00181E T H Y L CORPOBATION

CORPORATE E N V J H O N M E N T A X A J T F A I B S

A u g u s t 29, 1988

C E R T I F I E D M A I L - R E T U R N R E C E I P T R E Q U E S T E DM r . W i l l i a m B . D e V i l l eA d m i n i s t r a t o rI n a c t i v e a n d A b a n d o n e d W a s t e S i t e s D i v i s i o nD e p a r t m e n t o f E n v i r o n m e n t a l Q u a l i t yP.O. Box 44307Baton Rouge , LA 70804-4307

P L E A S E A D D R E S S R E P L YT O : 4 S I r L O R I D A B L V D

B A T O N R O U G E . L A . 7O8OI

L A . D £ P T . O FE N V I R O N M E N T A L Q U . A L i T '

I A S D I V I S I O N

Dear M r . D e V i l l e :R e : C o m b u s t i o n , I n c . S i t e M o n i t o r i n g

A t t a c h e d a r e t hr e e c op i e s o f t h e o u t f a l l m o n i t o r i n g r e p o r t s f o rt h e C o m b u s t i o n , I n c . s i t e f o r t h e month o f J u l y , 1988.\If you have any q u e s t i o n s about the s e r e p o r t s , p l e a s e contactme at ( 5 0 4 ) 388-7744 or Mr. David C. Bach at ( 5 0 4 ) 388-7058.

S i n c e r e l y ,

H . S t e v e n L i v e s a yS r . Environ. A f f a i r s EngrH S L / c m cEncl .1849Ecc: D. C. Bach - BRT-9

o 143997

ERM-Southw«st, inc.3501 North Causeway Boulevard • Suite 200 • Metairie, Louisiana 70002 • (504) 831-6700

August 25, 1988

f.»

M r . H . Steven Livesay, ChairmanCombust ion, I n c . T e c h n i c a l Commit t eec/o Ethyl Corporat ion451 F l o r i d a BoulevardBaton Rouge, LA 70801RE: J u l y 1988 Pond N Discharge A n a l y s i sCombus t ion, I n c .Dear Mr. Livesay:

LA. DEPT. OFE N V I R O N M E N T A L Q U A L I f v/ A S D I V I S I O N

The purpos e of thi s l e t t e r is to transmit to you the re su l t sof the J u l y 1988 o u t f a l l moni tor ing at the Combus t ion, I n c .site.O u t f a l l M o n i t o r i n gThe Pond N o u t f a l l s a m p l e was c o l l e c t e d by Mr. C. L] H a r r i sof ERM-Southwest on J u l y 28, 1988. The sample s were1 put onice when c o l l e c t ed and de l ivered to Wes t -Paine Laboratoriesin Baton Rouge by Mr. H a r r i s . The l a b o r a t o r y ' s ana ly t i ca lreport ( i n c l u d i n g comple ted chain-of-cus tody f o r m s ) areprov id ed in Atta chmen t 1.The r e su l t s were g e n e r a l l y consistent with previous re su l t s .No hazardous c on s t i t u en t s were d e t e c t ed in the sampl e .If you have any quest ions on th i s r epor t , or if you needa d d i t i o n a l i n f o r m a t i o n , p l e a s e ca l l u s .

S i n c e r e l y ,E R M - S O U T H W E S T , I N C .

N i c h o l a s W . H o i

.' Pi san i , P.E.Princ ipa lN W H / M E P : d e bAttachment scc: Combust ion. I n c . T e c h n i c a l CommitteeMs. Carol Murin Mr. F r a n k Dezzu t t oMr. K e v i n Romine Mr. R a l p h Feeney

Houston Of f i c e : 16000 Memorial Drive • Sui t e 200 • Houston, Texas 77079-4006 • (713) 496-9600An affiliate of the Environmental Resources Management Group with o f f i c e s inA n n a p o l i s , MD • Ann Arbor. Ml • Bloomington. MN • Boston. MA • Brentwood. TN • Charleston. WV • Charlot te . NC • Columbus.OH • Deer f i eW, IL • Engtewood.CO • Houston, TX • Louisville, KY • Marietta, GA • McLean.VA • Metairie, LA • Miami, FL • Newport Beach,CA • Plainview. NY • Rancho Cordova, CA • Redmond, WA • T a m p a , FL • Walnut Creek, CA • Wesl Chester, PA • Vancouver, BC

T A B L E IPOND AREA D I S C H A R G E M O N I T O R I N G

C O M B U S T I O N , I N C .

ParameterS a m p l e Date;T o t a l Organic Carbon, mg/1Oil & Grease , mg/1PHPCBs, ug /1Lead, mg/1 PbBiochemical O x y g e n ' D e m a n d ( m g / 1 O 2 )Prior i ty P o l l u t a n t s ;V o l a t i l e Organic Compounds

B a s e / N e u t r a l Organic Compounds

Acid Ex trac tab l e Organic Compounds

Pond Area DischargeJ u l y 28, 1988

70; 1.4

6.0

15

Below Detect ion L i m i t sf o r A l l CompoundsBelow Detec t ion L i m i t sf o r A l l CompoundsBelow Detect ion L i m i t sf o r A l l Compounds

ATTACHMENT 1 .POND AREA D I S C H A R G E M O N I T O R I N G

ANALYTICAL REPORT BYW E S T - P A I N E L A B O R A T O R I E S

AUGUST 23, 1988

E S T - P A I N E7 9 7 9 Q S R I A V E . • BATON ROUGE. LA 70*20

S A M P L E A N A L Y S E S

f o r

E R M - S o u t h w e s t , I n c .3501 N o r t h Causway Blvd.S u i t e 200M e t a i r i e , LA 70002

A T T E N T I O N : M r . N i c k H o l l i n g s h a d

August 23, 1988

hal 88-5556

' E S T - P A 1 N Eyj.—, wc'

n n o S N A V E . • BATON ROUGE, LA 7M»E R M - S o u t h w e s t , I n c .M e t a i r i e , LA 70002August 23, 1988

S a m p l e receipt at W e s t - P a i n e Labora t or i e s , I n c . is documented for yourde s igna t ed s a m p l e ( s ) . C h a i n - o f - c u s t o d y documenta t ion, i f p r o v i d e d , i s includedin this report. S a m p l e ana ly s i s was in accordance with Environmental Protect ionA g e n c y p r o t o c o l .A. S t a n d a r d M e t h o d s for the Examinat ion of W a t e r and Wast ewater . 16th Ed, 1985

ParameterBiochemical- Oxygen DemandOil & GreaseT o t a l Organic CarbonPH

Method507503A505A423

B. M e t h o d s f or Chemical A n a l y s i s o f W a t e r and W a s t e s . E P A - 6 0 0 / 4 - 7 9 - 0 2 0 , 1979ParameterLead Method239.1

C. M e t h o d s f o r Organic Chemical A n a l y s i s o f M u n i c i p a l & I n d u s t r i a l W a s t e w a t e r .E P A - 6 0 0 / 4 - 8 2 - 0 5 7 , J u l y 1982

Parameter :A c i d ( P h e n o l ) F r a c t i o n ;Base-Neutra l F r a c t i o nP C B ' SV o l a t i l e Organic F r a c t i o nDocumented r e su l t s are shown on the f o l l o w i n g p a g e ( s ) .

Method6 2 5 ( G C / M S )6 2 5 ( G C / M S )6086 2 4 ( G C / M S )

Lanchard I I IGeneral Manager

hal 88-5556

E S T - P A I N E\jy)A _ 1 , — — — — — . E R M - S o u t h w e s t , I n c .

r a n O S H I A V E . • BATON ROUGE. IA TOBO

S a m p l e Source: P O N D N D I S C H A R G EDate C o l l e c t e d : 8 8 / 0 7 / 2 8 . T i m eDate Received: 8 8 / 0 7 / 2 8 T i m eParameter( U n i t )

)cotal Organic Carbon( m g / L C )Oil & Grease( m g / L )PH ( U n i t s )Lead( m g / L P b )Biochemical Oxygen Demand( m g / L 0 2 ) .-:-.

M e t a i r i e ,August 23

PN 072888C o l l e c t e dReceived:

Result

70

1.4

6.0

< 0.1

15

LA 70002, 1988

: 10:0013:15

PercentRecovery

N / A

N / A

N / A

N / A

N / A

Q u a l i t y Assurance D a t e / T i m eA c t u a l / F o u n d A n a l v s t._-

2 5 / 2 4 8 8 / 0 8 / 0 2 15:00 RCD

1 0 . 0 / 9 . 8 8 8 / 0 7 / 2 9 11:35 D S L

7 . 0 / 7 . 0 8 8 / 0 7 / 2 8 14:30 CAEI

: i2 . 5 0 / 2 . 4 7 """ " 8 8 / 0 8 / 0 4 15': 3 O^FBB. .̂ b1 0 0 / 9 9 8 8 / 0 7 / 2 8 14:00 CAE

.. . - .!Afi

hal 88-5556

E S T - P A I N Eme.MTtOSRIAVt • BATON ROUGE. LA TM20

P R I O R I T Y P O L L U T A N T SA c i d ( P h e n o l ) F r a c t i o n

E R M - S o u t h w e s t , I n c .M e t a i r i e , LA 70002S A M P L E |: 880728-0039

All r e s u l t s in micrograms per l i t e rS A M P L E S O U R C E :S a m p l e Date:

!7.

P O N D N D I S C H A R G E PN 0728888 8 / 0 7 / 2 8 S a m p l e T i m e : 10:00Parameter2 - C h l o r o D h e n o l2 f 4-Dichlorophenol2 „ 4-Dime thy lpheho l4 . 6-Dinitro-o-cresol2 . 4-Dini trophenol " - . - • - .2 - N i t r o p h e n o l4 - N i t r o p h e n o lp-Chloro-m-cresol . ••• • •PentachlorophenolPhenol2.4. 6-Trich l oropheno l

Resul t< 10< 10< 10< 30< 50< 10< 40< 10< 10< 10< 10

Detect ionLimi t1010103050104010101010

Date o f A n a l y s i s : 8 8 / 0 8 / 1 1 A n a l y s t : C T N

hal 88-5556

E S T - P A 1 N E• BATON ROUGE. LA rouo

Parameter

E R M - S o u t h w e s t , I n c .M e t a i r i e , LA 70002S A M P L E |: 880728-0039

Q U A L I T Y A S S U R A N C E / Q U A L I T Y C O N T R O LP E R C E N T RECOVERY

A c i d ( P h e n o l ) F r a c t i o n

P O N D N D I S C H A R G EPN 072888

2 , 4 , 6 - T r i c h l o r o p h e n o i - d 22 - N i t r o p h e n o l - d 4

6988

hal 88-5556

^pV E S T - P A I N EI N C .

7 9 7 » G S R ! A v e . • BATON HOU6E, LA 70620

E R M - S o u t h w e s t , I n c .M e t a i r i e , LA 70002S A M P L E #: 880728-0039

P R I O R I T Y P O L L U T A N T SBase-Neutral F r a c t i o n All re sul t s in micrograms per l i t e rS A M P L E S O U R C E : POND N D I S C H A R G E PN 072888S a m p l e Date: 8 8 / 0 7 / 2 8 S a m p l e T i m e : 10:00

T.*

ParameterAcenaphtheneA c e n a p h t h v l e n eAnthraceneBenzid ineB e n z o f a ) anthracene .,-,.., v :

B e n z o f a ) t > v r e n eB e n z o ( b ) f l u o r a n t h e n eB e n z o f a h i ) pervlene : .Benzom f l u o r a n t h e n ebis ( 2 - C h l o r o e t h o x y ) methanebis ( 2 - C h l o r o e t h y U etherbis ( 2 - C h l o r o i s o p r o p v l ) etherbis ( 2 - E t h v l h e x v l l o h t h a l a t e4-Bromophenyl p h e n y l etherButyl benzvl p h t h a l a t e2 - C h l o r o n a p h t h a l e n e4-Chlorophenyl phenyl etherChryseneDibenzo (a . h) anthracene1 , 2— Dich lorobenzene1 , 3-Dich lorobenzene1 . 4— Dichlorobenzene3 , 3 ' - D i c h l o r o b e n z i d i n eDiethvl p h t h a l a t eD i m e t h y l p h t h a l a t eD i — n — butyl p h t h a l a t e2 M 4— D i n i t r o t o l u e n e2 . 6 - D i r i i t r o t o l u e n eDi-n-octyl p h t h a l a t eH e x a c h l o r o b u t a d i e n eF l u o r a n t h e n eF l u o r e n eHexach l orob enz eneH e x a c h l o r o c y c l o p e n t a d i e n eH e x a c h l o r o e thane

Result< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40

Detect ionLimi t4040404040404040404040404040404040404040404040404040404040404040404040

hal 88-5556

^ . .f E S T - P A l N E

• BATON ROUGE. LA 70620

ERM-Southwe s t , Inc .M e t a i r i e , LA 70002S A M P L E f : 880728-0039

P R I O R I T Y P O L L U T A N T SBase-Neutral F r a c t i o n All result s in micrograms per l i t e rS A M P L E S O U R C E : P O N D N D I S C H A R G E PN 072888S a m p l e Date: 8 8 / 0 7 / 2 8 S a m p l e T i m e : 10:00

Parameter ( C o n t i n u e d )I n d e n o f 1 . 2 . 3-c . d) pvreneIsoohoroneN a p h t h a l e n eN i t r o b e n z e n eN - N i t r o s o d i m e t h y l a m i n eN - N i t r o s o d i - n - p r o p v l a m i n eN - N i t r o s o d i p h e n v l a m i n ePhenanthrene . . ••• • •Pvrene1.2. 4— T r i c h l o r o b e n z e n e

Resul t< 40< 40< 40< 40< 40< 40< 40< 40< 40< 40

Detec t i onL i m i t40404040404040404040

Date o f A n a l y s i s : 8 8 / 0 8 / 1 1 A n a l y s t : C T N

hal , -L- .. . . 88-5556

V E S T - P A 1 N EI N C .7 9 7 V O S M A V E . • BATON ROUGE. LA 70620

E R M - S o u t h w e s t , I n c .M e t a i r i e , LA 70002S A M P L E #: 880728-0039

Q U A L I T Y A S S U R A N C E / Q U A L I T Y C O N T R O LP E R C E N T RECOVERY

Base-Neutra l F r a c t i o n

P O N D N D I S C H A R G EParameter _________._________ .____PN 0728881 , 2 - D i c h l o r o b e n z e n e - d 4 v 94F l u o r e n e - d l O . . 104

hal 88-5556

E S T - P A I N ET t n O S M A V t • BATON ROUQE, LA 70820

P R I O R I T Y P O L L U T A N T SP C B ' S

E R M - S o u t h w e s t , I n c .M e t a i r i e , LA 70002S A M P L E #: 880728-0039

AH r e s u l t s in micrograms per l i t e rS A M P L E S O U R C E : P O N D N D I S C H A R G E P N 072888S a m p l e Date: 8 8 / 0 7 / 2 8 S a m p l e T i m e : 10:00

Parameter________________________ Result

PCB-1268 < 1.0

Dete c t i onLimi tPCB-1242P C B - 1 2 5 4P C B - 1 2 2 1P C B - 1 2 3 2PCB-1248PCB-1260PCB-1016P C B - 1 2 6 2 • •••••

< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0< 1.0

1.01.01.01.01.01.01.01.0i.o

Date o f A n a l y s i s : 8 8 / 0 8 / 1 5 A n a l y s t : MEM

hal 88-5556

" W E S T - P A I N E\JajbotatotieA we.7 H 9 G S M A V E . • BATON ROUGE. I* 7WM

P R I O R I T Y P O L L U T A N T SV o l a t i l e Organic F r a c t i o n

E R M - S o u t h w e s t , I n c .M e t a i r i e , LA 70002S A M P L E #: 880728-0039

All r e su l t s in micrograms per l i t e rS A M P L E S O U R C E : P O N D N D I S C H A R G E PN 072888S a m p l e Date: 8 8 / 0 7 / 2 8 S a m p l e T i m e : 10:00

r.*

ParameterBenzeneBromoformCarbon t e t ra ch l or id eChlorobenzeneChlorod ibromomethaneC h l o r o e t h a n e2 - C h l o r o e t h v l v i n v l etherC h l o r o f o r m * •1, 2-Dich lo t ob enzene1 . 4-Dichlorobenzene1 . 3-DichlorobenzeneDichlorobromomethane1 . 1-Dichloroethane1 , 2-Dich loro e thane1, 1-Dich loroe thenetrans-1 . 2-Dichloroe thene1 . 2 - D i c h l o r o p r o p a n e1 . 2 - D i c h l o r o p r o p y l e n etrans-1, 3 - D i c h l o r o p r o p e n eE t h y l b e n z e n eM e t h y l bromideM e t h y l c h l o r i d eM e t h y l e n e c h l o r i d e1.1.2, 2 - T e t r a c h l o r o e t h a n eT e t r a c h l o r o e t h e n eT o l u e n e1.1. 1 - T r i c h l o r o e t h a n e1.1. 2 - T r i c h l o r o e t h a n eT r i c h l o r o e t h e n eT r i c h l o r o f l u o r o m e t h a n eVinvl c h l o r id eT o t a l X v l e n e

Result< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10< 10

Detec t i onLimi t

1010101010101010101010101010101010101010101010101010101010101010

Date o f A n a l y s i s : 8 8 / 0 8 / 0 3 A n a l y s t : RJV

hal 88-5556

V V E S T - P A 1 N E\jct6otatotie4 I N C .nnosniAvc. • BATON ROUGE, IA 70*20

E R M - S o u t h w e s t , I n c .M e t a i r i e , LA 70002S A M P L E #: 880728-0039

Q U A L I T Y A S S U R A N C E / Q U A L I T Y C O N T R O LP E R C E N T RECOVERY

V o l a t i l e Organic F r a c t i o n

POND N D I S C H A R G EParameter________________________ PN 072888Benzene 1241,2-Dichloroethane .... 137Ethy lb enz ene 120

!r

ha l 88-5556

PV V E S T - P A I N E717IGSRIAVE. • BATON ROUGE. LA 70606

Case No. ______ EPA 624 W A T E R M A T R I X S P I K E / M A T R I X S P I K E D U P L I C A T E RECOVERY

F R A C T I O N C O M P O U N DVOA 1.1-Dichloroethene

T r i c h l g r o e t h e n eS A M P L E N O . Chlorobenzene880722-90 T o l u e n e

Benzene1.2 . 4 - T r i c h l o r o b e n z e n eB/ ^V Acenaoh th ene

J 2.4 D i n i t r o t o l u e n eS A M P L E N O . D i - n - B u t v l p h t h a l a t e

Pvrene

C O N C . S P I K E S A M P L EA D D E D ( u g / L " ) R E S U L T

50 <1050 <1050 <1050 <1050 <10

. ••

C O N C . %MS gEC47 9456 10252 10458 11652 104

N - N i p r o s p - D i - n - P r o o v l a m i n e1 . 4-Dichlorobenzene

A C I D Peni;ach l oropheno lPhenol

S A M P L E N O . 2 - C h l o r o p h e n o l4 - C h l o r o - 3 - M e t h v l p h e n o l4 - N i t r o p h e n o l

P E S T I f i n d a n eJ i e p t a c h l o r

S A M P L E N O . A l d r i nD i e l d r i nEndrin4 . 4 ' D O T;A D V I S O R Y L I M I T S

RPD: VOAs out of :B/N out of :A C I D , , , , , , o u t o f :PEST out of :

COMMENTS :

—— ...

out s ide QC l imi t sou t s i d e QC l i m i t sou t s id e QC l i m i t sou t s i d e QC l i m i t s

RECOVERY: VOAsB/NA C I DP E S T

C O N C . % QC LIMITS*MSD REG RPD RPD RECOVERY

1414131311283138403138285042404250152022182127

0 out of 5 : outs ide OCout of : ou t s id e OCout of : ou t s id e OCout of : ou t s id e QC

61-14571-12075-13076-12576-12739-9846-11824-9611-11726-12741-11636-979-10312-8927-12323-97..10-8056-12340-13140-12052-12656-12138-127

l imi t sl i m i t sl i m i t sl i m i t s

*Contract Laboratory P r o t o c o lT h e s e l i m i t s are for advi sory p u r p o s e s only. T h e y are not to be used to de t ermine if a s a m p l e should be r eanalyzed ,s u f f i c i e n t m u l t i - l a b da ta are a v a i l a b l e , s tandard l i m i t s w i l l b e c a l c u l a t e d .

When

E S T - P A I N E• BATON ROUGE, LA 70608

W A T E R M A T R I X S P I K E / M A T R I X S P I K E D U P L I C A T E RECOVERYF R A C T I O N

( B / N )

( A / E )

C O M P O U N D

1 . 2 . 4 - T r i c h l o r o b e n z e n eA c e n a p h t h e n e2 .4-Dini tro to lueneDi-n-butvl u h t h a l a t ePvreneN - N i t r o s o d i - n - p r o D v l a m i n e1.4 -DichlorobenzeneP e n t a c h l o r o p h e n o lPhenol2 - C h l o r o p h e n o l4 - C h l o r o - 3 -me t h v l p h e n o l4 - N i t r o p h e n o l

C O N C .S P I K E D( u g / L )

100100100100100100

" 100200 .200200200200

S A M P L E C O N C .R E S U L T M S

<10 138<10 87.1<10 109

11.2 113<10 121<10 84 . 2<10 84 . 1<10 60.7<10 25.5<10 111<10 43.5<40 245

% CONC % RPD PCR E C O V E R Y M S D RECOVERY

138870109102121

848430135622

122

RPD

283138403138285042404250

L I M I T S *RECOVERY

39-9846-11824-9611-11726-12741-11636-979-10312-89 V27-12323-9710-80

D a t e / A n a l y s t : 0 7 - 0 8 - 8 8 / C T NA D V I S O R Y L I M I T S

RPD:B / N _A / E _

S U R R O G A T E R E C O V E R Y :

out of ___; Out s id e QC L i m i t sout of ___; Out s ide QC Limi t s

1 ,2-Dich lorob enzene-d4: (a)_83 ( b )RPD ]F l u o r e n e - d l O : (a)_95 ~RPD

B / N _ 2 _ out of _7_; Out s id e QC L i m i t sA / E _ 2 _ out of _5_; Out s id e QC L i m i t s

2 , 4 , 6 - T r i c h l o r o p h e n o l - d 2 : (a)_34 ( b )RPD

2 - N i t r o p h e n o l - d 4 : (a)_61 (b)"RPD

M S R E F E R E N C E N U M B E R : B N A W C - 0 3 7 A BS A M P L E I D E N T I F I C A T I O N : 880616-0092 — — "*Contract Laboratory Proto co lT h e s e l i m i t s are for advisory p u r p o s e s only. T h e y are not to be used to de t ermine if a s ampl e should be reanalyzed. Whens u f f i c i e n t m u l t i - l a b d a t a are a v i l a b l e , s tandard l i m i t s wi l l b e c a l c u l a t e d .

/e />?C H A I N O F C U S T O D Y RECORD

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