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e CDM ~ ~ SCrel!l&t/3. ~ & msM~ ~
August 11, 1986
Mr. John Cochnm U.S. Environmental Protection Agency First International Suilding 1201 Elm Street Dallas, TX 7S270
IE& CLP Data at Koppers/Texarkana Site
Ooc. Ctrl. No.: 142-TSl-EP-DCPN-1
Dear John:
CAMP DRESSER & McKEE INC.
9U2 CaOilal Of Texas ~ay !-lotll'I A.ll)Qr8'Cm Plaza rwo, Sule 400 Au9llr'I. Texas 78759 s,2 3"5-6861
Per your request ( letter dated July 22, 1986), I am sending a copy of the analytical results from split samples at the Koppers/I'exarkana Site.
TWo of the CLP samples (CLP IMFC214 and iMf'C216) sent to Cambridge Analytical are still in the system. We are awaiting the results.
An extra copy of the data are included for transmission to Koppers. If you have any questions, do not hesitate to contact me.
Sincerely,
~X--ll Yl/curf'-i> --. .,,,, , / "Cv ~ . . I I
(
S. Lynn Mays Site Manager
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- Surface Water
- Ground Watar .. - Leachate Mi:11:ed Media
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@ ANALYSIS LAB:
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@ SAMPLE MArnIX (Check One)
_,Water -1 Soil/Sediment
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Attn: JA~ l'.'. WR.l(~;n______ 1raruder Ship To:
© For each sample collected specify number of containers used and mark volume lettel on each bottle.
® Anal~t..b: Rec'd by: ~ ~ r _ C Date Ree'd~~f/g_._{f_ t"
Water (Extractable)
Water (VOA)
Boll/Sediment Extraata.ble
Number of Approxnnate Containers Total Volume
Sample Condition ton Receipt (e.g., broken, no rice, Chain-of-Custody, etc.) 0
0
'D 8oil/8ecllment (VOA) -----1------+------~-----------! Other
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e e Or-ganic1 Anaty•is Data Sheet
(Page 1 J
• •':ioritOl'y Na-ne ~OUTHWE.fil lf..BORATORY OF' OKLA.
..... b S1 "l"lple 10 No ---~--_c._· _7_7-_____ _ C1uNo
QC Report No SI~ t.e.t,11. ~q_._f ____ _ Contr1:1 No §_8-01~7168/JA 68-01-7168/2~01u Jt..luu Aut~orized By ¼J!YeOt S_hri nr:,arpure Date Sample Reeeived '2.- '2-/ - ~ 6
,,.9,.3 7'-83 9 75.0,-4 7!,-00-3 75.09 2 67,6,4-1
,.,s.o ?S-3!>..t 75 3-4 -3 \56-6-0·S -
67,$6-3 ,0?,06-2 79.93.3 11-SS-6 56 23-S 109.05.4
,s 27-•
c1-11o•ome1"•"e
: Volatile Compounds ,/"7--... Concentr111ori . ...__..,o~· Medium (C1tele One}
Date E1e1r1c1td /Prepared
Date .4.nalV?ed
Cone 10,1 Factor __ ~ ___ pH __ :t..i-....·9 .... , __
Percent Moisture {No1 Dec11nted) _____ l_8--... __ _
ug 11o~ fCi~~
10 U
CAS Number ,a e1.s
.. , 2-01tl-\fo,oo•ooa "le
B • o.,...o.,..t ! "• l\e 10 U 10061-02-6 T,1.,.s 1 3'.01c"1o•oo•ooe..,e V,f'lyl Cl'llor1df lU U ?9-01,6 Tr 1c:h10,oe1 l'\f "'If-
Cl'\lo•oe111a l'lt 10 U 124-•B 1 D1b, 0":>0C hlo, o""e1 ha "t
M,: ... vle"'lt Cf\loridt ~ II 79.0().!, , 1. 2-Tric:hloroeitiane
A.:t101'\f 1 n II 71 .43 .1 Be rite"• C••bofl C>tsvff,de ; II 10061.01 -S c•s • 1 3-.D~c"lo• :i-o,o~"e , 1 .t,,c "10,o,e1heM Ci II , ,o.,s-e _'2 ·Cl'IIO'.(>toll-\\'ho'•fl\lelht•
I. 'l ,D,cf\lo•o,e~"•l'le .. 5 lJ ?S--25-2 B•o"'olon,-.
Trtl'\s · 1. 2·D,c!'\10,ot1hel'le 5 U S91 78-6 4 · Met"v'- 2-Pt "118 !'iO"lt --
CMorofo~m ... 5 II 10810-1 2-Hed"lone
1. 2 •011:hlo•o-etP-t• 'te ; II 127-16-4 t tu 1:;"ilo•oe1"ie"e .. .
2-8 JIit l'IOrit IOU 79.34 5 1 1. 'J 2-1e11ac,-,10,~1"•"'e ·--
1. t. ,,Tr,ehloroetl-iOl'le 5 U 108-86-3 Toh.rtl'lt
Cotbo ... Te1•acMor1de 5 U 108 90? Cblorobt•'l1tt"I~
V11•,yl Aettllf! 10 U 100-41 •• £1 h~lbtl'lteflt -
B · o~o.::1,c1-iro1 ometha l'le ~ 11 100-•2-s Styrene
_To111 SC\'lti,es
Dita fl:ti»t'l•"O 0...,ht,ers
,.,, 111,0.,,"0 ,.,.,111 10 Pl. ~ ftJJom"Q "91"""-• ,.,.,A .. ,a ••• I/Md
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5 u 5 u
10 U t; II
1.0 IJ 10 ii 5 II 5 U ; ,, 5 u-5 lJ $ u 5 II
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•n.tf!H ltl lflt .. ,~ 1-""""'i't filpOrl
laborinory Name SOUTHWEST , 9no~Y OF OKLA. s-c;{-/_ Cue No
Sample Number
Contract N 68-01~7168/~A 68•0blJiWil~ Analysis Data Sheet (Page 2)
Fe. 807
Semivolatile Compounds
Date AN tvz,ed
Cone/0,t Factor I Percent Moisture (Oecanted) ___ /_f?.._ ___ _
CAS NumMr 108-95-2 ,1,.44.4
95-57-8 541.73.1
106-46-7 100-51-6 95.50., 95-48-' ~
"38-32-9 4..4-S
-6A-7 .. 67-72-1 98-95-3 78-59•1 es-n.s 105-67-9 65-85-0 . ---
111,91-1 -
t20·83·2 120-82·1 91-20-3 106•41-B
e::.6s-3 59-S0-7 91.57.g
'147◄ 99.1'.)6.J 95.95., 9_1-58-? es.,, .• 131-U,3
"·96-B .. .J9,2
P1'enol
b•t' -2· Cl'\lo,oe1"iv1JE 11'\er 2•Chlorop"ienol
1 3-0,cn!orob!-ite"e
1 4•Drchlo,ob!l'ltf'"lf'
Be~tvl A.lcotiol , 2-0ichlorobenzpne
2-Me•"v'p"'e:1101 ..
b1S(2 •Cl-iloro1sop•opvl)E U,tr
4-Metl)vlp"'leno
N. N11roso-D••n-P1opvl&rT11ne
Mu.11ct-iI0,oeIhane
NrHobef\.te'"lf'
lsoo"iorone
2 -N1trop"ie nol
2 4-0ime!hylphtnol
Bentoic Acid
b,s, · 2 •Chloroe1holvlMe11-i11 rie 2 4-0u:t-ilorop,.,enol . 1. 2. 4-Trichlorobel"izene
.. ---
Naphrha le tie
4 ,C'1I0roan1hne
He11.achl~robu111~1e l'lt
4-Ctiloro-3 •Me_thylphel'lo1
2•Me1hrln•phIh1te11_e
Hell&chloroevclo~r11ad1ene
2. A. 6•Tr1chloroi,hen0I
2 . •. S-Tuchlorophef'IOI
2,Chlorott1phthale_iie
2-~11,oar11hn-e
O,methvl "'~1ha111e . -
Acenaphthvl•".le
3•N•ttoanihne
ug110~ (Ci,~
330 U 330 U 111'1 II 33_0 U 1':W " 330 U .. 330_U 330 U 330 11 330 U 110 II
3~0 II
-- 330 U_ 330 U 330 U 330 U
u;no 11
330 U ~-!JU U
330 U 330 U 11n II j:lfl II 330 U 330 U 330 U 3;m u
1600 II 3~0 ll --
H,nn II ~-:in ti
_ 330 U , ,:;nn 11
GPC Cleanup 0Yes ~No
Separatorv Funnel Exuae1iori OYes
Continuous L1Quid • LiQuid Eic1rac1,on OYes
CAS Numtar
83-32·9 51-28-S 100-02., 132-64 9 121.14.2
606-20-2 8--4 ·66-2 7005-72•3 86-?J., 100.01 ·6 534-52-1
86-30·6 101.55.3 118-?4-t
87•86·5
85-01-8 120-12-7 64.74.2 206,44-0 129-00-0 BS-68-7 91-94• 1 56-55-3 ,,,.e1.1
121 B-01-9 117,84-0 205.99.2 20?,08-9 )0·32-8 193.39.5, 53-10-3 19t2•-2
---AcMap"lt,-.ene
2. ••D1n1trophenol
4-Nitropheriol
D1be"llOfuran
2 il-01n1tro1oruene
2 6•01nitro1oluene
Diet hylpht ha la le
4-Ct-,loropl-ienvt-pt-ief'l}'.lf!tt-ier
Fluorene
4-Nittoanil,ne
4. 6-_0m1tr0·2·Metliylplienof
N-N ,troSodJt>l-ienvra~ine fl I 4 •8rornop"ienv)•Pl-ienvlett-ie~
~ellachlorobenre,,e
Pentac'1 lor opl-i ertol
Phen1,'11hrene
Anthr•cene
01-n-Bu~yJp1·oh111111e
Fluor•nthene
Pyrenl!!
Butylb,e r\tylphtha late
3. 3 ·.01chlorobenz1d1r11!
DenzO(&fAnthraeene
b~Sl2:Ethylhoyl)Phtti_atate
Chrvae~ 01,n,(xtyl Phthol1te
Sento(b)Fluorant~~
Bento(k~ I uorat1tl'IG1ie Ber,_rO(•)Pvrel'\O lndenoc,. 2. 3--cd_~•~ 01bel'lt!i hJAnt~r•e•~ Benra1.o h. ilPervlen~
(\J
0 Ug 110~ f'-
(C1tc~
:-no n 1600 U 1 f.(\O II 330 U 330 U :lJO l/ 330 U JjU U
330 ll 1600 U lbUU U ·nn 11
1~n II 330_U
1600 U 330 U 310 II 330 U 330 U
330 II 330 U 6~0 U ':l.'V1 II
~nn 11 330 U 330 U 330 II ..
330 11 330 U 3~n II ~'.tn II 330 II
7:85
r-e 0
La~o• •tof~ ,._,.,,.,t . SOUTHWEST .AJORY Of ,ill'J,AHOM~ t;: ~ t (
Cut ~o --------------~--Contract t 68·01-7168/lA or 2AO • A , · 0 t Sh t - rgan,cs na v11s I a ee
(Page 3}
Pt1ticidelPCBs
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St"n"le "-u: F\t,er r~ r ( - V (- ~I
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CAS Nul'l'lber
3, 9 84-6
319 85-? 3'1~•86-B
i$8 89·9 16-4.4-8 )09 00-2 1024,57-3 ig59 98·8 60-51-1
12-55-9
72·20·8 332\3-E:5 9 '2·S4·8 l031-07-S !)0 29 3 72-43-S
Sl49-'·'0-!i S. ,. "14-9 8Xll -35 2 12674-11•2 \ U04-28 2 111'1-16 5 ~3469-2\-9 '2Ei72·29-6 1109'1-69-1 1109682,!
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A•octo••l221
A1oclot-1ll2 A1oclot• 12'2 A10tlot.1248
Aroclor,1254 A,oc10,,t260
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16.0 U 80.0 U 16.0 U 80.0 U
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160.0 U 160.0 u
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Organics Anatysis Data Sheet (Page 4)
tentatively Identified Compounds
N....,..._ Compound N•rrHt Fraction
t.+c.J- 7C ·· 1 Ace he C,1___{_.A. J "h-1€ -f/4,., /es 1-<v Gtv1i -2. .-- (,<,..J<._ YL(J""t.Vi.L__ t.
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21.
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23
24. --
25. ---
28 27.
28. ---
21. -30. - -- -
form 1. f'art D
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Sample Number
F=C. t?bl-
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_, ~Number
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on each bottle. Date Rec'd: _,_.Jc.-/ __
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Airbill Number:
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Organic, Anafyai, Data Sheet · (Page 1)
r=-c ~ (e J 'be;;,(~
• -~ritory Na~e SOUTHWEST LABORATORY OF OKLA.
L..0 Sa~le 10 No __ ?-i_, ..... r-.... - -_? ..... (..__-. _____ _ OC Report No _____ r ________ _
Sa~ Matri1. ____ Sr _____ ._;_f _____ _ Con1r1et No 68~01-:7l68!1A 68-0l-7168L2h_
01t1 f!WNu A.uthorired By Jax:ant Shri n.3e,r0;ure Uate Sample Received 2.- 2 )- b c~
,,.e,.3 74.93.9 1$-01-4
7S-00-3 -. ~-2 64-1 ~ 5-0
S-35-4 ,s-34-3 156-60-S
67-66-3 -107-06,2-
78-93·3 '11.55.g
!,6 2J-!, 108-05-4 ?S-21-4 -
Volatile Compounds.
Concentr11ion. e Medium (Circle One)
Date h1r1etedlPrep1red --Date Analyzed
Cone/Oil F•e1or _ u s;s-------"" -------
Percent Moisture (Nol Decentedl---2._c;-_· __ _
..,g 1fo~ CAS (Ci~~ Numbti,
Chloro,,.,e!"itl'le 10 U 76-8?-S 1 2 · 0•c: ,.,,o,op•op;, ... ,
e,o,,.,omet"arie 10 U 10061-02-6 Tta"ls 1 3-01C:l'llorop•ope"'le
V1nv1 Chlo••~ 10 U ?9-01 -6 Tr,clllOrMthf"'lf'
Chloroefl\81'\£' 10 U 124-48- 1 b 1br O'f'IOC hlo1 ome1h11 "le
Mt!"iyle"lf Ct\lOrtde 5 U '19,CXH, 1 1. 2-Trichloroetl-\ant
Ace,ol'le 10 II 71-•3-2 Bel'ltene
Ct•bon 0,1 ulr1de 5 II 1oos, .o, .s c,,.,. 3•01chlo•Jo1oc,ef'le
1.1-01tl\lori>rt'1trte t; l I 110-75-8 2-ChlO•Olthvlv•:"lvlethe,
1. 1-0,el'llo•oet"'•"" 5 U 75-25-2 81ornoform
Tr•l'ls• 1. 2•01el'\Jor~thel'lt 5 U 591-78,6 4-Me,"'vl-2-Pe"'lt&l'IO'lf
C/'\foroform 5 II 108 10-1 2•Mhll1'10t\f
, ' 2-011:hfo1oethll'II!' 5 U 127-16-4 T ~tr ae'11o•oet"e-"e
2•Bu1enol'le 10 U '19-34-S 1. 1. 2 2-Tetrac"ilorM-t"il"lf
1. t. I •Tr.c"iloroet'18rtt 5 U 108-86-3 To!uerit
Carbot-i Tttttc:Moride 5 U 108-90 7 C~loro~nie-nt
V,n~I Ac:elltt 10 U 100-41 ., ftl'lvl~n.z•"' -8 •o'T'IOd1el-\lo1omtthal'le 5 lJ 100-41-5 Stvrent
Total_X\·lef'll!'S
011a C!:t;i,o,,•"9 (wtlrf,_,t
eo, 1Spol'l1flt ._,11111 to £11.l t1't fe/lew,'IQ ,a~~IU ,.,11rf,e11 ••• l!lltO Adid•hOP\AI fllQl O• fOOl"iO!illl t!ll)la,1\11\Q 1fl111t, 11t O~o1,1<IQd tco-,..., tl'llt -,.i,1\11 IO".,,, ••th fl.I; ft'll,/Sl tal ♦J,lifJCr1
5 U 5 U 5 U 5 II 5 U 5 U 5 U
10 U 5 II
IO IJ 10 U 5 U 5 U 5 IJ 5 U 5 IJ 5 U 5 ll
W.. • .._ IW""1 11 a nl..it t•Ult• ffli" .. t,alJotl kl tf'lt CMlffllOl'l ""°'11 C . ..f'l'O" ttif 119 li,t
II Wc.,iaa lO""OOu"CI lltU tf\tlr1td fo, t>111 f'oill Stlttli,d .. flOII '"'
, ........ 91)"'31 ... IOMlhtodt N••-11•• ~·· , ... -,.111,l,u1,o· ..... h•" 1:0111,t~II bi GC MS &•"Sit to"I\Jl(l"'"t flfat,r•l5f'i? 1.:-,
fl& "' tf\ tilt'''"' lllfttl ~ .. COl\ft<~ 1h GC MS
.. ""l'l""'*ifC111l-" ltft\f1 lot ftlt M~ t1w•l"ti'lt Ult I 10UltMIM-d I
.,. ftkfflt•y u•1coi.110,...,, •frl,,11,0,,Kt,o,,, tfti,a II flOI A1ttt111•1lr tht ..... U-,lnO"I .. lftl,of'I "'11\,t t fhf ftot"411 Or-..wl!S ~ IJ· ~i.1'Wl' '"' 1..-1rteel',.....,. f'4I •umffl ,,_ ~• 11111V WMIMt!'lllfri llma•tiat>li *•ttuen MM ... ette- il1T'$11 Othef
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tn11 fllQ •• uUCI ....,,., ,,_ ~ • fo-.1'\d ""11'11 l>I•._. u ...,.1." 1
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Fe &,~ Contract# 68-01~7168/lA 68-0b'J~At?A tg!Me, Anervais Data Sheet
(Page 2}
Semivofatile Compound,
Col'\Cef'itrlff()h. ~ 0a1e Eirtracttd 'Prepared
Date ANtvled
Cor,t/O11 Factor
Medium (Circle One} '2. p 1.$- 8 k
I Percent Mo,stute (Oec:anted) ___ '"'2...._$.,. ___ -__ _
CAS Numbtt
108 95-2 111-44-4
95-57-8
541-73'. 1
10ti-46-7 100-51•6
95-50-1
95-48-7 ..... 8-32-9
'""" 10£-44-S 621-64-7 67.72., 98 9S-3 ,a 59., 88-?S-5 105-67•9
65_-es-o 111-91-1
120-83·2 120-8..2-1 91-20-3 106-47•8
8'?-68-3 59-50-7 91•5?-ts .,, ... , ... 86·06·2 IS-95•4 91-51-7 88 , •.• ,,,.11.3
' ~6-8 .. 9!:t·u9·2
..
Pl'\el"lol 330 U b•s1 -2-C"iloroet,-.,\IIJE ther 330 U 2-Ct:iloroptienol ~no u 1 3-0,chloroMf'l?f'l"le 330 U 1 ~-01cMo,ooo"tt'le ~no u Be rirvl Atco"o' 330 U 1 2-0,cliloroberite"lt 330 U 2 -Me1,-..vlp"ierio1 330 U . .
b•sl2•thloro1soo•opvllEtlitr 330 U 4-Mtt"lyfpheno 330 U N- N1troso•01•n-Propvfal'l'line ~1ft II Me dctiloroethll ne 1-".!.n II NrftObel"ill! 'if- 330 U lsop"iorone 330 U 2-N 1tt9_p!-ieno1 3J0 U 2 •·O,rne1hvlc,tienol 330 U 13tnto•c A.c1d lfinrl U b1s1 · 2-CM0,oetho1v1M,1"iane 330 U_ 2 41-0,tlilorop!-ienol 3JO U 1. 2. 4-Trielilorobel'lzene 330 U Naoll1h11ene 330 U 4 ·C"loro.an,hne ':l~n II
He• •c l'\lorobut•d•t ne_ ~:l.O ti •-Chloro,3-Methylpheriol 330 U 2-Methyln•ohth1lent 330 U He111chloroevcloprntad,ene 330 U 2. •· 6· Tuchloroo,henol JJO U 1 . .t. 6-Tt,chloroph~nol t,:;nn _11 2 •Ch_lorol'l&il)hth• ftt\f S:l.n ll 2 •N ,t ,ca "•hfW!t 11.nn 11 D•rntthvl ,hthelat• 330 II Ac tntr,hthvfol\~ 330 U _3•N11toanihnt 1,mn 11
GPC Cleanup OYes t!No
Separatorv funnel E~r•~iori CJV~s
Continuous LiQuid • liQurd E.:tract,ol"I OVes
CAS Numbtlr
83-32-9 51-28-5 t 00-02-7 1.32-64 g 121-14-2
606-20-2
iSA-66-2 ?005-?2-J 86_-13.1 100-01-6
534-52-1 86-30•6 101-55-3 118-74-1 87-86-5 85-01 ·B 120-12•? 84-74•2 296-44•0 129-00·0 85-68-? 91 •94-1 5,6-55-3 11,.s,.1
-
~18-01-9 111-84-0 205-99-2 207•08-9 :,0-32-8 ,93.39.5
·;:v,o-:i , 9t •24-2
ug 11o~ {Ci;~~
Ace: riap'ittient- ~30 II ~
2. 4-Dirutroptienol 1600 lJ 4-N,uoplitl'lOI l finn t1 D,bentofvr•n 330 U 2 4-01n1trotolue"e 330 U --
2 5-0,nitrb10fue"t 310 U D1elhyfplith•late 330 U 4-Chloroplieriyl-e>"iflriyle,.,er 330 U Fluor,ni! 330_ IJ 4-N•troa,.,il,ne 1600 U 4. 6-01l'11tro•2-Met.,v!c,tiel'lol 16UU U N-N1tro1od,p"ienyl&rn1f'lt! ft I ~1n IL 4 · 9ro,noplienyf .pht_riylethl'r -~30 I! Noa thlor obenze "e 330 U Pentaeliloroc,"e"o' 1600 U Ph1H'llr"ltlirtt'le 330 U Arithr■cent 11n 11 O,,n-8u1vlp'111-iara1P 330 U Fluoral'lthel'I~ _330 U __ Pyrene 1::ln II B utvlbel'l.tyll)l,f "·III e 330 11 3 3 ·•Oicl'llorobtl'IJ1d1rie 690 V Bef'IJO(IJAruh,acen• .'l1n If r:,,~2-E11tvlhe11vllPhttill8!('
. - 130 ti c,,,vuiit 330 U o,.n-Ocrv1 Phthtltre 330 U Ben1o(b)fluor&nt~l'l,f 130 II Bento(klf luDrlMhtl'lf 330 IJ 8tl\Joiai,Pvr•l'lrl 330 U lndtno(1. 2, l-cd~tllt ~1tl II 01t>.ni11 h~nthraeel'le 11n II Btl'llola h, ilJ'&ryl#,__ ~10 II
r---cr-r-0 0
l•bo,11or)' t-.a""'t SOUJHh'EST leATORY ,,Or QKr AHOMA (9 5=.\{ l Cut "-o ----~-..2....i;....,.._..._ ... _ ------
Contract I 68~0l .. 716S/lA or 2Aorganic• Anafy1is Date Sheet
.J._
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(Page 3J
Pesticide IPCBs l
Mtd•ul'fl (C,rcfe One)' low GPC Clea l"ILJP OYea JSNo
Otte £.a:v4cte-d 'P,epared - 2 - 9 - & l 0 "! .-_ 'L. - ,.. l:
111 AP\1 1yr~J ------..J------~------C.0"1c ro;rF•ctot 2 h,$ 1 'l
St;ia,atorv F' U!-11'\tl E11r•ct1on;QVe!>
Contin..ious LiQuid • Liqu•d £r1rac1,ori OVes
Pe·cent Mort!urt! (dec111'ted) .,.__ ....... 2 ....... ~ ___ . _c __ _
v, -------
.3,9 86 6 Alt)"iil 81•1(
Jl9 es., 6etll &1o1C 1319-Bt·B Ot•:, e~c 56 89 9 Ga..-.~,a 8"4C IL•ndb">!l
t?E-4.4-8 Hrp\lJChlor
~09 00-2 Alc,,,n
1024-S'·J Mtotll :"'10, £poK ,de 1959 98·8 £"-dos..ilf11n I
·-
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172-SS-9 4 4 -ODE f72•20·8 El'ldril'I
332t3-tS 9 Er.dcS..itf1" II
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!,'1,74 9 Ct-ilorda..,t
8,01-35 2 T ou p"'e "e -·
12674-11-2 A•c,clor-1016 '110,4-282 A1oc10•-t221 11141,165 A•ocio,-12J2 53469 2,_.9 Aroclor•U•2 12672'-29·6 Aroclo•• 1248 l 109'7,69-1 A•oc lor-1254
1 \096 82-5 Aroclo•· 1260
ug'lo~ fC1rt~
fi nu 8.0 U R n u 8.0 11 8.0 U A n 11 8.0 U 8.0 U
16.0 U 16.0 U 16.0 lJ 16.0 U J6.0 U 16 0 1t 16.0 II 80.0 U 16 0 Ir 80.0 U
H,n O II BP.0 U 80.0 U ou.u u 80.0 U 80.0 U
lbu.o U 160. 0 U_
V1 8 Volu,ne of ,st,1c1 11\j•cu-d (u1)
\11 • Volumt of Wlttt e1tr1e1td Cl'l'lfl
W" • We1.ah1 of IO'nplt t1tr.e11d (gt
v, • Voh,tnt of toltl t1ttlC'I h.ilt
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19.
20 21.
22.
23 ' ..
2, 25.
26 J-7,
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Organics Anarvsis Data Sheet (Page 41
Tonutivelv ldentifi&d Compounds
C01"npo1.1nd Ntl"l\t Ft1ittio,n
Ike he 0-c_.'d /me f.1,.,'i/ ~ s I-_~"' fb 1-J A l(,\,\k-,,.,_oii,'--V\ I•
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Sample Number
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@Regional Office:~. @ Po.-~ sample collected specify number- @. ~?:: 7 SamplingPersonnel:';:•- (!:j.;:• · ofcontainersusedandmarkvolumelevel -·i'· Rec'd~----~---;
o~eachbo~e. . . _ .. : _ ,.~. 0 ~ /... b. t - ·- --! ' -- • ~-- - . - - · - SampleCo~S.gr a.
Number of · ApproXllllate on Receipt {e.g., broken, o Containers Total Volume ice, Chain-of-Custody,-etc.).:-C
~- @ Sample Description
_ Surlace Water
__ Ground Water
---· _Leachate -
Otha·
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-dSolids _ Other(specify)-~--
@) specW ~ Instructions: (e.g., safety precautions, hazardous nature)
bjJOlH' :~ ·:) ::· .. ' ~ ~- ~: ::,--;k' :· .:.2 ~- ~~ :: : :>:: X VJGXs;:;: ·g J_V~;;_·ic; ~~-'.--~,: ho· B--~ g J8 . ...,_ ,.... ... ,b.,.--- •~vr-qc-"·--.·-~.- ... - ....... -·,· G '!UJJ I l ~, ~J,..,,!. ... ~-t.. .~,,. .. ~""-(.\,.it! - .
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Organics Analysis Data Sheet (Page 1)
case No: S s· C, I Laboratory Name. t.aa~L lab Sample 10 No: _........-:cf_.9'-'.£""--9~.Z...------Sampl~ Matr,ic ~==·-----~------Data Release Authorized By: iJ.aJ:(\M-t- (!. u.,)_ui.\..t--\.
QC Report No: _9.;._:.7 ___ ~-------
CAS Nurnoor 74-87-3
74-83-9 75-01--4
75-00-3 75-09-2 67-ti4-1 75-15-0 75~35--4 75-34-3 156-60-5 67-66-3 107-06-2 7_8-93-3 71-55-6 56-23-5 108-05--4 75-27--4
Chlorometha1,~
Contract No:
Date Sample Received:
Volatile Compounds
Concentration: e Medium {Circle One)
Date Extracted/Prepared: -------~--~-
Date Analyzed: J/.,t) (.IC:, Cone/Oil Factor: I pH........:&~. -=O ___ _
Percent Moisture: (Not Decanted I I 2. 7 °/4.
ug/lo~ (Cir~~
lit/
CAS Number 78-87-5 1, 2-DichloroprO(Jane
Brom.omethane IJ rJ 10061-02·6 Trans• 1, J•Dichforopr0pene
Vinyl Chloride 11 tJ 79-01-6 Trichloroethene ·
-Chloroethane //I) 124-48• t Dibromochloromethane
Methylene Chloride .:t7~ 79•00·5 1, 1. 2-Trichl0<ostha_ne
Acetone 9.t A 71.43.2 Bentene
Carbon Disulfide -/,. ii 10061 ·01 ·5 cis• 1. 3-DichlorOf)rOpene
1. 1-0ichloroethane t. ,J 110-75-8 2-Chloroethylvinyfether -·
1, 1-Dw::hl_oroethane t. 1) 75-25·2 Bromoform
Trans-1. 2-0ichloroothene _ t, ,, 108-10-1 4-Methyl• 2·P~ntanone --
Chloroform L ,, 591-78-6 2•Hexanone
1, 2-0ichloroethane /,, , I 127-18-4 Tetrachloroethene
2-Butanona I /J A 79.34.5 1. 1. 2. 2-Tetrachloroethane
t, 1, 1-Trichloroethane /,, IJ 108-88-3 Toluene
carbon Tetrachloride /,. ii 108-90-7 Chlorobenze ne -
Vinyl Acetate /I iJ 100-41-4 Ethylbenzene
Bromodichloromethane ln 100-42-5 Styrene
Total Xvlenes - -
Oaia ff.ipo,1,ng Ou.ahliers
l'o, t<!Q<>ll""il results 10 EPA. 1he lollo<Ning results quahf~ .ife used. Add,uonat nags o, lootnotu ekOll,ining re$ults are .n('Otj(~. ~•. the (kl11>1110n ol each flag mu u be 11.rplk:it.
.. -
.. ,l
ug/lo~ (Cir~'f
6tl
I, (/ t, 1/
bo t,v 0.5 .:f'
~u //u !nu
//11 /lu t. 1/
&. ~j
.i :J"fl J:. d
/4 0
6tJ i/.:r
II 1he r<!SUU IS a 11alue g,.,.,,,, tha11 OI ~1 ,o lhe ~1«1,oh lln\11.
rltpOI\ lhe v.iloo
C Thi$ f~o .tW!<eS to pest,c;,de pararrteletl wnete Iha ldent,IIC.IIIIOO h.1s hffo e0t1hr.ned by GCIMS Single CO<nt)Oner.t peslw:tdes~tO
tiglul '" lhc Ito.al e•tfttt lhould b$ COC'lflfmed by GCIMS. u
J
ln-dicacu compound WU llnl1Vled lor but not IIGloctl!d. flepo,-1 lhe m, nunum detcCIIO<'I Jmm fo, the sa mpi. ...,lh lhe U {e o .. I OUI b.ased 011 netesurv c(lneen11a11Qn/dilu11on achoo. lfl111 ts Nn t>Kesur"v the tns1rumen1 del~IOf\ hm•I.I The foolttote ihould read U· Comoound was ,11~1rre1d for bul flQI dclecictd Yhe numb!lt n lt>e m,n,mum 11111,nable det~Cl"1A r.mu '°' t~ Sl•llple
lnd1ea1es a11 astrm.111ed \'zlue. fhis llag rt used e,11-H!• when e-s111n.a1,ng a conce<11ra11on for 111nt111~1y tdtnulllld COln!)OUl\(H wt.e,e a I :I rcsgll)nse 11 assu,~ or ...-hen ttM trl.l1ss toeCtral daui iridica!ed thfl P,eS.I\CQ ol • Cl)fflll;Wnd th.al "'"II the idenlrflClllaon entefla but the rHutt tS leas th.an th. t()e(ifted det-.rtKM'I hn\it !MIi greater th.t<I tero. {e.g .. I OJI. U l,m11 of deiM;tton is t O pg/I aftd a Concflnlrll'ton ol 3 µgit is c.alcul.ued, reo,o,t a, JJ.
8 Th,s 019 ,, Us.ed ~" lhe al\lllft.t ta ,ouni:11n 1h41 blank .U well U a wmo~. 11 11\d,cac.1 POhlbltlp.robab\,t blanlo. CO<llamtn.lllH:l<'I and
warn$ me. d.111,1 - 10 tale ~°"'.au·, l!C11Qt1
Othet" Ot"- soec,hc flags ;and lootno1es ni.tybe ,eq1111ed 10 ,.,_.1y,1-,11ne the fHUlls H used. they mustltt! fullydeactlbsd lf'Xl IAICh deSCtlpl((>tl
a11Khed 10 lhe data IU<nrn.ttV ,epo,t ·
form I 11/85
C <X. r---0 0
Laboratory tfame---'=-~✓ e ~ ■case No: S Sl 1 . e
• Organics Analysis Data Sheet
(Page 2)
Sample Number
FC lb Q
Semivolatile Compounds
.Concentration: 9 Medium (Circl0 One)
Oate Extracted 1Prepared: .2., I .l. f / Gt _
.Dste Anatyzed: __ .J_I_. l_l.,..1 ...... 1....,Ce ......... _____ _
Cone/Oil factor: 1 S' d ~ a · q ~ a:n-h • Percent Moisture (OecantedJ
.CAS NumlMr
• • • • • • •
108-95·2 111-44-4
ss.s1-s 54 t•73·J . 106-40-7 100·51·6
-;;."50.1
$-48-7 -3!1'638-32-9
106-44·5 621-64-7 67-72-1 98-95-3
78-59-1
88-15-5 10$-67•9
65-85-0
111-91-1
120-83-2 120-82-1 --9\-20-3
106-47-8
87-68·3 59-50-7 91-57-6 77.47.4
88-06-2 95.95.4
--
. ''1enol
bis(· 2 -Ch lotoethvl}E I her
2-Chlo,ophenol
1 3 •0tchlorobenzene
1. A-01chlorobenlene
Benzyl Alcohol
1. 2•O1chlorobenze'le 2-Mettiylpheno!
b1S12•chloro1sopropv1lcthe,
4- Methylpheno:
N-Nitroso-Or-n,Ptopyiamirw
Hei.:.achloroelhane
N11robenzer.c
lsophorone 2-N1Hophenol
2. 4•Dunethylphenol
8ento1c Acid -·
b1st-2-Chforoeth01Cy!Methane
2. 4-D•chloroohenol
1. 2. 4-Tnchloroberuene
NaphthJlene
4-Chloroaruhne
He1Cathlo,obu1ad•ene
4-C!\loro-3-MetovtoheMI
l•Melhylnaphthalene
Hel(achlorocvclopeniad1ene
2. 4. 6-Trichlorophenor
2. 4. 5-TrichlototJhenol
og/lor~ (Circf~
/ Ill .:f.P, 7b0u 7tiJ,J 71.?u ?t,,l)u
7/-1),1 ?/,.,/Ju ,, /,./),,
7/.,/),J '? C. Du 7 r.. /),, ? t. /'J,, /)L/l,,
?1,,i);J 71...n ,, 7&-t?,,
31- n/J,, 7(.n,,
. ? r,0,, ,, ~ -~ (.1../5':r
,r .., t,,n,1
?'6- /),I
71 .. "'1,1.
7t:...ll,, ? 1,.,./), J
'7(,,/),,
~1 L IJ .-i ••
GPC Cleanup tg{es □No Separatorv Funnel E,araction □Yes
Continuous Liquid - Liquid E~raction OYes
CAS Number
83-32·9
51-28-5 100.02.1
132-64-9 121-14-2
606-20-2
84-66-2 1005.72.3 86-73-7 100-0t-6 534-52-1
86-30-6
101-55•3 118-74·1
-·
87-86·5 85-01-8
120-12-7 84-74-2
200-44-0 129-00-0 85-68-7
91-94-1
56-55-3 117-81-7
218-01·9 117-84•0
205-99·2 207-08-9
-·
Acenaphthe!le
2. 4-0initrophenol
4-Nitfophenol
Oiberuofuran
2. 4-0initrotoluene
2. 6-Dinitrotoluene
Oiethylc,hthafite
4-Chlorophenvl•phen'(lether
Fluorene
4-Nit'°aniline
4, 6-0initro-2-Methvfphenol
N-Nitrosodiphenylarnine (1 J 4-Bromophenvl-phenvlether
Hel(achlorobenzene
Pentaehlorophenot
Phenanthrene
Anthracei,.e
0,~n-8utv!Phlhalate
Fluoranthene
Pvrene
ButylbenzylpMhalate
3. 3·.01chlorobenz,oine -
8enzO:a1Anthr acene t}ls{2-Ethvlhe llVI IPhth.a late
Chtysene
01-n-Octyi Phthalate
Bento(b)Ff uor an1hen,• - -Benzo<~WI uor anthene
tJ:g/1~ (Ci~~
79v-... ~
.3 ~ 00 u .1t.OC>o
g,.r - c---
7t,o,, 7/,,,0u
3:J.:r- -/I,/) ,J
?l:,t),1
~ (; 0/Jv
3. "ia '2 ·L., '] I,. ,,,,,,
?t;/Jo 7~/J,,
:~/,.(I /J,, f .30 v "." >--
'lf..O,, tJ.(; ;, A
L 11:r _,._.
I /OJ' _ .... 71,. /) tJ
l'-~cW v 7 /,. /){)
o1.J)IJ J'B 71,0u 71,,0,, ~l,O" ?t./Ju
91-58-7 2 ·Chloronaphthalene .., /,./'Ju 88-74•4 2 •N1ttoar11hne ~1L fl/J \111
50-32·8 Benzo(a)Pvrene '1k /J,1 193.39.s lndeno(1. 2. 3-cdlf>Vt4?ne ..., /,./'J,1 53-70•3 131-11.3 D1mc1hyl Phthalate ,., r..n .• -
208-96~8 Acenaphthvlene '?t../1,, 99-09·2 J-Nuroanil1ne .1 I. A(/") ,I
!
!■ I
Oibenr(a. hlAnihracene ""It. ,1,,
191-24·2 Benzo<a. h. i)Peryfooe 71,/1,J
I
• I 7 85
• !
~
C ex. r-c C
• ■
•
8'
II II
111 I
i I !,!I I
!
!,I I
!U I !
!I I i
Organics Analysis Oata Sheet (Page 3~
Pesticide/ PC Bs
Concentration @ Medium (Circle One) GPC Cleanup ~s □No Oate Extracted 'Prepared ,il_-;I 1? - 8" Separatorv Funnel Extractron □ Yes
Date Analyzed J- 7- 8~ Continuous Liquid• liqutd Extraction □Yes Cone/Oil Factor
Percent Moisture (decanted) ----"-'-o-____ _
vs
CAS Numbe,
319-84-6
319-85-7
319-86-8
58-89-9
76-44-8
309-00-2 1024-57-3
959-98-8 60-51-1 72-55-9
72-20-8
33213-65-9
72-54•8
W31-07-8
50-29-3 72.43.5 53494-70-5 57.74.9
0001-35-2 12674-11-2
11104-28-2 11141-16-S
53469-21-9
12672-29-6
t\097-69-1
11096-82-5
Atpha-BHC
Beta-BHC
Delta-BHC
Gamma-BHC (Lmdanel
Heptachfot
Aldrin
t-!eptachlO( Ep0:r:1de
Er"ldosulfan I --
O,elddn
4. 4·.ooE Endrm
Endosulfan II
4. 4·.000
Endosulfan Sulfate 4. 4·.oor
M.ethOl'.'{Chlof ..
Endrin Ketone
Chlordane
louphene
Aroclm-1016
Aroclor-1221
Aroclor-1232
Aroclor-124:? ..
A.roclor-12(8
Aroclo, -t 2.54
A.roclor- t 250
ug/1 ot ug/Kg (Circl-e o~ei
fl,. b U /{,,. () lJ u.,n 11
/t,6 11 J(,,O 11.
IJ..O L(.
Jt,0 U /1,.D l(
.3:l-0 u. -~.o Q
..3.;J,D I.J.. ~-0 u J;;],O u .3,.'Z,Q l,l .3.J,O u
I t.l>.l> u. .3,2.0 U tt-t>,0 u
,:uo.(> L(
JbO,D _ U.. //,l>.t> u. Jl.a,IJ u JU).() u N,IJ.O tt .3;l0.6 u .3~t>.O ll
V 1 "Volume of ertract 1n1ected (oil
Vs _:: Volume of water ea:tracted (ml)
Ws ~ Weight of S3mple ektraC1ed (gl
• Vt : Volume of total ew:tfact (ulJ
forrn 1 7185
r. C (X_
r---0
C
• Organics Antalysis Data Sheet
(Page 4)
l" entativerv Identified Com90unds
• --------------,r---~-~---r CAS '8) ~r Scan Ht,J,mWt Compe,ond Name fract.an Number
1. l,LJ fll
2. ------1--------~----------,~--...J--~-➔------1
.r 20.
21.
22.
23.
24. - .
25.
26.
27.
\ -~a. a,29. :to.
fo,m I, Patt B 7 85
@Regional 9ffice:- ;ra_: Sampling Personnel: · ,r- ·, -:~:,-
r.. --
® For each sample collected specify nwnber· @ Anal~~ of containe:ts u.soo and mark volume level . Rec'd~----.--....._· on each bottle. · Oat~ Rec'd: ;;__? ai~ ~~
- ~' , ... /. / / -. Sam le Co di . /J //'•• , C/l,.,. <~ .-- p n tion ,.._ 11 H. (Name).-.:" . ·- , _. . Number of Approximate ~n Receipt (e.g., broken, 5 II: ~i?,~h!·?i-46• 51 ,___W._a-ter-------i----Co_n_~_-_e_rs-t-_To_tal_V._o __ l_um_e-t-1_ce_._Chain_·_-o_f_.C_us_;t_od_Y_, e_t_c.)___,
' ·1 GC· (Extr ctabl ) i I Sampllii~Da~e;7;~:. _. ,--- ._ 1-----a __ e_----f--___ ,-.,...-+-____ --t-_______ ---1
II 2·/7 )7/,7£.. WatP.r ~ l, (Begin) 2· • •. ;~•;"J (End) -~- (VOA)
Q ~Ship~inglnfonnation .. :. ~~!~-
0 .. r I - 0>:;--/', ·; - -- -. t-~-"----n-~Sedirn~)--e ..... n--t --+----7'--_ ------i--c-_"_
1_-;1---------.......
Name of Carrier·. , .. -. ...--------+---=t..--_______ _,._ _____ +-___..'--------.--i
t I Other
~I Date Shipped:
~I ---Air-.-!--~-~;-~-~-(,_:,,,_,._:-~'""". i __ ._Y:;._____~ ___ _.,_ _____ ..,_ ____ ~---------~
d===========::===~=~========¼ i I ® Sample Description ® Sample Location
✓YJ ·i ..51 'f,.) (I _ Surface Water ~ Mixed Media , .,
~ I - Ground Water ~~lids ~/J ~- JJ.S- / r; J
ll
II II II II II II Q
Q
q
1!1 i \Q I IQ I
!q I !
\q i
\
tn
• Sample Numbe,
~<:._ 17/J Organics Analysis Data Sheet
(Page 1)
Laboralorv Name: f-tru, MA,J.."F ~ ~ case No: ss, I ~::;;~•:t:::N_o_: _=_ . ....,.jlliaJ/..a:l:1::;.::_:i..'l~-=-· -~-~-· ~-~:-=_:_=-~--- :n~r:::o_: --_.C...a;;... ..... :_,_~ __ , ... l=t.-.::$".~·~..:: .. ;..__ ____ _
Data Release Authorized Bv: }Mox:~£UL\- C,. \l} U&¼ Date Sample Received: _ .a I .z.f I l(,
Volatile Compounds
Concentration: 9 M~dium {Circle One)
Oa1e Extracted/Prepared: ________ _
Date Analy2ed: .. J /,//it, Cone/Oil Factor: _..;../ ____ pH (,. ()
Perce.-.1 Mois1u,e: (Not Oecantedl _ __:/;.._;;f,_ .. ..;;.2-;-:;:;;.. __ _
CA$ Number
ug/10~ (Cir~
CAS Numbar
ug/lof~ (Ci~
74-87-3 Ctilorom~than~ LJ~1 78-87•5 1. 2-0ichlorOpropane ?._o 74-93.g Bromomethane I.~ •• , 10061-02·6 T ran$-1. 3-0ichloraprc,pene J.,u 75-0t-4 Vinyf Chloride /.1. J 79-01 ·6 T richfor-oethene •• ,J
75-00-3 Chloroethane 1.'1 .. 1.24-48•1 Oibromochlorom8thane __ 6v ..
15-09•2 Mcthyfene Chloride /. 3/J IJ 79-00-5 1, 1, 2-Trichforoethane _, •J
67•64-1 Acetone l/t:,, .II 71-43-2 Benzene L..~ --..
75-15-0 Carbon Disulfide I.. t/ .. 10061-01-5 cis• 1. 3-0ichloroprapene 1,,,/
75-35-4 1, 1 •Dichloroethone 6n 110-75-8 2-Chlotoethyfvinvlether /J..~ -·
75.34--3 1, 1-0ichloroethane t. ,. '15-25-2 Bromoform L. ·"' ...
156_-fiO.!:j Trans-1. 2-Dichloroethene _I,,, u 108-10·1 4-Methvt-2-Pentanone 1-'··J 67-66-3 Chloroform I, V 591•78•6 2-Hexanone j _, .•
-
107-00-2 1, 2-0ichloroethane .l. ,J 127-18-4 Tetrachlo1oethene I,,..,
78-93~3 2•8U1anone -·
I I .:f' IJ 79-34-5 1. 1. 2. 2-Tetrachloroethane /., ,/
71.55.5 1, 1. 1-Trichloroothane I,,. • , 108-88-3 Toluene Q I/ -
56-23-5 Carbon Tetrac~loride , ... ,J \08-90-7 Chlorober;zene L ., .. . .
108-05-4 Vinyl Acetate /~v t00-41-4 Ethylbenzene .)..J 75-_27-4 Bromodiehloramethane. t. ,J 100-42-5 StVfene t. -~ -·-
Total Xvlenes '1-~ Ou• ~ct>Q Qu&ldius
Vati.oe
u
J
F<>t •eoorl•"O •Hults 10 £PA.. the toUo,,,,ng tesurts 411.ahf~rs are u~. Add,1-,al flags c,, footl'IQIH eqilaollitlg ,esutH ••• encoo•11gcd. Ho•~•. the det,n11,on ot e'Klt II~ tnUfl be ,11q1l1Ctt.
II the ttsuh is ll w&lue o,ie11.e, lhan Qt equll lo the delkt'°'11 llfl'ld. C tt?r,o,t lhe walue
k>dcea1es cornoound was analy1ed IOI but •WM delCH:t4d Aef)Cl(I the t111n1tnum d.!lectlOft lnni1 I011he s,mi,14! ...,,h 1M U (e g . IOUlbtsad B
O<'-necflUC,~t&t10<,/d1l~tO<'I ldion. {thisil--ity lht! 1nsttumen1 detection l.,n.,I.J The fGOlnoce -should ,ead: U•
COt,\pound w~• .aqaly1td fo, but nor ckuaed. fM ~ is the mtnomum. iltll'-'table detectie.\ luml 1o, the nmpk Otf>e¥
1"1SK:&lcn .... tlsllfftaled Vlll,M!. This lta,g tt IIS<!d e,thcf ~ eu~c•ng .a CQl'leemtacoon fu l<fnUI~ identifted ~ ..,,,,.e I U •HOOftte tS Hsumed o, whan ~ mds IIO«ttM data iac:hc:.&t'lld 1M IW•sentill of~~ lhll _..flit ..,.,.dcat_, ctltf.tia tiuc 111• tnc.h IS lus titan the Wlt(:ified decau.on r.n1ic buC o,aatec- th.afl nto. (e.f .• 10./f. a, f,ffl<I ot OKOCflOn is 10 IJOII and a ~C\U&tllln (14 ) 51tll ti talculaled. repooi H 3J,
forml
ttws fuo aoc,loes 1ai:,e,1icic1e .,_,ame1.e,s whet• tht toMntd,cauo,, h.U bHn conllf-.1 by GCIMS. $11"1gle compo,,ent p,,-s1oetde~~tO ng,u1 on the foul e1t,.11ct V>OIAd be canhrmoed by GCIMS.
l"ht$ fl.tt os uu.:1 ~n tho ,..,..,vr• n1 foundtf'I ""blMlli as well as• ~- It tadocatU oou,ble/0(~ t,unlo. ~IIQCII and w,11,ns Iha QI& c,set lO tal.e ~op,c.!llt KtO'I
Ott>e• ~ofoefta,isend rooeno4esmavbetequMadioo,ropedy6tfHMt lheresu11s ffuwd.1heymtn1bofulfydffl;.,,-:'datldtcldldn0'-,...,,. Jilt~ 10 the data Sl,lffllna,y fllt)Of\ ,
.
..
-.c C oc to 0
-Laboratory Name d~◄ t4~ t' ~ I) Case No; _____ _..5.......,$._f, __ ._{ _______ _
Q
llconcentration: low ~
Organics Analysis Data Sheet (Page 2)
Semivolatile Compaunds
(Circle OM) GPC Cleanup □Yes Utf'io
Simple NUMbet
~C/10
_ Extracted 'Prepared: ~ ....... J ..... ..,.J.L.t .... f.,.,l.~------ilOate A!Uiilvzed
Cone/Oil Factor:
J / 1, / J t Separatory funnel Extraction QYes
Continuous Liquid - Liquid E,ctraction OYes
(j q Percent Mo,sture (Oecanted)
II CAS Nun1wr
ug /I or .<i'g/Kg". (Circ~
CAS ug/lo~g Number (Circ ~
II II
d d d II II
10B-95·2 l 11-44-4
95-B'7-8 541,7~-1 106-46,7
100-51-6 9_5-50-1 95·48-7 39638-32-9 106-44-5 621-64-7
..
67-72-1
98-95-3 78-59-1 88-75-S
105-61-9 65-85·0 111-91-1
120-83-2 ..
t 20-82·1 9\-20-3 106-47•8
-
87-68·3 59-50-7 91-57-6 77-47-4
88·06-2 9!>-95-4 91-58-7 88•74-4 q1-11-3 208-96-8 99-09-2
Phenol
b1s1-2 -Chli;>H>e1 hyl \Ethef
2-Chlorophenol
1 3-0 rChlorobe nzene
t. 4-0rchll')rob-em:tne
BentYI Alcohol
t. 2-0,chlutobenzene
2-Metnylphenol
b1st2 •chloro1sopropyl}E ther
4-Me1hylpheno1
N-Nmoso-0,-n-Propylamine
He x.achlotoet ha ne
N1ttobenzen~ --
lsophorone
2•N1oophenol ..
2. 4-0imethylphenol
Benzorc Acid
b,s( • 2 •Chloroe1how.y)Mf!1hane
2. 4-0ichlorophenol
, . 2. 4-TnchlofOben.t!'l'l'le
Naph1halene
4-Chloroaniline
He,cact\lorobu1ad,ene
G-Chloro-3-Methylphenol
2 -Met>iylnaphthalette
Hew.at.hlor?Cvc.lopentaoceoe
2. 4. 6-Tt1chlo1ophenol -
2. 4_ 5-Trrchl~rophcnol
2: ChloronaphthalenP.
2-Nnroanihne
01methyl Phlhahue
Acen~Ohlhylene -
3-N,uoal\lhne
-1.a/dOOfJ 83·32·9 _,, ,., ,J/./)IJ{! l} 51 ·28-5
.9. 1/-/) 0 /) t} 100·02·7 J tlnlJ/Ju 132-64-9
..1 IJ. () /JI) ll 121-14-2
,t Y IJ fJO d 606·20•2
.2.-1 '100 n 84-66-2
.J,t-/0/J/)u 7005-72•3
,:J.t.11JIJOt1 86-73-7
,_ c/-lJ/J /),,. 100-01-6
J., l,1./) I)(}" 534-52-1
~ 1/IJI){)., 86-30-6
.J.. "() /)/) ti 101·55-3
.;!. J./b/11? tJ 118-74. t
- _, ul'J/Jt? V 87 •86-5
~ _,U/)/),? I.I. 85·01 -8 • .. -~~ .... ,1 120-12-7
J ~ J' /1/)/) ,J 84-74-2
.:Jo..ll'JMo 206,44-0
.:l. 'I 0/JIJiJ ~ i,....,-- 129-00-0 . -
.1 9P tJl)d • l.....- i85•6B-7
c,.,' '"'"',1,; __ 191-94-1
..i ,f,-,,1,1) ".,_ 56-55-3
-2., ,j t) /)/)" 117-8 \ · 7
£/ Rooo ,..- ~18-01 ·9
J, I./ 0,JI),, t 17-84-0
:2 ';'-",.,u 205.99.2
l;/,IJIJ/X)o1 -'07-08-9
~"'-;'AAf'_ :,0-32-8 . -
/ ..1/) /)JJ/19_ 193 . .39.5 ,.j, ,1/}A/J
.. - . .,, ·u
_ 1,,10:ri ~ 53•70•3 191 ·_24-2
l,.U btJOu
form I
Acena ptuhe ne . "I 9 tJt1/) ,. L-,---"
Z. 4-0initrophen.ol /il..0()0011 4-t-.·:t,ophenol ,I . -, .n A f.'Jt' ti
D1benzofurari .!Jhntu, ,. v 2. 4-01n1trotoluRne .2., .,I l)tJOu
2. 6-0initrotoluene .l ildi'Jf',. Oi!lthvlphthalate .t~tJIJOv 4-Chlotophenvl·ohenylether J. ./l'IJOu V fluorene ..../.1/l/l/J
4•Nitroaniline / ,a1 l' /){) I.}
4. 6-0miuo-2-Me1hylphenol / .J.A "t't?,,, . N-Nitrosodrphenylamine 11 I .:tyMOv
4-Bromophenyf.phenvlether .,t 1/PtJtJv Hel(achloro~ntene .:l.,4.//Jt/()µ Pentachlornohenol /.k>t)~Ov Phenanthrene J' ¥/JA/Jd -
i..,.,
Attthracene .:M JJ /JO J" 01-n-8utylph1hala1e J./ '/d 3" 1J
l........-fluoranthene 7'-1:0()(J .,. Pvtene !?. <;'.' A¥\() •
,,..,-,--0utylbe1'\lylphthalate ,z ttOt>tJ tJ
3. J'-01chloroben21dine ;,;-J' /Jl)t) ti - V BeMCl(aJA.nlhracene / <tJOIJ.--r b,st2-Ethylhe~vljPhthal:ire ti 7 I)() :f /j
V Chrysene I :J.A/)/J < O••n-Octyl Phthalate ,,;tt./l)tJ/1 ,,
V Benzo{b\f'I u(>f a ntheJ ne .. 7/)tJt} :r Ben.to{lc }Fluor a nthene t. h/Jll.-r.
v ..... - . V Benzo(aJPvrene /,. ¼J/) :r
lndeno(1, 2. 3-cdlPv,ene .2<#J0t)n _ Otben:(a h)Anlhtacene _., . , ::/\1'1,,
_ Bcflzo<a. h. 11Pervlene o2 1/(JLJ(J J)
,-as
....... C CL
r--0 0
IJ IJ
II Q
q i
i,Q i
llq I I
II I I.
- ~ • f-
Labot aiorv NamrlAJJt,..4 J., Z.s~t
- -- . -~ - -
__ 49 ,oeecs, tu. , ~
. Organics A,rtalysis Oata-Stteet -(Page 3)
--Pesticide/PCB,
-Samp&. -Nu,nber -- ~
__ F-i!. ---:_'8:zo
Concentration low ~ (Circle Onet GPC Cleanup □Yes. mtfo Date Extracted 'Prepared· .3 - 3- F <;. Date Anafvzed . 3- Z- ~ <o _( .3- /z~s(.
Separatory Funnel Extractt0n O Yes·
Continuous Liquid - Liquid Extraction □Yes
- ------~•_'I.Q_k.. ~-t Conc/011 Factor: -~ b-- - -- -~
Percent Moisture (decanted) ~-----' ... i"------
CAS Numbm
319-84-6
319-05•7
319-86•8
58-89·9
76-44-8
309-00-2 1024-57-3
9S9-98-8 60-57-1
72.55.9 72-20-8 33213-65-9
72-54-8 1031-07-8
50·29-3 72.43.5
53494-70•5
57.74.9
8001-35-2
12674-11-2 ---·
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11O96-82-S
Alpha-BHC
Beta·BHC
OeUa-8HC
Gamma-8HC {lrndanel
Heptachlor
Aldt1n
Heptactilor Epox1de
Endosuffao I
D1eldrin
4. 4"-DOE
Endun
Endosulfan II
4. 4·.000
Endosulfan Sulfate
4. 4·.oor Methoxychlor
Endnn Ke1one
Chlordane
loxaphene
Arodor-1016
Arodor-1221
Aroclor-1232
Aroclor-124)
Aroclot • 1248
Aroclor • 1254
Aroclor-126O
ug/lo~ (Cir~~
,i.o, () u ,/ ... -I ~O. () Ji
l'J.O,D lJ J20 {'") l{
I 2(), 0 U )~O,fl lJ !~6.0 ll
;tl/0.0 lJ ::llJ /ll'I u
_.:Zl/u,D u ..:tito,o u .::tt/0,C __ 11 .Rt/0,0 11 2t./aD u
1:2(;(),0 u ~l/1),0 I)
/:l,00 0 11 ;il/iJO,D (J
J:)OD 0 /)
LlCD.O fl
l:JCJCJ,0 fl
/,;ltxJ, C 11
1..200.0 U ~(j_OO,t;J U ,;1lfob,D U
V, "' Volume of elCtract 1111ected {ulJ
Vs "' Volume of water e!(tracted (ml)
W 5 = Weight of sample e1ttracted (gl
V1 = Volume of to1al eictract Cull
. 11-f!tJ~ / & o. o /"' A ..,,, .. lt ~
~ ft} t.Af_
- V - .,l,_C) J .-
form 1 7185
ubora1orv Name. - (p ~ '- .,.,......:r,:Y · -
llaseNo· · 6"Sl,( ---- . Jrganics Analysis Data Sheet
• (Page 4)
T entfttively Identified Compounds
·-=--· --,---------,--~~·--I RT Sc:an CAS NUMMt ft•ction Numbet
E1tirnbtttd Cone.. (ug/1~
1.----½------------------+----+----JJ.------1 2-----f---------------------t-----t----Jl-------1 3. ------1---~-----~----------+----1------4,-----4
/¥OJ" 4 -=---==-----l--~.l.::!.~:&!.LJa~:::t'].,£,l:Jo:A,d"'6,:i~~..4,...j ..... k4d.L----J--6Z.£..J.~+-L....;z.u!(L_+-Sl....2~!:...---4
6. 9 .1.$.>. ,J. /4,00.f
6. --
7_..,..:--_,-b~~~¥.,{.._.~.,,µ.~:i.e:!!~~~~~-+~--f--~~~-.J-_!,,._~~--1 ,5' t> ,J
I ~Ot) ::r' .. _J :· .......,!;-===·;__· --1---·"_. ~--:-------r--~ ............... ~~--• 10.Z,h.U~L-j~~o!Zli4-'~~~T.:&..an,,1,&~~~----¼-----r·.J.J~..!lo,:::;:.-J-....L.L.!:::..J....-,I
,. ,. •• , . ,.
.. ,, J 11.
12 •. ~ lu 1
1• .. ... "' H
.9:t, " .. " ..
1/tJll ... el 21.~J.£./.~r.l-~.f,,LJ~g.t..t:U.,;.-..L::.;.....d~:U.::fJd11.&L-=-~~---+-..:::.--f-..J..:U.....td~..J--J.~U-!=L---f .
22---•-----jf--~-...-:::.a:::i.=~...-:;;.__, _____ .......,,....... _______ -+-----4----~ •• _ .w 7~.7---_ -23. '.ii) 8
24,---~1---------------------t----+------J----......... 25·---~1-------------------t----1------+-----1 26·-----1---------------------it------1------+--------t 21--------1,.--------~-------------it----t------+-------1 28·----+-------------------t---;-----~-----i 29·---~1.--------------------ii-----t-----1------t 30-------ii-.-----------------ii..---......._ ___ __._ ____ .........,
\. I i
II■ ! l
I• ~ l ........... __ "'"""""'&-&•••H ............. , • .,._ • ··•-N ..... _ .. c1 ................... ~ .. ---··
i
fo,m I. Part 8
······· ... ~ ........................................ ······~- ·-··········· ........ .
7 85
O' C a: t-0 0
6-
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