, -vThruN R:CORDD CTS . R · 2020. 12. 4. · according to Metho 6010/200.7d Sedimen. t sample analyzes wer foed alsr tota o res.dual solidsl Th. e results of analysis are provided

^ ̂ -* . r̂̂ . ^ -̂M ii-ii-i A K I CORPORATE OFFICES. Maine, Massachusetts,WOODARD &CURRAN New Hampshire, Connecticut, Illinois, FloridaEngineering - Science , Operations operation* off,ces throughout the u.s.

, -vThruND R:CORDS CTR ._ _

T T ^ A A A ' ^ ^/^SffSf. JE*™1» jfcL-̂ 1?-,January 7, 200U i ______ _ _ ......

Mr. Ed HathawayUSEPA Region IMaine, Vermont, and Connecticut Superfund SectionMailcode: HBT1 Congress StreetBoston, MA 02114

Subject: Saco Municipal LandfillFall 1999 Sampling Report

Dear Ed:

This letter serves to convey the results of the fall 1999 sampling event. This sampling was completed asdescribed in our November 5, 1999 letter to you.

Sample Collection and Analysis

Woodard & Curran collected surface water and sediment samples from 15 locations on November 19,7999 tlltrnpSwere analyzed at Katahdin Analytical Serv.es for total arsemc iron and manganeseaccording to Method 6010/200.7. Sediment samples were also analyzed for total res.dual solids. The

results of analysis are provided as Attachment 1.

of analysis are provided as Attachment 2.

All samples were collected in pre-cleaned and pre-preserved sample jars provided by the laboratory. Thesamples were kept on ice and delivered to the laboratory on the day of collection.

Data Quality

Quality control samples included one trip blank, one equipment blank, and six ™^^^S^r(MS/MSD) The laboratory analyzed blanks and laboratory control samples as part of their

- These ntS 'and 2.

41 Hutchms Drive .Portland, Maine 04102 , 207-774-2112 , 207-774-6635 (Fax) , 1-800-426-4262 , www.woodardcurran.com

O:/95093/Falll999samplmg/report/coverletter

WOODARD&CURRAN Engmeermg • Science > Opoiations

Mr. Ed Hathaway January 7, 2000 Page 2

Holding time requirements were met for all samples.

Percent recoveries from laboratory control samples (LCSs) were within established limits for all inorganic analytes. For VOAs, percent recoveries from the LCS were within established limits for all analytes with the exception of acetone and dichlorodifluoromethane, neither of which were detected at any concentration in the samples. This result does not affect data usability.

MS/MSD results were acceptable, with one exception. For one inorganic MS/MSD (WP 4764-006), the MS recovery was outside the laboratory-specified spike concentration acceptance range because the spike concentration was significantly below the sample concentration. As a result, the spike concentration could not be distinguished from the sample's analytical signal. However, the spike duplicate recovery and relative percent difference were acceptable. This result does not affect the data usability.

Findings

Results of groundwater, surface water, and sediment sampling conducted in November 1999 are generally consistent with previous results.

Surface water results from the November sampling event are shown on Table 1 with results from previous sampling events. These results indicate that concentrations of arsenic, manganese, and iron in samples collected 300 to 500 feet downstream from the confluence of Sandy Brook and Big Ledge Brook (SW-93, SW-98, SW-103) are at concentrations similar to background.

Sediment results are shown on Table 2 with results from previous sampling events. Results from the November sampling event are consistent with historical concentration ranges. Concentrations at the excavated seep location (SD-13) remain an order of magnitude below the pre-excavation concentrations. Arsenic concentrations in sediment decrease downstream from the confluence of Sandy Brook and Big Ledge Brook. Manganese and iron concentrations decrease downstream from the confluence, with the exception of SD-103, where concentrations increase.

O:\95093\Falll999samplingreport/cover letter

WOODARD&CURRAN ctngmeonng • ^c 'erce • Op>3Mt on

Mr. Ed Hathaway January 7, 2000 Page 3

Groundwater results from three wells at the foot of Landfill 4 (Table 3) illustrate the trends in groundwater concentrations. Results from the November 1999 sampling are at or within historical concentrations.

Please call me if you have questions or concerns on the enclosed report.

Sincerely,

WOODARD & CURRAN INC.

Karl D. Kasper, C.G. Project Manager

cc: W. Harper (MEDEP)/ 1 copy S. Mierzykowski (USFWS)/ 1 copy R. Roedner (City of Saco)/ 1 copy J. Cohn-Connor (Preti, Flaherty, Beliveau, & Pachios)/ 2 copies File (Project 95093.06)

O \95093\Fall 1999samphngreport/cover letter

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Table 1

Surface Water Analytical Data for Total Arsenic, Manganese, and Iron Saco Municipal Landfill

Saco, Maine

RESULT Arsenic Manganese Iron LOCATION DATE TYPE (ug/L) (ug/L) (ug/L)

Area 2 SW-7 11/17/95 Primary 2.8 U 93.4 596 SW-7 5/16/96 Primary 3 U 32.9 239 SW-7 11/19/96 Primary 3 U 21.9 315 SW-7 6/24/98 Primary 8 U 1880 SW-7(t) 10/1/98 Primary ND 3050 SW-7 6/10/99 Primary < 5 1620 1320 SW-7 11/19/99 Primary < 5 708 366 SW-8 11/17/95 Primary 2.8 U 77.9 582 SW-8 7/17/97 Primary 6.7 U 3620 SW-8 6/24/98 Primary 8 U 665 SW-9 11/17/95 Primary 2.8 U 95.6 611 SW-9 11/17/95 Duplicate 1 2.8 U 102 632 SW-9 5/16/96 Primary 3 U 86.8 805 SW-9 11/19/96 Primary 2.1 U 65.6 548 SW-9 11/19/96 Duplicate 1 2.1 U 67.6 557 SW-9 7/17/97 Primary 6 U 2680 SW-9 6/24/98 Primary 8 U 792 SW-9 6/10/99 Primary < 5 73 790 SW-9 11/19/99 Primary < 5 37.4 392 SW-10 11/17/95 Primary 2.8 U 97.2 619 SW-4 11/17/95 Primary 2.8 U 80.4 575 SW-4 7/17/97 Primary 4.6 U 2020 SW-4 7/17/97 Duplicate 1 6.9 U 2650 SW-4 6/24/98 Primary 8 U 839

Areas 3 and 4 SW-21 5/16/96 Primary 138 3530 15500 SW-21 5/16/96 Duplicate 1 136 3500 15400 SW-21 11/19/96 Primary 2.1 U 83.5 772 SW-21(t) 10/1/98 Primary ND 43 SW-21 6/10/99 Primary < 5 88 806 SW-21 6/10/99 Primary 34 875 4110 SW-21 11/19/99 Primary < 5 33.8 388 SW-52 11/19/99 Primary 16 515 1900 SW-6A 6/24/98 Primary 12 2130 SW-13 11/17/95 Primary 8.7 J 342 1570 SW-13 11/19/96 Primary 108 2950 12000 SW-13 6/24/98 Primary 14 2370 SW-13(t) 10/1/98 Primary 14 1940 SW-13 6/10/99 Primary 36 1300 3980 SW-13 6/10/99 Duplicate 1 34 1280 3850 SW-13 11/19/99 Primary 17 668 2010

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Table 1

Surface Water Analytical Data for Total Arsenic, Manganese, and Iron Saco Municipal Landfill

Saco, Maine

RESULT Arsenic Manganese Iron LOCATION DATE TYPE (ug/L) (ug/L) (ug/L)

SW-13 11/19/99 Duplicate 1 17 671 2010 SW-37 6/10/99 Primary 39 1350 4990 SW-37 11/19/99 Primary 15 704 1890 SW-5 11/17/95 Primary 10.9 239 1750 SW-34 6/24/98 Primary 10 1760 SW-34 6/24/98 Duplicate 1 12 1720 SW-34 (t) 10/1/98 Primary 10 448 SW-34 6/10/99 Primary 22 1150 2450 SW-34 11/19/99 Primary 14 634 1760 SW-31 6/10/99 Primary 14 816 1350 SW-31 11/19/99 Primary 8 427 827 SW-15 11/17/95 Primary 4.2 J 151 863 SW-15 11/19/96 Primary 12.2 381 1260 SW-15(t) 10/1/98 Primary ND 29.9 SW-15 6/10/99 Primary 13 769 1260 SW-15 11/19/99 Primary 5 J 274 601 SW-69 6/24/98 Primary 11 1480 SW-69 (t) 10/1/98 Primary 8 244 SW-69 6/10/99 Primary 12 762 1100 SW-69 11/19/99 Primary 6 J 352 684 SW-73 11/19/99 Primary 6 J 367 652 SW-75 6/10/99 Primary 12 772 1150 SW-78 6/10/99 Primary 11 778 1050 SW-78 6/10/99 Duplicate 1 12 756 1020 SW-83 6/10/99 Primary 11 787 1020 SW-84 11/19/99 Primary < 5 387 669 SW-86 6/10/99 Primary 11 794 1020 SW-20 11/17/95 Primary 2.8 U 89 677 SW-93 11/19/99 Primary < 5 374 621 SW-98 11/19/99 Primary 6 J 288 658 SW-103 11/19/99 Primary < 5 359 599 SW-103 11/19/99 Duplicate 1 < 5 375 630

Notes: Sampling locations are presented in upstream to downstream order. SW-6A - new location across from SW-13 J = estimated U = not detected at indicated reporting limit t = total arsenic analysis < = element was detected, but at a concentration less than the indicated value

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Table 2 Sediment Analytical Data for Total Arsenic, Manganese, and Iron

Saco Municipal Landfill Saco, Maine

RESULT Arsenic Manganese Iron LOCATION DATE TYPE (mg/kg) (mg/kg) (mg/kg)

Area 2 SD-7 11/95 Primary 6.5 J 329 J 10500 J SD-7 5/96 Primary 2.1 137 9420 SD-7 11/96 Primary 4.5 J 139 9410 SD-7 6/98 Primary 2.1 NA 10,100 B SD-7 11/99 Primary 1.5 255 5,760 SD-9 11/95 Primary 2.2 J 76.3 J 4700 J SD-9 11/95 Duplicate 1 2.2 J 91.8 J 5160 SD-9 5/96 Primary 3.5 230 8740 SD9D 5/96 Duplicate 1 4.7 305 10,900 SD-9 11/96 Primary 3.4 221 9080 SD-9 6/98 Primary 4.5 NA 10,300 B SD9 11/99 Primary 3.5 202 7,950

Areas 3 and 4 SD-21 5/96 Primary 29.2 102 8090 SD-21 11/96 Primary 9.88 214 11500 SD-21 6/98 Primary < 8.6 NA 10,000 B SD-21 11/99 Primary 6.8 162 10,300 SD-52 7/96 Primary 12.6 NA 9410 SD-52 11/99 Primary 29.8 85.1 10,400 SD-13 11/95 Primary 2250 J 1660 J 318,000 J SD-13 5/96 Primary 41.3 184 22,400 SD-13 1/96 Primary 8.7 92 9,350 SD-13 6/98 Primary 71 NA 15,700 B SD-13 11/99 Primary 98.5 508 36,200 SD-13D 11/99 Primary 105 551 39,000 SD-37 11/99 Primary 57.9 242 12,200 SD-34 7/96 Primary 19.6 NA 21,500 SD-34 6/98 Primary 140 NA 30,000 B SD-34 6/98 Duplicate 1 120 NA 27,500 D SD-34 11/99 Primary 60.4 109 9,920 SD-31 7/96 Primary 81.5 NA 13,700 SD-31 11/99 Primary 175 1420 30,900 SD-15 11/95 Primary 42.2 J 464J 16,000 J SD-15 5/96 Primary 84 NA 29,000 SD-15 11/96 Primary 26.1 305 17,200 SD-15 11/99 Primary 14.2 122 7,340

WOODARD CURRAN (95093.06) 0:/95093/fall1999 sampling/report/table 2-sediment

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Table 2 Sediment Analytical Data for Total Arsenic, Manganese, and Iron

Saco Municipal Landfill Saco, Maine

RESULT Arsenic Manganese Iron LOCATION DATE TYPE (mg/kg) (mg/kg) (mg/kg)

Areas 3 and 4 (continued) SD-69 11/99 Primary 18.3 338 6,380 SD-73 11/99 Primary 17.3 77 8,130 SD-84 11/99 Primary 16.8 405 5,650 SD-93 11/99 Primary 14.4 270 5,080 SD-98 11/99 Primary 12.4 262 5,360 SD-103 11/99 Primary 11 576 14,400 SD-103D 11/99 Duplicate 10 557 17,800

Notes: Sampling locations are presented in upstream to downstream order (see Figure 2-3) J = estimated < = element was detected, but at a concentration less than the indicated value NA = not analyzed

WOODARD CURRAN (95093.06) 0:/95093/fall1999 sampling/report/table 2-sediment

1/7/00

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Attachment 1

Reports of Analysis

Surface Water and Sediment

SACO MUNICIPAL LANDFILL NOVEMBER 1999 MONITORING

SAMPLE SUMMARY BY LABORATORY WORK ORDER

Surface Water , SW-103 SW-103 (DUP) SW-98 SW-93 SW-84 SW-73 SW-69 SW-15 SW-31 SW-34 SW-37 SW-13 SW-13 (DUP) SW-52 SW-21 SW-9 SW-7

Sediment SD-103 SD-103 (DUP) SD-98 SD-93 SD-84 SD-73 SD-69 SD-15 SD-31 SD-34 SD-37 SD-13 SD-13 (DUP) SD-52 SD-21 SD-9 SD-7

Work Order WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848

Groundwater MW-95-5R MW-95-5R (DUP) MW-95-8S MW-97-18S EQ-1 MW-97-14S1 MW-97-14S2 MW-95-4SA MW-95-4SB MW-97-19S MW-95-9S MW-95-11S MW-97-17R MW-95-8R MW-97-13S1 MW-97-13S2 MW-97-13R TB-1 MW-95-1R MW-95-1S MW-95-4RD MW-95-3R MW-95-4R MW-13 MW-13 (DUP) MW-13 MS MW-13 MSD MW-95-6S MW-93-3 MW-95-6R MW-97-16S MW-95-7S MW-95-7S (DUP) MW-95-7R MW-93-5 MW-96-9R

Work Order WP4803 WP4803 WP4803 WP4803 WP4803 WP4803 WP4803 WP4803 WP4803 WP4803 WP4825 WP4825 WP4825 WP4825 WP4825 WP4825 WP4825 WP4764 WP4764 WP4764 WP4764 WP4764 WP4764 WP4764 WP4764 WP4764 WP4764 WP4781 WP4781 WP4781 WP4781 WP4781 WP4781 WP4781 WP4781 WP4781

U /projects/sacoLF/nov99samploing/samphng summary doc

.Katahdi: A N A L Y T I C A L S E RV I C E S

December 29, 1999

Mr. Karl Kasper

Woodard & Curran

41 HutchinsDr.

Portland, ME 04102

RE: Katahdin Lab Number: WP4848

Project ID: SACO LF Project Manager: Ms. Andrea J. Colby Sample Receipt Date(s): 11/19/99

Dear Mr. Kasper:

Please find enclosed the following information:

* Report of Analysis

* Quality Control Data Summary

* Chain of Custody (COC)

* Confirmation

A copy of the Chain of Custody is included in the paginated report. The original COC is attached as an addendum to this report.

Should you have any questions or comments concerning this Report of Analysis, please do not hesitate to contact the project manager listed above. This cover letter is an integral part of the ROA.

We appreciate your continued use of our laboratory and look forward to working with you in the future. The following signature indicates technical review and acceptance of the data.

Sincerely,

KATAHDIN ANALYTICAL SERVICES

S -Authorized S/fsmature Date

340 County Road No. 5 210 West Road No 5, Portsmouth, NH 03801 PO Box 720, Westbrook, ME 04098

Tel ,207,874 24oo Fax,207,775 4029 ht tp / /katahdmlab com Tel (603)431-5777 Fax (603) 436-3356

Katahdin Analytical Services 0000001

TECHNICAL NARRATIVE

For work order WP4848 results for Arsenic analyses performed according to EPA 6010/200.7 have been reported to client-specified levels. These levels are indicated in the results and PQL fields of the analytical report. For hits that fell between the client-specified levels and Katahdin's PQL a "J" flag has been used.

340 Count; Koad No 1 210 West Road No 5, Portsmouth, N H 03801 PO. Box 720, Wcubrook Mt 04U98 hup -VkjuhdtnUb com Tel. (603)431-5777 Hx. (605)416 ii56 Pel (2fl7) 874-2400 Fat: (207) 775-4029


Katahdin S E R V I C E S

Lab Number : WP-4848-1

CLIENT: KARL KASPER Report Date: 12/29/99

Woodard & Curran PO No. : 95093.03

41 Hutchins Dr. Project : SACO LF

Portland, ME 04102

REPORT OF ANALYTICAL RESULTS Page 1 of 51

SAMPLE DESCRIPTION MATRIX SAMPLED BY SAMPLED DATE RECEIVED

SW-31 Aqueous D.DINSMORE 11/19/99 11/19/99

PARAMETER RESULT UNITS DF kPQL METHOD ANALYZED BY NOTES

Arsenic, Total 0.008 mg/L 1.0 0.005 6010/200.7 12/04/99 KD

Iron, Total 0.827 mg/L 1.0 0.025 6010/200.7 12/04/99 KD

Manganese, Total 0.427 mg/L 1.0 0.0050 6010/200.7 12/03/99 KD

* PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect satrplespecific reporting limits. Sample-specific limits are indicated by results annotated with '

.Katahdin A N A L Y T I C A L SERVICES

Lab Number : WP-4848-2 CLIENT: KARL KASPER Report Date: 12/29/99

Wcodard & Curran PO No. : 95093.03 41 Hutchins Dr. Project : SACO LF Portland, ME 04102




PARAMETER RESULT UNITS DF *PQL METHOD ANALYZED BY NOTES

Arsenic, Total 0.014 mg/L 1.0 0.005 6010/200 .7 12/04/99 KD 1 Iron, Total 1.76 mg/L 1.0 0.025 6010/200 .7 12/04/99 KD 1 Manganese, Total 0.634 mg/L 1.0 0. 0050 6010/200 .7 12/03/99 KD 1

* PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sample-

specific reporting limits. Sample-specific limits are indicated by results annotated with '

.Katahdin A N A L Y T I C A L S E R V I C E S


Woodard & Curran PO No. : 95093.03 41 Hutchins Dr. Project : SACO LF Portland, ME 04102





Arsenic, Total 0.015 mg/L 1.0 0.005 6010/200 .7 12/04/99 KD 1

Iron, Total 1.89 tng/L 1.0 0.025 6010/200 .7 12/04/99 KD 1

Manganese, Total 0.704 mg/L 1.0 0. 0050 6010/200 .7 12/03/99 KD 1


specific reporting limits. Sample-specific limits are indicated by results annotated with '> !!< HS(,


http:95093.03


Lab Number : WP-4848-4 CLIENT: KARL KASPER Report Date- 12/29/99

Woodard & Curran PO No. . 95093.03 41 Hutchins Dr. Project : SACS LF Portland, ME 04102





Arsenic, Total 0.017 mg/L 1.0 0.005 6010/200. .7 12/04/99 KD 1

Iron, Total 2 . 01 mg/L l.C 0.025 6010/200. .7 12/04/99 KD 1

Manganese, Total 0.668 mg/L 1.0 0.0050 6010/200 .7 12/03/99 KD 1

* PQL (Practical Cuantitation Level) represents laboratory reporting limits and may not reflect sample-


Lab Number : WP-4848-S CLIENT: KARL KASPER Report Date: 12/29/99

Woodard & Curran PO No. : 95093.03 41 Hutchins Dr. Project : SAGO LF Portland, ME 04102



SW-13(DUP) Aqueous D.DTNSMORE 11/19/99 11/19/99

PARAMETER RESULT UNITS DF *PQL METHOD. ANALYZED BY NOTES

Arsenic, Total 0.017 ng/L 1.0 0.005 6010/200.7 12/04/99 KD

Iron, Total 2.01 mg/L 1.0 0.025 6010/200.7 12/04/99 KD

Manganese, Total 0.671 mg/L 1.0 0.0050 6010/200.7 12/03/99 KD

* PQL (Practical Quantitacion Level) represents laboratory reporting limits and may not reflect sample-

specific reporting limits. Sample-specific limits are indicated by results annotated with 'k. Ml II lim li-l: (MM -i.?l-5~ K-l: CO"! X " t - ' - l ( l < > I j v


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CLIENT: KARL KASPER Report Date: 12/29/99


41 Hutchins Dr. Project : SACO LF

Portland, ME 04102



SW-52 Aqueous D.DTNSMORE 11/19/99 11/19/99

PARAMETER RESULT UNITS DF *PQL METHOD, ANALYZED BY NOTES

Arsenic, Total 0.016 mg/L 1.0 0.005 6010/200.7 12/04/99 KD 1 Iron, Total 1.90 mg/L 1.0 0.025 6010/200.7 12/04/99 KD 1 Manganese, Total 0.515 mg/L 1.0 0.0050 6010/200.7 12/04/99 KD 1








PARAMETER RESULT UNITS DP *PQL METHOD ANALYZED BY NOTES

Arsenic, Total




41 Hutchins Dr. Project : SACO LF Portland, ME 04102





Arsenic, Total ( l i l n i l ^~~ ' I l\ i f i D i l l« . HSfi


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Woodard & Curran PO No. : 95093.03 41 Hutchins Dr. Project -. SAGO LF

Portland, ME 04102



SW-7 Aqueous D.DTWSMORE 11/19/99 11/19/99


Arsenic, Total ' -l'" iiS(>

III !Jtr> S " i 1 mil l.i


http:95093.03

Lab NUmber : WP-4848-10 CLIENT: KARL KASPER Report Date: 12/29/99






Arsenic, Total






SW-103 (DUP) Aqueous D.DINSMORE 11/19/99 11/19/99


Arsenic, Total


Woodard & Curran PO No. : 95093.C3 41 Hutchins Dr. Project : SAOO LF Portland, ME 04102





Arsenic, Total JO .006 mg/L 1.0 0.005 6010/200 .7 12/04/99 KD 1,2 Iron, Total 0.658 mg/L 1.0 0.025 6010/200 .7 12/04/99 KD 1 Manganese, Total 0, .388 mg/L 1.0 0.0050 6010/200 .7 12/04/99 KD 1

* PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sanplespecific reporting limits. Sample-specific limits are indicated by results annotated with ', , | No ^ : i l ) \UM K o i d N i . ^ I'c.nsi unti l \H (HM)l ' i > B i > \ ~.v \\ ( . M ' U O I k Mi M ! i l ( J i r i . s" t - j iuo I .\ on


http:95093.C3

Lab Number : WP-4848-13 CLIENT: KARL KASPER Report Date- 12/29/99

Wbodard & Curran PO No. : 95093.03 41 Hutchins Dr. Project : SAOO LF Portland, ME 04102





Arsenic, Total

, ICatahdin A N A L Y T I C A L S E R V I C E S


Woodard & Curran PO No. : 95093.03 41 Hutchins Dr. Project : SAOO LF Portland, ME 04102


SAMPLE DESCRIPTION MATRIX SAMPLED 3Y SAMPLED DATE RECEIVED



-,Arsenic, Total

Katahdin A N A L Y T I C A L S E R V I C E S

Lab Number : WP-4848-15 CLIENT: KARL KASPER Report Dare: 12/29/99




SW-73 Aqueous D.DTNSMDRE 11/19/99 11/19/99


Arsenic, Total JO. 006 mg/L 1. .0 0.005 6010/200 .7 12/04/99 KD 1,2 Iron, Total 0.652 mg/L 1. C 0.025 6010/200 .7 12/04/99 KD _L Manganese, Total 0.367 mg/L 1. 0 0.0050 6010/200 .7 12/04/99 KD 1



Lab Number : KP-4848-16 CLIENT: KARL KASPER Report Date: 12/29/99






Arsenic, Total JO . 006 mg/L 1.0 0.005 6010/200.7 12/04/99 KD 1,2 Iron, Total 0.684 mg/L 1.0 0.025 6010/200.7 12/04/99 KD 1 Manganese, Total 0.352 mg/L 1.0 0. 0050 6010/200.7 12/04/99 KD 1









Arsenic, Total JO . 005 mg/L 1 . 0 0.005 S010/200 .7 12/04/99 KD 1,2 Iron, Total 0.601 mg/L 1.0 0.025 6010/200 .7 12/04/99 KD 1

Manganese, Total 0.274 mg/L 1.0 0.0050 6010/200 .7 12/04/99 KD 1


specific reporting limits. Sample-specific limits are indicated by results annotated with ' !> l ! < > SHI-,


http:95093.03





SD-31 Solid D.DINSMORE 11/19/99 11/19/99

PARAMETER RESULT UNITS DF *PQL METHOD( ANALYZED BY NOTES

Arsenic, Total 175. mg/Kgdrywt 1. 0 0.8 6010/200 .7 12/06/99 KD 1 Iron, Total 30900. mg/Kgdrywt 1 . 0 2.5 6010/200. .7 12/06/99 KD 1 Manganese, Total 1420. mg/Kgdrywt 1.0 0.50 6010/200. .7 12/06/99 KD 1

* PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sartplespecific reporting limits. Sample-specific limits are indicated by results annotated with ' I ' l . i i M i m u h M I O i b O ! K i ( . I l i r l i ] •> I is iMH) j'-i'* i i>6


http:95093.03

, Katahdin S E R V I C E S

Lab Nu-iiber : WP-4848-18 CLIENT: KARL KASPER Report Date: 12/29/99

Wocxiard & Curran PC NO. : 95093.03 41 Hutchins Dr. Project : SAOO LF Portland, ME 04102




PARAMETER RESULT UNITS DF *PQL METHOD , ANALYZED BY NOTES

Solids-Total Residue (TS) 37. wt % 1.0 0.10 CLP/CIP SOW 11/29/99 JF

* PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sairplespecific reporting limits. Sample-specific limits are indicated by results annotated with ' ) ! •) 11 =,— I is tdlHi -i ! ( . - * ) = > < >


1

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Wbodard & Curran PO No. : 95093.03 41 Hutchins Dr. Project : SAGO LF Rutland, ME 04102



SC-34 Solid D.DINSMORE 11/19/99 11/19/99


Arsenic, Total 60.4 mg/Kgdrywt 1.0 0.8 6010/200.7 12/06/99 KD 1 Iron, Total 9920. mg/Kgdrywt 1.0 2.5 6010/200.7 12/06/99 KD 1 Manganese, Total 109. mg/Kgdrywt 1.0 0.50 6010/200.7 12/06/99 KD i J


specific reporting limits. Sanple-specific limits are indicated by results annotated with '


Woodard & Curran PO NO. : 95093.03 41 Hutchins Dr. Project : SACO LF Portland, ME 04102



SC-34 Solid D.DINSMORE 11/19/99 11/19/99


Solids-Total Residue (TS) 77. wt % 1.0 0.10 CLP/CI? SOW 11/29/99 JF 1




Wbodard & Curran PO No. : 95093.03 41 Hutchins Dr. Project : SACO LF

Portland, ME 04102



SD-37 Solid D.DTNSM3RE 11/19/99 11/19/99


Arsenic, Total

Iron, Total Manganese, Total

57 . 912200 .242.

mg/Kgdrywt mg/Kgdrywt

rrg/Kgdrywt

1.0 l.C l.C

0.8 2.5 0.50

6010/200. 6010/200. 6010/200.

.7

.7 ,7

12/06/99 12/06/99 12/06/99

KD KD

KD

1

1 1


specific reporting limits. Sarple-specific limits are indicated by results annotated with '\ "JO \\ iMl,u>, k Ml 1) i KI r jcn.x • : iini 11 \ IJT, "i i








Solids-Total Residue (TS) 70. wt % 1.0 0.10 CLP/CIP SOW 11/29/99 JF 1

* PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sarrplespecific reporting limits. Sample-specific limits are indicated by results annotated with '






PARAMETER RESULT UNITS DF *PQL METHOD/ ANALYZED BY MOTES

Arsenic, Total 98.5 mg/Kgdrywt 2.0 0.8 6010/200. ,7 12/13/99 EM 1 Iron, Total 36200. mg/Kgdrywt 2.0 2.5 6010/200, .7 12/13/99 EM T_

Manganese, Total 508. mg/Kgdrywt 2.C 0.50 6010/200. -7 12/13/99 EM 1

PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sample-

specific reporting limits. Sample-specific limits are indicated by results annotated with '..\ ~2\) Vv n i l > . < , k IJ (Mil) (M S 1 i\ rMH; .,ii-lo(. (.'in s ~ i 2 i i iu I i v (Jo


http:95093.03


Lab Nutter : WP-4848-21 CLIENT: KARL KASPER Report Date: 12/29/99

Wocdard & Curran PO No- : 95093.03 41 Hutchins Dr. Project : SACO LF Portland, ME 04102




PARAMETER RESULT UNITS DF *PQL METHOD . ANALYZED BY NOTES


* PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sannplespecific reporting limits. Sample-specific limits are indicated by results annotated with '






SD-13 (DUP) Solid D.DINSMORE 11/19/99 11/19/99


Arsenic, Total 105. rrg/Kgdrywt 2.0 0.8 6010/200 .7 12/12/99 EM 1

Iron, Total 39000. mg/Kgdrywt 2.0 2.5 6010/200 .7 12/12/99 EM 1

Manganese, Total 551. mg/Kgdrywt 2.0 0.50 6010/200 .7 12/12/99 EM 1

* PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sarnplespecific reporting limits. Sample-specific limits are indicated by results annotated with '



Woodard & CXirran PO No. : 95093.03 41 Hutchins Dr. Project ; SACO LF Portland, ME 04102




PARAMETER RESULT UNITS DF *PQL METHOD ; ANALYZED BY NOTES






Wbodard & Curran PO No. : 95093.03 41 Hutchins Dr. Project : SACO LF Portland, ME 04102





Arsenic, Total 29.8 mg/Kgdrywt 1.0 0.8 6010/200 .7 12/06/99 KD 1 Iron, Total 10400 . mg/Kgdrywt 1.0 2.5 6010/200. .7 12/06/99 KD 1 Manganese, Total 85.1 mg/Kgdrywt 1.0 0.50 6010/200. .7 12/06/99 KD 1



Lab NuTTber : WP-4848-23 CLIENT: KARL KASPER Report Date: 12/29/99




SD-52 Solid D.DINSNORE 11/19/99 11/19/99











Arsenic, Total 6.8 mg/Kgdrywt 1. .0 0.8 6010/200. .7 12/07/99 KD 1 Iron, Total 10300. mg/Kgdrywt 1. .0 2.5 6010/200, .7 12/07/99 KD 1 Manganese, Total 162. mg/Kgdrywt 1. 0 0.50 6010/200. .7 12/07/99 KD 1

* POL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sample-


Katahdin A N A L Y T I C A L SERVICES










, Katahdin A N A L Y T I C A L S E R V I C E S

Lab Number : WP-4848-25 CLIENT: KARL KASFER Report Date: 12/29/99

Woodard & Curran PO No. : 95093.03 41 Kutchins Dr. Project : SAGO LF Portland, ME 04102




PARAMETER RESULT UNITS DF *PQL METHOD ' ANALYZED BY NOTES

Arsenic, Total 3.5 mg/Kgdrywt 1. .0 0.8 6010/200 .7 12/07/99 KD 1 Iron, Total 7950. mg/Kgdryv7t 1. .0 2.5 6010/200 .7 12/07/99 KD 1 Manganese, Total 202 . mg/Kgdrywt 1. .0 0.50 6010/200 .7 12/07/99 KD 1



t Katahdin A N A L Y T I C A L S E R V I C E S





SD-9 Solid D.DTNSMORE 11/19/99 11/19/99


Solids-Total Residue (TS) 54. wt % 1.0 0.10 CLP/CIP SOW 11/29/99 OF



klCatahdin A N A L Y T I C A L S E R V I C E S







Arsenic, Total 1. 5 mg/Kgdrywt 1.0 0.8 6010/200.7 12/07/99 KD 1 Iron, Total 5760. mg/Kgdrywt 1.0 2.5 6010/200.7 12/07/99 KD 1 Manganese, Total 255 . mg/Kgdrywt 1.0 0.50 6010/200.7 12/07/99 KD 1

* PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sairplespecific reporting limits. Sample-specific limits are indicated by results annotated with '







Solids-Total Residue (TS) 68. wt % l.C 0.10 CLP/CZP SOW 11/29/99 JF 1




Woodard & Curran PO No. : 95093.03 41 Hutchins Dr. Project : SAOO LF Portland, KE 04102





Arsenic , Total 11. mg/Kgdrywt 1. 0 0.8 6010/200 .7 12/07/99 KD 1 Iron, Total 14400. mg/Kgdrywt 1. 0 2.5 6010/200 .7 12/07/99 KD 1 Manganese, Total 576. mg/Kgdrywt 1. .0 0.50 6010/200, .7 12/07/99 KD 1











specific reporting limits. Sample-specific limits are indicated by results annotated with ' * i i f "^d


12/29/99

http:95093.03


Woodard & Curran PO No. : 95093.03 41 Hutchins Dr. Project . SACX) LF Portland, ME 04102



SD-103 (DUP) Solid D.DINSMORE 11/19/99 11/19/S9


Arsenic, Total 10. nrg/Kgdrywt 1.0 0.8 6010/200 .7 12/07/99 KD 1 Iron, Total 17800. mg/Kgdrywt 1.0 2.5 6010/200 .7 12/07/99 KD 1 Manganese, Total 557. mg/Kgdrywt 1.0 0.50 6010/200 .7 12/07/99 KD 1












specific reporting limits. Sample-specific Units are indicated by results annotated with '






PARAMETER RESULT UNITS DF *PQL METHOD' ANALYZED BY NOTES

Arsenic, Total 12.4 mg/Kgdrywt 1.0 0.8 6010/200 .7 12/07/99 KD 1 Iron, Total 5360. mg/Kgdrywt 1.0 2.5 6010/200, .7 12/07/99 KD 1

Manganese, Total 262. mg/Kgdrywt 1.0 0. 50 6010/200. .7 12/07/99 KD 1










* FQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect saitplespecific reporting limits. Sanple-specific limits are indicated by results annotated with 'l i In (MM |!(. !)V, Ul (Jn"1 s" i :j(i I I • ,


1

12/29/99

http:95093.03








Arsenic, Total 14 . 4 mg/Kgdrywt 1.0 . 0.8 6010/200.7 12/07/99 KD 1

Iron, Total 5080. mg/Kgdrywt 1. 0 2.5 6010/200.7 12/07/99 KD 1 Manganese, Total 270. mg/Kgdrywt 1. 0 0.50 6010/200.7 12/07/99 KD 1



tKatahdin A N A L Y T I C A L S E R V I C E S







Solids-Total Residue (TS) 78. wt % 1.0 0.10 CLP/CIP SOW 11/29/99 OF


specific reporting limits. Sample-specific limits are -ndicated by results annotated with ' 1)1, HSC, i l ,'l~lit~i ' i ( l l ) I n 'JTi —- p [ ) _ " >


1

12/29/99

http:istlmi.ikhttp:95093.03







Arsenic, Total 16.8 mg/Kgdrywt 1.0 0.8 6010/200.7 12/07/99 KD 1

Iron, Total 5650. mg/Kgdrywt 1.0 2.5 6010/200.7 12/07/99 KD 1

Manganese, Total 405. mg/Kgdrywt 1.0 0.50 6010/200.7 12/07/99 KD 1



,Katahdin A N A L Y T I C A L S E R V I C E S





SD-84 Sol id D. DINSMORE 11/19/99 11/19/99






Lab Number : WP-4848-32 CLIENT: KARL RASPER Report Date: 12/29/99

Woodard & Curran PO No. : 95093 .03 41 Hutchins Dr. Project : SACO LF Portland, ME 04102




PARAMETER RESULT UNITS DF *PQL METHOD i ANALYZED BY NOTES

Arsenic, Total 17. 3 mg/Kgdrywt 1.0 0.8 6010/200 .7 12/07/99 KD 1 Iron, Total 8130. mg/Kgdrywt 1.0 2.5 6010/200. .7 12/07/99 KD 1 Manganese, Total 464 . mg/Kgdrywt 1.0 0.50 6010/200. .7 12/07/99 KD 1

* PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect saiplespecific reporting limits. Sample-specific limits are indicated by results annotated with '



41 Hutchins Dr. Project : SACO LF Portland, ME 04102




PARAMETER RESULT UNITS DF *PQL METHOD ANALYZED BY MOTES



specific reporting limits. Sample-specific limits are indicated by results annotated with '. \ \ i M h o n k M l O H J ' J S K l on ,s " i - 2 - i i » j l.iv (2»~.i ™"..io.!'i


http:95093.03

Lab Number : WP-4848-33 CLIENT: KARL RASPER Report Dare: 12/29/99






Arsenic, Total 18.3 mg/Kgdrywt 1.0 0.8 6010/200. .7 12/07/99 KD 1 Iron, Total 6380. mg/Kgdrywt 1.0 2.5 6010/200. .7 12/07/99 KD 1 Manganese, Total 338. mg/Kgdrywt 1.0 0.50 6010/200. .7 12/07/99 KD 1

* PQL {Practical Quantitation Level) represents laboratory reporting limits and may not reflect sample-



http:95093.03







PARAMETER RESULT UNITS DF *PQL METHOD < ANALYZED BY NOTES










Arsenic, Total 14.2 mg/Kgdrywt 1. .0 0.8 6010/200.7 12/07/99 KD 1

Iron, Total 7340. mg/Kgdrywt 1. .0 2.5 6010/200.7 12/07/99 KD 1

Manganese, Total 122 . mg/Kgdrywt 1,0 12/07/99 KD 1. 0.50 6010/200.7

* PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sairplespecific reporting limits. Sample-specific limits are indicated by results annotated with '







PARAMETER RESULT UNITS DF *PQL METHOD • ANALYZED BY NOTES

Solids-Total Residue (TS) 80. wt % l.C 0.10 CLP/CIP SOW 11/29/99 JF

* PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sarplespecific reporting limits. Sample specific limits are indicated by results annotated with '

.Katahdin

^^^^^^^^^^^^^^^^M PREPARATION BLANK REPORT

Sample ID: PBWPL02ICWO Batch ID: PL02ICWO

Client: UJ obsf 6s e,( «- #X.Vt«,vv_ Work Order:

Element Name

ALUMINUM

ANTIMONY

ARSENIC

BARIUM

BERYLLIUM

BORON

CADMIUM

CALCIUM

CHROMIUM

COBALT

COPPER

IRON

LEAD

MAGNESIUM

MANGANESE

MOLYBDENUM

NICKEL

POTASSIUM

SELENIUM

SILICON

SILVER

SODIUM

STRONTIUM

THALLIUM

TIN

TITANIUM

VANADIUM

ZINC

Result Flag

0.01 U

0.002 U 0.002 U 0.001 1 J 0.0001 U

0.0144 J 0.003 U

0.02 J 0.0007 U 0.0007 U

0.0013 J 0.007 J 0.0007 U

0.01 U

0.0003 J 0.0009 U

0.0009 U 0.4 U

0.003 U 0.15 J

0.001 U

0.05 J 0.00008 J 0.002 U

0.002 U

0.0004 U

0.0007 U

0.0030 J

ttifWYt

PQL

0.10

0.008

0.008

00050

0.0050

0.100

0.010

0.05

0.0150

0.0300

0.0250

0.025

0.0050

0.05

0.0050

0.100

0.0400

1.0

0.010

0.20

0.015

0.10

0.100

0.015

0.100

0.0150

0.0250

0.0250

Units: mg/L

File

APL03B

APL04B

APL04B

APL03B

APL03B

APL03B

BPL03A

BPL03A

APL03B

APL03B

APL03B

BPL03A

APL04B

BPL03A

APL03B

APL04B

APL03B

BPL03A

APL03B

BPL03A

APL03B

BPL03A

APL04B

APL04B

APL04B

APL04B

APL03B

APL03B

U The analyte was not detected in the sample at a level greater than the instrument detection limit

J The analyte was detected in the sample at a concentration greater than the instrument detection limit, but

less than the laboratory's Practical Quamitation Level

11 The analyte was detected in the sample at a concentration greater than the laboratory's acceptance limit


trCatahdin A N A 1, Y T I C A L

PREPARATION BLANK REPORT

Sample ID: PBSPL03ICSO

Client:

Element Name

ALUMINUM

ANTIMONY

ARSENIC

BARIUM

BERYLLIUM

BORON

CADMIUM

CALCIUM

CHROMIUM

COBALT

COPPER

IRON

LEAD

MAGNESIUM

MANGANESE

MOLYBDENUM

NICKEL

SELENIUM

STRONTIUM

THALLIUM

TIN

TITANIUM

VANADIUM

ZJNC

Result

1.

0.2

0.2

0.04

0.01

0.64

0.01

0.8

0.07

0.07

0.1

0.8

0.07

0.6

0.02

0.09

0.09

0.3

0.007

0.2

3.4

0.04

0.07

0.16

BatchID:PL03ICSO

Work Order:

Flag

U

U

U

J U

J U

U

U

U

U

U

U

U

U

U U U U U J U

U

J

PQL

10.0

0.800

0.800

0.500

0.500

10.0

1.00

5.00

1.50

3.00

2.50

2.50

0.500

5.00

0.500

100

4.00

1.00

100

1.50

10.0

1.50

2.50

2.50

Units: mg/kgdryvvt

File

APL06C

APL06C

APL06C

APL06C

APL06C

APL06C

APL06C

APL06C

APL06C

APL06C

APL06C

APL06C

APL06C

APL06C

APL06C

APL06C

APL06C

APL06C

APL06C

APL06C

APL06C

APL06C

APL06C

APL06C

U The analytc was not detected in the sample ai a level greater than the instrument detection l imi t

J The analytc was detected in the sample at a concentration greater than the instrument detection limit, but

less than the laboratory's Practical Quantitation Level

H The analytc was detected in the sample at a concentration greater than the laboratory's accepumx limit


LABORATORY CONTROL SAMPLE REPORT

Sample ID: LCSWPL02ICWO Batch ID:PL02ICWO Units: mg/L

Client: UU»t>dci^A i- ClAs- Work Order:

Element Name True Value Result % REC Fla{ Limits File

ALUMINUM 2.00 2.27 113.5% 80. 120. APL03B ANTIMONY 0.500 0.482 96.4% 80. 120. APL04B ARSENIC 2.00 1.96 98.0% 80. 120. APL04B BARIUM 2.00 2.07 103.5% 80. 120. APL03B BERYLLIUM 0.0500 0.0508 101.6% 80. 120. APL03B BORON 0.500 0.499 99.8% 80. 120. APL03B CADMIUM 0.050 0.055 110.0% 80. 120. BPL03A CALCIUM 2.50 2.52 100.8% 80. 120. BPL03A CHROMIUM 0.200 0.216 108.0% 80. 120. APL03B COBALT 0.500 0.538 107.6% 80. 120. APL03B COPPER 0.250 0.253 101.2% 80. 120. APL03B IRON 1.00 1.01 101.0% 80. 120. BPL03A LEAD 0.500 0.525 105.0% 80. 120. APL04B MAGNESIUM 5.00 4.83 96.6% 80. 120. BPL03A MANGANESE 0.500 0.538 107.6% 80. 120. APL03B MOLYBDENUM 0.300 0.290 96.7% 80. 120. APL04B NICKEL 0.500 0.544 108.8% 80. 120. APL03B POTASSIUM 25.0 23.7 94.8% 80. 120. BPL03A SELENIUM 2.00 2.03 101.5% 80. 120. APL03B SILICON 5.23 5.54 105.9% 80. 120. BPL03A SILVER 0.050 0.050 1 00.0% 80. 120. APL03B SODIUM 7.50 7.10 94.7% 80. 120. BPL03A STRONTIUM 0.500 0.534 106.8% 80. 120. APL04B THALLIUM 2.00 2.04 102.0% 80. 120. APL04B TIN 0.500 0.493 98.6% 80. 120. APL04B TITANIUM 1. 00 0.990 99.0% 80. 120. APL04B VANADIUM 0.500 0.521 104.2% 80. 120. APL03B ZINC 0.500 0.505 101.0% 80. 120. APL03B



Sample ID: LCSSPL03ICSO

Client:

Batch ID:PL03ICSO

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• Road No. 5 CHAIN of CUSTODY Westbrook. ME 04092 Tel: (207) 874-2400 Fax: (207) 775-4029 PLEASE PRINT IN PEN Page ' of2.

Client

Address / /

Purchase Order #

V_ Contact

Proj. Name/No.

Phone #

state Mr

Fax#

Katahdm Quote #

Bill (if different than above) Address

KATAHDIN PROJECT MANAGER Filt. Filt. Filt. Filt. Filt. Filt. Filt. Filt. Filt. Filt. OYDN OYON OYDN DYCJN OYON OYON OYON OYON DYDN OYHN

REMARKS:

i SHIPPING INFO: O FED EX O UPS O CLIENT

AIRBILL NO: || TEMP°C O TEMP BLANK O INTACT O NOT INTACT if J

1 i ** *^

Date /Time No. OfSample Description Matrixcoll'd Cntrs.*

SUJ-)o2> n/i9/»/ r .̂6 ) I *

.Suj-iosO^) H/W/9/ 1 ) ll/W/99/ 1 )

f5p-/o^ro^ >V'^/ I ll/t^/^SU-9S 1

SD-98 ll/p/V' 1̂ \ Sui-Q3 u//^/ )

SD-93 H//^/^ i 1 1 \flQ.f^f/ I 1

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1

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»l/»9/95/ (STV/^ I COMMENTS y. /^/^-p -far As Fe M ̂ also

' / '

RsKnquishedJSy: (Signature) Date / Time Rece ved By: (Signature) Relinquished By: (Signature) Date / Time Received By: (Signature)

Relinquished By: (Signature) Date / Time Received ffy: (S gnature) Relinquished By: (Signature) Date / Time Received By: (Signature)

RMSOUP.CE INC 'S (207) 782-3311 3M I CHN-OF-CSTDY

ORIGINAL Katahdin Analytical Services 0000060

http:RMSOUP.CE

•̂M^VWM^^^^^^^H -44U Lounly Koad IN. 5 CHAIN of CUSTODY •UlQlUl̂ MHIIpRII P.O. Box 720 HBUuHAlLSl̂ imjm We^lhrnok- MR 04092

JUHJHlBgiaaiHHB Tel: (207) 874-2400 ••••••̂ •••i Fax:(207)775-4029 PLEASE PRINT IN PEN Paae ^ of"2

Client , , _ | Contact J-'d.Di^ \^V\A^>* -v2*-LX_ LAB USE ONLY ^^ |̂j|̂ |̂̂ ^^_^^g ANA! A'SIS^ND CONTAINER TYPE

KATAHDIN PROJECT MANAGER Filt. Filt. Filt. Filt. Filt. Filt. Filt. Filt. Filt. Filt. OYL-JN DYDN OYDN OYDN OYON OYON OYON OYON HY3N DYON

REMARKS: O

SHIPPING INFO: D FED EX D UPS O CLIENT ~ J

AIRBILL NO: PTEMP°C D TEMP BLANK O INTACT O NOT INTACT

* Sample Description Date /Time coll'd Matrix

No. of Cntrs.

5W-31 ^I

Attachment 2

Reports of Analysis

Groundwater

SACO MUNICIPAL LANDFILL NOVEMBER 1999 MONITORING

SAMPLE SUMMARY BY LABORATORY WORK ORDER

Surfece Water SW-103 SW-103 (DUP) SW-98 SW-93 SW-84 SW-73 SW-69 SW-15 SW-31 SW-34 SW-37 SW-13 SW-13(DUP) SW-52 SW-21 SW-9 SW-7

Sediment SD-103 SD-103 (DUP) SD-98 SD-93 SD-84 SD-73 SD-69 SD-15 SD-31 SD-34 SD-37 SD-13 SD-13(DUP) SD-52 SD-21 SD-9 SD-7

Work Order i WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848 WP4848

Groundwater . j ..» i- Work Order MW-95-5R WP4803 MW-95-5R (DUP) WP4803 MW-95-8S WP4803 MW-97-18S WP4803 EQ-1 WP4803 MW-97-14S1 WP4803 MW-97-14S2 WP4803 MW-95-4SA WP4803 MW-95-4SB WP4803 MW-97-19S WP4803 MW-95-9S WP4825 MW-95-11S WP4825 MW-97-17R WP4825 MW-95-8R WP4825 MW-97-13S1 WP4825 MW-97-13S2 WP4825 MW-97-13R WP4825 TB-1 WP4764 MW-95-1R WP4764 MW-95-1S WP4764 MW-95-4RD WP4764 MW-95-3R WP4764 MW-95-4R WP4764 MW-13 WP4764 MW-13 (DUP) WP4764 MW-13 MS WP4764 MW-13 MSD WP4764 MW-95-6S WP4781 MW-93-3 WP4781 MW-95-6R WP4781 MW-97-16S WP4781 MW-95-7S WP4781 MW-95-7S (DUP) WP4781 MW-95-7R WP4781 MW-93-5 WP4781 MW-96-9R WP4781

U:/projects/sacoLF/nov99samploing/sampling summary.doc

.Katahdin T I C A L S E R V I C E S

December 14, 1999

Mr. Karl Kasper

Woodard & Cuiran

41HutchinsDr.

Portland, ME 04102



Dear Mr. Kasper:


* Report of Analysis »



* Confirmation




Sincerely,


Authorized Signature Date

340 County Road No. 5 210 W«t Road No.5, Portsmouth, NH 03801 P.O. Box 720, Westbrook, ME 04098 ht tp //katahdmlab com Tel- (603) 431-5777 Fax: (603) 436-3356 Tel. (207) 874-2400 Fax: (207) 775-4029 Katahdin Analytical Services 0000001

vKatahdin S E R V I C E S

TECHNICAL NARRATIVE

For work order WP4803 results for Arsenic analyses performed according to EPA 6010/200.7 have been reported to client-specified levels. These levels are indicated in the results and PQL fields of the analytical report.

340 County Road No. 5 210 Wcsi Road No.5. Porumouih, NH 03801 P.O. Box 720. Wcstbrook, ME 04098 hup://katahd inlab.com Tel: (603) 431-5777 Fax: (603) 436-3356 Tel: (207) 874-2400 F«: (207) 775-4029



CLIENT: KARL KASPER Report Date: 12/14/99 Woodard & Curran PO No. : 95093.03 41 Hutchins Dr. Project : SAOO LF Portland, ME 04102


SAMPLE DESCRIPTICN MATRIX SAMPLED BY SAMPLED DATE RECEIVED

MW-95-5R Aqueous D.DTNSMORE 11/17/99 11/17/99

PARAMEIER RESULT UNITS DP *PQL METHOD ANALYZED BY NOTES

Arsenic, Total 0.018 mg/L 1.0 0.005 6010/200.7 12/06/99 EM 1 Iron, Total 0.051 mg/L 1.0 0.025 6010/200.7 12/06/99 EM I Manganese, Total 2'>

Katahdin Analytical Services OOOOOOc

http:95093.03


Lab Number : WP-4803-2 CLIENT; KARL KASPER Report Date: 12/14/99



SAMPLE' DESCRIPTION MATRIX SAMPLED BY SAMPLED DATE RECEIVED

MW-95-5R(DUP) Aqueous D.DINSMDRE 11/17/99 11/17/99


Arsenic, Total 0.018 mg/L 1.0 0.005 6010/200.7 12/06/99 EM 1 Iron, Total 0.032 tng/L 1.0 0.025 6010/200.7 12/06/99 EM 1 Manganese, Total U . \\Vstbr.Mil,. Ml-. O-lO'JS Tel (6031 431 -ST'7? l-'as. (603) 43fc-3'56 'Id (2tt~l S~4-24(W FJ* CII7) "S-402'J

Katahdin Analytical Services 000000.

http:Vstbr.Milhttp:95093.03




SAMPLE DESCRIPTICN MATRIX SAMPLED BY SAMPLED DATE RECEIVED

MW-95-8S Aqueous D.DXNSMORE 11/17/99 11/17/99


Arsenic, Total


Woodard & Curran PO No. : 95093.03 41 Rutchins Dr. Project : SACO LF Portland, ME 04102


SAMPLE DESCRIP1TCN MATRIX SAMPLED BY SAMPLED DATE RECEIVED

MW-97-18S Aqueous D.DINSMORE 11/17/99 11/17/99

PARAMETER RESULT UNITS DF *PQL METHpD ANALYZED BY NOTES

Arsenic, Total

.Katahdin ANALYTICAL SERVICES


Wocxiard & CXtrran PONb. : 95093.03 41 Hutchins Dr. Project : SACO LF Portland, ME 04102



EQ-1 Aqueous D.DTNSMORE 11/17/99 11/17/99


Arsenic, Total


Wcodard & Curran PO No. : 95093.03 41 Hutchins Dr. Project : SAOO LF Portland, ME 04102


SAMPLE -DESCRIPTION MATRIX SAMPLED BY SAMPLED DATE RECEIVED

MW-97-14S1 Aqueous D.DINSMORE 11/17/99 11/17/99


Arsenic, Total 0.242 mg/L 1.0 0.005 6010/200 .7 12/06/99 EM 1 Iron, Total 18.8 ng/L 1.0 0.025 6010/200 .7 12/06/99 EM 1 Manganese, Total 1.73 ng/L 1.0 0.0050 6010/200 .7 12/06/99 EM 1

* PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sanplespecific reporting limits. Sample-specific limits are indicated by results annotated with '. « cMhriioL. Ml II i()'),S '111: (!»'', JT-i-2-1(IO I.is: (21171 "V





SAMPLE DESCRIPTION MATRIX SAMPLED BY SAMPD3D DATE RECEIVED

MW-97-14S2 Aqueous D.DTNSM3RE 11/17/99 11/17/99


Arsenic, Total 0.186 mg/L 1.0 0.005 6010/200 .7 12/06/99 EM 1 Iron, Total 24 .5 mg/L 1.0 0.025 6010/200 .7 12/06/99 EM 1 Manganese, Total 3.26 mg/L 1.0 0.0050 6010/200 .7 12/06/99 EM 1


specific reporting limits. Sample-specific limits are indicated by results annotated with '. \ \ iMhrouL . Ml II-,0')S Id iwi.i)-»3I->~T H. Kl CO") S'4-2400 Ku (1\>~) — i-KU'I

Katahdin Analytical Services 000000!

http:95093.03


Lab Number : WP-4803-B CLIENT: KARL KASPER Report Date: 12/14/99




MW-95-4SA Aqueous D.DINSMORE 11/17/99 11/17/99


Arsenic, Total 0.201 mg/L 1.0 0.005 6010/200 .7 12/06/99 EM 1 Iron, Total 58 .6 mg/L 1.0 0.025 6010/200 .7 12/06/99 EM 1 Manganese, Total 9.94 mg/L 1.0 0.0050 6010/200 .7 12/06/99 EM 1




http:95093.03

Lab Number : WP-4803-9 CLIENT; KARL KASPER Report Date: 12/14/99

Wcodard & Curran PO No. : 95093.03 41 Hutchins Dr. Project : SACO LF Portland, ME 04102



MW-95-4SB Aqueous D.DINSMORE 11/17/99 11/17/99


Arsenic, Total 0.098 mg/L 1.0 0.005 6010/200.7 12/06/99 EM 1 Iron, Total 23.1 mg/L 1.0 0.025 6010/200.7 12/06/99 EM 1 Manganese, Total 11.1 mg/L 5.0 0.0050 6010/200.7 12/06/99 KD 1

* PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sanplespecific reporting limits. Sample-specific limits are indicated by results annotated with '





MW-97-19S Aqueous D.DIMSMORE 11/17/99 11/17/99

PARAMb'l'KK RESULT UNITS DF *PQL METHOp ANALYZED BY NOTES

Arsenic, Total 0.144 tng/L 1.0 0.005 6010/200.7 12/06/99 EM 1 Iron, Total 27.2 wg/L 1.0 0.025 6010/200.7 12/06/99 EM 1 Manganese, Total 8.47 mg/L 1.0 0.0050 6010/200.7 12/06/99 EM 1

* PQL (Practical aiantitation Level) represents laboratory reporting limits and may not reflect sanplespecific reporting limits. Sample-specific limits are indicated by results annotated with '

kj\atahdin A N A L Y T I C A L S E iv \ 1 C t S ̂ ^^^^^^^^^^^^^^^^^^^^^^^^^^^^^^^^^^^^^^^^^^^^^II^H


Sample ID: PBWPL05ICWO

Client: U)6t>dti^d

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Sample ID: LCSWPL05ICWO Batch ID: PL05ICWO Units: mg/L

Client: IjJooci&AsJL* OUAAO^ Work Order: Mf^SC?,

Element Name True Value ' Result % REC Flag Limits File ANTIMONY

ARSENIC

BARIUM

BERYLLIUM

BORON

CALCIUM

CHROMIUM COBALT

COPPER

IRON

MAGNESIUM MANGANESE

MOLYBDENUM NICKEL

SELENIUM

SILVER

THALLIUM TIN TITANIUM

VANADIUM ZINC

0.500

2.00 2.00 0.0500

0.500

2.50 0.200 0.500

0.250

1.00 5.00 0.500

0.300

0.500 2.00

0.050 2.00 0.500 1.00

0.500 0.500

0.496

1.99 2.26 0.0504

0.498

2.55 0.213 0.545

0.269

1.10 5.13 0.549 0.314 0.571 1.88 0.051 2.03 0.546

1.04 0.521 0.507

99.2% 99.5% 113.0%

100.8%

99.6% 102.0%

106.5% 109.0%

107.6%

110.0% 102.6%

109.8% 104.7%

114.2%

94.0% 102.0%

101.5% 109.2%

104.0%

104.2%

101.4%

80. 80. 80. 80. 80. 80. 80. 80. 80. 80. 80. 80. 80. 80. 80. 80. 80. 80. 80. 80. 80.

120.

120. 120. 120. 120. 120. 120. 120. 120. 120. 120. 120. 120. 120. 120. 120. 120. 120. 120. 120. 120.

APL05A

APL05A APL05A

APL05A

APL05A

APL05A

APL05A

APL05A

APL05A

APL05A APL05A

APL05A

APL05A APL05A

APL05A

APL05A

APL05A

APL05A

APL05A

APL05A APL05A


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•Onoraim £%%?* CHAIN oi CUSTODY m^myî lgjjEm Westbrook. ME 04092

UUHUiaUll ,'1';::™- PLEASE PRINT IN PEN Page of Client . Contact Weiri Phone # Fax#

lObctkz Address AJ | I ®tate Zip Code p^i i. _4i*̂ l̂ > ' . Tby ^^ ^ >*M -1 MP Purchase Order # Proj-Name/NaSUc

,JK.atahdin :AL s E R V I C ES

December 14, 1999

Mr. Karl Kasper

Woodard & Curran

41 Hutchins Dr.

Portland, ME 04102



Dear Mr. Kasper:


* Report of Analysis »



* Confirmation




Sincerely,


Authorized Signature Date

340 County Road No. 5 210 West Road No.5, Portsmouth, NH 03801 P.O. Box 720, Westbrook, ME 04098 http.//katahdin!ab com Tel: (603) 431 -5777 Fax: (603) 436-3356 Tel. (207) 874-2400 Fax- (207) 775-4029 Katahdin Analytical Services 0000001

Katahdin A N A L Y T I C A L

TECHNICAL NARRATIVE

For work order WP4825 results for Arsenic analyses performed according to EPA 6010/200.7 have been reported to client-specified levels. These levels are indicated in the results and PQL fields of the analytical report.

340 County Road No. 5 210 West Road No. 5. Portsmouth, NH 03801 P.O. Box 720, Wcstbrook, ME 04098 Tel: (207) 874-2400 Fax: (207) 775-4029

htrp'/i 'k jtjhdinlab.com TcL (603) 431-5777 Fax: (603) 436-3356






MW-95-9S Aqueous D.DINSMORE 11/18/99 11/18/99


Arsenic, Total cO.005 mg/L 1.0 0.005 6010/200.7 12/02/99 EM Iron, Total 0.64 mg/L 1.0 0.02 6010/200.7 12/02/99 EM Manganese, Total 1.16 mg/L 1.0 0.0050 6010/200.7 12/02/99 EM

* POL (Practical Ouantitation Level) represents laboratory reporting limits and may not reflect sample-







MW-95-11S Aqueous D.DDJSMORE 11/18/99 11/18/99


Arsenic, Total

Lab Number : WP-4825-3 CLIENT: KARL RASPER Report Date: 12/14/99




MN-97-17R Aqueous D.DTNSMORE 11/18/99 11/18/99

PARAMETER RESULT UNITS DF *PQL METHOD ANALYZED BY NOTES t

Arsenic, Total



Wbodard & Curran PO No. : 95093.03 41 Hutchins Dr. Project : SAOO LF Portland, ME 04102



MW-95-8R Aqueous D.DTNSMDRE 11/18/99 11/18/99

PARAMETER RESULT UNITS DF *PQL METHOD ANALYZED BY NOTES /

Arsenic, Total 0. .137 mg/L 1.0 0.005 6010/200 .7 12/02/99 EM 1 Iron, Total 40, .6 mg/L 1.0 0.02 6010/200 .7 12/02/99 EM 1 Manganese, Total 12, .2 mg/L 5.0 0.0050 6010/200 .7 12/04/99 KD 1

* PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sanplespecific reporting limits. Sample-specific limits are indicated by results annotated with '.i\ "JO. VU-MhmuL. Ml. (N0')l> Tel: C") .X'-t-VllXI l-'jv (21P) r'S-102'J

Tel: (60.)) 431-5777 hix: (003) 4.

7



Wbodard & Curran PO No. : 95093.03 41 Hutchins Dr. Project : SACO IF Portland, ME 04102





Arsenic, Total 0.907 mg/L 1.0 0.005 6010/200.7 12/02/99 EM 1 Iron, Total 78.2 mg/L 1.0 0.02 6010/200.7 12/02/99 EM 1 Manganese, Total 1.17 itg/L 1.0 0.0050 6010/200.7 12/02/99 EM 1

* PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sanplespecific reporting limits. Sample-specific limits are indicated by results annotated with '

Lab Nuniber : WP-4825-6 CLIENT: KARL KASPER Report Date: 12/14/99






Arsenic, Total 0.666 tng/L 1.0 0.005 6010/200 .7 12/02/99 EM 1 Iron, Total 35 .9 mg/L 1.0 0.02 6010/200 .7 12/02/99 EM 1 Manganese, Total 0.422 tng/L 1.0 0.0050 6010/200 .7 12/02/99 EM 1


specific reporting limits. Sample-specific limits are indicated by results annotated with ' 7"i-J():'l


http:95093.03





MW-97-13R Aqueous D.DINSMORE 11/18/99 11/18/99


Arsenic, Total 0.030 mg/L 1.0 0.005 6010/200.7 12/02/99 EM 1 Iron, Total 36.0 mg/L 1.0 0.02 6010/200.7 12/02/99 EM 1 Manganese, Total 1.25 mg/L 1.0 0.0050 6010/200.7 12/02/99 EM 1


specific reporting limits. Sample-specific limits are indicated by results annotated with ' —


http:95093.03

iKatahdin

A N A L Y T I C A L SE^MCLS^^^^^^^^^^^^^^^^^^^^^^^^H


Sample ID: PBWPL01ICW2 Batch ID: PL01ICW2 Units: mg/L

Client: £{)&>&d.ab

BBBJ8MBBI E^ .— _ _ _

^^^^^•ANA! V T r c A L s E R s l J(Mct(lL4t} f G^fMO^ Work Order: kJ/>iff2S~

Element Name True Value Result % REC Flag Limits File

ALUMINUM 2.00 2.23 111.5% 80. 120. APL02A ANTIMONY 0.500 0.463 92.6% 80. 120. APL02A ARSENIC 2.00 1.90 95.0% 80. 120. APL02A BARIUM 2.00 2.06 103.0% 80. 120. APL02A BERYLLIUM 0.0500 0.0475 95.0% 80. 120. APL02A BORON 0.500 0.487 97.4% 80. 120. APL02A CADMIUM 0.0500 0.0529 105.8% 80. 120. APL02A CALCIUM 2.50 2.59 103.6% 80. 120. APL02A CHROMIUM 0.200 0.199 99.5% 80. '120. APL02A COBALT 0.500 0.510 102.0% 80. 120. APL02A COPPER 0.250 0.251 100.4% 80. 120. APL02A IRON 1.00 1.02 102.0% 80. 120. APL02A LEAD 0.500 0.518 103.6% 80. 120. APL02A MAGNESIUM 5.00 5.09 101.8% 80. 120. APL02A MANGANESE 0.500 0.508 101.6% 80. 120. APL02A MOLYBDENUM 0.300 0.283 94.3% 80. 120. APL02A NICKEL 0.500 0.526 105.2% 80. 120. APL02A POTASSIUM 25.0 25.0 100.0% 80. 120. BPL02A SELENIUM 2.00 1.82 91.0% 80. 120. APL02A SILICON 5.23 5.61 107.3% 80. 120. BPL02A SILVER 0.0500 0.0484 96.8% 80. 120. APL02A SODIUM 7.50 7.52 100.3% 80. 120. BPL02A STRONTIUM 0.500 0.513 102.6% 80. 120. APL02A THALLIUM 2.00 2.01 100.5% 80. 120. APL02A

Documents

, -vThruN R:CORDD CTS . R · 2020. 12. 4. · according to Metho 6010/200.7d Sedimen. t sample analyzes wer foed alsr tota o res.dual solidsl Th. e results of analysis are provided