) BJ81788 SW8260 8/29/15 1 1,3,5-Trimethylbenzene (Mesitylene) ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Bromobenzene ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Toluene ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Chlorobenzene ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Tetrahydrofuran ug/kg U 2.2 8.714B2 (20-25) BJ81788 SW8260 8/29/15 1 Trans-1,4-Dichloro-2-Butene ug/kg U 2.2 8.714B2 (20-25) BJ81788 SW8260 8/29/15 1 1,2,4-Trichlorobenzene ug/kg U 0.87 4.4

Page 29 of 82



SDG: GBJ81780



14B2 (20-25) BJ81788 SW8260 8/29/15 1 1,4-Dioxane (P-Dioxane) ug/kg U 35 8714B2 (20-25) BJ81788 SW8260 8/29/15 1 Dibromochloromethane ug/kg U 0.87 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Tetrachloroethylene (PCE) ug/kg U 0.87 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Sec-Butylbenzene ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 1,3-Dichloropropane ug/kg U 0.87 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Trans-1,2-Dichloroethene 2.6 ug/kg J 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Tert-Butyl Methyl Ether ug/kg U 0.87 8.714B2 (20-25) BJ81788 SW8260 8/29/15 1 m,p-Xylene ug/kg U 0.87 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 O-Cymene (O-Isopropyltoluene) ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 1,3-Dichlorobenzene ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 1,1-Dichloropropene ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 2-Hexanone ug/kg U 4.4 2214B2 (20-25) BJ81788 SW8260 8/29/15 1 2,2-Dichloropropane ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 1,1,1,2-Tetrachloroethane ug/kg U 0.87 1714B2 (20-25) BJ81788 SW8260 8/29/15 1 Chloroform ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Benzene 1.0 ug/kg J 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 1,1,1-Trichloroethane ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Chloromethane ug/kg U 0.87 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Dibromomethane ug/kg U 0.87 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Bromochloromethane ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Vinyl Chloride 2.6 ug/kg J 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Carbon Disulfide ug/kg U 0.87 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Bromoform ug/kg U 0.87 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 1,1-Dichloroethane ug/kg U 0.87 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 1,1-Dichloroethene 0.50 ug/kg J 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Tert-Butyl Alcohol ug/kg U 17 8714B2 (20-25) BJ81788 SW8260 8/29/15 1 1,1,2-Trichloro-1,2,2-Trifluoroethane ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 1,2-Dichloropropane ug/kg U 0.87 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 1,1,2-Trichloroethane ug/kg U 0.87 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 1,1,2,2-Tetrachloroethane ug/kg U 0.87 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 1,2,3-Trichlorobenzene ug/kg U 0.87 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Hexachlorobutadiene ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Naphthalene ug/kg U 0.87 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 O-Xylene (1,2-Dimethylbenzene) ug/kg U 0.87 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 2-Chlorotoluene ug/kg U 0.87 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 1,2-Dichlorobenzene ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 1,2,4-Trimethylbenzene ug/kg U 0.44 4.4

Page 30 of 82



SDG: GBJ81780



14B2 (20-25) BJ81788 SW8260 8/29/15 1 1,2-Dibromo-3-Chloropropane ug/kg U 0.87 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 1,2,3-Trichloropropane ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 T-Butylbenzene ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Isopropylbenzene (Cumene) ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Cymene ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 50 Cis-1,2-Dichloroethylene 62 ug/kg J 35 25014B2 (20-25) BJ81788 SW8260 8/29/15 50 Trichloroethylene (TCE) 41 ug/kg J 35 35014B2 (20-25) BJ81788 SW8270 8/27/15 1 4-Nitroaniline ug/kg U 130 78014B2 (20-25) BJ81788 SW8270 8/27/15 1 4-Nitrophenol ug/kg U 180 39014B2 (20-25) BJ81788 SW8270 8/27/15 1 4-Bromophenyl Phenyl Ether ug/kg U 110 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 2,4-Dimethylphenol ug/kg U 96 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 1,4-Dichlorobenzene ug/kg U 120 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 4-Chloroaniline ug/kg U 180 31014B2 (20-25) BJ81788 SW8270 8/27/15 1 Phenol ug/kg U 120 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Pyridine ug/kg U 96 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Bis(2-Chloroethyl) Ether (2-Chloroethyl Ether) ug/kg U 100 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Bis(2-Chloroethoxy) Methane ug/kg U 110 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Bis(2-Ethylhexyl) Phthalate ug/kg U 110 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Di-N-Octylphthalate ug/kg U 100 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Hexachlorobenzene ug/kg U 110 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Anthracene ug/kg U 130 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 1,2,4-Trichlorobenzene ug/kg U 120 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 2,4-Dichlorophenol ug/kg U 140 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 2,4-Dinitrotoluene ug/kg U 150 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 1,2-Diphenylhydrazine ug/kg U 130 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Pyrene ug/kg U 130 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Dimethyl Phthalate ug/kg U 120 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Dibenzofuran ug/kg U 110 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Benzo(G,H,I)Perylene ug/kg U 130 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Indeno(1,2,3-C,D)Pyrene ug/kg U 130 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Benzo(B)Fluoranthene ug/kg U 130 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Fluoranthene ug/kg U 130 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Benzo(K)Fluoranthene ug/kg U 130 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Acenaphthylene ug/kg U 110 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Chrysene ug/kg U 130 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 2,2-Oxybis(2-Chloropropane) ug/kg U 110 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Benzo(A)Pyrene ug/kg U 130 270

Page 31 of 82



SDG: GBJ81780



14B2 (20-25) BJ81788 SW8270 8/27/15 1 2,4-Dinitrophenol ug/kg UJ 270 78014B2 (20-25) BJ81788 SW8270 8/27/15 1 4,6-Dinitro-2-Methylphenol ug/kg UJ 420 190014B2 (20-25) BJ81788 SW8270 8/27/15 1 Dibenz(A,H)Anthracene ug/kg U 130 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 1,3-Dichlorobenzene ug/kg U 120 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Benzo(A)Anthracene ug/kg U 130 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 4-Chloro-3-Methylphenol ug/kg U 140 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 2,6-Dinitrotoluene ug/kg U 120 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 N-Nitrosodi-N-Propylamine ug/kg U 130 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Aniline ug/kg U 310 31014B2 (20-25) BJ81788 SW8270 8/27/15 1 N-Nitrosodimethylamine ug/kg U 110 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Benzoic Acid ug/kg R 780 190014B2 (20-25) BJ81788 SW8270 8/27/15 1 Hexachloroethane ug/kg U 120 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 4-Chlorophenyl Phenyl Ether ug/kg U 130 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Hexachlorocyclopentadiene ug/kg UJ 120 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Isophorone ug/kg U 110 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Pentachloronitrobenzene ug/kg U 140 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Acenaphthene ug/kg U 120 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Diethyl Phthalate ug/kg U 120 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Di-N-Butyl Phthalate ug/kg U 100 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Phenanthrene ug/kg U 110 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Benzyl Butyl Phthalate ug/kg U 100 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 N-Nitrosodiphenylamine ug/kg U 150 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Fluorene ug/kg U 130 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Carbazole ug/kg U 290 190014B2 (20-25) BJ81788 SW8270 8/27/15 1 Hexachlorobutadiene ug/kg U 140 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Pentachlorophenol ug/kg UJ 150 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 2,4,6-Trichlorophenol ug/kg U 120 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 2-Nitroaniline ug/kg U 390 78014B2 (20-25) BJ81788 SW8270 8/27/15 1 2-Nitrophenol ug/kg U 250 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Naphthalene ug/kg U 110 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 2-Methylnaphthalene ug/kg U 120 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 2-Chloronaphthalene ug/kg U 110 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 3,3'-Dichlorobenzidine ug/kg U 180 78014B2 (20-25) BJ81788 SW8270 8/27/15 1 2-Methylphenol (O-Cresol) ug/kg U 180 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 1,2-Dichlorobenzene ug/kg U 110 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 2-Chlorophenol ug/kg U 110 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 1,2,4,5-Tetrachlorobenzene ug/kg U 140 270

Page 32 of 82



SDG: GBJ81780



14B2 (20-25) BJ81788 SW8270 8/27/15 1 2,4,5-Trichlorophenol ug/kg U 210 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Acetophenone ug/kg U 120 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 Nitrobenzene ug/kg U 140 27014B2 (20-25) BJ81788 SW8270 8/27/15 1 3-Nitroaniline ug/kg U 780 78014B2 (20-25) BJ81788 SW8270 8/27/15 1 3- And 4- Methylphenol (Total) ug/kg U 150 27014B2 (20-25) BJ81788 SW8260 8/29/15 1 Carbon Tetrachloride ug/kg U 0.87 4.414B2 (20-25) BJ81788 SW6010 8/28/15 1 Potassium 2830 mg/kg J+ 2.9 714B2 (20-25) BJ81788 SW8260 8/29/15 1 Methylene Chloride ug/kg U 4.4 4.414B2 (20-25) BJ81788 SW8270 8/27/15 1 Benzidine ug/kg UJ 230 78014B2 (20-25) BJ81788 SW6010 8/28/15 1 Zinc 47.3 mg/kg J+ 0.37 0.714B2 (20-25) BJ81788 SW8260 8/29/15 1 Chloroethane ug/kg UJ 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Dichlorodifluoromethane 0.88 ug/kg J 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Trans-1,3-Dichloropropene ug/kg U 0.44 4.414B2 (20-25) BJ81788 SW8260 8/29/15 1 Methyl Ethyl Ketone (2-Butanone) ug/kg U 4.4 2614B2 (20-25) BJ81788 SW8260 8/29/15 1 Trichlorofluoromethane ug/kg UJ 0.87 4.414B1 (0-5) BJ81789 E160.3 8/26/15 1 Solids, Percent 90 %14B1 (0-5) BJ81789 SW6010 8/28/15 10 Aluminum 8460 mg/kg 6.6 3314B1 (0-5) BJ81789 SW6010 8/28/15 10 Iron 17900 mg/kg 33 3314B1 (0-5) BJ81789 SW6010 8/28/15 10 Manganese 356 mg/kg 3.3 3.314B1 (0-5) BJ81789 SW6010 8/28/15 1 Lead 102 mg/kg 0.33 0.714B1 (0-5) BJ81789 SW6010 8/28/15 1 Magnesium 2530 mg/kg 3.3 3.314B1 (0-5) BJ81789 SW6010 8/28/15 1 Nickel 36.3 mg/kg 0.33 0.3314B1 (0-5) BJ81789 SW6010 8/28/15 1 Silver mg/kg U 0.33 0.3314B1 (0-5) BJ81789 SW6010 8/28/15 1 Sodium 290 mg/kg 2.8 714B1 (0-5) BJ81789 SW6010 8/28/15 1 Thallium mg/kg U 1.3 1.314B1 (0-5) BJ81789 SW6010 8/28/15 1 Antimony mg/kg U 1.7 1.714B1 (0-5) BJ81789 SW6010 8/28/15 1 Arsenic 3.6 mg/kg 0.66 0.714B1 (0-5) BJ81789 SW6010 8/28/15 1 Barium 72.0 mg/kg 0.33 0.714B1 (0-5) BJ81789 SW6010 8/28/15 1 Beryllium 0.45 mg/kg 0.13 0.2614B1 (0-5) BJ81789 SW6010 8/28/15 1 Cadmium 0.59 mg/kg 0.13 0.3314B1 (0-5) BJ81789 SW6010 8/28/15 1 Chromium, Total 31.3 mg/kg 0.33 0.3314B1 (0-5) BJ81789 SW6010 8/28/15 1 Cobalt 8.27 mg/kg 0.33 0.3314B1 (0-5) BJ81789 SW6010 8/28/15 1 Copper 25.1 mg/kg 0.33 0.3314B1 (0-5) BJ81789 SW6010 8/28/15 1 Vanadium 25.0 mg/kg 0.33 0.314B1 (0-5) BJ81789 SW6010 8/28/15 1 Calcium 5560 mg/kg 3.0 3.314B1 (0-5) BJ81789 SW6010 8/28/15 1 Selenium mg/kg U 1.1 1.314B1 (0-5) BJ81789 SW7471 8/27/15 1 Mercury 0.58 mg/kg 0.02 0.03

Page 33 of 82



SDG: GBJ81780



14B1 (0-5) BJ81789 SW8081 8/28/15 10 Heptachlor Epoxide ug/kg U 37 3714B1 (0-5) BJ81789 SW8081 8/28/15 10 Endosulfan Sulfate ug/kg U 37 3714B1 (0-5) BJ81789 SW8081 8/28/15 10 Aldrin ug/kg U 5.5 5.514B1 (0-5) BJ81789 SW8081 8/28/15 10 Alpha Bhc (Alpha Hexachlorocyclohexane) ug/kg U 18 1814B1 (0-5) BJ81789 SW8081 8/28/15 10 Beta Bhc (Beta Hexachlorocyclohexane) ug/kg U 18 1814B1 (0-5) BJ81789 SW8081 8/28/15 10 Delta BHC (Delta Hexachlorocyclohexane) ug/kg U 37 3714B1 (0-5) BJ81789 SW8081 8/28/15 10 Beta Endosulfan ug/kg U 37 3714B1 (0-5) BJ81789 SW8081 8/28/15 10 P,P'-DDT ug/kg U 9.1 9.114B1 (0-5) BJ81789 SW8081 8/28/15 10 cis-Chlordane 68 ug/kg 18 1814B1 (0-5) BJ81789 SW8081 8/28/15 10 trans-Chlordane 52 ug/kg 18 1814B1 (0-5) BJ81789 SW8081 8/28/15 10 Endrin Ketone ug/kg U 37 3714B1 (0-5) BJ81789 SW8081 8/28/15 10 Gamma Bhc (Lindane) ug/kg U 7.3 7.314B1 (0-5) BJ81789 SW8081 8/28/15 10 Dieldrin ug/kg U 5.5 5.514B1 (0-5) BJ81789 SW8081 8/28/15 10 Endrin ug/kg U 18 1814B1 (0-5) BJ81789 SW8081 8/28/15 10 Methoxychlor ug/kg U 180 18014B1 (0-5) BJ81789 SW8081 8/28/15 10 P,P'-DDD ug/kg U 9.1 9.114B1 (0-5) BJ81789 SW8081 8/28/15 10 P,P'-DDE ug/kg U 9.1 9.114B1 (0-5) BJ81789 SW8081 8/28/15 10 Endrin Aldehyde ug/kg U 37 3714B1 (0-5) BJ81789 SW8081 8/28/15 10 Heptachlor ug/kg U 37 3714B1 (0-5) BJ81789 SW8081 8/28/15 10 Toxaphene ug/kg U 730 73014B1 (0-5) BJ81789 SW8081 8/28/15 10 Alpha Endosulfan ug/kg U 37 3714B1 (0-5) BJ81789 SW8082 8/29/15 2 PCB-1260 (Aroclor 1260) ug/kg U 37 3714B1 (0-5) BJ81789 SW8082 8/29/15 2 PCB-1254 (Aroclor 1254) ug/kg U 37 3714B1 (0-5) BJ81789 SW8082 8/29/15 2 PCB-1268 (Aroclor 1268) ug/kg U 37 3714B1 (0-5) BJ81789 SW8082 8/29/15 2 PCB-1221 (Aroclor 1221) ug/kg U 37 3714B1 (0-5) BJ81789 SW8082 8/29/15 2 PCB-1232 (Aroclor 1232) ug/kg U 37 3714B1 (0-5) BJ81789 SW8082 8/29/15 2 PCB-1248 (Aroclor 1248) ug/kg U 37 3714B1 (0-5) BJ81789 SW8082 8/29/15 2 PCB-1016 (Aroclor 1016) ug/kg U 37 3714B1 (0-5) BJ81789 SW8082 8/29/15 2 PCB-1262 (Aroclor 1262) ug/kg U 37 3714B1 (0-5) BJ81789 SW8082 8/29/15 2 PCB-1242 (Aroclor 1242) ug/kg U 37 3714B1 (0-5) BJ81789 SW8260 8/29/15 1 Ethylbenzene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Styrene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Cis-1,3-Dichloropropene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 N-Propylbenzene ug/kg U 0.89 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 N-Butylbenzene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 4-Chlorotoluene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 1,4-Dichlorobenzene ug/kg U 0.49 4.9

Page 34 of 82



SDG: GBJ81780



14B1 (0-5) BJ81789 SW8260 8/29/15 1 1,2-Dibromoethane (Ethylene Dibromide) ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Acrolein ug/kg U 2.5 2014B1 (0-5) BJ81789 SW8260 8/29/15 1 1,2-Dichloroethane ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Acrylonitrile ug/kg U 0.49 2014B1 (0-5) BJ81789 SW8260 8/29/15 1 Methyl Isobutyl Ketone (4-Methyl-2-Pentanone) ug/kg U 4.9 2514B1 (0-5) BJ81789 SW8260 8/29/15 1 1,3,5-Trimethylbenzene (Mesitylene) ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Bromobenzene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Toluene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Chlorobenzene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Tetrahydrofuran ug/kg U 2.5 9.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Trans-1,4-Dichloro-2-Butene ug/kg U 2.5 9.914B1 (0-5) BJ81789 SW8260 8/29/15 1 1,2,4-Trichlorobenzene ug/kg U 0.99 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 1,4-Dioxane (P-Dioxane) ug/kg U 40 9914B1 (0-5) BJ81789 SW8260 8/29/15 1 Dibromochloromethane ug/kg U 0.99 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Tetrachloroethylene (PCE) ug/kg U 0.99 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Sec-Butylbenzene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 1,3-Dichloropropane ug/kg U 0.99 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Cis-1,2-Dichloroethylene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Trans-1,2-Dichloroethene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Tert-Butyl Methyl Ether ug/kg U 0.99 9.914B1 (0-5) BJ81789 SW8260 8/29/15 1 m,p-Xylene ug/kg U 0.99 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 O-Cymene (O-Isopropyltoluene) ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 1,3-Dichlorobenzene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 1,1-Dichloropropene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 2-Hexanone ug/kg U 4.9 2514B1 (0-5) BJ81789 SW8260 8/29/15 1 2,2-Dichloropropane ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 1,1,1,2-Tetrachloroethane ug/kg U 0.99 2014B1 (0-5) BJ81789 SW8260 8/29/15 1 Chloroform ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Benzene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 1,1,1-Trichloroethane ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Chloromethane ug/kg U 0.99 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Dibromomethane ug/kg U 0.99 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Bromochloromethane ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Vinyl Chloride ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Carbon Disulfide ug/kg U 0.99 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Bromoform ug/kg U 0.99 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 1,1-Dichloroethane ug/kg U 0.99 4.9

Page 35 of 82



SDG: GBJ81780



14B1 (0-5) BJ81789 SW8260 8/29/15 1 1,1-Dichloroethene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Tert-Butyl Alcohol ug/kg U 20 9914B1 (0-5) BJ81789 SW8260 8/29/15 1 1,1,2-Trichloro-1,2,2-Trifluoroethane ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 1,2-Dichloropropane ug/kg U 0.99 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Methyl Ethyl Ketone (2-Butanone) ug/kg U 4.9 3014B1 (0-5) BJ81789 SW8260 8/29/15 1 1,1,2-Trichloroethane ug/kg U 0.99 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Trichloroethylene (TCE) 1.7 ug/kg J 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 1,1,2,2-Tetrachloroethane ug/kg U 0.99 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 1,2,3-Trichlorobenzene ug/kg U 0.99 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Hexachlorobutadiene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Naphthalene ug/kg U 0.99 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 O-Xylene (1,2-Dimethylbenzene) ug/kg U 0.99 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 2-Chlorotoluene ug/kg U 0.99 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 1,2-Dichlorobenzene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 1,2,4-Trimethylbenzene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 1,2-Dibromo-3-Chloropropane ug/kg U 0.99 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 1,2,3-Trichloropropane ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 T-Butylbenzene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Isopropylbenzene (Cumene) ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Cymene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8270 8/27/15 1 4-Nitroaniline ug/kg U 120 73014B1 (0-5) BJ81789 SW8270 8/27/15 1 4-Nitrophenol ug/kg U 160 36014B1 (0-5) BJ81789 SW8270 8/27/15 1 4-Bromophenyl Phenyl Ether ug/kg U 110 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 2,4-Dimethylphenol ug/kg U 90 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 1,4-Dichlorobenzene 500 ug/kg 110 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 4-Chloroaniline ug/kg U 170 29014B1 (0-5) BJ81789 SW8270 8/27/15 1 Phenol ug/kg U 120 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Pyridine ug/kg U 89 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Bis(2-Chloroethyl) Ether (2-Chloroethyl Ether) ug/kg U 98 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Bis(2-Chloroethoxy) Methane ug/kg U 100 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Bis(2-Ethylhexyl) Phthalate ug/kg U 100 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Di-N-Octylphthalate ug/kg U 94 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Hexachlorobenzene ug/kg U 110 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Anthracene 860 ug/kg 120 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 1,2,4-Trichlorobenzene ug/kg U 110 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 2,4-Dichlorophenol ug/kg U 130 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 2,4-Dinitrotoluene ug/kg U 140 250

Page 36 of 82



SDG: GBJ81780



14B1 (0-5) BJ81789 SW8270 8/27/15 1 1,2-Diphenylhydrazine ug/kg U 120 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Pyrene 4100 ug/kg 130 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Dimethyl Phthalate ug/kg U 110 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Dibenzofuran 240 ug/kg J 110 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Benzo(G,H,I)Perylene 3000 ug/kg 120 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Indeno(1,2,3-C,D)Pyrene 3900 ug/kg 120 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Benzo(B)Fluoranthene 4500 ug/kg 120 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Fluoranthene 4300 ug/kg 120 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Benzo(K)Fluoranthene 3400 ug/kg 120 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Acenaphthylene 110 ug/kg J 100 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Chrysene 3300 ug/kg 120 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 2,2-Oxybis(2-Chloropropane) ug/kg U 100 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Benzo(A)Pyrene 3200 ug/kg 120 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 2,4-Dinitrophenol ug/kg UJ 250 73014B1 (0-5) BJ81789 SW8270 8/27/15 1 4,6-Dinitro-2-Methylphenol ug/kg UJ 390 180014B1 (0-5) BJ81789 SW8270 8/27/15 1 Dibenz(A,H)Anthracene 1400 ug/kg 120 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 1,3-Dichlorobenzene ug/kg U 110 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Benzo(A)Anthracene 3500 ug/kg 120 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 4-Chloro-3-Methylphenol ug/kg U 130 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 2,6-Dinitrotoluene ug/kg U 110 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 N-Nitrosodi-N-Propylamine ug/kg U 120 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Aniline ug/kg U 290 29014B1 (0-5) BJ81789 SW8270 8/27/15 1 N-Nitrosodimethylamine ug/kg U 100 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Benzoic Acid ug/kg R 730 180014B1 (0-5) BJ81789 SW8270 8/27/15 1 Hexachloroethane ug/kg U 110 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 4-Chlorophenyl Phenyl Ether ug/kg U 120 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Hexachlorocyclopentadiene ug/kg UJ 110 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Isophorone ug/kg U 100 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Pentachloronitrobenzene ug/kg U 140 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Acenaphthene ug/kg U 110 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Diethyl Phthalate ug/kg U 110 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Di-N-Butyl Phthalate ug/kg U 97 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Phenanthrene 2500 ug/kg 100 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Benzyl Butyl Phthalate ug/kg U 94 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 N-Nitrosodiphenylamine ug/kg U 140 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Fluorene 230 ug/kg J 120 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Carbazole 350 ug/kg J 280 1800

Page 37 of 82



SDG: GBJ81780



14B1 (0-5) BJ81789 SW8270 8/27/15 1 Hexachlorobutadiene ug/kg U 130 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Pentachlorophenol ug/kg UJ 140 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 2,4,6-Trichlorophenol ug/kg U 120 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 2-Nitroaniline ug/kg U 370 73014B1 (0-5) BJ81789 SW8270 8/27/15 1 2-Nitrophenol ug/kg U 230 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Naphthalene 240 ug/kg J 100 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 2-Methylnaphthalene ug/kg U 110 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 2-Chloronaphthalene ug/kg U 100 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 3,3'-Dichlorobenzidine ug/kg U 170 73014B1 (0-5) BJ81789 SW8270 8/27/15 1 2-Methylphenol (O-Cresol) ug/kg U 170 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 1,2-Dichlorobenzene ug/kg U 100 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 2-Chlorophenol ug/kg U 100 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 1,2,4,5-Tetrachlorobenzene ug/kg U 130 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 2,4,5-Trichlorophenol ug/kg U 200 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Acetophenone ug/kg U 110 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 Nitrobenzene ug/kg U 130 25014B1 (0-5) BJ81789 SW8270 8/27/15 1 3-Nitroaniline ug/kg U 730 73014B1 (0-5) BJ81789 SW8270 8/27/15 1 3- And 4- Methylphenol (Total) ug/kg U 140 25014B1 (0-5) BJ81789 SW8260 8/29/15 1 Acetone ug/kg UJ 4.9 4914B1 (0-5) BJ81789 SW8260 8/29/15 1 Bromodichloromethane ug/kg U 0.99 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Bromomethane ug/kg U 2.0 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Carbon Tetrachloride ug/kg U 0.99 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Methylene Chloride ug/kg U 4.9 4.914B1 (0-5) BJ81789 SW6010 8/28/15 1 Potassium 1420 mg/kg J+ 2.6 714B1 (0-5) BJ81789 SW8270 8/27/15 1 Benzidine ug/kg UJ 210 73014B1 (0-5) BJ81789 SW6010 8/28/15 1 Zinc 88.5 mg/kg J+ 0.33 0.714B1 (0-5) BJ81789 SW8260 8/29/15 1 Chloroethane ug/kg UJ 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Dichlorodifluoromethane ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Trans-1,3-Dichloropropene ug/kg U 0.49 4.914B1 (0-5) BJ81789 SW8260 8/29/15 1 Trichlorofluoromethane ug/kg UJ 0.99 4.914B3 (0-5) BJ81791 SW6010 8/28/15 10 Iron 13900 mg/kg 34 3414B3 (0-5) BJ81791 E160.3 8/26/15 1 Solids, Percent 91 %14B3 (0-5) BJ81791 SW6010 8/28/15 10 Aluminum 8780 mg/kg 6.9 3414B3 (0-5) BJ81791 SW6010 8/28/15 10 Manganese 252 mg/kg 3.4 3.414B3 (0-5) BJ81791 SW6010 8/28/15 1 Lead 29.9 mg/kg 0.34 0.714B3 (0-5) BJ81791 SW6010 8/28/15 1 Magnesium 2230 mg/kg 3.4 3.414B3 (0-5) BJ81791 SW6010 8/28/15 1 Nickel 17.3 mg/kg 0.34 0.34

Page 38 of 82



SDG: GBJ81780



14B3 (0-5) BJ81791 SW6010 8/28/15 1 Silver mg/kg U 0.34 0.3414B3 (0-5) BJ81791 SW6010 8/28/15 1 Sodium 157 mg/kg 3.0 714B3 (0-5) BJ81791 SW6010 8/28/15 1 Thallium mg/kg U 1.4 1.414B3 (0-5) BJ81791 SW6010 8/28/15 1 Antimony mg/kg U 1.7 1.714B3 (0-5) BJ81791 SW6010 8/28/15 1 Arsenic 2.4 mg/kg 0.69 0.714B3 (0-5) BJ81791 SW6010 8/28/15 1 Barium 54.2 mg/kg 0.34 0.714B3 (0-5) BJ81791 SW6010 8/28/15 1 Beryllium 0.39 mg/kg 0.14 0.2714B3 (0-5) BJ81791 SW6010 8/28/15 1 Cadmium mg/kg U 0.14 0.3414B3 (0-5) BJ81791 SW6010 8/28/15 1 Chromium, Total 17.5 mg/kg 0.34 0.3414B3 (0-5) BJ81791 SW6010 8/28/15 1 Cobalt 6.29 mg/kg 0.34 0.3414B3 (0-5) BJ81791 SW6010 8/28/15 1 Copper 21.5 mg/kg 0.34 0.3414B3 (0-5) BJ81791 SW6010 8/28/15 1 Vanadium 23.9 mg/kg 0.34 0.314B3 (0-5) BJ81791 SW6010 8/28/15 1 Calcium 3950 mg/kg 3.2 3.414B3 (0-5) BJ81791 SW6010 8/28/15 1 Selenium mg/kg U 1.2 1.414B3 (0-5) BJ81791 SW7471 8/27/15 1 Mercury 0.09 mg/kg 0.02 0.0314B3 (0-5) BJ81791 SW8081 8/28/15 10 Heptachlor Epoxide ug/kg U 36 3614B3 (0-5) BJ81791 SW8081 8/28/15 10 Endosulfan Sulfate ug/kg U 36 3614B3 (0-5) BJ81791 SW8081 8/28/15 10 Aldrin ug/kg U 18 1814B3 (0-5) BJ81791 SW8081 8/28/15 10 Alpha Bhc (Alpha Hexachlorocyclohexane) ug/kg U 36 3614B3 (0-5) BJ81791 SW8081 8/28/15 10 Beta Bhc (Beta Hexachlorocyclohexane) ug/kg U 36 3614B3 (0-5) BJ81791 SW8081 8/28/15 10 Delta BHC (Delta Hexachlorocyclohexane) ug/kg U 36 3614B3 (0-5) BJ81791 SW8081 8/28/15 10 Beta Endosulfan ug/kg U 36 3614B3 (0-5) BJ81791 SW8081 8/28/15 10 P,P'-DDT ug/kg U 11 1114B3 (0-5) BJ81791 SW8081 8/28/15 10 cis-Chlordane 130 ug/kg 18 1814B3 (0-5) BJ81791 SW8081 8/28/15 10 trans-Chlordane 160 ug/kg 18 1814B3 (0-5) BJ81791 SW8081 8/28/15 10 Endrin Ketone ug/kg U 36 3614B3 (0-5) BJ81791 SW8081 8/28/15 10 Chlordane ug/kg U 180 18014B3 (0-5) BJ81791 SW8081 8/28/15 10 Gamma Bhc (Lindane) ug/kg U 7.2 7.214B3 (0-5) BJ81791 SW8081 8/28/15 10 Dieldrin ug/kg U 18 1814B3 (0-5) BJ81791 SW8081 8/28/15 10 Endrin ug/kg U 36 3614B3 (0-5) BJ81791 SW8081 8/28/15 10 Methoxychlor ug/kg U 180 18014B3 (0-5) BJ81791 SW8081 8/28/15 10 P,P'-DDD ug/kg U 60 6014B3 (0-5) BJ81791 SW8081 8/28/15 10 P,P'-DDE ug/kg U 11 1114B3 (0-5) BJ81791 SW8081 8/28/15 10 Endrin Aldehyde ug/kg U 36 3614B3 (0-5) BJ81791 SW8081 8/28/15 10 Heptachlor ug/kg U 36 3614B3 (0-5) BJ81791 SW8081 8/28/15 10 Toxaphene ug/kg U 720 72014B3 (0-5) BJ81791 SW8081 8/28/15 10 Alpha Endosulfan ug/kg U 36 36

Page 39 of 82



SDG: GBJ81780



14B3 (0-5) BJ81791 SW8082 8/31/15 2 PCB-1260 (Aroclor 1260) ug/kg U 36 3614B3 (0-5) BJ81791 SW8082 8/31/15 2 PCB-1254 (Aroclor 1254) ug/kg U 36 3614B3 (0-5) BJ81791 SW8082 8/31/15 2 PCB-1268 (Aroclor 1268) ug/kg U 36 3614B3 (0-5) BJ81791 SW8082 8/31/15 2 PCB-1221 (Aroclor 1221) ug/kg U 36 3614B3 (0-5) BJ81791 SW8082 8/31/15 2 PCB-1232 (Aroclor 1232) ug/kg U 36 3614B3 (0-5) BJ81791 SW8082 8/31/15 2 PCB-1248 (Aroclor 1248) ug/kg U 36 3614B3 (0-5) BJ81791 SW8082 8/31/15 2 PCB-1016 (Aroclor 1016) ug/kg U 36 3614B3 (0-5) BJ81791 SW8082 8/31/15 2 PCB-1262 (Aroclor 1262) ug/kg U 36 3614B3 (0-5) BJ81791 SW8082 8/31/15 2 PCB-1242 (Aroclor 1242) ug/kg U 36 3614B3 (0-5) BJ81791 SW8260 8/31/15 1 Ethylbenzene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Styrene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Cis-1,3-Dichloropropene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Trans-1,3-Dichloropropene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 N-Propylbenzene ug/kg U 1.0 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 N-Butylbenzene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 4-Chlorotoluene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 1,4-Dichlorobenzene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 1,2-Dibromoethane (Ethylene Dibromide) ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Acrolein ug/kg U 2.9 2314B3 (0-5) BJ81791 SW8260 8/31/15 1 1,2-Dichloroethane ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Acrylonitrile ug/kg U 0.58 2314B3 (0-5) BJ81791 SW8260 8/31/15 1 Methyl Isobutyl Ketone (4-Methyl-2-Pentanone) ug/kg U 5.8 2914B3 (0-5) BJ81791 SW8260 8/31/15 1 1,3,5-Trimethylbenzene (Mesitylene) ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Bromobenzene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Toluene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Chlorobenzene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Tetrahydrofuran ug/kg U 2.9 1214B3 (0-5) BJ81791 SW8260 8/31/15 1 Trans-1,4-Dichloro-2-Butene ug/kg UJ 2.9 1214B3 (0-5) BJ81791 SW8260 8/31/15 1 1,2,4-Trichlorobenzene ug/kg U 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 1,4-Dioxane (P-Dioxane) ug/kg UJ 46 10014B3 (0-5) BJ81791 SW8260 8/31/15 1 Dibromochloromethane ug/kg UJ 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Tetrachloroethylene (PCE) ug/kg U 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Sec-Butylbenzene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 1,3-Dichloropropane ug/kg U 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Cis-1,2-Dichloroethylene 6.4 ug/kg 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Trans-1,2-Dichloroethene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Tert-Butyl Methyl Ether ug/kg U 1.2 12

Page 40 of 82



SDG: GBJ81780



14B3 (0-5) BJ81791 SW8260 8/31/15 1 m,p-Xylene ug/kg U 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 O-Cymene (O-Isopropyltoluene) ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 1,3-Dichlorobenzene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Carbon Tetrachloride ug/kg U 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 1,1-Dichloropropene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 2-Hexanone ug/kg UJ 5.8 2914B3 (0-5) BJ81791 SW8260 8/31/15 1 2,2-Dichloropropane ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 1,1,1,2-Tetrachloroethane ug/kg U 1.2 2314B3 (0-5) BJ81791 SW8260 8/31/15 1 Chloroform ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Benzene 0.59 ug/kg J 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 1,1,1-Trichloroethane ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Chloromethane ug/kg U 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Dibromomethane ug/kg U 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Bromochloromethane ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Chloroethane ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Vinyl Chloride 2.2 ug/kg J 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Carbon Disulfide ug/kg U 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Bromoform ug/kg UJ 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Bromodichloromethane ug/kg U 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 1,1-Dichloroethane ug/kg U 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 1,1-Dichloroethene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Tert-Butyl Alcohol ug/kg U 23 12014B3 (0-5) BJ81791 SW8260 8/31/15 1 Trichlorofluoromethane ug/kg UJ 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Dichlorodifluoromethane ug/kg UJ 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 1,1,2-Trichloro-1,2,2-Trifluoroethane ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 1,2-Dichloropropane ug/kg U 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 1,1,2-Trichloroethane ug/kg U 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Trichloroethylene (TCE) 2.1 ug/kg J 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 1,1,2,2-Tetrachloroethane ug/kg U 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 1,2,3-Trichlorobenzene ug/kg U 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Hexachlorobutadiene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Naphthalene ug/kg U 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 O-Xylene (1,2-Dimethylbenzene) ug/kg UJ 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 2-Chlorotoluene ug/kg U 1.2 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 1,2-Dichlorobenzene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 1,2,4-Trimethylbenzene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 1,2-Dibromo-3-Chloropropane ug/kg U 1.2 5.8

Page 41 of 82



SDG: GBJ81780



14B3 (0-5) BJ81791 SW8260 8/31/15 1 1,2,3-Trichloropropane ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 T-Butylbenzene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Isopropylbenzene (Cumene) ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8260 8/31/15 1 Cymene ug/kg U 0.58 5.814B3 (0-5) BJ81791 SW8270 8/27/15 1 4-Nitroaniline ug/kg U 120 71014B3 (0-5) BJ81791 SW8270 8/27/15 1 4-Nitrophenol ug/kg U 160 36014B3 (0-5) BJ81791 SW8270 8/27/15 1 4-Bromophenyl Phenyl Ether ug/kg U 110 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 2,4-Dimethylphenol ug/kg U 89 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 1,4-Dichlorobenzene ug/kg U 110 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 4-Chloroaniline ug/kg U 170 29014B3 (0-5) BJ81791 SW8270 8/27/15 1 Phenol ug/kg U 110 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Pyridine ug/kg U 88 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Bis(2-Chloroethyl) Ether (2-Chloroethyl Ether) ug/kg U 96 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Bis(2-Chloroethoxy) Methane ug/kg U 99 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Bis(2-Ethylhexyl) Phthalate ug/kg U 100 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Di-N-Octylphthalate ug/kg U 92 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Hexachlorobenzene ug/kg U 100 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Anthracene 150 ug/kg J 120 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 1,2,4-Trichlorobenzene ug/kg U 110 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 2,4-Dichlorophenol ug/kg U 130 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 2,4-Dinitrotoluene ug/kg U 140 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 1,2-Diphenylhydrazine ug/kg U 120 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Pyrene 780 ug/kg 120 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Dimethyl Phthalate ug/kg U 110 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Dibenzofuran ug/kg U 100 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Benzo(G,H,I)Perylene 530 ug/kg 120 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Indeno(1,2,3-C,D)Pyrene 600 ug/kg 120 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Benzo(B)Fluoranthene 660 ug/kg 120 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Fluoranthene 860 ug/kg 120 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Benzo(K)Fluoranthene 850 ug/kg 120 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Acenaphthylene ug/kg U 100 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Chrysene 690 ug/kg 120 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 2,2-Oxybis(2-Chloropropane) ug/kg U 99 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Benzo(A)Pyrene 1000 ug/kg 120 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 2,4-Dinitrophenol ug/kg UJ 250 71014B3 (0-5) BJ81791 SW8270 8/27/15 1 4,6-Dinitro-2-Methylphenol ug/kg UJ 380 180014B3 (0-5) BJ81791 SW8270 8/27/15 1 Dibenz(A,H)Anthracene 180 ug/kg J 120 250

Page 42 of 82



SDG: GBJ81780



14B3 (0-5) BJ81791 SW8270 8/27/15 1 1,3-Dichlorobenzene ug/kg U 110 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Benzo(A)Anthracene 750 ug/kg 120 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 4-Chloro-3-Methylphenol ug/kg U 130 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 2,6-Dinitrotoluene ug/kg U 110 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 N-Nitrosodi-N-Propylamine ug/kg U 120 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Aniline ug/kg U 290 29014B3 (0-5) BJ81791 SW8270 8/27/15 1 N-Nitrosodimethylamine ug/kg U 100 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Benzoic Acid ug/kg R 710 180014B3 (0-5) BJ81791 SW8270 8/27/15 1 Hexachloroethane ug/kg U 110 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 4-Chlorophenyl Phenyl Ether ug/kg U 120 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Hexachlorocyclopentadiene ug/kg UJ 110 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Isophorone ug/kg U 100 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Pentachloronitrobenzene ug/kg U 130 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Acenaphthene ug/kg U 110 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Diethyl Phthalate ug/kg U 110 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Di-N-Butyl Phthalate ug/kg U 95 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Phenanthrene 440 ug/kg 100 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Benzyl Butyl Phthalate ug/kg U 92 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 N-Nitrosodiphenylamine ug/kg U 140 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Fluorene ug/kg U 120 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Carbazole ug/kg U 270 180014B3 (0-5) BJ81791 SW8270 8/27/15 1 Hexachlorobutadiene ug/kg U 130 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Pentachlorophenol ug/kg UJ 140 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 2,4,6-Trichlorophenol ug/kg U 110 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 2-Nitroaniline ug/kg U 360 71014B3 (0-5) BJ81791 SW8270 8/27/15 1 2-Nitrophenol ug/kg U 230 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Naphthalene ug/kg U 100 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 2-Methylnaphthalene ug/kg U 110 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 2-Chloronaphthalene ug/kg U 100 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 3,3'-Dichlorobenzidine ug/kg U 170 71014B3 (0-5) BJ81791 SW8270 8/27/15 1 2-Methylphenol (O-Cresol) ug/kg U 170 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 1,2-Dichlorobenzene ug/kg U 100 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 2-Chlorophenol ug/kg U 100 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 1,2,4,5-Tetrachlorobenzene ug/kg U 130 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 2,4,5-Trichlorophenol ug/kg U 200 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Acetophenone ug/kg U 110 25014B3 (0-5) BJ81791 SW8270 8/27/15 1 Nitrobenzene ug/kg U 130 250

Page 43 of 82



SDG: GBJ81780



14B3 (0-5) BJ81791 SW8270 8/27/15 1 3-Nitroaniline ug/kg U 710 71014B3 (0-5) BJ81791 SW8270 8/27/15 1 3- And 4- Methylphenol (Total) ug/kg U 140 25014B3 (0-5) BJ81791 SW8260 8/31/15 1 Acetone ug/kg UJ 5.8 5014B3 (0-5) BJ81791 SW8260 8/31/15 1 Bromomethane ug/kg UJ 2.3 5.814B3 (0-5) BJ81791 SW6010 8/28/15 1 Potassium 1120 mg/kg J+ 2.7 714B3 (0-5) BJ81791 SW8260 8/31/15 1 Methylene Chloride ug/kg U 5.8 5.814B3 (0-5) BJ81791 SW8270 8/27/15 1 Benzidine ug/kg UJ 210 71014B3 (0-5) BJ81791 SW6010 8/28/15 1 Zinc 41.7 mg/kg J+ 0.34 0.714B3 (0-5) BJ81791 SW8260 8/31/15 1 Methyl Ethyl Ketone (2-Butanone) ug/kg UJ 5.8 3514B3 (15-18) BJ81793 SW6010 8/28/15 10 Iron 19600 mg/kg 42 4214B3 (15-18) BJ81793 SW8260 8/31/15 50 2-Hexanone ug/kg UJ 700 350014B3 (15-18) BJ81793 E160.3 8/26/15 1 Solids, Percent 80 %14B3 (15-18) BJ81793 SW6010 8/28/15 10 Aluminum 7200 mg/kg 8.3 4214B3 (15-18) BJ81793 SW6010 8/28/15 10 Manganese 521 mg/kg 4.2 4.214B3 (15-18) BJ81793 SW6010 8/28/15 10 Calcium 27000 mg/kg 38 4214B3 (15-18) BJ81793 SW6010 8/28/15 1 Lead 121 mg/kg 0.42 0.814B3 (15-18) BJ81793 SW6010 8/28/15 1 Magnesium 3490 mg/kg 4.2 4.214B3 (15-18) BJ81793 SW6010 8/28/15 1 Nickel 14.1 mg/kg 0.42 0.4214B3 (15-18) BJ81793 SW6010 8/28/15 1 Silver mg/kg U 0.42 0.4214B3 (15-18) BJ81793 SW6010 8/28/15 1 Sodium 548 mg/kg 3.6 814B3 (15-18) BJ81793 SW6010 8/28/15 1 Thallium mg/kg U 1.7 1.714B3 (15-18) BJ81793 SW6010 8/28/15 1 Antimony mg/kg U 2.1 2.114B3 (15-18) BJ81793 SW6010 8/28/15 1 Arsenic 2.8 mg/kg 0.83 0.814B3 (15-18) BJ81793 SW6010 8/28/15 1 Barium 72.0 mg/kg 0.42 0.814B3 (15-18) BJ81793 SW6010 8/28/15 1 Beryllium 0.44 mg/kg 0.17 0.3314B3 (15-18) BJ81793 SW6010 8/28/15 1 Cadmium 0.21 mg/kg J 0.17 0.4214B3 (15-18) BJ81793 SW6010 8/28/15 1 Chromium, Total 14.1 mg/kg 0.42 0.4214B3 (15-18) BJ81793 SW6010 8/28/15 1 Cobalt 6.86 mg/kg 0.42 0.4214B3 (15-18) BJ81793 SW6010 8/28/15 1 Copper 20.5 mg/kg 0.42 0.4214B3 (15-18) BJ81793 SW6010 8/28/15 1 Vanadium 24.3 mg/kg 0.42 0.414B3 (15-18) BJ81793 SW6010 8/28/15 1 Selenium mg/kg U 1.4 1.714B3 (15-18) BJ81793 SW7471 8/27/15 1 Mercury 0.41 mg/kg 0.02 0.0314B3 (15-18) BJ81793 SW8081 9/3/15 20 Heptachlor Epoxide ug/kg U 41 4114B3 (15-18) BJ81793 SW8081 9/3/15 20 Endosulfan Sulfate ug/kg U 82 8214B3 (15-18) BJ81793 SW8081 9/3/15 20 Aldrin ug/kg U 12 1214B3 (15-18) BJ81793 SW8081 9/3/15 20 Alpha Bhc (Alpha Hexachlorocyclohexane) ug/kg U 41 4114B3 (15-18) BJ81793 SW8081 9/3/15 20 Beta Bhc (Beta Hexachlorocyclohexane) ug/kg U 41 41

Page 44 of 82



SDG: GBJ81780



14B3 (15-18) BJ81793 SW8081 9/3/15 20 Delta BHC (Delta Hexachlorocyclohexane) ug/kg U 41 4114B3 (15-18) BJ81793 SW8081 9/3/15 20 Beta Endosulfan ug/kg U 20 2014B3 (15-18) BJ81793 SW8081 9/3/15 20 P,P'-DDT ug/kg U 25 2514B3 (15-18) BJ81793 SW8081 9/3/15 20 cis-Chlordane ug/kg U 41 4114B3 (15-18) BJ81793 SW8081 9/3/15 20 trans-Chlordane ug/kg U 41 4114B3 (15-18) BJ81793 SW8081 9/3/15 20 Endrin Ketone ug/kg U 82 8214B3 (15-18) BJ81793 SW8081 9/3/15 20 Gamma Bhc (Lindane) ug/kg U 16 1614B3 (15-18) BJ81793 SW8081 9/3/15 20 Dieldrin ug/kg U 12 1214B3 (15-18) BJ81793 SW8081 9/3/15 20 Endrin ug/kg U 41 4114B3 (15-18) BJ81793 SW8081 9/3/15 20 Methoxychlor ug/kg U 410 41014B3 (15-18) BJ81793 SW8081 9/3/15 20 P,P'-DDD ug/kg U 20 2014B3 (15-18) BJ81793 SW8081 9/3/15 20 P,P'-DDE ug/kg U 20 2014B3 (15-18) BJ81793 SW8081 9/3/15 20 Endrin Aldehyde ug/kg U 82 8214B3 (15-18) BJ81793 SW8081 9/3/15 20 Heptachlor ug/kg U 41 4114B3 (15-18) BJ81793 SW8081 9/3/15 20 Toxaphene ug/kg U 1600 160014B3 (15-18) BJ81793 SW8081 9/3/15 20 Alpha Endosulfan ug/kg U 82 8214B3 (15-18) BJ81793 SW8082 8/29/15 2 PCB-1260 (Aroclor 1260) ug/kg U 41 4114B3 (15-18) BJ81793 SW8082 8/29/15 2 PCB-1254 (Aroclor 1254) ug/kg U 41 4114B3 (15-18) BJ81793 SW8082 8/29/15 2 PCB-1268 (Aroclor 1268) ug/kg U 41 4114B3 (15-18) BJ81793 SW8082 8/29/15 2 PCB-1221 (Aroclor 1221) ug/kg U 41 4114B3 (15-18) BJ81793 SW8082 8/29/15 2 PCB-1232 (Aroclor 1232) ug/kg U 41 4114B3 (15-18) BJ81793 SW8082 8/29/15 2 PCB-1248 (Aroclor 1248) ug/kg U 41 4114B3 (15-18) BJ81793 SW8082 8/29/15 2 PCB-1016 (Aroclor 1016) ug/kg U 41 4114B3 (15-18) BJ81793 SW8082 8/29/15 2 PCB-1262 (Aroclor 1262) ug/kg U 41 4114B3 (15-18) BJ81793 SW8082 8/29/15 2 PCB-1242 (Aroclor 1242) ug/kg U 41 4114B3 (15-18) BJ81793 SW8260 8/31/15 50 Ethylbenzene 640 ug/kg J 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Styrene ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Cis-1,3-Dichloropropene ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Trans-1,3-Dichloropropene ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 N-Propylbenzene ug/kg U 130 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 N-Butylbenzene ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 4-Chlorotoluene ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,4-Dichlorobenzene ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,2-Dibromoethane (Ethylene Dibromide) ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Acrolein ug/kg U 350 280014B3 (15-18) BJ81793 SW8260 8/31/15 50 Acrylonitrile ug/kg U 140 140014B3 (15-18) BJ81793 SW8260 8/31/15 50 Methyl Isobutyl Ketone (4-Methyl-2-Pentanone) ug/kg U 700 3500

Page 45 of 82



SDG: GBJ81780



14B3 (15-18) BJ81793 SW8260 8/31/15 50 1,3,5-Trimethylbenzene (Mesitylene) 89 ug/kg J 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Bromobenzene ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Toluene 290 ug/kg J 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Chlorobenzene ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Tetrahydrofuran ug/kg U 350 140014B3 (15-18) BJ81793 SW8260 8/31/15 50 Trans-1,4-Dichloro-2-Butene ug/kg UJ 350 140014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,2,4-Trichlorobenzene ug/kg U 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,4-Dioxane (P-Dioxane) ug/kg UJ 5600 1400014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,2-Dichloroethane ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Tetrachloroethylene (PCE) ug/kg U 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Sec-Butylbenzene ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,3-Dichloropropane ug/kg U 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Cis-1,2-Dichloroethylene 7600 ug/kg 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Trans-1,2-Dichloroethene 160 ug/kg J 70 15014B3 (15-18) BJ81793 SW8260 8/31/15 50 Tert-Butyl Methyl Ether ug/kg U 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 m,p-Xylene 820 ug/kg 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 O-Cymene (O-Isopropyltoluene) ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,3-Dichlorobenzene ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Dibromochloromethane ug/kg UJ 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,1-Dichloropropene ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 2,2-Dichloropropane ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Carbon Tetrachloride ug/kg U 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Chloroform ug/kg U 70 25014B3 (15-18) BJ81793 SW8260 8/31/15 50 Benzene 2800 ug/kg 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,1,1,2-Tetrachloroethane ug/kg U 140 280014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,1,1-Trichloroethane ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Chloromethane ug/kg U 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Dibromomethane ug/kg U 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Bromochloromethane ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Vinyl Chloride 2600 ug/kg 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Carbon Disulfide ug/kg U 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Chloroethane ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Bromoform ug/kg UJ 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,1-Dichloroethane ug/kg U 140 25014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,1-Dichloroethene ug/kg U 70 25014B3 (15-18) BJ81793 SW8260 8/31/15 50 Bromodichloromethane ug/kg U 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Tert-Butyl Alcohol ug/kg U 2800 14000

Page 46 of 82



SDG: GBJ81780



14B3 (15-18) BJ81793 SW8260 8/31/15 50 Trichlorofluoromethane ug/kg UJ 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,1,2-Trichloro-1,2,2-Trifluoroethane ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,2-Dichloropropane ug/kg U 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,1,2-Trichloroethane ug/kg U 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Trichloroethylene (TCE) 3700 ug/kg 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,1,2,2-Tetrachloroethane ug/kg U 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,2,3-Trichlorobenzene ug/kg U 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Dichlorodifluoromethane ug/kg UJ 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Naphthalene 6500 ug/kg 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 O-Xylene (1,2-Dimethylbenzene) 230 ug/kg J 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 2-Chlorotoluene ug/kg U 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,2-Dichlorobenzene ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,2,4-Trimethylbenzene 240 ug/kg J 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,2-Dibromo-3-Chloropropane ug/kg U 140 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 1,2,3-Trichloropropane ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 T-Butylbenzene ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Isopropylbenzene (Cumene) ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Cymene ug/kg U 70 70014B3 (15-18) BJ81793 SW8270 8/27/15 10 4-Nitroaniline ug/kg U 1400 830014B3 (15-18) BJ81793 SW8270 8/27/15 10 4-Nitrophenol ug/kg U 1900 410014B3 (15-18) BJ81793 SW8270 8/27/15 10 4-Bromophenyl Phenyl Ether ug/kg U 1200 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 2,4-Dimethylphenol ug/kg U 1000 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 1,4-Dichlorobenzene ug/kg U 1200 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 4-Chloroaniline ug/kg U 1900 330014B3 (15-18) BJ81793 SW8270 8/27/15 10 Phenol ug/kg U 1300 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Pyridine ug/kg U 1000 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Bis(2-Chloroethyl) Ether (2-Chloroethyl Ether) ug/kg U 1100 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Bis(2-Chloroethoxy) Methane ug/kg U 1100 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Bis(2-Ethylhexyl) Phthalate ug/kg U 1200 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Di-N-Octylphthalate ug/kg U 1100 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Hexachlorobenzene ug/kg U 1200 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Anthracene 16000 ug/kg 1400 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 1,2,4-Trichlorobenzene ug/kg U 1200 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 2,4-Dichlorophenol ug/kg U 1500 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 2,4-Dinitrotoluene ug/kg U 1600 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 1,2-Diphenylhydrazine ug/kg U 1300 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Pyrene 20000 ug/kg 1400 2900

Page 47 of 82



SDG: GBJ81780



14B3 (15-18) BJ81793 SW8270 8/27/15 10 Dimethyl Phthalate ug/kg U 1300 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Dibenzofuran 12000 ug/kg 1200 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Benzo(G,H,I)Perylene 5000 ug/kg 1300 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Indeno(1,2,3-C,D)Pyrene 6400 ug/kg 1400 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Benzo(B)Fluoranthene 9900 ug/kg 1400 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Fluoranthene 25000 ug/kg 1300 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Benzo(K)Fluoranthene 10000 ug/kg 1400 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Acenaphthylene 8400 ug/kg 1200 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Chrysene 13000 ug/kg 1400 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 2,2-Oxybis(2-Chloropropane) ug/kg U 1100 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Benzo(A)Pyrene 13000 ug/kg 1300 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 2,4-Dinitrophenol ug/kg UJ 2900 830014B3 (15-18) BJ81793 SW8270 8/27/15 10 4,6-Dinitro-2-Methylphenol ug/kg UJ 4500 2100014B3 (15-18) BJ81793 SW8270 8/27/15 10 Dibenz(A,H)Anthracene 2000 ug/kg J 1300 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 1,3-Dichlorobenzene ug/kg U 1200 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Benzo(A)Anthracene 14000 ug/kg 1400 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 4-Chloro-3-Methylphenol ug/kg U 1500 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 2,6-Dinitrotoluene ug/kg U 1300 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 N-Nitrosodi-N-Propylamine ug/kg U 1300 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Aniline ug/kg U 3300 330014B3 (15-18) BJ81793 SW8270 8/27/15 10 N-Nitrosodimethylamine ug/kg U 1200 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Benzoic Acid ug/kg R 8300 2100014B3 (15-18) BJ81793 SW8270 8/27/15 10 Hexachloroethane ug/kg U 1200 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 4-Chlorophenyl Phenyl Ether ug/kg U 1400 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Hexachlorocyclopentadiene ug/kg UJ 1300 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Isophorone ug/kg U 1200 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Pentachloronitrobenzene ug/kg U 1500 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Acenaphthene 2900 ug/kg 1300 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Diethyl Phthalate ug/kg U 1300 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Di-N-Butyl Phthalate ug/kg U 1100 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Phenanthrene 45000 ug/kg 1200 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Benzyl Butyl Phthalate ug/kg U 1100 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 N-Nitrosodiphenylamine ug/kg U 1600 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Fluorene 18000 ug/kg 1400 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Carbazole 5700 ug/kg J 3100 2100014B3 (15-18) BJ81793 SW8270 8/27/15 10 Hexachlorobutadiene ug/kg U 1500 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Pentachlorophenol ug/kg UJ 1600 2900

Page 48 of 82



SDG: GBJ81780



14B3 (15-18) BJ81793 SW8270 8/27/15 10 2,4,6-Trichlorophenol ug/kg U 1300 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 2-Nitroaniline ug/kg U 4200 830014B3 (15-18) BJ81793 SW8270 8/27/15 10 2-Nitrophenol ug/kg U 2600 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Naphthalene 43000 ug/kg 1200 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 2-Methylnaphthalene 19000 ug/kg 1200 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 2-Chloronaphthalene ug/kg U 1200 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 3,3'-Dichlorobenzidine ug/kg U 2000 830014B3 (15-18) BJ81793 SW8270 8/27/15 10 Benzidine ug/kg U 2400 830014B3 (15-18) BJ81793 SW8270 8/27/15 10 2-Methylphenol (O-Cresol) ug/kg U 1900 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 1,2-Dichlorobenzene ug/kg U 1200 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 2-Chlorophenol ug/kg U 1200 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 1,2,4,5-Tetrachlorobenzene ug/kg U 1500 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 2,4,5-Trichlorophenol ug/kg U 2300 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Acetophenone ug/kg U 1300 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 Nitrobenzene ug/kg U 1400 290014B3 (15-18) BJ81793 SW8270 8/27/15 10 3-Nitroaniline ug/kg U 8300 830014B3 (15-18) BJ81793 SW8270 8/27/15 10 3- And 4- Methylphenol (Total) ug/kg U 1600 290014B3 (15-18) BJ81793 SW8260 8/31/15 50 Hexachlorobutadiene ug/kg U 70 70014B3 (15-18) BJ81793 SW8260 8/31/15 50 Acetone ug/kg UJ 700 700014B3 (15-18) BJ81793 SW8260 8/31/15 50 Bromomethane ug/kg UJ 280 70014B3 (15-18) BJ81793 SW6010 8/28/15 1 Potassium 1670 mg/kg J+ 3.2 814B3 (15-18) BJ81793 SW8260 8/31/15 50 Methylene Chloride ug/kg U 700 70014B3 (15-18) BJ81793 SW6010 8/28/15 1 Zinc 51.4 mg/kg J+ 0.42 0.814B3 (15-18) BJ81793 SW8260 8/31/15 50 Methyl Ethyl Ketone (2-Butanone) ug/kg UJ 700 420014B6 (0-5) BJ81794 SW8260 8/31/15 1 2-Hexanone ug/kg UJ 5.2 2614B6 (0-5) BJ81794 SW6010 8/28/15 10 Iron 10500 mg/kg 32 3214B6 (0-5) BJ81794 SW8260 8/31/15 1 Dibromochloromethane ug/kg UJ 1.0 5.214B6 (0-5) BJ81794 SW8260 8/31/15 50 Hexachlorobutadiene ug/kg U 27 27014B6 (0-5) BJ81794 SW8260 8/31/15 1 1,2-Dichloroethane ug/kg UJ 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Bromoform ug/kg UJ 1.0 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Trichlorofluoromethane ug/kg UJ 1.0 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Carbon Tetrachloride ug/kg UJ 1.0 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 1,1,1,2-Tetrachloroethane ug/kg UJ 1.0 2114B6 (0-5) BJ81794 SW8260 8/31/15 1 1,1,1-Trichloroethane ug/kg UJ 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Chloroethane ug/kg UJ 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Dichlorodifluoromethane ug/kg UJ 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Bromodichloromethane ug/kg UJ 1.0 5.2

Page 49 of 82



SDG: GBJ81780



14B6 (0-5) BJ81794 SW8260 8/31/15 1 Tert-Butyl Alcohol ug/kg UJ 21 10014B6 (0-5) BJ81794 SW8260 8/31/15 50 Trans-1,4-Dichloro-2-Butene ug/kg UJ 130 54014B6 (0-5) BJ81794 SW8260 8/31/15 1 1,4-Dioxane (P-Dioxane) ug/kg UJ 42 10014B6 (0-5) BJ81794 SW8260 8/31/15 1 O-Xylene (1,2-Dimethylbenzene) ug/kg UJ 1.0 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Acetone 7.6 ug/kg J 5.2 5014B6 (0-5) BJ81794 SW8260 8/31/15 1 Bromomethane ug/kg UJ 2.1 5.214B6 (0-5) BJ81794 E160.3 8/26/15 1 Solids, Percent 93 %14B6 (0-5) BJ81794 SW6010 8/28/15 10 Aluminum 7140 mg/kg 6.5 3214B6 (0-5) BJ81794 SW6010 8/28/15 10 Manganese 184 mg/kg 3.2 3.214B6 (0-5) BJ81794 SW6010 8/28/15 1 Lead 46.4 mg/kg 0.32 0.614B6 (0-5) BJ81794 SW6010 8/28/15 1 Magnesium 1960 mg/kg 3.2 3.214B6 (0-5) BJ81794 SW6010 8/28/15 1 Nickel 12.3 mg/kg 0.32 0.3214B6 (0-5) BJ81794 SW6010 8/28/15 1 Potassium 790 mg/kg J+ 2.5 614B6 (0-5) BJ81794 SW6010 8/28/15 1 Silver mg/kg U 0.32 0.3214B6 (0-5) BJ81794 SW6010 8/28/15 1 Sodium 164 mg/kg 2.8 614B6 (0-5) BJ81794 SW6010 8/28/15 1 Thallium mg/kg U 1.3 1.314B6 (0-5) BJ81794 SW6010 8/28/15 1 Antimony mg/kg U 1.6 1.614B6 (0-5) BJ81794 SW6010 8/28/15 1 Arsenic 2.0 mg/kg 0.65 0.614B6 (0-5) BJ81794 SW6010 8/28/15 1 Barium 48.8 mg/kg 0.32 0.614B6 (0-5) BJ81794 SW6010 8/28/15 1 Beryllium 0.28 mg/kg 0.13 0.2614B6 (0-5) BJ81794 SW6010 8/28/15 1 Cadmium mg/kg U 0.13 0.3214B6 (0-5) BJ81794 SW6010 8/28/15 1 Chromium, Total 14.0 mg/kg 0.32 0.3214B6 (0-5) BJ81794 SW6010 8/28/15 1 Cobalt 4.60 mg/kg 0.32 0.3214B6 (0-5) BJ81794 SW6010 8/28/15 1 Copper 14.4 mg/kg 0.32 0.3214B6 (0-5) BJ81794 SW6010 8/28/15 1 Vanadium 19.9 mg/kg 0.32 0.314B6 (0-5) BJ81794 SW6010 8/28/15 1 Calcium 3090 mg/kg 3.0 3.214B6 (0-5) BJ81794 SW6010 8/28/15 1 Selenium mg/kg U 1.1 1.314B6 (0-5) BJ81794 SW7471 8/27/15 1 Mercury 0.08 mg/kg 0.02 0.0314B6 (0-5) BJ81794 SW8081 8/28/15 2 Heptachlor Epoxide ug/kg U 7.0 7.014B6 (0-5) BJ81794 SW8081 8/28/15 2 Endosulfan Sulfate ug/kg U 7.0 7.014B6 (0-5) BJ81794 SW8081 8/28/15 2 Aldrin ug/kg U 3.5 3.514B6 (0-5) BJ81794 SW8081 8/28/15 2 Alpha Bhc (Alpha Hexachlorocyclohexane) ug/kg U 7.0 7.014B6 (0-5) BJ81794 SW8081 8/28/15 2 Beta Bhc (Beta Hexachlorocyclohexane) ug/kg U 7.0 7.014B6 (0-5) BJ81794 SW8081 8/28/15 2 Delta BHC (Delta Hexachlorocyclohexane) ug/kg U 7.0 7.014B6 (0-5) BJ81794 SW8081 8/28/15 2 Beta Endosulfan ug/kg U 7.0 7.014B6 (0-5) BJ81794 SW8081 8/28/15 2 P,P'-DDT ug/kg U 2.1 2.114B6 (0-5) BJ81794 SW8081 8/28/15 2 cis-Chlordane ug/kg U 3.5 3.5

Page 50 of 82



SDG: GBJ81780



14B6 (0-5) BJ81794 SW8081 8/28/15 2 trans-Chlordane ug/kg U 3.5 3.514B6 (0-5) BJ81794 SW8081 8/28/15 2 Endrin Ketone ug/kg U 7.0 7.014B6 (0-5) BJ81794 SW8081 8/28/15 2 Gamma Bhc (Lindane) ug/kg U 8.0 8.014B6 (0-5) BJ81794 SW8081 8/28/15 2 Dieldrin ug/kg U 3.5 3.514B6 (0-5) BJ81794 SW8081 8/28/15 2 Endrin ug/kg U 7.0 7.014B6 (0-5) BJ81794 SW8081 8/28/15 2 Methoxychlor ug/kg U 35 3514B6 (0-5) BJ81794 SW8081 8/28/15 2 P,P'-DDD ug/kg U 2.1 2.114B6 (0-5) BJ81794 SW8081 8/28/15 2 P,P'-DDE ug/kg U 2.1 2.114B6 (0-5) BJ81794 SW8081 8/28/15 2 Endrin Aldehyde ug/kg U 7.0 7.014B6 (0-5) BJ81794 SW8081 8/28/15 2 Heptachlor ug/kg U 7.0 7.014B6 (0-5) BJ81794 SW8081 8/28/15 2 Toxaphene ug/kg U 140 14014B6 (0-5) BJ81794 SW8081 8/28/15 2 Alpha Endosulfan ug/kg U 7.0 7.014B6 (0-5) BJ81794 SW8082 8/29/15 2 PCB-1260 (Aroclor 1260) ug/kg U 35 3514B6 (0-5) BJ81794 SW8082 8/29/15 2 PCB-1254 (Aroclor 1254) ug/kg U 35 3514B6 (0-5) BJ81794 SW8082 8/29/15 2 PCB-1268 (Aroclor 1268) ug/kg U 35 3514B6 (0-5) BJ81794 SW8082 8/29/15 2 PCB-1221 (Aroclor 1221) ug/kg U 35 3514B6 (0-5) BJ81794 SW8082 8/29/15 2 PCB-1232 (Aroclor 1232) ug/kg U 35 3514B6 (0-5) BJ81794 SW8082 8/29/15 2 PCB-1248 (Aroclor 1248) ug/kg U 35 3514B6 (0-5) BJ81794 SW8082 8/29/15 2 PCB-1016 (Aroclor 1016) ug/kg U 35 3514B6 (0-5) BJ81794 SW8082 8/29/15 2 PCB-1262 (Aroclor 1262) ug/kg U 35 3514B6 (0-5) BJ81794 SW8082 8/29/15 2 PCB-1242 (Aroclor 1242) ug/kg U 35 3514B6 (0-5) BJ81794 SW8260 8/31/15 50 N-Propylbenzene ug/kg U 48 27014B6 (0-5) BJ81794 SW8260 8/31/15 50 N-Butylbenzene ug/kg U 27 27014B6 (0-5) BJ81794 SW8260 8/31/15 50 4-Chlorotoluene ug/kg U 27 27014B6 (0-5) BJ81794 SW8260 8/31/15 50 1,4-Dichlorobenzene ug/kg U 27 27014B6 (0-5) BJ81794 SW8260 8/31/15 50 1,3,5-Trimethylbenzene (Mesitylene) ug/kg U 27 27014B6 (0-5) BJ81794 SW8260 8/31/15 50 Bromobenzene ug/kg U 27 27014B6 (0-5) BJ81794 SW8260 8/31/15 50 1,2,4-Trichlorobenzene ug/kg U 54 27014B6 (0-5) BJ81794 SW8260 8/31/15 50 Sec-Butylbenzene ug/kg U 27 27014B6 (0-5) BJ81794 SW8260 8/31/15 50 O-Cymene (O-Isopropyltoluene) ug/kg U 27 27014B6 (0-5) BJ81794 SW8260 8/31/15 50 1,3-Dichlorobenzene ug/kg U 27 27014B6 (0-5) BJ81794 SW8260 8/31/15 50 Trichloroethylene (TCE) 32 ug/kg J 27 27014B6 (0-5) BJ81794 SW8260 8/31/15 50 1,2,3-Trichlorobenzene ug/kg UJ 54 27014B6 (0-5) BJ81794 SW8260 8/31/15 50 Naphthalene 140 ug/kg J 54 27014B6 (0-5) BJ81794 SW8260 8/31/15 50 2-Chlorotoluene ug/kg U 54 27014B6 (0-5) BJ81794 SW8260 8/31/15 50 1,2-Dichlorobenzene ug/kg U 27 27014B6 (0-5) BJ81794 SW8260 8/31/15 50 1,2,4-Trimethylbenzene ug/kg U 27 270

Page 51 of 82



SDG: GBJ81780



14B6 (0-5) BJ81794 SW8260 8/31/15 50 1,2-Dibromo-3-Chloropropane ug/kg U 54 27014B6 (0-5) BJ81794 SW8260 8/31/15 50 1,2,3-Trichloropropane ug/kg U 27 27014B6 (0-5) BJ81794 SW8260 8/31/15 50 T-Butylbenzene ug/kg U 27 27014B6 (0-5) BJ81794 SW8260 8/31/15 50 Isopropylbenzene (Cumene) ug/kg U 27 27014B6 (0-5) BJ81794 SW8260 8/31/15 50 Cymene ug/kg U 27 27014B6 (0-5) BJ81794 SW8260 8/31/15 1 Ethylbenzene ug/kg UJ 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Styrene ug/kg UJ 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Cis-1,3-Dichloropropene ug/kg UJ 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Trans-1,3-Dichloropropene ug/kg UJ 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 1,2-Dibromoethane (Ethylene Dibromide) ug/kg UJ 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Acrolein ug/kg UJ 2.6 2114B6 (0-5) BJ81794 SW8260 8/31/15 1 Acrylonitrile ug/kg UJ 0.52 2114B6 (0-5) BJ81794 SW8260 8/31/15 1 Methyl Isobutyl Ketone (4-Methyl-2-Pentanone) ug/kg UJ 5.2 2614B6 (0-5) BJ81794 SW8260 8/31/15 1 Toluene 0.64 ug/kg J 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Chlorobenzene ug/kg UJ 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Tetrahydrofuran ug/kg UJ 2.6 1014B6 (0-5) BJ81794 SW8260 8/31/15 1 Tetrachloroethylene (PCE) ug/kg UJ 1.0 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 1,3-Dichloropropane ug/kg UJ 1.0 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Cis-1,2-Dichloroethylene 0.92 ug/kg J 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Trans-1,2-Dichloroethene ug/kg UJ 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Tert-Butyl Methyl Ether ug/kg UJ 1.0 1014B6 (0-5) BJ81794 SW8260 8/31/15 1 m,p-Xylene ug/kg UJ 1.0 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 1,1-Dichloropropene ug/kg UJ 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 2,2-Dichloropropane ug/kg UJ 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Chloroform ug/kg UJ 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Benzene ug/kg UJ 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Chloromethane ug/kg UJ 1.0 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Dibromomethane ug/kg UJ 1.0 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Bromochloromethane ug/kg UJ 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Vinyl Chloride ug/kg UJ 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Methylene Chloride ug/kg UJ 5.2 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 Carbon Disulfide ug/kg UJ 1.0 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 1,1-Dichloroethane ug/kg UJ 1.0 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 1,1-Dichloroethene ug/kg UJ 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 1,1,2-Trichloro-1,2,2-Trifluoroethane ug/kg UJ 0.52 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 1,2-Dichloropropane ug/kg UJ 1.0 5.214B6 (0-5) BJ81794 SW8260 8/31/15 1 1,1,2-Trichloroethane ug/kg UJ 1.0 5.2

Page 52 of 82



SDG: GBJ81780



14B6 (0-5) BJ81794 SW8260 8/31/15 1 1,1,2,2-Tetrachloroethane ug/kg UJ 1.0 5.214B6 (0-5) BJ81794 SW8270 8/27/15 1 4-Nitroaniline ug/kg U 120 70014B6 (0-5) BJ81794 SW8270 8/27/15 1 4-Nitrophenol ug/kg U 160 35014B6 (0-5) BJ81794 SW8270 8/27/15 1 4-Bromophenyl Phenyl Ether ug/kg U 100 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 2,4-Dimethylphenol ug/kg U 87 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 1,4-Dichlorobenzene ug/kg U 100 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 4-Chloroaniline ug/kg U 160 28014B6 (0-5) BJ81794 SW8270 8/27/15 1 Phenol ug/kg U 110 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Pyridine ug/kg U 86 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Bis(2-Chloroethyl) Ether (2-Chloroethyl Ether) ug/kg U 95 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Bis(2-Chloroethoxy) Methane ug/kg U 97 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Hexachlorobenzene ug/kg U 100 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Anthracene ug/kg U 120 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 1,2,4-Trichlorobenzene ug/kg U 110 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 2,4-Dichlorophenol ug/kg U 120 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 2,4-Dinitrotoluene ug/kg U 140 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 1,2-Diphenylhydrazine ug/kg U 110 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Pyrene 300 ug/kg 120 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Dimethyl Phthalate ug/kg U 110 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Dibenzofuran ug/kg U 100 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Fluoranthene 340 ug/kg 110 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Acenaphthylene ug/kg U 98 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 2,2-Oxybis(2-Chloropropane) ug/kg U 98 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 2,4-Dinitrophenol ug/kg UJ 250 70014B6 (0-5) BJ81794 SW8270 8/27/15 1 4,6-Dinitro-2-Methylphenol ug/kg UJ 380 180014B6 (0-5) BJ81794 SW8270 8/27/15 1 1,3-Dichlorobenzene ug/kg U 100 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 4-Chloro-3-Methylphenol ug/kg U 120 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 2,6-Dinitrotoluene ug/kg U 110 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 N-Nitrosodi-N-Propylamine ug/kg U 110 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Aniline ug/kg U 280 28014B6 (0-5) BJ81794 SW8270 8/27/15 1 N-Nitrosodimethylamine ug/kg U 99 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Benzoic Acid ug/kg R 700 180014B6 (0-5) BJ81794 SW8270 8/27/15 1 Hexachloroethane ug/kg U 110 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 4-Chlorophenyl Phenyl Ether ug/kg U 120 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Hexachlorocyclopentadiene ug/kg UJ 110 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Isophorone ug/kg U 98 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Pentachloronitrobenzene ug/kg U 130 250

Page 53 of 82



SDG: GBJ81780



14B6 (0-5) BJ81794 SW8270 8/27/15 1 Acenaphthene ug/kg U 110 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Diethyl Phthalate ug/kg U 110 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Di-N-Butyl Phthalate ug/kg U 93 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Phenanthrene 150 ug/kg J 100 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 N-Nitrosodiphenylamine ug/kg U 130 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Fluorene ug/kg U 120 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Carbazole ug/kg U 270 180014B6 (0-5) BJ81794 SW8270 8/27/15 1 Hexachlorobutadiene ug/kg U 130 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Pentachlorophenol ug/kg UJ 130 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 2,4,6-Trichlorophenol ug/kg U 110 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 2-Nitroaniline ug/kg U 350 70014B6 (0-5) BJ81794 SW8270 8/27/15 1 2-Nitrophenol ug/kg U 220 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Naphthalene ug/kg U 100 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 2-Methylnaphthalene ug/kg U 100 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 2-Chloronaphthalene ug/kg U 100 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Benzidine ug/kg U 210 70014B6 (0-5) BJ81794 SW8270 8/27/15 1 2-Methylphenol (O-Cresol) ug/kg U 160 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 1,2-Dichlorobenzene ug/kg U 99 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 2-Chlorophenol ug/kg U 100 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 1,2,4,5-Tetrachlorobenzene ug/kg U 120 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 2,4,5-Trichlorophenol ug/kg U 190 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Acetophenone ug/kg U 110 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Nitrobenzene ug/kg U 120 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 3-Nitroaniline ug/kg U 700 70014B6 (0-5) BJ81794 SW8270 8/27/15 1 3- And 4- Methylphenol (Total) ug/kg U 140 25014B6 (0-5) BJ81794 SW6010 8/28/15 1 Zinc 56.6 mg/kg J+ 0.32 0.614B6 (0-5) BJ81794 SW8270 8/27/15 1 Bis(2-Ethylhexyl) Phthalate ug/kg UJ 100 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Di-N-Octylphthalate ug/kg UJ 91 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Benzo(G,H,I)Perylene 150 ug/kg J 110 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Indeno(1,2,3-C,D)Pyrene 180 ug/kg J 120 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Benzo(B)Fluoranthene 160 ug/kg J 120 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Benzo(K)Fluoranthene 160 ug/kg J 120 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Chrysene 180 ug/kg J 120 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Benzo(A)Pyrene 170 ug/kg J 110 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Dibenz(A,H)Anthracene ug/kg UJ 110 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Benzo(A)Anthracene 170 ug/kg J 120 25014B6 (0-5) BJ81794 SW8270 8/27/15 1 Benzyl Butyl Phthalate ug/kg UJ 91 250

Page 54 of 82



SDG: GBJ81780



14B6 (0-5) BJ81794 SW8270 8/27/15 1 3,3'-Dichlorobenzidine ug/kg UJ 170 70014B6 (0-5) BJ81794 SW8260 8/31/15 1 Methyl Ethyl Ketone (2-Butanone) ug/kg UJ 5.2 3114B6 (15-17) BJ81796 SW6010 8/28/15 10 Iron 14400 mg/kg 43 4314B6 (15-17) BJ81796 E160.3 8/26/15 1 Solids, Percent 74 %14B6 (15-17) BJ81796 SW6010 8/28/15 10 Aluminum 8350 mg/kg 8.7 4314B6 (15-17) BJ81796 SW6010 8/28/15 10 Manganese 235 mg/kg 4.3 4.314B6 (15-17) BJ81796 SW6010 8/28/15 1 Lead 107 mg/kg 0.43 0.914B6 (15-17) BJ81796 SW6010 8/28/15 1 Magnesium 2680 mg/kg 4.3 4.314B6 (15-17) BJ81796 SW6010 8/28/15 1 Nickel 16.5 mg/kg 0.43 0.4314B6 (15-17) BJ81796 SW6010 8/28/15 1 Potassium 1060 mg/kg J+ 3.4 914B6 (15-17) BJ81796 SW6010 8/28/15 1 Silver mg/kg U 0.43 0.4314B6 (15-17) BJ81796 SW6010 8/28/15 1 Sodium 1110 mg/kg 3.7 914B6 (15-17) BJ81796 SW6010 8/28/15 1 Thallium mg/kg U 1.7 1.714B6 (15-17) BJ81796 SW6010 8/28/15 1 Antimony mg/kg U 2.2 2.214B6 (15-17) BJ81796 SW6010 8/28/15 1 Arsenic 8.2 mg/kg 0.87 0.914B6 (15-17) BJ81796 SW6010 8/28/15 1 Barium 65.4 mg/kg 0.43 0.914B6 (15-17) BJ81796 SW6010 8/28/15 1 Beryllium 0.53 mg/kg 0.17 0.3514B6 (15-17) BJ81796 SW6010 8/28/15 1 Cadmium mg/kg U 0.17 0.4314B6 (15-17) BJ81796 SW6010 8/28/15 1 Chromium, Total 14.2 mg/kg 0.43 0.4314B6 (15-17) BJ81796 SW6010 8/28/15 1 Cobalt 5.73 mg/kg 0.43 0.4314B6 (15-17) BJ81796 SW6010 8/28/15 1 Copper 15.4 mg/kg 0.43 0.4314B6 (15-17) BJ81796 SW6010 8/28/15 1 Vanadium 24.7 mg/kg 0.43 0.414B6 (15-17) BJ81796 SW6010 8/28/15 1 Calcium 8210 mg/kg 4.0 4.314B6 (15-17) BJ81796 SW6010 8/28/15 1 Selenium mg/kg U 1.5 1.714B6 (15-17) BJ81796 SW7471 8/27/15 1 Mercury 0.18 mg/kg 0.02 0.0314B6 (15-17) BJ81796 SW8081 8/29/15 20 Heptachlor Epoxide ug/kg U 89 8914B6 (15-17) BJ81796 SW8081 8/29/15 20 Endosulfan Sulfate ug/kg U 89 8914B6 (15-17) BJ81796 SW8081 8/29/15 20 Aldrin ug/kg U 13 1314B6 (15-17) BJ81796 SW8081 8/29/15 20 Alpha Bhc (Alpha Hexachlorocyclohexane) ug/kg U 44 4414B6 (15-17) BJ81796 SW8081 8/29/15 20 Beta Bhc (Beta Hexachlorocyclohexane) ug/kg U 44 4414B6 (15-17) BJ81796 SW8081 8/29/15 20 Delta BHC (Delta Hexachlorocyclohexane) ug/kg U 44 4414B6 (15-17) BJ81796 SW8081 8/29/15 20 Beta Endosulfan ug/kg U 89 8914B6 (15-17) BJ81796 SW8081 8/29/15 20 P,P'-DDT ug/kg U 27 2714B6 (15-17) BJ81796 SW8081 8/29/15 20 cis-Chlordane ug/kg U 44 4414B6 (15-17) BJ81796 SW8081 8/29/15 20 trans-Chlordane ug/kg U 44 4414B6 (15-17) BJ81796 SW8081 8/29/15 20 Endrin Ketone ug/kg U 89 8914B6 (15-17) BJ81796 SW8081 8/29/15 20 Gamma Bhc (Lindane) ug/kg U 30 30

Page 55 of 82



SDG: GBJ81780



14B6 (15-17) BJ81796 SW8081 8/29/15 20 Dieldrin ug/kg U 44 4414B6 (15-17) BJ81796 SW8081 8/29/15 20 Endrin ug/kg U 89 8914B6 (15-17) BJ81796 SW8081 8/29/15 20 Methoxychlor ug/kg U 440 44014B6 (15-17) BJ81796 SW8081 8/29/15 20 P,P'-DDD ug/kg U 27 2714B6 (15-17) BJ81796 SW8081 8/29/15 20 P,P'-DDE ug/kg U 27 2714B6 (15-17) BJ81796 SW8081 8/29/15 20 Endrin Aldehyde ug/kg U 89 8914B6 (15-17) BJ81796 SW8081 8/29/15 20 Heptachlor ug/kg U 44 4414B6 (15-17) BJ81796 SW8081 8/29/15 20 Toxaphene ug/kg U 1800 180014B6 (15-17) BJ81796 SW8081 8/29/15 20 Alpha Endosulfan ug/kg U 89 8914B6 (15-17) BJ81796 SW8082 8/29/15 2 PCB-1260 (Aroclor 1260) ug/kg U 44 4414B6 (15-17) BJ81796 SW8082 8/29/15 2 PCB-1254 (Aroclor 1254) ug/kg U 44 4414B6 (15-17) BJ81796 SW8082 8/29/15 2 PCB-1268 (Aroclor 1268) ug/kg U 44 4414B6 (15-17) BJ81796 SW8082 8/29/15 2 PCB-1221 (Aroclor 1221) ug/kg U 44 4414B6 (15-17) BJ81796 SW8082 8/29/15 2 PCB-1232 (Aroclor 1232) ug/kg U 44 4414B6 (15-17) BJ81796 SW8082 8/29/15 2 PCB-1248 (Aroclor 1248) ug/kg U 44 4414B6 (15-17) BJ81796 SW8082 8/29/15 2 PCB-1016 (Aroclor 1016) ug/kg U 44 4414B6 (15-17) BJ81796 SW8082 8/29/15 2 PCB-1262 (Aroclor 1262) ug/kg U 44 4414B6 (15-17) BJ81796 SW8082 8/29/15 2 PCB-1242 (Aroclor 1242) ug/kg U 44 4414B6 (15-17) BJ81796 SW8260 9/1/15 50 Ethylbenzene 280 ug/kg J 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Styrene ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Cis-1,3-Dichloropropene ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Trans-1,3-Dichloropropene ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 N-Propylbenzene ug/kg U 72 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 N-Butylbenzene 63 ug/kg J 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 4-Chlorotoluene ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,4-Dichlorobenzene ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,2-Dibromoethane (Ethylene Dibromide) ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Acrolein ug/kg U 200 160014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,2-Dichloroethane ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Acrylonitrile ug/kg U 40 160014B6 (15-17) BJ81796 SW8260 9/1/15 50 Methyl Isobutyl Ketone (4-Methyl-2-Pentanone) ug/kg U 400 200014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,3,5-Trimethylbenzene (Mesitylene) 47 ug/kg J 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Bromobenzene ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Toluene 150 ug/kg J 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Chlorobenzene ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Tetrahydrofuran ug/kg U 200 80014B6 (15-17) BJ81796 SW8260 9/1/15 50 Trans-1,4-Dichloro-2-Butene ug/kg U 200 800

Page 56 of 82



SDG: GBJ81780



14B6 (15-17) BJ81796 SW8260 9/1/15 50 1,2,4-Trichlorobenzene ug/kg U 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,4-Dioxane (P-Dioxane) ug/kg U 3200 800014B6 (15-17) BJ81796 SW8260 9/1/15 50 Dibromochloromethane ug/kg U 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Tetrachloroethylene (PCE) ug/kg U 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Sec-Butylbenzene ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,3-Dichloropropane ug/kg U 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Cis-1,2-Dichloroethylene 8700 ug/kg 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Trans-1,2-Dichloroethene 94 ug/kg J 40 15014B6 (15-17) BJ81796 SW8260 9/1/15 50 Tert-Butyl Methyl Ether ug/kg U 80 80014B6 (15-17) BJ81796 SW8260 9/1/15 50 m,p-Xylene 270 ug/kg J 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 O-Cymene (O-Isopropyltoluene) ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,3-Dichlorobenzene ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Carbon Tetrachloride ug/kg U 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,1-Dichloropropene ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 2-Hexanone ug/kg U 400 200014B6 (15-17) BJ81796 SW8260 9/1/15 50 2,2-Dichloropropane ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,1,1,2-Tetrachloroethane ug/kg U 80 160014B6 (15-17) BJ81796 SW8260 9/1/15 50 Acetone ug/kg U 400 400014B6 (15-17) BJ81796 SW8260 9/1/15 50 Chloroform ug/kg U 40 25014B6 (15-17) BJ81796 SW8260 9/1/15 50 Benzene 890 ug/kg 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,1,1-Trichloroethane ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Bromomethane ug/kg U 160 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Chloromethane ug/kg U 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Dibromomethane ug/kg U 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Bromochloromethane ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Chloroethane ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Vinyl Chloride 1100 ug/kg 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Methylene Chloride 570 ug/kg J 400 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Carbon Disulfide ug/kg U 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Bromoform ug/kg U 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Bromodichloromethane ug/kg U 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,1-Dichloroethane ug/kg U 80 25014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,1-Dichloroethene ug/kg U 40 30014B6 (15-17) BJ81796 SW8260 9/1/15 50 Tert-Butyl Alcohol ug/kg U 1600 800014B6 (15-17) BJ81796 SW8260 9/1/15 50 Trichlorofluoromethane ug/kg U 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Dichlorodifluoromethane ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,1,2-Trichloro-1,2,2-Trifluoroethane ug/kg U 40 400

Page 57 of 82



SDG: GBJ81780



14B6 (15-17) BJ81796 SW8260 9/1/15 50 1,2-Dichloropropane ug/kg U 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Methyl Ethyl Ketone (2-Butanone) ug/kg U 400 240014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,1,2-Trichloroethane ug/kg U 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Trichloroethylene (TCE) 14000 ug/kg 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,1,2,2-Tetrachloroethane ug/kg U 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,2,3-Trichlorobenzene ug/kg U 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Hexachlorobutadiene ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Naphthalene 2700 ug/kg 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 O-Xylene (1,2-Dimethylbenzene) 130 ug/kg J 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 2-Chlorotoluene ug/kg U 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,2-Dichlorobenzene ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,2,4-Trimethylbenzene 150 ug/kg J 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,2-Dibromo-3-Chloropropane ug/kg U 80 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 1,2,3-Trichloropropane ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 T-Butylbenzene ug/kg U 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Isopropylbenzene (Cumene) 43 ug/kg J 40 40014B6 (15-17) BJ81796 SW8260 9/1/15 50 Cymene 170 ug/kg J 40 40014B6 (15-17) BJ81796 SW8270 8/27/15 1 4-Nitroaniline ug/kg U 150 90014B6 (15-17) BJ81796 SW8270 8/27/15 1 4-Nitrophenol ug/kg U 200 45014B6 (15-17) BJ81796 SW8270 8/27/15 1 4-Bromophenyl Phenyl Ether ug/kg U 130 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 2,4-Dimethylphenol ug/kg U 110 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 1,4-Dichlorobenzene ug/kg U 130 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 4-Chloroaniline ug/kg U 210 36014B6 (15-17) BJ81796 SW8270 8/27/15 1 Phenol ug/kg U 140 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Pyridine ug/kg U 110 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Bis(2-Chloroethyl) Ether (2-Chloroethyl Ether) ug/kg U 120 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Bis(2-Chloroethoxy) Methane ug/kg U 120 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Bis(2-Ethylhexyl) Phthalate ug/kg U 130 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Di-N-Octylphthalate ug/kg U 120 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Hexachlorobenzene ug/kg U 130 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Anthracene 3900 ug/kg 150 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 1,2,4-Trichlorobenzene ug/kg U 140 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 2,4-Dichlorophenol ug/kg U 160 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 2,4-Dinitrotoluene ug/kg U 180 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 1,2-Diphenylhydrazine ug/kg U 150 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Pyrene 7200 ug/kg 150 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Dimethyl Phthalate ug/kg U 140 310

Page 58 of 82



SDG: GBJ81780



14B6 (15-17) BJ81796 SW8270 8/27/15 1 Dibenzofuran 3200 ug/kg 130 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Benzo(G,H,I)Perylene 5100 ug/kg 150 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Indeno(1,2,3-C,D)Pyrene 6200 ug/kg 150 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Benzo(B)Fluoranthene 8800 ug/kg 150 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Fluoranthene 8800 ug/kg 150 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Benzo(K)Fluoranthene 4600 ug/kg 150 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Acenaphthylene 620 ug/kg 130 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Chrysene 6100 ug/kg 150 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 2,2-Oxybis(2-Chloropropane) ug/kg U 120 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Benzo(A)Pyrene 2100 ug/kg 150 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 2,4-Dinitrophenol ug/kg UJ 310 90014B6 (15-17) BJ81796 SW8270 8/27/15 1 4,6-Dinitro-2-Methylphenol ug/kg UJ 480 220014B6 (15-17) BJ81796 SW8270 8/27/15 1 Dibenz(A,H)Anthracene 1900 ug/kg 150 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 1,3-Dichlorobenzene ug/kg U 130 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Benzo(A)Anthracene 6300 ug/kg 150 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 4-Chloro-3-Methylphenol ug/kg U 160 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 2,6-Dinitrotoluene ug/kg U 140 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 N-Nitrosodi-N-Propylamine ug/kg U 150 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Aniline ug/kg U 360 36014B6 (15-17) BJ81796 SW8270 8/27/15 1 N-Nitrosodimethylamine ug/kg U 130 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Benzoic Acid ug/kg R 900 220014B6 (15-17) BJ81796 SW8270 8/27/15 1 Hexachloroethane ug/kg U 130 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 4-Chlorophenyl Phenyl Ether ug/kg U 150 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Hexachlorocyclopentadiene ug/kg UJ 140 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Isophorone ug/kg U 130 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Pentachloronitrobenzene ug/kg U 170 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Acenaphthene 330 ug/kg 140 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Diethyl Phthalate ug/kg U 140 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Di-N-Butyl Phthalate ug/kg U 120 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Phenanthrene 8100 ug/kg 130 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Benzyl Butyl Phthalate ug/kg U 120 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 N-Nitrosodiphenylamine ug/kg U 170 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Fluorene 3700 ug/kg 150 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Carbazole 1700 ug/kg J 340 220014B6 (15-17) BJ81796 SW8270 8/27/15 1 Hexachlorobutadiene ug/kg U 160 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Pentachlorophenol ug/kg UJ 170 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 2,4,6-Trichlorophenol ug/kg U 140 310

Page 59 of 82



SDG: GBJ81780



14B6 (15-17) BJ81796 SW8270 8/27/15 1 2-Nitroaniline ug/kg U 450 90014B6 (15-17) BJ81796 SW8270 8/27/15 1 2-Nitrophenol ug/kg U 290 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Naphthalene 4300 ug/kg 130 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 2-Methylnaphthalene ug/kg U 130 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 2-Chloronaphthalene ug/kg U 130 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 3,3'-Dichlorobenzidine ug/kg U 210 90014B6 (15-17) BJ81796 SW8270 8/27/15 1 2-Methylphenol (O-Cresol) ug/kg U 210 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 1,2-Dichlorobenzene ug/kg U 130 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 2-Chlorophenol ug/kg U 130 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 1,2,4,5-Tetrachlorobenzene ug/kg U 160 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 2,4,5-Trichlorophenol ug/kg U 250 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Acetophenone ug/kg U 140 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Nitrobenzene ug/kg U 160 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 3-Nitroaniline ug/kg U 900 90014B6 (15-17) BJ81796 SW8270 8/27/15 1 3- And 4- Methylphenol (Total) ug/kg U 180 31014B6 (15-17) BJ81796 SW8270 8/27/15 1 Benzidine ug/kg UJ 260 90014B6 (15-17) BJ81796 SW6010 8/31/15 1 Zinc 26.5 mg/kg 0.43 0.914B4 (0-5) BJ81797 SW6010 8/28/15 10 Iron 15000 mg/kg 33 3314B4 (0-5) BJ81797 SW8260 8/31/15 1 2-Hexanone ug/kg UJ 5.9 3014B4 (0-5) BJ81797 E160.3 8/26/15 1 Solids, Percent 94 %14B4 (0-5) BJ81797 SW6010 8/28/15 10 Aluminum 8810 mg/kg 6.6 3314B4 (0-5) BJ81797 SW6010 8/28/15 10 Manganese 266 mg/kg 3.3 3.314B4 (0-5) BJ81797 SW6010 8/28/15 1 Lead 79.2 mg/kg 0.33 0.714B4 (0-5) BJ81797 SW6010 8/28/15 1 Magnesium 3210 mg/kg 3.3 3.314B4 (0-5) BJ81797 SW6010 8/28/15 1 Nickel 17.0 mg/kg 0.33 0.3314B4 (0-5) BJ81797 SW6010 8/28/15 1 Silver mg/kg U 0.33 0.3314B4 (0-5) BJ81797 SW6010 8/28/15 1 Sodium 374 mg/kg 2.9 714B4 (0-5) BJ81797 SW6010 8/28/15 1 Thallium mg/kg U 1.3 1.314B4 (0-5) BJ81797 SW6010 8/28/15 1 Antimony mg/kg U 1.7 1.714B4 (0-5) BJ81797 SW6010 8/28/15 1 Arsenic 2.6 mg/kg 0.66 0.714B4 (0-5) BJ81797 SW6010 8/28/15 1 Barium 80.9 mg/kg 0.33 0.714B4 (0-5) BJ81797 SW6010 8/28/15 1 Beryllium 0.35 mg/kg 0.13 0.2714B4 (0-5) BJ81797 SW6010 8/28/15 1 Cadmium mg/kg U 0.13 0.3314B4 (0-5) BJ81797 SW6010 8/28/15 1 Chromium, Total 17.1 mg/kg 0.33 0.3314B4 (0-5) BJ81797 SW6010 8/28/15 1 Cobalt 6.24 mg/kg 0.33 0.3314B4 (0-5) BJ81797 SW6010 8/28/15 1 Copper 22.2 mg/kg 0.33 0.3314B4 (0-5) BJ81797 SW6010 8/28/15 1 Vanadium 29.5 mg/kg 0.33 0.3

Page 60 of 82



SDG: GBJ81780



14B4 (0-5) BJ81797 SW6010 8/28/15 1 Calcium 5440 mg/kg 3.1 3.314B4 (0-5) BJ81797 SW6010 8/28/15 1 Selenium mg/kg U 1.1 1.314B4 (0-5) BJ81797 SW7471 8/27/15 1 Mercury 0.05 mg/kg 0.02 0.0314B4 (0-5) BJ81797 SW8081 8/28/15 2 Heptachlor Epoxide ug/kg U 6.9 6.914B4 (0-5) BJ81797 SW8081 8/28/15 2 Endosulfan Sulfate ug/kg U 6.9 6.914B4 (0-5) BJ81797 SW8081 8/28/15 2 Aldrin ug/kg U 3.4 3.414B4 (0-5) BJ81797 SW8081 8/28/15 2 Alpha Bhc (Alpha Hexachlorocyclohexane) ug/kg U 6.9 6.914B4 (0-5) BJ81797 SW8081 8/28/15 2 Beta Bhc (Beta Hexachlorocyclohexane) ug/kg U 6.9 6.914B4 (0-5) BJ81797 SW8081 8/28/15 2 Delta BHC (Delta Hexachlorocyclohexane) ug/kg U 6.9 6.914B4 (0-5) BJ81797 SW8081 8/28/15 2 Beta Endosulfan ug/kg U 6.9 6.914B4 (0-5) BJ81797 SW8081 8/28/15 2 P,P'-DDT ug/kg U 2.1 2.114B4 (0-5) BJ81797 SW8081 8/28/15 2 cis-Chlordane 22 ug/kg 3.4 3.414B4 (0-5) BJ81797 SW8081 8/28/15 2 trans-Chlordane 19 ug/kg 3.4 3.414B4 (0-5) BJ81797 SW8081 8/28/15 2 Endrin Ketone ug/kg U 6.9 6.914B4 (0-5) BJ81797 SW8081 8/28/15 2 Gamma Bhc (Lindane) ug/kg U 1.4 1.414B4 (0-5) BJ81797 SW8081 8/28/15 2 Dieldrin ug/kg U 3.4 3.414B4 (0-5) BJ81797 SW8081 8/28/15 2 Endrin ug/kg U 6.9 6.914B4 (0-5) BJ81797 SW8081 8/28/15 2 Methoxychlor ug/kg U 34 3414B4 (0-5) BJ81797 SW8081 8/28/15 2 P,P'-DDD 4.3 ug/kg 3.3 3.314B4 (0-5) BJ81797 SW8081 8/28/15 2 P,P'-DDE 4.0 ug/kg 2.1 2.114B4 (0-5) BJ81797 SW8081 8/28/15 2 Endrin Aldehyde ug/kg U 6.9 6.914B4 (0-5) BJ81797 SW8081 8/28/15 2 Heptachlor ug/kg U 6.9 6.914B4 (0-5) BJ81797 SW8081 8/28/15 2 Toxaphene ug/kg U 140 14014B4 (0-5) BJ81797 SW8081 8/28/15 2 Alpha Endosulfan ug/kg U 6.9 6.914B4 (0-5) BJ81797 SW8082 8/29/15 2 PCB-1260 (Aroclor 1260) ug/kg U 34 3414B4 (0-5) BJ81797 SW8082 8/29/15 2 PCB-1254 (Aroclor 1254) ug/kg U 34 3414B4 (0-5) BJ81797 SW8082 8/29/15 2 PCB-1268 (Aroclor 1268) ug/kg U 34 3414B4 (0-5) BJ81797 SW8082 8/29/15 2 PCB-1221 (Aroclor 1221) ug/kg U 34 3414B4 (0-5) BJ81797 SW8082 8/29/15 2 PCB-1232 (Aroclor 1232) ug/kg U 34 3414B4 (0-5) BJ81797 SW8082 8/29/15 2 PCB-1248 (Aroclor 1248) ug/kg U 34 3414B4 (0-5) BJ81797 SW8082 8/29/15 2 PCB-1016 (Aroclor 1016) ug/kg U 34 3414B4 (0-5) BJ81797 SW8082 8/29/15 2 PCB-1262 (Aroclor 1262) ug/kg U 34 3414B4 (0-5) BJ81797 SW8082 8/29/15 2 PCB-1242 (Aroclor 1242) ug/kg U 34 3414B4 (0-5) BJ81797 SW8260 8/31/15 1 Ethylbenzene ug/kg UJ 0.59 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Styrene ug/kg UJ 0.59 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Cis-1,3-Dichloropropene ug/kg UJ 0.59 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Trans-1,3-Dichloropropene ug/kg UJ 0.59 5.9

Page 61 of 82



SDG: GBJ81780



14B4 (0-5) BJ81797 SW8260 8/31/15 1 1,2-Dibromoethane (Ethylene Dibromide) ug/kg UJ 0.59 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Acrolein ug/kg UJ 3.0 2414B4 (0-5) BJ81797 SW8260 8/31/15 1 Acrylonitrile ug/kg UJ 0.59 2414B4 (0-5) BJ81797 SW8260 8/31/15 1 Methyl Isobutyl Ketone (4-Methyl-2-Pentanone) ug/kg UJ 5.9 3014B4 (0-5) BJ81797 SW8260 8/31/15 1 Toluene 0.72 ug/kg J 0.59 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Chlorobenzene ug/kg UJ 0.59 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Tetrahydrofuran ug/kg UJ 3.0 1214B4 (0-5) BJ81797 SW8260 8/31/15 1 Tetrachloroethylene (PCE) ug/kg UJ 1.2 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 1,3-Dichloropropane ug/kg UJ 1.2 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Cis-1,2-Dichloroethylene 0.73 ug/kg J 0.59 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Trans-1,2-Dichloroethene ug/kg UJ 0.59 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Tert-Butyl Methyl Ether ug/kg UJ 1.2 1214B4 (0-5) BJ81797 SW8260 8/31/15 1 m,p-Xylene ug/kg UJ 1.2 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 1,1-Dichloropropene ug/kg UJ 0.59 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 2,2-Dichloropropane ug/kg UJ 0.59 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Chloroform ug/kg UJ 0.59 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Benzene ug/kg UJ 0.59 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Chloromethane ug/kg UJ 1.2 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Dibromomethane ug/kg UJ 1.2 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Bromochloromethane ug/kg UJ 0.59 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Vinyl Chloride ug/kg UJ 0.59 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Carbon Disulfide ug/kg UJ 1.2 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 1,1-Dichloroethane ug/kg UJ 1.2 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 1,1-Dichloroethene ug/kg UJ 0.59 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 1,1,2-Trichloro-1,2,2-Trifluoroethane ug/kg UJ 0.59 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 1,2-Dichloropropane ug/kg UJ 1.2 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 1,1,2-Trichloroethane ug/kg UJ 1.2 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 1,1,2,2-Tetrachloroethane ug/kg UJ 1.2 5.914B4 (0-5) BJ81797 SW8260 9/1/15 50 N-Propylbenzene ug/kg U 48 27014B4 (0-5) BJ81797 SW8260 9/1/15 50 N-Butylbenzene ug/kg U 27 27014B4 (0-5) BJ81797 SW8260 9/1/15 50 4-Chlorotoluene ug/kg U 27 27014B4 (0-5) BJ81797 SW8260 9/1/15 50 1,4-Dichlorobenzene ug/kg U 27 27014B4 (0-5) BJ81797 SW8260 9/1/15 50 1,3,5-Trimethylbenzene (Mesitylene) ug/kg U 27 27014B4 (0-5) BJ81797 SW8260 9/1/15 50 Bromobenzene ug/kg U 27 27014B4 (0-5) BJ81797 SW8260 9/1/15 50 1,2,4-Trichlorobenzene ug/kg U 54 27014B4 (0-5) BJ81797 SW8260 9/1/15 50 Sec-Butylbenzene ug/kg U 27 27014B4 (0-5) BJ81797 SW8260 9/1/15 50 O-Cymene (O-Isopropyltoluene) ug/kg U 27 270

Page 62 of 82



SDG: GBJ81780



14B4 (0-5) BJ81797 SW8260 9/1/15 50 1,3-Dichlorobenzene ug/kg U 27 27014B4 (0-5) BJ81797 SW8260 9/1/15 50 Trichloroethylene (TCE) 360 ug/kg 27 27014B4 (0-5) BJ81797 SW8260 9/1/15 50 1,2,3-Trichlorobenzene ug/kg U 54 27014B4 (0-5) BJ81797 SW8260 9/1/15 50 Naphthalene 61 ug/kg J 54 27014B4 (0-5) BJ81797 SW8260 9/1/15 50 2-Chlorotoluene ug/kg U 54 27014B4 (0-5) BJ81797 SW8260 9/1/15 50 1,2-Dichlorobenzene ug/kg U 27 27014B4 (0-5) BJ81797 SW8260 9/1/15 50 1,2,4-Trimethylbenzene ug/kg U 27 27014B4 (0-5) BJ81797 SW8260 9/1/15 50 1,2-Dibromo-3-Chloropropane ug/kg U 54 27014B4 (0-5) BJ81797 SW8260 9/1/15 50 1,2,3-Trichloropropane ug/kg U 27 27014B4 (0-5) BJ81797 SW8260 9/1/15 50 T-Butylbenzene ug/kg U 27 27014B4 (0-5) BJ81797 SW8260 9/1/15 50 Isopropylbenzene (Cumene) ug/kg U 27 27014B4 (0-5) BJ81797 SW8260 9/1/15 50 Cymene ug/kg U 27 27014B4 (0-5) BJ81797 SW8270 8/27/15 1 4-Nitroaniline ug/kg U 120 70014B4 (0-5) BJ81797 SW8270 8/27/15 1 4-Nitrophenol ug/kg U 160 35014B4 (0-5) BJ81797 SW8270 8/27/15 1 4-Bromophenyl Phenyl Ether ug/kg U 100 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 2,4-Dimethylphenol ug/kg U 86 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 1,4-Dichlorobenzene ug/kg U 100 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 4-Chloroaniline ug/kg U 160 28014B4 (0-5) BJ81797 SW8270 8/27/15 1 Phenol ug/kg U 110 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Pyridine ug/kg UJ 86 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Bis(2-Chloroethyl) Ether (2-Chloroethyl Ether) ug/kg U 94 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Bis(2-Chloroethoxy) Methane ug/kg U 96 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Bis(2-Ethylhexyl) Phthalate ug/kg U 100 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Di-N-Octylphthalate ug/kg U 90 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Hexachlorobenzene ug/kg U 100 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Anthracene 120 ug/kg J 110 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 1,2,4-Trichlorobenzene ug/kg U 110 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 2,4-Dichlorophenol ug/kg U 120 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 2,4-Dinitrotoluene ug/kg U 140 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 1,2-Diphenylhydrazine ug/kg U 110 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Pyrene 690 ug/kg 120 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Dimethyl Phthalate ug/kg U 110 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Dibenzofuran ug/kg U 100 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Benzo(G,H,I)Perylene 430 ug/kg 110 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Indeno(1,2,3-C,D)Pyrene 500 ug/kg 120 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Benzo(B)Fluoranthene 420 ug/kg 120 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Fluoranthene 770 ug/kg 110 240

Page 63 of 82



SDG: GBJ81780



14B4 (0-5) BJ81797 SW8270 8/27/15 1 Benzo(K)Fluoranthene 490 ug/kg 120 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Acenaphthylene ug/kg U 98 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Chrysene 510 ug/kg 120 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 2,2-Oxybis(2-Chloropropane) ug/kg U 97 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Benzo(A)Pyrene 600 ug/kg 110 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 2,4-Dinitrophenol ug/kg UJ 240 70014B4 (0-5) BJ81797 SW8270 8/27/15 1 4,6-Dinitro-2-Methylphenol ug/kg UJ 380 170014B4 (0-5) BJ81797 SW8270 8/27/15 1 Dibenz(A,H)Anthracene 150 ug/kg J 110 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 1,3-Dichlorobenzene ug/kg U 100 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Benzo(A)Anthracene 480 ug/kg 120 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 4-Chloro-3-Methylphenol ug/kg U 120 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 2,6-Dinitrotoluene ug/kg U 110 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 N-Nitrosodi-N-Propylamine ug/kg U 110 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Aniline ug/kg U 280 28014B4 (0-5) BJ81797 SW8270 8/27/15 1 N-Nitrosodimethylamine ug/kg U 98 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Benzoic Acid ug/kg R 700 170014B4 (0-5) BJ81797 SW8270 8/27/15 1 Hexachloroethane ug/kg U 100 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 4-Chlorophenyl Phenyl Ether ug/kg U 120 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Hexachlorocyclopentadiene ug/kg UJ 110 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Isophorone ug/kg U 98 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Pentachloronitrobenzene ug/kg U 130 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Acenaphthene ug/kg U 110 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Diethyl Phthalate ug/kg U 110 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Di-N-Butyl Phthalate ug/kg U 93 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Phenanthrene 470 ug/kg 100 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Benzyl Butyl Phthalate ug/kg U 90 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 N-Nitrosodiphenylamine ug/kg U 130 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Fluorene ug/kg U 120 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Carbazole ug/kg U 260 170014B4 (0-5) BJ81797 SW8270 8/27/15 1 Hexachlorobutadiene ug/kg U 130 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Pentachlorophenol ug/kg UJ 130 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 2,4,6-Trichlorophenol ug/kg U 110 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 2-Nitroaniline ug/kg U 350 70014B4 (0-5) BJ81797 SW8270 8/27/15 1 2-Nitrophenol ug/kg U 220 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Naphthalene ug/kg U 100 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 2-Methylnaphthalene ug/kg U 100 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 2-Chloronaphthalene ug/kg U 99 240

Page 64 of 82



SDG: GBJ81780



14B4 (0-5) BJ81797 SW8270 8/27/15 1 3,3'-Dichlorobenzidine ug/kg U 160 70014B4 (0-5) BJ81797 SW8270 8/27/15 1 2-Methylphenol (O-Cresol) ug/kg U 160 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 1,2-Dichlorobenzene ug/kg U 98 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 2-Chlorophenol ug/kg U 99 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 1,2,4,5-Tetrachlorobenzene ug/kg U 120 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 2,4,5-Trichlorophenol ug/kg U 190 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Acetophenone ug/kg U 110 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 Nitrobenzene ug/kg U 120 24014B4 (0-5) BJ81797 SW8270 8/27/15 1 3-Nitroaniline ug/kg U 700 70014B4 (0-5) BJ81797 SW8270 8/27/15 1 3- And 4- Methylphenol (Total) ug/kg U 140 24014B4 (0-5) BJ81797 SW8260 8/31/15 1 1,4-Dioxane (P-Dioxane) ug/kg UJ 47 10014B4 (0-5) BJ81797 SW8260 8/31/15 1 Acetone ug/kg UJ 5.9 5014B4 (0-5) BJ81797 SW8260 8/31/15 1 1,2-Dichloroethane ug/kg UJ 0.59 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 O-Xylene (1,2-Dimethylbenzene) ug/kg UJ 1.2 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Carbon Tetrachloride ug/kg UJ 1.2 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 1,1,1,2-Tetrachloroethane ug/kg UJ 1.2 2414B4 (0-5) BJ81797 SW8260 8/31/15 1 1,1,1-Trichloroethane ug/kg UJ 0.59 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Chloroethane ug/kg UJ 0.59 5.914B4 (0-5) BJ81797 SW8260 9/1/15 50 Trans-1,4-Dichloro-2-Butene ug/kg U 130 54014B4 (0-5) BJ81797 SW8260 8/31/15 1 Bromodichloromethane ug/kg UJ 1.2 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Dibromochloromethane ug/kg UJ 1.2 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Tert-Butyl Alcohol ug/kg UJ 24 12014B4 (0-5) BJ81797 SW8260 8/31/15 1 Bromoform ug/kg UJ 1.2 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Trichlorofluoromethane ug/kg UJ 1.2 5.914B4 (0-5) BJ81797 SW8260 8/31/15 1 Dichlorodifluoromethane ug/kg UJ 0.59 5.914B4 (0-5) BJ81797 SW8260 9/1/15 50 Hexachlorobutadiene ug/kg U 27 27014B4 (0-5) BJ81797 SW8260 8/31/15 1 Bromomethane ug/kg UJ 2.4 5.914B4 (0-5) BJ81797 SW6010 8/28/15 1 Zinc 56.7 mg/kg J+ 0.33 0.714B4 (0-5) BJ81797 SW6010 8/28/15 1 Potassium 1310 mg/kg J+ 2.6 714B4 (0-5) BJ81797 SW8260 8/31/15 1 Methylene Chloride ug/kg UJ 5.9 5.914B4 (0-5) BJ81797 SW8270 8/27/15 1 Benzidine ug/kg UJ 200 70014B4 (0-5) BJ81797 SW8260 8/31/15 1 Methyl Ethyl Ketone (2-Butanone) ug/kg UJ 5.9 3514B4 (20-21) BJ81799 SW6010 8/28/15 10 Iron 16700 mg/kg 40 4014B4 (20-21) BJ81799 SW8260 8/30/15 714 2-Hexanone ug/kg UJ 6000 3000014B4 (20-21) BJ81799 E160.3 8/26/15 1 Solids, Percent 79 %14B4 (20-21) BJ81799 SW6010 8/28/15 10 Aluminum 9810 mg/kg 7.9 4014B4 (20-21) BJ81799 SW6010 8/28/15 10 Magnesium 10100 mg/kg 40 40

Page 65 of 82



SDG: GBJ81780



14B4 (20-21) BJ81799 SW6010 8/28/15 10 Manganese 649 mg/kg 4.0 4.014B4 (20-21) BJ81799 SW6010 8/28/15 1 Lead 50.8 mg/kg 0.40 0.814B4 (20-21) BJ81799 SW6010 8/28/15 1 Nickel 11.9 mg/kg 0.40 0.4014B4 (20-21) BJ81799 SW6010 8/28/15 1 Silver mg/kg U 0.40 0.4014B4 (20-21) BJ81799 SW6010 8/28/15 1 Sodium 1100 mg/kg 3.4 814B4 (20-21) BJ81799 SW6010 8/28/15 1 Thallium mg/kg U 1.6 1.614B4 (20-21) BJ81799 SW6010 8/28/15 1 Antimony mg/kg U 2.0 2.014B4 (20-21) BJ81799 SW6010 8/28/15 1 Arsenic 3.3 mg/kg 0.79 0.814B4 (20-21) BJ81799 SW6010 8/28/15 1 Barium 69.7 mg/kg 0.40 0.814B4 (20-21) BJ81799 SW6010 8/28/15 1 Beryllium 0.49 mg/kg 0.16 0.3214B4 (20-21) BJ81799 SW6010 8/28/15 1 Cadmium mg/kg U 0.16 0.4014B4 (20-21) BJ81799 SW6010 8/28/15 1 Chromium, Total 15.7 mg/kg 0.40 0.4014B4 (20-21) BJ81799 SW6010 8/28/15 1 Cobalt 5.40 mg/kg 0.40 0.4014B4 (20-21) BJ81799 SW6010 8/28/15 1 Copper 15.7 mg/kg 0.40 0.4014B4 (20-21) BJ81799 SW6010 8/28/15 1 Vanadium 30.3 mg/kg 0.40 0.414B4 (20-21) BJ81799 SW6010 8/28/15 1 Calcium 11300 mg/kg 3.6 4.014B4 (20-21) BJ81799 SW6010 8/28/15 1 Selenium mg/kg U 1.3 1.614B4 (20-21) BJ81799 SW7471 8/27/15 1 Mercury 0.06 mg/kg 0.02 0.0314B4 (20-21) BJ81799 SW8081 8/28/15 20 Heptachlor Epoxide ug/kg U 82 8214B4 (20-21) BJ81799 SW8081 8/28/15 20 Endosulfan Sulfate ug/kg U 82 8214B4 (20-21) BJ81799 SW8081 8/28/15 20 Aldrin ug/kg U 12 1214B4 (20-21) BJ81799 SW8081 8/28/15 20 Alpha Bhc (Alpha Hexachlorocyclohexane) ug/kg U 41 4114B4 (20-21) BJ81799 SW8081 8/28/15 20 Beta Bhc (Beta Hexachlorocyclohexane) ug/kg U 41 4114B4 (20-21) BJ81799 SW8081 8/28/15 20 Delta BHC (Delta Hexachlorocyclohexane) ug/kg U 41 4114B4 (20-21) BJ81799 SW8081 8/28/15 20 Beta Endosulfan ug/kg U 82 8214B4 (20-21) BJ81799 SW8081 8/28/15 20 P,P'-DDT ug/kg U 30 3014B4 (20-21) BJ81799 SW8081 8/28/15 20 cis-Chlordane 170 ug/kg 41 4114B4 (20-21) BJ81799 SW8081 8/28/15 20 trans-Chlordane 99 ug/kg 41 4114B4 (20-21) BJ81799 SW8081 8/28/15 20 Endrin Ketone ug/kg U 82 8214B4 (20-21) BJ81799 SW8081 8/28/15 20 Gamma Bhc (Lindane) ug/kg U 30 3014B4 (20-21) BJ81799 SW8081 8/28/15 20 Dieldrin ug/kg U 12 1214B4 (20-21) BJ81799 SW8081 8/28/15 20 Endrin ug/kg U 41 4114B4 (20-21) BJ81799 SW8081 8/28/15 20 Methoxychlor ug/kg U 410 41014B4 (20-21) BJ81799 SW8081 8/28/15 20 P,P'-DDD ug/kg U 60 6014B4 (20-21) BJ81799 SW8081 8/28/15 20 P,P'-DDE ug/kg U 40 4014B4 (20-21) BJ81799 SW8081 8/28/15 20 Endrin Aldehyde ug/kg U 82 8214B4 (20-21) BJ81799 SW8081 8/28/15 20 Heptachlor ug/kg U 41 41

Page 66 of 82



SDG: GBJ81780



14B4 (20-21) BJ81799 SW8081 8/28/15 20 Toxaphene ug/kg U 1600 160014B4 (20-21) BJ81799 SW8081 8/28/15 20 Alpha Endosulfan ug/kg U 82 8214B4 (20-21) BJ81799 SW8082 8/29/15 2 PCB-1260 (Aroclor 1260) ug/kg U 41 4114B4 (20-21) BJ81799 SW8082 8/29/15 2 PCB-1254 (Aroclor 1254) ug/kg U 41 4114B4 (20-21) BJ81799 SW8082 8/29/15 2 PCB-1268 (Aroclor 1268) ug/kg U 41 4114B4 (20-21) BJ81799 SW8082 8/29/15 2 PCB-1221 (Aroclor 1221) ug/kg U 41 4114B4 (20-21) BJ81799 SW8082 8/29/15 2 PCB-1232 (Aroclor 1232) ug/kg U 41 4114B4 (20-21) BJ81799 SW8082 8/29/15 2 PCB-1248 (Aroclor 1248) ug/kg U 41 4114B4 (20-21) BJ81799 SW8082 8/29/15 2 PCB-1016 (Aroclor 1016) ug/kg U 41 4114B4 (20-21) BJ81799 SW8082 8/29/15 2 PCB-1262 (Aroclor 1262) ug/kg U 41 4114B4 (20-21) BJ81799 SW8082 8/29/15 2 PCB-1242 (Aroclor 1242) ug/kg U 41 4114B4 (20-21) BJ81799 SW8260 8/30/15 714 Ethylbenzene 21000 ug/kg 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Styrene 1100 ug/kg J 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Cis-1,3-Dichloropropene ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Trans-1,3-Dichloropropene ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 N-Propylbenzene ug/kg U 1100 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 N-Butylbenzene ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 4-Chlorotoluene ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,4-Dichlorobenzene ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,2-Dibromoethane (Ethylene Dibromide) ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Acrolein ug/kg U 3000 2400014B4 (20-21) BJ81799 SW8260 8/30/15 714 Acrylonitrile ug/kg U 1200 1200014B4 (20-21) BJ81799 SW8260 8/30/15 714 Methyl Isobutyl Ketone (4-Methyl-2-Pentanone) ug/kg U 6000 3000014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,3,5-Trimethylbenzene (Mesitylene) 16000 ug/kg 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Bromobenzene ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Toluene 22000 ug/kg 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Chlorobenzene ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Tetrahydrofuran ug/kg U 3000 1200014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,2,4-Trichlorobenzene ug/kg U 1200 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Tetrachloroethylene (PCE) ug/kg U 1200 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Sec-Butylbenzene ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,3-Dichloropropane ug/kg U 1200 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Cis-1,2-Dichloroethylene 730 ug/kg J 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Trans-1,2-Dichloroethene ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Tert-Butyl Methyl Ether ug/kg U 1200 1200014B4 (20-21) BJ81799 SW8260 8/30/15 714 m,p-Xylene 62000 ug/kg 1200 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 O-Cymene (O-Isopropyltoluene) ug/kg U 600 6000

Page 67 of 82



SDG: GBJ81780



14B4 (20-21) BJ81799 SW8260 8/30/15 714 1,3-Dichlorobenzene ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,1-Dichloropropene ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 2,2-Dichloropropane ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Chloroform ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Benzene 8600 ug/kg 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Chloromethane ug/kg U 1200 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Dibromomethane ug/kg U 1200 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Bromochloromethane ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Vinyl Chloride ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Carbon Disulfide ug/kg U 1200 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,1-Dichloroethane ug/kg U 1200 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,1-Dichloroethene ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,1,2-Trichloro-1,2,2-Trifluoroethane ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,2-Dichloropropane ug/kg U 1200 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,1,2-Trichloroethane ug/kg U 1200 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Trichloroethylene (TCE) ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,1,2,2-Tetrachloroethane ug/kg U 1200 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,2,3-Trichlorobenzene ug/kg U 1200 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 2-Chlorotoluene ug/kg U 1200 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,2-Dichlorobenzene ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,2,4-Trimethylbenzene 27000 ug/kg 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,2-Dibromo-3-Chloropropane ug/kg U 1200 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,2,3-Trichloropropane ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 T-Butylbenzene ug/kg U 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Isopropylbenzene (Cumene) 910 ug/kg J 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Cymene 780 ug/kg J 600 600014B4 (20-21) BJ81799 SW8260 8/31/15 10000 Naphthalene 620000 ug/kg 17000 8500014B4 (20-21) BJ81799 SW8270 8/27/15 10 4-Nitroaniline ug/kg U 1400 820014B4 (20-21) BJ81799 SW8270 8/27/15 10 4-Nitrophenol ug/kg U 1900 410014B4 (20-21) BJ81799 SW8270 8/27/15 10 4-Bromophenyl Phenyl Ether ug/kg U 1200 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 2,4-Dimethylphenol ug/kg U 1000 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 1,4-Dichlorobenzene ug/kg U 1200 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 4-Chloroaniline ug/kg U 1900 330014B4 (20-21) BJ81799 SW8270 8/27/15 10 Phenol ug/kg U 1300 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Pyridine ug/kg U 1000 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Bis(2-Chloroethyl) Ether (2-Chloroethyl Ether) ug/kg U 1100 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Bis(2-Chloroethoxy) Methane ug/kg U 1100 2900

Page 68 of 82



SDG: GBJ81780



14B4 (20-21) BJ81799 SW8270 8/27/15 10 Bis(2-Ethylhexyl) Phthalate ug/kg U 1200 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Di-N-Octylphthalate ug/kg U 1100 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Hexachlorobenzene ug/kg U 1200 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Anthracene 50000 ug/kg 1300 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 1,2,4-Trichlorobenzene ug/kg U 1200 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 2,4-Dichlorophenol ug/kg U 1400 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 2,4-Dinitrotoluene ug/kg U 1600 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 1,2-Diphenylhydrazine ug/kg U 1300 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Pyrene 73000 ug/kg 1400 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Dimethyl Phthalate ug/kg U 1300 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Dibenzofuran 43000 ug/kg 1200 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Benzo(G,H,I)Perylene 9700 ug/kg J 1300 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Indeno(1,2,3-C,D)Pyrene 11000 ug/kg J 1400 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Benzo(B)Fluoranthene 21000 ug/kg J 1400 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Benzo(K)Fluoranthene 26000 ug/kg J 1400 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Acenaphthylene 20000 ug/kg 1200 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Chrysene 38000 ug/kg 1400 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 2,2-Oxybis(2-Chloropropane) ug/kg U 1100 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Benzo(A)Pyrene 28000 ug/kg J 1300 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 2,4-Dinitrophenol ug/kg UJ 2900 820014B4 (20-21) BJ81799 SW8270 8/27/15 10 4,6-Dinitro-2-Methylphenol ug/kg UJ 4400 2100014B4 (20-21) BJ81799 SW8270 8/27/15 10 Dibenz(A,H)Anthracene 3800 ug/kg J 1300 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 1,3-Dichlorobenzene ug/kg U 1200 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Benzo(A)Anthracene 41000 ug/kg 1400 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 4-Chloro-3-Methylphenol ug/kg U 1400 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 2,6-Dinitrotoluene ug/kg U 1300 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 N-Nitrosodi-N-Propylamine ug/kg U 1300 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Aniline ug/kg U 3300 330014B4 (20-21) BJ81799 SW8270 8/27/15 10 N-Nitrosodimethylamine ug/kg U 1200 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Benzoic Acid ug/kg R 8200 2100014B4 (20-21) BJ81799 SW8270 8/27/15 10 Hexachloroethane ug/kg U 1200 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 4-Chlorophenyl Phenyl Ether ug/kg U 1400 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Hexachlorocyclopentadiene ug/kg UJ 1300 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Isophorone ug/kg U 1200 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Pentachloronitrobenzene ug/kg U 1500 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Acenaphthene 12000 ug/kg 1300 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Diethyl Phthalate ug/kg U 1300 2900

Page 69 of 82



SDG: GBJ81780



14B4 (20-21) BJ81799 SW8270 8/27/15 10 Di-N-Butyl Phthalate ug/kg U 1100 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Benzyl Butyl Phthalate ug/kg U 1100 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 N-Nitrosodiphenylamine ug/kg U 1600 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Fluorene 66000 ug/kg 1400 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Carbazole 20000 ug/kg J 3100 2100014B4 (20-21) BJ81799 SW8270 8/27/15 10 Hexachlorobutadiene ug/kg U 1500 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Pentachlorophenol ug/kg UJ 1600 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 2,4,6-Trichlorophenol ug/kg U 1300 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 2-Nitroaniline ug/kg U 4200 820014B4 (20-21) BJ81799 SW8270 8/27/15 10 2-Nitrophenol ug/kg U 2600 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 2-Methylnaphthalene 74000 ug/kg 1200 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 2-Chloronaphthalene ug/kg U 1200 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 3,3'-Dichlorobenzidine ug/kg U 1900 820014B4 (20-21) BJ81799 SW8270 8/27/15 10 Benzidine ug/kg U 2400 820014B4 (20-21) BJ81799 SW8270 8/27/15 10 2-Methylphenol (O-Cresol) ug/kg U 1900 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 1,2-Dichlorobenzene ug/kg U 1200 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 2-Chlorophenol ug/kg U 1200 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 1,2,4,5-Tetrachlorobenzene ug/kg U 1400 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 2,4,5-Trichlorophenol ug/kg U 2300 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Acetophenone ug/kg U 1300 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 Nitrobenzene ug/kg U 1400 290014B4 (20-21) BJ81799 SW8270 8/27/15 10 3-Nitroaniline ug/kg U 8200 820014B4 (20-21) BJ81799 SW8270 8/27/15 10 3- And 4- Methylphenol (Total) ug/kg U 1600 290014B4 (20-21) BJ81799 SW8270 8/27/15 50 Fluoranthene 70000 ug/kg 6700 1400014B4 (20-21) BJ81799 SW8270 8/27/15 50 Phenanthrene 140000 ug/kg 5900 1400014B4 (20-21) BJ81799 SW8270 8/27/15 50 Naphthalene 190000 ug/kg 5900 1400014B4 (20-21) BJ81799 SW8260 8/30/15 714 Trans-1,4-Dichloro-2-Butene ug/kg U 3000 1200014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,4-Dioxane (P-Dioxane) ug/kg U 48000 12000014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,2-Dichloroethane ug/kg UJ 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Acetone ug/kg UJ 6000 6000014B4 (20-21) BJ81799 SW8260 8/30/15 714 Carbon Tetrachloride ug/kg UJ 1200 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,1,1,2-Tetrachloroethane ug/kg UJ 1200 2400014B4 (20-21) BJ81799 SW8260 8/30/15 714 1,1,1-Trichloroethane ug/kg UJ 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Bromodichloromethane ug/kg UJ 1200 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 O-Xylene (1,2-Dimethylbenzene) 21000 ug/kg 1200 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Dibromochloromethane ug/kg UJ 1200 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Bromoform ug/kg UJ 1200 6000

Page 70 of 82



SDG: GBJ81780



14B4 (20-21) BJ81799 SW8260 8/30/15 714 Tert-Butyl Alcohol ug/kg UJ 24000 12000014B4 (20-21) BJ81799 SW8260 8/30/15 714 Dichlorodifluoromethane ug/kg UJ 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Trichlorofluoromethane ug/kg UJ 1200 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Hexachlorobutadiene ug/kg UJ 600 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Bromomethane ug/kg UJ 2400 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Chloroethane ug/kg UJ 600 600014B4 (20-21) BJ81799 SW6010 8/31/15 1 Zinc 28.4 mg/kg 0.40 0.814B4 (20-21) BJ81799 SW6010 8/28/15 1 Potassium 1150 mg/kg J+ 3.1 814B4 (20-21) BJ81799 SW8260 8/30/15 714 Methylene Chloride ug/kg U 6000 600014B4 (20-21) BJ81799 SW8260 8/30/15 714 Methyl Ethyl Ketone (2-Butanone) ug/kg UJ 6000 3600014B5 (0-5) BJ81800 SW6010 8/28/15 10 Iron 14900 mg/kg 32 3214B5 (0-5) BJ81800 SW8260 8/30/15 1 2-Hexanone ug/kg UJ 4.8 2414B5 (0-5) BJ81800 E160.3 8/26/15 1 Solids, Percent 92 %14B5 (0-5) BJ81800 SW6010 8/28/15 10 Aluminum 9240 mg/kg 6.5 3214B5 (0-5) BJ81800 SW6010 8/28/15 10 Magnesium 5620 mg/kg 32 3214B5 (0-5) BJ81800 SW6010 8/28/15 10 Manganese 294 mg/kg 3.2 3.214B5 (0-5) BJ81800 SW6010 8/28/15 10 Calcium 14300 mg/kg 30 3214B5 (0-5) BJ81800 SW6010 8/28/15 1 Lead 55.5 mg/kg 0.32 0.614B5 (0-5) BJ81800 SW6010 8/28/15 1 Nickel 16.1 mg/kg 0.32 0.3214B5 (0-5) BJ81800 SW6010 8/28/15 1 Silver mg/kg U 0.32 0.3214B5 (0-5) BJ81800 SW6010 8/28/15 1 Sodium 321 mg/kg 2.8 614B5 (0-5) BJ81800 SW6010 8/28/15 1 Thallium mg/kg U 1.3 1.314B5 (0-5) BJ81800 SW6010 8/28/15 1 Antimony mg/kg U 1.6 1.614B5 (0-5) BJ81800 SW6010 8/28/15 1 Arsenic 3.4 mg/kg 0.65 0.614B5 (0-5) BJ81800 SW6010 8/28/15 1 Barium 70.1 mg/kg 0.32 0.614B5 (0-5) BJ81800 SW6010 8/28/15 1 Beryllium 0.41 mg/kg 0.13 0.2614B5 (0-5) BJ81800 SW6010 8/28/15 1 Cadmium mg/kg U 0.13 0.3214B5 (0-5) BJ81800 SW6010 8/28/15 1 Chromium, Total 19.2 mg/kg 0.32 0.3214B5 (0-5) BJ81800 SW6010 8/28/15 1 Cobalt 6.94 mg/kg 0.32 0.3214B5 (0-5) BJ81800 SW6010 8/28/15 1 Copper 26.0 mg/kg 0.32 0.3214B5 (0-5) BJ81800 SW6010 8/28/15 1 Vanadium 29.7 mg/kg 0.32 0.314B5 (0-5) BJ81800 SW6010 8/28/15 1 Selenium mg/kg U 1.1 1.314B5 (0-5) BJ81800 SW7471 8/27/15 1 Mercury 0.23 mg/kg 0.02 0.0314B5 (0-5) BJ81800 SW8081 8/28/15 20 Heptachlor Epoxide ug/kg U 70 7014B5 (0-5) BJ81800 SW8081 8/28/15 20 Endosulfan Sulfate ug/kg U 70 7014B5 (0-5) BJ81800 SW8081 8/28/15 20 Aldrin ug/kg U 11 1114B5 (0-5) BJ81800 SW8081 8/28/15 20 Alpha Bhc (Alpha Hexachlorocyclohexane) ug/kg U 35 35

Page 71 of 82



SDG: GBJ81780



14B5 (0-5) BJ81800 SW8081 8/28/15 20 Beta Bhc (Beta Hexachlorocyclohexane) ug/kg U 35 3514B5 (0-5) BJ81800 SW8081 8/28/15 20 Delta BHC (Delta Hexachlorocyclohexane) ug/kg U 35 3514B5 (0-5) BJ81800 SW8081 8/28/15 20 Beta Endosulfan ug/kg U 70 7014B5 (0-5) BJ81800 SW8081 8/28/15 20 P,P'-DDT ug/kg U 21 2114B5 (0-5) BJ81800 SW8081 8/28/15 20 cis-Chlordane ug/kg U 35 3514B5 (0-5) BJ81800 SW8081 8/28/15 20 trans-Chlordane ug/kg U 35 3514B5 (0-5) BJ81800 SW8081 8/28/15 20 Endrin Ketone ug/kg U 70 7014B5 (0-5) BJ81800 SW8081 8/28/15 20 Gamma Bhc (Lindane) ug/kg U 14 1414B5 (0-5) BJ81800 SW8081 8/28/15 20 Dieldrin ug/kg U 11 1114B5 (0-5) BJ81800 SW8081 8/28/15 20 Endrin ug/kg U 35 3514B5 (0-5) BJ81800 SW8081 8/28/15 20 Methoxychlor ug/kg U 350 35014B5 (0-5) BJ81800 SW8081 8/28/15 20 P,P'-DDD ug/kg U 21 2114B5 (0-5) BJ81800 SW8081 8/28/15 20 P,P'-DDE ug/kg U 21 2114B5 (0-5) BJ81800 SW8081 8/28/15 20 Endrin Aldehyde ug/kg U 70 7014B5 (0-5) BJ81800 SW8081 8/28/15 20 Heptachlor ug/kg U 35 3514B5 (0-5) BJ81800 SW8081 8/28/15 20 Toxaphene ug/kg U 1400 140014B5 (0-5) BJ81800 SW8081 8/28/15 20 Alpha Endosulfan ug/kg U 70 7014B5 (0-5) BJ81800 SW8082 8/31/15 2 PCB-1260 (Aroclor 1260) ug/kg U 35 3514B5 (0-5) BJ81800 SW8082 8/31/15 2 PCB-1254 (Aroclor 1254) ug/kg U 35 3514B5 (0-5) BJ81800 SW8082 8/31/15 2 PCB-1268 (Aroclor 1268) ug/kg U 35 3514B5 (0-5) BJ81800 SW8082 8/31/15 2 PCB-1221 (Aroclor 1221) ug/kg U 35 3514B5 (0-5) BJ81800 SW8082 8/31/15 2 PCB-1232 (Aroclor 1232) ug/kg U 35 3514B5 (0-5) BJ81800 SW8082 8/31/15 2 PCB-1248 (Aroclor 1248) ug/kg U 35 3514B5 (0-5) BJ81800 SW8082 8/31/15 2 PCB-1016 (Aroclor 1016) ug/kg U 35 3514B5 (0-5) BJ81800 SW8082 8/31/15 2 PCB-1262 (Aroclor 1262) ug/kg U 35 3514B5 (0-5) BJ81800 SW8082 8/31/15 2 PCB-1242 (Aroclor 1242) ug/kg U 35 3514B5 (0-5) BJ81800 SW8260 8/30/15 1 Ethylbenzene ug/kg UJ 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Styrene ug/kg UJ 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Cis-1,3-Dichloropropene ug/kg UJ 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Trans-1,3-Dichloropropene ug/kg UJ 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 1,2-Dibromoethane (Ethylene Dibromide) ug/kg UJ 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Acrolein ug/kg UJ 2.4 1914B5 (0-5) BJ81800 SW8260 8/30/15 1 Acrylonitrile ug/kg UJ 0.48 1914B5 (0-5) BJ81800 SW8260 8/30/15 1 Methyl Isobutyl Ketone (4-Methyl-2-Pentanone) ug/kg UJ 4.8 2414B5 (0-5) BJ81800 SW8260 8/30/15 1 Toluene ug/kg UJ 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Chlorobenzene ug/kg UJ 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Tetrahydrofuran ug/kg UJ 2.4 9.7

Page 72 of 82



SDG: GBJ81780



14B5 (0-5) BJ81800 SW8260 8/30/15 1 Tetrachloroethylene (PCE) ug/kg UJ 0.97 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 1,3-Dichloropropane ug/kg UJ 0.97 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Cis-1,2-Dichloroethylene 3.7 ug/kg J 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Trans-1,2-Dichloroethene ug/kg UJ 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Tert-Butyl Methyl Ether ug/kg UJ 0.97 9.714B5 (0-5) BJ81800 SW8260 8/30/15 1 m,p-Xylene ug/kg UJ 0.97 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 1,1-Dichloropropene ug/kg UJ 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 2,2-Dichloropropane ug/kg UJ 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Chloroform ug/kg UJ 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Benzene 0.78 ug/kg J 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Chloromethane ug/kg UJ 0.97 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Dibromomethane ug/kg UJ 0.97 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Bromochloromethane ug/kg UJ 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Vinyl Chloride ug/kg UJ 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Carbon Disulfide ug/kg UJ 0.97 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 1,1-Dichloroethane ug/kg UJ 0.97 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 1,1-Dichloroethene ug/kg UJ 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 1,1,2-Trichloro-1,2,2-Trifluoroethane ug/kg UJ 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 1,2-Dichloropropane ug/kg UJ 0.97 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 1,1,2-Trichloroethane ug/kg UJ 0.97 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 1,1,2,2-Tetrachloroethane ug/kg UJ 0.97 4.814B5 (0-5) BJ81800 SW8260 8/31/15 50 N-Propylbenzene ug/kg U 42 23014B5 (0-5) BJ81800 SW8260 8/31/15 50 N-Butylbenzene ug/kg U 23 23014B5 (0-5) BJ81800 SW8260 8/31/15 50 4-Chlorotoluene ug/kg U 23 23014B5 (0-5) BJ81800 SW8260 8/31/15 50 1,4-Dichlorobenzene ug/kg U 23 23014B5 (0-5) BJ81800 SW8260 8/31/15 50 1,3,5-Trimethylbenzene (Mesitylene) ug/kg U 23 23014B5 (0-5) BJ81800 SW8260 8/31/15 50 Bromobenzene ug/kg U 23 23014B5 (0-5) BJ81800 SW8260 8/31/15 50 1,2,4-Trichlorobenzene ug/kg U 47 23014B5 (0-5) BJ81800 SW8260 8/31/15 50 Sec-Butylbenzene ug/kg U 23 23014B5 (0-5) BJ81800 SW8260 8/31/15 50 O-Cymene (O-Isopropyltoluene) ug/kg U 23 23014B5 (0-5) BJ81800 SW8260 8/31/15 50 1,3-Dichlorobenzene ug/kg U 23 23014B5 (0-5) BJ81800 SW8260 8/31/15 50 Trichloroethylene (TCE) 56 ug/kg J 23 23014B5 (0-5) BJ81800 SW8260 8/31/15 50 1,2,3-Trichlorobenzene ug/kg U 47 23014B5 (0-5) BJ81800 SW8260 8/31/15 50 Naphthalene 210 ug/kg J 47 23014B5 (0-5) BJ81800 SW8260 8/31/15 50 2-Chlorotoluene ug/kg U 47 23014B5 (0-5) BJ81800 SW8260 8/31/15 50 1,2-Dichlorobenzene ug/kg U 23 23014B5 (0-5) BJ81800 SW8260 8/31/15 50 1,2,4-Trimethylbenzene ug/kg U 23 230

Page 73 of 82



SDG: GBJ81780



14B5 (0-5) BJ81800 SW8260 8/31/15 50 1,2-Dibromo-3-Chloropropane ug/kg U 47 23014B5 (0-5) BJ81800 SW8260 8/31/15 50 1,2,3-Trichloropropane ug/kg U 23 23014B5 (0-5) BJ81800 SW8260 8/31/15 50 T-Butylbenzene ug/kg U 23 23014B5 (0-5) BJ81800 SW8260 8/31/15 50 Isopropylbenzene (Cumene) ug/kg U 23 23014B5 (0-5) BJ81800 SW8260 8/31/15 50 Cymene ug/kg U 23 23014B5 (0-5) BJ81800 SW8270 8/27/15 1 4-Nitroaniline ug/kg U 120 72014B5 (0-5) BJ81800 SW8270 8/27/15 1 4-Nitrophenol ug/kg U 160 36014B5 (0-5) BJ81800 SW8270 8/27/15 1 4-Bromophenyl Phenyl Ether ug/kg U 110 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 2,4-Dimethylphenol ug/kg U 89 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 1,4-Dichlorobenzene ug/kg U 110 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 4-Chloroaniline ug/kg U 170 29014B5 (0-5) BJ81800 SW8270 8/27/15 1 Phenol ug/kg U 120 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Benzo(B)Fluoranthene 980 ug/kg J 120 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Bis(2-Chloroethyl) Ether (2-Chloroethyl Ether) ug/kg U 97 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Bis(2-Chloroethoxy) Methane ug/kg U 100 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Hexachlorobenzene ug/kg U 110 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Anthracene 210 ug/kg J 120 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 1,2,4-Trichlorobenzene ug/kg U 110 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 2,4-Dichlorophenol ug/kg U 130 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 2,4-Dinitrotoluene ug/kg U 140 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 1,2-Diphenylhydrazine ug/kg U 120 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Chrysene 910 ug/kg J 120 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Dimethyl Phthalate ug/kg U 110 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Dibenzofuran ug/kg U 110 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Benzo(A)Pyrene 1000 ug/kg J 120 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Acenaphthylene 120 ug/kg J 100 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 2,2-Oxybis(2-Chloropropane) ug/kg U 100 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 2,4-Dinitrophenol ug/kg UJ 250 72014B5 (0-5) BJ81800 SW8270 8/27/15 1 4,6-Dinitro-2-Methylphenol ug/kg UJ 390 180014B5 (0-5) BJ81800 SW8270 8/27/15 1 1,3-Dichlorobenzene ug/kg U 110 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 4-Chloro-3-Methylphenol ug/kg U 130 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 2,6-Dinitrotoluene ug/kg U 110 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 N-Nitrosodi-N-Propylamine ug/kg U 120 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Aniline ug/kg U 290 29014B5 (0-5) BJ81800 SW8270 8/27/15 1 Benzo(A)Anthracene 850 ug/kg J 120 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Benzoic Acid ug/kg R 720 180014B5 (0-5) BJ81800 SW8270 8/27/15 1 Hexachloroethane ug/kg U 110 250

Page 74 of 82



SDG: GBJ81780



14B5 (0-5) BJ81800 SW8270 8/27/15 1 4-Chlorophenyl Phenyl Ether ug/kg U 120 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Pyridine ug/kg UJ 89 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Isophorone ug/kg U 100 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Pentachloronitrobenzene ug/kg U 130 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Acenaphthene ug/kg U 110 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Diethyl Phthalate ug/kg U 110 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Di-N-Butyl Phthalate ug/kg U 96 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 N-Nitrosodimethylamine ug/kg UJ 100 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 N-Nitrosodiphenylamine ug/kg U 140 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Fluorene ug/kg U 120 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Carbazole ug/kg U 270 180014B5 (0-5) BJ81800 SW8270 8/27/15 1 Hexachlorobutadiene ug/kg U 130 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Pentachlorophenol ug/kg UJ 140 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 2,4,6-Trichlorophenol ug/kg U 120 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 2-Nitroaniline ug/kg U 360 72014B5 (0-5) BJ81800 SW8270 8/27/15 1 2-Nitrophenol ug/kg U 230 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Naphthalene ug/kg U 100 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 2-Methylnaphthalene ug/kg U 110 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 2-Chloronaphthalene ug/kg U 100 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Benzidine ug/kg UJ 210 72014B5 (0-5) BJ81800 SW8270 8/27/15 1 2-Methylphenol (O-Cresol) ug/kg U 170 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 1,2-Dichlorobenzene ug/kg U 100 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 2-Chlorophenol ug/kg U 100 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 1,2,4,5-Tetrachlorobenzene ug/kg U 130 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 2,4,5-Trichlorophenol ug/kg U 200 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Acetophenone ug/kg U 110 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Nitrobenzene ug/kg U 130 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 3-Nitroaniline ug/kg U 720 72014B5 (0-5) BJ81800 SW8270 8/27/15 1 3- And 4- Methylphenol (Total) ug/kg U 140 25014B5 (0-5) BJ81800 SW8260 8/30/15 1 1,4-Dioxane (P-Dioxane) ug/kg UJ 39 9714B5 (0-5) BJ81800 SW8260 8/30/15 1 Acetone 11 ug/kg J 4.8 4814B5 (0-5) BJ81800 SW8260 8/30/15 1 1,2-Dichloroethane ug/kg UJ 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 O-Xylene (1,2-Dimethylbenzene) ug/kg UJ 0.97 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Carbon Tetrachloride ug/kg UJ 0.97 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 1,1,1,2-Tetrachloroethane ug/kg UJ 0.97 1914B5 (0-5) BJ81800 SW8260 8/30/15 1 1,1,1-Trichloroethane ug/kg UJ 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Bromomethane ug/kg UJ 1.9 4.8

Page 75 of 82



SDG: GBJ81780



14B5 (0-5) BJ81800 SW8260 8/31/15 50 Trans-1,4-Dichloro-2-Butene ug/kg UJ 120 47014B5 (0-5) BJ81800 SW8260 8/30/15 1 Dibromochloromethane ug/kg UJ 0.97 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Bromodichloromethane ug/kg UJ 0.97 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Bromoform ug/kg UJ 0.97 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Dichlorodifluoromethane ug/kg UJ 0.48 4.814B5 (0-5) BJ81800 SW8260 8/30/15 1 Tert-Butyl Alcohol ug/kg UJ 19 9714B5 (0-5) BJ81800 SW8260 8/30/15 1 Trichlorofluoromethane ug/kg UJ 0.97 4.814B5 (0-5) BJ81800 SW8260 8/31/15 50 Hexachlorobutadiene ug/kg U 23 23014B5 (0-5) BJ81800 SW8260 8/30/15 1 Chloroethane ug/kg UJ 0.48 4.814B5 (0-5) BJ81800 SW6010 8/28/15 1 Zinc 63.9 mg/kg J+ 0.32 0.614B5 (0-5) BJ81800 SW6010 8/28/15 1 Potassium 1940 mg/kg J+ 2.5 614B5 (0-5) BJ81800 SW8260 8/30/15 1 Methylene Chloride ug/kg UJ 4.8 4.814B5 (0-5) BJ81800 SW8270 8/27/15 1 Bis(2-Ethylhexyl) Phthalate 140 ug/kg J 100 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Di-N-Octylphthalate ug/kg UJ 93 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Benzo(G,H,I)Perylene 660 ug/kg J 120 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Indeno(1,2,3-C,D)Pyrene 710 ug/kg J 120 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Hexachlorocyclopentadiene ug/kg R 110 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Benzo(K)Fluoranthene 870 ug/kg J 120 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Pyrene 1100 ug/kg J 120 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Fluoranthene 1300 ug/kg J 120 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Dibenz(A,H)Anthracene 250 ug/kg J 120 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Phenanthrene 750 ug/kg J 100 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 Benzyl Butyl Phthalate ug/kg UJ 93 25014B5 (0-5) BJ81800 SW8270 8/27/15 1 3,3'-Dichlorobenzidine ug/kg UJ 170 72014B5 (0-5) BJ81800 SW8260 8/30/15 1 Methyl Ethyl Ketone (2-Butanone) ug/kg UJ 4.8 2914B5 (15-19.5) BJ81802 SW6010 8/28/15 10 Iron 18200 mg/kg 39 3914B5 (15-19.5) BJ81802 SW8260 8/31/15 1 2-Hexanone ug/kg UJ 5.0 2514B5 (15-19.5) BJ81802 E160.3 8/26/15 1 Solids, Percent 78 %14B5 (15-19.5) BJ81802 SW6010 8/28/15 10 Aluminum 11800 mg/kg 7.7 3914B5 (15-19.5) BJ81802 SW6010 8/28/15 10 Manganese 406 mg/kg 3.9 3.914B5 (15-19.5) BJ81802 SW6010 8/28/15 1 Lead 52.8 mg/kg 0.39 0.814B5 (15-19.5) BJ81802 SW6010 8/28/15 1 Magnesium 3070 mg/kg 3.9 3.914B5 (15-19.5) BJ81802 SW6010 8/28/15 1 Nickel 20.3 mg/kg 0.39 0.3914B5 (15-19.5) BJ81802 SW6010 8/28/15 1 Silver mg/kg U 0.39 0.3914B5 (15-19.5) BJ81802 SW6010 8/28/15 1 Sodium 206 mg/kg 3.3 814B5 (15-19.5) BJ81802 SW6010 8/28/15 1 Thallium mg/kg U 1.5 1.514B5 (15-19.5) BJ81802 SW6010 8/28/15 1 Antimony mg/kg U 1.9 1.9

Page 76 of 82



SDG: GBJ81780



14B5 (15-19.5) BJ81802 SW6010 8/28/15 1 Arsenic 4.5 mg/kg 0.77 0.814B5 (15-19.5) BJ81802 SW6010 8/28/15 1 Barium 77.7 mg/kg 0.39 0.814B5 (15-19.5) BJ81802 SW6010 8/28/15 1 Beryllium 0.48 mg/kg 0.15 0.3114B5 (15-19.5) BJ81802 SW6010 8/28/15 1 Cadmium mg/kg U 0.15 0.3914B5 (15-19.5) BJ81802 SW6010 8/28/15 1 Chromium, Total 25.3 mg/kg 0.39 0.3914B5 (15-19.5) BJ81802 SW6010 8/28/15 1 Cobalt 8.21 mg/kg 0.39 0.3914B5 (15-19.5) BJ81802 SW6010 8/28/15 1 Copper 24.5 mg/kg 0.39 0.3914B5 (15-19.5) BJ81802 SW6010 8/28/15 1 Vanadium 30.2 mg/kg 0.39 0.414B5 (15-19.5) BJ81802 SW6010 8/28/15 1 Calcium 6810 mg/kg 3.6 3.914B5 (15-19.5) BJ81802 SW6010 8/28/15 1 Selenium mg/kg U 1.3 1.514B5 (15-19.5) BJ81802 SW7471 8/27/15 1 Mercury 0.10 mg/kg 0.02 0.0314B5 (15-19.5) BJ81802 SW8081 8/28/15 20 Heptachlor Epoxide ug/kg U 83 8314B5 (15-19.5) BJ81802 SW8081 8/28/15 20 Endosulfan Sulfate ug/kg U 83 8314B5 (15-19.5) BJ81802 SW8081 8/28/15 20 Aldrin ug/kg U 12 1214B5 (15-19.5) BJ81802 SW8081 8/28/15 20 Alpha Bhc (Alpha Hexachlorocyclohexane) ug/kg U 42 4214B5 (15-19.5) BJ81802 SW8081 8/28/15 20 Beta Bhc (Beta Hexachlorocyclohexane) ug/kg U 42 4214B5 (15-19.5) BJ81802 SW8081 8/28/15 20 Delta BHC (Delta Hexachlorocyclohexane) ug/kg U 42 4214B5 (15-19.5) BJ81802 SW8081 8/28/15 20 Beta Endosulfan ug/kg U 83 8314B5 (15-19.5) BJ81802 SW8081 8/28/15 20 P,P'-DDT ug/kg U 25 2514B5 (15-19.5) BJ81802 SW8081 8/28/15 20 cis-Chlordane ug/kg U 42 4214B5 (15-19.5) BJ81802 SW8081 8/28/15 20 trans-Chlordane ug/kg U 180 18014B5 (15-19.5) BJ81802 SW8081 8/28/15 20 Endrin Ketone ug/kg U 83 8314B5 (15-19.5) BJ81802 SW8081 8/28/15 20 Gamma Bhc (Lindane) ug/kg U 40 4014B5 (15-19.5) BJ81802 SW8081 8/28/15 20 Dieldrin ug/kg U 15 1514B5 (15-19.5) BJ81802 SW8081 8/28/15 20 Endrin ug/kg U 42 4214B5 (15-19.5) BJ81802 SW8081 8/28/15 20 Methoxychlor ug/kg U 420 42014B5 (15-19.5) BJ81802 SW8081 8/28/15 20 P,P'-DDD ug/kg U 25 2514B5 (15-19.5) BJ81802 SW8081 8/28/15 20 P,P'-DDE ug/kg U 25 2514B5 (15-19.5) BJ81802 SW8081 8/28/15 20 Endrin Aldehyde ug/kg U 120 12014B5 (15-19.5) BJ81802 SW8081 8/28/15 20 Heptachlor ug/kg U 42 4214B5 (15-19.5) BJ81802 SW8081 8/28/15 20 Toxaphene ug/kg U 1700 170014B5 (15-19.5) BJ81802 SW8081 8/28/15 20 Alpha Endosulfan ug/kg U 83 8314B5 (15-19.5) BJ81802 SW8082 8/29/15 2 PCB-1260 (Aroclor 1260) ug/kg U 42 4214B5 (15-19.5) BJ81802 SW8082 8/29/15 2 PCB-1254 (Aroclor 1254) ug/kg U 42 4214B5 (15-19.5) BJ81802 SW8082 8/29/15 2 PCB-1268 (Aroclor 1268) ug/kg U 42 4214B5 (15-19.5) BJ81802 SW8082 8/29/15 2 PCB-1221 (Aroclor 1221) ug/kg U 42 4214B5 (15-19.5) BJ81802 SW8082 8/29/15 2 PCB-1232 (Aroclor 1232) ug/kg U 42 42

Page 77 of 82



SDG: GBJ81780



14B5 (15-19.5) BJ81802 SW8082 8/29/15 2 PCB-1248 (Aroclor 1248) ug/kg U 42 4214B5 (15-19.5) BJ81802 SW8082 8/29/15 2 PCB-1016 (Aroclor 1016) ug/kg U 42 4214B5 (15-19.5) BJ81802 SW8082 8/29/15 2 PCB-1262 (Aroclor 1262) ug/kg U 42 4214B5 (15-19.5) BJ81802 SW8082 8/29/15 2 PCB-1242 (Aroclor 1242) ug/kg U 42 4214B5 (15-19.5) BJ81802 SW8260 8/30/15 50 Cis-1,2-Dichloroethylene 50 ug/kg J 35 25014B5 (15-19.5) BJ81802 SW8260 8/30/15 50 m,p-Xylene 77 ug/kg J 70 35014B5 (15-19.5) BJ81802 SW8260 8/30/15 50 Benzene 160 ug/kg 35 6014B5 (15-19.5) BJ81802 SW8260 8/30/15 50 Naphthalene 1100 ug/kg 70 35014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Ethylbenzene 0.96 ug/kg J 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Styrene ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Cis-1,3-Dichloropropene ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Trans-1,3-Dichloropropene ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 N-Propylbenzene ug/kg U 0.90 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 N-Butylbenzene ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 4-Chlorotoluene ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,4-Dichlorobenzene ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,2-Dibromoethane (Ethylene Dibromide) ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Acrolein ug/kg U 2.5 2014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Acrylonitrile ug/kg U 0.50 2014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Methyl Isobutyl Ketone (4-Methyl-2-Pentanone) ug/kg U 5.0 2514B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,3,5-Trimethylbenzene (Mesitylene) ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Bromobenzene ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Toluene 0.51 ug/kg J 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Chlorobenzene ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Tetrahydrofuran ug/kg U 2.5 1014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,2,4-Trichlorobenzene ug/kg U 1.0 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Tetrachloroethylene (PCE) ug/kg U 1.0 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Sec-Butylbenzene ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,3-Dichloropropane ug/kg U 1.0 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Trans-1,2-Dichloroethene ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Tert-Butyl Methyl Ether ug/kg U 1.0 1014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 O-Cymene (O-Isopropyltoluene) ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,3-Dichlorobenzene ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,1-Dichloropropene ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 2,2-Dichloropropane ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Chloroform ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Chloromethane ug/kg U 1.0 5.0

Page 78 of 82



SDG: GBJ81780



14B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Dibromomethane ug/kg U 1.0 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Bromochloromethane ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Vinyl Chloride 2.2 ug/kg J 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Carbon Disulfide 3.4 ug/kg J 1.0 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,1-Dichloroethane ug/kg U 1.0 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,1-Dichloroethene ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,1,2-Trichloro-1,2,2-Trifluoroethane ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,2-Dichloropropane ug/kg U 1.0 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,1,2-Trichloroethane ug/kg U 1.0 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Trichloroethylene (TCE) 2.4 ug/kg J 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,1,2,2-Tetrachloroethane ug/kg U 1.0 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,2,3-Trichlorobenzene ug/kg U 1.0 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 2-Chlorotoluene ug/kg U 1.0 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,2-Dichlorobenzene ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,2,4-Trimethylbenzene ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,2-Dibromo-3-Chloropropane ug/kg U 1.0 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,2,3-Trichloropropane ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 T-Butylbenzene ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Isopropylbenzene (Cumene) ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Cymene ug/kg U 0.50 5.014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 4-Nitroaniline ug/kg U 140 84014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 4-Nitrophenol ug/kg U 190 42014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 4-Bromophenyl Phenyl Ether ug/kg U 120 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 2,4-Dimethylphenol ug/kg U 100 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 1,4-Dichlorobenzene ug/kg U 120 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 4-Chloroaniline ug/kg U 200 34014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Phenol ug/kg U 130 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Pyridine ug/kg U 100 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Bis(2-Chloroethyl) Ether (2-Chloroethyl Ether) ug/kg U 110 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Bis(2-Chloroethoxy) Methane ug/kg U 120 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Bis(2-Ethylhexyl) Phthalate ug/kg U 120 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Di-N-Octylphthalate ug/kg U 110 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Hexachlorobenzene ug/kg U 120 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Anthracene 2700 ug/kg 140 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 1,2,4-Trichlorobenzene ug/kg U 130 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 2,4-Dichlorophenol ug/kg U 150 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 2,4-Dinitrotoluene ug/kg U 170 290

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SDG: GBJ81780



14B5 (15-19.5) BJ81802 SW8270 8/27/15 1 1,2-Diphenylhydrazine ug/kg U 140 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Dimethyl Phthalate ug/kg U 130 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Dibenzofuran 1300 ug/kg 120 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Benzo(K)Fluoranthene 6500 ug/kg 140 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Acenaphthylene 330 ug/kg 120 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 2,2-Oxybis(2-Chloropropane) ug/kg U 120 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 2,4-Dinitrophenol ug/kg UJ 290 84014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 4,6-Dinitro-2-Methylphenol ug/kg UJ 450 210014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Dibenz(A,H)Anthracene 4200 ug/kg 140 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 1,3-Dichlorobenzene ug/kg U 120 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 4-Chloro-3-Methylphenol ug/kg U 150 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 2,6-Dinitrotoluene ug/kg U 130 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 N-Nitrosodi-N-Propylamine ug/kg U 140 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Aniline ug/kg U 340 34014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 N-Nitrosodimethylamine ug/kg U 120 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Benzoic Acid ug/kg R 840 210014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Hexachloroethane ug/kg U 130 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 4-Chlorophenyl Phenyl Ether ug/kg U 140 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Hexachlorocyclopentadiene ug/kg UJ 130 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Isophorone ug/kg U 120 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Pentachloronitrobenzene ug/kg U 160 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Acenaphthene ug/kg U 130 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Diethyl Phthalate ug/kg U 130 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Di-N-Butyl Phthalate ug/kg U 110 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Phenanthrene 5200 ug/kg 120 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Benzyl Butyl Phthalate ug/kg U 110 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 N-Nitrosodiphenylamine ug/kg U 160 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Fluorene 2300 ug/kg 140 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Carbazole 2500 ug/kg 320 210014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Hexachlorobutadiene ug/kg U 150 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Pentachlorophenol ug/kg UJ 160 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 2,4,6-Trichlorophenol ug/kg U 130 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 2-Nitroaniline ug/kg U 430 84014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 2-Nitrophenol ug/kg U 270 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Naphthalene 2300 ug/kg 120 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 2-Methylnaphthalene 470 ug/kg 130 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 2-Chloronaphthalene ug/kg U 120 290

Page 80 of 82



SDG: GBJ81780



14B5 (15-19.5) BJ81802 SW8270 8/27/15 1 3,3'-Dichlorobenzidine ug/kg U 200 84014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 2-Methylphenol (O-Cresol) ug/kg U 200 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 1,2-Dichlorobenzene ug/kg U 120 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 2-Chlorophenol ug/kg U 120 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 1,2,4,5-Tetrachlorobenzene ug/kg U 150 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 2,4,5-Trichlorophenol ug/kg U 230 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Acetophenone ug/kg U 130 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Nitrobenzene ug/kg U 150 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 3-Nitroaniline ug/kg U 840 84014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 3- And 4- Methylphenol (Total) ug/kg U 170 29014B5 (15-19.5) BJ81802 SW8270 8/27/15 5 Pyrene 8100 ug/kg 720 150014B5 (15-19.5) BJ81802 SW8270 8/27/15 5 Benzo(G,H,I)Perylene 6200 ug/kg 680 150014B5 (15-19.5) BJ81802 SW8270 8/27/15 5 Indeno(1,2,3-C,D)Pyrene 7400 ug/kg 700 150014B5 (15-19.5) BJ81802 SW8270 8/27/15 5 Benzo(B)Fluoranthene 9700 ug/kg 720 150014B5 (15-19.5) BJ81802 SW8270 8/27/15 5 Fluoranthene 8500 ug/kg 680 150014B5 (15-19.5) BJ81802 SW8270 8/27/15 5 Chrysene 8200 ug/kg 710 150014B5 (15-19.5) BJ81802 SW8270 8/27/15 5 Benzo(A)Pyrene 14000 ug/kg 690 150014B5 (15-19.5) BJ81802 SW8270 8/27/15 5 Benzo(A)Anthracene 8000 ug/kg 710 150014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Bromomethane ug/kg UJ 2.0 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Trans-1,4-Dichloro-2-Butene ug/kg UJ 2.5 1014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,4-Dioxane (P-Dioxane) ug/kg UJ 40 10014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Acetone 8.7 ug/kg J 5.0 5014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,2-Dichloroethane ug/kg UJ 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Carbon Tetrachloride ug/kg UJ 1.0 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,1,1,2-Tetrachloroethane ug/kg UJ 1.0 2014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 1,1,1-Trichloroethane ug/kg UJ 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 O-Xylene (1,2-Dimethylbenzene) ug/kg UJ 1.0 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Dibromochloromethane ug/kg UJ 1.0 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Bromoform ug/kg UJ 1.0 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Bromodichloromethane ug/kg UJ 1.0 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Tert-Butyl Alcohol ug/kg UJ 20 10014B5 (15-19.5) BJ81802 SW6010 8/28/15 1 Zinc 67.6 mg/kg J+ 0.39 0.814B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Dichlorodifluoromethane ug/kg UJ 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Hexachlorobutadiene ug/kg UJ 0.50 5.014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Trichlorofluoromethane ug/kg UJ 1.0 5.014B5 (15-19.5) BJ81802 SW6010 8/28/15 1 Potassium 1420 mg/kg J+ 3.0 814B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Chloroethane ug/kg UJ 0.50 5.0

Page 81 of 82



SDG: GBJ81780



14B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Methylene Chloride ug/kg U 5.0 5.014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Benzidine ug/kg UJ 250 84014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Methyl Ethyl Ketone (2-Butanone) ug/kg UJ 5.0 30

Page 82 of 82



USEPA Region II –Data Validation Project Name: 510 Driggs Avenue Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBJ89517 Client: Environmental Business Consultants Date: 12/24/2015 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for four (4) water samples for Semi-volatiles

by SW-846 Method 8270D [full scan and Selected Ion Monitoring (SIM)] in accordance with the NYSDEC, Analytical Services Protocol (ASP) Format.









Collection Date


14MW 5 BJ89517 9/08/15 SVO Water 14MW 6 BJ89518 9/08/15 SVO Water 14MW 7 BJ89519 9/08/15 SVO Water

DUPLICATE BJ89520 9/08/15 SVO Water Field Duplicate to sample 14MW 6 Sample Conditions/Problems: 1. The Traffic Reports/Chain-of-Custody Records, Sampling Report and/or Laboratory Case


Holding Times: 1. All water samples were extracted within 7 days from sample collection and analyzed

within 40 days following sample extraction. No qualifications were required. GC/MS Tuning: 1. All of the DFTPP tunes in the initial and continuing calibrations met the percent relative

abundance criteria. No qualifications were required. Initial Calibration: 1. Initial calibration curve analyzed on 09/10/2015 (CHEM05)-Full Scan exhibited

acceptable %RSD (30.0%) for CCC compounds and average RRF values for SPCC compounds. Also, %RSDs for all other compounds were 20.0% and average RRF (>0.050). No qualifications were required.

2. Initial calibration curve analyzed on 09/10/2015 (CHEM04)-SIM Scan exhibited



Continuing Calibration Verification (CCV): 1. CCV analyzed on 09/14/2015 @ 08:07 (CHEM05)-Full scan exhibited acceptable %Ds

(40.0%) for CCC compounds and RRF values for SPCC compounds. Also, %Ds for all other compounds were 25.0%. No qualifications were required.

2. CCV analyzed on 09/14/2015 @ 17:49 (CHEM05)-Full scan exhibited acceptable %Ds


3. CCV analyzed on 09/11/2015 @ 09:06 (CHEM04)-SIM scan exhibited acceptable %Ds




Surrogates: 1. All surrogate %REC values were within the QC acceptance limits for the full scan. No

qualifications were required. 2. All surrogate %REC values were within the QC acceptance limits for the SIM scan. No

qualifications were required. Internal Standard (IS) Area Performance: 1. All samples exhibited acceptable area count for all six internal standards. No

qualifications were required. Method Blank (MB), Storage Blank (SB), Trip Blank (TB), Field Blank (FB), Rinsate Blank (RB) and Equipment Blank (EB): 1. Method Blank (BJ89518 BLANK)-full Scan associated with the water samples extracted

on 09/09/2015 and analyzed on 09/14/2015 was free of contamination. No qualifications were required.

2. Method Blank (BJ89518 BLANK)-SIM Scan associated with the water samples extracted



Laboratory Control Sample (LCS)/ Laboratory Control Sample Duplicate (LCSD): 1. Laboratory Control Sample and Laboratory Control Sample Duplicate associated with

Batch ID: BJ89518-SIM were analyzed on 09/11/2015. All %RECs and RPDs were within the laboratory control limits. No qualifications were required.


Batch ID: BJ89518 were analyzed on 09/14/2015. All %RECs and RPDs were within the laboratory control limits with the following exception(s):


Affected Action

N-Nitrosodimethylanmine A/A/29.9 14MW 6, 14MW 7 1MW 5 DUPLICATE

UJ

Pyridine A/A/39.2 14MW 6, 14MW 7 1MW 5 DUPLICATE

UJ

Hexachlorocyclopentadiene A/A/27.0 14MW 6, 14MW 7 1MW 5 DUPLICATE

UJ

Benzidine A/A/89.4 14MW 6, 14MW 7 1MW 5 DUPLICATE

UJ

Field Duplicate: 1. Sample DUPLICATE (BJ89520) was collected as a field duplicate of sample 14MW 6

(BJ89518). Both sample results were reported as non-detects with the exception of chrysene. Chrysene was detected in the field sample duplicate but was non-detect in the field sample.

Matrix Spike (MS)/Matrix Spike Duplicate (MSD): 1. Matrix Spike (MS)/Matrix Spike Duplicate (MSD) were performed on sample 14MW 6

(BJ89518). All %RECs/RPDs were within the laboratory control limits with the following exception(s):

Compound %R/%R/RPD Action N-Nitrosodimethylamine A/A/40.7 UJ

Pyridine A/A/62.5 UJ(1) Phenol A/A/28.6 UJ Aniline A/A/47.8 UJ

Benzoic Acid 122/A/A UJ Benzidine 0/0/NC UJ(1)

3,3’-Dichlorobenzidine 4/2/64.4 UJ A= Acceptable


NC=Not calculated Target Compound Identification: 1. All Relative Retention Times (RRTs) of the reported compounds were within 0.06


2. Sample compound spectra were compared against the laboratory standard spectra. 3. No QC deviations were observed. Compound Quantitation and Reported Detection Limits: 1. All sample results were reported within the linear calibration range. 2. Manual Calculation:

Cx = (Ax)(IS)(VE)(DF) (Ais)(RRF)(Volume injected, L)(V)

Cx = concentration of analyte as ug/L Ax = Area of the characteristic ion for the compound to be measured, counts. Ais = Area of the characteristic ion for the specific internal standard, counts. IS = Concentration of the internal standard spiking mixture, ng RRF= Mean relative response factor from the initial calibration. DF = Dilution factor calculated. If no dilution is performed, DF= 1 V= Volume for liquids in ml, weight for soils/solids in grams. VE= final volume of concentrated extract Sample: 14MW 5 (BJ89517)

Benzo(b)fluoranthene Initial Volume: 1000ml Final volume: 1ml Volume injected: 1l Dilution Factor: 1 Concentration (g/L) = 5297 x 4 x 1ml x 1 x 1000 = 0.0173g/L 880810 x 1.386 x 1l x 1000ml

Compound Laboratory

(g/L) Validation

(g/L) %D

Benzo(b)fluoranthene 0.02 0.02 0.0


Comments: 1. Semivolatile data package meet requirement for New York State Department of





USEPA Region II –Data Validation Project Name: 510 Driggs Avenue Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBJ89517 Client: Environmental Business Consultants Date: 12/27/2015 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for four (4) water samples analyzed for

Volatiles by SW-846 Method 8260C in accordance to NYSDEC, Analytical Services Protocol (ASP) Format.



3. The USEPA Region-II SOP HW-24, Revision 2, August 2008, Validating Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry, SW-846 Method 8260B was used in evaluating the Volatiles data in this summary report.






Collection Date


14MW 5 BJ89517 9/08/15 VOA Water 14MW 6 BJ89518 9/08/15 VOA Water 14MW 7 BJ89519 9/08/15 VOA Water

DUPLICATE BJ89520 9/08/15 VOA Water Field Duplicate to sample 14MW 6 Sample Conditions/Problems: 1. The Traffic Reports/Chain-of-Custody Records, Sampling Report and/or Laboratory Case


Holding Times: 1. All water samples were analyzed within 14 days from sample collection. No

qualifications were required. GC/MS Tuning: 1. All of the BFB tunes in the initial and continuing calibrations met the percent relative

abundance criteria. No qualifications were required. Initial Calibration: 1. Initial calibration curve analyzed on 09/08/2015 (Chem17) exhibited acceptable %RSDs

(30.0%) for CCC compounds and average RRF values for SPCC compounds. Also, %RSDs for all other compounds, were 20.0% and average RRF (>0.050) with the following exception(s):

Compound RRF %D

Bromomethane A 21.7 A= Acceptable



Compound Action

14MW 5 BJ89517 Bromomethane UJ 14MW 6 BJ89518 Bromomethane UJ 14MW 7 BJ89519 Bromomethane UJ

DUPLICATE BJ89520 Bromomethane UJ



Compound %D

Bromomethane(1) 29.8 Acrolein -24.7

Acrylonitrile -24.9 Tetrahydrofuran -23.2

Methyl Ethyl Ketone -25.9 2-Hexanone -24.6

A= Acceptable (1) Results for these compounds were previously qualified due to ICV criteria.



14MW 5 BJ89517 Bromomethane, Acrolein, Acrylonitrile, Tetrahydrofuran, Methyl Ethyl Ketone,

2-Hexanone

UJ


2-Hexanone

UJ


2-Hexanone

UJ

DUPLICATE BJ89520 Bromomethane, Acrolein, Acrylonitrile, Tetrahydrofuran, Methyl Ethyl Ketone,

2-Hexanone

UJ




Compound %D Acrolein(1) -21.3

2,2-Dichloropropane 22.0 A= Acceptable

(1) Results for this compound were previously qualified due to initial CCV criteria.


Compound Action

14MW 5 BJ89517 Acrolein, 2,2-Dichloropropane UJ 14MW 6 BJ89518 Acrolein, 2,2-Dichloropropane UJ 14MW 7 BJ89519 Acrolein, 2,2-Dichloropropane UJ

DUPLICATE BJ89520 Acrolein, 2,2-Dichloropropane UJ

Surrogates: 1. All surrogates %RECs values for all water samples and associated QC were within the

laboratory control limits. No qualifications were required. Internal Standard (IS) Area Performance: 1. All samples exhibited acceptable area count for all four internal standards within the QC

limits. No qualifications were required. Method Blank (MB), Storage Blank (SB), Trip Blank (TB), Field Blank (FB), Rinsate Blank (RB) and Equipment Blank (EB): 1. Method Blank (BLANK BJ89518) was analyzed on 09/10/2015 was free of

contamination. No qualifications were required. Laboratory Control Sample (LCS)/ Laboratory Control Sample Duplicate (LCSD):


Batch ID: BJ89518 were analyzed on 09/10/2015. All %RECs and RPDs were within the laboratory control limits. No qualifications were required.


(BJ89518). All RPDs were 30% with the exception of benzene, chloroethane,


chloromethane, cis-1,2-dichloroethylene, toluene, trans-1,2-dichloroethene, trichloroethylene, and vinyl chloride.

Field Sample Analyte Analytical Method Result Units Field Duplicate Result Units RPD Qualifier

14 MW 6 Acetone SW-846 8260 5.1 g/L Duplicate 3.8 g/L 29.2 None

14 MW 6 Benzene SW-846 8260 2.1 g/L Duplicate ND g/L NC J/UJ

14 MW 6 Chloroethane SW-846 8260 0.31 g/L Duplicate ND g/L NC J/UJ

14 MW 6 Chloromethane SW-846 8260 0.63 g/L Duplicate 1.7 g/L 91.8 J

14 MW 6 Cis-1,2-Dichloroethylene SW-846 8260 16 g/L Duplicate 8.9 g/L 57.0 J

14 MW 6 Toluene SW-846 8260 ND g/L Duplicate 0.64 g/L NC UJ/J

14 MW 6 Trans-1,2-Dichloroethene SW-846 8260 0.40 g/L Duplicate ND g/L NC J/UJ

14 MW 6 Trichloroethylene SW-846 8260 1.4 g/L Duplicate 3.3 g/L 80.9 J

14 MW 6 Vinyl Chloride SW-846 8260 0.28 g/L Duplicate 1.3 g/L 129.1 J

Matrix Spike (MS)/ Matrix Spike Duplicate (MSD): 1. Matrix Spike (MS)/Matrix Spike Duplicate (MSD) were performed on sample 14MW 6

(BJ89518). All %RECs were within the laboratory control limits with the following exception(s):

Compound %R/%R/RPD Action

Cis-1,2-Dichloroethene NC/NC/NC J NC=Not calculated




were required.


2. Manual Calculation: Cx = (Ax)(IS)(DF)

(Ais)(RRF)(V)

Cx = concentration of analyte as g/L Ax = Area of the characteristic ion for the compound to be measured, counts. Ais = Area of the characteristic ion for the specific internal standard, counts. IS = Concentration of the internal standard spiking mixture, ng RRF= Mean relative response factor from the initial calibration. DF = Dilution factor calculated. If no dilution is performed, DF= 1 V= Volume for liquids in ml, weight for soils/solids in grams.

14MW 5 (BJ89517) Chloromethane Sample Volume= 25ml Volume purged=25ml DF = 1 Concentration (g/L)= 7890 x 25 x 10 x 1 = 0.7596g/L 247890 x 0.419 x 25

Compound Laboratory

(g/L) Validation

(g/L) %D

Chloromethane 0.76 0.76 0.0 Comments: 1. Volatile data package meet requirement for New York State Department of






Project Name: 510 Driggs Avenue Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBJ89517 Client: Environmental Business Consultants Date: 12/27/2015 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for four (4) water samples analyzed for



Environmental Laboratories, Inc., Manchester, CT on 9/09/2015 for analysis. 3. The USEPA Region-II SOP HW-44, Revision 1, October 2006, Validating Pesticide







Collection Date


14MW 5 BJ89517 9/08/15 Pesticides Water 14MW 6 BJ89518 9/08/15 Pesticides Water 14MW 7 BJ89519 9/08/15 Pesticides Water

DUPLICATE BJ89520 9/08/15 Pesticides Water Field Duplicate to sample 14MW 6





were required. Initial Calibration: 1. Initial calibration curve analyzed on 9/03/2015 (ECD35) exhibited acceptable %RSD. No

qualifications are required. All sample results were reported from Column A. No qualifications were required.


Continuing Calibration Verification (CCV): 1. The CCVs analyzed on 9/10/2015 exhibited acceptable %Ds (20.0%) for all compounds

on Column A. No qualifications were required. Surrogates: 1. All surrogates %RECs values for all water samples and associated QC were within the

laboratory control limits. Note: Recovery values for tetrachloro-m-xylene were below the QC limits on column B for sample 14MW 6. Results were taken from column A. No qualifications were required.

Method Blank (MB), Storage Blank (SB), Trip Blank (TB), Field Blank (FB), Rinsate Blank (RB) and Equipment Blank (EB): 1. Method Blank (BJ89518) associated with the water samples extracted on 9/09/2015 and

analyzed on 09/10/2015 was free of contamination. No qualifications were required. Laboratory Control Sample (LCS)/ Laboratory Control Sample Duplicate (LCSD): 1. Laboratory Control Sample and Laboratory Control Sample Duplicate associated with

ID: BJ89518 were analyzed on 9/10/2015. All %RECs and RPDs were within the laboratory control limits. No qualifications were required.

Field Duplicate:

1. Sample DUPLICATE (BJ89520) was collected as a field duplicate of sample 14MW 6 (BJ89518). Both sample results were reported as non-detects. No qualifications were required.


(BJ89518). All %RECs were within the laboratory control limits. No qualifications were required.

Compound Quantitation, Compound Identification and Reported Detection Limits: 1. All sample results were reported within the linear calibration range.


2. Manual Calculation: BJ89518

Alpha-BHC

On Column concentration (B)= 49.6357ng Sample Volume= 1000ml DF = 1 Concentration (g/L) = 49.6357ng x 5 x 1ml = 0.248g/L 1000

Compound Laboratory

(g/L) Validation

(g/L) %D

Alpha-BHC 0.248 0.248 0.0 Comments: 1. Pesticides data package meet requirement for New York State Department of






Project Name: 510 Driggs Avenue Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBJ89517 Client: Environmental Business Consultants Date: 12/27/2015 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for four (4) water samples analyzed for PCBs

by SW-846 Method 8082A in accordance with NYSDEC, Analytical Services Protocol (ASP) Format.









Collection Date


14MW 5 BJ89517 9/08/15 PCBs Water 14MW 6 BJ89518 9/08/15 PCBs Water 14MW 7 BJ89519 9/08/15 PCBs Water

DUPLICATE BJ89520 9/08/15 PCBs Water Field Duplicate to sample 14MW 6





(20.0%) on both columns. No qualifications were required. 2. All sample results were reported from Column B. Continuing Calibration Verification (CCV): 1. All CCVs analyzed on 09/10/2015 exhibited acceptable %Ds (15.0%) for all

compounds. No qualifications were required.



laboratory control limits. No qualifications were required. Method Blank (MB), Storage Blank (SB), Trip Blank (TB), Field Blank (FB), Rinsate Blank (RB) and Equipment Blank (EB): 1. Method Blank (BJ89518 BL) associated with the water samples extracted on 9/09/2015




(BJ89518). Both sample results were reported as non-detects. No qualifications were required.


(BJ89518). All %RECs were within the laboratory control limits. No qualifications were required.

Compound Quantitation, Compound Identification and Reported Detection Limits: 1. All sample results were reported within the linear calibration range. 2. Manual Calculation: BJ89518 LCS

Aroclor-1016

On Column concentration (B)= 389.202ng


Sample Volume= 1000ml DF= 1 Vi= 5ml Concentration (g/L) = 389.202ng x 5ml x 1 = 1.95g/L 1000

Compound Laboratory

(g/L) Validation

(g/L) %D

Aroclor-1016 1.95 1.95 0.0 Comments: 1. PCBs data package meet requirement for New York State Department of Environmental




USEPA Region II –Data Validation Project Name: 510 Driggs Avenue Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBJ79227 Client: Environmental Business Consultants Date: 12/27/2015 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for four (4) water samples (both total and

dissolved) analyzed for the following analyses:

1.1 Trace Metals-ICP-AES by SW-846 Method 6010C. 1.2 Thallium, antimony, and selenium by SW-846 Method 7010 (GFAA). 1.3 Mercury by SW-846 Method 7470A.


Environmental Laboratories, Inc., Manchester, CT on 9/09/2015 for analysis. 3. The USEPA Region-II SOP No. HW-2, Revision 13, September 2006, Validation of

Metals for Contract Laboratory Program (CLP), based on SOW-ILM05.3 (SOP Revision 13) was used in evaluating the Trace Metals (total and dissolved) data in this summary report.






Collection Date


14 MW 5 BJ89517 9/08/15 ICP, GFAA and CVAA Water 14 MW 6 BJ89518 9/08/15 ICP, GFAA and CVAA Water 14 MW 7 BJ89519 9/08/15 ICP, GFAA and CVAA Water

DUPLICATE BJ89520 9/08/15 ICP, GFAA and CVAA Water Field Duplicate to sample 14 MW 6



Holding Times: 1. All water samples were analyzed within the 6 months holding times for Trace Metals

analyses by ICP-AES and GFAA. No qualifications were required. 2. All water samples were digested and analyzed within the 28 days holding times for

Mercury analysis. No qualifications were required. Initial and Continuing Calibration Verification (ICV and CCV): ICP-AES and GFAA: 1. All %RECs in the ICV and CCVs were within QC limits (90-110%) for total samples. No

qualifications were requied. Mercury: 1 All correlation coefficient for Mercury calibration curve analyzed were 0.995. No



qualifications were required. CRQL Check Standard (CRI): 1. All CRI analyzed on 8/22/2015 %RECs were within the control limits (70-130%) with

the following exception(s):

Analyte Date Analyzed

Initial %R

Final %R


Nickel 9/10/2015: 20:53

A 148.0 None None

9/10/2015: 22:10

A 136.0 14 MW 6 J

ICP-AES Interference Check Sample: 1. All %REC values were within the QC limits (80-120%) for ICSA and ICSAB. No

qualifications were required. Blanks (Method Blank, ICB and CCB): ICP-AES and GFAA: 1. Method Blank-Water (BJ87737 BLK) (furnace) digested on 9/09/2015 was free of

contamination. No qualifications were required. 2. Method Blank-Water (BJ89518 BLK) (furnace) digested on 9/10/2015 was free of

contamination. No qualifications were required. 3. Method Blank-Water (BJ89518 BLK) (ICP) digested on 9/09/2015 was free of

contamination with the exception of calcium (0.014 mg/L). Sample results were >10X the blank contamination. No qualifications were required.

4. ICBs and CCBs analyzed on 9/10/2015.

Element Concentration (µg/L)

CRQL* (µg/L)


Nickel 1 4 None None 2 4 None None 1 4 None None 1 4 14 MW 6 None 2 4 None None


*= If sample concentration >MDL but < Reporting limit, then sample result qualified as non-detect (U). If sample concentration greater than CRQL but less than10x the blank result, then qualify estimated (J). If sample concentration greater than 10x the blank results or sample was not detected then no qualifications or action is required.

Mercury: 1. All ICB and CCBs were free of contamination. No qualifications were required. 2. Method Blank-Water (BJ89518BLK) digested on 9/10/2015 was free of contamination.

No qualifications were required. Field Blank (FB) and Equipment Blank (EB): 1. Field Blanks were not submitted with this SDG. Laboratory Control Sample (LCS)/ Laboratory Control Sample Duplicate (LCSD): ICP-AES, GFAA and CVAA: 1. Laboratory Control Sample was analyzed on 9/10/2015. All %RECs were within the

laboratory control limits. No qualifications were required. Field Duplicate: 1. Sample GW DUPLICATE (BJ79231) was collected as a field duplicate of sample 14

MW 6 (BJ89518). RPDs were ≤35% (absolute difference is <2MDL where the results were <5X MDL) with the exception of aluminum, arsenic, barium, calcium, chromium, copper, iron, lead, magnesium, manganese, nickel, potassium, sodium, vanadium, and zinc.

Field Sample Analyte Analytical Method Result Units Field Duplicate Result Units RPD/

(Difference*) Qualifier

14 MW 6 Aluminum SW8466010B 9.02 mg/L DUPLICATE 0.569 mg/L 176.3 J

14 MW 6 Arsenic SW8466010B 0.007 mg/L DUPLICATE 0.003 mg/L 80.0 J

14 MW 6 Barium SW8466010B 0.071 mg/L DUPLICATE 0.011 mg/L 146.3 J

14 MW 6 Calcium SW8466010B 6.49 mg/L DUPLICATE 26.5 mg/L 121.3 J

14 MW 6 Chromium SW8466010B 0.021 mg/L DUPLICATE 0.001 mg/L 181.8 J

14 MW 6 Cobalt SW8466010B 0.006 mg/L DUPLICATE ND mg/L (0.001) None

14 MW 6 Copper SW8466010B 0.017 mg/L DUPLICATE 0.002 mg/L 157.9 J


Field Sample Analyte Analytical Method Result Units Field Duplicate Result Units RPD/

(Difference*) Qualifier

14 MW 6 Iron SW8466010B 12.4 mg/L DUPLICATE 0.75 mg/L 177.2 J

14 MW 6 Lead SW8466010B 0.006 mg/L DUPLICATE 0.004 mg/L 40.0 J

14 MW 6 Magnesium SW8466010B 5.69 mg/L DUPLICATE 1.65 mg/L 110.1 J

14 MW 6 Manganese SW8466010B 0.468 mg/L DUPLICATE 0.315 mg/L 39.1 J

14 MW 6 Nickel SW8466010B 0.017 mg/L DUPLICATE 0.004 mg/L 123.8 J

14 MW 6 Potassium SW8466010B 6.7 mg/L DUPLICATE 2.9 mg/L 79.2 J

14 MW 6 Sodium SW8466010B 75.5 mg/L DUPLICATE 8.1 mg/L 161.2 J

14 MW 6 Vanadium SW8466010B 0.022 mg/L DUPLICATE 0.001 mg/L 182.6 J

14 MW 6 Zinc SW8466010B 0.025 mg/L DUPLICATE 0.003 mg/L 157.1 J

*If one of the results is non-detect the MDL will be used as the result to calculate the difference. Matrix Spike (MS)/ Matrix Spike Duplicate (MSD): ICP-AES, GFAA and CVAA: 1. Matrix Spike (MS) was performed on sample 14 MW 6 (BJ89518) for total metals and

mercury. All %Rs were within the laboratory control limits. No qualifications were required.

Sample Duplicate: ICP-AES, GFAA and CVAA: 1. Laboratory Duplicate was performed on sample 14 MW 6 (BJ89518) for mercury ICP-

AES, and GFAA. All RPDs were within the laboratory control limits. No qualifications were required.

ICP-AES Serial Dilution: 1. ICP serial dilution was performed on sample 14 MW 6 (BJ89518). For all results for

which the concentration in the original sample is ≥ 50x the Method Detection Limits (MDL), the serial dilution analysis (a five-fold dilution) was within the acceptable limit (%D 10%) with the following exception(s):

Element %D Sample

Affected Action

Aluminum 13.1 14 MW 5, 14 MW 6, 14 MW 7, Duplicate J Sodium 18.1 14 MW 5, 14 MW 6, 14 MW 7, Duplicate J




Compound Quantitation and Reported Detection Limits: 1. All sample results were reported within the linear calibration range. 2. Manual calculation: Sample: 14 MW 5 (BJ89517) Arsenic DF: 1 0.004 mg/L was reported on the raw data and the laboratory reported 0.004 mg/L on

Form-I. Comments: 1. Trace Metals data package meet requirement for New York State Department of




DATA SUMMARY TABLEAQUEOUS

SDG: GBJ89517

Sample Name Lab ID Analytical Analysis Dilution Analyte Result Unit Qualifier RLMethod Date Factor

14MW5 BJ89517 7010 09/14/15 1 Antimony mg/l U 0.00214MW5 BJ89517 7010 09/11/15 1 Selenium mg/l U 0.00214MW5 BJ89517 7010 09/15/15 1 Thallium mg/l U 0.000514MW5 BJ89517 SW6010 09/10/15 1 Aluminum 1.65 mg/l J 0.01014MW5 BJ89517 SW6010 09/10/15 1 Arsenic 0.004 mg/l J 0.00414MW5 BJ89517 SW6010 09/10/15 1 Barium 0.020 mg/l 0.01014MW5 BJ89517 SW6010 09/10/15 1 Beryllium mg/l U 0.00114MW5 BJ89517 SW6010 09/10/15 1 Cadmium mg/l U 0.00414MW5 BJ89517 SW6010 09/10/15 1 Calcium 26.6 mg/l 0.01014MW5 BJ89517 SW6010 09/10/15 1 Chromium, Total 0.005 mg/l 0.00114MW5 BJ89517 SW6010 09/10/15 1 Cobalt mg/l U 0.00514MW5 BJ89517 SW6010 09/10/15 1 Copper 0.006 mg/l 0.00514MW5 BJ89517 SW6010 09/10/15 1 Iron 2.75 mg/l 0.0114MW5 BJ89517 SW6010 09/10/15 1 Lead 0.006 mg/l 0.00214MW5 BJ89517 SW6010 09/10/15 1 Magnesium 2.03 mg/l 0.0114MW5 BJ89517 SW6010 09/10/15 1 Manganese 0.358 mg/l 0.00514MW5 BJ89517 SW6010 09/12/15 1 Nickel 0.006 mg/l 0.00414MW5 BJ89517 SW6010 09/10/15 1 Potassium 3.5 mg/l 0.114MW5 BJ89517 SW6010 09/10/15 1 Silver mg/l U 0.00514MW5 BJ89517 SW6010 09/10/15 1 Sodium 9.2 mg/l J 0.114MW5 BJ89517 SW6010 09/10/15 1 Vanadium 0.005 mg/l J 0.01014MW5 BJ89517 SW6010 09/10/15 1 Zinc 0.006 mg/l J 0.01014MW5 BJ89517 SW7470 09/10/15 1 Mercury mg/l U 0.000214MW5 BJ89517 SW8081 09/10/15 1 Heptachlor Epoxide ug/l U 0.01014MW5 BJ89517 SW8081 09/10/15 1 Heptachlor Epoxide ug/l U 0.01014MW5 BJ89517 SW8081 09/10/15 1 Endosulfan Sulfate ug/l U 0.01014MW5 BJ89517 SW8081 09/10/15 1 Alachlor ug/l U 0.07514MW5 BJ89517 SW8081 09/10/15 1 Aldrin ug/l U 0.00314MW5 BJ89517 SW8081 09/10/15 1 Alpha Bhc (Alpha Hexachlorocyclohexane) ug/l U 0.00514MW5 BJ89517 SW8081 09/10/15 1 Beta Bhc (Beta Hexachlorocyclohexane) ug/l U 0.01514MW5 BJ89517 SW8081 09/10/15 1 Delta BHC (Delta Hexachlorocyclohexane) ug/l U 0.00514MW5 BJ89517 SW8081 09/10/15 1 Beta Endosulfan ug/l U 0.01014MW5 BJ89517 SW8081 09/10/15 1 P,P'-DDT ug/l U 0.01014MW5 BJ89517 SW8081 09/10/15 1 cis-Chlordane ug/l U 0.01014MW5 BJ89517 SW8081 09/10/15 1 trans-Chlordane ug/l U 0.01614MW5 BJ89517 SW8081 09/10/15 1 Endrin Ketone ug/l U 0.01014MW5 BJ89517 SW8081 09/10/15 1 Chlordane ug/l U 0.0514MW5 BJ89517 SW8081 09/10/15 1 Gamma Bhc (Lindane) ug/l U 0.01114MW5 BJ89517 SW8081 09/10/15 1 Dieldrin ug/l U 0.00414MW5 BJ89517 SW8081 09/10/15 1 Endrin ug/l U 0.01014MW5 BJ89517 SW8081 09/10/15 1 Methoxychlor ug/l U 0.10

Page 1 of 20



SDG: GBJ89517


14MW5 BJ89517 SW8081 09/10/15 1 P,P'-DDD ug/l U 0.01014MW5 BJ89517 SW8081 09/10/15 1 P,P'-DDE ug/l U 0.01014MW5 BJ89517 SW8081 09/10/15 1 Endrin Aldehyde ug/l U 0.01014MW5 BJ89517 SW8081 09/10/15 1 Heptachlor ug/l U 0.01014MW5 BJ89517 SW8081 09/10/15 1 Toxaphene ug/l U 0.2514MW5 BJ89517 SW8081 09/10/15 1 Alpha Endosulfan ug/l U 0.01014MW5 BJ89517 SW8082 09/10/15 1 PCB-1260 (Aroclor 1260) ug/l U 0.05014MW5 BJ89517 SW8082 09/10/15 1 PCB-1254 (Aroclor 1254) ug/l U 0.05014MW5 BJ89517 SW8082 09/10/15 1 PCB-1268 (Aroclor 1268) ug/l U 0.05014MW5 BJ89517 SW8082 09/10/15 1 PCB-1221 (Aroclor 1221) ug/l U 0.05014MW5 BJ89517 SW8082 09/10/15 1 PCB-1232 (Aroclor 1232) ug/l U 0.05014MW5 BJ89517 SW8082 09/10/15 1 PCB-1248 (Aroclor 1248) ug/l U 0.05014MW5 BJ89517 SW8082 09/10/15 1 PCB-1016 (Aroclor 1016) ug/l U 0.05014MW5 BJ89517 SW8082 09/10/15 1 PCB-1262 (Aroclor 1262) ug/l U 0.05014MW5 BJ89517 SW8082 09/10/15 1 PCB-1242 (Aroclor 1242) ug/l U 0.05014MW5 BJ89517 SW8260 09/10/15 1 Ethylbenzene ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Styrene ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Cis-1,3-Dichloropropene ug/l U 0.4014MW5 BJ89517 SW8260 09/10/15 1 Trans-1,3-Dichloropropene ug/l U 0.4014MW5 BJ89517 SW8260 09/10/15 1 N-Propylbenzene ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 N-Butylbenzene ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 4-Chlorotoluene ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 1,4-Dichlorobenzene ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 1 2-Dibromoethane (Ethylene Dibromide) ug/l U 1 014MW5 BJ89517 SW8260 09/10/15 1 1,2 Dibromoethane (Ethylene Dibromide) ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Acrolein ug/l UJ 5.014MW5 BJ89517 SW8260 09/10/15 1 1,2-Dichloroethane ug/l U 0.6014MW5 BJ89517 SW8260 09/10/15 1 Acrylonitrile ug/l UJ 5.014MW5 BJ89517 SW8260 09/10/15 1 Methyl Isobutyl Ketone (4-Methyl-2-Pentanone) ug/l U 2.514MW5 BJ89517 SW8260 09/10/15 1 1,3,5-Trimethylbenzene (Mesitylene) ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Bromobenzene ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Toluene 0.56 ug/l J 1.014MW5 BJ89517 SW8260 09/10/15 1 Chlorobenzene ug/l U 5.014MW5 BJ89517 SW8260 09/10/15 1 Tetrahydrofuran ug/l UJ 5.014MW5 BJ89517 SW8260 09/10/15 1 Trans-1,4-Dichloro-2-Butene ug/l U 2.514MW5 BJ89517 SW8260 09/10/15 1 1,2,4-Trichlorobenzene ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Dibromochloromethane ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Tetrachloroethylene (PCE) ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Sec-Butylbenzene ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 1,3-Dichloropropane ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Cis-1,2-Dichloroethylene 8.4 ug/l 1.0

Page 2 of 20



SDG: GBJ89517


14MW5 BJ89517 SW8260 09/10/15 1 Trans-1,2-Dichloroethene ug/l U 5.014MW5 BJ89517 SW8260 09/10/15 1 Tert-Butyl Methyl Ether ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 m,p-Xylene ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 O-Cymene (O-Isopropyltoluene) ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 1,3-Dichlorobenzene ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Carbon Tetrachloride ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 1,1-Dichloropropene ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 2-Hexanone ug/l UJ 2.514MW5 BJ89517 SW8260 09/10/15 1 2,2-Dichloropropane ug/l UJ 1.014MW5 BJ89517 SW8260 09/10/15 1 1,1,1,2-Tetrachloroethane ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Acetone 2.7 ug/l J 5.014MW5 BJ89517 SW8260 09/10/15 1 Chloroform ug/l U 5.014MW5 BJ89517 SW8260 09/10/15 1 Benzene ug/l U 0.7014MW5 BJ89517 SW8260 09/10/15 1 1,1,1-Trichloroethane ug/l U 5.014MW5 BJ89517 SW8260 09/10/15 1 Bromomethane ug/l UJ 5.014MW5 BJ89517 SW8260 09/10/15 1 Chloromethane 0.76 ug/l J 5.014MW5 BJ89517 SW8260 09/10/15 1 Dibromomethane ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Bromochloromethane ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Chloroethane ug/l U 5.014MW5 BJ89517 SW8260 09/10/15 1 Vinyl Chloride 0.96 ug/l J 1.014MW5 BJ89517 SW8260 09/10/15 1 Methylene Chloride ug/l U 3.014MW5 BJ89517 SW8260 09/10/15 1 Carbon Disulfide ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Bromoform ug/l U 5.014MW5 BJ89517 SW8260 09/10/15 1 Bromodichloromethane ug/l U 1 014MW5 BJ89517 SW8260 09/10/15 1 Bromodichloromethane ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 1,1-Dichloroethane ug/l U 5.014MW5 BJ89517 SW8260 09/10/15 1 1,1-Dichloroethene ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Trichlorofluoromethane ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Dichlorodifluoromethane ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 1,1,2-Trichloro-1,2,2-Trifluoroethane ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 1,2-Dichloropropane ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Methyl Ethyl Ketone (2-Butanone) ug/l UJ 2.514MW5 BJ89517 SW8260 09/10/15 1 1,1,2-Trichloroethane ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Trichloroethylene (TCE) 4.0 ug/l 1.014MW5 BJ89517 SW8260 09/10/15 1 1,1,2,2-Tetrachloroethane ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 1,2,3-Trichlorobenzene ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Hexachlorobutadiene ug/l U 0.514MW5 BJ89517 SW8260 09/10/15 1 Naphthalene ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 O-Xylene (1,2-Dimethylbenzene) ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 2-Chlorotoluene ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 1,2-Dichlorobenzene ug/l U 1.0

Page 3 of 20



SDG: GBJ89517


14MW5 BJ89517 SW8260 09/10/15 1 1,2,4-Trimethylbenzene ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 1,2-Dibromo-3-Chloropropane ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 1,2,3-Trichloropropane ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 T-Butylbenzene ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Isopropylbenzene (Cumene) ug/l U 1.014MW5 BJ89517 SW8260 09/10/15 1 Cymene ug/l U 1.014MW5 BJ89517 SW8270 09/14/15 1 4-Nitroaniline ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 4-Nitrophenol ug/l U 1.014MW5 BJ89517 SW8270 09/14/15 1 4-Bromophenyl Phenyl Ether ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 2,4-Dimethylphenol ug/l U 1.014MW5 BJ89517 SW8270 09/14/15 1 1,4-Dichlorobenzene ug/l U 1.014MW5 BJ89517 SW8270 09/14/15 1 4-Chloroaniline ug/l U 3.514MW5 BJ89517 SW8270 09/14/15 1 Phenol ug/l U 1.014MW5 BJ89517 SW8270 09/14/15 1 Pyridine ug/l UJ 1014MW5 BJ89517 SW8270 09/14/15 1 Bis(2-Chloroethyl) Ether (2-Chloroethyl Ether) ug/l U 1.014MW5 BJ89517 SW8270 09/14/15 1 Bis(2-Chloroethoxy) Methane ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 Di-N-Octylphthalate ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 Anthracene ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 1,2,4-Trichlorobenzene ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 2,4-Dichlorophenol ug/l U 1.014MW5 BJ89517 SW8270 09/14/15 1 2,4-Dinitrotoluene ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 1,2-Diphenylhydrazine ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 Pyrene ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 Dimethyl Phthalate ug/l U 5 014MW5 BJ89517 SW8270 09/14/15 1 Dimethyl Phthalate ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 Dibenzofuran ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 Fluoranthene ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 2,2-Oxybis(2-Chloropropane) ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 2,4-Dinitrophenol ug/l U 1.014MW5 BJ89517 SW8270 09/14/15 1 4,6-Dinitro-2-Methylphenol ug/l U 1.014MW5 BJ89517 SW8270 09/14/15 1 1,3-Dichlorobenzene ug/l U 1.014MW5 BJ89517 SW8270 09/14/15 1 4-Chloro-3-Methylphenol ug/l U 1.014MW5 BJ89517 SW8270 09/14/15 1 2,6-Dinitrotoluene ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 N-Nitrosodi-N-Propylamine ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 Aniline ug/l U 3.514MW5 BJ89517 SW8270 09/14/15 1 N-Nitrosodimethylamine ug/l U 1.014MW5 BJ89517 SW8270 09/14/15 1 Benzoic Acid ug/l U 2514MW5 BJ89517 SW8270 09/14/15 1 4-Chlorophenyl Phenyl Ether ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 Hexachlorocyclopentadiene ug/l UJ 5.014MW5 BJ89517 SW8270 09/14/15 1 Isophorone ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 Acenaphthene ug/l U 5.0

Page 4 of 20



SDG: GBJ89517


14MW5 BJ89517 SW8270 09/14/15 1 Diethyl Phthalate ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 Di-N-Butyl Phthalate ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 Benzyl Butyl Phthalate ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 N-Nitrosodiphenylamine ug/l UJ 5.014MW5 BJ89517 SW8270 09/14/15 1 Fluorene ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 Carbazole ug/l U 2514MW5 BJ89517 SW8270 09/14/15 1 2,4,6-Trichlorophenol ug/l U 1.014MW5 BJ89517 SW8270 09/14/15 1 2-Nitroaniline ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 2-Nitrophenol ug/l U 1.014MW5 BJ89517 SW8270 09/14/15 1 Naphthalene ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 2-Methylnaphthalene ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 2-Chloronaphthalene ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 3,3'-Dichlorobenzidine ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 Benzidine ug/l UJ 4.514MW5 BJ89517 SW8270 09/14/15 1 2-Methylphenol (O-Cresol) ug/l U 1.014MW5 BJ89517 SW8270 09/14/15 1 1,2-Dichlorobenzene ug/l U 1.014MW5 BJ89517 SW8270 09/14/15 1 2-Chlorophenol ug/l U 1.014MW5 BJ89517 SW8270 09/14/15 1 2,4,5-Trichlorophenol ug/l U 1.014MW5 BJ89517 SW8270 09/14/15 1 Acetophenone ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 3-Nitroaniline ug/l U 5.014MW5 BJ89517 SW8270 09/14/15 1 3- And 4- Methylphenol (Total) ug/l U 1.014MW5 BJ89517 SW8270C-SIM 09/11/15 1 Bis(2-Ethylhexyl) Phthalate ug/l U 1.014MW5 BJ89517 SW8270C-SIM 09/11/15 1 Hexachlorobenzene ug/l U 0.0214MW5 BJ89517 SW8270C-SIM 09/11/15 1 Benzo(G H I)Perylene ug/l U 0 0214MW5 BJ89517 SW8270C SIM 09/11/15 1 Benzo(G,H,I)Perylene ug/l U 0.0214MW5 BJ89517 SW8270C-SIM 09/11/15 1 Indeno(1,2,3-C,D)Pyrene ug/l U 0.0214MW5 BJ89517 SW8270C-SIM 09/11/15 1 Benzo(B)Fluoranthene 0.02 ug/l 0.0214MW5 BJ89517 SW8270C-SIM 09/11/15 1 Benzo(K)Fluoranthene ug/l U 0.0214MW5 BJ89517 SW8270C-SIM 09/11/15 1 Acenaphthylene ug/l U 0.1014MW5 BJ89517 SW8270C-SIM 09/11/15 1 Chrysene 0.02 ug/l 0.0214MW5 BJ89517 SW8270C-SIM 09/11/15 1 Benzo(A)Pyrene 0.02 ug/l 0.0214MW5 BJ89517 SW8270C-SIM 09/11/15 1 Dibenz(A,H)Anthracene ug/l U 0.0214MW5 BJ89517 SW8270C-SIM 09/11/15 1 Benzo(A)Anthracene 0.03 ug/l 0.0214MW5 BJ89517 SW8270C-SIM 09/11/15 1 Hexachloroethane ug/l U 0.5014MW5 BJ89517 SW8270C-SIM 09/11/15 1 Pentachloronitrobenzene ug/l U 0.1014MW5 BJ89517 SW8270C-SIM 09/11/15 1 Phenanthrene ug/l U 0.1014MW5 BJ89517 SW8270C-SIM 09/11/15 1 Hexachlorobutadiene ug/l U 0.4014MW5 BJ89517 SW8270C-SIM 09/11/15 1 Pentachlorophenol ug/l U 1.014MW5 BJ89517 SW8270C-SIM 09/11/15 1 1,2,4,5-Tetrachlorobenzene ug/l U 0.5014MW5 BJ89517 SW8270C-SIM 09/11/15 1 Nitrobenzene ug/l U 0.1014MW6 BJ89518 7010 09/14/15 1 Antimony mg/l U 0.002

Page 5 of 20



SDG: GBJ89517


14MW6 BJ89518 7010 09/11/15 1 Selenium mg/l U 0.00214MW6 BJ89518 7010 09/15/15 1 Thallium mg/l U 0.000514MW6 BJ89518 SW6010 09/10/15 1 Aluminum 9.02 mg/l J 0.01014MW6 BJ89518 SW6010 09/10/15 1 Arsenic 0.007 mg/l 0.00414MW6 BJ89518 SW6010 09/10/15 1 Beryllium mg/l U 0.00114MW6 BJ89518 SW6010 09/10/15 1 Cadmium mg/l U 0.00414MW6 BJ89518 SW6010 09/10/15 1 Barium 0.071 mg/l J 0.01014MW6 BJ89518 SW6010 09/10/15 1 Calcium 6.49 mg/l J 0.01014MW6 BJ89518 SW6010 09/10/15 1 Chromium, Total 0.021 mg/l J 0.00114MW6 BJ89518 SW6010 09/10/15 1 Cobalt 0.006 mg/l 0.00514MW6 BJ89518 SW6010 09/10/15 1 Copper 0.017 mg/l J 0.00514MW6 BJ89518 SW6010 09/10/15 1 Silver mg/l U 0.00514MW6 BJ89518 SW6010 09/10/15 1 Iron 12.4 mg/l J 0.0114MW6 BJ89518 SW6010 09/10/15 1 Lead 0.006 mg/l J 0.00214MW6 BJ89518 SW6010 09/10/15 1 Magnesium 5.69 mg/l J 0.0114MW6 BJ89518 SW6010 09/10/15 1 Manganese 0.468 mg/l J 0.00514MW6 BJ89518 SW6010 09/10/15 1 Nickel 0.017 mg/l J 0.00414MW6 BJ89518 SW6010 09/10/15 1 Potassium 6.7 mg/l J 0.114MW6 BJ89518 SW6010 09/10/15 10 Sodium 75.5 mg/l J 1.014MW6 BJ89518 SW6010 09/10/15 1 Vanadium 0.022 mg/l J 0.01014MW6 BJ89518 SW6010 09/10/15 1 Zinc 0.025 mg/l J 0.01014MW6 BJ89518 SW7470 09/10/15 1 Mercury mg/l U 0.000214MW6 BJ89518 SW8081 09/10/15 1 Heptachlor Epoxide ug/l U 0.01014MW6 BJ89518 SW8081 09/10/15 1 Endosulfan Sulfate ug/l U 0 01014MW6 BJ89518 SW8081 09/10/15 1 Endosulfan Sulfate ug/l U 0.01014MW6 BJ89518 SW8081 09/10/15 1 Alachlor ug/l U 0.07514MW6 BJ89518 SW8081 09/10/15 1 Aldrin ug/l U 0.00314MW6 BJ89518 SW8081 09/10/15 1 Alpha Bhc (Alpha Hexachlorocyclohexane) ug/l U 0.00514MW6 BJ89518 SW8081 09/10/15 1 Beta Bhc (Beta Hexachlorocyclohexane) ug/l U 0.01514MW6 BJ89518 SW8081 09/10/15 1 Delta BHC (Delta Hexachlorocyclohexane) ug/l U 0.00514MW6 BJ89518 SW8081 09/10/15 1 Beta Endosulfan ug/l U 0.01014MW6 BJ89518 SW8081 09/10/15 1 P,P'-DDT ug/l U 0.01014MW6 BJ89518 SW8081 09/10/15 1 cis-Chlordane ug/l U 0.01014MW6 BJ89518 SW8081 09/10/15 1 trans-Chlordane ug/l U 0.01614MW6 BJ89518 SW8081 09/10/15 1 Endrin Ketone ug/l U 0.01014MW6 BJ89518 SW8081 09/10/15 1 Chlordane ug/l U 0.0514MW6 BJ89518 SW8081 09/10/15 1 Gamma Bhc (Lindane) ug/l U 0.01114MW6 BJ89518 SW8081 09/10/15 1 Dieldrin ug/l U 0.00414MW6 BJ89518 SW8081 09/10/15 1 Endrin ug/l U 0.01014MW6 BJ89518 SW8081 09/10/15 1 Methoxychlor ug/l U 0.1014MW6 BJ89518 SW8081 09/10/15 1 P,P'-DDD ug/l U 0.010

Page 6 of 20



SDG: GBJ89517


14MW6 BJ89518 SW8081 09/10/15 1 P,P'-DDE ug/l U 0.01014MW6 BJ89518 SW8081 09/10/15 1 Endrin Aldehyde ug/l U 0.01014MW6 BJ89518 SW8081 09/10/15 1 Heptachlor ug/l U 0.01014MW6 BJ89518 SW8081 09/10/15 1 Toxaphene ug/l U 0.2514MW6 BJ89518 SW8081 09/10/15 1 Alpha Endosulfan ug/l U 0.01014MW6 BJ89518 SW8082 09/10/15 1 PCB-1260 (Aroclor 1260) ug/l U 0.05014MW6 BJ89518 SW8082 09/10/15 1 PCB-1254 (Aroclor 1254) ug/l U 0.05014MW6 BJ89518 SW8082 09/10/15 1 PCB-1268 (Aroclor 1268) ug/l U 0.05014MW6 BJ89518 SW8082 09/10/15 1 PCB-1221 (Aroclor 1221) ug/l U 0.05014MW6 BJ89518 SW8082 09/10/15 1 PCB-1232 (Aroclor 1232) ug/l U 0.05014MW6 BJ89518 SW8082 09/10/15 1 PCB-1248 (Aroclor 1248) ug/l U 0.05014MW6 BJ89518 SW8082 09/10/15 1 PCB-1016 (Aroclor 1016) ug/l U 0.05014MW6 BJ89518 SW8082 09/10/15 1 PCB-1262 (Aroclor 1262) ug/l U 0.05014MW6 BJ89518 SW8082 09/10/15 1 PCB-1242 (Aroclor 1242) ug/l U 0.05014MW6 BJ89518 SW8260 09/10/15 1 Ethylbenzene ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Styrene ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Cis-1,3-Dichloropropene ug/l U 0.4014MW6 BJ89518 SW8260 09/10/15 1 Trans-1,3-Dichloropropene ug/l U 0.4014MW6 BJ89518 SW8260 09/10/15 1 N-Propylbenzene ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 N-Butylbenzene ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 4-Chlorotoluene ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 1,4-Dichlorobenzene ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 1,2-Dibromoethane (Ethylene Dibromide) ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Acrolein ug/l UJ 5 014MW6 BJ89518 SW8260 09/10/15 1 Acrolein ug/l UJ 5.014MW6 BJ89518 SW8260 09/10/15 1 1,2-Dichloroethane ug/l U 0.6014MW6 BJ89518 SW8260 09/10/15 1 Acrylonitrile ug/l UJ 5.014MW6 BJ89518 SW8260 09/10/15 1 Methyl Isobutyl Ketone (4-Methyl-2-Pentanone) ug/l U 2.514MW6 BJ89518 SW8260 09/10/15 1 1,3,5-Trimethylbenzene (Mesitylene) ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Bromobenzene ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Toluene ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Chlorobenzene ug/l U 5.014MW6 BJ89518 SW8260 09/10/15 1 Tetrahydrofuran ug/l UJ 5.014MW6 BJ89518 SW8260 09/10/15 1 Trans-1,4-Dichloro-2-Butene ug/l U 2.514MW6 BJ89518 SW8260 09/10/15 1 1,2,4-Trichlorobenzene ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Dibromochloromethane ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Tetrachloroethylene (PCE) ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Sec-Butylbenzene ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 1,3-Dichloropropane ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Acetone 5.1 ug/l 5.014MW6 BJ89518 SW8260 09/10/15 1 Benzene 2.1 ug/l 0.70

Page 7 of 20



SDG: GBJ89517


14MW6 BJ89518 SW8260 09/10/15 1 Tert-Butyl Methyl Ether ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 m,p-Xylene ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 O-Cymene (O-Isopropyltoluene) ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 1,3-Dichlorobenzene ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Carbon Tetrachloride ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 1,1-Dichloropropene ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 2-Hexanone ug/l UJ 2.514MW6 BJ89518 SW8260 09/10/15 1 2,2-Dichloropropane ug/l UJ 1.014MW6 BJ89518 SW8260 09/10/15 1 1,1,1,2-Tetrachloroethane ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Chloroethane 0.31 ug/l J 5.014MW6 BJ89518 SW8260 09/10/15 1 Chloroform ug/l U 5.014MW6 BJ89518 SW8260 09/10/15 1 Chloromethane 0.63 ug/l J 5.014MW6 BJ89518 SW8260 09/10/15 1 1,1,1-Trichloroethane ug/l U 5.014MW6 BJ89518 SW8260 09/10/15 1 Bromomethane ug/l UJ 5.014MW6 BJ89518 SW8260 09/10/15 1 Cis-1,2-Dichloroethylene 16 ug/l J 1.014MW6 BJ89518 SW8260 09/10/15 1 Dibromomethane ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Bromochloromethane ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Trans-1,2-Dichloroethene 0.40 ug/l J 5.014MW6 BJ89518 SW8260 09/10/15 1 Trichloroethylene (TCE) 1.4 ug/l 1.014MW6 BJ89518 SW8260 09/10/15 1 Methylene Chloride ug/l U 3.014MW6 BJ89518 SW8260 09/10/15 1 Carbon Disulfide ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Bromoform ug/l U 5.014MW6 BJ89518 SW8260 09/10/15 1 Bromodichloromethane ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 1 1-Dichloroethane ug/l U 5 014MW6 BJ89518 SW8260 09/10/15 1 1,1 Dichloroethane ug/l U 5.014MW6 BJ89518 SW8260 09/10/15 1 1,1-Dichloroethene ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Trichlorofluoromethane ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Dichlorodifluoromethane ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 1,1,2-Trichloro-1,2,2-Trifluoroethane ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 1,2-Dichloropropane ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Methyl Ethyl Ketone (2-Butanone) ug/l UJ 2.514MW6 BJ89518 SW8260 09/10/15 1 1,1,2-Trichloroethane ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Vinyl Chloride 0.28 ug/l J 1.014MW6 BJ89518 SW8260 09/10/15 1 1,1,2,2-Tetrachloroethane ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 1,2,3-Trichlorobenzene ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Hexachlorobutadiene ug/l U 0.514MW6 BJ89518 SW8260 09/10/15 1 Naphthalene ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 O-Xylene (1,2-Dimethylbenzene) ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 2-Chlorotoluene ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 1,2-Dichlorobenzene ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 1,2,4-Trimethylbenzene ug/l U 1.0

Page 8 of 20



SDG: GBJ89517


14MW6 BJ89518 SW8260 09/10/15 1 1,2-Dibromo-3-Chloropropane ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 1,2,3-Trichloropropane ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 T-Butylbenzene ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Isopropylbenzene (Cumene) ug/l U 1.014MW6 BJ89518 SW8260 09/10/15 1 Cymene ug/l U 1.014MW6 BJ89518 SW8270 09/14/15 1 4-Nitroaniline ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 4-Nitrophenol ug/l U 1.014MW6 BJ89518 SW8270 09/14/15 1 4-Bromophenyl Phenyl Ether ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 2,4-Dimethylphenol ug/l U 1.014MW6 BJ89518 SW8270 09/14/15 1 1,4-Dichlorobenzene ug/l U 1.014MW6 BJ89518 SW8270 09/14/15 1 4-Chloroaniline ug/l U 3.514MW6 BJ89518 SW8270 09/14/15 1 Phenol ug/l UJ 1.014MW6 BJ89518 SW8270 09/14/15 1 Pyridine ug/l UJ 1014MW6 BJ89518 SW8270 09/14/15 1 Bis(2-Chloroethyl) Ether (2-Chloroethyl Ether) ug/l U 1.014MW6 BJ89518 SW8270 09/14/15 1 Bis(2-Chloroethoxy) Methane ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 Di-N-Octylphthalate ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 Anthracene ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 1,2,4-Trichlorobenzene ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 2,4-Dichlorophenol ug/l U 1.014MW6 BJ89518 SW8270 09/14/15 1 2,4-Dinitrotoluene ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 1,2-Diphenylhydrazine ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 Pyrene ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 Dimethyl Phthalate ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 Dibenzofuran ug/l U 5 014MW6 BJ89518 SW8270 09/14/15 1 Dibenzofuran ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 Fluoranthene ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 2,2-Oxybis(2-Chloropropane) ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 2,4-Dinitrophenol ug/l U 1.014MW6 BJ89518 SW8270 09/14/15 1 4,6-Dinitro-2-Methylphenol ug/l U 1.014MW6 BJ89518 SW8270 09/14/15 1 1,3-Dichlorobenzene ug/l U 1.014MW6 BJ89518 SW8270 09/14/15 1 4-Chloro-3-Methylphenol ug/l U 1.014MW6 BJ89518 SW8270 09/14/15 1 2,6-Dinitrotoluene ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 N-Nitrosodi-N-Propylamine ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 Aniline ug/l UJ 3.514MW6 BJ89518 SW8270 09/14/15 1 N-Nitrosodimethylamine ug/l UJ 1.014MW6 BJ89518 SW8270 09/14/15 1 Benzoic Acid ug/l UJ 2514MW6 BJ89518 SW8270 09/14/15 1 4-Chlorophenyl Phenyl Ether ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 Hexachlorocyclopentadiene ug/l UJ 5.014MW6 BJ89518 SW8270 09/14/15 1 Isophorone ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 Acenaphthene ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 Diethyl Phthalate ug/l U 5.0

Page 9 of 20



SDG: GBJ89517


14MW6 BJ89518 SW8270 09/14/15 1 Di-N-Butyl Phthalate ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 Benzyl Butyl Phthalate ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 N-Nitrosodiphenylamine ug/l UJ 5.014MW6 BJ89518 SW8270 09/14/15 1 Fluorene ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 Carbazole ug/l U 2514MW6 BJ89518 SW8270 09/14/15 1 2,4,6-Trichlorophenol ug/l U 1.014MW6 BJ89518 SW8270 09/14/15 1 2-Nitroaniline ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 2-Nitrophenol ug/l U 1.014MW6 BJ89518 SW8270 09/14/15 1 Naphthalene ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 2-Methylnaphthalene ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 2-Chloronaphthalene ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 3,3'-Dichlorobenzidine ug/l UJ 5.014MW6 BJ89518 SW8270 09/14/15 1 Benzidine ug/l UJ 4.514MW6 BJ89518 SW8270 09/14/15 1 2-Methylphenol (O-Cresol) ug/l U 1.014MW6 BJ89518 SW8270 09/14/15 1 1,2-Dichlorobenzene ug/l U 1.014MW6 BJ89518 SW8270 09/14/15 1 2-Chlorophenol ug/l U 1.014MW6 BJ89518 SW8270 09/14/15 1 2,4,5-Trichlorophenol ug/l U 1.014MW6 BJ89518 SW8270 09/14/15 1 Acetophenone ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 3-Nitroaniline ug/l U 5.014MW6 BJ89518 SW8270 09/14/15 1 3- And 4- Methylphenol (Total) ug/l U 1.014MW6 BJ89518 SW8270C-SIM 09/11/15 1 Bis(2-Ethylhexyl) Phthalate ug/l U 1.014MW6 BJ89518 SW8270C-SIM 09/11/15 1 Hexachlorobenzene ug/l U 0.0214MW6 BJ89518 SW8270C-SIM 09/11/15 1 Benzo(G,H,I)Perylene ug/l U 0.0214MW6 BJ89518 SW8270C-SIM 09/11/15 1 Indeno(1 2 3-C D)Pyrene ug/l U 0 0214MW6 BJ89518 SW8270C SIM 09/11/15 1 Indeno(1,2,3 C,D)Pyrene ug/l U 0.0214MW6 BJ89518 SW8270C-SIM 09/11/15 1 Benzo(B)Fluoranthene ug/l U 0.0214MW6 BJ89518 SW8270C-SIM 09/11/15 1 Benzo(K)Fluoranthene ug/l U 0.0214MW6 BJ89518 SW8270C-SIM 09/11/15 1 Acenaphthylene ug/l U 0.1014MW6 BJ89518 SW8270C-SIM 09/11/15 1 Chrysene ug/l U 0.0214MW6 BJ89518 SW8270C-SIM 09/11/15 1 Benzo(A)Pyrene ug/l U 0.0214MW6 BJ89518 SW8270C-SIM 09/11/15 1 Dibenz(A,H)Anthracene ug/l U 0.0214MW6 BJ89518 SW8270C-SIM 09/11/15 1 Benzo(A)Anthracene ug/l U 0.0214MW6 BJ89518 SW8270C-SIM 09/11/15 1 Hexachloroethane ug/l U 0.5014MW6 BJ89518 SW8270C-SIM 09/11/15 1 Pentachloronitrobenzene ug/l U 0.1014MW6 BJ89518 SW8270C-SIM 09/11/15 1 Phenanthrene ug/l U 0.1014MW6 BJ89518 SW8270C-SIM 09/11/15 1 Hexachlorobutadiene ug/l U 0.4014MW6 BJ89518 SW8270C-SIM 09/11/15 1 Pentachlorophenol ug/l U 0.8014MW6 BJ89518 SW8270C-SIM 09/11/15 1 1,2,4,5-Tetrachlorobenzene ug/l U 0.5014MW6 BJ89518 SW8270C-SIM 09/11/15 1 Nitrobenzene ug/l U 0.1014MW7 BJ89519 7010 09/14/15 1 Antimony mg/l U 0.00214MW7 BJ89519 7010 09/11/15 1 Selenium mg/l U 0.002

Page 10 of 20



SDG: GBJ89517


14MW7 BJ89519 7010 09/15/15 1 Thallium mg/l U 0.000514MW7 BJ89519 SW6010 09/10/15 1 Aluminum 1.84 mg/l J 0.01014MW7 BJ89519 SW6010 09/10/15 1 Arsenic 0.001 mg/l J 0.00414MW7 BJ89519 SW6010 09/10/15 1 Barium 0.025 mg/l 0.01014MW7 BJ89519 SW6010 09/10/15 1 Beryllium mg/l U 0.00114MW7 BJ89519 SW6010 09/10/15 1 Cadmium mg/l U 0.00414MW7 BJ89519 SW6010 09/10/15 1 Calcium 12.2 mg/l 0.01014MW7 BJ89519 SW6010 09/10/15 1 Chromium, Total 0.004 mg/l 0.00114MW7 BJ89519 SW6010 09/10/15 1 Cobalt 0.002 mg/l J 0.00514MW7 BJ89519 SW6010 09/10/15 1 Copper 0.003 mg/l J 0.00514MW7 BJ89519 SW6010 09/10/15 1 Iron 2.11 mg/l 0.0114MW7 BJ89519 SW6010 09/10/15 1 Lead mg/l U 0.00214MW7 BJ89519 SW6010 09/10/15 1 Magnesium 6.26 mg/l 0.0114MW7 BJ89519 SW6010 09/10/15 1 Manganese 0.496 mg/l 0.00514MW7 BJ89519 SW6010 09/12/15 1 Nickel 0.005 mg/l 0.00414MW7 BJ89519 SW6010 09/10/15 1 Potassium 8.1 mg/l 0.114MW7 BJ89519 SW6010 09/10/15 1 Silver mg/l U 0.00514MW7 BJ89519 SW6010 09/10/15 10 Sodium 68.6 mg/l J 1.014MW7 BJ89519 SW6010 09/10/15 1 Vanadium 0.006 mg/l J 0.01014MW7 BJ89519 SW6010 09/10/15 1 Zinc 0.003 mg/l J 0.01014MW7 BJ89519 SW7470 09/10/15 1 Mercury mg/l U 0.000214MW7 BJ89519 SW8081 09/10/15 1 Heptachlor Epoxide ug/l U 0.01014MW7 BJ89519 SW8081 09/10/15 1 Endosulfan Sulfate ug/l U 0.01014MW7 BJ89519 SW8081 09/10/15 1 Alachlor ug/l U 0 07514MW7 BJ89519 SW8081 09/10/15 1 Alachlor ug/l U 0.07514MW7 BJ89519 SW8081 09/10/15 1 Aldrin ug/l U 0.00314MW7 BJ89519 SW8081 09/10/15 1 Alpha Bhc (Alpha Hexachlorocyclohexane) ug/l U 0.00514MW7 BJ89519 SW8081 09/10/15 1 Beta Bhc (Beta Hexachlorocyclohexane) ug/l U 0.01514MW7 BJ89519 SW8081 09/10/15 1 Delta BHC (Delta Hexachlorocyclohexane) ug/l U 0.00514MW7 BJ89519 SW8081 09/10/15 1 Beta Endosulfan ug/l U 0.01014MW7 BJ89519 SW8081 09/10/15 1 P,P'-DDT ug/l U 0.01014MW7 BJ89519 SW8081 09/10/15 1 cis-Chlordane ug/l U 0.01014MW7 BJ89519 SW8081 09/10/15 1 trans-Chlordane ug/l U 0.01614MW7 BJ89519 SW8081 09/10/15 1 Endrin Ketone ug/l U 0.01014MW7 BJ89519 SW8081 09/10/15 1 Chlordane ug/l U 0.0514MW7 BJ89519 SW8081 09/10/15 1 Gamma Bhc (Lindane) ug/l U 0.01114MW7 BJ89519 SW8081 09/10/15 1 Dieldrin ug/l U 0.00414MW7 BJ89519 SW8081 09/10/15 1 Endrin ug/l U 0.01014MW7 BJ89519 SW8081 09/10/15 1 Methoxychlor ug/l U 0.1014MW7 BJ89519 SW8081 09/10/15 1 P,P'-DDD ug/l U 0.01014MW7 BJ89519 SW8081 09/10/15 1 P,P'-DDE ug/l U 0.010

Page 11 of 20



SDG: GBJ89517


14MW7 BJ89519 SW8081 09/10/15 1 Endrin Aldehyde ug/l U 0.01014MW7 BJ89519 SW8081 09/10/15 1 Heptachlor ug/l U 0.01014MW7 BJ89519 SW8081 09/10/15 1 Toxaphene ug/l U 0.2514MW7 BJ89519 SW8081 09/10/15 1 Alpha Endosulfan ug/l U 0.01014MW7 BJ89519 SW8082 09/10/15 1 PCB-1260 (Aroclor 1260) ug/l U 0.05014MW7 BJ89519 SW8082 09/10/15 1 PCB-1254 (Aroclor 1254) ug/l U 0.05014MW7 BJ89519 SW8082 09/10/15 1 PCB-1268 (Aroclor 1268) ug/l U 0.05014MW7 BJ89519 SW8082 09/10/15 1 PCB-1221 (Aroclor 1221) ug/l U 0.05014MW7 BJ89519 SW8082 09/10/15 1 PCB-1232 (Aroclor 1232) ug/l U 0.05014MW7 BJ89519 SW8082 09/10/15 1 PCB-1248 (Aroclor 1248) ug/l U 0.05014MW7 BJ89519 SW8082 09/10/15 1 PCB-1016 (Aroclor 1016) ug/l U 0.05014MW7 BJ89519 SW8082 09/10/15 1 PCB-1262 (Aroclor 1262) ug/l U 0.05014MW7 BJ89519 SW8082 09/10/15 1 PCB-1242 (Aroclor 1242) ug/l U 0.05014MW7 BJ89519 SW8260 09/10/15 1 Ethylbenzene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Styrene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Cis-1,3-Dichloropropene ug/l U 0.4014MW7 BJ89519 SW8260 09/10/15 1 Trans-1,3-Dichloropropene ug/l U 0.4014MW7 BJ89519 SW8260 09/10/15 1 N-Propylbenzene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 N-Butylbenzene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 4-Chlorotoluene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 1,4-Dichlorobenzene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 1,2-Dibromoethane (Ethylene Dibromide) ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Acrolein ug/l UJ 5.014MW7 BJ89519 SW8260 09/10/15 1 1 2-Dichloroethane ug/l U 0 6014MW7 BJ89519 SW8260 09/10/15 1 1,2 Dichloroethane ug/l U 0.6014MW7 BJ89519 SW8260 09/10/15 1 Acrylonitrile ug/l UJ 5.014MW7 BJ89519 SW8260 09/10/15 1 Methyl Isobutyl Ketone (4-Methyl-2-Pentanone) ug/l U 2.514MW7 BJ89519 SW8260 09/10/15 1 1,3,5-Trimethylbenzene (Mesitylene) ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Bromobenzene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Toluene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Chlorobenzene ug/l U 5.014MW7 BJ89519 SW8260 09/10/15 1 Tetrahydrofuran ug/l UJ 5.014MW7 BJ89519 SW8260 09/10/15 1 Trans-1,4-Dichloro-2-Butene ug/l U 2.514MW7 BJ89519 SW8260 09/10/15 1 1,2,4-Trichlorobenzene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Dibromochloromethane ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Tetrachloroethylene (PCE) ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Sec-Butylbenzene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 1,3-Dichloropropane ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Cis-1,2-Dichloroethylene 14 ug/l 1.014MW7 BJ89519 SW8260 09/10/15 1 Trans-1,2-Dichloroethene 0.67 ug/l J 5.014MW7 BJ89519 SW8260 09/10/15 1 Tert-Butyl Methyl Ether ug/l U 1.0

Page 12 of 20



SDG: GBJ89517


14MW7 BJ89519 SW8260 09/10/15 1 m,p-Xylene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 O-Cymene (O-Isopropyltoluene) ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 1,3-Dichlorobenzene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Carbon Tetrachloride ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 1,1-Dichloropropene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 2-Hexanone ug/l UJ 2.514MW7 BJ89519 SW8260 09/10/15 1 2,2-Dichloropropane ug/l UJ 1.014MW7 BJ89519 SW8260 09/10/15 1 1,1,1,2-Tetrachloroethane ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Acetone 3.9 ug/l J 5.014MW7 BJ89519 SW8260 09/10/15 1 Chloroform ug/l U 5.014MW7 BJ89519 SW8260 09/10/15 1 Benzene 0.28 ug/l J 0.7014MW7 BJ89519 SW8260 09/10/15 1 1,1,1-Trichloroethane ug/l U 5.014MW7 BJ89519 SW8260 09/10/15 1 Bromomethane ug/l UJ 5.014MW7 BJ89519 SW8260 09/10/15 1 Chloromethane 1.1 ug/l J 5.014MW7 BJ89519 SW8260 09/10/15 1 Dibromomethane ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Bromochloromethane ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Chloroethane ug/l U 5.014MW7 BJ89519 SW8260 09/10/15 1 Vinyl Chloride 0.63 ug/l J 1.014MW7 BJ89519 SW8260 09/10/15 1 Methylene Chloride ug/l U 3.014MW7 BJ89519 SW8260 09/10/15 1 Carbon Disulfide ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Bromoform ug/l U 5.014MW7 BJ89519 SW8260 09/10/15 1 Bromodichloromethane ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 1,1-Dichloroethane ug/l U 5.014MW7 BJ89519 SW8260 09/10/15 1 1 1-Dichloroethene ug/l U 1 014MW7 BJ89519 SW8260 09/10/15 1 1,1 Dichloroethene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Trichlorofluoromethane ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Dichlorodifluoromethane ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 1,1,2-Trichloro-1,2,2-Trifluoroethane ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 1,2-Dichloropropane ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Methyl Ethyl Ketone (2-Butanone) ug/l UJ 2.514MW7 BJ89519 SW8260 09/10/15 1 1,1,2-Trichloroethane ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Trichloroethylene (TCE) 2.6 ug/l 1.014MW7 BJ89519 SW8260 09/10/15 1 1,1,2,2-Tetrachloroethane ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 1,2,3-Trichlorobenzene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Hexachlorobutadiene ug/l U 0.514MW7 BJ89519 SW8260 09/10/15 1 Naphthalene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 O-Xylene (1,2-Dimethylbenzene) ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 2-Chlorotoluene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 1,2-Dichlorobenzene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 1,2,4-Trimethylbenzene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 1,2-Dibromo-3-Chloropropane ug/l U 1.0

Page 13 of 20



SDG: GBJ89517


14MW7 BJ89519 SW8260 09/10/15 1 1,2,3-Trichloropropane ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 T-Butylbenzene ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Isopropylbenzene (Cumene) ug/l U 1.014MW7 BJ89519 SW8260 09/10/15 1 Cymene ug/l U 1.014MW7 BJ89519 SW8270 09/14/15 1 4-Nitroaniline ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 4-Nitrophenol ug/l U 1.014MW7 BJ89519 SW8270 09/14/15 1 4-Bromophenyl Phenyl Ether ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 2,4-Dimethylphenol ug/l U 1.014MW7 BJ89519 SW8270 09/14/15 1 1,4-Dichlorobenzene ug/l U 1.014MW7 BJ89519 SW8270 09/14/15 1 4-Chloroaniline ug/l U 3.514MW7 BJ89519 SW8270 09/14/15 1 Phenol ug/l U 1.014MW7 BJ89519 SW8270 09/14/15 1 Pyridine ug/l UJ 1014MW7 BJ89519 SW8270 09/14/15 1 Bis(2-Chloroethyl) Ether (2-Chloroethyl Ether) ug/l U 1.014MW7 BJ89519 SW8270 09/14/15 1 Bis(2-Chloroethoxy) Methane ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 Di-N-Octylphthalate ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 Anthracene ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 1,2,4-Trichlorobenzene ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 2,4-Dichlorophenol ug/l U 1.014MW7 BJ89519 SW8270 09/14/15 1 2,4-Dinitrotoluene ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 1,2-Diphenylhydrazine ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 Pyrene ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 Dimethyl Phthalate ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 Dibenzofuran ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 Fluoranthene ug/l U 5 014MW7 BJ89519 SW8270 09/14/15 1 Fluoranthene ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 2,2-Oxybis(2-Chloropropane) ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 2,4-Dinitrophenol ug/l U 1.014MW7 BJ89519 SW8270 09/14/15 1 4,6-Dinitro-2-Methylphenol ug/l U 1.014MW7 BJ89519 SW8270 09/14/15 1 1,3-Dichlorobenzene ug/l U 1.014MW7 BJ89519 SW8270 09/14/15 1 4-Chloro-3-Methylphenol ug/l U 1.014MW7 BJ89519 SW8270 09/14/15 1 2,6-Dinitrotoluene ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 N-Nitrosodi-N-Propylamine ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 Aniline ug/l U 3.514MW7 BJ89519 SW8270 09/14/15 1 N-Nitrosodimethylamine ug/l U 1.014MW7 BJ89519 SW8270 09/14/15 1 Benzoic Acid ug/l U 2514MW7 BJ89519 SW8270 09/14/15 1 4-Chlorophenyl Phenyl Ether ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 Hexachlorocyclopentadiene ug/l UJ 5.014MW7 BJ89519 SW8270 09/14/15 1 Isophorone ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 Acenaphthene ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 Diethyl Phthalate ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 Di-N-Butyl Phthalate ug/l U 5.0

Page 14 of 20



SDG: GBJ89517


14MW7 BJ89519 SW8270 09/14/15 1 Benzyl Butyl Phthalate ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 N-Nitrosodiphenylamine ug/l UJ 5.014MW7 BJ89519 SW8270 09/14/15 1 Fluorene ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 Carbazole ug/l U 2514MW7 BJ89519 SW8270 09/14/15 1 2,4,6-Trichlorophenol ug/l U 1.014MW7 BJ89519 SW8270 09/14/15 1 2-Nitroaniline ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 2-Nitrophenol ug/l U 1.014MW7 BJ89519 SW8270 09/14/15 1 Naphthalene ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 2-Methylnaphthalene ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 2-Chloronaphthalene ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 3,3'-Dichlorobenzidine ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 Benzidine ug/l UJ 4.514MW7 BJ89519 SW8270 09/14/15 1 2-Methylphenol (O-Cresol) ug/l U 1.014MW7 BJ89519 SW8270 09/14/15 1 1,2-Dichlorobenzene ug/l U 1.014MW7 BJ89519 SW8270 09/14/15 1 2-Chlorophenol ug/l U 1.014MW7 BJ89519 SW8270 09/14/15 1 2,4,5-Trichlorophenol ug/l U 1.014MW7 BJ89519 SW8270 09/14/15 1 Acetophenone ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 3-Nitroaniline ug/l U 5.014MW7 BJ89519 SW8270 09/14/15 1 3- And 4- Methylphenol (Total) ug/l U 1.014MW7 BJ89519 SW8270C-SIM 09/11/15 1 Bis(2-Ethylhexyl) Phthalate ug/l U 1.014MW7 BJ89519 SW8270C-SIM 09/11/15 1 Hexachlorobenzene ug/l U 0.0214MW7 BJ89519 SW8270C-SIM 09/11/15 1 Benzo(G,H,I)Perylene ug/l U 0.0214MW7 BJ89519 SW8270C-SIM 09/11/15 1 Indeno(1,2,3-C,D)Pyrene ug/l U 0.0214MW7 BJ89519 SW8270C-SIM 09/11/15 1 Benzo(B)Fluoranthene ug/l U 0 0214MW7 BJ89519 SW8270C SIM 09/11/15 1 Benzo(B)Fluoranthene ug/l U 0.0214MW7 BJ89519 SW8270C-SIM 09/11/15 1 Benzo(K)Fluoranthene ug/l U 0.0214MW7 BJ89519 SW8270C-SIM 09/11/15 1 Acenaphthylene ug/l U 0.1014MW7 BJ89519 SW8270C-SIM 09/11/15 1 Chrysene 0.02 ug/l 0.0214MW7 BJ89519 SW8270C-SIM 09/11/15 1 Benzo(A)Pyrene ug/l U 0.0214MW7 BJ89519 SW8270C-SIM 09/11/15 1 Dibenz(A,H)Anthracene ug/l U 0.0214MW7 BJ89519 SW8270C-SIM 09/11/15 1 Benzo(A)Anthracene 0.02 ug/l 0.0214MW7 BJ89519 SW8270C-SIM 09/11/15 1 Hexachloroethane ug/l U 0.5014MW7 BJ89519 SW8270C-SIM 09/11/15 1 Pentachloronitrobenzene ug/l U 0.1014MW7 BJ89519 SW8270C-SIM 09/11/15 1 Phenanthrene ug/l U 0.1014MW7 BJ89519 SW8270C-SIM 09/11/15 1 Hexachlorobutadiene ug/l U 0.4014MW7 BJ89519 SW8270C-SIM 09/11/15 1 Pentachlorophenol ug/l U 0.8014MW7 BJ89519 SW8270C-SIM 09/11/15 1 1,2,4,5-Tetrachlorobenzene ug/l U 0.5014MW7 BJ89519 SW8270C-SIM 09/11/15 1 Nitrobenzene ug/l U 0.10DUPLICATE BJ89520 7010 09/14/15 1 Antimony mg/l U 0.002DUPLICATE BJ89520 7010 09/11/15 1 Selenium mg/l U 0.002DUPLICATE BJ89520 7010 09/15/15 1 Thallium mg/l U 0.0005

Page 15 of 20



SDG: GBJ89517


DUPLICATE BJ89520 SW6010 09/10/15 1 Aluminum 0.569 mg/l J 0.010DUPLICATE BJ89520 SW6010 09/10/15 1 Arsenic 0.003 mg/l J 0.004DUPLICATE BJ89520 SW6010 09/10/15 1 Barium 0.011 mg/l J 0.010DUPLICATE BJ89520 SW6010 09/10/15 1 Calcium 26.5 mg/l J 0.010DUPLICATE BJ89520 SW6010 09/10/15 1 Chromium, Total 0.001 mg/l J 0.001DUPLICATE BJ89520 SW6010 09/10/15 1 Copper 0.002 mg/l J 0.005DUPLICATE BJ89520 SW6010 09/10/15 1 Iron 0.75 mg/l J 0.01DUPLICATE BJ89520 SW6010 09/10/15 1 Lead 0.004 mg/l J 0.002DUPLICATE BJ89520 SW6010 09/10/15 1 Magnesium 1.65 mg/l J 0.01DUPLICATE BJ89520 SW6010 09/10/15 1 Beryllium mg/l U 0.001DUPLICATE BJ89520 SW6010 09/10/15 1 Cadmium mg/l U 0.004DUPLICATE BJ89520 SW6010 09/10/15 1 Manganese 0.315 mg/l J 0.005DUPLICATE BJ89520 SW6010 09/10/15 1 Cobalt mg/l U 0.005DUPLICATE BJ89520 SW6010 09/12/15 1 Nickel 0.004 mg/l J 0.004DUPLICATE BJ89520 SW6010 09/10/15 1 Potassium 2.9 mg/l J 0.1DUPLICATE BJ89520 SW6010 09/10/15 1 Sodium 8.1 mg/l J 0.1DUPLICATE BJ89520 SW6010 09/10/15 1 Silver mg/l U 0.005DUPLICATE BJ89520 SW6010 09/10/15 1 Vanadium 0.001 mg/l J 0.010DUPLICATE BJ89520 SW6010 09/10/15 1 Zinc 0.003 mg/l J 0.010DUPLICATE BJ89520 SW7470 09/10/15 1 Mercury mg/l U 0.0002DUPLICATE BJ89520 SW8081 09/10/15 1 Heptachlor Epoxide ug/l U 0.010DUPLICATE BJ89520 SW8081 09/10/15 1 Endosulfan Sulfate ug/l U 0.010DUPLICATE BJ89520 SW8081 09/10/15 1 Alachlor ug/l U 0.075DUPLICATE BJ89520 SW8081 09/10/15 1 Aldrin ug/l U 0 003DUPLICATE BJ89520 SW8081 09/10/15 1 Aldrin ug/l U 0.003DUPLICATE BJ89520 SW8081 09/10/15 1 Alpha Bhc (Alpha Hexachlorocyclohexane) ug/l U 0.005DUPLICATE BJ89520 SW8081 09/10/15 1 Beta Bhc (Beta Hexachlorocyclohexane) ug/l U 0.015DUPLICATE BJ89520 SW8081 09/10/15 1 Delta BHC (Delta Hexachlorocyclohexane) ug/l U 0.005DUPLICATE BJ89520 SW8081 09/10/15 1 Beta Endosulfan ug/l U 0.010DUPLICATE BJ89520 SW8081 09/10/15 1 P,P'-DDT ug/l U 0.010DUPLICATE BJ89520 SW8081 09/10/15 1 cis-Chlordane ug/l U 0.010DUPLICATE BJ89520 SW8081 09/10/15 1 trans-Chlordane ug/l U 0.016DUPLICATE BJ89520 SW8081 09/10/15 1 Endrin Ketone ug/l U 0.010DUPLICATE BJ89520 SW8081 09/10/15 1 Chlordane ug/l U 0.05DUPLICATE BJ89520 SW8081 09/10/15 1 Gamma Bhc (Lindane) ug/l U 0.011DUPLICATE BJ89520 SW8081 09/10/15 1 Dieldrin ug/l U 0.004DUPLICATE BJ89520 SW8081 09/10/15 1 Endrin ug/l U 0.010DUPLICATE BJ89520 SW8081 09/10/15 1 Methoxychlor ug/l U 0.10DUPLICATE BJ89520 SW8081 09/10/15 1 P,P'-DDD ug/l U 0.010DUPLICATE BJ89520 SW8081 09/10/15 1 P,P'-DDE ug/l U 0.010DUPLICATE BJ89520 SW8081 09/10/15 1 Endrin Aldehyde ug/l U 0.010

Page 16 of 20



SDG: GBJ89517


DUPLICATE BJ89520 SW8081 09/10/15 1 Heptachlor ug/l U 0.010DUPLICATE BJ89520 SW8081 09/10/15 1 Toxaphene ug/l U 0.25DUPLICATE BJ89520 SW8081 09/10/15 1 Alpha Endosulfan ug/l U 0.010DUPLICATE BJ89520 SW8082 09/10/15 1 PCB-1260 (Aroclor 1260) ug/l U 0.050DUPLICATE BJ89520 SW8082 09/10/15 1 PCB-1254 (Aroclor 1254) ug/l U 0.050DUPLICATE BJ89520 SW8082 09/10/15 1 PCB-1268 (Aroclor 1268) ug/l U 0.050DUPLICATE BJ89520 SW8082 09/10/15 1 PCB-1221 (Aroclor 1221) ug/l U 0.050DUPLICATE BJ89520 SW8082 09/10/15 1 PCB-1232 (Aroclor 1232) ug/l U 0.050DUPLICATE BJ89520 SW8082 09/10/15 1 PCB-1248 (Aroclor 1248) ug/l U 0.050DUPLICATE BJ89520 SW8082 09/10/15 1 PCB-1016 (Aroclor 1016) ug/l U 0.050DUPLICATE BJ89520 SW8082 09/10/15 1 PCB-1262 (Aroclor 1262) ug/l U 0.050DUPLICATE BJ89520 SW8082 09/10/15 1 PCB-1242 (Aroclor 1242) ug/l U 0.050DUPLICATE BJ89520 SW8260 09/10/15 1 Ethylbenzene ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Styrene ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Cis-1,3-Dichloropropene ug/l U 0.40DUPLICATE BJ89520 SW8260 09/10/15 1 Trans-1,3-Dichloropropene ug/l U 0.40DUPLICATE BJ89520 SW8260 09/10/15 1 N-Propylbenzene ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 N-Butylbenzene ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 4-Chlorotoluene ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 1,4-Dichlorobenzene ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 1,2-Dibromoethane (Ethylene Dibromide) ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Acrolein ug/l UJ 5.0DUPLICATE BJ89520 SW8260 09/10/15 1 1,2-Dichloroethane ug/l U 0.60DUPLICATE BJ89520 SW8260 09/10/15 1 Acrylonitrile ug/l UJ 5 0DUPLICATE BJ89520 SW8260 09/10/15 1 Acrylonitrile ug/l UJ 5.0DUPLICATE BJ89520 SW8260 09/10/15 1 Methyl Isobutyl Ketone (4-Methyl-2-Pentanone) ug/l U 2.5DUPLICATE BJ89520 SW8260 09/10/15 1 1,3,5-Trimethylbenzene (Mesitylene) ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Bromobenzene ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Acetone 3.8 ug/l J 5.0DUPLICATE BJ89520 SW8260 09/10/15 1 Chlorobenzene ug/l U 5.0DUPLICATE BJ89520 SW8260 09/10/15 1 Tetrahydrofuran ug/l UJ 5.0DUPLICATE BJ89520 SW8260 09/10/15 1 Trans-1,4-Dichloro-2-Butene ug/l U 2.5DUPLICATE BJ89520 SW8260 09/10/15 1 1,2,4-Trichlorobenzene ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Dibromochloromethane ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Tetrachloroethylene (PCE) ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Sec-Butylbenzene ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 1,3-Dichloropropane ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Chloromethane 1.7 ug/l J 5.0DUPLICATE BJ89520 SW8260 09/10/15 1 Trans-1,2-Dichloroethene ug/l U 5.0DUPLICATE BJ89520 SW8260 09/10/15 1 Tert-Butyl Methyl Ether ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 m,p-Xylene ug/l U 1.0

Page 17 of 20



SDG: GBJ89517


DUPLICATE BJ89520 SW8260 09/10/15 1 O-Cymene (O-Isopropyltoluene) ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 1,3-Dichlorobenzene ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Carbon Tetrachloride ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 1,1-Dichloropropene ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 2-Hexanone ug/l UJ 2.5DUPLICATE BJ89520 SW8260 09/10/15 1 2,2-Dichloropropane ug/l UJ 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 1,1,1,2-Tetrachloroethane ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Cis-1,2-Dichloroethylene 8.9 ug/l 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Chloroform ug/l U 5.0DUPLICATE BJ89520 SW8260 09/10/15 1 Benzene ug/l U 0.70DUPLICATE BJ89520 SW8260 09/10/15 1 1,1,1-Trichloroethane ug/l U 5.0DUPLICATE BJ89520 SW8260 09/10/15 1 Bromomethane ug/l UJ 5.0DUPLICATE BJ89520 SW8260 09/10/15 1 Toluene 0.64 ug/l J 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Dibromomethane ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Bromochloromethane ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Chloroethane ug/l U 5.0DUPLICATE BJ89520 SW8260 09/10/15 1 Trichloroethylene (TCE) 3.3 ug/l 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Methylene Chloride ug/l U 3.0DUPLICATE BJ89520 SW8260 09/10/15 1 Carbon Disulfide ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Bromoform ug/l U 5.0DUPLICATE BJ89520 SW8260 09/10/15 1 Bromodichloromethane ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 1,1-Dichloroethane ug/l U 5.0DUPLICATE BJ89520 SW8260 09/10/15 1 1,1-Dichloroethene ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Trichlorofluoromethane ug/l U 1 0DUPLICATE BJ89520 SW8260 09/10/15 1 Trichlorofluoromethane ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Dichlorodifluoromethane ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 1,1,2-Trichloro-1,2,2-Trifluoroethane ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 1,2-Dichloropropane ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Methyl Ethyl Ketone (2-Butanone) ug/l UJ 2.5DUPLICATE BJ89520 SW8260 09/10/15 1 1,1,2-Trichloroethane ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Vinyl Chloride 1.3 ug/l 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 1,1,2,2-Tetrachloroethane ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 1,2,3-Trichlorobenzene ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Hexachlorobutadiene ug/l U 0.5DUPLICATE BJ89520 SW8260 09/10/15 1 Naphthalene ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 O-Xylene (1,2-Dimethylbenzene) ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 2-Chlorotoluene ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 1,2-Dichlorobenzene ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 1,2,4-Trimethylbenzene ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 1,2-Dibromo-3-Chloropropane ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 1,2,3-Trichloropropane ug/l U 1.0

Page 18 of 20



SDG: GBJ89517


DUPLICATE BJ89520 SW8260 09/10/15 1 T-Butylbenzene ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Isopropylbenzene (Cumene) ug/l U 1.0DUPLICATE BJ89520 SW8260 09/10/15 1 Cymene ug/l U 1.0DUPLICATE BJ89520 SW8270 09/14/15 1 4-Nitroaniline ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 4-Nitrophenol ug/l U 1.0DUPLICATE BJ89520 SW8270 09/14/15 1 4-Bromophenyl Phenyl Ether ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 2,4-Dimethylphenol ug/l U 1.0DUPLICATE BJ89520 SW8270 09/14/15 1 1,4-Dichlorobenzene ug/l U 1.0DUPLICATE BJ89520 SW8270 09/14/15 1 4-Chloroaniline ug/l U 3.5DUPLICATE BJ89520 SW8270 09/14/15 1 Phenol ug/l U 1.0DUPLICATE BJ89520 SW8270 09/14/15 1 Pyridine ug/l UJ 10DUPLICATE BJ89520 SW8270 09/14/15 1 Bis(2-Chloroethyl) Ether (2-Chloroethyl Ether) ug/l U 1.0DUPLICATE BJ89520 SW8270 09/14/15 1 Bis(2-Chloroethoxy) Methane ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 Di-N-Octylphthalate ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 Anthracene ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 1,2,4-Trichlorobenzene ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 2,4-Dichlorophenol ug/l U 1.0DUPLICATE BJ89520 SW8270 09/14/15 1 2,4-Dinitrotoluene ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 1,2-Diphenylhydrazine ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 Pyrene ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 Dimethyl Phthalate ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 Dibenzofuran ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 Fluoranthene ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 2 2-Oxybis(2-Chloropropane) ug/l U 5 0DUPLICATE BJ89520 SW8270 09/14/15 1 2,2 Oxybis(2 Chloropropane) ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 2,4-Dinitrophenol ug/l U 1.0DUPLICATE BJ89520 SW8270 09/14/15 1 4,6-Dinitro-2-Methylphenol ug/l U 1.0DUPLICATE BJ89520 SW8270 09/14/15 1 1,3-Dichlorobenzene ug/l U 1.0DUPLICATE BJ89520 SW8270 09/14/15 1 4-Chloro-3-Methylphenol ug/l U 1.0DUPLICATE BJ89520 SW8270 09/14/15 1 2,6-Dinitrotoluene ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 N-Nitrosodi-N-Propylamine ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 Aniline ug/l U 3.5DUPLICATE BJ89520 SW8270 09/14/15 1 N-Nitrosodimethylamine ug/l U 1.0DUPLICATE BJ89520 SW8270 09/14/15 1 Benzoic Acid ug/l U 25DUPLICATE BJ89520 SW8270 09/14/15 1 4-Chlorophenyl Phenyl Ether ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 Hexachlorocyclopentadiene ug/l UJ 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 Isophorone ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 Acenaphthene ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 Diethyl Phthalate ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 Di-N-Butyl Phthalate ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 Benzyl Butyl Phthalate ug/l U 5.0

Page 19 of 20



SDG: GBJ89517


DUPLICATE BJ89520 SW8270 09/14/15 1 N-Nitrosodiphenylamine ug/l UJ 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 Fluorene ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 Carbazole ug/l U 25DUPLICATE BJ89520 SW8270 09/14/15 1 2,4,6-Trichlorophenol ug/l U 1.0DUPLICATE BJ89520 SW8270 09/14/15 1 2-Nitroaniline ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 2-Nitrophenol ug/l U 1.0DUPLICATE BJ89520 SW8270 09/14/15 1 Naphthalene ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 2-Methylnaphthalene ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 2-Chloronaphthalene ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 3,3'-Dichlorobenzidine ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 Benzidine ug/l UJ 4.5DUPLICATE BJ89520 SW8270 09/14/15 1 2-Methylphenol (O-Cresol) ug/l U 1.0DUPLICATE BJ89520 SW8270 09/14/15 1 1,2-Dichlorobenzene ug/l U 1.0DUPLICATE BJ89520 SW8270 09/14/15 1 2-Chlorophenol ug/l U 1.0DUPLICATE BJ89520 SW8270 09/14/15 1 2,4,5-Trichlorophenol ug/l U 1.0DUPLICATE BJ89520 SW8270 09/14/15 1 Acetophenone ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 3-Nitroaniline ug/l U 5.0DUPLICATE BJ89520 SW8270 09/14/15 1 3- And 4- Methylphenol (Total) ug/l U 1.0DUPLICATE BJ89520 SW8270C-SIM 09/11/15 1 Bis(2-Ethylhexyl) Phthalate ug/l U 1.0DUPLICATE BJ89520 SW8270C-SIM 09/11/15 1 Hexachlorobenzene ug/l U 0.02DUPLICATE BJ89520 SW8270C-SIM 09/11/15 1 Benzo(G,H,I)Perylene ug/l U 0.02DUPLICATE BJ89520 SW8270C-SIM 09/11/15 1 Indeno(1,2,3-C,D)Pyrene ug/l U 0.02DUPLICATE BJ89520 SW8270C-SIM 09/11/15 1 Benzo(B)Fluoranthene ug/l U 0.02DUPLICATE BJ89520 SW8270C-SIM 09/11/15 1 Benzo(K)Fluoranthene ug/l U 0 02DUPLICATE BJ89520 SW8270C SIM 09/11/15 1 Benzo(K)Fluoranthene ug/l U 0.02DUPLICATE BJ89520 SW8270C-SIM 09/11/15 1 Acenaphthylene ug/l U 0.10DUPLICATE BJ89520 SW8270C-SIM 09/11/15 1 Chrysene 0.03 ug/l 0.02DUPLICATE BJ89520 SW8270C-SIM 09/11/15 1 Benzo(A)Pyrene ug/l U 0.02DUPLICATE BJ89520 SW8270C-SIM 09/11/15 1 Dibenz(A,H)Anthracene ug/l U 0.02DUPLICATE BJ89520 SW8270C-SIM 09/11/15 1 Benzo(A)Anthracene ug/l U 0.02DUPLICATE BJ89520 SW8270C-SIM 09/11/15 1 Hexachloroethane ug/l U 0.50DUPLICATE BJ89520 SW8270C-SIM 09/11/15 1 Pentachloronitrobenzene ug/l U 0.10DUPLICATE BJ89520 SW8270C-SIM 09/11/15 1 Phenanthrene ug/l U 0.10DUPLICATE BJ89520 SW8270C-SIM 09/11/15 1 Hexachlorobutadiene ug/l U 0.40DUPLICATE BJ89520 SW8270C-SIM 09/11/15 1 Pentachlorophenol ug/l U 0.80DUPLICATE BJ89520 SW8270C-SIM 09/11/15 1 1,2,4,5-Tetrachlorobenzene ug/l U 0.50DUPLICATE BJ89520 SW8270C-SIM 09/11/15 1 Nitrobenzene ug/l U 0.10

Page 20 of 20



USEPA Region II –Data Validation Project Name: 510 Driggs Avenue Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBJ90192 Client: Environmental Business Consultants Date: 12/30/2015 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for three (3) water samples for Semi-volatiles

by SW-846 Method 8270D [full scan and Selected Ion Monitoring (SIM)] in accordance with the NYSDEC, Analytical Services Protocol (ASP) Format.









Collection Date


14MW 1 BJ90192 9/09/15 SVO Water 14MW 3 BJ90193 9/09/15 SVO Water 14MW 4 BJ90194 9/09/15 SVO Water





abundance criteria. No qualifications were required. Initial Calibration: 1. Initial calibration curve analyzed on 09/10/2015 (CHEM05)-Full Scan exhibited


2. Initial calibration curve analyzed on 09/10/2015 (CHEM04)-SIM Scan exhibited



Continuing Calibration Verification (CCV): 1. CCV analyzed on 09/15/2015 @ 07:57 (CHEM05)-Full scan exhibited acceptable %Ds


2. CCV analyzed on 09/15/2015 @ 15:46 (CHEM05)-Full scan exhibited acceptable %Ds






Surrogates: 1. All surrogate %REC values were within the QC acceptance limits for the full scan. No

qualifications were required. 2. All surrogate %REC values were within the QC acceptance limits for the SIM scan. No

qualifications were required. Internal Standard (IS) Area Performance: 1. All samples exhibited acceptable area count for all six internal standards. No

qualifications were required. Method Blank (MB), Storage Blank (SB), Trip Blank (TB), Field Blank (FB), Rinsate Blank (RB) and Equipment Blank (EB): 1. Method Blank (BJ90192 BLANK)-full Scan associated with the water samples extracted


2. Method Blank (BJ90192 BLANK)-SIM Scan associated with the water samples extracted

on 9/10/2015 and analyzed on 09/14/2015.



Compound Results (g/L)

Action Level (2x CRQL)

(g/L)

Sample Affected

Action

BLANK BJ90192 Bis(2-ethylhexyl)phthalate

0.17 0.10 14MW 1, 14MW 3 1MW 4

U


Batch ID: BJ90192-SIM were analyzed on 09/14/2015. All %RECs and RPDs were within the laboratory control limits with the following exception(s):


Affected Action

Bis(2-ethylhexyl)phthalate 126/140/A 14MW 1, 14MW 3 1MW 4 None 2. Laboratory Control Sample and Laboratory Control Sample Duplicate associated with



Affected Action

Benzyl Alcohol A/A/20.4 14MW 1, 14MW 3 1MW 4 UJ Hexachlorocyclopentadiene A/A/21.1 14MW 1, 14MW 3 1MW 4 UJ

Field Duplicate: 1. A field duplicate pair was not submitted with this SDG. Matrix Spike (MS)/Matrix Spike Duplicate (MSD): 1. Matrix Spike (MS)/Matrix Spike Duplicate (MSD) were not performed on sample from

this SDG. Target Compound Identification: 1. All Relative Retention Times (RRTs) of the reported compounds were within 0.06


2. Sample compound spectra were compared against the laboratory standard spectra.


3. No QC deviations were observed. Compound Quantitation and Reported Detection Limits: 1. All sample results were reported within the linear calibration range. 2. Manual Calculation:

Cx = (Ax)(IS)(VE)(DF) (Ais)(RRF)(Volume injected, L)(V)

Cx = concentration of analyte as ug/L Ax = Area of the characteristic ion for the compound to be measured, counts. Ais = Area of the characteristic ion for the specific internal standard, counts. IS = Concentration of the internal standard spiking mixture, ng RRF= Mean relative response factor from the initial calibration. DF = Dilution factor calculated. If no dilution is performed, DF= 1 V= Volume for liquids in ml, weight for soils/solids in grams. VE= final volume of concentrated extract Sample: 14MW 1 (BJ90192)

Acenaphthylene Initial Volume: 1000ml Final volume: 1ml Volume injected: 1l Dilution Factor: 1 Concentration (g/L) = 656454 x 4 x 1ml x 1 x 1000 = 1.8372g/L 887721 x 1.610 x 1l x 1000ml

Compound Laboratory

(g/L) Validation

(g/L) %D

Acenaphthylene 1.8 1.8 0.0 Comments: 1. Semivolatile data package meet requirement for New York State Department of





USEPA Region II –Data Validation Project Name: 510 Driggs Avenue Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBJ90192 Client: Environmental Business Consultants Date: 12/30/2015 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for three (3) water samples and one (1) trip

blank analyzed for Volatiles by SW-846 Method 8260C in accordance to NYSDEC, Analytical Services Protocol (ASP) Format.









Collection Date


14MW 1 BJ90192 9/09/15 VOA Water 14MW 3 BJ90193 9/09/15 VOA Water 14MW 4 BJ90194 9/09/15 VOA Water

TRIP BLANK BJ90195 9/09/15 VOA Water Trip Blank Sample Conditions/Problems: 1. The Traffic Reports/Chain-of-Custody Records, Sampling Report and/or Laboratory Case






Compound RRF %D

Acetone A 24.5 Acrylonitrile A 20.4

Tetrahydrofuran A 20.2 A= Acceptable




14MW 3 BJ90193 Acetone Acrylonitrile, Tetrahydrofuran

J UJ

14MW 4 BJ90194 Acetone, Acrylonitrile, Tetrahydrofuran UJ TRIP BLANK BJ90195 Acetone, Acrylonitrile, Tetrahydrofuran UJ

2. Initial calibration curve analyzed on 09/13/2015 (Chem02) exhibited acceptable %RSDs (30.0%) for CCC compounds and average RRF values for SPCC compounds. Also, %RSDs for all other compounds, were 20.0% and average RRF (>0.050) with the following exception(s):

Compound RRF %D

Bromomethane A 25.9 Bromoform A 22.5

Trans-1,4-Dichloro-2-butene A 21.3 A= Acceptable


Compound Action

14MW 1 BJ90192 Bromomethane, Bromoform, Trans-1,4-Dichloro-2-butene

UJ


None


None



Compound %D

Bromomethane(1) 34.2 A= Acceptable

(1) Results for these compounds were previously qualified due to ICV criteria.



Compound Action

14MW 3 BJ90193 Bromomethane UJ 14MW 4 BJ90194 Bromomethane UJ

TRIP BLANK BJ90195 Bromomethane UJ 2. CCV analyzed on 09/12/2015 @ 07:11 (CHEM02) exhibited acceptable %Ds (20.0%)


Compound %D

Dichlorodifluoromethane 27.0 Bromomethane(1) 25.7

Trichlorofluoromethane 25.7 Trichlorotrifluoroethane 30.1

Acetone(1) 20.6 2,2-Dichloropropane 29.4

A= Acceptable (1) Results for this compound were previously qualified due to IVC/initial CCV criteria.



14MW 3 BJ90193 Dichlorodifluoromethane, Bromomethane, Trichlorofluoromethane, Trichlorotrifluoroethane,

2,2-Dichloropropane Acetone

UJ UJ UJ J

14MW 4 BJ90194 Dichlorodifluoromethane, Bromomethane, Trichlorofluoromethane, Trichlorotrifluoroethane,

Acetone, 2,2-Dichloropropane

UJ

TRIP BLANK BJ90195 Dichlorodifluoromethane, Bromomethane, Trichlorofluoromethane, Trichlorotrifluoroethane,

Acetone, 2,2-Dichloropropane

UJ








Compound %D

Bromomethane 40.2 Acrolein 27.7

Methylene Chloride 27.2 Methyl t-Butyl Ether 23.1 2,2-Dichloropropane 33.0 1,2-Dichloroethane 21.1

Bromodichloromethane 20.2 Cis-1,3-Dichloropropene 21.8 4-Methyl-2-Pentanone 23.2

Trans-1,3-Dichloropropene 25.0 1,1,2-Trichloroethane 22.9

Dibromochloromethane 23.1 1,2-Dibromoethane 20.6

2-Hexanone 23.0 1,1,1,2-Tetrachloroethane 20.8

Bromoform 29.0 Bromobenzene 21.3

1,1,2,2-Tetrachloroethane 21.8 Trans-1,4-Dichloro-2-butene 44.8

1,3-Dichlorobenzene 20.9 1,4-Dichlorobenzene 21.9 1,2-Dichlorobenzene 21.8

1,2-Dibromo-3-Chloropropane 32.0 Hexachlorobutadiene 26.5

1,2,4-Trichlorobenzene 27.4 Naphthalene 27.4

1,2,3-Trichlorobenzene 29.0 A= Acceptable


Compound Action

14MW 1DL BJ90192 Bromomethane, Acrolein, Methylene Chloride, Methyl t-Butyl Ether, 2,2-Dichloropropane, 1,2-Dichloroethane, Bromodichloromethane,

None



Compound Action

Cis-1,3-Dichloropropene, 4-Methyl-2-Pentanone, Trans-1,3-Dichloropropene, 1,1,2-Trichloroethane,

Dibromochloromethane, 1,2-Dibromoethane, 2-Hexanone, 1,1,1,2-Tetrachloroethane, Bromoform,

Bromobenzene, 1,1,2,2-Tetrachloroethane, Trans-1,4-Dichloro-2-butene, 1,3-Dichlorobenzene,

1,4-Dichlorobenzene, 1,2-Dichlorobenzene, 1,2-Dibromo-3-Chloropropane, Hexachlorobutadiene,

1,2,4-Trichlorobenzene, Naphthalene, 1,2,3-Trichlorobenzene



limits. No qualifications were required. Method Blank (MB), Storage Blank (SB), Trip Blank (TB), Field Blank (FB), Rinsate Blank (RB) and Equipment Blank (EB): 1. Method Blank (BLANK BJ90195) was analyzed on 09/11/2015.



Action Level

(2x CRQL) (g/L)

Sample Affected

Action

BLANK BJ90195 Hexachlorobutadiene 0.13 0.40 14MW4, 14MW3, Trip Blank

None


2. Method Blank (BLANK BJ91084) was analyzed on 09/14/2015.



Action Level

(2x CRQL) (g/L)

Sample Affected

Action

BLANK BJ91084 Hexachlorobutadiene 0.13 0.40 14MW4DL, 14MW3DL, 14MW1

None

3. Method Blank (BLANK BJ91360) was analyzed on 09/15/2015.



Action Level

(2x CRQL) (g/L)

Sample Affected

Action

BLANK BJ91360 Hexachlorobutadiene 0.13 0.40 14MW1DL None 4. Trip Blank (BJ90195) was analyzed on 09/11/2015 was free of contamination. No

qualifications were required. Laboratory Control Sample (LCS)/ Laboratory Control Sample Duplicate (LCSD):


Batch ID: BJ90195 were analyzed on 09/11/2015. All %RECs and RPDs were within the laboratory control limits. No qualifications were required.




Affected Action

Bromomethane A/NC/NC 14MW3DL, 14MW4DL, 14MW1 None A= Acceptable NC=Not calculatated

3. Laboratory Control Sample and Laboratory Control Sample Duplicate associated with Batch ID: BJ91360 were analyzed on 09/15/2015. All %RECs and RPDs were within the laboratory control limits with the following exception(s):



Action

Dichlorodifluoromethane 146/143/A 14MW1DL None Bromomethane 137/140/A 14MW1DL None

A= Acceptable Field Duplicate: 1. A field duplicate pair was not submitted with this SDG. Matrix Spike (MS)/ Matrix Spike Duplicate (MSD): 1. Matrix Spike (MS)/Matrix Spike Duplicate (MSD) were not performed on sample from




were required. 2. Manual Calculation: Cx = (Ax)(IS)(DF)

(Ais)(RRF)(V)



14MW 1 (BJ90192) Chloromethane Sample Volume= 25ml Volume purged=25ml DF = 1 Concentration (g/L)= 12191 x 25 x 10 x 1 = 0.7443g/L 327592 x 0.500 x 25

Compound Laboratory

(g/L) Validation

(g/L) %D

Chloromethane 0.74 0.74 0.0 Comments: 1. Volatile data package meet requirement for New York State Department of






Project Name: 510 Driggs Avenue Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBJ90192 Client: Environmental Business Consultants Date: 12/30/2015 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for three (3) water samples analyzed for



Environmental Laboratories, Inc., Manchester, CT on 9/10/2015 for analysis. 3. The USEPA Region-II SOP HW-44, Revision 1, October 2006, Validating Pesticide







Collection Date


14MW 1 BJ90192 9/09/15 Pesticides Water 14MW 3 BJ90193 9/09/15 Pesticides Water 14MW 4 BJ90194 9/09/15 Pesticides Water





were required. Initial Calibration: 1. Initial calibration curve analyzed on 9/03/2015 (ECD35) exhibited acceptable %RSD. No

qualifications are required. All sample results were reported from Column A. No qualifications were required. Continuing Calibration Verification (CCV): 1. The CCVs analyzed on 9/16-17/2015 exhibited acceptable %Ds (20.0%) with the



9/17/2015 @ 0:58:

Compound Column %D Endosulfan I A 24.0

4,4’-DDD B 22 Methoxychlor B 34

Note: Results were reported from the A column.

Client Sample ID


Compound Action

14MW 1 BJ90192 Endosulfan I UJ 14MW 3 BJ90193 Endosulfan I UJ 14MW 4 BJ90194 Endosulfan I UJ


laboratory control limits. Results were taken from column A. No qualifications were required.

Method Blank (MB), Storage Blank (SB), Trip Blank (TB), Field Blank (FB), Rinsate Blank (RB) and Equipment Blank (EB): 1. Method Blank (BJ90192) associated with the water samples extracted on 9/15/2015 and

analyzed on 09/16/2015 was free of contamination. No qualifications were required. Laboratory Control Sample (LCS)/ Laboratory Control Sample Duplicate (LCSD): 1. Laboratory Control Sample and Laboratory Control Sample Duplicate associated with


Field Duplicate: 1. A field duplicate pair was not submitted with this SDG.


Matrix Spike (MS)/ Matrix Spike Duplicate (MSD): 1. Matrix Spike (MS)/Matrix Spike Duplicate (MSD) were not performed on sample from

this SDG. Compound Quantitation, Compound Identification and Reported Detection Limits: 1. All sample results were reported within the linear calibration range. 2. Manual Calculation: BJ90192

Alpha-BHC

On Column concentration (A)= 44.7861ng Sample Volume= 1000ml DF = 1 Concentration (g/L) = 44.7861ng x 5 x 1ml = 0.2239g/L 1000

Compound Laboratory

(g/L) Validation

(g/L) %D

Alpha-BHC 0.224 0.224 0.0 Comments: 1. Pesticides data package meet requirement for New York State Department of






Project Name: 510 Driggs Avenue Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBJ90192 Client: Environmental Business Consultants Date: 12/30/2015 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for three (3) water samples analyzed for PCBs










Collection Date


14MW 1 BJ90192 9/09/15 PCBs Water 14MW 3 BJ90193 9/09/15 PCBs Water 14MW 4 BJ90194 9/09/15 PCBs Water





(20.0%) on both columns. No qualifications were required. 2. All sample results were reported from Column B. Continuing Calibration Verification (CCV): 1. All CCVs analyzed on 09/11/2015 exhibited acceptable %Ds (15.0%) for all

compounds. No qualifications were required. Surrogates: 1. All surrogates %RECs values for all water samples and associated QC were within the

laboratory control limits. No qualifications were required.


Method Blank (MB), Storage Blank (SB), Trip Blank (TB), Field Blank (FB), Rinsate Blank (RB) and Equipment Blank (EB): 1. Method Blank (BJ90192 BL) associated with the water samples extracted on 9/10/2015



Field Duplicate: 1. A field duplicate pair was not submitted with this SDG. Matrix Spike (MS)/ Matrix Spike Duplicate (MSD): 1. Matrix Spike (MS)/Matrix Spike Duplicate (MSD) were not performed on sample from

this SDG. Compound Quantitation, Compound Identification and Reported Detection Limits: 1. All sample results were reported within the linear calibration range. 2. Manual Calculation: BJ90192 LCS

Aroclor-1016

On Column concentration (B)= 344.363ng Sample Volume= 1000ml DF= 1 Vi= 5ml Concentration (g/L) = 344.363ng x 5ml x 1 = 1.72g/L 1000


Compound Laboratory

(g/L) Validation

(g/L) %D

Aroclor-1016 1.72 1.72 0.0 Comments: 1. PCBs data package meet requirement for New York State Department of Environmental




USEPA Region II –Data Validation Project Name: 510 Driggs Avenue Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBJ90192 Client: Environmental Business Consultants Date: 12/30/2015 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for three (3) water samples (both total and

dissolved) analyzed for the following analyses:

1.1 Trace Metals-ICP-AES by SW-846 Method 6010C. 1.2 Thallium, antimony, and selenium by SW-846 Method 7010 (GFAA). 1.3 Mercury by SW-846 Method 7470A.



Metals for Contract Laboratory Program (CLP), based on SOW-ILM05.3 (SOP Revision 13) was used in evaluating the Trace Metals (total and dissolved) data in this summary report.






Collection Date


14MW 1* BJ90192 9/09/15 ICP, GFAA and CVAA Water 14MW 3* BJ90193 9/09/15 ICP, GFAA and CVAA Water 14MW 4* BJ90194 9/09/15 ICP, GFAA and CVAA Water

*Total and dissolved analyses Sample Conditions/Problems: 1. The Traffic Reports/Chain-of-Custody Records, Sampling Report and/or Laboratory Case


Holding Times: 1. All water samples were analyzed within the 6 months holding times for Trace Metals

analyses by ICP-AES and GFAA. No qualifications were required. 2. All water samples were digested and analyzed within the 28 days holding times for

Mercury analysis. No qualifications were required. Initial and Continuing Calibration Verification (ICV and CCV): ICP-AES and GFAA: 1. All %RECs in the ICV and CCVs were within QC limits (90-110%) for total samples

with the following exception(s): Analyte Date


Antimony (Total)

9/14/15: 13:10 110.3 14MW1, 14MW3, 14MW4 None


Mercury: 1 All correlation coefficient for Mercury calibration curve analyzed were 0.995. No


qualifications were required. CRQL Check Standard (CRI): 1. All CRI analyzed on 8/22/2015 %RECs were within the control limits (70-130%). No

qualifications were required. ICP-AES Interference Check Sample: 1. All %REC values were within the QC limits (80-120%) for ICSA and ICSAB with the

following exception(s): Analyte Date


Potassium (Dissolved/

Total)

9/15/15: 8:03/8:06

122.5 14MW1 (Total), 14MW3 (Total), 14MW4 (Total)

J+

9/15/15: 9:34/9:37

123.2 14MW1 (Dissolved), 14MW3 (Dissolved), 14MW4 (Dissolved)

J+

Blanks (Method Blank, ICB and CCB): ICP-AES and GFAA: 1. Method Blank-Water (Dissolved) (BJ90194 BLK) (furnace) digested on 9/11/2015 was

free of contamination. No qualifications were required. 2. Method Blank-Water (Dissolved) (BJ90193 BLK) (ICP) digested on 9/11/2015 was free

of contamination. No qualifications were required. 3. Method Blank-Water (Total) (BJ90193 BLK) (ICP) digested on 9/11/2015 was free of

contamination. No qualifications were required.


4. Method Blank-Water (Total) (BJ90194 BLK) (ICP) digested on 9/10/2015 was free of contamination. No qualifications were required.

5. Method Blank-Water (Total) (BJ90192 BLK) (furnace) digested on 9/10/2015 was free

of contamination. No qualifications were required. 6. ICBs and CCBs analyzed on 9/10-15/2015.

Element Concentration (µg/L)

CRQL* (µg/L)


Lead 2 2 None None (Dissolved) 2 2 14MW1, 14MW4 U

2 2 None None Lead 2 4 None None

(Total) 2 4 None None Nickel 2 4 None None (Total) 2 4 14MW4 U

Arsenic (Total) 1 4 None None *= If sample concentration >MDL but < Reporting limit, then sample result qualified as non-

detect (U). If sample concentration greater than CRQL but less than10x the blank result, then qualify estimated (J). If sample concentration greater than 10x the blank results or sample was not detected then no qualifications or action is required.

Mercury: 1. All ICB and CCBs were free of contamination. No qualifications were required. 2. Method Blank-Water (Dissolved) (BJ89633BLK) digested on 9/14/2015 was free of

contamination. No qualifications were required. 3. Method Blank-Water (Total) (BJ89651BLK) digested on 9/11/2015 was free of

contamination. No qualifications were required. Field Blank (FB) and Equipment Blank (EB): 1. Field Blanks were not submitted with this SDG.


Laboratory Control Sample (LCS)/ Laboratory Control Sample Duplicate (LCSD): ICP-AES, GFAA and CVAA: 1. Laboratory Control Sample was analyzed on 9/10/2015. All %RECs were within the

laboratory control limits. No qualifications were required. Field Duplicate: 1. A field duplicate pair was not submitted with this SDG. Matrix Spike (MS)/ Matrix Spike Duplicate (MSD): ICP-AES, GFAA and CVAA: 1. Matrix Spike (MS) was performed on sample 14MW3 (BJ90193) for dissolved metals.

All %Rs were within the laboratory control limits. No qualifications were required. 2. Matrix Spike (MS) was performed on sample 14MW4 (BJ90194) for dissolved metals.

All %Rs were within the laboratory control limits. No qualifications were required. 3. Matrix Spike (MS) was performed on sample 14MW1 (BJ90192) for total metals. All

%Rs were within the laboratory control limits. No qualifications were required. 4. Matrix Spike (MS) was performed on sample 14MW4 (BJ90194) for total metals. All

%Rs were within the laboratory control limits. No qualifications were required. Sample Duplicate: ICP-AES, GFAA and CVAA: 1. Laboratory Duplicate was performed on sample 14 MW 4 (BJ90194) for GFAA. All

RPDs were within the laboratory control limits. No qualifications were required. 2. Laboratory Duplicate was performed on sample 14 MW 3 (BJ90193) for ICP-AES. All

RPDs were within the laboratory control limits. No qualifications were required. 3. Laboratory Duplicate was performed on sample 14 MW 1 (BJ90192) for GFAA. All

RPDs were within the laboratory control limits. No qualifications were required.


4. Laboratory Duplicate was performed on sample 14 MW 4 (BJ90194) for ICP-AES. All RPDs were within the laboratory control limits. No qualifications were required.

ICP-AES Serial Dilution: 1. ICP serial dilution was performed on sample 14 MW 3 (BJ90193) (Dissolved). For all

results for which the concentration in the original sample is ≥ 50x the Method Detection Limits (MDL), the serial dilution analysis (a five-fold dilution) was within the acceptable limit (%D 10%) with the following exception(s):

Element %D Sample

Affected Action

Potassium (Dissolved) 12.2 14MW3 J+ 2. ICP serial dilution was performed on sample 14 MW 4 (BJ90194) (Total). For all results

for which the concentration in the original sample is ≥ 50x the Method Detection Limits (MDL), the serial dilution analysis (a five-fold dilution) was within the acceptable limit (%D 10%) with the following exception(s):

Element %D Sample

Affected Action

Aluminum (Total) 60.6 14MW4 J Calcium (Total) 12.4 14MW4 J

Iron (Total) 12.4 14MW4 J Magnesium (Total) 12.3 14MW4 J Verification of Instrumental Parameters: 1. The following Forms were present in the data package:


Compound Quantitation and Reported Detection Limits: 1. All sample results were reported within the linear calibration range.


2. Manual calculation: Sample: 14 MW 1 (BJ90192) Arsenic DF: 1 0.0101 mg/L was reported on the raw data and the laboratory reported 0.010 mg/L on

Form-I. Comments: 1. Trace Metals data package meet requirement for New York State Department of





SDG: GBJ90192


14MW1 BJ90192 7010 9/14/2015 1 Antimony mg/L U 0.00214MW1 BJ90192 7010 9/14/2015 1 Antimony, (Dissolved) mg/L U 0.00314MW1 BJ90192 7010 9/11/2015 1 Selenium mg/L U 0.00214MW1 BJ90192 7010 9/16/2015 1 Selenium, (Dissolved) mg/L U 0.00414MW1 BJ90192 7010 9/15/2015 1 Thallium - LDL mg/L U 0.00114MW1 BJ90192 7010 9/15/2015 1 Thallium , (Dissolved) mg/L U 0.00114MW1 BJ90192 SW6010 9/11/2015 10 Sodium 110 mg/L 1.014MW1 BJ90192 SW6010 9/12/2015 1 Aluminum 0.048 mg/L 0.01014MW1 BJ90192 SW6010 9/12/2015 1 Iron 2.38 mg/L 0.0114MW1 BJ90192 SW6010 9/12/2015 1 Lead 0.002 mg/L J 0.00214MW1 BJ90192 SW6010 9/12/2015 1 Magnesium 18.8 mg/L 0.0114MW1 BJ90192 SW6010 9/12/2015 1 Manganese 0.380 mg/L 0.00514MW1 BJ90192 SW6010 9/12/2015 1 Nickel 0.002 mg/L J 0.00414MW1 BJ90192 SW6010 9/12/2015 1 Potassium 10.9 mg/L J+ 0.114MW1 BJ90192 SW6010 9/12/2015 1 Silver mg/L U 0.00514MW1 BJ90192 SW6010 9/12/2015 1 Arsenic - LDL 0.010 mg/L 0.00414MW1 BJ90192 SW6010 9/12/2015 1 Barium 0.087 mg/L 0.01014MW1 BJ90192 SW6010 9/12/2015 1 Beryllium mg/L U 0.00114MW1 BJ90192 SW6010 9/12/2015 1 Cadmium mg/L U 0.00414MW1 BJ90192 SW6010 9/12/2015 1 Chromium 0.004 mg/L 0.00114MW1 BJ90192 SW6010 9/12/2015 1 Cobalt mg/L U 0.00514MW1 BJ90192 SW6010 9/12/2015 1 Copper mg/L U 0.00514MW1 BJ90192 SW6010 9/12/2015 1 Vanadium mg/L U 0.01014MW1 BJ90192 SW6010 9/12/2015 1 Zinc mg/L U 0.01014MW1 BJ90192 SW6010 9/12/2015 1 Zinc mg/L U 0.01014MW1 BJ90192 SW6010 9/12/2015 1 Calcium 80.3 mg/L 0.01014MW1 BJ90192 SW6010 9/15/2015 10 Sodium (Dissolved) 103 mg/L 1.114MW1 BJ90192 SW6010 9/15/2015 1 Aluminum (Dissolved) mg/L U 0.01114MW1 BJ90192 SW6010 9/15/2015 1 Iron, (Dissolved) 0.04 mg/L 0.0114MW1 BJ90192 SW6010 9/15/2015 1 Lead (Dissolved) 0.003 mg/L U 0.00214MW1 BJ90192 SW6010 9/15/2015 1 Magnesium (Dissolved) 16.8 mg/L 0.0114MW1 BJ90192 SW6010 9/15/2015 1 Manganese, (Dissolved) 0.349 mg/L 0.00514MW1 BJ90192 SW6010 9/15/2015 1 Nickel, (Dissolved) mg/L U 0.00414MW1 BJ90192 SW6010 9/15/2015 1 Potassium (Dissolved) 10.7 mg/L J+ 0.114MW1 BJ90192 SW6010 9/15/2015 1 Silver (Dissolved) mg/L U 0.00514MW1 BJ90192 SW6010 9/15/2015 1 Arsenic, (Dissolved) 0.004 mg/L 0.00314MW1 BJ90192 SW6010 9/15/2015 1 Barium (Dissolved) 0.070 mg/L 0.01114MW1 BJ90192 SW6010 9/15/2015 1 Beryllium (Dissolved) mg/L U 0.00114MW1 BJ90192 SW6010 9/15/2015 1 Cadmium (Dissolved) mg/L U 0.00414MW1 BJ90192 SW6010 9/15/2015 1 Chromium (Dissolved) 0.001 mg/L 0.00114MW1 BJ90192 SW6010 9/15/2015 1 Cobalt, (Dissolved) mg/L U 0.005

Page 1 of 17



SDG: GBJ90192


14MW1 BJ90192 SW6010 9/15/2015 1 Copper, (Dissolved) mg/L U 0.00514MW1 BJ90192 SW6010 9/15/2015 1 Vanadium, (Dissolved) mg/L U 0.01114MW1 BJ90192 SW6010 9/15/2015 1 Zinc, (Dissolved) mg/L U 0.01114MW1 BJ90192 SW6010 9/15/2015 1 Calcium (Dissolved) 72.4 mg/L 0.0114MW1 BJ90192 SW7470 9/11/2015 1 Mercury mg/L U 0.000214MW1 BJ90192 SW7470 9/14/2015 1 Mercury (Dissolved) 0.0002 mg/L 0.000214MW1 BJ90192 SW8081 9/16/2015 1 Heptachlor epoxide ug/L U 0.01014MW1 BJ90192 SW8081 9/16/2015 1 Endosulfan Sulfate ug/L U 0.01014MW1 BJ90192 SW8081 9/16/2015 1 Alachlor ug/L U 0.07514MW1 BJ90192 SW8081 9/16/2015 1 Aldrin ug/L U 0.00314MW1 BJ90192 SW8081 9/16/2015 1 a-BHC ug/L U 0.00514MW1 BJ90192 SW8081 9/16/2015 1 b-BHC ug/L U 0.01514MW1 BJ90192 SW8081 9/16/2015 1 d-BHC ug/L U 0.00514MW1 BJ90192 SW8081 9/16/2015 1 Endosulfan II ug/L U 0.01014MW1 BJ90192 SW8081 9/16/2015 1 4,4' -DDT ug/L U 0.01014MW1 BJ90192 SW8081 9/16/2015 1 a-chlordane ug/L U 0.01014MW1 BJ90192 SW8081 9/16/2015 1 g-chlordane ug/L U 0.01014MW1 BJ90192 SW8081 9/16/2015 1 Endrin ketone ug/L U 0.01014MW1 BJ90192 SW8081 9/16/2015 1 Chlordane ug/L U 0.1014MW1 BJ90192 SW8081 9/16/2015 1 g-BHC (Lindane) ug/L U 0.01614MW1 BJ90192 SW8081 9/16/2015 1 Dieldrin ug/L U 0.01514MW1 BJ90192 SW8081 9/16/2015 1 Endrin ug/L U 0.01014MW1 BJ90192 SW8081 9/16/2015 1 Methoxychlor ug/L U 0.1014MW1 BJ90192 SW8081 9/16/2015 1 4 4' -DDD ug/L U 0 01014MW1 BJ90192 SW8081 9/16/2015 1 4,4 DDD ug/L U 0.01014MW1 BJ90192 SW8081 9/16/2015 1 4,4' -DDE ug/L U 0.01014MW1 BJ90192 SW8081 9/16/2015 1 Endrin Aldehyde ug/L U 0.01014MW1 BJ90192 SW8081 9/16/2015 1 Heptachlor ug/L U 0.01014MW1 BJ90192 SW8081 9/16/2015 1 Toxaphene ug/L U 0.2514MW1 BJ90192 SW8081 9/16/2015 1 Endosulfan I ug/L UJ 0.08014MW1 BJ90192 SW8082 9/11/2015 1 PCB-1260 ug/L U 0.05014MW1 BJ90192 SW8082 9/11/2015 1 PCB-1254 ug/L U 0.05014MW1 BJ90192 SW8082 9/11/2015 1 PCB-1268 ug/L U 0.05014MW1 BJ90192 SW8082 9/11/2015 1 PCB-1221 ug/L U 0.05014MW1 BJ90192 SW8082 9/11/2015 1 PCB-1232 ug/L U 0.05014MW1 BJ90192 SW8082 9/11/2015 1 PCB-1248 ug/L U 0.05014MW1 BJ90192 SW8082 9/11/2015 1 PCB-1016 ug/L U 0.05014MW1 BJ90192 SW8082 9/11/2015 1 PCB-1262 ug/L U 0.05014MW1 BJ90192 SW8082 9/11/2015 1 PCB-1242 ug/L U 0.05014MW1 BJ90192 SW8260 9/14/2015 1 Ethylbenzene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 Styrene ug/L U 1.0

Page 2 of 17



SDG: GBJ90192


14MW1 BJ90192 SW8260 9/14/2015 1 cis-1,3-Dichloropropene ug/L U 0.4014MW1 BJ90192 SW8260 9/14/2015 1 trans-1,3-Dichloropropene ug/L U 0.4014MW1 BJ90192 SW8260 9/14/2015 1 n-Propylbenzene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 n-Butylbenzene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 4-Chlorotoluene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 1,4-Dichlorobenzene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 1,2-Dibromoethane ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 Acrolein ug/L U 5.014MW1 BJ90192 SW8260 9/14/2015 1 1,2-Dichloroethane ug/L U 0.6014MW1 BJ90192 SW8260 9/14/2015 1 Acrylonitrile ug/L U 5.014MW1 BJ90192 SW8260 9/14/2015 1 4-Methyl-2-pentanone ug/L U 2.514MW1 BJ90192 SW8260 9/14/2015 1 1,3,5-Trimethylbenzene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 Bromobenzene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 Toluene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 Chlorobenzene ug/L U 5.014MW1 BJ90192 SW8260 9/14/2015 1 Tetrahydrofuran (THF) ug/L U 5.014MW1 BJ90192 SW8260 9/14/2015 1 trans-1,4-dichloro-2-butene ug/L UJ 2.514MW1 BJ90192 SW8260 9/14/2015 1 1,2,4-Trichlorobenzene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 Dibromochloromethane ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 Tetrachloroethene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 sec-Butylbenzene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 1,3-Dichloropropane ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 trans-1,2-Dichloroethene 6.3 ug/L 5.014MW1 BJ90192 SW8260 9/14/2015 1 Methyl t-butyl ether (MTBE) ug/L U 1 014MW1 BJ90192 SW8260 9/14/2015 1 Methyl t butyl ether (MTBE) ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 m&p-Xylene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 2-Isopropyltoluene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 1,3-Dichlorobenzene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 Carbon tetrachloride ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 1,1-Dichloropropene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 2-Hexanone ug/L U 2.514MW1 BJ90192 SW8260 9/14/2015 1 2,2-Dichloropropane ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 1,1,1,2-Tetrachloroethane ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 Acetone 6.8 ug/L 5.014MW1 BJ90192 SW8260 9/14/2015 1 Chloroform ug/L U 5.014MW1 BJ90192 SW8260 9/14/2015 1 Benzene 18 ug/L 0.7014MW1 BJ90192 SW8260 9/14/2015 1 1,1,1-Trichloroethane ug/L U 5.014MW1 BJ90192 SW8260 9/14/2015 1 Bromomethane ug/L UJ 5.014MW1 BJ90192 SW8260 9/14/2015 1 Chloromethane 0.74 ug/L J 5.014MW1 BJ90192 SW8260 9/14/2015 1 Dibromomethane ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 Bromochloromethane ug/L U 1.0

Page 3 of 17



SDG: GBJ90192


14MW1 BJ90192 SW8260 9/14/2015 1 Chloroethane ug/L U 5.014MW1 BJ90192 SW8260 9/14/2015 1 Methylene chloride ug/L U 3.014MW1 BJ90192 SW8260 9/14/2015 1 Carbon Disulfide ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 Bromoform ug/L UJ 5.014MW1 BJ90192 SW8260 9/14/2015 1 Bromodichloromethane ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 1,1-Dichloroethane 0.67 ug/L J 5.014MW1 BJ90192 SW8260 9/14/2015 1 1,1-Dichloroethene 0.29 ug/L J 1.014MW1 BJ90192 SW8260 9/14/2015 1 Trichlorofluoromethane ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 Dichlorodifluoromethane ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 Trichlorotrifluoroethane ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 1,2-Dichloropropane ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 Methyl ethyl ketone ug/L U 2.514MW1 BJ90192 SW8260 9/14/2015 1 1,1,2-Trichloroethane ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 Trichloroethene 6.3 ug/L 1.014MW1 BJ90192 SW8260 9/14/2015 1 1,1,2,2-Tetrachloroethane ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 1,2,3-Trichlorobenzene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 Hexachlorobutadiene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 Naphthalene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 o-Xylene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 2-Chlorotoluene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 1,2-Dichlorobenzene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 1,2,4-Trimethylbenzene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 1,2-Dibromo-3-chloropropane ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 1 2 3-Trichloropropane ug/L U 1 014MW1 BJ90192 SW8260 9/14/2015 1 1,2,3 Trichloropropane ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 tert-Butylbenzene ug/L U 1.014MW1 BJ90192 SW8260 9/14/2015 1 Isopropylbenzene 0.26 ug/L J 1.014MW1 BJ90192 SW8260 9/14/2015 1 p-Isopropyltoluene ug/L U 1.014MW1 BJ90192 SW8260 9/15/2015 5 cis-1,2-Dichloroethene 70 ug/L 5.014MW1 BJ90192 SW8260 9/15/2015 5 Vinyl chloride 36 ug/L 5.014MW1 BJ90192 SW8270 9/15/2015 1 4-Nitroaniline ug/L U 2014MW1 BJ90192 SW8270 9/15/2015 1 Benzyl Alcohol ug/L UJ 5.014MW1 BJ90192 SW8270 9/15/2015 1 4-Bromophenyl phenyl ether ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 1,4-Dichlorobenzene ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 4-Chloroaniline ug/L U 2014MW1 BJ90192 SW8270 9/15/2015 1 Bis(2-chloroethyl)ether ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 Bis(2-chloroethoxy)methane ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 Di-n-octylphthalate ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 1,2,4-Trichlorobenzene ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 2,4-Dinitrotoluene ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 1,2-Diphenylhydrazine ug/L U 5.0

Page 4 of 17



SDG: GBJ90192


14MW1 BJ90192 SW8270 9/15/2015 1 Dimethylphthalate ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 Dibenzofuran 4.1 ug/L J 5.014MW1 BJ90192 SW8270 9/15/2015 1 Bis(2-chloroisopropyl)ether ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 1,3-Dichlorobenzene ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 2,6-Dinitrotoluene ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 N-Nitrosodi-n-propylamine ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 Benzoic acid ug/L U 2014MW1 BJ90192 SW8270 9/15/2015 1 4-Chlorophenyl phenyl ether ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 Hexachlorocyclopentadiene ug/L UJ 5.014MW1 BJ90192 SW8270 9/15/2015 1 Isophorone ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 Diethyl phthalate ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 Di-n-butylphthalate ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 Benzyl butyl phthalate ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 N-Nitrosodiphenylamine ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 2-Nitroaniline ug/L U 2014MW1 BJ90192 SW8270 9/15/2015 1 2-Chloronaphthalene ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 3,3'-Dichlorobenzidine ug/L U 2014MW1 BJ90192 SW8270 9/15/2015 1 Benzidine ug/L U 1814MW1 BJ90192 SW8270 9/15/2015 1 1,2-Dichlorobenzene ug/L U 5.014MW1 BJ90192 SW8270 9/15/2015 1 3-Nitroaniline ug/L U 2014MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Bis(2-ethylhexyl)phthalate 0.11 ug/L U 0.0514MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Hexachlorobenzene ug/L U 0.0214MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Anthracene 0.65 ug/L 0.0514MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Pyrene 0 27 ug/L 0 0514MW1 BJ90192 SW8270C SIM 9/14/2015 1 Pyrene 0.27 ug/L 0.0514MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Benzo(ghi)perylene ug/L U 0.0514MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Indeno(1,2,3-cd)pyrene ug/L U 0.0514MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Benzo(b)fluoranthene ug/L U 0.0514MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Fluoranthene 0.35 ug/L 0.0514MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Benzo(k)fluoranthene ug/L U 0.0514MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Acenaphthylene 1.8 ug/L 0.0514MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Chrysene ug/L U 0.0514MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Benzo(a)pyrene ug/L U 0.0214MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Dibenz(a,h)anthracene ug/L U 0.0514MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Benz(a)anthracene 0.06 ug/L 0.0514MW1 BJ90192 SW8270C-SIM 9/14/2015 1 N-Nitrosodimethylamine ug/L U 0.0514MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Hexachloroethane ug/L U 0.0514MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Acenaphthene 6.0 ug/L 0.0514MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Phenanthrene 0.13 ug/L 0.0514MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Fluorene 1.5 ug/L 0.0514MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Hexachlorobutadiene ug/L U 0.05

Page 5 of 17



SDG: GBJ90192


14MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Naphthalene ug/L U 0.0514MW1 BJ90192 SW8270C-SIM 9/14/2015 1 2-Methylnaphthalene ug/L U 0.0514MW1 BJ90192 SW8270C-SIM 9/14/2015 1 Nitrobenzene ug/L U 0.0514MW3 BJ90193 7010 9/14/2015 1 Antimony mg/L U 0.00214MW3 BJ90193 7010 9/14/2015 1 Antimony, (Dissolved) mg/L U 0.00314MW3 BJ90193 7010 9/11/2015 1 Selenium mg/L U 0.00214MW3 BJ90193 7010 9/16/2015 1 Selenium, (Dissolved) mg/L U 0.00414MW3 BJ90193 7010 9/15/2015 1 Thallium - LDL mg/L U 0.00114MW3 BJ90193 7010 9/15/2015 1 Thallium , (Dissolved) mg/L U 0.00114MW3 BJ90193 SW6010 9/11/2015 10 Sodium 84.1 mg/L 1.014MW3 BJ90193 SW6010 9/12/2015 1 Aluminum 1.50 mg/L 0.01014MW3 BJ90193 SW6010 9/12/2015 1 Iron 2.40 mg/L 0.0114MW3 BJ90193 SW6010 9/12/2015 1 Lead 0.012 mg/L 0.00214MW3 BJ90193 SW6010 9/12/2015 1 Magnesium 22.0 mg/L 0.0114MW3 BJ90193 SW6010 9/12/2015 1 Manganese 0.285 mg/L 0.00514MW3 BJ90193 SW6010 9/12/2015 1 Nickel 0.003 mg/L J 0.00414MW3 BJ90193 SW6010 9/12/2015 1 Potassium 11.1 mg/L J+ 0.114MW3 BJ90193 SW6010 9/12/2015 1 Silver mg/L U 0.00514MW3 BJ90193 SW6010 9/12/2015 1 Arsenic - LDL 0.005 mg/L 0.00414MW3 BJ90193 SW6010 9/12/2015 1 Barium 0.084 mg/L 0.01014MW3 BJ90193 SW6010 9/12/2015 1 Beryllium mg/L U 0.00114MW3 BJ90193 SW6010 9/12/2015 1 Cadmium mg/L U 0.00414MW3 BJ90193 SW6010 9/12/2015 1 Chromium 0.003 mg/L 0.00114MW3 BJ90193 SW6010 9/12/2015 1 Cobalt mg/L U 0 00514MW3 BJ90193 SW6010 9/12/2015 1 Cobalt mg/L U 0.00514MW3 BJ90193 SW6010 9/12/2015 1 Copper 0.003 mg/L J 0.00514MW3 BJ90193 SW6010 9/12/2015 1 Vanadium 0.003 mg/L J 0.01014MW3 BJ90193 SW6010 9/12/2015 1 Zinc 0.006 mg/L J 0.01014MW3 BJ90193 SW6010 9/12/2015 1 Calcium 65.0 mg/L 0.01014MW3 BJ90193 SW6010 9/15/2015 10 Sodium (Dissolved) 76.5 mg/L 1.114MW3 BJ90193 SW6010 9/15/2015 1 Aluminum (Dissolved) 0.007 mg/L J 0.01114MW3 BJ90193 SW6010 9/15/2015 1 Iron, (Dissolved) 0.05 mg/L 0.0114MW3 BJ90193 SW6010 9/15/2015 1 Lead (Dissolved) 0.002 mg/L 0.00214MW3 BJ90193 SW6010 9/15/2015 1 Magnesium (Dissolved) 19.0 mg/L 0.0114MW3 BJ90193 SW6010 9/15/2015 1 Manganese, (Dissolved) 0.230 mg/L 0.00514MW3 BJ90193 SW6010 9/15/2015 1 Nickel, (Dissolved) mg/L U 0.00414MW3 BJ90193 SW6010 9/15/2015 1 Potassium (Dissolved) 11.5 mg/L J+ 0.114MW3 BJ90193 SW6010 9/15/2015 1 Silver (Dissolved) mg/L U 0.00514MW3 BJ90193 SW6010 9/15/2015 1 Arsenic, (Dissolved) mg/L U 0.00314MW3 BJ90193 SW6010 9/15/2015 1 Barium (Dissolved) 0.064 mg/L 0.01114MW3 BJ90193 SW6010 9/15/2015 1 Beryllium (Dissolved) mg/L U 0.001

Page 6 of 17



SDG: GBJ90192


14MW3 BJ90193 SW6010 9/15/2015 1 Cadmium (Dissolved) mg/L U 0.00414MW3 BJ90193 SW6010 9/15/2015 1 Chromium (Dissolved) mg/L U 0.00114MW3 BJ90193 SW6010 9/15/2015 1 Cobalt, (Dissolved) mg/L U 0.00514MW3 BJ90193 SW6010 9/15/2015 1 Copper, (Dissolved) mg/L U 0.00514MW3 BJ90193 SW6010 9/15/2015 1 Vanadium, (Dissolved) mg/L U 0.01114MW3 BJ90193 SW6010 9/15/2015 1 Zinc, (Dissolved) mg/L U 0.01114MW3 BJ90193 SW6010 9/15/2015 1 Calcium (Dissolved) 56.0 mg/L 0.0114MW3 BJ90193 SW7470 9/11/2015 1 Mercury mg/L U 0.000214MW3 BJ90193 SW7470 9/14/2015 1 Mercury (Dissolved) mg/L U 0.000214MW3 BJ90193 SW8081 9/16/2015 1 Heptachlor epoxide ug/L U 0.01014MW3 BJ90193 SW8081 9/16/2015 1 Endosulfan Sulfate ug/L U 0.01014MW3 BJ90193 SW8081 9/16/2015 1 Alachlor ug/L U 0.07514MW3 BJ90193 SW8081 9/16/2015 1 Aldrin ug/L U 0.00514MW3 BJ90193 SW8081 9/16/2015 1 a-BHC ug/L U 0.00514MW3 BJ90193 SW8081 9/16/2015 1 b-BHC ug/L U 0.01514MW3 BJ90193 SW8081 9/16/2015 1 d-BHC ug/L U 0.02014MW3 BJ90193 SW8081 9/16/2015 1 Endosulfan II ug/L U 0.01014MW3 BJ90193 SW8081 9/16/2015 1 4,4' -DDT ug/L U 0.01514MW3 BJ90193 SW8081 9/16/2015 1 a-chlordane ug/L U 0.01014MW3 BJ90193 SW8081 9/16/2015 1 g-chlordane ug/L U 0.01514MW3 BJ90193 SW8081 9/16/2015 1 Endrin ketone ug/L U 0.01014MW3 BJ90193 SW8081 9/16/2015 1 Chlordane ug/L U 0.1014MW3 BJ90193 SW8081 9/16/2015 1 g-BHC (Lindane) ug/L U 0.00514MW3 BJ90193 SW8081 9/16/2015 1 Dieldrin ug/L U 0 01514MW3 BJ90193 SW8081 9/16/2015 1 Dieldrin ug/L U 0.01514MW3 BJ90193 SW8081 9/16/2015 1 Endrin ug/L U 0.01014MW3 BJ90193 SW8081 9/16/2015 1 Methoxychlor ug/L U 0.1014MW3 BJ90193 SW8081 9/16/2015 1 4,4' -DDD ug/L U 0.01014MW3 BJ90193 SW8081 9/16/2015 1 4,4' -DDE ug/L U 0.01014MW3 BJ90193 SW8081 9/16/2015 1 Endrin Aldehyde ug/L U 0.01014MW3 BJ90193 SW8081 9/16/2015 1 Heptachlor ug/L U 0.06014MW3 BJ90193 SW8081 9/16/2015 1 Toxaphene ug/L U 0.2514MW3 BJ90193 SW8081 9/16/2015 1 Endosulfan I ug/L UJ 0.01514MW3 BJ90193 SW8082 9/11/2015 1 PCB-1260 ug/L U 0.05014MW3 BJ90193 SW8082 9/11/2015 1 PCB-1254 ug/L U 0.05014MW3 BJ90193 SW8082 9/11/2015 1 PCB-1268 ug/L U 0.05014MW3 BJ90193 SW8082 9/11/2015 1 PCB-1221 ug/L U 0.05014MW3 BJ90193 SW8082 9/11/2015 1 PCB-1232 ug/L U 0.05014MW3 BJ90193 SW8082 9/11/2015 1 PCB-1248 ug/L U 0.05014MW3 BJ90193 SW8082 9/11/2015 1 PCB-1016 ug/L U 0.05014MW3 BJ90193 SW8082 9/11/2015 1 PCB-1262 ug/L U 0.050

Page 7 of 17



SDG: GBJ90192


14MW3 BJ90193 SW8082 9/11/2015 1 PCB-1242 ug/L U 0.05014MW3 BJ90193 SW8260 9/12/2015 1 Ethylbenzene 0.66 ug/L J 1.014MW3 BJ90193 SW8260 9/12/2015 1 Styrene ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 cis-1,3-Dichloropropene ug/L U 0.4014MW3 BJ90193 SW8260 9/12/2015 1 trans-1,3-Dichloropropene ug/L U 0.4014MW3 BJ90193 SW8260 9/12/2015 1 n-Propylbenzene ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 n-Butylbenzene ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 4-Chlorotoluene ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 1,4-Dichlorobenzene ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 1,2-Dibromoethane ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 Acrolein ug/L U 5.014MW3 BJ90193 SW8260 9/12/2015 1 1,2-Dichloroethane ug/L U 0.6014MW3 BJ90193 SW8260 9/12/2015 1 Acrylonitrile ug/L UJ 5.014MW3 BJ90193 SW8260 9/12/2015 1 4-Methyl-2-pentanone ug/L U 2.514MW3 BJ90193 SW8260 9/12/2015 1 1,3,5-Trimethylbenzene ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 Bromobenzene ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 Toluene 1.5 ug/L 1.014MW3 BJ90193 SW8260 9/12/2015 1 Chlorobenzene ug/L U 5.014MW3 BJ90193 SW8260 9/12/2015 1 Tetrahydrofuran (THF) ug/L UJ 5.014MW3 BJ90193 SW8260 9/12/2015 1 trans-1,4-dichloro-2-butene ug/L U 2.514MW3 BJ90193 SW8260 9/12/2015 1 1,2,4-Trichlorobenzene ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 Dibromochloromethane ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 Tetrachloroethene ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 sec-Butylbenzene ug/L U 1 014MW3 BJ90193 SW8260 9/12/2015 1 sec Butylbenzene ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 1,3-Dichloropropane ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 trans-1,2-Dichloroethene 12 ug/L 5.014MW3 BJ90193 SW8260 9/12/2015 1 Methyl t-butyl ether (MTBE) ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 m&p-Xylene 0.63 ug/L J 1.014MW3 BJ90193 SW8260 9/12/2015 1 2-Isopropyltoluene ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 1,3-Dichlorobenzene ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 Carbon tetrachloride ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 1,1-Dichloropropene ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 2-Hexanone ug/L U 2.514MW3 BJ90193 SW8260 9/12/2015 1 2,2-Dichloropropane ug/L UJ 1.014MW3 BJ90193 SW8260 9/12/2015 1 1,1,1,2-Tetrachloroethane ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 Acetone 3.4 ug/L J 5.014MW3 BJ90193 SW8260 9/12/2015 1 Chloroform ug/L U 5.014MW3 BJ90193 SW8260 9/12/2015 1 Benzene 23 ug/L 0.7014MW3 BJ90193 SW8260 9/12/2015 1 1,1,1-Trichloroethane ug/L U 5.014MW3 BJ90193 SW8260 9/12/2015 1 Bromomethane ug/L UJ 5.0

Page 8 of 17



SDG: GBJ90192


14MW3 BJ90193 SW8260 9/12/2015 1 Chloromethane ug/L U 5.014MW3 BJ90193 SW8260 9/12/2015 1 Dibromomethane ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 Bromochloromethane ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 Chloroethane ug/L U 5.014MW3 BJ90193 SW8260 9/12/2015 1 Methylene chloride ug/L U 3.014MW3 BJ90193 SW8260 9/12/2015 1 Carbon Disulfide ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 Bromoform ug/L U 5.014MW3 BJ90193 SW8260 9/12/2015 1 Bromodichloromethane ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 1,1-Dichloroethane 0.85 ug/L J 5.014MW3 BJ90193 SW8260 9/12/2015 1 1,1-Dichloroethene 5.8 ug/L 1.014MW3 BJ90193 SW8260 9/12/2015 1 Trichlorofluoromethane ug/L UJ 1.014MW3 BJ90193 SW8260 9/12/2015 1 Dichlorodifluoromethane ug/L UJ 1.014MW3 BJ90193 SW8260 9/12/2015 1 Trichlorotrifluoroethane ug/L UJ 1.014MW3 BJ90193 SW8260 9/12/2015 1 1,2-Dichloropropane ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 Methyl ethyl ketone ug/L U 2.514MW3 BJ90193 SW8260 9/12/2015 1 1,1,2-Trichloroethane ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 Trichloroethene 12 ug/L 1.014MW3 BJ90193 SW8260 9/12/2015 1 1,1,2,2-Tetrachloroethane ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 1,2,3-Trichlorobenzene ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 Hexachlorobutadiene ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 Naphthalene 3.4 ug/L 1.014MW3 BJ90193 SW8260 9/12/2015 1 o-Xylene 0.67 ug/L J 1.014MW3 BJ90193 SW8260 9/12/2015 1 2-Chlorotoluene ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 1 2-Dichlorobenzene ug/L U 1 014MW3 BJ90193 SW8260 9/12/2015 1 1,2 Dichlorobenzene ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 1,2,4-Trimethylbenzene ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 1,2-Dibromo-3-chloropropane ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 1,2,3-Trichloropropane ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 tert-Butylbenzene ug/L U 1.014MW3 BJ90193 SW8260 9/12/2015 1 Isopropylbenzene 0.35 ug/L J 1.014MW3 BJ90193 SW8260 9/12/2015 1 p-Isopropyltoluene ug/L U 1.014MW3 BJ90193 SW8260 9/14/2015 100 cis-1,2-Dichloroethene 1200 ug/L 10014MW3 BJ90193 SW8260 9/14/2015 100 Vinyl chloride 470 ug/L 10014MW3 BJ90193 SW8270 9/15/2015 1 4-Nitroaniline ug/L U 2014MW3 BJ90193 SW8270 9/15/2015 1 Benzyl Alcohol ug/L UJ 5.014MW3 BJ90193 SW8270 9/15/2015 1 4-Bromophenyl phenyl ether ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 1,4-Dichlorobenzene ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 4-Chloroaniline ug/L U 2014MW3 BJ90193 SW8270 9/15/2015 1 Bis(2-chloroethyl)ether ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 Bis(2-chloroethoxy)methane ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 Di-n-octylphthalate ug/L U 5.0

Page 9 of 17



SDG: GBJ90192


14MW3 BJ90193 SW8270 9/15/2015 1 1,2,4-Trichlorobenzene ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 2,4-Dinitrotoluene ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 1,2-Diphenylhydrazine ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 Dimethylphthalate ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 Dibenzofuran 7.6 ug/L 5.014MW3 BJ90193 SW8270 9/15/2015 1 Bis(2-chloroisopropyl)ether ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 1,3-Dichlorobenzene ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 2,6-Dinitrotoluene ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 N-Nitrosodi-n-propylamine ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 Benzoic acid ug/L U 2014MW3 BJ90193 SW8270 9/15/2015 1 4-Chlorophenyl phenyl ether ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 Hexachlorocyclopentadiene ug/L UJ 5.014MW3 BJ90193 SW8270 9/15/2015 1 Isophorone ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 Diethyl phthalate ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 Di-n-butylphthalate ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 Benzyl butyl phthalate ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 N-Nitrosodiphenylamine ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 2-Nitroaniline ug/L U 2014MW3 BJ90193 SW8270 9/15/2015 1 2-Chloronaphthalene ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 3,3'-Dichlorobenzidine ug/L U 2014MW3 BJ90193 SW8270 9/15/2015 1 Benzidine ug/L U 1814MW3 BJ90193 SW8270 9/15/2015 1 1,2-Dichlorobenzene ug/L U 5.014MW3 BJ90193 SW8270 9/15/2015 1 3-Nitroaniline ug/L U 2014MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Bis(2-ethylhexyl)phthalate 0 12 ug/L U 0 0514MW3 BJ90193 SW8270C SIM 9/14/2015 1 Bis(2 ethylhexyl)phthalate 0.12 ug/L U 0.0514MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Hexachlorobenzene ug/L U 0.0214MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Anthracene 2.3 ug/L 0.0514MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Pyrene 1.5 ug/L 0.0514MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Benzo(ghi)perylene 0.20 ug/L 0.0514MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Indeno(1,2,3-cd)pyrene 0.18 ug/L 0.0514MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Benzo(b)fluoranthene 0.20 ug/L 0.0514MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Fluoranthene 2.2 ug/L 0.0514MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Benzo(k)fluoranthene 0.27 ug/L 0.0514MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Acenaphthylene 4.3 ug/L 0.0514MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Chrysene 0.31 ug/L 0.0514MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Benzo(a)pyrene 0.29 ug/L 0.0214MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Dibenz(a,h)anthracene 0.07 ug/L 0.0514MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Benz(a)anthracene 0.35 ug/L 0.0514MW3 BJ90193 SW8270C-SIM 9/14/2015 1 N-Nitrosodimethylamine ug/L U 0.0514MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Hexachloroethane ug/L U 0.0514MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Acenaphthene 3.8 ug/L 0.05

Page 10 of 17



SDG: GBJ90192


14MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Phenanthrene 0.95 ug/L 0.0514MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Fluorene 1.3 ug/L 0.0514MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Hexachlorobutadiene ug/L U 0.0514MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Naphthalene 1.9 ug/L 0.0514MW3 BJ90193 SW8270C-SIM 9/14/2015 1 2-Methylnaphthalene 0.12 ug/L 0.0514MW3 BJ90193 SW8270C-SIM 9/14/2015 1 Nitrobenzene ug/L U 0.0514MW4 BJ90194 7010 9/14/2015 1 Antimony mg/L U 0.00214MW4 BJ90194 7010 9/14/2015 1 Antimony, (Dissolved) mg/L U 0.00314MW4 BJ90194 7010 9/11/2015 1 Selenium mg/L U 0.00214MW4 BJ90194 7010 9/16/2015 1 Selenium, (Dissolved) mg/L U 0.00414MW4 BJ90194 7010 9/15/2015 1 Thallium - LDL mg/L U 0.00114MW4 BJ90194 7010 9/15/2015 1 Thallium , (Dissolved) mg/L U 0.00114MW4 BJ90194 SW6010 9/11/2015 10 Sodium 58.7 mg/L 1.014MW4 BJ90194 SW6010 9/12/2015 1 Aluminum 0.492 mg/L J 0.01014MW4 BJ90194 SW6010 9/12/2015 1 Iron 0.40 mg/L J 0.0114MW4 BJ90194 SW6010 9/12/2015 1 Lead 0.004 mg/L 0.00214MW4 BJ90194 SW6010 9/12/2015 1 Magnesium 6.05 mg/L J 0.0114MW4 BJ90194 SW6010 9/12/2015 1 Manganese 0.152 mg/L 0.00514MW4 BJ90194 SW6010 9/12/2015 1 Nickel 0.003 mg/L U 0.00414MW4 BJ90194 SW6010 9/12/2015 1 Potassium 6.1 mg/L J+ 0.114MW4 BJ90194 SW6010 9/12/2015 1 Silver mg/L U 0.00514MW4 BJ90194 SW6010 9/12/2015 1 Arsenic - LDL 0.003 mg/L J 0.00414MW4 BJ90194 SW6010 9/12/2015 1 Barium 0.021 mg/L 0.01014MW4 BJ90194 SW6010 9/12/2015 1 Beryllium mg/L U 0 00114MW4 BJ90194 SW6010 9/12/2015 1 Beryllium mg/L U 0.00114MW4 BJ90194 SW6010 9/12/2015 1 Cadmium mg/L U 0.00414MW4 BJ90194 SW6010 9/12/2015 1 Chromium mg/L U 0.00114MW4 BJ90194 SW6010 9/12/2015 1 Cobalt mg/L U 0.00514MW4 BJ90194 SW6010 9/12/2015 1 Copper 0.002 mg/L J 0.00514MW4 BJ90194 SW6010 9/12/2015 1 Vanadium 0.008 mg/L J 0.01014MW4 BJ90194 SW6010 9/12/2015 1 Zinc mg/L U 0.01014MW4 BJ90194 SW6010 9/12/2015 1 Calcium 28.0 mg/L J 0.01014MW4 BJ90194 SW6010 9/15/2015 10 Sodium (Dissolved) 55.4 mg/L 1.114MW4 BJ90194 SW6010 9/15/2015 1 Aluminum (Dissolved) 0.140 mg/L 0.01114MW4 BJ90194 SW6010 9/15/2015 1 Iron, (Dissolved) 0.02 mg/L 0.0114MW4 BJ90194 SW6010 9/15/2015 1 Lead (Dissolved) 0.001 mg/L U 0.00214MW4 BJ90194 SW6010 9/15/2015 1 Magnesium (Dissolved) 5.37 mg/L 0.0114MW4 BJ90194 SW6010 9/15/2015 1 Manganese, (Dissolved) 0.112 mg/L 0.00514MW4 BJ90194 SW6010 9/15/2015 1 Nickel, (Dissolved) mg/L U 0.00414MW4 BJ90194 SW6010 9/15/2015 1 Potassium (Dissolved) 6.0 mg/L J+ 0.114MW4 BJ90194 SW6010 9/15/2015 1 Silver (Dissolved) mg/L U 0.005

Page 11 of 17



SDG: GBJ90192


14MW4 BJ90194 SW6010 9/15/2015 1 Arsenic, (Dissolved) mg/L U 0.00314MW4 BJ90194 SW6010 9/15/2015 1 Barium (Dissolved) 0.016 mg/L 0.01114MW4 BJ90194 SW6010 9/15/2015 1 Beryllium (Dissolved) mg/L U 0.00114MW4 BJ90194 SW6010 9/15/2015 1 Cadmium (Dissolved) mg/L U 0.00414MW4 BJ90194 SW6010 9/15/2015 1 Chromium (Dissolved) mg/L U 0.00114MW4 BJ90194 SW6010 9/15/2015 1 Cobalt, (Dissolved) mg/L U 0.00514MW4 BJ90194 SW6010 9/15/2015 1 Copper, (Dissolved) mg/L U 0.00514MW4 BJ90194 SW6010 9/15/2015 1 Vanadium, (Dissolved) 0.005 mg/L J 0.01114MW4 BJ90194 SW6010 9/15/2015 1 Zinc, (Dissolved) mg/L U 0.01114MW4 BJ90194 SW6010 9/15/2015 1 Calcium (Dissolved) 25.4 mg/L 0.0114MW4 BJ90194 SW7470 9/11/2015 1 Mercury mg/L U 0.000214MW4 BJ90194 SW7470 9/14/2015 1 Mercury (Dissolved) mg/L U 0.000214MW4 BJ90194 SW8081 9/16/2015 1 Heptachlor epoxide ug/L U 0.01014MW4 BJ90194 SW8081 9/16/2015 1 Endosulfan Sulfate ug/L U 0.01514MW4 BJ90194 SW8081 9/16/2015 1 Alachlor ug/L U 0.07514MW4 BJ90194 SW8081 9/16/2015 1 Aldrin ug/L U 0.00214MW4 BJ90194 SW8081 9/16/2015 1 a-BHC ug/L U 0.00514MW4 BJ90194 SW8081 9/16/2015 1 b-BHC ug/L U 0.01514MW4 BJ90194 SW8081 9/16/2015 1 d-BHC ug/L U 0.00514MW4 BJ90194 SW8081 9/16/2015 1 Endosulfan II ug/L U 0.01014MW4 BJ90194 SW8081 9/16/2015 1 4,4' -DDT ug/L U 0.01014MW4 BJ90194 SW8081 9/16/2015 1 a-chlordane ug/L U 0.01014MW4 BJ90194 SW8081 9/16/2015 1 g-chlordane ug/L U 0.01514MW4 BJ90194 SW8081 9/16/2015 1 Endrin ketone ug/L U 0 01014MW4 BJ90194 SW8081 9/16/2015 1 Endrin ketone ug/L U 0.01014MW4 BJ90194 SW8081 9/16/2015 1 Chlordane ug/L U 0.1014MW4 BJ90194 SW8081 9/16/2015 1 g-BHC (Lindane) ug/L U 0.01014MW4 BJ90194 SW8081 9/16/2015 1 Dieldrin ug/L U 0.00814MW4 BJ90194 SW8081 9/16/2015 1 Endrin ug/L U 0.01014MW4 BJ90194 SW8081 9/16/2015 1 Methoxychlor ug/L U 0.1014MW4 BJ90194 SW8081 9/16/2015 1 4,4' -DDD ug/L U 0.02014MW4 BJ90194 SW8081 9/16/2015 1 4,4' -DDE ug/L U 0.01014MW4 BJ90194 SW8081 9/16/2015 1 Endrin Aldehyde ug/L U 0.01014MW4 BJ90194 SW8081 9/16/2015 1 Heptachlor ug/L U 0.01014MW4 BJ90194 SW8081 9/16/2015 1 Toxaphene ug/L U 0.2514MW4 BJ90194 SW8081 9/16/2015 1 Endosulfan I ug/L UJ 0.01514MW4 BJ90194 SW8082 9/11/2015 1 PCB-1260 ug/L U 0.05014MW4 BJ90194 SW8082 9/11/2015 1 PCB-1254 ug/L U 0.05014MW4 BJ90194 SW8082 9/11/2015 1 PCB-1268 ug/L U 0.05014MW4 BJ90194 SW8082 9/11/2015 1 PCB-1221 ug/L U 0.05014MW4 BJ90194 SW8082 9/11/2015 1 PCB-1232 ug/L U 0.050

Page 12 of 17



SDG: GBJ90192


14MW4 BJ90194 SW8082 9/11/2015 1 PCB-1248 ug/L U 0.05014MW4 BJ90194 SW8082 9/11/2015 1 PCB-1016 ug/L U 0.05014MW4 BJ90194 SW8082 9/11/2015 1 PCB-1262 ug/L U 0.05014MW4 BJ90194 SW8082 9/11/2015 1 PCB-1242 ug/L U 0.05014MW4 BJ90194 SW8260 9/12/2015 1 Ethylbenzene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 Styrene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 cis-1,3-Dichloropropene ug/L U 0.4014MW4 BJ90194 SW8260 9/12/2015 1 trans-1,3-Dichloropropene ug/L U 0.4014MW4 BJ90194 SW8260 9/12/2015 1 n-Propylbenzene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 n-Butylbenzene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 4-Chlorotoluene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 1,4-Dichlorobenzene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 1,2-Dibromoethane ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 Acrolein ug/L U 5.014MW4 BJ90194 SW8260 9/12/2015 1 1,2-Dichloroethane ug/L U 0.6014MW4 BJ90194 SW8260 9/12/2015 1 Acrylonitrile ug/L UJ 5.014MW4 BJ90194 SW8260 9/12/2015 1 4-Methyl-2-pentanone ug/L U 2.514MW4 BJ90194 SW8260 9/12/2015 1 1,3,5-Trimethylbenzene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 Bromobenzene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 Toluene 2.1 ug/L 1.014MW4 BJ90194 SW8260 9/12/2015 1 Chlorobenzene ug/L U 5.014MW4 BJ90194 SW8260 9/12/2015 1 Tetrahydrofuran (THF) ug/L UJ 5.014MW4 BJ90194 SW8260 9/12/2015 1 trans-1,4-dichloro-2-butene ug/L U 2.514MW4 BJ90194 SW8260 9/12/2015 1 1 2 4-Trichlorobenzene ug/L U 1 014MW4 BJ90194 SW8260 9/12/2015 1 1,2,4 Trichlorobenzene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 Dibromochloromethane ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 Tetrachloroethene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 sec-Butylbenzene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 1,3-Dichloropropane ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 trans-1,2-Dichloroethene 0.82 ug/L J 5.014MW4 BJ90194 SW8260 9/12/2015 1 Methyl t-butyl ether (MTBE) ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 m&p-Xylene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 2-Isopropyltoluene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 1,3-Dichlorobenzene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 Carbon tetrachloride ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 1,1-Dichloropropene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 2-Hexanone ug/L U 2.514MW4 BJ90194 SW8260 9/12/2015 1 2,2-Dichloropropane ug/L UJ 1.014MW4 BJ90194 SW8260 9/12/2015 1 1,1,1,2-Tetrachloroethane ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 Acetone ug/L UJ 5.014MW4 BJ90194 SW8260 9/12/2015 1 Chloroform ug/L U 5.0

Page 13 of 17



SDG: GBJ90192


14MW4 BJ90194 SW8260 9/12/2015 1 Benzene 0.33 ug/L J 0.7014MW4 BJ90194 SW8260 9/12/2015 1 1,1,1-Trichloroethane ug/L U 5.014MW4 BJ90194 SW8260 9/12/2015 1 Bromomethane ug/L UJ 5.014MW4 BJ90194 SW8260 9/12/2015 1 Chloromethane ug/L U 5.014MW4 BJ90194 SW8260 9/12/2015 1 Dibromomethane ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 Bromochloromethane ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 Chloroethane ug/L U 5.014MW4 BJ90194 SW8260 9/12/2015 1 Vinyl chloride 0.75 ug/L J 1.014MW4 BJ90194 SW8260 9/12/2015 1 Methylene chloride ug/L U 3.014MW4 BJ90194 SW8260 9/12/2015 1 Carbon Disulfide ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 Bromoform ug/L U 5.014MW4 BJ90194 SW8260 9/12/2015 1 Bromodichloromethane ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 1,1-Dichloroethane ug/L U 5.014MW4 BJ90194 SW8260 9/12/2015 1 1,1-Dichloroethene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 Trichlorofluoromethane ug/L UJ 1.014MW4 BJ90194 SW8260 9/12/2015 1 Dichlorodifluoromethane ug/L UJ 1.014MW4 BJ90194 SW8260 9/12/2015 1 Trichlorotrifluoroethane ug/L UJ 1.014MW4 BJ90194 SW8260 9/12/2015 1 1,2-Dichloropropane ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 Methyl ethyl ketone ug/L U 2.514MW4 BJ90194 SW8260 9/12/2015 1 1,1,2-Trichloroethane ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 Trichloroethene 2.4 ug/L 1.014MW4 BJ90194 SW8260 9/12/2015 1 1,1,2,2-Tetrachloroethane ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 1,2,3-Trichlorobenzene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 Hexachlorobutadiene ug/L U 1 014MW4 BJ90194 SW8260 9/12/2015 1 Hexachlorobutadiene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 Naphthalene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 o-Xylene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 2-Chlorotoluene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 1,2-Dichlorobenzene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 1,2,4-Trimethylbenzene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 1,2-Dibromo-3-chloropropane ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 1,2,3-Trichloropropane ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 tert-Butylbenzene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 Isopropylbenzene ug/L U 1.014MW4 BJ90194 SW8260 9/12/2015 1 p-Isopropyltoluene ug/L U 1.014MW4 BJ90194 SW8260 9/14/2015 5 cis-1,2-Dichloroethene 51 ug/L 5.014MW4 BJ90194 SW8270 9/15/2015 1 4-Nitroaniline ug/L U 2014MW4 BJ90194 SW8270 9/15/2015 1 Benzyl Alcohol ug/L UJ 5.014MW4 BJ90194 SW8270 9/15/2015 1 4-Bromophenyl phenyl ether ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 1,4-Dichlorobenzene ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 4-Chloroaniline ug/L U 20

Page 14 of 17



SDG: GBJ90192


14MW4 BJ90194 SW8270 9/15/2015 1 Bis(2-chloroethyl)ether ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 Bis(2-chloroethoxy)methane ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 Di-n-octylphthalate ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 1,2,4-Trichlorobenzene ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 2,4-Dinitrotoluene ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 1,2-Diphenylhydrazine ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 Dimethylphthalate ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 Dibenzofuran ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 Bis(2-chloroisopropyl)ether ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 1,3-Dichlorobenzene ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 2,6-Dinitrotoluene ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 N-Nitrosodi-n-propylamine ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 Benzoic acid ug/L U 2014MW4 BJ90194 SW8270 9/15/2015 1 4-Chlorophenyl phenyl ether ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 Hexachlorocyclopentadiene ug/L UJ 5.014MW4 BJ90194 SW8270 9/15/2015 1 Isophorone ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 Diethyl phthalate ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 Di-n-butylphthalate ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 Benzyl butyl phthalate ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 N-Nitrosodiphenylamine ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 2-Nitroaniline ug/L U 2014MW4 BJ90194 SW8270 9/15/2015 1 2-Chloronaphthalene ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 3,3'-Dichlorobenzidine ug/L U 2014MW4 BJ90194 SW8270 9/15/2015 1 Benzidine ug/L U 1814MW4 BJ90194 SW8270 9/15/2015 1 Benzidine ug/L U 1814MW4 BJ90194 SW8270 9/15/2015 1 1,2-Dichlorobenzene ug/L U 5.014MW4 BJ90194 SW8270 9/15/2015 1 3-Nitroaniline ug/L U 2014MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Bis(2-ethylhexyl)phthalate 0.11 ug/L U 0.0514MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Hexachlorobenzene ug/L U 0.0214MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Anthracene 0.10 ug/L 0.0514MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Pyrene 0.05 ug/L 0.0514MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Benzo(ghi)perylene ug/L U 0.0514MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Indeno(1,2,3-cd)pyrene ug/L U 0.0514MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Benzo(b)fluoranthene ug/L U 0.0514MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Fluoranthene ug/L U 0.0514MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Benzo(k)fluoranthene ug/L U 0.0514MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Acenaphthylene ug/L U 0.0514MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Chrysene ug/L U 0.0514MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Benzo(a)pyrene ug/L U 0.0214MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Dibenz(a,h)anthracene ug/L U 0.0514MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Benz(a)anthracene ug/L U 0.05

Page 15 of 17



SDG: GBJ90192


14MW4 BJ90194 SW8270C-SIM 9/14/2015 1 N-Nitrosodimethylamine ug/L U 0.0514MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Hexachloroethane ug/L U 0.0514MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Acenaphthene ug/L U 0.0514MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Phenanthrene ug/L U 0.0514MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Fluorene ug/L U 0.0514MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Hexachlorobutadiene ug/L U 0.0514MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Naphthalene 0.27 ug/L 0.0514MW4 BJ90194 SW8270C-SIM 9/14/2015 1 2-Methylnaphthalene ug/L U 0.0514MW4 BJ90194 SW8270C-SIM 9/14/2015 1 Nitrobenzene ug/L U 0.05BJ90195-TB BJ90195 SW8260 9/11/2015 1 Ethylbenzene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Styrene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 cis-1,3-Dichloropropene ug/L U 0.40BJ90195-TB BJ90195 SW8260 9/11/2015 1 trans-1,3-Dichloropropene ug/L U 0.40BJ90195-TB BJ90195 SW8260 9/11/2015 1 n-Propylbenzene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 n-Butylbenzene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 4-Chlorotoluene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 1,4-Dichlorobenzene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 1,2-Dibromoethane ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Acrolein ug/L U 5.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 1,2-Dichloroethane ug/L U 0.60BJ90195-TB BJ90195 SW8260 9/11/2015 1 Acrylonitrile ug/L UJ 5.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 4-Methyl-2-pentanone ug/L U 2.5BJ90195-TB BJ90195 SW8260 9/11/2015 1 1,3,5-Trimethylbenzene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Bromobenzene ug/L U 1 0BJ90195 TB BJ90195 SW8260 9/11/2015 1 Bromobenzene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Toluene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Chlorobenzene ug/L U 5.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Tetrahydrofuran (THF) ug/L UJ 5.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 trans-1,4-dichloro-2-butene ug/L U 2.5BJ90195-TB BJ90195 SW8260 9/11/2015 1 1,2,4-Trichlorobenzene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Dibromochloromethane ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Tetrachloroethene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 sec-Butylbenzene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 1,3-Dichloropropane ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 cis-1,2-Dichloroethene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 trans-1,2-Dichloroethene ug/L U 5.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Methyl t-butyl ether (MTBE) ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 m&p-Xylene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 2-Isopropyltoluene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 1,3-Dichlorobenzene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Carbon tetrachloride ug/L U 1.0

Page 16 of 17



SDG: GBJ90192


BJ90195-TB BJ90195 SW8260 9/11/2015 1 1,1-Dichloropropene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 2-Hexanone ug/L U 2.5BJ90195-TB BJ90195 SW8260 9/11/2015 1 2,2-Dichloropropane ug/L UJ 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 1,1,1,2-Tetrachloroethane ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Acetone ug/L UJ 5.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Chloroform ug/L U 5.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Benzene ug/L U 0.70BJ90195-TB BJ90195 SW8260 9/11/2015 1 1,1,1-Trichloroethane ug/L U 5.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Bromomethane ug/L UJ 5.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Chloromethane ug/L U 5.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Dibromomethane ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Bromochloromethane ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Chloroethane ug/L U 5.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Vinyl chloride ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Methylene chloride ug/L U 3.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Carbon Disulfide ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Bromoform ug/L U 5.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Bromodichloromethane ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 1,1-Dichloroethane ug/L U 5.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 1,1-Dichloroethene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Trichlorofluoromethane ug/L UJ 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Dichlorodifluoromethane ug/L UJ 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Trichlorotrifluoroethane ug/L UJ 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 1 2-Dichloropropane ug/L U 1 0BJ90195 TB BJ90195 SW8260 9/11/2015 1 1,2 Dichloropropane ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Methyl ethyl ketone ug/L U 2.5BJ90195-TB BJ90195 SW8260 9/11/2015 1 1,1,2-Trichloroethane ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Trichloroethene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 1,1,2,2-Tetrachloroethane ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 1,2,3-Trichlorobenzene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Hexachlorobutadiene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Naphthalene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 o-Xylene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 2-Chlorotoluene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 1,2-Dichlorobenzene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 1,2,4-Trimethylbenzene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 1,2-Dibromo-3-chloropropane ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 1,2,3-Trichloropropane ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 tert-Butylbenzene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 Isopropylbenzene ug/L U 1.0BJ90195-TB BJ90195 SW8260 9/11/2015 1 p-Isopropyltoluene ug/L U 1.0

Page 17 of 17



USEPA Region II –Data Validation Project Name: 510 Driggs Ave Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBJ89522 Client: Environmental Business Consultants Date: 12/24/2015 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for seven (7) air samples analyzed for

Volatiles by TO-15 in accordance to NYSDEC, Analytical Services Protocol (ASP) Format.



3. The USEPA Region-II SOP # HW-31, Revision 4, October 2006, Validating Air Samples Volatile Organic Analysis of Ambient Air in Canister By Method TO-15 was used in evaluating the Volatiles data in this summary report.






Collection Date


14SG5 BJ89522 09/08/15 VOA Air 489 14SG7 BJ89523 09/08/15 VOA Air 13636 14SG6 BJ89524 09/08/15 VOA Air 494 14SG1 BJ89525 09/08/15 VOA Air 480 14SG3 BJ89526 09/08/15 VOA Air 12862 14SG4 BJ89527 09/08/15 VOA Air 11288 14SG2 BJ89528 09/08/15 VOA Air 487



Holding Times: 1. All air samples were analyzed within the method holding time for summa canisters (30

days). No qualifications were required. GC/MS Tuning: 1. All of the BFB tunes in the initial and continuing calibrations met the percent relative


(30.0%) for all compounds and average RRF values (for all compounds with the exception of some compounds listed in section 15.5, Page 13 in SOP # HW-31, were with the following exception(s):


Compound %D 1,1,2-Trichloroethane 30.2

Client Sample ID Laboratory Sample ID Compound Action

14SG5 BJ89522 1,1,2-Trichloroethane UJ 14SG7 BJ89523 1,1,2-Trichloroethane UJ 14SG6 BJ89524 1,1,2-Trichloroethane UJ

2. Initial calibration curve analyzed on 09/14/2015 (Chem24) exhibited acceptable %RSDs (30.0%) for all compounds and average RRF values (for all compounds with the exception of some compounds listed in section 15.5, Page 13 in SOP # HW-31, were . No qualifications were required.


for all compounds with the following exception(s):

Compound %D 4-Isopropyltoluene -32.2

Client Sample ID Laboratory Sample ID Compound Action

14SG5 Dil A BJ89522 4-Isopropyltoluene None 14SG7 Dil A BJ89523 4-Isopropyltoluene None 14SG6 Dil BJ89524 4-Isopropyltoluene None 14SG1 Dil BJ89525 4-Isopropyltoluene None 14SG3 Dil BJ89526 4-Isopropyltoluene None

14SG4 Dil A BJ89527 4-Isopropyltoluene None 14SG2 Dil A BJ89528 4-Isopropyltoluene None 14SG7 Dil B BJ89523 4-Isopropyltoluene None 14SG4 Dil B BJ89527 4-Isopropyltoluene None 14SG2 Dil B BJ89528 4-Isopropyltoluene None 14SG5 Dil B BJ89522 4-Isopropyltoluene None


for all compounds with the following exception(s):

Compound %D 1,1,2-Trichloroethane 35.2


Client Sample ID Laboratory Sample ID Compound Action 14SG5 Dil A BJ89522 1,1,2-Trichloroethane None 14SG7 Dil A BJ89523 1,1,2-Trichloroethane None 14SG6 Dil BJ89524 1,1,2-Trichloroethane None 14SG1 Dil BJ89525 1,1,2-Trichloroethane None 14SG3 Dil BJ89526 1,1,2-Trichloroethane None

14SG4 Dil A BJ89527 1,1,2-Trichloroethane None 14SG2 Dil A BJ89528 1,1,2-Trichloroethane None 14SG7 Dil B BJ89523 1,1,2-Trichloroethane None 14SG4 Dil B BJ89527 1,1,2-Trichloroethane None 14SG2 Dil B BJ89528 1,1,2-Trichloroethane None 14SG5 Dil B BJ89522 1,1,2-Trichloroethane None

Surrogates: 1. 4-Bromofluorobenzene (BFB) surrogate spike recovered within the laboratory control

limits (70-130%) for all samples and associated QC. No qualifications were required. Internal Standard (IS) Area Performance: 1. All samples exhibited acceptable area count for all three internal standards within the QC

limits. No qualifications were required. Method Blank (MB), Storage Blank (SB), Trip Blank (TB), Field Blank (FB), Rinsate Blank (RB, Equipment Blank (EB) and Canister Certification: 1. Method Blank (BLANK BJ89532) analyzed on 09/11/15 was free of contamination. No

qualifications were required. 2. Method Blank (BLANK BJ90968) analyzed on 09/15/15 was free of contamination. No

qualifications were required. 3. Method Blank (BLANK BJ90974) analyzed on 09/14/15 was free of contamination. No

qualifications were required.


4. Canister Certification Check:

Batch ID Date Analyzed

Compound Result (ppbv)

Certification Contamination

Level (5x)*

(ppbv)

Sample Affected

Canister ID #

Action

707 07/20/15 Ethanol 2.30 0.531 14SG4 11288 None Methyl Ethyl

Ketone 0.610 0.339 14SG4 11288 None

713 07/27/15 Ethanol 1.80 0.531 14SG5 489 None Methylene

Chloride 0.400 0.288 14SG5 489 None

Methyl Ethyl Ketone

0.490 0.339 14SG5 489 None

714 07/23/15 None - - 14SG3 14SG1 14SG6

12862 480 494

None

719 07/28/15 None - - 14SG7 13636 None

735 08/18/15 Ethanol 1.40 0.531 14SG2 487 None Acetone 0.730 0.421 14SG2 487 None

*= If sample concentration less than the certification contamination level (CCL), then sample result qualified as non-detect (U). If sample concentration greater than the certification contamination level (CCL) or sample result was not detected, no qualifications/action required.

Laboratory Control Sample (LCS)/ Laboratory Control Sample Duplicate (LCSD):

1. Laboratory Control Sample (LCS BJ89532) was analyzed on 9/11/2015. All %RECs were within the laboratory control limits with the following exception(s):

Compound %R Sample Affected

Action

Styrene 138 14SG5, 14SG7, 14SG6 None

A= Acceptable



Action

1,3-Butadiene 136 14SG5 Dil A, 14SG7 Dil A, 14SG6 Dil, 14SG1 Dil, 14SG3 Dil, 14SG4 Dil A, 14SG2 Dil A,

14SG7 Dil B, 14SG4 Dil B, 14SG2 Dil B, 14SG5

None



Action

Dil B

1,1,2-Trichloroethane 63 14SG5 Dil A, 14SG7 Dil A, 14SG6 Dil, 14SG1 Dil, 14SG3 Dil, 14SG4 Dil A, 14SG2 Dil A,

14SG7 Dil B, 14SG4 Dil B, 14SG2 Dil B, 14SG5 Dil B

None

Styrene 136 14SG5 Dil A, 14SG7 Dil A, 14SG6 Dil, 14SG1 Dil, 14SG3 Dil, 14SG4 Dil A, 14SG2 Dil A,

14SG7 Dil B, 14SG4 Dil B, 14SG2 Dil B, 14SG5 Dil B

None

A= Acceptable



Action

1,3-Butadiene 136 14SG1, 14SG3, 14SG4, 14SG2 None

1,1,2-Trichloroethane 62 14SG1, 14SG3, 14SG4, 14SG2 UJ

Styrene 133 14SG1, 14SG3, 14SG4 14SG2

None J

A= Acceptable Field Duplicate: 1. A field duplicate pair was not submitted with this SDG. Target Compound Identification: 1. All Relative Retention Times (RRTs) of the reported compounds were within 0.06

RRT units of the standard (opening CCV). 2. The following compounds were qualified as estimated due to reported value exceeding

the calibration curve:

Compound Sample Affected

Action

Ethanol 14SG1, 14SG3, 14SG4, 14SG2, 14SG5, 14SG6, 14SG7

J



were required. 2. Manual Calculation: Concentration (g/m3) = Result (ppbv) x Molecular weight x DF

24.46 14SG5 (BJ89522)

Toluene Result (ppbv) = 8.09 Molecular Weight @ 25C=92.14 DF = 1 Concentration (g/m3) = 8.09 x 92.14 x 1 = 30.47g/m3

24.46

Compound Laboratory

(g/m3) Validation

(g/m3) %D

Toluene 30.5 30.5 0.0 Comments: 1. Volatile data package meet requirement for New York State Department of



510 DRIGGS AVENUEBrooklyn, NY

DATA SUMMARY TABLEAir

SDG: GBJ89522

Sample Name Lab ID Analytical Method Analysis Date Dilution Factor Analyte Result Unit Qualifier RL

14SG5 BJ89522 TO15 9/12/2015 1 1,1,1,2-Tetrachloroethane ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 1,1,1-Trichloroethane 2.02 ug/m3 1.0014SG5 BJ89522 TO15 9/12/2015 1 1,1,2,2-Tetrachloroethane ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 1,1,2-Trichloroethane ug/m3 UJ 1.0014SG5 BJ89522 TO15 9/12/2015 1 1,1-Dichloroethane 54.6 ug/m3 1.0014SG5 BJ89522 TO15 9/15/2015 75 1,1-Dichloroethene 1100 ug/m3 74.914SG5 BJ89522 TO15 9/12/2015 1 1,2,4-Trichlorobenzene ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 1,2,4-Trimethylbenzene 1.72 ug/m3 1.0014SG5 BJ89522 TO15 9/12/2015 1 1,2-Dibromoethane(EDB) ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 1,2-Dichlorobenzene ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 1,2-Dichloroethane ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 1,2-dichloropropane ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 1,2-Dichlorotetrafluoroethane ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 1,3,5-Trimethylbenzene ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 1,3-Butadiene ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 1,3-Dichlorobenzene 5.62 ug/m3 1.0014SG5 BJ89522 TO15 9/12/2015 1 1,4-Dichlorobenzene ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 1,4-Dioxane ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 2-Hexanone(MBK) ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 4-Ethyltoluene ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 4-Isopropyltoluene ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 4-Methyl-2-pentanone(MIBK) ug/m3 U 1.0014SG5 BJ89522 TO15 9/15/2015 75 Acetone 1410 ug/m3 75.014SG5 BJ89522 TO15 9/12/2015 1 Acrylonitrile ug/m3 U 1.0014SG5 BJ89522 TO15 9/15/2015 75 Benzene 1240 ug/m3 75.014SG5 BJ89522 TO15 9/12/2015 1 Benzyl chloride ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 Bromodichloromethane ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 Bromoform ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 Bromomethane ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 Carbon Disulfide ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 Carbon Tetrachloride ug/m3 U 0.2514SG5 BJ89522 TO15 9/12/2015 1 Chlorobenzene ug/m3 U 1.0014SG5 BJ89522 TO15 9/15/2015 75 Chloroethane 245 ug/m3 74.914SG5 BJ89522 TO15 9/12/2015 1 Chloroform ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 Chloromethane ug/m3 U 1.0014SG5 BJ89522 TO15 9/16/2015 1500 Cis-1,2-Dichloroethene 44400 ug/m3 150014SG5 BJ89522 TO15 9/12/2015 1 cis-1,3-Dichloropropene ug/m3 U 1.00

Page 1 of 13



SDG: GBJ89522


14SG5 BJ89522 TO15 9/15/2015 75 Cyclohexane 396 ug/m3 75.014SG5 BJ89522 TO15 9/12/2015 1 Dibromochloromethane ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 Dichlorodifluoromethane 90.9 ug/m3 1.0014SG5 BJ89522 TO15 9/12/2015 1 Ethanol 97.9 ug/m3 J 1.0014SG5 BJ89522 TO15 9/12/2015 1 Ethyl acetate ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 Ethylbenzene 4.86 ug/m3 1.0014SG5 BJ89522 TO15 9/12/2015 1 Heptane 9.7 ug/m3 1.0014SG5 BJ89522 TO15 9/12/2015 1 Hexachlorobutadiene ug/m3 U 1.0014SG5 BJ89522 TO15 9/15/2015 75 Hexane 722 ug/m3 75.014SG5 BJ89522 TO15 9/12/2015 1 Isopropylalcohol 19.6 ug/m3 1.0014SG5 BJ89522 TO15 9/12/2015 1 Isopropylbenzene 2.36 ug/m3 1.0014SG5 BJ89522 TO15 9/12/2015 1 m,p-Xylene 16.4 ug/m3 1.0014SG5 BJ89522 TO15 9/12/2015 1 Methyl Ethyl Ketone ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 Methyl tert-butyl ether(MTBE) ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 Methylene Chloride ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 n-Butylbenzene ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 o-Xylene 10.2 ug/m3 1.0014SG5 BJ89522 TO15 9/15/2015 75 Propylene 3780 ug/m3 75.014SG5 BJ89522 TO15 9/12/2015 1 sec-Butylbenzene ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 Styrene ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 Tetrachloroethene 8.74 ug/m3 0.2514SG5 BJ89522 TO15 9/12/2015 1 Tetrahydrofuran ug/m3 U 1.0014SG5 BJ89522 TO15 9/12/2015 1 Toluene 30.5 ug/m3 1.0014SG5 BJ89522 TO15 9/15/2015 75 Trans-1,2-Dichloroethene 1380 ug/m3 74.914SG5 BJ89522 TO15 9/12/2015 1 trans-1,3-Dichloropropene ug/m3 U 1.0014SG5 BJ89522 TO15 9/15/2015 75 Trichloroethene 5690 ug/m3 18.714SG5 BJ89522 TO15 9/12/2015 1 Trichlorofluoromethane 19.9 ug/m3 1.0014SG5 BJ89522 TO15 9/12/2015 1 Trichlorotrifluoroethane ug/m3 U 1.0014SG5 BJ89522 TO15 9/16/2015 1500 Vinyl Chloride 116000 ug/m3 37614SG7 BJ89523 TO15 9/12/2015 1 1,1,1,2-Tetrachloroethane ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 1,1,1-Trichloroethane 2.21 ug/m3 1.0014SG7 BJ89523 TO15 9/12/2015 1 1,1,2,2-Tetrachloroethane ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 1,1,2-Trichloroethane ug/m3 UJ 1.0014SG7 BJ89523 TO15 9/12/2015 1 1,1-Dichloroethane 25.2 ug/m3 1.0014SG7 BJ89523 TO15 9/15/2015 75 1,1-Dichloroethene 586 ug/m3 74.914SG7 BJ89523 TO15 9/12/2015 1 1,2,4-Trichlorobenzene ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 1,2,4-Trimethylbenzene 1.89 ug/m3 1.00

Page 2 of 13



SDG: GBJ89522


14SG7 BJ89523 TO15 9/12/2015 1 1,2-Dibromoethane(EDB) ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 1,2-Dichlorobenzene ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 1,2-Dichloroethane ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 1,2-dichloropropane ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 1,2-Dichlorotetrafluoroethane ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 1,3,5-Trimethylbenzene ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 1,3-Butadiene ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 1,3-Dichlorobenzene 5.57 ug/m3 1.0014SG7 BJ89523 TO15 9/12/2015 1 1,4-Dichlorobenzene ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 1,4-Dioxane ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 2-Hexanone(MBK) 67.5 ug/m3 1.0014SG7 BJ89523 TO15 9/12/2015 1 4-Ethyltoluene ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 4-Isopropyltoluene ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 4-Methyl-2-pentanone(MIBK) 9.6 ug/m3 1.0014SG7 BJ89523 TO15 9/15/2015 75 Acetone 1510 ug/m3 75.014SG7 BJ89523 TO15 9/12/2015 1 Acrylonitrile ug/m3 U 1.0014SG7 BJ89523 TO15 9/15/2015 75 Benzene 390 ug/m3 75.014SG7 BJ89523 TO15 9/12/2015 1 Benzyl chloride ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 Bromodichloromethane ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 Bromoform ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 Bromomethane ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 Carbon Disulfide ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 Carbon Tetrachloride ug/m3 U 0.2514SG7 BJ89523 TO15 9/12/2015 1 Chlorobenzene ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 Chloroethane 33.2 ug/m3 1.0014SG7 BJ89523 TO15 9/12/2015 1 Chloroform 1.73 ug/m3 1.0014SG7 BJ89523 TO15 9/12/2015 1 Chloromethane 1.40 ug/m3 1.0014SG7 BJ89523 TO15 9/15/2015 75 Cis-1,2-Dichloroethene 4200 ug/m3 74.914SG7 BJ89523 TO15 9/12/2015 1 cis-1,3-Dichloropropene ug/m3 U 1.0014SG7 BJ89523 TO15 9/15/2015 75 Cyclohexane 172 ug/m3 75.014SG7 BJ89523 TO15 9/12/2015 1 Dibromochloromethane ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 Dichlorodifluoromethane 47.0 ug/m3 1.0014SG7 BJ89523 TO15 9/12/2015 1 Ethanol 84.0 ug/m3 J 1.0014SG7 BJ89523 TO15 9/12/2015 1 Ethyl acetate ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 Ethylbenzene 4.34 ug/m3 1.0014SG7 BJ89523 TO15 9/12/2015 1 Heptane ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 Hexachlorobutadiene ug/m3 U 1.00

Page 3 of 13



SDG: GBJ89522


14SG7 BJ89523 TO15 9/15/2015 75 Hexane 262 ug/m3 75.014SG7 BJ89523 TO15 9/12/2015 1 Isopropylalcohol 20.9 ug/m3 1.0014SG7 BJ89523 TO15 9/12/2015 1 Isopropylbenzene ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 m,p-Xylene 11.5 ug/m3 1.0014SG7 BJ89523 TO15 9/15/2015 75 Methyl Ethyl Ketone 162 ug/m3 74.914SG7 BJ89523 TO15 9/12/2015 1 Methyl tert-butyl ether(MTBE) ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 Methylene Chloride 20.0 ug/m3 1.0014SG7 BJ89523 TO15 9/12/2015 1 n-Butylbenzene ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 o-Xylene 6.94 ug/m3 1.0014SG7 BJ89523 TO15 9/16/2015 150 Propylene 5610 ug/m3 15014SG7 BJ89523 TO15 9/12/2015 1 sec-Butylbenzene ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 Styrene ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 Tetrachloroethene 23.4 ug/m3 0.2514SG7 BJ89523 TO15 9/12/2015 1 Tetrahydrofuran ug/m3 U 1.0014SG7 BJ89523 TO15 9/12/2015 1 Toluene 11.3 ug/m3 1.0014SG7 BJ89523 TO15 9/12/2015 1 Trans-1,2-Dichloroethene 128 ug/m3 1.0014SG7 BJ89523 TO15 9/12/2015 1 trans-1,3-Dichloropropene ug/m3 U 1.0014SG7 BJ89523 TO15 9/15/2015 75 Trichloroethene 6120 ug/m3 18.714SG7 BJ89523 TO15 9/12/2015 1 Trichlorofluoromethane 14.1 ug/m3 1.0014SG7 BJ89523 TO15 9/12/2015 1 Trichlorotrifluoroethane ug/m3 U 1.0014SG7 BJ89523 TO15 9/16/2015 150 Vinyl Chloride 10800 ug/m3 37.614SG6 BJ89524 TO15 9/12/2015 1 1,1,1,2-Tetrachloroethane ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 1,1,1-Trichloroethane 2.74 ug/m3 1.0014SG6 BJ89524 TO15 9/12/2015 1 1,1,2,2-Tetrachloroethane ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 1,1,2-Trichloroethane ug/m3 UJ 1.0014SG6 BJ89524 TO15 9/12/2015 1 1,1-Dichloroethane ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 1,1-Dichloroethene ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 1,2,4-Trichlorobenzene ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 1,2,4-Trimethylbenzene 2.23 ug/m3 1.0014SG6 BJ89524 TO15 9/12/2015 1 1,2-Dibromoethane(EDB) ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 1,2-Dichlorobenzene ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 1,2-Dichloroethane ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 1,2-dichloropropane ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 1,2-Dichlorotetrafluoroethane ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 1,3,5-Trimethylbenzene ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 1,3-Butadiene ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 1,3-Dichlorobenzene 7.93 ug/m3 1.00

Page 4 of 13



SDG: GBJ89522


14SG6 BJ89524 TO15 9/12/2015 1 1,4-Dichlorobenzene ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 1,4-Dioxane ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 2-Hexanone(MBK) 80.2 ug/m3 1.0014SG6 BJ89524 TO15 9/12/2015 1 4-Ethyltoluene ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 4-Isopropyltoluene ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 4-Methyl-2-pentanone(MIBK) 13.8 ug/m3 1.0014SG6 BJ89524 TO15 9/16/2015 32 Acetone 1650 ug/m3 32.014SG6 BJ89524 TO15 9/12/2015 1 Acrylonitrile ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 Benzene 6.61 ug/m3 1.0014SG6 BJ89524 TO15 9/12/2015 1 Benzyl chloride ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 Bromodichloromethane ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 Bromoform ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 Bromomethane ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 Carbon Disulfide 1.10 ug/m3 1.0014SG6 BJ89524 TO15 9/12/2015 1 Carbon Tetrachloride 0.26 ug/m3 0.2514SG6 BJ89524 TO15 9/12/2015 1 Chlorobenzene ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 Chloroethane ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 Chloroform 8.44 ug/m3 1.0014SG6 BJ89524 TO15 9/12/2015 1 Chloromethane ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 Cis-1,2-Dichloroethene 5.27 ug/m3 1.0014SG6 BJ89524 TO15 9/12/2015 1 cis-1,3-Dichloropropene ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 Cyclohexane ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 Dibromochloromethane ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 Dichlorodifluoromethane 25.8 ug/m3 1.0014SG6 BJ89524 TO15 9/12/2015 1 Ethanol 178 ug/m3 J 1.0014SG6 BJ89524 TO15 9/12/2015 1 Ethyl acetate ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 Ethylbenzene 5.82 ug/m3 1.0014SG6 BJ89524 TO15 9/12/2015 1 Heptane 7.04 ug/m3 1.0014SG6 BJ89524 TO15 9/12/2015 1 Hexachlorobutadiene ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 Hexane 6.52 ug/m3 1.0014SG6 BJ89524 TO15 9/12/2015 1 Isopropylalcohol 36.8 ug/m3 1.0014SG6 BJ89524 TO15 9/12/2015 1 Isopropylbenzene ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 m,p-Xylene 21.2 ug/m3 1.0014SG6 BJ89524 TO15 9/16/2015 32 Methyl Ethyl Ketone 469 ug/m3 32.114SG6 BJ89524 TO15 9/12/2015 1 Methyl tert-butyl ether(MTBE) ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 Methylene Chloride ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 n-Butylbenzene ug/m3 U 1.00

Page 5 of 13



SDG: GBJ89522


14SG6 BJ89524 TO15 9/12/2015 1 o-Xylene 8.46 ug/m3 1.0014SG6 BJ89524 TO15 9/16/2015 32 Propylene 79.8 ug/m3 32.014SG6 BJ89524 TO15 9/12/2015 1 sec-Butylbenzene ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 Styrene ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 Tetrachloroethene 4.74 ug/m3 0.2514SG6 BJ89524 TO15 9/12/2015 1 Tetrahydrofuran ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 Toluene 7.76 ug/m3 1.0014SG6 BJ89524 TO15 9/12/2015 1 Trans-1,2-Dichloroethene ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 trans-1,3-Dichloropropene ug/m3 U 1.0014SG6 BJ89524 TO15 9/16/2015 32 Trichloroethene 763 ug/m3 8.0014SG6 BJ89524 TO15 9/12/2015 1 Trichlorofluoromethane 183 ug/m3 1.0014SG6 BJ89524 TO15 9/12/2015 1 Trichlorotrifluoroethane ug/m3 U 1.0014SG6 BJ89524 TO15 9/12/2015 1 Vinyl Chloride ug/m3 U 0.2514SG1 BJ89525 TO15 9/15/2015 1 1,1,1,2-Tetrachloroethane ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 1,1,1-Trichloroethane 13.8 ug/m3 1.0014SG1 BJ89525 TO15 9/15/2015 1 1,1,2,2-Tetrachloroethane ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 1,1,2-Trichloroethane ug/m3 UJ 1.0014SG1 BJ89525 TO15 9/15/2015 1 1,1-Dichloroethane ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 1,1-Dichloroethene ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 1,2,4-Trichlorobenzene ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 1,2,4-Trimethylbenzene 2.05 ug/m3 1.0014SG1 BJ89525 TO15 9/15/2015 1 1,2-Dibromoethane(EDB) ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 1,2-Dichlorobenzene ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 1,2-Dichloroethane ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 1,2-dichloropropane ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 1,2-Dichlorotetrafluoroethane ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 1,3,5-Trimethylbenzene ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 1,3-Butadiene ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 1,3-Dichlorobenzene 9.31 ug/m3 1.0014SG1 BJ89525 TO15 9/15/2015 1 1,4-Dichlorobenzene ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 1,4-Dioxane ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 2-Hexanone(MBK) 113 ug/m3 1.0014SG1 BJ89525 TO15 9/15/2015 1 4-Ethyltoluene ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 4-Isopropyltoluene ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 4-Methyl-2-pentanone(MIBK) 10.4 ug/m3 1.0014SG1 BJ89525 TO15 9/16/2015 40 Acetone 1550 ug/m3 39.914SG1 BJ89525 TO15 9/15/2015 1 Acrylonitrile ug/m3 U 1.00

Page 6 of 13



SDG: GBJ89522


14SG1 BJ89525 TO15 9/15/2015 1 Benzene 2.93 ug/m3 1.0014SG1 BJ89525 TO15 9/15/2015 1 Benzyl chloride ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 Bromodichloromethane ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 Bromoform ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 Bromomethane ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 Carbon Disulfide 1.02 ug/m3 1.0014SG1 BJ89525 TO15 9/15/2015 1 Carbon Tetrachloride 0.33 ug/m3 0.2514SG1 BJ89525 TO15 9/15/2015 1 Chlorobenzene ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 Chloroethane ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 Chloroform 84.4 ug/m3 1.0014SG1 BJ89525 TO15 9/15/2015 1 Chloromethane ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 Cis-1,2-Dichloroethene 5.43 ug/m3 1.0014SG1 BJ89525 TO15 9/15/2015 1 cis-1,3-Dichloropropene ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 Cyclohexane ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 Dibromochloromethane ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 Dichlorodifluoromethane 75.1 ug/m3 1.0014SG1 BJ89525 TO15 9/15/2015 1 Ethanol 138 ug/m3 J 1.0014SG1 BJ89525 TO15 9/15/2015 1 Ethyl acetate 2.30 ug/m3 1.0014SG1 BJ89525 TO15 9/15/2015 1 Ethylbenzene 4.69 ug/m3 1.0014SG1 BJ89525 TO15 9/15/2015 1 Heptane 5.98 ug/m3 1.0014SG1 BJ89525 TO15 9/15/2015 1 Hexachlorobutadiene ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 Hexane 4.97 ug/m3 1.0014SG1 BJ89525 TO15 9/15/2015 1 Isopropylalcohol 28.7 ug/m3 1.0014SG1 BJ89525 TO15 9/15/2015 1 Isopropylbenzene ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 m,p-Xylene 17.0 ug/m3 1.0014SG1 BJ89525 TO15 9/16/2015 40 Methyl Ethyl Ketone 327 ug/m3 40.114SG1 BJ89525 TO15 9/15/2015 1 Methyl tert-butyl ether(MTBE) ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 Methylene Chloride 1.19 ug/m3 1.0014SG1 BJ89525 TO15 9/15/2015 1 n-Butylbenzene ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 o-Xylene 7.51 ug/m3 1.0014SG1 BJ89525 TO15 9/16/2015 40 Propylene 71.9 ug/m3 40.114SG1 BJ89525 TO15 9/15/2015 1 sec-Butylbenzene ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 Styrene ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 Tetrachloroethene 30.0 ug/m3 0.2514SG1 BJ89525 TO15 9/15/2015 1 Tetrahydrofuran ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 Toluene 7.34 ug/m3 1.0014SG1 BJ89525 TO15 9/15/2015 1 Trans-1,2-Dichloroethene ug/m3 U 1.00

Page 7 of 13



SDG: GBJ89522


14SG1 BJ89525 TO15 9/15/2015 1 trans-1,3-Dichloropropene ug/m3 U 1.0014SG1 BJ89525 TO15 9/16/2015 40 Trichloroethene 2910 ug/m3 10.014SG1 BJ89525 TO15 9/16/2015 40 Trichlorofluoromethane 249 ug/m3 40.014SG1 BJ89525 TO15 9/15/2015 1 Trichlorotrifluoroethane ug/m3 U 1.0014SG1 BJ89525 TO15 9/15/2015 1 Vinyl Chloride 0.82 ug/m3 0.2514SG3 BJ89526 TO15 9/15/2015 1 1,1,1,2-Tetrachloroethane ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 1,1,1-Trichloroethane 7.36 ug/m3 1.0014SG3 BJ89526 TO15 9/15/2015 1 1,1,2,2-Tetrachloroethane ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 1,1,2-Trichloroethane ug/m3 UJ 1.0014SG3 BJ89526 TO15 9/15/2015 1 1,1-Dichloroethane 2.51 ug/m3 1.0014SG3 BJ89526 TO15 9/15/2015 1 1,1-Dichloroethene ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 1,2,4-Trichlorobenzene ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 1,2,4-Trimethylbenzene 2.52 ug/m3 1.0014SG3 BJ89526 TO15 9/15/2015 1 1,2-Dibromoethane(EDB) ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 1,2-Dichlorobenzene ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 1,2-Dichloroethane ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 1,2-dichloropropane ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 1,2-Dichlorotetrafluoroethane ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 1,3,5-Trimethylbenzene ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 1,3-Butadiene ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 1,3-Dichlorobenzene 16.6 ug/m3 1.0014SG3 BJ89526 TO15 9/15/2015 1 1,4-Dichlorobenzene ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 1,4-Dioxane ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 2-Hexanone(MBK) 102 ug/m3 1.0014SG3 BJ89526 TO15 9/15/2015 1 4-Ethyltoluene ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 4-Isopropyltoluene ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 4-Methyl-2-pentanone(MIBK) 9.13 ug/m3 1.0014SG3 BJ89526 TO15 9/16/2015 40 Acetone 1580 ug/m3 39.914SG3 BJ89526 TO15 9/15/2015 1 Acrylonitrile ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 Benzene 2.26 ug/m3 1.0014SG3 BJ89526 TO15 9/15/2015 1 Benzyl chloride ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 Bromodichloromethane ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 Bromoform ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 Bromomethane ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 Carbon Disulfide ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 Carbon Tetrachloride 0.57 ug/m3 0.2514SG3 BJ89526 TO15 9/15/2015 1 Chlorobenzene ug/m3 U 1.00

Page 8 of 13



SDG: GBJ89522


14SG3 BJ89526 TO15 9/15/2015 1 Chloroethane ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 Chloroform 10.3 ug/m3 1.0014SG3 BJ89526 TO15 9/15/2015 1 Chloromethane ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 Cis-1,2-Dichloroethene 31.7 ug/m3 1.0014SG3 BJ89526 TO15 9/15/2015 1 cis-1,3-Dichloropropene ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 Cyclohexane ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 Dibromochloromethane ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 Dichlorodifluoromethane 152 ug/m3 1.0014SG3 BJ89526 TO15 9/15/2015 1 Ethanol 169 ug/m3 J 1.0014SG3 BJ89526 TO15 9/15/2015 1 Ethyl acetate 1.82 ug/m3 1.0014SG3 BJ89526 TO15 9/15/2015 1 Ethylbenzene 5.08 ug/m3 1.0014SG3 BJ89526 TO15 9/15/2015 1 Heptane 4.26 ug/m3 1.0014SG3 BJ89526 TO15 9/15/2015 1 Hexachlorobutadiene ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 Hexane 3.80 ug/m3 1.0014SG3 BJ89526 TO15 9/15/2015 1 Isopropylalcohol 27.0 ug/m3 1.0014SG3 BJ89526 TO15 9/15/2015 1 Isopropylbenzene ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 m,p-Xylene 19.4 ug/m3 1.0014SG3 BJ89526 TO15 9/16/2015 40 Methyl Ethyl Ketone 318 ug/m3 40.114SG3 BJ89526 TO15 9/15/2015 1 Methyl tert-butyl ether(MTBE) ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 Methylene Chloride ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 n-Butylbenzene ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 o-Xylene 8.42 ug/m3 1.0014SG3 BJ89526 TO15 9/16/2015 40 Propylene 83.8 ug/m3 40.114SG3 BJ89526 TO15 9/15/2015 1 sec-Butylbenzene ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 Styrene ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 Tetrachloroethene 25.6 ug/m3 0.2514SG3 BJ89526 TO15 9/15/2015 1 Tetrahydrofuran 4.13 ug/m3 1.0014SG3 BJ89526 TO15 9/15/2015 1 Toluene 6.36 ug/m3 1.0014SG3 BJ89526 TO15 9/15/2015 1 Trans-1,2-Dichloroethene 3.48 ug/m3 1.0014SG3 BJ89526 TO15 9/15/2015 1 trans-1,3-Dichloropropene ug/m3 U 1.0014SG3 BJ89526 TO15 9/16/2015 40 Trichloroethene 1840 ug/m3 10.014SG3 BJ89526 TO15 9/16/2015 40 Trichlorofluoromethane 691 ug/m3 40.014SG3 BJ89526 TO15 9/15/2015 1 Trichlorotrifluoroethane ug/m3 U 1.0014SG3 BJ89526 TO15 9/15/2015 1 Vinyl Chloride ug/m3 U 0.2514SG4 BJ89527 TO15 9/15/2015 1 1,1,1,2-Tetrachloroethane ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 1,1,1-Trichloroethane 1.07 ug/m3 1.0014SG4 BJ89527 TO15 9/15/2015 1 1,1,2,2-Tetrachloroethane ug/m3 U 1.00

Page 9 of 13



SDG: GBJ89522


14SG4 BJ89527 TO15 9/15/2015 1 1,1,2-Trichloroethane ug/m3 UJ 1.0014SG4 BJ89527 TO15 9/15/2015 1 1,1-Dichloroethane 58.2 ug/m3 1.0014SG4 BJ89527 TO15 9/15/2015 1 1,1-Dichloroethene 44.4 ug/m3 1.0014SG4 BJ89527 TO15 9/15/2015 1 1,2,4-Trichlorobenzene ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 1,2,4-Trimethylbenzene 1.46 ug/m3 1.0014SG4 BJ89527 TO15 9/15/2015 1 1,2-Dibromoethane(EDB) ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 1,2-Dichlorobenzene ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 1,2-Dichloroethane ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 1,2-dichloropropane ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 1,2-Dichlorotetrafluoroethane ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 1,3,5-Trimethylbenzene ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 1,3-Butadiene ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 1,3-Dichlorobenzene 9.01 ug/m3 1.0014SG4 BJ89527 TO15 9/15/2015 1 1,4-Dichlorobenzene ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 1,4-Dioxane ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 2-Hexanone(MBK) 107 ug/m3 1.0014SG4 BJ89527 TO15 9/15/2015 1 4-Ethyltoluene ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 4-Isopropyltoluene ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 4-Methyl-2-pentanone(MIBK) 6.10 ug/m3 1.0014SG4 BJ89527 TO15 9/16/2015 30 Acetone 1370 ug/m3 29.914SG4 BJ89527 TO15 9/15/2015 1 Acrylonitrile ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 Benzene 79.5 ug/m3 1.0014SG4 BJ89527 TO15 9/15/2015 1 Benzyl chloride ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 Bromodichloromethane ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 Bromoform ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 Bromomethane ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 Carbon Disulfide ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 Carbon Tetrachloride ug/m3 U 0.2514SG4 BJ89527 TO15 9/15/2015 1 Chlorobenzene ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 Chloroethane ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 Chloroform 2.53 ug/m3 1.0014SG4 BJ89527 TO15 9/15/2015 1 Chloromethane ug/m3 U 1.0014SG4 BJ89527 TO15 9/16/2015 30 Cis-1,2-Dichloroethene 3140 ug/m3 30.014SG4 BJ89527 TO15 9/15/2015 1 cis-1,3-Dichloropropene ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 Cyclohexane 8.60 ug/m3 1.0014SG4 BJ89527 TO15 9/15/2015 1 Dibromochloromethane ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 Dichlorodifluoromethane 140 ug/m3 1.00

Page 10 of 13



SDG: GBJ89522


14SG4 BJ89527 TO15 9/15/2015 1 Ethanol 104 ug/m3 J 1.0014SG4 BJ89527 TO15 9/15/2015 1 Ethyl acetate ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 Ethylbenzene 2.84 ug/m3 1.0014SG4 BJ89527 TO15 9/15/2015 1 Heptane 7.09 ug/m3 1.0014SG4 BJ89527 TO15 9/15/2015 1 Hexachlorobutadiene ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 Hexane 12.2 ug/m3 1.0014SG4 BJ89527 TO15 9/15/2015 1 Isopropylalcohol 35.9 ug/m3 1.0014SG4 BJ89527 TO15 9/15/2015 1 Isopropylbenzene ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 m,p-Xylene 10.1 ug/m3 1.0014SG4 BJ89527 TO15 9/16/2015 30 Methyl Ethyl Ketone 304 ug/m3 30.114SG4 BJ89527 TO15 9/15/2015 1 Methyl tert-butyl ether(MTBE) ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 Methylene Chloride 1.82 ug/m3 1.0014SG4 BJ89527 TO15 9/15/2015 1 n-Butylbenzene ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 o-Xylene 5.21 ug/m3 1.0014SG4 BJ89527 TO15 9/16/2015 30 Propylene 390 ug/m3 29.914SG4 BJ89527 TO15 9/15/2015 1 sec-Butylbenzene ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 Styrene ug/m3 U 1.0014SG4 BJ89527 TO15 9/15/2015 1 Tetrachloroethene 7.25 ug/m3 0.2514SG4 BJ89527 TO15 9/15/2015 1 Tetrahydrofuran 2.63 ug/m3 1.0014SG4 BJ89527 TO15 9/15/2015 1 Toluene 5.27 ug/m3 1.0014SG4 BJ89527 TO15 9/15/2015 1 Trans-1,2-Dichloroethene 64.6 ug/m3 1.0014SG4 BJ89527 TO15 9/15/2015 1 trans-1,3-Dichloropropene ug/m3 U 1.0014SG4 BJ89527 TO15 9/16/2015 30 Trichloroethene 1330 ug/m3 7.5214SG4 BJ89527 TO15 9/15/2015 1 Trichlorofluoromethane 14.4 ug/m3 1.0014SG4 BJ89527 TO15 9/15/2015 1 Trichlorotrifluoroethane ug/m3 U 1.0014SG4 BJ89527 TO15 9/16/2015 75 Vinyl Chloride 3240 ug/m3 18.814SG2 BJ89528 TO15 9/15/2015 1 1,1,1,2-Tetrachloroethane ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 1,1,1-Trichloroethane 86.2 ug/m3 1.0014SG2 BJ89528 TO15 9/15/2015 1 1,1,2,2-Tetrachloroethane ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 1,1,2-Trichloroethane ug/m3 UJ 1.0014SG2 BJ89528 TO15 9/15/2015 1 1,1-Dichloroethane 4.77 ug/m3 1.0014SG2 BJ89528 TO15 9/15/2015 1 1,1-Dichloroethene ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 1,2,4-Trichlorobenzene ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 1,2,4-Trimethylbenzene 2.67 ug/m3 1.0014SG2 BJ89528 TO15 9/15/2015 1 1,2-Dibromoethane(EDB) ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 1,2-Dichlorobenzene ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 1,2-Dichloroethane ug/m3 U 1.00

Page 11 of 13



SDG: GBJ89522


14SG2 BJ89528 TO15 9/15/2015 1 1,2-dichloropropane ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 1,2-Dichlorotetrafluoroethane ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 1,3,5-Trimethylbenzene ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 1,3-Butadiene ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 1,3-Dichlorobenzene 11.0 ug/m3 1.0014SG2 BJ89528 TO15 9/15/2015 1 1,4-Dichlorobenzene ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 1,4-Dioxane ug/m3 U 1.0014SG2 BJ89528 TO15 9/16/2015 40 2-Hexanone(MBK) 148 ug/m3 40.014SG2 BJ89528 TO15 9/15/2015 1 4-Ethyltoluene ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 4-Isopropyltoluene ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 4-Methyl-2-pentanone(MIBK) 10.4 ug/m3 1.0014SG2 BJ89528 TO15 9/16/2015 40 Acetone 2920 ug/m3 39.914SG2 BJ89528 TO15 9/15/2015 1 Acrylonitrile ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 Benzene 6.93 ug/m3 1.0014SG2 BJ89528 TO15 9/15/2015 1 Benzyl chloride ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 Bromodichloromethane ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 Bromoform ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 Bromomethane ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 Carbon Disulfide 1.75 ug/m3 1.0014SG2 BJ89528 TO15 9/15/2015 1 Carbon Tetrachloride 0.35 ug/m3 0.2514SG2 BJ89528 TO15 9/15/2015 1 Chlorobenzene ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 Chloroethane ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 Chloroform 165 ug/m3 1.0014SG2 BJ89528 TO15 9/15/2015 1 Chloromethane 2.33 ug/m3 1.0014SG2 BJ89528 TO15 9/16/2015 40 Cis-1,2-Dichloroethene 452 ug/m3 40.014SG2 BJ89528 TO15 9/15/2015 1 cis-1,3-Dichloropropene ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 Cyclohexane ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 Dibromochloromethane ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 Dichlorodifluoromethane 32.8 ug/m3 1.0014SG2 BJ89528 TO15 9/15/2015 1 Ethanol 215 ug/m3 J 1.0014SG2 BJ89528 TO15 9/15/2015 1 Ethyl acetate 7.02 ug/m3 1.0014SG2 BJ89528 TO15 9/15/2015 1 Ethylbenzene 5.12 ug/m3 1.0014SG2 BJ89528 TO15 9/15/2015 1 Heptane 13.9 ug/m3 1.0014SG2 BJ89528 TO15 9/15/2015 1 Hexachlorobutadiene ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 Hexane 11.9 ug/m3 1.0014SG2 BJ89528 TO15 9/15/2015 1 Isopropylalcohol 75.4 ug/m3 1.0014SG2 BJ89528 TO15 9/15/2015 1 Isopropylbenzene ug/m3 U 1.00

Page 12 of 13



SDG: GBJ89522


14SG2 BJ89528 TO15 9/15/2015 1 m,p-Xylene 18.3 ug/m3 1.0014SG2 BJ89528 TO15 9/16/2015 40 Methyl Ethyl Ketone 796 ug/m3 40.114SG2 BJ89528 TO15 9/15/2015 1 Methyl tert-butyl ether(MTBE) ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 Methylene Chloride 4.30 ug/m3 1.0014SG2 BJ89528 TO15 9/15/2015 1 n-Butylbenzene ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 o-Xylene 7.68 ug/m3 1.0014SG2 BJ89528 TO15 9/16/2015 40 Propylene 104 ug/m3 40.114SG2 BJ89528 TO15 9/15/2015 1 sec-Butylbenzene ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 Styrene 1.08 ug/m3 J 1.0014SG2 BJ89528 TO15 9/15/2015 1 Tetrachloroethene 113 ug/m3 0.2514SG2 BJ89528 TO15 9/15/2015 1 Tetrahydrofuran 1.69 ug/m3 1.0014SG2 BJ89528 TO15 9/15/2015 1 Toluene 17.6 ug/m3 1.0014SG2 BJ89528 TO15 9/15/2015 1 Trans-1,2-Dichloroethene 13.7 ug/m3 1.0014SG2 BJ89528 TO15 9/15/2015 1 trans-1,3-Dichloropropene ug/m3 U 1.0014SG2 BJ89528 TO15 9/16/2015 100 Trichloroethene 16900 ug/m3 25.014SG2 BJ89528 TO15 9/15/2015 1 Trichlorofluoromethane 62.9 ug/m3 1.0014SG2 BJ89528 TO15 9/15/2015 1 Trichlorotrifluoroethane ug/m3 U 1.0014SG2 BJ89528 TO15 9/15/2015 1 Vinyl Chloride ug/m3 U 0.25

Page 13 of 13

Page 1 of 8 Environmental Business Consultants SDG #: GBH21773


USEPA Region II –Data Validation Project Name: 510 Driggs Ave Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBH21773 Client: Environmental Business Consultants Date: 12/24/2015 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for three (3) water samples analyzed for

Volatiles by SW-846 Method 8260C in accordance to NYSDEC, Analytical Services Protocol (ASP) Format.









Collection Date


GW 1 BH21773 09/30/14 VOA Water GW 3 BH21774 09/30/14 VOA Water GW 4 BH21775 09/30/14 VOA Water







Compound RRF %D

Methylene Chloride A 23.2 A= Acceptable



Compound Action

GW 1 BH21773 Methylene Chloride UJ GW 3 BH21774 Methylene Chloride J GW 4 BH21775 Methylene Chloride UJ




Compound RRF %D

Chloromethane A -21.1 Vinyl Chloride A -21.5 Bromomethane A -31.9

1,1-Dichloroethene A -24.4 Trans-1,2-Dichloroethene A -26.7

1,1-Dichloroethane A -24.3 Cis-1,2-Dichloroethene A -24.4

Chloroform A -20.7 1,1,1-Trichloroethane A -28.7 1,1-Dichloropropene A -26.3 Carbon Tetrachloride A -28.8

Benzene A -24.6 Trichloroethene A -24.9

Toluene A -25.2 Tetrachloroethene A -33.3

Chlorobenzene A -27.3 1,1,1,2-Tetrachloroethane A -24.5

Ethylbenzene A -34.7 M&p-Xylene A -28.7

o-Xylene A -26.4 Styrene A -25.4

Isopropylbenzene A -40.9 Bromobenzene A -26.5

n-Propylbenzene A -40.0 2-Chlorotoluene A -35.5


Compound RRF %D 1,3,5-Trimethylbenzene A -40.3

4-Chlorotoluene A -35.9 Tert-Butylbenzene A -43.1

1,2,4-Trimethylbenzene A -39.1 Sec-Butylbenzene A -42.3

1,3-Dichlorobenzene A -31.3 p-Isopropyltoluene A -47.5

1,4-Dichlorobenzene A -23.7 2-Isopropyltoluene A -43.4

n-Butylbenzene A -43.8 1,2-Dichlorobenzene A -23.4

1,2,4-Trichlorobenzene A -27.0 Hexachlorobutadiene A -43.1

Naphthalene A -43.1 1,2,3-Trichlorobenzene A -24.6

A= Acceptable (1) Results for these compounds were previously qualified due to ICV criteria. (2) Results for these compounds were previously qualified due to the opening CCV criteria.



GW 1 BH21773 Trans-1,2-Dichloroethene, Cis-1,2-Dichloroethene Benzene, Vinyl Chloride, Trichloroethene

Bromomethane, Chloromethane 1,1-Dichloroethene, 1,1-Dichloroethane, Chloroform

1,1,1-Trichloroethane, 1,1-Dichloropropene Carbon Tetrachloride, Toluene, Tetrachloroethene

Chlorobenzene, 1,1,1,2-Tetrachloroethane Ethylbenzene, M&p-Xylene, o-Xylene, Styrene

Isopropylbenzene, Bromobenzene, n-Propylbenzene 2-Chlorotoluene, 1,3,5-Trimethylbenzene

4-Chlorotoluene, Tert-Butylbenzene 1,2,4-Trimethylbenzene, Sec-Butylbenzene 1,3-Dichlorobenzene, p-Isopropyltoluene

1,4-Dichlorobenzene, n-Butylbenzene 1,2-Dichlorobenzene, 1,2,4-Trichlorobenzene

Hexachlorobutadiene, Naphthalene 1,2,3- Trichlorobenzene

J J

UJ UJ UJ UJ UJ UJ UJ UJ UJ UJ UJ UJ UJ UJ UJ

GW 3 BH21774 Toluene, Benzene, Ethylbenzene, Naphthalene, Styrene, 1,3,5-Trimethylbenzene Vinyl Chloride,

Cis-1,2-Dichloroethene, M&p-Xylene, Trichloroethene, o-Xylene, 1,2,4-Trimethylbenzene

Trans-1,2-Dichloroethene, Bromomethane,

J J J J

UJ



Compound Action

Chloromethane, 1,1-Dichloroethene 1,1-Dichloroethane, Chloroform 1,1,1-Trichloroethane

1,1-Dichloropropene Carbon Tetrachloride, Tetrachloroethene Chlorobenzene, 1,1,1,2-Tetrachloroethane

Isopropylbenzene, Bromobenzene, n-Propylbenzene 2-Chlorotoluene, 4-Chlorotoluene, Tert-Butylbenzene

Sec-Butylbenzene, 1,3-Dichlorobenzene p-Isopropyltoluene, 1,4-Dichlorobenzene

n-Butylbenzene, 1,2-Dichlorobenzene 1,2,4-Trichlorobenzene Hexachlorobutadiene


UJ UJ UJ UJ UJ UJ UJ UJ UJ UJ UJ UJ

GW 4 BH21775 Benzene, Ethylbenzene, Toluene, M&p-Xylene, o-Xylene, Styrene,

n-Propylbenzene 1,3,5-Trimethylbenzene Chloromethane,Vinyl Chloride, Naphthalene, 1,2,4-Trimethylbenzene, Isopropylbenzene,

p-Isopropyltoluene Cis-1,2-Dichloroethene, Trichloroethene,

Trans-1,2-Dichloroethene, Bromomethane, 1,1-Dichloroethene, 1,1-Dichloroethane, Chloroform

1,1,1-Trichloroethane, 1,1-Dichloropropene Carbon Tetrachloride, Tetrachloroethene Chlorobenzene, 1,1,1,2-Tetrachloroethane

Bromobenzene, 2-Chlorotoluene, 4-Chlorotoluene, Tert-Butylbenzene, Sec-Butylbenzene,

1,3-Dichlorobenzene,1,4-Dichlorobenzene n-Butylbenzene, 1,2-Dichlorobenzene,

1,2,4-Trichlorobenzene Hexachlorobutadiene, 1,2,3-Trichlorobenzene

J J J J J J

UJ UJ UJ UJ UJ UJ UJ UJ UJ UJ UJ UJ



limits. No qualifications were required.


Method Blank (MB), Storage Blank (SB), Trip Blank (TB), Field Blank (FB), Rinsate Blank (RB) and Equipment Blank (EB): 1. Method Blank (BLANK BH21734) was analyzed on 10/03/2014.




(g/L)

Sample Affected

Action

METHOD BLANK BH21734

Acetone 0.50 10 GW1, GW4 GW3

U None

Carbon Disulfide 0.36 1 GW1 GW3, GW4

U None

Methylene Chloride 0.34 6 GW1, GW3 GW4

None U

1,2,4-Trichlorobenzene 0.20 1 GW1, GW3, GW4 None Naphthalene 0.25 0.19 GW1, GW3, GW4 None 1,2,3-Trichlorobenzene 0.32 1 GW1, GW3, GW4 None

Laboratory Control Sample (LCS)/ Laboratory Control Sample Duplicate (LCSD):

1. Laboratory Control Sample and Laboratory Control Sample Duplicate associated with Batch ID: BH21734 were analyzed on 10/03/2014. All %RECs and RPDs were within the laboratory control limits. No qualifications were required.

Field Duplicate: 1. A field duplicate pair was not submitted with this SDG. Matrix Spike (MS)/ Matrix Spike Duplicate (MSD): 1. Matrix Spike (MS)/Matrix Spike Duplicate (MSD) were not performed on sample from





were required. 2. Manual Calculation: Cx = (Ax)(IS)(DF)

(Ais)(RRF)(V)


GW1 (BH21773) Trichloroethene Sample Volume= 25ml Volume purged=25ml DF = 1 Concentration (g/L)= 215457 x 25 x 10 x 1 = 17.8g/L 356750 x 0.339 x 25

Compound Laboratory

(g/L) Validation

(g/L) %D

Trichloroethene 18 18 0.0


Comments: 1. Volatile data package meet requirement for New York State Department of


2. Validation qualifiers (if required) were entered into the EDD for SDG: GBH21773. 3. Summary of the qualified data is listed in the Data Summary Table for SDG: GBH21773.



SDG: GBH21773


GW1 BH21773 SW8260 10/3/2014 1 1,1,1,2-Tetrachloroethane ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 1,1,1-Trichloroethane ug/L UJ 5.0GW1 BH21773 SW8260 10/3/2014 1 1,1-Dichloroethane ug/L UJ 5.0GW1 BH21773 SW8260 10/3/2014 1 1,1-Dichloroethene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 1,1-Dichloropropene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 1,2,3-Trichlorobenzene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 1,2,4-Trichlorobenzene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 1,2,4-Trimethylbenzene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 1,2-Dichlorobenzene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 1,3,5-Trimethylbenzene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 1,3-Dichlorobenzene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 1,4-Dichlorobenzene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 2-Chlorotoluene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 4-Chlorotoluene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 Benzene 0.32 ug/L J 0.70GW1 BH21773 SW8260 10/3/2014 1 Bromobenzene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 Bromomethane ug/L UJ 5.0GW1 BH21773 SW8260 10/3/2014 1 Carbon tetrachloride ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 Chlorobenzene ug/L UJ 5.0GW1 BH21773 SW8260 10/3/2014 1 Chloroform ug/L UJ 5.0GW1 BH21773 SW8260 10/3/2014 1 Chloromethane ug/L UJ 5.0GW1 BH21773 SW8260 10/3/2014 1 cis-1,2-Dichloroethene 18 ug/L J 1.0GW1 BH21773 SW8260 10/3/2014 1 Ethylbenzene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 Hexachlorobutadiene ug/L UJ 0.50GW1 BH21773 SW8260 10/3/2014 1 Hexachlorobutadiene ug/L UJ 0.50GW1 BH21773 SW8260 10/3/2014 1 Isopropylbenzene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 m&p-Xylene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 Naphthalene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 n-Butylbenzene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 n-Propylbenzene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 o-Xylene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 p-Isopropyltoluene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 sec-Butylbenzene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 Styrene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 tert-Butylbenzene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 Tetrachloroethene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 Toluene ug/L UJ 1.0GW1 BH21773 SW8260 10/3/2014 1 trans-1,2-Dichloroethene 0.98 ug/L J 5.0GW1 BH21773 SW8260 10/3/2014 1 Trichloroethene 18 ug/L J 1.0GW1 BH21773 SW8260 10/3/2014 1 Vinyl chloride 2.5 ug/L J 1.0GW3 BH21774 SW8260 10/3/2014 50 1,1,1,2-Tetrachloroethane ug/L UJ 50

Page 1 of 3



SDG: GBH21773


GW3 BH21774 SW8260 10/3/2014 50 1,1,1-Trichloroethane ug/L UJ 250GW3 BH21774 SW8260 10/3/2014 50 1,1-Dichloroethane ug/L UJ 250GW3 BH21774 SW8260 10/3/2014 50 1,1-Dichloroethene ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 50 1,1-Dichloropropene ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 50 1,2,3-Trichlorobenzene ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 50 1,2,4-Trichlorobenzene ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 50 1,2,4-Trimethylbenzene 380 ug/L J 50GW3 BH21774 SW8260 10/3/2014 50 1,2-Dichlorobenzene ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 50 1,3,5-Trimethylbenzene 180 ug/L J 50GW3 BH21774 SW8260 10/3/2014 50 1,3-Dichlorobenzene ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 50 1,4-Dichlorobenzene ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 50 2-Chlorotoluene ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 50 4-Chlorotoluene ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 400 Benzene 4300 ug/L J 280GW3 BH21774 SW8260 10/3/2014 50 Bromobenzene ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 50 Bromomethane ug/L UJ 250GW3 BH21774 SW8260 10/3/2014 50 Carbon tetrachloride ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 50 Chlorobenzene ug/L UJ 250GW3 BH21774 SW8260 10/3/2014 50 Chloroform ug/L UJ 250GW3 BH21774 SW8260 10/3/2014 50 Chloromethane ug/L UJ 250GW3 BH21774 SW8260 10/3/2014 50 cis-1,2-Dichloroethene 470 ug/L J 50GW3 BH21774 SW8260 10/3/2014 50 Ethylbenzene 350 ug/L J 50GW3 BH21774 SW8260 10/3/2014 50 Hexachlorobutadiene ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 50 Isopropylbenzene ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 50 Isopropylbenzene ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 50 m&p-Xylene 1600 ug/L J 50GW3 BH21774 SW8260 10/3/2014 400 Naphthalene 9400 ug/L J 400GW3 BH21774 SW8260 10/3/2014 50 n-Butylbenzene ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 50 n-Propylbenzene ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 50 o-Xylene 570 ug/L J 50GW3 BH21774 SW8260 10/3/2014 50 p-Isopropyltoluene ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 50 sec-Butylbenzene ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 50 Styrene 270 ug/L J 50GW3 BH21774 SW8260 10/3/2014 50 tert-Butylbenzene ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 50 Tetrachloroethene ug/L UJ 50GW3 BH21774 SW8260 10/3/2014 400 Toluene 3800 ug/L J 400GW3 BH21774 SW8260 10/3/2014 50 trans-1,2-Dichloroethene ug/L UJ 250GW3 BH21774 SW8260 10/3/2014 50 Trichloroethene 27 ug/L J 50GW3 BH21774 SW8260 10/3/2014 50 Vinyl chloride 530 ug/L J 50GW4 BH21775 SW8260 10/3/2014 5 1,1,1,2-Tetrachloroethane ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 5 1,1,1-Trichloroethane ug/L UJ 5.0

Page 2 of 3



SDG: GBH21773


GW4 BH21775 SW8260 10/3/2014 5 1,1-Dichloroethane ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 5 1,1-Dichloroethene ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 5 1,1-Dichloropropene ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 5 1,2,3-Trichlorobenzene ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 5 1,2,4-Trichlorobenzene ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 5 1,2,4-Trimethylbenzene 110 ug/L J 5.0GW4 BH21775 SW8260 10/3/2014 5 1,2-Dichlorobenzene ug/L UJ 4.0GW4 BH21775 SW8260 10/3/2014 5 1,3,5-Trimethylbenzene 52 ug/L J 5.0GW4 BH21775 SW8260 10/3/2014 5 1,3-Dichlorobenzene ug/L UJ 3.0GW4 BH21775 SW8260 10/3/2014 5 1,4-Dichlorobenzene ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 5 2-Chlorotoluene ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 5 4-Chlorotoluene ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 100 Benzene 730 ug/L J 70GW4 BH21775 SW8260 10/3/2014 5 Bromobenzene ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 5 Bromomethane ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 5 Carbon tetrachloride ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 5 Chlorobenzene ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 5 Chloroform ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 5 Chloromethane 1.4 ug/L J 5.0GW4 BH21775 SW8260 10/3/2014 5 cis-1,2-Dichloroethene ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 25 Ethylbenzene 270 ug/L J 25GW4 BH21775 SW8260 10/3/2014 5 Hexachlorobutadiene ug/L UJ 1.0GW4 BH21775 SW8260 10/3/2014 5 Isopropylbenzene 15 ug/L J 5.0GW4 BH21775 SW8260 10/3/2014 25 m&p-Xylene 520 ug/L J 25GW4 BH21775 SW8260 10/3/2014 25 m&p Xylene 520 ug/L J 25GW4 BH21775 SW8260 10/3/2014 100 Naphthalene 2000 ug/L J 100GW4 BH21775 SW8260 10/3/2014 5 n-Butylbenzene ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 5 n-Propylbenzene 1.4 ug/L J 5.0GW4 BH21775 SW8260 10/3/2014 25 o-Xylene 230 ug/L J 25GW4 BH21775 SW8260 10/3/2014 5 p-Isopropyltoluene 1.6 ug/L J 5.0GW4 BH21775 SW8260 10/3/2014 5 sec-Butylbenzene ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 5 Styrene 13 ug/L J 5.0GW4 BH21775 SW8260 10/3/2014 5 tert-Butylbenzene ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 5 Tetrachloroethene ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 25 Toluene 630 ug/L J 25GW4 BH21775 SW8260 10/3/2014 5 trans-1,2-Dichloroethene ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 5 Trichloroethene ug/L UJ 5.0GW4 BH21775 SW8260 10/3/2014 5 Vinyl chloride 4.3 ug/L J 5.0

Page 3 of 3



USEPA Region II –Data Validation Project Name: 510 Driggs Avenue Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBH21768 Client: Environmental Business Consultants Date: 12/23/2015 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for two (2) soil samples analyzed for Semi-

volatiles by SW-846 Method 8270D in accordance with the NYSDEC, Analytical Services Protocol (ASP) Format.


Environmental Laboratories, Inc., Manchester, CT on 10/01/2014 for analysis. 3. The USEPA Region-II SOP HW-22, Revision 4, August 2008, Validating Semivolatile







Collection Date


B3 18-20 BH21768 9/30/14 SVO Soil B4 23-25 BH21772 9/30/14 SVO Soil





abundance criteria. No qualifications were required. Initial Calibration: 1. Initial calibration curve analyzed on 09/26/2014 (CHEM05) exhibited acceptable %RSDs


Compound %D Benzidine 26.7

Client Sample

ID Laboratory Sample ID

Compound Action

B4 23-25 BH21772 Benzidine UJ


2. Initial calibration curve analyzed on 09/24/2014 (CHEM19) exhibited acceptable %RSDs (40.0%) for CCC compounds and average RRF values for SPCC compounds. Also, %RSDs for all other compounds were 20.0% and average RRF (>0.050). No qualifications were required.

Continuing Calibration Verification (CCV): 1. CCV analyzed on 10/01/2014 @ 21:37PM (CHEM05) exhibited acceptable %Ds




3. CCV analyzed on 10/02/2014 @ 08:42PM (CHEM19) exhibited acceptable %Ds (40.0%) for CCC compounds and RRF values for SPCC compounds. Also, %Ds for all other compounds were 25.0%. No qualifications were required.



Surrogates: 1. All surrogate %REC values in the original extracts were within the QC acceptance limits.

No qualifications were required. Note: Surrogates were diluted out of sample B3 18-20 and therefore could not be evaluated for surrogate recoveries.

Internal Standard (IS) Area Performance: 1. All samples exhibited acceptable area count for all six internal standards. No


Method Blank (MB), Storage Blank (SB), Trip Blank (TB), Field Blank (FB), Rinsate Blank (RB) and Equipment Blank (EB): 1. Method Blank (BH21772 BLANK) associated with the soil samples extracted on




Batch ID: BH21772 were analyzed on 10/01/2014. All %RECs and RPDs were within the laboratory control limits with the following exception(s):


Affected Action

Benzoic Acid 6/13/69.4 B4 23-25 R 2,4-Dinitrophenol 11/16/A B4 23-25 UJ

4-Nitrophenol A/A/32.8 B4 23-25 UJ

Benzidine 18/A/58.8 B4 23-25 UJ(1)

Indeno(1,2,3-cd)pyrene A/A/33.3 B4 23-25 UJ

Dibenz(a,h)anthracene A/A/33.3 B4 23-25 UJ

Benzo(ghi)perylene A/A/31.8 B4 23-25 UJ

A= Acceptable (1) Result for this compound was previously qualified due to ICV criteria.

Field Duplicate: 1. A field duplicate pair was not submitted with this SDG. Matrix Spike (MS)/Matrix Spike Duplicate (MSD):

1. Matrix Spike (MS)/Matrix Spike Duplicate (MSD) were performed on sample B4 23-25 (BH21772). All %RECs/RPDs were within the laboratory control limits with the following exception(s):


Affected Action

Benzoic Acid 2/5/72.2 B4 23-25 R(1)

2,4-Dinitrophenol 23/29/A B4 23-25 UJ(2)

4-Nitrophenol 131/134/A B4 23-25 None

2-Nitroaniline A/136/A B4 23-25 None

A= Acceptable (1) Result for this compound was qualified for very low LCS recovery. (2) Result for this compound was qualified for LCS criteria.




2. Sample compound spectra were compared against the laboratory standard spectra. 3. No QC deviations were observed. Compound Quantitation and Reported Detection Limits: 1. All sample results were reported within the linear calibration range. 2. %Solids for all soil samples in this SDG were >50%. No qualifications were required. 3. Manual Calculation:

Cx = (Ax)(IS)(VE)(DF) (Ais)(RRF)(Volume injected, L)(V)(%Solids)

Cx = concentration of analyte as ug/kg Ax = Area of the characteristic ion for the compound to be measured, counts. Ais = Area of the characteristic ion for the specific internal standard, counts. IS = Concentration of the internal standard spiking mixture, ng RRF= Mean relative response factor from the initial calibration. DF = Dilution factor calculated. If no dilution is performed, DF= 1 V= Volume for liquids in ml, weight for soils/solids in grams. VE= final volume of concentrated extract Sample: 10-01-14LCS (BH21772)

Naphthalene Sample weight: 15.0g Final volume: 1ml Dilution Factor: 1 Concentration (g/kg)(dry) = 1867934 x 40 x 1ml x 1000 = 2143.94g/kg 2240470 x 1.037 x 15.0g

Compound Laboratory

(g/kg) Validation

(g/kg) %D

Naphthalene 2145 2145 0.0


Comments: 1. Semivolatile data package meet requirement for New York State Department of





USEPA Region II –Data Validation Project Name: 510 Driggs Avenue Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBH21768 Client: Environmental Business Consultants Date: 12/23/2015 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for two (2) soil samples analyzed for Volatiles

by SW-846 Method 8260B in accordance to NYSDEC, Analytical Services Protocol (ASP) Format.









Collection Date


B3 18-20 BH21768 9/30/14 VOA Soil B4 23-25 BH21772 9/30/14 VOA Soil



Holding Times: 1. All soil samples were analyzed within 14days from sample collection. No qualifications

were required. GC/MS Tuning: 1. All of the BFB tunes in the initial and continuing calibrations met the percent relative



Compound RRF %RSD Chloroethane A 25.2

2,2-Dichloropropane A 22.6 Trans-1,4-Dichloro-2-butene A 37.9

Hexachlorobutadiene A 24.0 A= Acceptable


Client Sample ID


Compound Action

B3 18-20 BH21768 None None B4 23-25 BH21772 Trans-1,4-dichloro-2-butene, 2,2-Dichloropropane,

chloroethane, hexachlorobutadiene UJ

2. Initial calibration curve analyzed on 10/02/2014 (Chem18) exhibited acceptable %RSDs (30.0%) for CCC compounds and average RRF values for SPCC compounds. Also, %RSDs for all other compounds were 20.0% and average RRF (>0.050). No qualifications were required.

Continuing Calibration Verification (CCV):



Compound RRF %D

Methylene Chloride A -41.8 2,2-Dichloropropane A -25.4 1,1,1-Trichloroethane A -21.2 Methyl t-Butyl Ether A -20.3 Carbon Tetrachloride A -27.2 4-Methyl-2-Pentanone A -21.1

Trans-1,3-Dichloropropene A -24.0 1,2-Dibromomethane A -20.9

2-Hexanone A -20.6 Dibromochloromethane A -33.7

1,1,1,2-Tetrachloroethane A -25.9 Bromoform A -43.9

1,2,3-Trichloropropane A -22.7 Trans-1,4-Dichloro-2-butene(1) A -39.3 1,2-Dibromo-3-chloropropane A -46.3

Naphthalene A -22.7 A= Acceptable

(1) Results for this compound were qualified by beginning CCV.


Client Sample ID


Compound Action

B3 18-20 BH21768 Methylene Chloride 2,2-Dichloropropane

1,1,1-Trichloroethane, Methyl t-Butyl Ether Carbon Tetrachloride, 4-Methyl-2-Pentanone

Trans-1,3-Dichloropropene, 1,2-Dibromomethane, 2-Hexanone Dibromochloromethane, 1,1,1,2-Tetrachloroethane Bromoform,

1,2,3-Trichloropropane Trans-1,4-Dichloro-2-butene, 1,2-Dibromo-3-chloropropane

J UJ UJ UJ UJ UJ UJ UJ

B4 23-25 BH21772 Methylene Chloride, 2,2-Dichloropropane, 1,1,1-Trichloroethane, Methyl t-Butyl Ether,

Carbon Tetrachloride, 4-Methyl-2-Pentanone, Trans-1,3-Dichloropropene, 1,2-Dibromomethane, 2-Hexanone,

Dibromochloromethane, 1,1,1,2-Tetrachloroethane, Bromoform, 1,2,3-Trichloropropane,

Trans-1,4-Dichloro-2-butene, 1,2-Dibromo-3-chloropropane, Naphthalene

UJ





Surrogates: 1. All surrogates %RECs values for all soil samples and associated QC were within the

laboratory control limits. No qualifications were required. Internal Standard (IS) Area Performance: 1. All samples exhibited acceptable area count for all three internal standards within the QC

limits. No qualifications were required. Method Blank (MB), Storage Blank (SB), Trip Blank (TB), Field Blank (FB), Rinsate Blank (RB) and Equipment Blank (EB): 1. Method Blank (BH20148 Blank) analyzed on 10/02/2014.



Compound Results (g/Kg)


(g/Kg)

Sample Affected

Action

BLANK BH20148 Carbon Disulfide 0.81 5.0 B3 18-20 B4 23-25

None U

Methylene Chloride 2.7 10 B3 18-20 B4 23-25

None U

2. Method Blank (BH21472 Blank) analyzed on 10/02/2014.


Compound Results (g/Kg)

Action Level

(2x CRQL) (g/Kg)

Sample Affected

Action

BLANK BH21472 Methylene Chloride 1.8 5 B3 18-20 None Laboratory Control Sample (LCS)/ Laboratory Control Sample Duplicate (LCSD): 1. Laboratory Control Sample associated with Batch ID: BH20148 were analyzed on

10/02/2014. All %RECs were within the laboratory control limits with the following exception(s):

Compound %R Sample

Affected Action

Chloromethane 137 B4 23-25 None Trans-1,4-Dichloro-2-butene 134 B4 23-25 None

A= Acceptable 2. Laboratory Control Sample and Laboratory Control Sample Duplicate associated with

Batch ID: BH21472 were analyzed on 10/02/2014. All %RECs and RPDs were within the laboratory control limits. No qualifications were required.

Field Duplicate: 1. A field duplicate pair was not submitted with this SDG. Matrix Spike (MS)/ Matrix Spike Duplicate (MSD): 1. Matrix Spike (MS)/Matrix Spike Duplicate (MSD) were not performed on a sample from

this SDG.





were required. 2. %Solids for all soil samples in this SDG were >50%. No qualifications were required. 3. Manual Calculation: Cx = (Ax)(IS)(DF)

(Ais)(RRF)(V)(%Solids)

Cx = concentration of analyte as ug/kg Ax = Area of the characteristic ion for the compound to be measured, counts. Ais = Area of the characteristic ion for the specific internal standard, counts. IS = Concentration of the internal standard spiking mixture, ng RRF= Mean relative response factor from the initial calibration. DF = Dilution factor calculated. If no dilution is performed, DF= 1 V= Volume for liquids in ml, weight for soils/solids in grams.

B4 23-25 (BH21772) Benzene Sample weight= 3.62g Volume purged=5.0ml DF = 1 %Solids=90% Concentration (g/kg) (dry) = 27437 x50 x1x 5.0 = 4.97g/kg 296551 x 1.428 x 3.62 x 0.90

Compound Laboratory

(g/kg) Validation

(g/kg) %D

Benzene 5.0 5.0 0.0


Comments: 1. Volatile data package meet requirement for New York State Department of





USEPA Region II –Data Validation Project Name: 510 Driggs Avenue Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBH21768 Client: Environmental Business Consultants Date: 12/23/2015 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for three (3) soil samples analyzed for the

following analyses:

1.1 Trace Metals-ICP-AES by SW-846 Method 6010C (including TCLP by SW-846 Method 1311 for lead). 1.2 Mercury by SW-846 Method 7471A.



Metals for Contract Laboratory Program (CLP), based on SOW-ILM05.3 (SOP Revision 13) was used in evaluating the Trace Metals data in this summary report.






Collection Date


B1 0-2 BH21769 9/30/14 ICP (including TCLP Pb) and CVAA

Soil


Soil


Soil



Holding Times: 1. All soil samples (including TCLP lead) were analyzed within the 6 months holding times

for Trace Metals analysis by ICP-AES. No qualifications were required. 2. All soil samples (including TCLP lead) were digested and analyzed within the 28 days

holding times for Mercury analysis. No qualifications were required. Initial and Continuing Calibration Verification (ICV and CCV): ICP-AES (including TCLP lead): 1. All %RECs in the ICV and CCVs were within QC limits (90-110%). No qualifications

were required. Mercury: 1 All correlation coefficient for Mercury calibration curve analyzed were 0.995. No




CRQL Check Standard (CRI): 1. All CRI %RECs were within the control limits (70-130%). No qualifications were

required. ICP-AES Interference Check Sample: 1. All %REC values were within the QC limits (80-120%) for ICSA and ICSAB. No

qualifications were required. . Blanks (Method Blank, ICB and CCB): ICP-AES: 1. Method Blank-Soil (BH21769) digested on 10/01/2014 was free of contamination. No

qualifications were required. 2. All ICB and CCBs were free of contamination. No qualifications were required. Mercury: 1. All ICB and CCBs were free of contamination. No qualifications were required. 2. Method Blank (BH21323) digested on 10/02/2014 was free of contamination. No

qualifications were required. ICP-AES (TCLP lead): 1. Method Blank-Soil (BH21771) digested on 10/02/2014 was free of contamination. No

qualifications were required. 2. All ICB and CCBs contained low levels of TCLP lead (1 µg/L). Sample results were

either non-detect or greater than the detected blank level. No qualifications were required.

Field Blank (FB) and Equipment Blank (EB): 1. Field Blanks were not submitted with this SDG.


Laboratory Control Sample (LCS)/ Laboratory Control Sample Duplicate (LCSD): ICP-AES (including TCLP lead) and Mercury: 1. Laboratory Control Sample %RECs were within the laboratory control limits (75-125%).

No qualifications were required. Field Duplicate: 1. A field duplicate pair was not submitted with this SDG. Matrix Spike (MS)/ Matrix Spike Duplicate (MSD): ICP-AES and Mercury: 1. Matrix Spike (MS) was performed on sample B1 0-2 (BH21769). All %Rs were within

the laboratory control limits with the following exception(s):

Element %R Sample Affected

Action

Barium 290/A B1 0-2 J+ ICP-AES (TCLP lead): 1. Matrix Spike (MS) was performed on sample B4 0-2 (BH21771). All %Rs were within

the laboratory control limits. No qualifications were required. Sample Duplicate: ICP-AES and Mercury: 1. Sample Duplicate was performed on sample B1 0-2 (BH21769). All RPDs were within

the laboratory control limits. No qualifications were required. ICP-AES (TCLP lead): 1. Sample Duplicate was performed on sample B4 0-2 (BH21771). All RPDs were within

the laboratory control limits. No qualifications were required.


ICP-AES Serial Dilution: 1. ICP serial dilution was performed on sample B1 0-2 (BH21769). For all results for which

the concentration in the original sample is ≥ 50x the Method Detection Limits (MDL), the serial dilution analysis (a five-fold dilution) was within the acceptable limit (%D 10%). No qualifications were required.

2. ICP serial dilution for TCLP lead was performed on sample B4 0-2 (BH21771). For all

results for which the concentration in the original sample is ≥ 50x the Method Detection Limits (MDL), the serial dilution analysis (a five-fold dilution) was within the acceptable limit (%D 10%). No qualifications were required.



Compound Quantitation and Reported Detection Limits: 1. All sample results were reported within the linear calibration range. 2. %Solids for all soil samples in this SDG were >50%. No qualifications were required. 3. Manual calculation: Sample: B3 0-2 (BH21770) Barium Concentration (mg/Kg) (dry wt.)= C x V x DF x 1Lx 1000gx 1mg W x S x 1000ml x 1 kg x 1000ug V= 50ml W= 0.76g %Solids =91.0 DF=1.0 Concentration (mg/Kg) (dry wt.)= 1135.883ug/L x 50 x 1.0 x 1Lx 1000gx 1mg = 82.12 mg/kg 0.76 x 0.91 x 1000ml x 1 kg x 1000ug


Compound Laboratory

(mg/kg) Validation

(mg/kg) %D

Barium 82.1 82.1 0.0 Comments: 1. Trace Metals data package meet requirement for New York State Department of






Project Name: 510 Driggs Avenue Location: Brooklyn, New York Project Number: 3020-017 SDG #: GBH21768 Client: Environmental Business Consultants Date: 12/23/2015 Laboratory: Phoenix Environmental Laboratories, Inc. Reviewer: Sherri Pullar Summary: 1. Data validation was performed on the data for three (3) soil samples analyzed for PCBs



Environmental Laboratories, Inc., Manchester, CT on 10/01/2014 for analysis. 3. The USEPA Region-II SOP HW-45, Revision 1, October 2006, Validating PCBs

compounds by Gas Chromatography, SW-846 Method 8082A was used in evaluating the PCBs data in this summary report.






Collection Date


B1 0-2 BH21769 9/30/14 PCBs Soil B3 0-2 BH21770 9/30/14 PCBs Soil B4 0-2 BH21771 9/30/14 PCBs Soil Sample Conditions/Problems: 1. The Traffic Reports/Chain-of-Custody Records, Sampling Report and/or Laboratory Case




(20.0%) on both columns. No qualifications were required. Continuing Calibration Verification (CCV): 1. All CCVs analyzed on 10/02/2014 exhibited acceptable %Ds (15.0%) for all

compounds. No qualifications were required. Surrogates: 1. All surrogates %RECs values for all soil samples and associated QC were within the

laboratory control limits. No qualifications were required.


Method Blank (MB), Storage Blank (SB), Trip Blank (TB), Field Blank (FB), Rinsate Blank (RB) and Equipment Blank (EB): 1. Method Blank (BH21770 BL) associated with the soil samples extracted on 10/01/2014


ID: GBH21770 were analyzed on 10/02/2014. All %RECs and RPDs were within the laboratory control limits. No qualifications were required.

Field Duplicate: 1. A field duplicate pair was not submitted with this SDG. Matrix Spike (MS)/ Matrix Spike Duplicate (MSD):

1. Matrix Spike (MS)/Matrix Spike Duplicate (MSD) were performed on sample B3 0-2 (BH21770). All %RECs/RPDs were within the laboratory control. No qualifications were required.

Compound Quantitation, Compound Identification and Reported Detection Limits: 1. All sample results were reported within the linear calibration range. 2. %Solids for all soil samples in this SDG were >50%. No qualifications were required. 3. Manual Calculation: BH21770 LCS

Aroclor-1260

On Column concentration (B)= 479.9110ng Sample weight= 15.0g DF= 10 Vi= 5ml %Solids= 100%


Concentration (g/kg) (dry) = 479.9110ng x 5ml x10 = 1599.70g/kg 15.0g

Compound Laboratory

(g/kg) Validation

(g/kg) %D

Aroclor-1260 1600 1600 0.0 Comments: 1. PCBs data package meet requirement for New York State Department of Environmental

Conservation (NYSDEC) Analytical Services Protocol (ASP) Category B Deliverables. 2. Validation qualifiers (if required) were entered into the EDD for SDG: GBH21768. 3. Summary of the qualified data is listed in the Data Summary Table for SDG: GBH21768.



SDG: GBH21768

Sample Name Lab ID

Analytical Method Analysis Date

Dilution Factor Analyte Result Unit Qualifier MDL RL

B3 18-20 BH21768 E160.3 10/1/2014 1 SOLIDS, PERCENT 85 %B3 18-20 BH21768 SW8260 10/2/2014 2500 Ethylbenzene 9200 ug/Kg J 2200 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Styrene 12000 ug/Kg J 3500 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 cis-1,3-Dichloropropene ug/Kg U 1300 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,1,1,2-Tetrachloroethane ug/Kg UJ 2000 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 n-Propylbenzene ug/Kg U 2200 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 n-Butylbenzene ug/Kg U 2200 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 4-Chlorotoluene ug/Kg U 1400 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,4-Dichlorobenzene ug/Kg U 1900 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,2-Dichloroethane ug/Kg U 1100 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Acrylonitrile ug/Kg U 6800 24000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,1,1-Trichloroethane ug/Kg UJ 2400 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,3,5-Trimethylbenzene 12000 ug/Kg J 1600 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Bromobenzene ug/Kg U 1600 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Chlorobenzene ug/Kg U 1800 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Tetrahydrofuran (THF) ug/Kg U 11000 24000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,2,4-Trichlorobenzene ug/Kg U 2400 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,2,3-Trichloropropane ug/Kg UJ 1700 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Tetrachloroethene ug/Kg U 2500 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 sec-Butylbenzene ug/Kg U 2300 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,3-Dichloropropane ug/Kg U 1300 12000p p g gB3 18-20 BH21768 SW8260 10/2/2014 2500 cis-1,2-Dichloroethene ug/Kg U 2600 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 trans-1,2-Dichloroethene ug/Kg U 2400 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 2-Isopropyltoluene ug/Kg U 1700 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,3-Dichlorobenzene ug/Kg U 1800 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,2-Dibromo-3-chloropropane ug/Kg UJ 3200 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,1-Dichloropropene ug/Kg U 2300 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,2-Dibromoethane ug/Kg UJ 3200 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Acetone ug/Kg U 12000 120000B3 18-20 BH21768 SW8260 10/2/2014 2500 Chloroform ug/Kg U 2200 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Benzene 43000 ug/Kg 2400 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 2,2-Dichloropropane ug/Kg UJ 2000 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Bromomethane ug/Kg U 9300 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Dibromomethane ug/Kg U 1500 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Bromochloromethane ug/Kg U 1800 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Chloroethane ug/Kg U 2800 12000

Page 1 of 10



SDG: GBH21768

Sample Name Lab ID



B3 18-20 BH21768 SW8260 10/2/2014 2500 Vinyl chloride ug/Kg U 3900 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 2-Hexanone ug/Kg UJ 5400 60000B3 18-20 BH21768 SW8260 10/2/2014 2500 Carbon Disulfide ug/Kg U 2000 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Bromodichloromethane ug/Kg U 1500 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,1-Dichloroethane ug/Kg U 2400 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,1-Dichloroethene ug/Kg U 2600 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Trichlorofluoromethane ug/Kg U 2700 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Dichlorodifluoromethane ug/Kg U 3200 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Trichlorotrifluoroethane ug/Kg U 1900 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,2-Dichloropropane ug/Kg U 1700 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Methyl Ethyl Ketone ug/Kg U 10000 73000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,1,2-Trichloroethane ug/Kg U 1200 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Trichloroethene ug/Kg U 2600 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,1,2,2-Tetrachloroethane ug/Kg U 1700 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,2,3-Trichlorobenzene ug/Kg U 2400 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Hexachlorobutadiene ug/Kg U 2500 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 o-Xylene 18000 ug/Kg 4600 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 2-Chlorotoluene ug/Kg U 1900 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,2-Dichlorobenzene ug/Kg U 1300 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 1,2,4-Trimethylbenzene 21000 ug/Kg 1700 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 4-Methyl-2-pentanone ug/Kg UJ 2900 60000y p g gB3 18-20 BH21768 SW8260 10/2/2014 2500 tert-Butylbenzene ug/Kg U 1900 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Isopropylbenzene ug/Kg U 2300 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 p-Isopropyltoluene ug/Kg U 1700 12000B3 18-20 BH21768 SW8260 10/2/2014 12500 Toluene 91000 ug/Kg 9500 60000B3 18-20 BH21768 SW8260 10/2/2014 12500 m&p-Xylene 82000 ug/Kg 24000 60000B3 18-20 BH21768 SW8260 10/2/2014 12500 Naphthalene 880000 ug/Kg 16000 60000B3 18-20 BH21768 SW8260 10/2/2014 2500 Bromoform ug/Kg UJ 1700 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Carbon tetrachloride ug/Kg UJ 1400 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Chloromethane ug/Kg U 6300 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Dibromochloromethane ug/Kg UJ 1400 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 Methyl t-butyl ether (MTBE) ug/Kg UJ 3300 24000B3 18-20 BH21768 SW8260 10/2/2014 2500 Methylene chloride 5600 ug/Kg J 2000 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 trans-1,3-Dichloropropene ug/Kg UJ 2500 12000B3 18-20 BH21768 SW8260 10/2/2014 2500 trans-1,4-dichloro-2-butene ug/Kg UJ 22000 24000B3 18-20 BH21768 SW8270 10/2/2014 200 4-Nitroaniline ug/Kg U 26000 390000

Page 2 of 10



SDG: GBH21768

Sample Name Lab ID



B3 18-20 BH21768 SW8270 10/2/2014 200 4-Nitrophenol ug/Kg U 35000 390000B3 18-20 BH21768 SW8270 10/2/2014 200 4-Bromophenyl phenyl ether ug/Kg U 23000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 2,4-Dimethylphenol 46000 ug/Kg J 19000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 1,4-Dichlorobenzene ug/Kg U 23000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 4-Chloroaniline ug/Kg U 36000 150000B3 18-20 BH21768 SW8270 10/2/2014 200 Phenol ug/Kg U 25000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Pyridine ug/Kg U 19000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Bis(2-chloroethyl)ether ug/Kg U 21000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Bis(2-chloroethoxy)methane ug/Kg U 21000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Bis(2-ethylhexyl)phthalate ug/Kg U 22000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Di-n-octylphthalate ug/Kg U 20000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Hexachlorobenzene ug/Kg U 23000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Anthracene 190000 ug/Kg 25000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 1,2,4-Trichlorobenzene ug/Kg U 23000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 2,4-Dichlorophenol ug/Kg U 27000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 2,4-Dinitrotoluene ug/Kg U 30000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 1,2-Diphenylhydrazine ug/Kg U 25000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Pyrene 280000 ug/Kg 27000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Dimethylphthalate ug/Kg U 24000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Dibenzofuran 170000 ug/Kg 23000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Benzo(ghi)perylene 30000 ug/Kg J 25000 54000(g )p y g gB3 18-20 BH21768 SW8270 10/2/2014 200 Indeno(1,2,3-cd)pyrene 27000 ug/Kg J 26000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Benzo(b)fluoranthene 100000 ug/Kg 26000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Fluoranthene 330000 ug/Kg 25000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Benzo(k)fluoranthene 37000 ug/Kg J 26000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Acenaphthylene 170000 ug/Kg 22000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Chrysene 120000 ug/Kg 26000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Bis(2-chloroisopropyl)ether ug/Kg U 22000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Benzo(a)pyrene 86000 ug/Kg 25000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 2,4-Dinitrophenol ug/Kg U 54000 390000B3 18-20 BH21768 SW8270 10/2/2014 200 4,6-Dinitro-2-methylphenol ug/Kg U 83000 390000B3 18-20 BH21768 SW8270 10/2/2014 200 Dibenz(a,h)anthracene ug/Kg U 25000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 1,3-Dichlorobenzene ug/Kg U 23000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Benz(a)anthracene 150000 ug/Kg 26000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 4-Chloro-3-methylphenol ug/Kg U 27000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 2,6-Dinitrotoluene ug/Kg U 24000 54000

Page 3 of 10



SDG: GBH21768

Sample Name Lab ID



B3 18-20 BH21768 SW8270 10/2/2014 200 N-Nitrosodi-n-propylamine ug/Kg U 25000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Aniline ug/Kg U 160000 390000B3 18-20 BH21768 SW8270 10/2/2014 200 N-Nitrosodimethylamine ug/Kg U 22000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Benzoic acid ug/Kg U 150000 390000B3 18-20 BH21768 SW8270 10/2/2014 200 Hexachloroethane ug/Kg U 23000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 4-Chlorophenyl phenyl ether ug/Kg U 26000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Hexachlorocyclopentadiene ug/Kg U 24000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Isophorone ug/Kg U 22000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Pentachloronitrobenzene ug/Kg U 29000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Acenaphthene 49000 ug/Kg J 24000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Diethyl phthalate ug/Kg U 24000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Di-n-butylphthalate ug/Kg U 21000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Phenanthrene 660000 ug/Kg 22000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Benzyl butyl phthalate ug/Kg U 20000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 N-Nitrosodiphenylamine ug/Kg U 30000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Fluorene 240000 ug/Kg 26000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Carbazole 120000 ug/Kg J 59000 390000B3 18-20 BH21768 SW8270 10/2/2014 200 Hexachlorobutadiene ug/Kg U 28000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Pentachlorophenol ug/Kg U 29000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 2,4,6-Trichlorophenol ug/Kg U 25000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 2-Nitroaniline ug/Kg U 78000 390000g gB3 18-20 BH21768 SW8270 10/2/2014 200 2-Nitrophenol ug/Kg U 49000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 2-Methylnaphthalene 400000 ug/Kg 23000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 2-Chloronaphthalene ug/Kg U 22000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 3,3'-Dichlorobenzidine ug/Kg U 37000 150000B3 18-20 BH21768 SW8270 10/2/2014 200 Benzidine ug/Kg U 45000 150000B3 18-20 BH21768 SW8270 10/2/2014 200 2-Methylphenol (o-cresol) ug/Kg U 36000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 1,2-Dichlorobenzene ug/Kg U 22000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 2-Chlorophenol ug/Kg U 22000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 1,2,4,5-Tetrachlorobenzene ug/Kg U 27000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 2,4,5-Trichlorophenol ug/Kg U 42000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Acetophenone ug/Kg U 24000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 Nitrobenzene ug/Kg U 27000 54000B3 18-20 BH21768 SW8270 10/2/2014 200 3-Nitroaniline ug/Kg U 170000 390000B3 18-20 BH21768 SW8270 10/2/2014 200 3&4-Methylphenol (m&p-cresol) 53000 ug/Kg J 30000 54000B3 18-20 BH21768 SW8270 10/2/2014 1000 Naphthalene 1100000 ug/Kg 110000 270000

Page 4 of 10



SDG: GBH21768

Sample Name Lab ID



B1 0-2 BH21769 E160.3 10/1/2014 1 SOLIDS, PERCENT 91 %B1 0-2 BH21769 SW6010 10/3/2014 1 TCLP Lead 0.01 mg/L J 0.010 0.10B1 0-2 BH21769 SW6010 10/6/2014 1 Lead 38.4 mg/Kg 0.36 0.7B1 0-2 BH21769 SW6010 10/6/2014 1 Silver mg/Kg U 0.36 0.36B1 0-2 BH21769 SW6010 10/6/2014 1 Arsenic 2.6 mg/Kg 0.71 0.7B1 0-2 BH21769 SW6010 10/6/2014 1 Barium 62.5 mg/Kg J+ 0.36 0.7B1 0-2 BH21769 SW6010 10/6/2014 1 Cadmium mg/Kg U 0.14 0.36B1 0-2 BH21769 SW6010 10/6/2014 1 Chromium 21.2 mg/Kg 0.36 0.36B1 0-2 BH21769 SW6010 10/6/2014 1 Selenium mg/Kg U 1.2 1.4B1 0-2 BH21769 SW7471 10/2/2014 1 Mercury 0.08 mg/Kg 0.04 0.06B1 0-2 BH21769 SW8082 10/2/2014 2 PCB-1260 ug/Kg U 36 36B1 0-2 BH21769 SW8082 10/2/2014 2 PCB-1254 ug/Kg U 36 36B1 0-2 BH21769 SW8082 10/2/2014 2 PCB-1268 ug/Kg U 36 36B1 0-2 BH21769 SW8082 10/2/2014 2 PCB-1221 ug/Kg U 36 36B1 0-2 BH21769 SW8082 10/2/2014 2 PCB-1232 ug/Kg U 36 36B1 0-2 BH21769 SW8082 10/2/2014 2 PCB-1248 ug/Kg U 36 36B1 0-2 BH21769 SW8082 10/2/2014 2 PCB-1016 ug/Kg U 36 36B1 0-2 BH21769 SW8082 10/2/2014 2 PCB-1262 ug/Kg U 36 36B1 0-2 BH21769 SW8082 10/2/2014 2 PCB-1242 ug/Kg U 36 36B3 0-2 BH21770 E160.3 10/1/2014 1 SOLIDS, PERCENT 91 %B3 0-2 BH21770 SW6010 10/3/2014 1 TCLP Lead 0.05 mg/L J 0.010 0.10gB3 0-2 BH21770 SW6010 10/6/2014 1 Lead 84.7 mg/Kg 0.36 0.7B3 0-2 BH21770 SW6010 10/6/2014 1 Silver mg/Kg U 0.36 0.36B3 0-2 BH21770 SW6010 10/6/2014 1 Arsenic 4.6 mg/Kg 0.72 0.7B3 0-2 BH21770 SW6010 10/6/2014 1 Barium 82.1 mg/Kg N 0.36 0.7B3 0-2 BH21770 SW6010 10/6/2014 1 Cadmium 0.17 mg/Kg J 0.14 0.36B3 0-2 BH21770 SW6010 10/6/2014 1 Chromium 21.7 mg/Kg 0.36 0.36B3 0-2 BH21770 SW6010 10/6/2014 1 Selenium mg/Kg U 1.2 1.4B3 0-2 BH21770 SW7471 10/2/2014 1 Mercury 0.19 mg/Kg 0.04 0.06B3 0-2 BH21770 SW8082 10/2/2014 2 PCB-1260 ug/Kg U 36 36B3 0-2 BH21770 SW8082 10/2/2014 2 PCB-1254 ug/Kg U 36 36B3 0-2 BH21770 SW8082 10/2/2014 2 PCB-1268 ug/Kg U 36 36B3 0-2 BH21770 SW8082 10/2/2014 2 PCB-1221 ug/Kg U 36 36B3 0-2 BH21770 SW8082 10/2/2014 2 PCB-1232 ug/Kg U 36 36B3 0-2 BH21770 SW8082 10/2/2014 2 PCB-1248 ug/Kg U 36 36B3 0-2 BH21770 SW8082 10/2/2014 2 PCB-1016 ug/Kg U 36 36

Page 5 of 10



SDG: GBH21768

Sample Name Lab ID



B3 0-2 BH21770 SW8082 10/2/2014 2 PCB-1262 ug/Kg U 36 36B3 0-2 BH21770 SW8082 10/2/2014 2 PCB-1242 ug/Kg U 36 36B4 0-2 BH21771 E160.3 10/1/2014 1 SOLIDS, PERCENT 90 %B4 0-2 BH21771 SW6010 10/3/2014 1 TCLP Lead mg/L U 0.010 0.10B4 0-2 BH21771 SW6010 10/6/2014 1 Lead 89.1 mg/Kg 0.39 0.8B4 0-2 BH21771 SW6010 10/6/2014 1 Silver mg/Kg U 0.39 0.39B4 0-2 BH21771 SW6010 10/6/2014 1 Arsenic 3.1 mg/Kg 0.78 0.8B4 0-2 BH21771 SW6010 10/6/2014 1 Barium 111 mg/Kg N 0.39 0.8B4 0-2 BH21771 SW6010 10/6/2014 1 Cadmium mg/Kg U 0.16 0.39B4 0-2 BH21771 SW6010 10/6/2014 1 Chromium 18.3 mg/Kg 0.39 0.39B4 0-2 BH21771 SW6010 10/6/2014 1 Selenium mg/Kg U 1.3 1.6B4 0-2 BH21771 SW7471 10/2/2014 1 Mercury 0.17 mg/Kg 0.05 0.08B4 0-2 BH21771 SW8082 10/2/2014 2 PCB-1260 ug/Kg U 36 36B4 0-2 BH21771 SW8082 10/2/2014 2 PCB-1254 ug/Kg U 36 36B4 0-2 BH21771 SW8082 10/2/2014 2 PCB-1268 ug/Kg U 36 36B4 0-2 BH21771 SW8082 10/2/2014 2 PCB-1221 ug/Kg U 36 36B4 0-2 BH21771 SW8082 10/2/2014 2 PCB-1232 ug/Kg U 36 36B4 0-2 BH21771 SW8082 10/2/2014 2 PCB-1248 ug/Kg U 36 36B4 0-2 BH21771 SW8082 10/2/2014 2 PCB-1016 ug/Kg U 36 36B4 0-2 BH21771 SW8082 10/2/2014 2 PCB-1262 ug/Kg U 36 36B4 0-2 BH21771 SW8082 10/2/2014 2 PCB-1242 ug/Kg U 36 36g gB4 23-25 BH21772 E160.3 10/1/2014 1 SOLIDS, PERCENT 90 %B4 23-25 BH21772 SW8260 10/2/2014 1 1,1,1,2-Tetrachloroethane ug/Kg UJ 1.3 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 1,1,1-Trichloroethane ug/Kg UJ 1.5 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 1,2,3-Trichloropropane ug/Kg UJ 1.1 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 1,2-Dibromo-3-chloropropane ug/Kg UJ 2.1 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 1,2-Dibromoethane ug/Kg UJ 2.0 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 2,2-Dichloropropane ug/Kg UJ 1.3 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 2-Hexanone ug/Kg UJ 3.5 38B4 23-25 BH21772 SW8260 10/2/2014 1 4-Methyl-2-pentanone ug/Kg UJ 1.8 38B4 23-25 BH21772 SW8260 10/2/2014 1 Ethylbenzene ug/Kg U 1.4 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Styrene ug/Kg U 2.2 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 cis-1,3-Dichloropropene ug/Kg U 0.83 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 n-Propylbenzene ug/Kg U 1.4 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 n-Butylbenzene ug/Kg U 1.4 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 4-Chlorotoluene ug/Kg U 0.89 7.7

Page 6 of 10



SDG: GBH21768

Sample Name Lab ID



B4 23-25 BH21772 SW8260 10/2/2014 1 1,4-Dichlorobenzene ug/Kg U 1.2 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Bromoform ug/Kg UJ 1.1 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 1,2-Dichloroethane ug/Kg U 0.67 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Acrylonitrile ug/Kg U 4.3 15B4 23-25 BH21772 SW8260 10/2/2014 1 1,3,5-Trimethylbenzene ug/Kg U 1.0 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Bromobenzene ug/Kg U 1.0 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Toluene ug/Kg U 1.2 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Chlorobenzene ug/Kg U 1.1 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Tetrahydrofuran (THF) ug/Kg U 6.9 15B4 23-25 BH21772 SW8260 10/2/2014 1 Carbon tetrachloride ug/Kg UJ 0.89 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 1,2,4-Trichlorobenzene ug/Kg U 1.5 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Tetrachloroethene ug/Kg U 1.6 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 sec-Butylbenzene ug/Kg U 1.4 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 1,3-Dichloropropane ug/Kg U 0.81 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 cis-1,2-Dichloroethene ug/Kg U 1.7 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 trans-1,2-Dichloroethene ug/Kg U 1.5 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Chloromethane ug/Kg U 4.0 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 m&p-Xylene ug/Kg U 3.0 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 2-Isopropyltoluene ug/Kg U 1.1 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 1,3-Dichlorobenzene ug/Kg U 1.1 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 1,1-Dichloropropene ug/Kg U 1.5 7.7p p g gB4 23-25 BH21772 SW8260 10/2/2014 1 Dibromochloromethane ug/Kg UJ 0.86 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Methyl t-butyl ether (MTBE) ug/Kg UJ 2.1 15B4 23-25 BH21772 SW8260 10/2/2014 1 Acetone ug/Kg U 7.6 50B4 23-25 BH21772 SW8260 10/2/2014 1 Chloroform ug/Kg U 1.4 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Benzene 5.0 ug/Kg J 1.5 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Bromomethane ug/Kg U 5.9 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Methylene chloride 1.5 ug/Kg UJ 1.3 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Dibromomethane ug/Kg U 0.97 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Bromochloromethane ug/Kg U 1.1 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Chloroethane ug/Kg U 1.8 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Vinyl chloride ug/Kg U 2.5 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Naphthalene ug/Kg UJ 2.1 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Carbon Disulfide 2.2 ug/Kg U 1.2 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Bromodichloromethane ug/Kg U 0.95 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 1,1-Dichloroethane ug/Kg U 1.5 7.7

Page 7 of 10



SDG: GBH21768

Sample Name Lab ID



B4 23-25 BH21772 SW8260 10/2/2014 1 1,1-Dichloroethene ug/Kg U 1.7 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Trichlorofluoromethane ug/Kg U 1.7 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Dichlorodifluoromethane ug/Kg U 2.0 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Trichlorotrifluoroethane ug/Kg U 1.2 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 1,2-Dichloropropane ug/Kg U 1.1 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Methyl Ethyl Ketone ug/Kg U 6.7 46B4 23-25 BH21772 SW8260 10/2/2014 1 1,1,2-Trichloroethane ug/Kg U 0.75 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Trichloroethene ug/Kg U 1.6 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 1,1,2,2-Tetrachloroethane ug/Kg U 1.1 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 1,2,3-Trichlorobenzene ug/Kg U 1.5 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Hexachlorobutadiene ug/Kg U 1.6 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 trans-1,3-Dichloropropene ug/Kg UJ 1.6 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 o-Xylene ug/Kg U 2.9 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 2-Chlorotoluene ug/Kg U 1.2 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 1,2-Dichlorobenzene ug/Kg U 0.84 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 1,2,4-Trimethylbenzene 1.6 ug/Kg J 1.1 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 trans-1,4-dichloro-2-butene ug/Kg UJ 14 15B4 23-25 BH21772 SW8260 10/2/2014 1 tert-Butylbenzene ug/Kg U 1.2 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 Isopropylbenzene ug/Kg U 1.5 7.7B4 23-25 BH21772 SW8260 10/2/2014 1 p-Isopropyltoluene ug/Kg U 1.1 7.7B4 23-25 BH21772 SW8270 10/2/2014 1 4-Nitroaniline ug/Kg U 120 1800g gB4 23-25 BH21772 SW8270 10/2/2014 1 4-Nitrophenol ug/Kg UJ 160 1800B4 23-25 BH21772 SW8270 10/2/2014 1 4-Bromophenyl phenyl ether ug/Kg U 110 260B4 23-25 BH21772 SW8270 10/2/2014 1 2,4-Dimethylphenol ug/Kg U 90 260B4 23-25 BH21772 SW8270 10/2/2014 1 1,4-Dichlorobenzene ug/Kg U 110 260B4 23-25 BH21772 SW8270 10/2/2014 1 4-Chloroaniline ug/Kg U 170 730B4 23-25 BH21772 SW8270 10/2/2014 1 Phenol ug/Kg U 120 260B4 23-25 BH21772 SW8270 10/2/2014 1 Pyridine ug/Kg U 90 260B4 23-25 BH21772 SW8270 10/2/2014 1 Bis(2-chloroethyl)ether ug/Kg U 98 260B4 23-25 BH21772 SW8270 10/2/2014 1 Bis(2-chloroethoxy)methane ug/Kg U 100 260B4 23-25 BH21772 SW8270 10/2/2014 1 Bis(2-ethylhexyl)phthalate ug/Kg U 100 260B4 23-25 BH21772 SW8270 10/2/2014 1 Di-n-octylphthalate ug/Kg U 94 260B4 23-25 BH21772 SW8270 10/2/2014 1 Hexachlorobenzene ug/Kg U 110 260B4 23-25 BH21772 SW8270 10/2/2014 1 Anthracene ug/Kg U 120 260B4 23-25 BH21772 SW8270 10/2/2014 1 1,2,4-Trichlorobenzene ug/Kg U 110 260B4 23-25 BH21772 SW8270 10/2/2014 1 2,4-Dichlorophenol ug/Kg U 130 260

Page 8 of 10



SDG: GBH21768

Sample Name Lab ID



B4 23-25 BH21772 SW8270 10/2/2014 1 2,4-Dinitrotoluene ug/Kg U 140 260B4 23-25 BH21772 SW8270 10/2/2014 1 1,2-Diphenylhydrazine ug/Kg U 120 260B4 23-25 BH21772 SW8270 10/2/2014 1 Pyrene ug/Kg U 130 260B4 23-25 BH21772 SW8270 10/2/2014 1 Dimethylphthalate ug/Kg U 110 260B4 23-25 BH21772 SW8270 10/2/2014 1 Dibenzofuran ug/Kg U 110 260B4 23-25 BH21772 SW8270 10/2/2014 1 Benzo(ghi)perylene ug/Kg UJ 120 260B4 23-25 BH21772 SW8270 10/2/2014 1 Indeno(1,2,3-cd)pyrene ug/Kg UJ 120 260B4 23-25 BH21772 SW8270 10/2/2014 1 Benzo(b)fluoranthene ug/Kg U 120 260B4 23-25 BH21772 SW8270 10/2/2014 1 Fluoranthene ug/Kg U 120 260B4 23-25 BH21772 SW8270 10/2/2014 1 Benzo(k)fluoranthene ug/Kg U 120 260B4 23-25 BH21772 SW8270 10/2/2014 1 Acenaphthylene ug/Kg U 100 260B4 23-25 BH21772 SW8270 10/2/2014 1 Chrysene ug/Kg U 120 260B4 23-25 BH21772 SW8270 10/2/2014 1 Bis(2-chloroisopropyl)ether ug/Kg U 100 260B4 23-25 BH21772 SW8270 10/2/2014 1 Benzo(a)pyrene ug/Kg U 120 260B4 23-25 BH21772 SW8270 10/2/2014 1 2,4-Dinitrophenol ug/Kg UJ 260 1800B4 23-25 BH21772 SW8270 10/2/2014 1 4,6-Dinitro-2-methylphenol ug/Kg U 390 1800B4 23-25 BH21772 SW8270 10/2/2014 1 Dibenz(a,h)anthracene ug/Kg UJ 120 260B4 23-25 BH21772 SW8270 10/2/2014 1 1,3-Dichlorobenzene ug/Kg U 110 260B4 23-25 BH21772 SW8270 10/2/2014 1 Benz(a)anthracene ug/Kg U 120 260B4 23-25 BH21772 SW8270 10/2/2014 1 4-Chloro-3-methylphenol ug/Kg U 130 260B4 23-25 BH21772 SW8270 10/2/2014 1 2,6-Dinitrotoluene ug/Kg U 120 260g gB4 23-25 BH21772 SW8270 10/2/2014 1 N-Nitrosodi-n-propylamine ug/Kg U 120 260B4 23-25 BH21772 SW8270 10/2/2014 1 Aniline ug/Kg U 740 1800B4 23-25 BH21772 SW8270 10/2/2014 1 N-Nitrosodimethylamine ug/Kg U 100 260B4 23-25 BH21772 SW8270 10/2/2014 1 Benzoic acid ug/Kg R 730 1800B4 23-25 BH21772 SW8270 10/2/2014 1 Hexachloroethane ug/Kg U 110 260B4 23-25 BH21772 SW8270 10/2/2014 1 4-Chlorophenyl phenyl ether ug/Kg U 120 260B4 23-25 BH21772 SW8270 10/2/2014 1 Hexachlorocyclopentadiene ug/Kg U 110 260B4 23-25 BH21772 SW8270 10/2/2014 1 Isophorone ug/Kg U 100 260B4 23-25 BH21772 SW8270 10/2/2014 1 Pentachloronitrobenzene ug/Kg U 140 260B4 23-25 BH21772 SW8270 10/2/2014 1 Acenaphthene ug/Kg U 110 260B4 23-25 BH21772 SW8270 10/2/2014 1 Diethyl phthalate ug/Kg U 120 260B4 23-25 BH21772 SW8270 10/2/2014 1 Di-n-butylphthalate ug/Kg U 97 260B4 23-25 BH21772 SW8270 10/2/2014 1 Phenanthrene ug/Kg U 100 260B4 23-25 BH21772 SW8270 10/2/2014 1 Benzyl butyl phthalate ug/Kg U 94 260B4 23-25 BH21772 SW8270 10/2/2014 1 N-Nitrosodiphenylamine ug/Kg U 140 260

Page 9 of 10



SDG: GBH21768

Sample Name Lab ID



B4 23-25 BH21772 SW8270 10/2/2014 1 Fluorene ug/Kg U 120 260B4 23-25 BH21772 SW8270 10/2/2014 1 Carbazole ug/Kg U 280 1800B4 23-25 BH21772 SW8270 10/2/2014 1 Hexachlorobutadiene ug/Kg U 130 260B4 23-25 BH21772 SW8270 10/2/2014 1 Pentachlorophenol ug/Kg U 140 260B4 23-25 BH21772 SW8270 10/2/2014 1 2,4,6-Trichlorophenol ug/Kg U 120 260B4 23-25 BH21772 SW8270 10/2/2014 1 2-Nitroaniline ug/Kg U 370 1800B4 23-25 BH21772 SW8270 10/2/2014 1 2-Nitrophenol ug/Kg U 230 260B4 23-25 BH21772 SW8270 10/2/2014 1 Naphthalene ug/Kg U 100 260B4 23-25 BH21772 SW8270 10/2/2014 1 2-Methylnaphthalene ug/Kg U 110 260B4 23-25 BH21772 SW8270 10/2/2014 1 2-Chloronaphthalene ug/Kg U 100 260B4 23-25 BH21772 SW8270 10/2/2014 1 3,3'-Dichlorobenzidine ug/Kg U 170 730B4 23-25 BH21772 SW8270 10/2/2014 1 Benzidine ug/Kg UJ 210 730B4 23-25 BH21772 SW8270 10/2/2014 1 2-Methylphenol (o-cresol) ug/Kg U 170 260B4 23-25 BH21772 SW8270 10/2/2014 1 1,2-Dichlorobenzene ug/Kg U 100 260B4 23-25 BH21772 SW8270 10/2/2014 1 2-Chlorophenol ug/Kg U 100 260B4 23-25 BH21772 SW8270 10/2/2014 1 1,2,4,5-Tetrachlorobenzene ug/Kg U 130 260B4 23-25 BH21772 SW8270 10/2/2014 1 2,4,5-Trichlorophenol ug/Kg U 200 260B4 23-25 BH21772 SW8270 10/2/2014 1 Acetophenone ug/Kg U 110 260B4 23-25 BH21772 SW8270 10/2/2014 1 Nitrobenzene ug/Kg U 130 260B4 23-25 BH21772 SW8270 10/2/2014 1 3-Nitroaniline ug/Kg U 790 1800B4 23-25 BH21772 SW8270 10/2/2014 1 3&4-Methylphenol (m&p-cresol) ug/Kg U 140 260y p ( p ) g g

Page 10 of 10



SDG: GBJ81780



14B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Methylene Chloride ug/kg U 5.0 5.014B5 (15-19.5) BJ81802 SW8270 8/27/15 1 Benzidine ug/kg UJ 250 84014B5 (15-19.5) BJ81802 SW8260 8/31/15 1 Methyl Ethyl Ketone (2-Butanone) ug/kg UJ 5.0 30

Page 82 of 82

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510 DRIGGS AVENUE BROOKLYN, NEW YORK Block 2312 Lot 23 … · 2019-03-15 · FORMER STERLING TRANSFORMER CORP. 510 DRIGGS AVENUE BROOKLYN, NEW YORK Block 2312 Lot 23 SITE No. C224203