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Quality Characteristics and Nutritional Profiles of DDGSDr. Jerry ShursonDepartment of Animal ScienceUniversity of Minnesota
DDGS Varies in Nutrient Content and Digestibility, Color, and Particle Size Among U.S. Sources
0.42 – 0.990.75 (19.4)Phosphorus, %0.61 – 1.060.90 (11.4)Lysine, %3504 – 40483810 (3.5)Swine ME, kcal/kg
3.0 – 9.86.0 (26.6)Ash, %5.4 – 10.47.2 (18.0)Crude fiber, %8.8 – 12.410.7 (16.4)Crude fat, %28.7 – 32.930.9 (4.7)Crude protein, %87.3 – 92.489.3Dry matter, %
RangeAverageNutrient
Averages, Coefficients of Variation, and Ranges of Selected Nutrients Among 32 U.S. DDGS Sources (100% Dry Matter Basis)
How Does DDGS Compare to Soybean Meal?
Variability (CV, %) of Selected Nutrients Among U.S. DDGS Sources vs. U.S. Soybean Meal Sources
9.119.4Phosphorus25.8117.5Calcium7.312.0Tryptophan4.25.8Threonine5.38.5Methionine3.012.1Lysine6.627.2Ash9.518.9Crude fiber30.917.1Crude fat2.34.5Crude proteinSoybean MealDDGSNutrient
Variation in Particle Size Among DDGS Samples Representing 25 U.S. Ethanol Plants
2005
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Variation in Particle Size Among Soybean Meal Samples Representing 6 U.S. Plants
2005
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400
600
800
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1,200
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Variation in Bulk Density (Lbs/Cubic Ft.) Among DDGS Samples Representing 25 U.S. Ethanol Plants
1/05
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Variation in Bulk Density (Lbs/Cubic Ft.) Among Soybean Meal Samples Representing 6 U.S. Plants
2003
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DDGS Definition and Terminology in the Market
Distillers Products Definitions27.6 Distillers Dried Grains with Solubles is the product obtained after the removal of ethyl alcohol by distillation from the yeast fermentation of a grain or a grain mixture by condensing and drying at least ¾ of the solids of the resultant whole stillageand drying it by methods employed in the grain distilling industry. The predominating grain shall be declared as the first word in the name.
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Grains Solubles
DM, %CP, %Fat, %CF, %Ash, %Ca, %P, %
Comparison of the Nutrient Content of Corn Distiller’s Grains and Corn Condensed Distiller’s Solubles
0.620.570.680.890.780.77P, %
0.170.040.510.060.120.07Ca, %
No data0.270.250.230.180.25Trp, %
No data1.101.131.041.011.17Thr, %
No data0.610.660.540.540.62Met, %
No data0.990.830.900.610.92Lys, %
No data37893560No data35773781ME, kcal/kg*
No dataNo data3796No data38084053DE, kcal/kg*
4.283.77.34.65.36.9Ash, %
No data20.221.017.911.812.4ADF, %
15.1010.67.8No data7.96.3Crude fiber, %
9.008.88.915.33.511.3Fat, %
27.029.930.131.629.331.8Protein, %
PelletedDDGS
Whiskey DDGS
Partial De-germed
DDGS
High Fat DDGS“DDGS”
Golden Corn
DDGS
*Calculated energy values for swine
Comparison of Nutrient Composition of Golden DDGS to Other “DDGS Sources” (100% Dry Matter Basis)
Grain Source Affects Nutrient Content and Digestibility
Comparison of Nutrient Composition of Corn DDGS, Sorghum DDGS, and a Corn-Sorghum Blend (As-is basis)
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Protein%
Fat % ADF % Ash %
Corn DDGSSorghum DDGSCorn-Sorghum DDGS
Urriola et al. (2006)
Comparison of Total Lysine, Methionine, Threonine, and Tryptophan of Corn DDGS, Sorghum DDGS, and a Corn-Sorghum Blend of DDGS for Swine
0
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Lys Met Thr Trp
Corn DDGSSorghum DDGSCorn-Sorghum DDGS
Urriola et al. (2006)
Comparison of Lys, Met, Thr, and Trp Digestibilities of Corn DDGS, Sorghum DDGS, and a Corn-Sorghum Blend of DDGS for Swine
0102030405060708090
Lys Met Thr Trp
Corn DDGSSorghum DDGSCorn-Sorghum DDGS
Urriola et al. (2006)
Standardized Ileal Lysine Digestibility Coefficients Among 10 “Golden” Corn DDGS Sources for Swine (Stein et al., 2005)
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DDGS Source
12345678910
%
Differences in Digestible Amino Acid Content Among DDGS Sources for Poultry
0
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0.6
0.8
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Digest. AA (%)
Cys Lys ThrAmino acid
S1S2S3S4S5
Noll et al. (2006)
Prediction of Amino Acid Digestibility Among Sources of DDGS for Swine and Poultry
Lightness 25% Lightness 50% Lightness 75%
Commission of illumination color scale (Minolta):L* = Lightnessa* = rednessb* = yellowness
Hunter Lab and Minolta Color Measurements
Fig. 1. Regression of digestible lys (%) and color (L*, b*)
R2 = 0.71
R2 = 0.74
20
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60
0.20 0.30 0.40 0.50 0.60 0.70 0.80
Lys (%)
L*, b
* sc
ore L*
b*Linear (L*)Linear (b*)
Source: Dr. Sally Noll (2003)
Prediction of Digestible Lysine from Color (L*, a*, and b*) Among DDGS Sources for Swine
R2 = 0.12, RMSE = 0.10, PC = 1
0.30
0.40
0.50
0.60
0.70
0.80
0.90
0.30 0.40 0.50 0.60 0.70 0.80 0.90
In vitro digestible lysine, %
In v
ivo
dig
estib
le ly
sine
, % .
Urriola et al. (2006)
Prediction of Digestible Lysine from Color L*, a*, and b* (L* < 50 in corn DDGS)
R2 = 0.40, RMSE = 0.07, PC = 1
0.300.350.400.450.500.550.600.650.700.750.80
30.00 35.00 40.00 45.00 50.00 55.00 60.00
Lightness (L*)
In v
ivo
dig
estib
le ly
sine
, %..
Urriola et al. (2006)
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400 450 500 550 600 650 700Wavelengh frecuency, nm
Ligh
t int
ensit
y, m
n
0.77% digestible lysine
0.54% digestible lysine 0.33% digestible lysine
Prediction of Digestible Lysine Content of DDGS Using Optical Density
Prediction of Digestible Lysine from Optical Density (400 to 700 nm)
R2 = 0.86, RMSE = 0.05, PC = 14
0.30
0.35
0.40
0.45
0.50
0.55
0.60
0.65
0.70
0.75
0.80
0.30 0.35 0.40 0.45 0.50 0.55 0.60 0.65 0.70 0.75 0.80In vitro digestible lysine, % .
In v
ivo
dig
estib
le ly
sine
, % .
Urriola et al. (2006)
Prediction of Digestible Lysine in DDGS Using Front Face Fluorescence
R2 = 0.98, RMSE = 0.07, PC = 9
0.30
0.35
0.40
0.45
0.50
0.55
0.60
0.65
0.70
0.75
0.80
0.30 0.40 0.50 0.60 0.70 0.80
In vitro digestible lysine, % .
In v
ivo
dig
estib
le ly
sine,
%.
Urriola et al. (2006)
Some of the Nutrient Variability Among DDGS Sources is Due to the Use of Different Laboratory Testing Procedures
Comparison of AOAC Approved Moisture Testing Methods
130-135° C for 1 hour
100-105° C for 3 hours
100-105° C for 4 hours
60-70° C for 24 hours
Variability of Laboratory Results from the Same DDGS Sample Sent to 5 Different Commercial Laboratories
Moisture Fat ProteinLab 1 12.69 13.73 26.00Lab 2 10.48 10.01 26.30Lab 3 10.09 10.04 27.02Lab 4 10.64 8.73 26.13Lab 5 13.30 10.15 26.29NIR 12.60 9.40 25.00
An “Ideal” DDGS Quality Assurance Program for Ethanol Plants
Monitor incoming corn for mycotoxins and reject postive loads
Standardize the amount of solubles added to the grains fraction to produce DDGS
Use minimal drying time and temperature to produce DDGSDryer temperatures range from 445° F to 1150°F
Segregate poor quality DDGS from good quality DDGS when it is producedPrice different qualities accordingly
Provide transparent and frequent nutrient profile information to customers on the DDGS being produced
Specify the testing procedures used to determine nutrient content
Become ISO 9000:2001 and HAACP certified
Physical Characteristics to MonitorBulk densityParticle sizeHunter color scores
L*a*b*
pH
Nutrients to MonitorMoistureCrude proteinCrude fatCrude fiberADFNDFAshSwine DE, ME, NE (calculated)Starch
MineralsCalciumPhosphorusSulfurChlorideSodium
Amino acidsLysineMethionineThreonineTryptophanCystine
MycotoxinsAflatoxins
B1, B2, G1, G2
Deoxynivalenol (DON)ZearalenoneFumonisins
B1, B2, B3
The Value of New Distiller’s By-Products in Swine Diets
Comparison of Mineral Content of Dakota Gold DDGS with High Protein Dakota Gold and Corn Protein Concentrate (100% DM Basis)
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0.8
1
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Ca, % P, % Na, % S, %
DDGSHP DDGSCPC
Comparison of Nutrient Content of Dakota Gold DDGS with High Protein Dakota Gold and Corn Protein Concentrate (100% DM Basis)
05
101520253035404550
Protein, % Fat, % NDF, % Ash, %
DDGSHP DDGSCPC
Comparison of Amino Acid Content of Dakota Gold DDGS with High Protein Dakota Gold and Corn Protein Concentrate (100% DM Basis)
00.20.40.60.8
11.21.41.61.8
Lys, % Met, % Cys, % Thr, % Trp, %
DDGSHP DDGSCPC
Opportunity Costs of Corn By-Products in Swine and Poultry Diets
$43.00$75.20$53.00$75.20$80.00Poultry
$61.60$63.40$51.00$78.00$80.00Swine
CPCGlutenolHP DDGS
DDGS Spec. 2
DDGS Spec. 1
U of M DDGS Web Sitewww.ddgs.umn.edu
We have developed a DDGS web site featuring:* nutrient profiles and photos of DDGS samples
* research summaries
- swine, poultry, dairy, & beef
- DDGS quality
* presentations given* links to other DDGS related web sites* international audiences