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+5056060864 T-782 POOI F-443Jan-1S-Z00e 0425pm From-EP TA21
-TA21 CLOSURE PROJECT
lOS ALAMOS NATIONAL LABORATORY MAIL STOP C 349
231-0727 FAX 606-1526
DATE -$ - 0 ~
ORGANIZATION PHONE ---------------shy
PHONE ____~_______________
PAGESINCLCQVER
MESSAGE
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~~ cA -eel lt -J ---e ~Yshy
3 v-J ltz CS ltcJ ) )0 u (gtJ ~ - VVI c~ () r- - ~N - 5 Y (c)1 ()0 ~)-v- =cAJ -C~(gt
~ dXVI ~uC)V ~ cgt~y )~~) ~-1-
30307
11111111111111111111111111111111111
F-443 +5056060864 T-78Z P002Jan-15-2008 0425pm From-EP TAZl ~
DP Site Aggregate Area Investigation Work Plan
CJ Structure Investigation area
bull Proposed sample location
reg Proposed boreholQ location
reg FreViQU5 borehole location
Road Pipeline (surveyed location)
Pipeline (engineering drawing location)
- Fence
10-11 contour
0 30 60
FEET 993 NAO t
Borehole 21middot01678 11
- -~-- --
ScmfQO GISL8Il M2tl12S7 amp M200881 Juno 2004 modmed lor F614middot3 DP Cleanup zilo 022805 ptm
Figure 514-3 SWMU 21-024(k) proposed sample locations
June 2005 88 ER2004-04D9
F-443+5056060864 T-782 P003Jan-15-200B 04 25pm From-EP TA21 ~- lage 1 ot
SAMPLE COLLECTION LOGFIELD CHAIN OF CUSTODY EVENT ID 134 EVENT NAME 21-024(k) Dp Aggregate
SAMPLE ID RE21-07-3893
ASfLANNED AIPLANNRD AS COLIReTED
J1PDATE COLLECTED(MMIDYYYy) M)J)[A ~ 0(11)1 OxIfTgt ~ ~~O=-h-~~~-------TlME COLLECTED (H1lMM) SOBmiddotMEDIA
rTct f shyPRS W SAMlLE ftea CODE ampa-- 7(7(07 1-1amp LoeATION 11) =L--~=-=-=---__ FIELD QC TYPE tvf- ) f LOCATlON TIPE GENERlq F~Ll)~fREP amp I TOP DEP1R f~IrII~Jj ----L~-~-- SAMPilEUSAGE lliL Jshy
~IKI]6~7
--------- shyBOTIOM nEPTH fIkrnb3 (07 SCREENiPORT DESC fif FIELDMA1rux ~~ B _____ EXCAVATED YESamp-N-A~---f-~------~----
COMPOSITll TYPE COMPOSITli TIME INTERVAL - WATER FLOWING YEStsectPNA
BOREHOLpound YESampNA BOREHOLED1lCL[NATION ___~__ BOREliOLEDlRECTION ______
=L-2=--~__
PRIORI1y ORDER CNTNR PRESERVATIVE COLLECTED SPECIAL INSTRUCTIONS YIN
2 8082 125 ML GLASS Ice y 2 8290 125 ML GLASS Ice ry I NMED
Explosives list ~MBERGLASS ~ rIhln
Ice y JAMPfEDESC
b ro -r~Pf-
FIELD SCREENINGIlVIEASUREMENT RESULTS shy
pro - 0 c 10 COU-E~D BY (P~ REVIEWED BY (PRINT) ~4-u 1 Jh-t- ~-( 6 bull ~~ 11 L ~ID
RECEIVED BYDateTime DatefTimeRELINQUISHED BY P107(Printed Name) 7110(printed Name) ~~
-(SIgnature) shy(Signature)~~ t)i16CXgt RECEIVED BYDatelTlmoHELINQUISHED BY DateTime
(Printed Name)(Printed Name)
(Signature)Signature)) -
r--
l
Sample]]) RE21-07-3893
(Jie-nt Data
Narue Los Alamos National Laboratory Prajcct 07-294C Dale Collected 17-Jul-07 Tirol Collecied 1415 ~
Analyle Cone (pglg) DL a
2378-TCDD ND 00757
1)378-PeCDD ND 0101
J)3478-HxCDD ND 0370
123678-HxCDD ND 0413
123789-HxCDD 0367
123467S-HpCDD 863
OCDD 52~1
237Jl-TCDF 0]54
12378-PeCDF ND 23478middotPeCDF ND
123478-HxCDF 0301
123678-HxCDF 0207
234678-HxCDF 0229
123789-HxCDF ND 0174
1234678-HpCDF 357
1234789-HpCDF ND 0286
OCDF amp80
Toblls
TolalTCDD ND 00757
TolaIPeCDD middotm 0118
Total HxCDD 254
Total HpCDD 159
Total TCDF 0)78
TotalPeCDF 0729 Total HxCDF 320
Iotal HpCDF 658 ~
Analysi RAS
Project 29211
SUD pTe Data
Matrix Soil Sample SUe 100 g Solids 995
EM PCb Qualifiers
J
J 0136
0128
J J j
0993
EPA Metbod 8290
UibonliOn Data
Lab Sample 29211~OOJ Date Reoeived 19-Jul)7 QC Bald N(l 9210 Date Extracted 25middotulmiddot07 Date A olllyzed DB-S Date Analyzed DJ322S27-Jul-07 NA
Labeled Standard R LCL-UCLd Oualifiers
IS J3C-2378-TCDD 101 40 - 135 13C-I 2378-PeCDD 108 40 - 135
13C-l2347S-HxCDD 109 40-135 BCmiddotl 2367amp-HxCDD 895 40 - 135
I3C-12346 78-HpCDD 100 40 -135
13C-OCDD 795 40middot135 13C-237-TCDF 980 40- 135 13C-1 237amp-PeCDF 106 40- 135
13C-23478-PeCDF 103 40 - 135 Be-123478-HxCDF 114 40 - 135
13C-l23678-HxCDF 892 40 - 135 13C-234678-HxCDF 961 40 - 135
13C-l23789-HxCDF 102 40- [35
13C-I 23467 8middotHpCDF 921 40 - 135 I3C -] 2347 89-HpCDF 110 40 - 135 13CmiddotOCDF 840 40 - 135
CRS 37Cl2378-TCDD 908 40-135 eToxic EquhalcDt Quotien1 (TE-Q) Data
TEQ(Min) 0309
II Sample spaific eslimated detalOO IUn ii
b EStirowted mruciIDWll possi hie oollCWlJati01l
( Melhod detalionlirniL
d WVIeT centroT limil- upper oontroJ limit
e TEQ based on (l989) lnfemal100al To~i1 EjuLAlenl Faclors (lTE)
The results are reported In dry weight The sample size is reported in e4 veiBJlt --- -- -shy
APPnJve1 B) WiHlam J Luksernburg Ol-Aug-20070843
ltshy
i en
I rv lt=gt lt=gt CD
lt=gt ~
en T5 3
a 3 I
rn -0
-I po
+ UI lt=gt U1 0)
cgt 0)
cgt co agt ~
-I I-
co -0
cgt cgt ~
shycgt
I ~ ~
P3pounde 6 of25
F-443 Jan-15-200S 0426pm From-EP TA21 Iigt +5056060864 T-782 P00501S ~~v~~~~~~ ~N~ORHA-~~~wNO unauthorized reproduet1on witbout ~~en pe~io1on fr~ Gg~
1_-()~4tt) High Explosives Analysts Data Sheet
Lab Name General Engineering laboratories Client Sample ID RB21-07-3S93
Lab Code GEl GELJobNo(SDG) ~
Matrb ~ GEL Sample ID 189817001
Sample AIIlount 2 Molstue 2
Date Received 19middotJOL07Amount Vnlb S
Extract-bID Type Sonioation Extraction Bakh ID 653048
Copwf1Cl-atea Extract Volumt(mL) 12 Date Extracted 25JUL07
DllutllWlFactorr a InJ~ton Volume (uL) 50
Daee Analyzed02-AUG07 2023 GEL dUII file BXS080a0J16wiff
Untts ugkg______bull _____wow _______
r ----~ ( - Cas No 1 Compound QConcentration
TATB 1000 U3058-38-6 i 2ampDiamino-4-nitrotoluene 200059229-75-3 U
35-Dinitroaniline 1000 U~_ 618-8-1 24jDiamino6-nitrotoluene 2000 U 6629-29-4 tris(ocresyl) phosphate 1000 UCmiddot 78-30~8
I ~Coln~atmtion bull
llnSrrUlDtlt X ConcentrudExtract Volume x Dilution Vahtl Ie Amoun Factor
Page 2 of 2
Page 18 of329
Jan-15-Z00a 0426pm From-EP TAZl +5056060B64 T-7B2 P0060l3 F-443 _v~ ~MV~ middotU unu=aa roproaUat10Jl wlthout 1ft bull ~n pS1lll1allion flOlII GlBL
1 High Explosives Analysis Data Sheet
Lub Name General Engineerillg Laboratories Cllent Sample ID RE21-07-3893
Lab Code GEt GEL Job No (SDG) 07-293
Matrix ~ioIL GEL Sample ID 189817001
Sample AnDllDt a MoisCure ll
Date Received Amount llhl~ g
Extraction Batch ID 653048ExtradlonType ~tion
Coneentrlllted Rxtla~Hfolulne (mL) lQ Date Extracted 25middotJUL-07
DUatlon fictor ~ bUection Volumo (nL) ~
nte Analy2tdr 30-IDL-07 1916GEL dauHlile BXm130015a
Units ugkg
I
I
I
--UasNo 18-96-7
L21-14-2
111-82-4
U~06middot51middot0
~5e1-41-0
31572middot78middot2
9-45-8Ei6-0-2 nmiddotllmiddot5
bull li8middot7zZ 11-95-3
middot1J108-1
I 993$-4
1
~)j65-0
9~J99middot0 - shy -__--_-
C03J]ound 246middotTriIIlitrotoJuene
24-pidrotoluelle
aDX
4-Amino-2ampdinitrotoluene
aMX 2-Amino-4dinitrotoluene
retryl
26-DiDitrotoluene
mTN
o-Nilrololuene
Nitr~enzene
m-Nitratoluene
135-TriniCrobcnzene
m-Dinittobenzene
p-NirrorQuene
Concentration 500
500
500
500
SOO SOO SOO 500
1000
500
i 500
500
500
SOO soo
-~
U
U
U
U
U
U
u I
U -I U
U i
U i U
U
U
~J
Concentrwon =0
Instrument X Concentllllted Bxrract Volumll X Dilution Value Sam~e Amoun Factor
Page 1 of 2
Page 17 of 329
T-782 POO7l013 F-443 $ +5056060864Jan-15-200S 04 26pm From-EP TA2l __r
GEL lAboratQlies LLC Report Dllte AuguSll 2007
PCB Page 1 of 1 Certificate of Analysis
Sample Summary
SDG NUlllber 07-293 Da~ Collected 07171Z0071200 Man-Ix SOIL
Lab Sample ID 189817001 Date Reccied 071l9J200709)0 Moislure 7 Client SlUllple 12 Client LANL006 Project LANLOOGOO ClientID RE2-07-3893 Method SW846)082 SOP Ref CL-OA-E-04ll
Batch ID 653073 lrut ECD2A1 DIlution 1
Run Daoo 0712712007 1258 AnaYBt JXM Inj Vol tIlL lnpDllte 071J320070800 Aliquot 30~ FInal Volume ImL Dab File 014tl401d Column 1 eLFl Level LOW
014b140~d 2CLP2
CAS No Parnmame Qualifler Result Units Ml)ULOD PQULOQ CoIWl1lI
12674-lJ-2 Aroclor-1016 U 336 uglkg Ll2 336
11104-28-2 Aroclor-1221 U 3~6 uglkg 112 336
1114l-16-) Atoclor-1232 U 336 lIglkg 112 336
53469-21-9 Arocor-1242 U 336 Ilglkg LI2 336
12672-29-lt ArocIOr-l24amp U 336 uSlkg 112 336
1I097-6H Aroclor-12S4 J 120 lIgkg 112 336
11096-82-5 Aroclar-1260 U 336 uglkg 112 336
Page 208 of329
-----
~ 2 ~ o lt0
f
o (N
~ ltll
g 01
-~ - --~
11gt319
21-353 21-485 J I Investigation area
~ Ifor SWMU 21-027(a) j( 4-in floor drain pipe ~ U engineerillg drawing location) I
f r I ~~ ~12~n storm drarfl cemeflt culvert _lturveyecl location)
J I I
_I I I J
I J J shylI
I -~
-
cJ Slructu ra
l- I Former slructure
Jilvestigalion area
bull Proposed sample toeation
reg Prop()Sed borehole location amp Previous sample localirm euroI Previous bOfehole localion
Pipeline (surveyed location)
Pjpeline (enQineering drawjng localion)
Road
Fenoe 10-fl c1I110Uf
0 40 80
FEET 19113 HAl) t
bull 7rlltJ bull
- _shy
- ~ ~ 7050---middot
- -------- -~--~-
-
-- ~-~
- -~ --~ --- ~ - -- - -~~t= _
- - - --~~~
r050- _15 - -~- -- - - -~
---- ~ -~- _--_ -
- ~ ~--~~ -- ~ ----- -----~-i~ ~~-~ shy ~ - ~ ~
Slu1s GISLab tA201224 061 4ll4 mgtflfied far F5193 IlPwai sile 1l3D1igt5 plrn
Figure 519-3 SWMU 21-027(a) proposed sample locations
tI ll (()
ft ) ltc co ~ (0 fIl iii p a IJ)
s ~ ~ IJ)
amp 3
~ ~ J1)J
L
-
I c c 0
c jgt
0 = C 5 I
~
+ UI c UI en cl
cl jo
-4
-I ltXl
C
= = ltXl- = cJ
-n I
___
Jilil-IO-UUO U4QPm rrum-tr IA +bUb1i060664 T-78Z P009013 F-443 LU~ fllUllU~ rl~110nal Luoorarory Page I or
SAMPLE COLLECTION LOGFIELD CHAIN OF CUSTODY EVENT ID 198 EVENT NAME CU21-027(a) DP Site Summer]a1l2007
) SAMPLE ID RE21-07-SS93
ASPLANNtP
DATE COLLECfED(MMlDDIVYYV)
TIME COLLECTED (HlIMM)
PRS ID ZHIZ(JI
LOCATIONm ~~11u1 LOCATION TYPE GENpoundRlC
~~v
TOP DEPTH-fIljrid 7
BonOM DEPTH -r i01 FIElJlMTR1X --5- ~~~I
i ~( ~()T COMPOSITETVPpound --
ASCQLLECTpoundll
2 ftro 7
u C bull 2( o h
R- II01d-2S lei( 4b
4 0 ft- 4 0 f 1shy
bull (
MEDIA
SUBmiddotli--shy~w
SAMPLE TECH CODE
FIELD QCTVPE
FIELD PREP
SAMlLtlJSAGE
SCREENIlOlU DESC
AS PLANNED rev
~ lJhlt77
W 11 rJ
~ 1)
amp
amp
INV
A
ASCQLLECTED
(1 h 1- 3 D tC1 A Cd t
1
tY
EXCAVATED YfSte~N--A----------------Ii
COMPOSITpoundnME1NTERVAL WATER FLOWING YES~NA
BOREHOLE YES~A BOREHOLE DECLINATION ___~__ BOREHOLE DIRECTION shy
PRIOnlTY ORD~R CNTNR PRESERVATIVE COLLECTED YIN
SPECIAL INSTRUCTIONS
2
2
1
8082
8290
NMED Explosives list
125MLGLASS
125MLGLASS
250 l1L AMBER GLASS
_ _-_ _shy
Ice
Ice
Ice
V y
L _____ --_ )SAMPLE DESC t Quck I uGrvi- 15~ Gr~v TIImiddotH
SAMPLE COMMENTS
LOCATIONDESC Y-1lt~tLev ~k
shy
~c~~ 4(0 ]n Ie r fr-Dt71 (one) 113 ~r~ 1110 CIir
FIELD SCREENINGIMEASUREMENT RESULTS flO bf-c ygtY1rxi- 0 -0 r31r
f ~ I rf olcJ1f p j tJ~ Ot p17d 7-tdfM
REVIEWED BY (PRINT ___________COLLECT~DBY (pRINT) _ __---Vi shyr shy -
DateffilneDateffime RECEIVED BYRELINQUISHED BY I070 r (Printed Name)
(Signature)
(Printed Name) )C20(Signature) Jo~~
RECEIVED BY Datetrime
I (Printed Name)
DateITimeRELINQUISHED BY
(Printed N arne)
(Signature)(Signature)
I I
I
I
CL
cYgt
shy
u Sample ill RE21-07-5893 (Q
Client Data = Los Alamoo National Laboratory 0amp-347 S-Dee-07 0830
Samlc Data
Malrix Soil Sample Size t 13 g
middotSolids 894
shycgt
cgt
Name Project Date Collected Time Collected
co I Analyte Cone (pglg) DL a EWCb Qualifierst-
2378-TCDD 12378-PeCDD
l23478-HxCDD
123678-HxCDD
ltJgt CO Cgt 123789-HxCDDUgt cgt lt0 LO
1234678-HpCDD = In + OeDD
2378-TCDF
12378-PeCDF 23478-PeCDF
123478-HxCDF 12367 8-HxC DF
23 467amp-HxCDF
123789middotHxCDF
1234678-HpCDF 1234789-HpCDF
aCDF
Totals
0599 322
63amp
379
16l
1320
15200 0302
0503 L4J
492
382
692
129 [52
142
503
423
279 259 2790
643
276
205
726
435
284
699
J
I J
J B
B
EPA lVlcthod 8290
labontoa Data
Lab Sample 30042~OOl Dare Reeeind 7-Dec-07 QC Batch No 9763 Date ExlIllc[ltd 1O-Dec-07 Dale Analyzed DB-5 13-Dee-07 [)ate Analyzrd DB-225 NA
_shy
Labeled Standard R LeL-UCLd Qualifiers _ shy
IS t3C-2J78-TCDD 898 4) - 13S 13C-[2J7S-PeCDD 916 40 - 135 13C-l23478-HxCDD 935 40- 135 13C-l236 78-HltCD 0 816 40 - 135
lJC-l234678-HpCDD 104shy 40 shy 135 13C-OCDD 122 40 shy l35 13C-2378-TCDF 100 40 - 135 llC-l 2378- PeC DF [04 40- 135 13C-23478-PeCDF 109 40- fJ5 [3C-I2JA78-HKCDF 914 40 - 135
l3C- 123678-HxCDF 792 4() - lJ5 l3C-234678-HxCDP 842 40 shy 135
13C-l23789-HxCDF 9l2 40- 135 [3C-1234678-HpCDF 847 40 shy [35
13C-1234789-HpCDF 991 40 - DS L3C-QCDF 985 40 shy 135
CRS 37Cl-2378-TCDD 936 40 shy 135 eTodc Equivalent Qnotient (fEQ) Data
-lt t-CL UJ
I E o ~
LL
E n
lt0
cgt agt lt=gt cgt
I tn
I c
TotalrCDD
Total PeCDD Total HxCDD Total HpCDD Total TCDF Total PeCDF Total HxCDF
Tota[ HpCDF
Anal~st MAS
P
P
P BP
TEQ(Min) 413
a Sample specific etimated detection j iInil
b Eslilnated maximum possible cQfcenlfatioll
c Method detec1iol1lirniL
d Lo1r~oltrollimil- uppNcolltrollimit
e 7EQ based an (1989) [nternatiooal roxie EquiaIent Filltturs (ITEn
The fltlltl-Wll are repooed in dry weighl The sam pIe size is rej)lJrtild in wltt weight
AwrovedBy Martha M Maier lJ-Dec-2007 1527
T-782 P 011013 F-443Jilll-IO-UUO U4 opm rrom-II III +5056060864
1 High Explosives Analysls Data Sheet
I CalNo 118-96-7
I 121~14-2 Irshy 121-82-4
19406-51-0
2691-41middot0
35572~7g2
479-45-8
606middot20middot2 78-11-5
88-72-2
98-95-3
99-08-1 -~
9935-4
99middot65middot0 f
99w99-0l
Lab Name General Engineering Lahorarcries Client Sample ID RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sample ID 198941001
Moistm-e 103Sample Amount pound
Amoullt Units l Date Received 07~DECmiddot07
Extl8ction Type Sonicatioll Extraction Batch In 709399
COllcenhated Extlllct Volume (UlL) ill Dale Extracted 12middotDEC-07
PllutlOll Facto ~ Injection Volume CuLl ~
Date Analyzed 1H)EC-07 1529GEL (lata tJle EXP12l20S7a
Units ugJkg __ n _
ComJound Concentration -Q]- - 500246-Trinitrotoh Hme 1 U I
~ 24middotDinitrotolu~ene SOD I U
Rl)X 500 I u1 4-Amino-26dinibmiddoto l) illene 500 r-u-
HMX
2-Amino-46-dinitro ojuelle
Tetryl
I 26-Dlllltrotolul~ ~ lUi middot-------~------~----~-----~--t
a
PElN 1000 U wNitrotoluellc
500 ~-1 Nitrobenzen 500 I U
i m-NitrotolUefle SOD I u 135-Tdnitrober zelle 500 I U
ffi-Dinitrobenzi ne 1 500 lUi p-Nitrotoluel1e 500 I U
____ ___-l_____ _ __ ___ L___~ - ~
_ soo U
500 U -i 500 U
-J
-----~~------------ ----- shy Concentration
Instnment X ConcenUllred Extract Volume X Dilutioll Value Samele ArnouD Factor
Page of 2
Page 93 of344
Jan-IO-UU~ U4pm Irom-t IAll +5056060864 T-782 P012013 F-443
1 High Explosives Analysis DII tn Sheet
Lab Name Qeneml Engineering Laboratories Client Sample llgt RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sam)Je lD 198947001
Moisture 103Sample Amount 2
Date Received 07-DEC-07Amount Unitli g
Extmction Type Sonication Extractiou Batch ID 709399
Concentrated Extract Volume (mL) 12 Date Extracted 12-DECmiddot07
Dilution Fact6r Injection Volume (uL) 50
Date Analyzed 17middotDECmiddot07 1903 GEL data file EXS12 17035wiff
Units ugkg
Cas No 3058middot386
59229-7S-3
Compound TATB
26-Diminc-4-nitI
- shy --- Concentnnkm -~T-0-1 1000 -~
2000 1u 618middot87-1 3SmiddotDinitroaniIinc 1000 U
6629--29-4
78-30-8
24Dlamlno-6-iroii~n-trls(o-cresyl) phosphate _~___~ bull -
- ] 2000 U bull
1000 U -1I __bullbull_ bullbullbull___ ~_________ I--_~ I
-~-------- ---shyConcenlrarion
IloSlfllmem X Concanrated Etracr Volllrne Dilution L Value ~__~ Sample Amoun X Factor
Page 2 of 2
Page 96 of344
-
II-IO-UUC Uflpm rrom-cr 111pound I +5056060864 T-782 P013013 F-443
GE~ Inboratories LLe Report Date December 15 2007
SDGNuwber 08-348 Lab Sample ill 198947001
CilelltID REZT-Ol-S893
)llltch fI) 10954l
RunDllte 1211412007 0149
Prep Date 121102007 1953
DlItli FIle 049f4901d
049b49111d
CAS No Fucmname --shy
12674-Il-2 Aruclor-l 0 16
11104-28-2 Arocior-1221
11141-16-5 AroelOr- 1232
53469-21-9 Aroclor-1242
12672-29-6 Aroclor-1248
11097-69-1 Aroclor-1254
11096-81-5 Aroclor-1260
PCB Certifieate of Analysts
Sample Summary
Date Collected 1210512007 1200
Dute Received 120712007 0930 Client LANL008
Method SW84ti8082
In8t EC02Al
Analyst JXM Aliquot 29911 Column lCLPl
2CLP2
Quulitiec Result l1nits ------ U 373 Ij1kg
U 373 uglkg
U 373 ujlkg
U 373 uglkg
U 373 u1kg
950 uglkg
690 uglkg
Page I of 1
Ma[th S
Moistllre 103 Project LANLOO800 SOPRlf GL-oA-E-040 Dilution 1
Inj Vol luI binlll Volume ImL
Level LOW
MDLtrOD PQt1OQ Column shy
124 373
124 373
124 373
124 373
24 373
124 373 2
124 373
Page 232 of 344
-
F-443 +5056060864 T-78Z P002Jan-15-2008 0425pm From-EP TAZl ~
DP Site Aggregate Area Investigation Work Plan
CJ Structure Investigation area
bull Proposed sample location
reg Proposed boreholQ location
reg FreViQU5 borehole location
Road Pipeline (surveyed location)
Pipeline (engineering drawing location)
- Fence
10-11 contour
0 30 60
FEET 993 NAO t
Borehole 21middot01678 11
- -~-- --
ScmfQO GISL8Il M2tl12S7 amp M200881 Juno 2004 modmed lor F614middot3 DP Cleanup zilo 022805 ptm
Figure 514-3 SWMU 21-024(k) proposed sample locations
June 2005 88 ER2004-04D9
F-443+5056060864 T-782 P003Jan-15-200B 04 25pm From-EP TA21 ~- lage 1 ot
SAMPLE COLLECTION LOGFIELD CHAIN OF CUSTODY EVENT ID 134 EVENT NAME 21-024(k) Dp Aggregate
SAMPLE ID RE21-07-3893
ASfLANNED AIPLANNRD AS COLIReTED
J1PDATE COLLECTED(MMIDYYYy) M)J)[A ~ 0(11)1 OxIfTgt ~ ~~O=-h-~~~-------TlME COLLECTED (H1lMM) SOBmiddotMEDIA
rTct f shyPRS W SAMlLE ftea CODE ampa-- 7(7(07 1-1amp LoeATION 11) =L--~=-=-=---__ FIELD QC TYPE tvf- ) f LOCATlON TIPE GENERlq F~Ll)~fREP amp I TOP DEP1R f~IrII~Jj ----L~-~-- SAMPilEUSAGE lliL Jshy
~IKI]6~7
--------- shyBOTIOM nEPTH fIkrnb3 (07 SCREENiPORT DESC fif FIELDMA1rux ~~ B _____ EXCAVATED YESamp-N-A~---f-~------~----
COMPOSITll TYPE COMPOSITli TIME INTERVAL - WATER FLOWING YEStsectPNA
BOREHOLpound YESampNA BOREHOLED1lCL[NATION ___~__ BOREliOLEDlRECTION ______
=L-2=--~__
PRIORI1y ORDER CNTNR PRESERVATIVE COLLECTED SPECIAL INSTRUCTIONS YIN
2 8082 125 ML GLASS Ice y 2 8290 125 ML GLASS Ice ry I NMED
Explosives list ~MBERGLASS ~ rIhln
Ice y JAMPfEDESC
b ro -r~Pf-
FIELD SCREENINGIlVIEASUREMENT RESULTS shy
pro - 0 c 10 COU-E~D BY (P~ REVIEWED BY (PRINT) ~4-u 1 Jh-t- ~-( 6 bull ~~ 11 L ~ID
RECEIVED BYDateTime DatefTimeRELINQUISHED BY P107(Printed Name) 7110(printed Name) ~~
-(SIgnature) shy(Signature)~~ t)i16CXgt RECEIVED BYDatelTlmoHELINQUISHED BY DateTime
(Printed Name)(Printed Name)
(Signature)Signature)) -
r--
l
Sample]]) RE21-07-3893
(Jie-nt Data
Narue Los Alamos National Laboratory Prajcct 07-294C Dale Collected 17-Jul-07 Tirol Collecied 1415 ~
Analyle Cone (pglg) DL a
2378-TCDD ND 00757
1)378-PeCDD ND 0101
J)3478-HxCDD ND 0370
123678-HxCDD ND 0413
123789-HxCDD 0367
123467S-HpCDD 863
OCDD 52~1
237Jl-TCDF 0]54
12378-PeCDF ND 23478middotPeCDF ND
123478-HxCDF 0301
123678-HxCDF 0207
234678-HxCDF 0229
123789-HxCDF ND 0174
1234678-HpCDF 357
1234789-HpCDF ND 0286
OCDF amp80
Toblls
TolalTCDD ND 00757
TolaIPeCDD middotm 0118
Total HxCDD 254
Total HpCDD 159
Total TCDF 0)78
TotalPeCDF 0729 Total HxCDF 320
Iotal HpCDF 658 ~
Analysi RAS
Project 29211
SUD pTe Data
Matrix Soil Sample SUe 100 g Solids 995
EM PCb Qualifiers
J
J 0136
0128
J J j
0993
EPA Metbod 8290
UibonliOn Data
Lab Sample 29211~OOJ Date Reoeived 19-Jul)7 QC Bald N(l 9210 Date Extracted 25middotulmiddot07 Date A olllyzed DB-S Date Analyzed DJ322S27-Jul-07 NA
Labeled Standard R LCL-UCLd Oualifiers
IS J3C-2378-TCDD 101 40 - 135 13C-I 2378-PeCDD 108 40 - 135
13C-l2347S-HxCDD 109 40-135 BCmiddotl 2367amp-HxCDD 895 40 - 135
I3C-12346 78-HpCDD 100 40 -135
13C-OCDD 795 40middot135 13C-237-TCDF 980 40- 135 13C-1 237amp-PeCDF 106 40- 135
13C-23478-PeCDF 103 40 - 135 Be-123478-HxCDF 114 40 - 135
13C-l23678-HxCDF 892 40 - 135 13C-234678-HxCDF 961 40 - 135
13C-l23789-HxCDF 102 40- [35
13C-I 23467 8middotHpCDF 921 40 - 135 I3C -] 2347 89-HpCDF 110 40 - 135 13CmiddotOCDF 840 40 - 135
CRS 37Cl2378-TCDD 908 40-135 eToxic EquhalcDt Quotien1 (TE-Q) Data
TEQ(Min) 0309
II Sample spaific eslimated detalOO IUn ii
b EStirowted mruciIDWll possi hie oollCWlJati01l
( Melhod detalionlirniL
d WVIeT centroT limil- upper oontroJ limit
e TEQ based on (l989) lnfemal100al To~i1 EjuLAlenl Faclors (lTE)
The results are reported In dry weight The sample size is reported in e4 veiBJlt --- -- -shy
APPnJve1 B) WiHlam J Luksernburg Ol-Aug-20070843
ltshy
i en
I rv lt=gt lt=gt CD
lt=gt ~
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rn -0
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F-443 Jan-15-200S 0426pm From-EP TA21 Iigt +5056060864 T-782 P00501S ~~v~~~~~~ ~N~ORHA-~~~wNO unauthorized reproduet1on witbout ~~en pe~io1on fr~ Gg~
1_-()~4tt) High Explosives Analysts Data Sheet
Lab Name General Engineering laboratories Client Sample ID RB21-07-3S93
Lab Code GEl GELJobNo(SDG) ~
Matrb ~ GEL Sample ID 189817001
Sample AIIlount 2 Molstue 2
Date Received 19middotJOL07Amount Vnlb S
Extract-bID Type Sonioation Extraction Bakh ID 653048
Copwf1Cl-atea Extract Volumt(mL) 12 Date Extracted 25JUL07
DllutllWlFactorr a InJ~ton Volume (uL) 50
Daee Analyzed02-AUG07 2023 GEL dUII file BXS080a0J16wiff
Untts ugkg______bull _____wow _______
r ----~ ( - Cas No 1 Compound QConcentration
TATB 1000 U3058-38-6 i 2ampDiamino-4-nitrotoluene 200059229-75-3 U
35-Dinitroaniline 1000 U~_ 618-8-1 24jDiamino6-nitrotoluene 2000 U 6629-29-4 tris(ocresyl) phosphate 1000 UCmiddot 78-30~8
I ~Coln~atmtion bull
llnSrrUlDtlt X ConcentrudExtract Volume x Dilution Vahtl Ie Amoun Factor
Page 2 of 2
Page 18 of329
Jan-15-Z00a 0426pm From-EP TAZl +5056060B64 T-7B2 P0060l3 F-443 _v~ ~MV~ middotU unu=aa roproaUat10Jl wlthout 1ft bull ~n pS1lll1allion flOlII GlBL
1 High Explosives Analysis Data Sheet
Lub Name General Engineerillg Laboratories Cllent Sample ID RE21-07-3893
Lab Code GEt GEL Job No (SDG) 07-293
Matrix ~ioIL GEL Sample ID 189817001
Sample AnDllDt a MoisCure ll
Date Received Amount llhl~ g
Extraction Batch ID 653048ExtradlonType ~tion
Coneentrlllted Rxtla~Hfolulne (mL) lQ Date Extracted 25middotJUL-07
DUatlon fictor ~ bUection Volumo (nL) ~
nte Analy2tdr 30-IDL-07 1916GEL dauHlile BXm130015a
Units ugkg
I
I
I
--UasNo 18-96-7
L21-14-2
111-82-4
U~06middot51middot0
~5e1-41-0
31572middot78middot2
9-45-8Ei6-0-2 nmiddotllmiddot5
bull li8middot7zZ 11-95-3
middot1J108-1
I 993$-4
1
~)j65-0
9~J99middot0 - shy -__--_-
C03J]ound 246middotTriIIlitrotoJuene
24-pidrotoluelle
aDX
4-Amino-2ampdinitrotoluene
aMX 2-Amino-4dinitrotoluene
retryl
26-DiDitrotoluene
mTN
o-Nilrololuene
Nitr~enzene
m-Nitratoluene
135-TriniCrobcnzene
m-Dinittobenzene
p-NirrorQuene
Concentration 500
500
500
500
SOO SOO SOO 500
1000
500
i 500
500
500
SOO soo
-~
U
U
U
U
U
U
u I
U -I U
U i
U i U
U
U
~J
Concentrwon =0
Instrument X Concentllllted Bxrract Volumll X Dilution Value Sam~e Amoun Factor
Page 1 of 2
Page 17 of 329
T-782 POO7l013 F-443 $ +5056060864Jan-15-200S 04 26pm From-EP TA2l __r
GEL lAboratQlies LLC Report Dllte AuguSll 2007
PCB Page 1 of 1 Certificate of Analysis
Sample Summary
SDG NUlllber 07-293 Da~ Collected 07171Z0071200 Man-Ix SOIL
Lab Sample ID 189817001 Date Reccied 071l9J200709)0 Moislure 7 Client SlUllple 12 Client LANL006 Project LANLOOGOO ClientID RE2-07-3893 Method SW846)082 SOP Ref CL-OA-E-04ll
Batch ID 653073 lrut ECD2A1 DIlution 1
Run Daoo 0712712007 1258 AnaYBt JXM Inj Vol tIlL lnpDllte 071J320070800 Aliquot 30~ FInal Volume ImL Dab File 014tl401d Column 1 eLFl Level LOW
014b140~d 2CLP2
CAS No Parnmame Qualifler Result Units Ml)ULOD PQULOQ CoIWl1lI
12674-lJ-2 Aroclor-1016 U 336 uglkg Ll2 336
11104-28-2 Aroclor-1221 U 3~6 uglkg 112 336
1114l-16-) Atoclor-1232 U 336 lIglkg 112 336
53469-21-9 Arocor-1242 U 336 Ilglkg LI2 336
12672-29-lt ArocIOr-l24amp U 336 uSlkg 112 336
1I097-6H Aroclor-12S4 J 120 lIgkg 112 336
11096-82-5 Aroclar-1260 U 336 uglkg 112 336
Page 208 of329
-----
~ 2 ~ o lt0
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21-353 21-485 J I Investigation area
~ Ifor SWMU 21-027(a) j( 4-in floor drain pipe ~ U engineerillg drawing location) I
f r I ~~ ~12~n storm drarfl cemeflt culvert _lturveyecl location)
J I I
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I J J shylI
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-
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l- I Former slructure
Jilvestigalion area
bull Proposed sample toeation
reg Prop()Sed borehole location amp Previous sample localirm euroI Previous bOfehole localion
Pipeline (surveyed location)
Pjpeline (enQineering drawjng localion)
Road
Fenoe 10-fl c1I110Uf
0 40 80
FEET 19113 HAl) t
bull 7rlltJ bull
- _shy
- ~ ~ 7050---middot
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-
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Slu1s GISLab tA201224 061 4ll4 mgtflfied far F5193 IlPwai sile 1l3D1igt5 plrn
Figure 519-3 SWMU 21-027(a) proposed sample locations
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SAMPLE COLLECTION LOGFIELD CHAIN OF CUSTODY EVENT ID 198 EVENT NAME CU21-027(a) DP Site Summer]a1l2007
) SAMPLE ID RE21-07-SS93
ASPLANNtP
DATE COLLECfED(MMlDDIVYYV)
TIME COLLECTED (HlIMM)
PRS ID ZHIZ(JI
LOCATIONm ~~11u1 LOCATION TYPE GENpoundRlC
~~v
TOP DEPTH-fIljrid 7
BonOM DEPTH -r i01 FIElJlMTR1X --5- ~~~I
i ~( ~()T COMPOSITETVPpound --
ASCQLLECTpoundll
2 ftro 7
u C bull 2( o h
R- II01d-2S lei( 4b
4 0 ft- 4 0 f 1shy
bull (
MEDIA
SUBmiddotli--shy~w
SAMPLE TECH CODE
FIELD QCTVPE
FIELD PREP
SAMlLtlJSAGE
SCREENIlOlU DESC
AS PLANNED rev
~ lJhlt77
W 11 rJ
~ 1)
amp
amp
INV
A
ASCQLLECTED
(1 h 1- 3 D tC1 A Cd t
1
tY
EXCAVATED YfSte~N--A----------------Ii
COMPOSITpoundnME1NTERVAL WATER FLOWING YES~NA
BOREHOLE YES~A BOREHOLE DECLINATION ___~__ BOREHOLE DIRECTION shy
PRIOnlTY ORD~R CNTNR PRESERVATIVE COLLECTED YIN
SPECIAL INSTRUCTIONS
2
2
1
8082
8290
NMED Explosives list
125MLGLASS
125MLGLASS
250 l1L AMBER GLASS
_ _-_ _shy
Ice
Ice
Ice
V y
L _____ --_ )SAMPLE DESC t Quck I uGrvi- 15~ Gr~v TIImiddotH
SAMPLE COMMENTS
LOCATIONDESC Y-1lt~tLev ~k
shy
~c~~ 4(0 ]n Ie r fr-Dt71 (one) 113 ~r~ 1110 CIir
FIELD SCREENINGIMEASUREMENT RESULTS flO bf-c ygtY1rxi- 0 -0 r31r
f ~ I rf olcJ1f p j tJ~ Ot p17d 7-tdfM
REVIEWED BY (PRINT ___________COLLECT~DBY (pRINT) _ __---Vi shyr shy -
DateffilneDateffime RECEIVED BYRELINQUISHED BY I070 r (Printed Name)
(Signature)
(Printed Name) )C20(Signature) Jo~~
RECEIVED BY Datetrime
I (Printed Name)
DateITimeRELINQUISHED BY
(Printed N arne)
(Signature)(Signature)
I I
I
I
CL
cYgt
shy
u Sample ill RE21-07-5893 (Q
Client Data = Los Alamoo National Laboratory 0amp-347 S-Dee-07 0830
Samlc Data
Malrix Soil Sample Size t 13 g
middotSolids 894
shycgt
cgt
Name Project Date Collected Time Collected
co I Analyte Cone (pglg) DL a EWCb Qualifierst-
2378-TCDD 12378-PeCDD
l23478-HxCDD
123678-HxCDD
ltJgt CO Cgt 123789-HxCDDUgt cgt lt0 LO
1234678-HpCDD = In + OeDD
2378-TCDF
12378-PeCDF 23478-PeCDF
123478-HxCDF 12367 8-HxC DF
23 467amp-HxCDF
123789middotHxCDF
1234678-HpCDF 1234789-HpCDF
aCDF
Totals
0599 322
63amp
379
16l
1320
15200 0302
0503 L4J
492
382
692
129 [52
142
503
423
279 259 2790
643
276
205
726
435
284
699
J
I J
J B
B
EPA lVlcthod 8290
labontoa Data
Lab Sample 30042~OOl Dare Reeeind 7-Dec-07 QC Batch No 9763 Date ExlIllc[ltd 1O-Dec-07 Dale Analyzed DB-5 13-Dee-07 [)ate Analyzrd DB-225 NA
_shy
Labeled Standard R LeL-UCLd Qualifiers _ shy
IS t3C-2J78-TCDD 898 4) - 13S 13C-[2J7S-PeCDD 916 40 - 135 13C-l23478-HxCDD 935 40- 135 13C-l236 78-HltCD 0 816 40 - 135
lJC-l234678-HpCDD 104shy 40 shy 135 13C-OCDD 122 40 shy l35 13C-2378-TCDF 100 40 - 135 llC-l 2378- PeC DF [04 40- 135 13C-23478-PeCDF 109 40- fJ5 [3C-I2JA78-HKCDF 914 40 - 135
l3C- 123678-HxCDF 792 4() - lJ5 l3C-234678-HxCDP 842 40 shy 135
13C-l23789-HxCDF 9l2 40- 135 [3C-1234678-HpCDF 847 40 shy [35
13C-1234789-HpCDF 991 40 - DS L3C-QCDF 985 40 shy 135
CRS 37Cl-2378-TCDD 936 40 shy 135 eTodc Equivalent Qnotient (fEQ) Data
-lt t-CL UJ
I E o ~
LL
E n
lt0
cgt agt lt=gt cgt
I tn
I c
TotalrCDD
Total PeCDD Total HxCDD Total HpCDD Total TCDF Total PeCDF Total HxCDF
Tota[ HpCDF
Anal~st MAS
P
P
P BP
TEQ(Min) 413
a Sample specific etimated detection j iInil
b Eslilnated maximum possible cQfcenlfatioll
c Method detec1iol1lirniL
d Lo1r~oltrollimil- uppNcolltrollimit
e 7EQ based an (1989) [nternatiooal roxie EquiaIent Filltturs (ITEn
The fltlltl-Wll are repooed in dry weighl The sam pIe size is rej)lJrtild in wltt weight
AwrovedBy Martha M Maier lJ-Dec-2007 1527
T-782 P 011013 F-443Jilll-IO-UUO U4 opm rrom-II III +5056060864
1 High Explosives Analysls Data Sheet
I CalNo 118-96-7
I 121~14-2 Irshy 121-82-4
19406-51-0
2691-41middot0
35572~7g2
479-45-8
606middot20middot2 78-11-5
88-72-2
98-95-3
99-08-1 -~
9935-4
99middot65middot0 f
99w99-0l
Lab Name General Engineering Lahorarcries Client Sample ID RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sample ID 198941001
Moistm-e 103Sample Amount pound
Amoullt Units l Date Received 07~DECmiddot07
Extl8ction Type Sonicatioll Extraction Batch In 709399
COllcenhated Extlllct Volume (UlL) ill Dale Extracted 12middotDEC-07
PllutlOll Facto ~ Injection Volume CuLl ~
Date Analyzed 1H)EC-07 1529GEL (lata tJle EXP12l20S7a
Units ugJkg __ n _
ComJound Concentration -Q]- - 500246-Trinitrotoh Hme 1 U I
~ 24middotDinitrotolu~ene SOD I U
Rl)X 500 I u1 4-Amino-26dinibmiddoto l) illene 500 r-u-
HMX
2-Amino-46-dinitro ojuelle
Tetryl
I 26-Dlllltrotolul~ ~ lUi middot-------~------~----~-----~--t
a
PElN 1000 U wNitrotoluellc
500 ~-1 Nitrobenzen 500 I U
i m-NitrotolUefle SOD I u 135-Tdnitrober zelle 500 I U
ffi-Dinitrobenzi ne 1 500 lUi p-Nitrotoluel1e 500 I U
____ ___-l_____ _ __ ___ L___~ - ~
_ soo U
500 U -i 500 U
-J
-----~~------------ ----- shy Concentration
Instnment X ConcenUllred Extract Volume X Dilutioll Value Samele ArnouD Factor
Page of 2
Page 93 of344
Jan-IO-UU~ U4pm Irom-t IAll +5056060864 T-782 P012013 F-443
1 High Explosives Analysis DII tn Sheet
Lab Name Qeneml Engineering Laboratories Client Sample llgt RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sam)Je lD 198947001
Moisture 103Sample Amount 2
Date Received 07-DEC-07Amount Unitli g
Extmction Type Sonication Extractiou Batch ID 709399
Concentrated Extract Volume (mL) 12 Date Extracted 12-DECmiddot07
Dilution Fact6r Injection Volume (uL) 50
Date Analyzed 17middotDECmiddot07 1903 GEL data file EXS12 17035wiff
Units ugkg
Cas No 3058middot386
59229-7S-3
Compound TATB
26-Diminc-4-nitI
- shy --- Concentnnkm -~T-0-1 1000 -~
2000 1u 618middot87-1 3SmiddotDinitroaniIinc 1000 U
6629--29-4
78-30-8
24Dlamlno-6-iroii~n-trls(o-cresyl) phosphate _~___~ bull -
- ] 2000 U bull
1000 U -1I __bullbull_ bullbullbull___ ~_________ I--_~ I
-~-------- ---shyConcenlrarion
IloSlfllmem X Concanrated Etracr Volllrne Dilution L Value ~__~ Sample Amoun X Factor
Page 2 of 2
Page 96 of344
-
II-IO-UUC Uflpm rrom-cr 111pound I +5056060864 T-782 P013013 F-443
GE~ Inboratories LLe Report Date December 15 2007
SDGNuwber 08-348 Lab Sample ill 198947001
CilelltID REZT-Ol-S893
)llltch fI) 10954l
RunDllte 1211412007 0149
Prep Date 121102007 1953
DlItli FIle 049f4901d
049b49111d
CAS No Fucmname --shy
12674-Il-2 Aruclor-l 0 16
11104-28-2 Arocior-1221
11141-16-5 AroelOr- 1232
53469-21-9 Aroclor-1242
12672-29-6 Aroclor-1248
11097-69-1 Aroclor-1254
11096-81-5 Aroclor-1260
PCB Certifieate of Analysts
Sample Summary
Date Collected 1210512007 1200
Dute Received 120712007 0930 Client LANL008
Method SW84ti8082
In8t EC02Al
Analyst JXM Aliquot 29911 Column lCLPl
2CLP2
Quulitiec Result l1nits ------ U 373 Ij1kg
U 373 uglkg
U 373 ujlkg
U 373 uglkg
U 373 u1kg
950 uglkg
690 uglkg
Page I of 1
Ma[th S
Moistllre 103 Project LANLOO800 SOPRlf GL-oA-E-040 Dilution 1
Inj Vol luI binlll Volume ImL
Level LOW
MDLtrOD PQt1OQ Column shy
124 373
124 373
124 373
124 373
24 373
124 373 2
124 373
Page 232 of 344
-
F-443+5056060864 T-782 P003Jan-15-200B 04 25pm From-EP TA21 ~- lage 1 ot
SAMPLE COLLECTION LOGFIELD CHAIN OF CUSTODY EVENT ID 134 EVENT NAME 21-024(k) Dp Aggregate
SAMPLE ID RE21-07-3893
ASfLANNED AIPLANNRD AS COLIReTED
J1PDATE COLLECTED(MMIDYYYy) M)J)[A ~ 0(11)1 OxIfTgt ~ ~~O=-h-~~~-------TlME COLLECTED (H1lMM) SOBmiddotMEDIA
rTct f shyPRS W SAMlLE ftea CODE ampa-- 7(7(07 1-1amp LoeATION 11) =L--~=-=-=---__ FIELD QC TYPE tvf- ) f LOCATlON TIPE GENERlq F~Ll)~fREP amp I TOP DEP1R f~IrII~Jj ----L~-~-- SAMPilEUSAGE lliL Jshy
~IKI]6~7
--------- shyBOTIOM nEPTH fIkrnb3 (07 SCREENiPORT DESC fif FIELDMA1rux ~~ B _____ EXCAVATED YESamp-N-A~---f-~------~----
COMPOSITll TYPE COMPOSITli TIME INTERVAL - WATER FLOWING YEStsectPNA
BOREHOLpound YESampNA BOREHOLED1lCL[NATION ___~__ BOREliOLEDlRECTION ______
=L-2=--~__
PRIORI1y ORDER CNTNR PRESERVATIVE COLLECTED SPECIAL INSTRUCTIONS YIN
2 8082 125 ML GLASS Ice y 2 8290 125 ML GLASS Ice ry I NMED
Explosives list ~MBERGLASS ~ rIhln
Ice y JAMPfEDESC
b ro -r~Pf-
FIELD SCREENINGIlVIEASUREMENT RESULTS shy
pro - 0 c 10 COU-E~D BY (P~ REVIEWED BY (PRINT) ~4-u 1 Jh-t- ~-( 6 bull ~~ 11 L ~ID
RECEIVED BYDateTime DatefTimeRELINQUISHED BY P107(Printed Name) 7110(printed Name) ~~
-(SIgnature) shy(Signature)~~ t)i16CXgt RECEIVED BYDatelTlmoHELINQUISHED BY DateTime
(Printed Name)(Printed Name)
(Signature)Signature)) -
r--
l
Sample]]) RE21-07-3893
(Jie-nt Data
Narue Los Alamos National Laboratory Prajcct 07-294C Dale Collected 17-Jul-07 Tirol Collecied 1415 ~
Analyle Cone (pglg) DL a
2378-TCDD ND 00757
1)378-PeCDD ND 0101
J)3478-HxCDD ND 0370
123678-HxCDD ND 0413
123789-HxCDD 0367
123467S-HpCDD 863
OCDD 52~1
237Jl-TCDF 0]54
12378-PeCDF ND 23478middotPeCDF ND
123478-HxCDF 0301
123678-HxCDF 0207
234678-HxCDF 0229
123789-HxCDF ND 0174
1234678-HpCDF 357
1234789-HpCDF ND 0286
OCDF amp80
Toblls
TolalTCDD ND 00757
TolaIPeCDD middotm 0118
Total HxCDD 254
Total HpCDD 159
Total TCDF 0)78
TotalPeCDF 0729 Total HxCDF 320
Iotal HpCDF 658 ~
Analysi RAS
Project 29211
SUD pTe Data
Matrix Soil Sample SUe 100 g Solids 995
EM PCb Qualifiers
J
J 0136
0128
J J j
0993
EPA Metbod 8290
UibonliOn Data
Lab Sample 29211~OOJ Date Reoeived 19-Jul)7 QC Bald N(l 9210 Date Extracted 25middotulmiddot07 Date A olllyzed DB-S Date Analyzed DJ322S27-Jul-07 NA
Labeled Standard R LCL-UCLd Oualifiers
IS J3C-2378-TCDD 101 40 - 135 13C-I 2378-PeCDD 108 40 - 135
13C-l2347S-HxCDD 109 40-135 BCmiddotl 2367amp-HxCDD 895 40 - 135
I3C-12346 78-HpCDD 100 40 -135
13C-OCDD 795 40middot135 13C-237-TCDF 980 40- 135 13C-1 237amp-PeCDF 106 40- 135
13C-23478-PeCDF 103 40 - 135 Be-123478-HxCDF 114 40 - 135
13C-l23678-HxCDF 892 40 - 135 13C-234678-HxCDF 961 40 - 135
13C-l23789-HxCDF 102 40- [35
13C-I 23467 8middotHpCDF 921 40 - 135 I3C -] 2347 89-HpCDF 110 40 - 135 13CmiddotOCDF 840 40 - 135
CRS 37Cl2378-TCDD 908 40-135 eToxic EquhalcDt Quotien1 (TE-Q) Data
TEQ(Min) 0309
II Sample spaific eslimated detalOO IUn ii
b EStirowted mruciIDWll possi hie oollCWlJati01l
( Melhod detalionlirniL
d WVIeT centroT limil- upper oontroJ limit
e TEQ based on (l989) lnfemal100al To~i1 EjuLAlenl Faclors (lTE)
The results are reported In dry weight The sample size is reported in e4 veiBJlt --- -- -shy
APPnJve1 B) WiHlam J Luksernburg Ol-Aug-20070843
ltshy
i en
I rv lt=gt lt=gt CD
lt=gt ~
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P3pounde 6 of25
F-443 Jan-15-200S 0426pm From-EP TA21 Iigt +5056060864 T-782 P00501S ~~v~~~~~~ ~N~ORHA-~~~wNO unauthorized reproduet1on witbout ~~en pe~io1on fr~ Gg~
1_-()~4tt) High Explosives Analysts Data Sheet
Lab Name General Engineering laboratories Client Sample ID RB21-07-3S93
Lab Code GEl GELJobNo(SDG) ~
Matrb ~ GEL Sample ID 189817001
Sample AIIlount 2 Molstue 2
Date Received 19middotJOL07Amount Vnlb S
Extract-bID Type Sonioation Extraction Bakh ID 653048
Copwf1Cl-atea Extract Volumt(mL) 12 Date Extracted 25JUL07
DllutllWlFactorr a InJ~ton Volume (uL) 50
Daee Analyzed02-AUG07 2023 GEL dUII file BXS080a0J16wiff
Untts ugkg______bull _____wow _______
r ----~ ( - Cas No 1 Compound QConcentration
TATB 1000 U3058-38-6 i 2ampDiamino-4-nitrotoluene 200059229-75-3 U
35-Dinitroaniline 1000 U~_ 618-8-1 24jDiamino6-nitrotoluene 2000 U 6629-29-4 tris(ocresyl) phosphate 1000 UCmiddot 78-30~8
I ~Coln~atmtion bull
llnSrrUlDtlt X ConcentrudExtract Volume x Dilution Vahtl Ie Amoun Factor
Page 2 of 2
Page 18 of329
Jan-15-Z00a 0426pm From-EP TAZl +5056060B64 T-7B2 P0060l3 F-443 _v~ ~MV~ middotU unu=aa roproaUat10Jl wlthout 1ft bull ~n pS1lll1allion flOlII GlBL
1 High Explosives Analysis Data Sheet
Lub Name General Engineerillg Laboratories Cllent Sample ID RE21-07-3893
Lab Code GEt GEL Job No (SDG) 07-293
Matrix ~ioIL GEL Sample ID 189817001
Sample AnDllDt a MoisCure ll
Date Received Amount llhl~ g
Extraction Batch ID 653048ExtradlonType ~tion
Coneentrlllted Rxtla~Hfolulne (mL) lQ Date Extracted 25middotJUL-07
DUatlon fictor ~ bUection Volumo (nL) ~
nte Analy2tdr 30-IDL-07 1916GEL dauHlile BXm130015a
Units ugkg
I
I
I
--UasNo 18-96-7
L21-14-2
111-82-4
U~06middot51middot0
~5e1-41-0
31572middot78middot2
9-45-8Ei6-0-2 nmiddotllmiddot5
bull li8middot7zZ 11-95-3
middot1J108-1
I 993$-4
1
~)j65-0
9~J99middot0 - shy -__--_-
C03J]ound 246middotTriIIlitrotoJuene
24-pidrotoluelle
aDX
4-Amino-2ampdinitrotoluene
aMX 2-Amino-4dinitrotoluene
retryl
26-DiDitrotoluene
mTN
o-Nilrololuene
Nitr~enzene
m-Nitratoluene
135-TriniCrobcnzene
m-Dinittobenzene
p-NirrorQuene
Concentration 500
500
500
500
SOO SOO SOO 500
1000
500
i 500
500
500
SOO soo
-~
U
U
U
U
U
U
u I
U -I U
U i
U i U
U
U
~J
Concentrwon =0
Instrument X Concentllllted Bxrract Volumll X Dilution Value Sam~e Amoun Factor
Page 1 of 2
Page 17 of 329
T-782 POO7l013 F-443 $ +5056060864Jan-15-200S 04 26pm From-EP TA2l __r
GEL lAboratQlies LLC Report Dllte AuguSll 2007
PCB Page 1 of 1 Certificate of Analysis
Sample Summary
SDG NUlllber 07-293 Da~ Collected 07171Z0071200 Man-Ix SOIL
Lab Sample ID 189817001 Date Reccied 071l9J200709)0 Moislure 7 Client SlUllple 12 Client LANL006 Project LANLOOGOO ClientID RE2-07-3893 Method SW846)082 SOP Ref CL-OA-E-04ll
Batch ID 653073 lrut ECD2A1 DIlution 1
Run Daoo 0712712007 1258 AnaYBt JXM Inj Vol tIlL lnpDllte 071J320070800 Aliquot 30~ FInal Volume ImL Dab File 014tl401d Column 1 eLFl Level LOW
014b140~d 2CLP2
CAS No Parnmame Qualifler Result Units Ml)ULOD PQULOQ CoIWl1lI
12674-lJ-2 Aroclor-1016 U 336 uglkg Ll2 336
11104-28-2 Aroclor-1221 U 3~6 uglkg 112 336
1114l-16-) Atoclor-1232 U 336 lIglkg 112 336
53469-21-9 Arocor-1242 U 336 Ilglkg LI2 336
12672-29-lt ArocIOr-l24amp U 336 uSlkg 112 336
1I097-6H Aroclor-12S4 J 120 lIgkg 112 336
11096-82-5 Aroclar-1260 U 336 uglkg 112 336
Page 208 of329
-----
~ 2 ~ o lt0
f
o (N
~ ltll
g 01
-~ - --~
11gt319
21-353 21-485 J I Investigation area
~ Ifor SWMU 21-027(a) j( 4-in floor drain pipe ~ U engineerillg drawing location) I
f r I ~~ ~12~n storm drarfl cemeflt culvert _lturveyecl location)
J I I
_I I I J
I J J shylI
I -~
-
cJ Slructu ra
l- I Former slructure
Jilvestigalion area
bull Proposed sample toeation
reg Prop()Sed borehole location amp Previous sample localirm euroI Previous bOfehole localion
Pipeline (surveyed location)
Pjpeline (enQineering drawjng localion)
Road
Fenoe 10-fl c1I110Uf
0 40 80
FEET 19113 HAl) t
bull 7rlltJ bull
- _shy
- ~ ~ 7050---middot
- -------- -~--~-
-
-- ~-~
- -~ --~ --- ~ - -- - -~~t= _
- - - --~~~
r050- _15 - -~- -- - - -~
---- ~ -~- _--_ -
- ~ ~--~~ -- ~ ----- -----~-i~ ~~-~ shy ~ - ~ ~
Slu1s GISLab tA201224 061 4ll4 mgtflfied far F5193 IlPwai sile 1l3D1igt5 plrn
Figure 519-3 SWMU 21-027(a) proposed sample locations
tI ll (()
ft ) ltc co ~ (0 fIl iii p a IJ)
s ~ ~ IJ)
amp 3
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~
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___
Jilil-IO-UUO U4QPm rrum-tr IA +bUb1i060664 T-78Z P009013 F-443 LU~ fllUllU~ rl~110nal Luoorarory Page I or
SAMPLE COLLECTION LOGFIELD CHAIN OF CUSTODY EVENT ID 198 EVENT NAME CU21-027(a) DP Site Summer]a1l2007
) SAMPLE ID RE21-07-SS93
ASPLANNtP
DATE COLLECfED(MMlDDIVYYV)
TIME COLLECTED (HlIMM)
PRS ID ZHIZ(JI
LOCATIONm ~~11u1 LOCATION TYPE GENpoundRlC
~~v
TOP DEPTH-fIljrid 7
BonOM DEPTH -r i01 FIElJlMTR1X --5- ~~~I
i ~( ~()T COMPOSITETVPpound --
ASCQLLECTpoundll
2 ftro 7
u C bull 2( o h
R- II01d-2S lei( 4b
4 0 ft- 4 0 f 1shy
bull (
MEDIA
SUBmiddotli--shy~w
SAMPLE TECH CODE
FIELD QCTVPE
FIELD PREP
SAMlLtlJSAGE
SCREENIlOlU DESC
AS PLANNED rev
~ lJhlt77
W 11 rJ
~ 1)
amp
amp
INV
A
ASCQLLECTED
(1 h 1- 3 D tC1 A Cd t
1
tY
EXCAVATED YfSte~N--A----------------Ii
COMPOSITpoundnME1NTERVAL WATER FLOWING YES~NA
BOREHOLE YES~A BOREHOLE DECLINATION ___~__ BOREHOLE DIRECTION shy
PRIOnlTY ORD~R CNTNR PRESERVATIVE COLLECTED YIN
SPECIAL INSTRUCTIONS
2
2
1
8082
8290
NMED Explosives list
125MLGLASS
125MLGLASS
250 l1L AMBER GLASS
_ _-_ _shy
Ice
Ice
Ice
V y
L _____ --_ )SAMPLE DESC t Quck I uGrvi- 15~ Gr~v TIImiddotH
SAMPLE COMMENTS
LOCATIONDESC Y-1lt~tLev ~k
shy
~c~~ 4(0 ]n Ie r fr-Dt71 (one) 113 ~r~ 1110 CIir
FIELD SCREENINGIMEASUREMENT RESULTS flO bf-c ygtY1rxi- 0 -0 r31r
f ~ I rf olcJ1f p j tJ~ Ot p17d 7-tdfM
REVIEWED BY (PRINT ___________COLLECT~DBY (pRINT) _ __---Vi shyr shy -
DateffilneDateffime RECEIVED BYRELINQUISHED BY I070 r (Printed Name)
(Signature)
(Printed Name) )C20(Signature) Jo~~
RECEIVED BY Datetrime
I (Printed Name)
DateITimeRELINQUISHED BY
(Printed N arne)
(Signature)(Signature)
I I
I
I
CL
cYgt
shy
u Sample ill RE21-07-5893 (Q
Client Data = Los Alamoo National Laboratory 0amp-347 S-Dee-07 0830
Samlc Data
Malrix Soil Sample Size t 13 g
middotSolids 894
shycgt
cgt
Name Project Date Collected Time Collected
co I Analyte Cone (pglg) DL a EWCb Qualifierst-
2378-TCDD 12378-PeCDD
l23478-HxCDD
123678-HxCDD
ltJgt CO Cgt 123789-HxCDDUgt cgt lt0 LO
1234678-HpCDD = In + OeDD
2378-TCDF
12378-PeCDF 23478-PeCDF
123478-HxCDF 12367 8-HxC DF
23 467amp-HxCDF
123789middotHxCDF
1234678-HpCDF 1234789-HpCDF
aCDF
Totals
0599 322
63amp
379
16l
1320
15200 0302
0503 L4J
492
382
692
129 [52
142
503
423
279 259 2790
643
276
205
726
435
284
699
J
I J
J B
B
EPA lVlcthod 8290
labontoa Data
Lab Sample 30042~OOl Dare Reeeind 7-Dec-07 QC Batch No 9763 Date ExlIllc[ltd 1O-Dec-07 Dale Analyzed DB-5 13-Dee-07 [)ate Analyzrd DB-225 NA
_shy
Labeled Standard R LeL-UCLd Qualifiers _ shy
IS t3C-2J78-TCDD 898 4) - 13S 13C-[2J7S-PeCDD 916 40 - 135 13C-l23478-HxCDD 935 40- 135 13C-l236 78-HltCD 0 816 40 - 135
lJC-l234678-HpCDD 104shy 40 shy 135 13C-OCDD 122 40 shy l35 13C-2378-TCDF 100 40 - 135 llC-l 2378- PeC DF [04 40- 135 13C-23478-PeCDF 109 40- fJ5 [3C-I2JA78-HKCDF 914 40 - 135
l3C- 123678-HxCDF 792 4() - lJ5 l3C-234678-HxCDP 842 40 shy 135
13C-l23789-HxCDF 9l2 40- 135 [3C-1234678-HpCDF 847 40 shy [35
13C-1234789-HpCDF 991 40 - DS L3C-QCDF 985 40 shy 135
CRS 37Cl-2378-TCDD 936 40 shy 135 eTodc Equivalent Qnotient (fEQ) Data
-lt t-CL UJ
I E o ~
LL
E n
lt0
cgt agt lt=gt cgt
I tn
I c
TotalrCDD
Total PeCDD Total HxCDD Total HpCDD Total TCDF Total PeCDF Total HxCDF
Tota[ HpCDF
Anal~st MAS
P
P
P BP
TEQ(Min) 413
a Sample specific etimated detection j iInil
b Eslilnated maximum possible cQfcenlfatioll
c Method detec1iol1lirniL
d Lo1r~oltrollimil- uppNcolltrollimit
e 7EQ based an (1989) [nternatiooal roxie EquiaIent Filltturs (ITEn
The fltlltl-Wll are repooed in dry weighl The sam pIe size is rej)lJrtild in wltt weight
AwrovedBy Martha M Maier lJ-Dec-2007 1527
T-782 P 011013 F-443Jilll-IO-UUO U4 opm rrom-II III +5056060864
1 High Explosives Analysls Data Sheet
I CalNo 118-96-7
I 121~14-2 Irshy 121-82-4
19406-51-0
2691-41middot0
35572~7g2
479-45-8
606middot20middot2 78-11-5
88-72-2
98-95-3
99-08-1 -~
9935-4
99middot65middot0 f
99w99-0l
Lab Name General Engineering Lahorarcries Client Sample ID RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sample ID 198941001
Moistm-e 103Sample Amount pound
Amoullt Units l Date Received 07~DECmiddot07
Extl8ction Type Sonicatioll Extraction Batch In 709399
COllcenhated Extlllct Volume (UlL) ill Dale Extracted 12middotDEC-07
PllutlOll Facto ~ Injection Volume CuLl ~
Date Analyzed 1H)EC-07 1529GEL (lata tJle EXP12l20S7a
Units ugJkg __ n _
ComJound Concentration -Q]- - 500246-Trinitrotoh Hme 1 U I
~ 24middotDinitrotolu~ene SOD I U
Rl)X 500 I u1 4-Amino-26dinibmiddoto l) illene 500 r-u-
HMX
2-Amino-46-dinitro ojuelle
Tetryl
I 26-Dlllltrotolul~ ~ lUi middot-------~------~----~-----~--t
a
PElN 1000 U wNitrotoluellc
500 ~-1 Nitrobenzen 500 I U
i m-NitrotolUefle SOD I u 135-Tdnitrober zelle 500 I U
ffi-Dinitrobenzi ne 1 500 lUi p-Nitrotoluel1e 500 I U
____ ___-l_____ _ __ ___ L___~ - ~
_ soo U
500 U -i 500 U
-J
-----~~------------ ----- shy Concentration
Instnment X ConcenUllred Extract Volume X Dilutioll Value Samele ArnouD Factor
Page of 2
Page 93 of344
Jan-IO-UU~ U4pm Irom-t IAll +5056060864 T-782 P012013 F-443
1 High Explosives Analysis DII tn Sheet
Lab Name Qeneml Engineering Laboratories Client Sample llgt RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sam)Je lD 198947001
Moisture 103Sample Amount 2
Date Received 07-DEC-07Amount Unitli g
Extmction Type Sonication Extractiou Batch ID 709399
Concentrated Extract Volume (mL) 12 Date Extracted 12-DECmiddot07
Dilution Fact6r Injection Volume (uL) 50
Date Analyzed 17middotDECmiddot07 1903 GEL data file EXS12 17035wiff
Units ugkg
Cas No 3058middot386
59229-7S-3
Compound TATB
26-Diminc-4-nitI
- shy --- Concentnnkm -~T-0-1 1000 -~
2000 1u 618middot87-1 3SmiddotDinitroaniIinc 1000 U
6629--29-4
78-30-8
24Dlamlno-6-iroii~n-trls(o-cresyl) phosphate _~___~ bull -
- ] 2000 U bull
1000 U -1I __bullbull_ bullbullbull___ ~_________ I--_~ I
-~-------- ---shyConcenlrarion
IloSlfllmem X Concanrated Etracr Volllrne Dilution L Value ~__~ Sample Amoun X Factor
Page 2 of 2
Page 96 of344
-
II-IO-UUC Uflpm rrom-cr 111pound I +5056060864 T-782 P013013 F-443
GE~ Inboratories LLe Report Date December 15 2007
SDGNuwber 08-348 Lab Sample ill 198947001
CilelltID REZT-Ol-S893
)llltch fI) 10954l
RunDllte 1211412007 0149
Prep Date 121102007 1953
DlItli FIle 049f4901d
049b49111d
CAS No Fucmname --shy
12674-Il-2 Aruclor-l 0 16
11104-28-2 Arocior-1221
11141-16-5 AroelOr- 1232
53469-21-9 Aroclor-1242
12672-29-6 Aroclor-1248
11097-69-1 Aroclor-1254
11096-81-5 Aroclor-1260
PCB Certifieate of Analysts
Sample Summary
Date Collected 1210512007 1200
Dute Received 120712007 0930 Client LANL008
Method SW84ti8082
In8t EC02Al
Analyst JXM Aliquot 29911 Column lCLPl
2CLP2
Quulitiec Result l1nits ------ U 373 Ij1kg
U 373 uglkg
U 373 ujlkg
U 373 uglkg
U 373 u1kg
950 uglkg
690 uglkg
Page I of 1
Ma[th S
Moistllre 103 Project LANLOO800 SOPRlf GL-oA-E-040 Dilution 1
Inj Vol luI binlll Volume ImL
Level LOW
MDLtrOD PQt1OQ Column shy
124 373
124 373
124 373
124 373
24 373
124 373 2
124 373
Page 232 of 344
-
Sample]]) RE21-07-3893
(Jie-nt Data
Narue Los Alamos National Laboratory Prajcct 07-294C Dale Collected 17-Jul-07 Tirol Collecied 1415 ~
Analyle Cone (pglg) DL a
2378-TCDD ND 00757
1)378-PeCDD ND 0101
J)3478-HxCDD ND 0370
123678-HxCDD ND 0413
123789-HxCDD 0367
123467S-HpCDD 863
OCDD 52~1
237Jl-TCDF 0]54
12378-PeCDF ND 23478middotPeCDF ND
123478-HxCDF 0301
123678-HxCDF 0207
234678-HxCDF 0229
123789-HxCDF ND 0174
1234678-HpCDF 357
1234789-HpCDF ND 0286
OCDF amp80
Toblls
TolalTCDD ND 00757
TolaIPeCDD middotm 0118
Total HxCDD 254
Total HpCDD 159
Total TCDF 0)78
TotalPeCDF 0729 Total HxCDF 320
Iotal HpCDF 658 ~
Analysi RAS
Project 29211
SUD pTe Data
Matrix Soil Sample SUe 100 g Solids 995
EM PCb Qualifiers
J
J 0136
0128
J J j
0993
EPA Metbod 8290
UibonliOn Data
Lab Sample 29211~OOJ Date Reoeived 19-Jul)7 QC Bald N(l 9210 Date Extracted 25middotulmiddot07 Date A olllyzed DB-S Date Analyzed DJ322S27-Jul-07 NA
Labeled Standard R LCL-UCLd Oualifiers
IS J3C-2378-TCDD 101 40 - 135 13C-I 2378-PeCDD 108 40 - 135
13C-l2347S-HxCDD 109 40-135 BCmiddotl 2367amp-HxCDD 895 40 - 135
I3C-12346 78-HpCDD 100 40 -135
13C-OCDD 795 40middot135 13C-237-TCDF 980 40- 135 13C-1 237amp-PeCDF 106 40- 135
13C-23478-PeCDF 103 40 - 135 Be-123478-HxCDF 114 40 - 135
13C-l23678-HxCDF 892 40 - 135 13C-234678-HxCDF 961 40 - 135
13C-l23789-HxCDF 102 40- [35
13C-I 23467 8middotHpCDF 921 40 - 135 I3C -] 2347 89-HpCDF 110 40 - 135 13CmiddotOCDF 840 40 - 135
CRS 37Cl2378-TCDD 908 40-135 eToxic EquhalcDt Quotien1 (TE-Q) Data
TEQ(Min) 0309
II Sample spaific eslimated detalOO IUn ii
b EStirowted mruciIDWll possi hie oollCWlJati01l
( Melhod detalionlirniL
d WVIeT centroT limil- upper oontroJ limit
e TEQ based on (l989) lnfemal100al To~i1 EjuLAlenl Faclors (lTE)
The results are reported In dry weight The sample size is reported in e4 veiBJlt --- -- -shy
APPnJve1 B) WiHlam J Luksernburg Ol-Aug-20070843
ltshy
i en
I rv lt=gt lt=gt CD
lt=gt ~
en T5 3
a 3 I
rn -0
-I po
+ UI lt=gt U1 0)
cgt 0)
cgt co agt ~
-I I-
co -0
cgt cgt ~
shycgt
I ~ ~
P3pounde 6 of25
F-443 Jan-15-200S 0426pm From-EP TA21 Iigt +5056060864 T-782 P00501S ~~v~~~~~~ ~N~ORHA-~~~wNO unauthorized reproduet1on witbout ~~en pe~io1on fr~ Gg~
1_-()~4tt) High Explosives Analysts Data Sheet
Lab Name General Engineering laboratories Client Sample ID RB21-07-3S93
Lab Code GEl GELJobNo(SDG) ~
Matrb ~ GEL Sample ID 189817001
Sample AIIlount 2 Molstue 2
Date Received 19middotJOL07Amount Vnlb S
Extract-bID Type Sonioation Extraction Bakh ID 653048
Copwf1Cl-atea Extract Volumt(mL) 12 Date Extracted 25JUL07
DllutllWlFactorr a InJ~ton Volume (uL) 50
Daee Analyzed02-AUG07 2023 GEL dUII file BXS080a0J16wiff
Untts ugkg______bull _____wow _______
r ----~ ( - Cas No 1 Compound QConcentration
TATB 1000 U3058-38-6 i 2ampDiamino-4-nitrotoluene 200059229-75-3 U
35-Dinitroaniline 1000 U~_ 618-8-1 24jDiamino6-nitrotoluene 2000 U 6629-29-4 tris(ocresyl) phosphate 1000 UCmiddot 78-30~8
I ~Coln~atmtion bull
llnSrrUlDtlt X ConcentrudExtract Volume x Dilution Vahtl Ie Amoun Factor
Page 2 of 2
Page 18 of329
Jan-15-Z00a 0426pm From-EP TAZl +5056060B64 T-7B2 P0060l3 F-443 _v~ ~MV~ middotU unu=aa roproaUat10Jl wlthout 1ft bull ~n pS1lll1allion flOlII GlBL
1 High Explosives Analysis Data Sheet
Lub Name General Engineerillg Laboratories Cllent Sample ID RE21-07-3893
Lab Code GEt GEL Job No (SDG) 07-293
Matrix ~ioIL GEL Sample ID 189817001
Sample AnDllDt a MoisCure ll
Date Received Amount llhl~ g
Extraction Batch ID 653048ExtradlonType ~tion
Coneentrlllted Rxtla~Hfolulne (mL) lQ Date Extracted 25middotJUL-07
DUatlon fictor ~ bUection Volumo (nL) ~
nte Analy2tdr 30-IDL-07 1916GEL dauHlile BXm130015a
Units ugkg
I
I
I
--UasNo 18-96-7
L21-14-2
111-82-4
U~06middot51middot0
~5e1-41-0
31572middot78middot2
9-45-8Ei6-0-2 nmiddotllmiddot5
bull li8middot7zZ 11-95-3
middot1J108-1
I 993$-4
1
~)j65-0
9~J99middot0 - shy -__--_-
C03J]ound 246middotTriIIlitrotoJuene
24-pidrotoluelle
aDX
4-Amino-2ampdinitrotoluene
aMX 2-Amino-4dinitrotoluene
retryl
26-DiDitrotoluene
mTN
o-Nilrololuene
Nitr~enzene
m-Nitratoluene
135-TriniCrobcnzene
m-Dinittobenzene
p-NirrorQuene
Concentration 500
500
500
500
SOO SOO SOO 500
1000
500
i 500
500
500
SOO soo
-~
U
U
U
U
U
U
u I
U -I U
U i
U i U
U
U
~J
Concentrwon =0
Instrument X Concentllllted Bxrract Volumll X Dilution Value Sam~e Amoun Factor
Page 1 of 2
Page 17 of 329
T-782 POO7l013 F-443 $ +5056060864Jan-15-200S 04 26pm From-EP TA2l __r
GEL lAboratQlies LLC Report Dllte AuguSll 2007
PCB Page 1 of 1 Certificate of Analysis
Sample Summary
SDG NUlllber 07-293 Da~ Collected 07171Z0071200 Man-Ix SOIL
Lab Sample ID 189817001 Date Reccied 071l9J200709)0 Moislure 7 Client SlUllple 12 Client LANL006 Project LANLOOGOO ClientID RE2-07-3893 Method SW846)082 SOP Ref CL-OA-E-04ll
Batch ID 653073 lrut ECD2A1 DIlution 1
Run Daoo 0712712007 1258 AnaYBt JXM Inj Vol tIlL lnpDllte 071J320070800 Aliquot 30~ FInal Volume ImL Dab File 014tl401d Column 1 eLFl Level LOW
014b140~d 2CLP2
CAS No Parnmame Qualifler Result Units Ml)ULOD PQULOQ CoIWl1lI
12674-lJ-2 Aroclor-1016 U 336 uglkg Ll2 336
11104-28-2 Aroclor-1221 U 3~6 uglkg 112 336
1114l-16-) Atoclor-1232 U 336 lIglkg 112 336
53469-21-9 Arocor-1242 U 336 Ilglkg LI2 336
12672-29-lt ArocIOr-l24amp U 336 uSlkg 112 336
1I097-6H Aroclor-12S4 J 120 lIgkg 112 336
11096-82-5 Aroclar-1260 U 336 uglkg 112 336
Page 208 of329
-----
~ 2 ~ o lt0
f
o (N
~ ltll
g 01
-~ - --~
11gt319
21-353 21-485 J I Investigation area
~ Ifor SWMU 21-027(a) j( 4-in floor drain pipe ~ U engineerillg drawing location) I
f r I ~~ ~12~n storm drarfl cemeflt culvert _lturveyecl location)
J I I
_I I I J
I J J shylI
I -~
-
cJ Slructu ra
l- I Former slructure
Jilvestigalion area
bull Proposed sample toeation
reg Prop()Sed borehole location amp Previous sample localirm euroI Previous bOfehole localion
Pipeline (surveyed location)
Pjpeline (enQineering drawjng localion)
Road
Fenoe 10-fl c1I110Uf
0 40 80
FEET 19113 HAl) t
bull 7rlltJ bull
- _shy
- ~ ~ 7050---middot
- -------- -~--~-
-
-- ~-~
- -~ --~ --- ~ - -- - -~~t= _
- - - --~~~
r050- _15 - -~- -- - - -~
---- ~ -~- _--_ -
- ~ ~--~~ -- ~ ----- -----~-i~ ~~-~ shy ~ - ~ ~
Slu1s GISLab tA201224 061 4ll4 mgtflfied far F5193 IlPwai sile 1l3D1igt5 plrn
Figure 519-3 SWMU 21-027(a) proposed sample locations
tI ll (()
ft ) ltc co ~ (0 fIl iii p a IJ)
s ~ ~ IJ)
amp 3
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L
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Jilil-IO-UUO U4QPm rrum-tr IA +bUb1i060664 T-78Z P009013 F-443 LU~ fllUllU~ rl~110nal Luoorarory Page I or
SAMPLE COLLECTION LOGFIELD CHAIN OF CUSTODY EVENT ID 198 EVENT NAME CU21-027(a) DP Site Summer]a1l2007
) SAMPLE ID RE21-07-SS93
ASPLANNtP
DATE COLLECfED(MMlDDIVYYV)
TIME COLLECTED (HlIMM)
PRS ID ZHIZ(JI
LOCATIONm ~~11u1 LOCATION TYPE GENpoundRlC
~~v
TOP DEPTH-fIljrid 7
BonOM DEPTH -r i01 FIElJlMTR1X --5- ~~~I
i ~( ~()T COMPOSITETVPpound --
ASCQLLECTpoundll
2 ftro 7
u C bull 2( o h
R- II01d-2S lei( 4b
4 0 ft- 4 0 f 1shy
bull (
MEDIA
SUBmiddotli--shy~w
SAMPLE TECH CODE
FIELD QCTVPE
FIELD PREP
SAMlLtlJSAGE
SCREENIlOlU DESC
AS PLANNED rev
~ lJhlt77
W 11 rJ
~ 1)
amp
amp
INV
A
ASCQLLECTED
(1 h 1- 3 D tC1 A Cd t
1
tY
EXCAVATED YfSte~N--A----------------Ii
COMPOSITpoundnME1NTERVAL WATER FLOWING YES~NA
BOREHOLE YES~A BOREHOLE DECLINATION ___~__ BOREHOLE DIRECTION shy
PRIOnlTY ORD~R CNTNR PRESERVATIVE COLLECTED YIN
SPECIAL INSTRUCTIONS
2
2
1
8082
8290
NMED Explosives list
125MLGLASS
125MLGLASS
250 l1L AMBER GLASS
_ _-_ _shy
Ice
Ice
Ice
V y
L _____ --_ )SAMPLE DESC t Quck I uGrvi- 15~ Gr~v TIImiddotH
SAMPLE COMMENTS
LOCATIONDESC Y-1lt~tLev ~k
shy
~c~~ 4(0 ]n Ie r fr-Dt71 (one) 113 ~r~ 1110 CIir
FIELD SCREENINGIMEASUREMENT RESULTS flO bf-c ygtY1rxi- 0 -0 r31r
f ~ I rf olcJ1f p j tJ~ Ot p17d 7-tdfM
REVIEWED BY (PRINT ___________COLLECT~DBY (pRINT) _ __---Vi shyr shy -
DateffilneDateffime RECEIVED BYRELINQUISHED BY I070 r (Printed Name)
(Signature)
(Printed Name) )C20(Signature) Jo~~
RECEIVED BY Datetrime
I (Printed Name)
DateITimeRELINQUISHED BY
(Printed N arne)
(Signature)(Signature)
I I
I
I
CL
cYgt
shy
u Sample ill RE21-07-5893 (Q
Client Data = Los Alamoo National Laboratory 0amp-347 S-Dee-07 0830
Samlc Data
Malrix Soil Sample Size t 13 g
middotSolids 894
shycgt
cgt
Name Project Date Collected Time Collected
co I Analyte Cone (pglg) DL a EWCb Qualifierst-
2378-TCDD 12378-PeCDD
l23478-HxCDD
123678-HxCDD
ltJgt CO Cgt 123789-HxCDDUgt cgt lt0 LO
1234678-HpCDD = In + OeDD
2378-TCDF
12378-PeCDF 23478-PeCDF
123478-HxCDF 12367 8-HxC DF
23 467amp-HxCDF
123789middotHxCDF
1234678-HpCDF 1234789-HpCDF
aCDF
Totals
0599 322
63amp
379
16l
1320
15200 0302
0503 L4J
492
382
692
129 [52
142
503
423
279 259 2790
643
276
205
726
435
284
699
J
I J
J B
B
EPA lVlcthod 8290
labontoa Data
Lab Sample 30042~OOl Dare Reeeind 7-Dec-07 QC Batch No 9763 Date ExlIllc[ltd 1O-Dec-07 Dale Analyzed DB-5 13-Dee-07 [)ate Analyzrd DB-225 NA
_shy
Labeled Standard R LeL-UCLd Qualifiers _ shy
IS t3C-2J78-TCDD 898 4) - 13S 13C-[2J7S-PeCDD 916 40 - 135 13C-l23478-HxCDD 935 40- 135 13C-l236 78-HltCD 0 816 40 - 135
lJC-l234678-HpCDD 104shy 40 shy 135 13C-OCDD 122 40 shy l35 13C-2378-TCDF 100 40 - 135 llC-l 2378- PeC DF [04 40- 135 13C-23478-PeCDF 109 40- fJ5 [3C-I2JA78-HKCDF 914 40 - 135
l3C- 123678-HxCDF 792 4() - lJ5 l3C-234678-HxCDP 842 40 shy 135
13C-l23789-HxCDF 9l2 40- 135 [3C-1234678-HpCDF 847 40 shy [35
13C-1234789-HpCDF 991 40 - DS L3C-QCDF 985 40 shy 135
CRS 37Cl-2378-TCDD 936 40 shy 135 eTodc Equivalent Qnotient (fEQ) Data
-lt t-CL UJ
I E o ~
LL
E n
lt0
cgt agt lt=gt cgt
I tn
I c
TotalrCDD
Total PeCDD Total HxCDD Total HpCDD Total TCDF Total PeCDF Total HxCDF
Tota[ HpCDF
Anal~st MAS
P
P
P BP
TEQ(Min) 413
a Sample specific etimated detection j iInil
b Eslilnated maximum possible cQfcenlfatioll
c Method detec1iol1lirniL
d Lo1r~oltrollimil- uppNcolltrollimit
e 7EQ based an (1989) [nternatiooal roxie EquiaIent Filltturs (ITEn
The fltlltl-Wll are repooed in dry weighl The sam pIe size is rej)lJrtild in wltt weight
AwrovedBy Martha M Maier lJ-Dec-2007 1527
T-782 P 011013 F-443Jilll-IO-UUO U4 opm rrom-II III +5056060864
1 High Explosives Analysls Data Sheet
I CalNo 118-96-7
I 121~14-2 Irshy 121-82-4
19406-51-0
2691-41middot0
35572~7g2
479-45-8
606middot20middot2 78-11-5
88-72-2
98-95-3
99-08-1 -~
9935-4
99middot65middot0 f
99w99-0l
Lab Name General Engineering Lahorarcries Client Sample ID RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sample ID 198941001
Moistm-e 103Sample Amount pound
Amoullt Units l Date Received 07~DECmiddot07
Extl8ction Type Sonicatioll Extraction Batch In 709399
COllcenhated Extlllct Volume (UlL) ill Dale Extracted 12middotDEC-07
PllutlOll Facto ~ Injection Volume CuLl ~
Date Analyzed 1H)EC-07 1529GEL (lata tJle EXP12l20S7a
Units ugJkg __ n _
ComJound Concentration -Q]- - 500246-Trinitrotoh Hme 1 U I
~ 24middotDinitrotolu~ene SOD I U
Rl)X 500 I u1 4-Amino-26dinibmiddoto l) illene 500 r-u-
HMX
2-Amino-46-dinitro ojuelle
Tetryl
I 26-Dlllltrotolul~ ~ lUi middot-------~------~----~-----~--t
a
PElN 1000 U wNitrotoluellc
500 ~-1 Nitrobenzen 500 I U
i m-NitrotolUefle SOD I u 135-Tdnitrober zelle 500 I U
ffi-Dinitrobenzi ne 1 500 lUi p-Nitrotoluel1e 500 I U
____ ___-l_____ _ __ ___ L___~ - ~
_ soo U
500 U -i 500 U
-J
-----~~------------ ----- shy Concentration
Instnment X ConcenUllred Extract Volume X Dilutioll Value Samele ArnouD Factor
Page of 2
Page 93 of344
Jan-IO-UU~ U4pm Irom-t IAll +5056060864 T-782 P012013 F-443
1 High Explosives Analysis DII tn Sheet
Lab Name Qeneml Engineering Laboratories Client Sample llgt RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sam)Je lD 198947001
Moisture 103Sample Amount 2
Date Received 07-DEC-07Amount Unitli g
Extmction Type Sonication Extractiou Batch ID 709399
Concentrated Extract Volume (mL) 12 Date Extracted 12-DECmiddot07
Dilution Fact6r Injection Volume (uL) 50
Date Analyzed 17middotDECmiddot07 1903 GEL data file EXS12 17035wiff
Units ugkg
Cas No 3058middot386
59229-7S-3
Compound TATB
26-Diminc-4-nitI
- shy --- Concentnnkm -~T-0-1 1000 -~
2000 1u 618middot87-1 3SmiddotDinitroaniIinc 1000 U
6629--29-4
78-30-8
24Dlamlno-6-iroii~n-trls(o-cresyl) phosphate _~___~ bull -
- ] 2000 U bull
1000 U -1I __bullbull_ bullbullbull___ ~_________ I--_~ I
-~-------- ---shyConcenlrarion
IloSlfllmem X Concanrated Etracr Volllrne Dilution L Value ~__~ Sample Amoun X Factor
Page 2 of 2
Page 96 of344
-
II-IO-UUC Uflpm rrom-cr 111pound I +5056060864 T-782 P013013 F-443
GE~ Inboratories LLe Report Date December 15 2007
SDGNuwber 08-348 Lab Sample ill 198947001
CilelltID REZT-Ol-S893
)llltch fI) 10954l
RunDllte 1211412007 0149
Prep Date 121102007 1953
DlItli FIle 049f4901d
049b49111d
CAS No Fucmname --shy
12674-Il-2 Aruclor-l 0 16
11104-28-2 Arocior-1221
11141-16-5 AroelOr- 1232
53469-21-9 Aroclor-1242
12672-29-6 Aroclor-1248
11097-69-1 Aroclor-1254
11096-81-5 Aroclor-1260
PCB Certifieate of Analysts
Sample Summary
Date Collected 1210512007 1200
Dute Received 120712007 0930 Client LANL008
Method SW84ti8082
In8t EC02Al
Analyst JXM Aliquot 29911 Column lCLPl
2CLP2
Quulitiec Result l1nits ------ U 373 Ij1kg
U 373 uglkg
U 373 ujlkg
U 373 uglkg
U 373 u1kg
950 uglkg
690 uglkg
Page I of 1
Ma[th S
Moistllre 103 Project LANLOO800 SOPRlf GL-oA-E-040 Dilution 1
Inj Vol luI binlll Volume ImL
Level LOW
MDLtrOD PQt1OQ Column shy
124 373
124 373
124 373
124 373
24 373
124 373 2
124 373
Page 232 of 344
-
F-443 Jan-15-200S 0426pm From-EP TA21 Iigt +5056060864 T-782 P00501S ~~v~~~~~~ ~N~ORHA-~~~wNO unauthorized reproduet1on witbout ~~en pe~io1on fr~ Gg~
1_-()~4tt) High Explosives Analysts Data Sheet
Lab Name General Engineering laboratories Client Sample ID RB21-07-3S93
Lab Code GEl GELJobNo(SDG) ~
Matrb ~ GEL Sample ID 189817001
Sample AIIlount 2 Molstue 2
Date Received 19middotJOL07Amount Vnlb S
Extract-bID Type Sonioation Extraction Bakh ID 653048
Copwf1Cl-atea Extract Volumt(mL) 12 Date Extracted 25JUL07
DllutllWlFactorr a InJ~ton Volume (uL) 50
Daee Analyzed02-AUG07 2023 GEL dUII file BXS080a0J16wiff
Untts ugkg______bull _____wow _______
r ----~ ( - Cas No 1 Compound QConcentration
TATB 1000 U3058-38-6 i 2ampDiamino-4-nitrotoluene 200059229-75-3 U
35-Dinitroaniline 1000 U~_ 618-8-1 24jDiamino6-nitrotoluene 2000 U 6629-29-4 tris(ocresyl) phosphate 1000 UCmiddot 78-30~8
I ~Coln~atmtion bull
llnSrrUlDtlt X ConcentrudExtract Volume x Dilution Vahtl Ie Amoun Factor
Page 2 of 2
Page 18 of329
Jan-15-Z00a 0426pm From-EP TAZl +5056060B64 T-7B2 P0060l3 F-443 _v~ ~MV~ middotU unu=aa roproaUat10Jl wlthout 1ft bull ~n pS1lll1allion flOlII GlBL
1 High Explosives Analysis Data Sheet
Lub Name General Engineerillg Laboratories Cllent Sample ID RE21-07-3893
Lab Code GEt GEL Job No (SDG) 07-293
Matrix ~ioIL GEL Sample ID 189817001
Sample AnDllDt a MoisCure ll
Date Received Amount llhl~ g
Extraction Batch ID 653048ExtradlonType ~tion
Coneentrlllted Rxtla~Hfolulne (mL) lQ Date Extracted 25middotJUL-07
DUatlon fictor ~ bUection Volumo (nL) ~
nte Analy2tdr 30-IDL-07 1916GEL dauHlile BXm130015a
Units ugkg
I
I
I
--UasNo 18-96-7
L21-14-2
111-82-4
U~06middot51middot0
~5e1-41-0
31572middot78middot2
9-45-8Ei6-0-2 nmiddotllmiddot5
bull li8middot7zZ 11-95-3
middot1J108-1
I 993$-4
1
~)j65-0
9~J99middot0 - shy -__--_-
C03J]ound 246middotTriIIlitrotoJuene
24-pidrotoluelle
aDX
4-Amino-2ampdinitrotoluene
aMX 2-Amino-4dinitrotoluene
retryl
26-DiDitrotoluene
mTN
o-Nilrololuene
Nitr~enzene
m-Nitratoluene
135-TriniCrobcnzene
m-Dinittobenzene
p-NirrorQuene
Concentration 500
500
500
500
SOO SOO SOO 500
1000
500
i 500
500
500
SOO soo
-~
U
U
U
U
U
U
u I
U -I U
U i
U i U
U
U
~J
Concentrwon =0
Instrument X Concentllllted Bxrract Volumll X Dilution Value Sam~e Amoun Factor
Page 1 of 2
Page 17 of 329
T-782 POO7l013 F-443 $ +5056060864Jan-15-200S 04 26pm From-EP TA2l __r
GEL lAboratQlies LLC Report Dllte AuguSll 2007
PCB Page 1 of 1 Certificate of Analysis
Sample Summary
SDG NUlllber 07-293 Da~ Collected 07171Z0071200 Man-Ix SOIL
Lab Sample ID 189817001 Date Reccied 071l9J200709)0 Moislure 7 Client SlUllple 12 Client LANL006 Project LANLOOGOO ClientID RE2-07-3893 Method SW846)082 SOP Ref CL-OA-E-04ll
Batch ID 653073 lrut ECD2A1 DIlution 1
Run Daoo 0712712007 1258 AnaYBt JXM Inj Vol tIlL lnpDllte 071J320070800 Aliquot 30~ FInal Volume ImL Dab File 014tl401d Column 1 eLFl Level LOW
014b140~d 2CLP2
CAS No Parnmame Qualifler Result Units Ml)ULOD PQULOQ CoIWl1lI
12674-lJ-2 Aroclor-1016 U 336 uglkg Ll2 336
11104-28-2 Aroclor-1221 U 3~6 uglkg 112 336
1114l-16-) Atoclor-1232 U 336 lIglkg 112 336
53469-21-9 Arocor-1242 U 336 Ilglkg LI2 336
12672-29-lt ArocIOr-l24amp U 336 uSlkg 112 336
1I097-6H Aroclor-12S4 J 120 lIgkg 112 336
11096-82-5 Aroclar-1260 U 336 uglkg 112 336
Page 208 of329
-----
~ 2 ~ o lt0
f
o (N
~ ltll
g 01
-~ - --~
11gt319
21-353 21-485 J I Investigation area
~ Ifor SWMU 21-027(a) j( 4-in floor drain pipe ~ U engineerillg drawing location) I
f r I ~~ ~12~n storm drarfl cemeflt culvert _lturveyecl location)
J I I
_I I I J
I J J shylI
I -~
-
cJ Slructu ra
l- I Former slructure
Jilvestigalion area
bull Proposed sample toeation
reg Prop()Sed borehole location amp Previous sample localirm euroI Previous bOfehole localion
Pipeline (surveyed location)
Pjpeline (enQineering drawjng localion)
Road
Fenoe 10-fl c1I110Uf
0 40 80
FEET 19113 HAl) t
bull 7rlltJ bull
- _shy
- ~ ~ 7050---middot
- -------- -~--~-
-
-- ~-~
- -~ --~ --- ~ - -- - -~~t= _
- - - --~~~
r050- _15 - -~- -- - - -~
---- ~ -~- _--_ -
- ~ ~--~~ -- ~ ----- -----~-i~ ~~-~ shy ~ - ~ ~
Slu1s GISLab tA201224 061 4ll4 mgtflfied far F5193 IlPwai sile 1l3D1igt5 plrn
Figure 519-3 SWMU 21-027(a) proposed sample locations
tI ll (()
ft ) ltc co ~ (0 fIl iii p a IJ)
s ~ ~ IJ)
amp 3
~ ~ J1)J
L
-
I c c 0
c jgt
0 = C 5 I
~
+ UI c UI en cl
cl jo
-4
-I ltXl
C
= = ltXl- = cJ
-n I
___
Jilil-IO-UUO U4QPm rrum-tr IA +bUb1i060664 T-78Z P009013 F-443 LU~ fllUllU~ rl~110nal Luoorarory Page I or
SAMPLE COLLECTION LOGFIELD CHAIN OF CUSTODY EVENT ID 198 EVENT NAME CU21-027(a) DP Site Summer]a1l2007
) SAMPLE ID RE21-07-SS93
ASPLANNtP
DATE COLLECfED(MMlDDIVYYV)
TIME COLLECTED (HlIMM)
PRS ID ZHIZ(JI
LOCATIONm ~~11u1 LOCATION TYPE GENpoundRlC
~~v
TOP DEPTH-fIljrid 7
BonOM DEPTH -r i01 FIElJlMTR1X --5- ~~~I
i ~( ~()T COMPOSITETVPpound --
ASCQLLECTpoundll
2 ftro 7
u C bull 2( o h
R- II01d-2S lei( 4b
4 0 ft- 4 0 f 1shy
bull (
MEDIA
SUBmiddotli--shy~w
SAMPLE TECH CODE
FIELD QCTVPE
FIELD PREP
SAMlLtlJSAGE
SCREENIlOlU DESC
AS PLANNED rev
~ lJhlt77
W 11 rJ
~ 1)
amp
amp
INV
A
ASCQLLECTED
(1 h 1- 3 D tC1 A Cd t
1
tY
EXCAVATED YfSte~N--A----------------Ii
COMPOSITpoundnME1NTERVAL WATER FLOWING YES~NA
BOREHOLE YES~A BOREHOLE DECLINATION ___~__ BOREHOLE DIRECTION shy
PRIOnlTY ORD~R CNTNR PRESERVATIVE COLLECTED YIN
SPECIAL INSTRUCTIONS
2
2
1
8082
8290
NMED Explosives list
125MLGLASS
125MLGLASS
250 l1L AMBER GLASS
_ _-_ _shy
Ice
Ice
Ice
V y
L _____ --_ )SAMPLE DESC t Quck I uGrvi- 15~ Gr~v TIImiddotH
SAMPLE COMMENTS
LOCATIONDESC Y-1lt~tLev ~k
shy
~c~~ 4(0 ]n Ie r fr-Dt71 (one) 113 ~r~ 1110 CIir
FIELD SCREENINGIMEASUREMENT RESULTS flO bf-c ygtY1rxi- 0 -0 r31r
f ~ I rf olcJ1f p j tJ~ Ot p17d 7-tdfM
REVIEWED BY (PRINT ___________COLLECT~DBY (pRINT) _ __---Vi shyr shy -
DateffilneDateffime RECEIVED BYRELINQUISHED BY I070 r (Printed Name)
(Signature)
(Printed Name) )C20(Signature) Jo~~
RECEIVED BY Datetrime
I (Printed Name)
DateITimeRELINQUISHED BY
(Printed N arne)
(Signature)(Signature)
I I
I
I
CL
cYgt
shy
u Sample ill RE21-07-5893 (Q
Client Data = Los Alamoo National Laboratory 0amp-347 S-Dee-07 0830
Samlc Data
Malrix Soil Sample Size t 13 g
middotSolids 894
shycgt
cgt
Name Project Date Collected Time Collected
co I Analyte Cone (pglg) DL a EWCb Qualifierst-
2378-TCDD 12378-PeCDD
l23478-HxCDD
123678-HxCDD
ltJgt CO Cgt 123789-HxCDDUgt cgt lt0 LO
1234678-HpCDD = In + OeDD
2378-TCDF
12378-PeCDF 23478-PeCDF
123478-HxCDF 12367 8-HxC DF
23 467amp-HxCDF
123789middotHxCDF
1234678-HpCDF 1234789-HpCDF
aCDF
Totals
0599 322
63amp
379
16l
1320
15200 0302
0503 L4J
492
382
692
129 [52
142
503
423
279 259 2790
643
276
205
726
435
284
699
J
I J
J B
B
EPA lVlcthod 8290
labontoa Data
Lab Sample 30042~OOl Dare Reeeind 7-Dec-07 QC Batch No 9763 Date ExlIllc[ltd 1O-Dec-07 Dale Analyzed DB-5 13-Dee-07 [)ate Analyzrd DB-225 NA
_shy
Labeled Standard R LeL-UCLd Qualifiers _ shy
IS t3C-2J78-TCDD 898 4) - 13S 13C-[2J7S-PeCDD 916 40 - 135 13C-l23478-HxCDD 935 40- 135 13C-l236 78-HltCD 0 816 40 - 135
lJC-l234678-HpCDD 104shy 40 shy 135 13C-OCDD 122 40 shy l35 13C-2378-TCDF 100 40 - 135 llC-l 2378- PeC DF [04 40- 135 13C-23478-PeCDF 109 40- fJ5 [3C-I2JA78-HKCDF 914 40 - 135
l3C- 123678-HxCDF 792 4() - lJ5 l3C-234678-HxCDP 842 40 shy 135
13C-l23789-HxCDF 9l2 40- 135 [3C-1234678-HpCDF 847 40 shy [35
13C-1234789-HpCDF 991 40 - DS L3C-QCDF 985 40 shy 135
CRS 37Cl-2378-TCDD 936 40 shy 135 eTodc Equivalent Qnotient (fEQ) Data
-lt t-CL UJ
I E o ~
LL
E n
lt0
cgt agt lt=gt cgt
I tn
I c
TotalrCDD
Total PeCDD Total HxCDD Total HpCDD Total TCDF Total PeCDF Total HxCDF
Tota[ HpCDF
Anal~st MAS
P
P
P BP
TEQ(Min) 413
a Sample specific etimated detection j iInil
b Eslilnated maximum possible cQfcenlfatioll
c Method detec1iol1lirniL
d Lo1r~oltrollimil- uppNcolltrollimit
e 7EQ based an (1989) [nternatiooal roxie EquiaIent Filltturs (ITEn
The fltlltl-Wll are repooed in dry weighl The sam pIe size is rej)lJrtild in wltt weight
AwrovedBy Martha M Maier lJ-Dec-2007 1527
T-782 P 011013 F-443Jilll-IO-UUO U4 opm rrom-II III +5056060864
1 High Explosives Analysls Data Sheet
I CalNo 118-96-7
I 121~14-2 Irshy 121-82-4
19406-51-0
2691-41middot0
35572~7g2
479-45-8
606middot20middot2 78-11-5
88-72-2
98-95-3
99-08-1 -~
9935-4
99middot65middot0 f
99w99-0l
Lab Name General Engineering Lahorarcries Client Sample ID RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sample ID 198941001
Moistm-e 103Sample Amount pound
Amoullt Units l Date Received 07~DECmiddot07
Extl8ction Type Sonicatioll Extraction Batch In 709399
COllcenhated Extlllct Volume (UlL) ill Dale Extracted 12middotDEC-07
PllutlOll Facto ~ Injection Volume CuLl ~
Date Analyzed 1H)EC-07 1529GEL (lata tJle EXP12l20S7a
Units ugJkg __ n _
ComJound Concentration -Q]- - 500246-Trinitrotoh Hme 1 U I
~ 24middotDinitrotolu~ene SOD I U
Rl)X 500 I u1 4-Amino-26dinibmiddoto l) illene 500 r-u-
HMX
2-Amino-46-dinitro ojuelle
Tetryl
I 26-Dlllltrotolul~ ~ lUi middot-------~------~----~-----~--t
a
PElN 1000 U wNitrotoluellc
500 ~-1 Nitrobenzen 500 I U
i m-NitrotolUefle SOD I u 135-Tdnitrober zelle 500 I U
ffi-Dinitrobenzi ne 1 500 lUi p-Nitrotoluel1e 500 I U
____ ___-l_____ _ __ ___ L___~ - ~
_ soo U
500 U -i 500 U
-J
-----~~------------ ----- shy Concentration
Instnment X ConcenUllred Extract Volume X Dilutioll Value Samele ArnouD Factor
Page of 2
Page 93 of344
Jan-IO-UU~ U4pm Irom-t IAll +5056060864 T-782 P012013 F-443
1 High Explosives Analysis DII tn Sheet
Lab Name Qeneml Engineering Laboratories Client Sample llgt RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sam)Je lD 198947001
Moisture 103Sample Amount 2
Date Received 07-DEC-07Amount Unitli g
Extmction Type Sonication Extractiou Batch ID 709399
Concentrated Extract Volume (mL) 12 Date Extracted 12-DECmiddot07
Dilution Fact6r Injection Volume (uL) 50
Date Analyzed 17middotDECmiddot07 1903 GEL data file EXS12 17035wiff
Units ugkg
Cas No 3058middot386
59229-7S-3
Compound TATB
26-Diminc-4-nitI
- shy --- Concentnnkm -~T-0-1 1000 -~
2000 1u 618middot87-1 3SmiddotDinitroaniIinc 1000 U
6629--29-4
78-30-8
24Dlamlno-6-iroii~n-trls(o-cresyl) phosphate _~___~ bull -
- ] 2000 U bull
1000 U -1I __bullbull_ bullbullbull___ ~_________ I--_~ I
-~-------- ---shyConcenlrarion
IloSlfllmem X Concanrated Etracr Volllrne Dilution L Value ~__~ Sample Amoun X Factor
Page 2 of 2
Page 96 of344
-
II-IO-UUC Uflpm rrom-cr 111pound I +5056060864 T-782 P013013 F-443
GE~ Inboratories LLe Report Date December 15 2007
SDGNuwber 08-348 Lab Sample ill 198947001
CilelltID REZT-Ol-S893
)llltch fI) 10954l
RunDllte 1211412007 0149
Prep Date 121102007 1953
DlItli FIle 049f4901d
049b49111d
CAS No Fucmname --shy
12674-Il-2 Aruclor-l 0 16
11104-28-2 Arocior-1221
11141-16-5 AroelOr- 1232
53469-21-9 Aroclor-1242
12672-29-6 Aroclor-1248
11097-69-1 Aroclor-1254
11096-81-5 Aroclor-1260
PCB Certifieate of Analysts
Sample Summary
Date Collected 1210512007 1200
Dute Received 120712007 0930 Client LANL008
Method SW84ti8082
In8t EC02Al
Analyst JXM Aliquot 29911 Column lCLPl
2CLP2
Quulitiec Result l1nits ------ U 373 Ij1kg
U 373 uglkg
U 373 ujlkg
U 373 uglkg
U 373 u1kg
950 uglkg
690 uglkg
Page I of 1
Ma[th S
Moistllre 103 Project LANLOO800 SOPRlf GL-oA-E-040 Dilution 1
Inj Vol luI binlll Volume ImL
Level LOW
MDLtrOD PQt1OQ Column shy
124 373
124 373
124 373
124 373
24 373
124 373 2
124 373
Page 232 of 344
-
Jan-15-Z00a 0426pm From-EP TAZl +5056060B64 T-7B2 P0060l3 F-443 _v~ ~MV~ middotU unu=aa roproaUat10Jl wlthout 1ft bull ~n pS1lll1allion flOlII GlBL
1 High Explosives Analysis Data Sheet
Lub Name General Engineerillg Laboratories Cllent Sample ID RE21-07-3893
Lab Code GEt GEL Job No (SDG) 07-293
Matrix ~ioIL GEL Sample ID 189817001
Sample AnDllDt a MoisCure ll
Date Received Amount llhl~ g
Extraction Batch ID 653048ExtradlonType ~tion
Coneentrlllted Rxtla~Hfolulne (mL) lQ Date Extracted 25middotJUL-07
DUatlon fictor ~ bUection Volumo (nL) ~
nte Analy2tdr 30-IDL-07 1916GEL dauHlile BXm130015a
Units ugkg
I
I
I
--UasNo 18-96-7
L21-14-2
111-82-4
U~06middot51middot0
~5e1-41-0
31572middot78middot2
9-45-8Ei6-0-2 nmiddotllmiddot5
bull li8middot7zZ 11-95-3
middot1J108-1
I 993$-4
1
~)j65-0
9~J99middot0 - shy -__--_-
C03J]ound 246middotTriIIlitrotoJuene
24-pidrotoluelle
aDX
4-Amino-2ampdinitrotoluene
aMX 2-Amino-4dinitrotoluene
retryl
26-DiDitrotoluene
mTN
o-Nilrololuene
Nitr~enzene
m-Nitratoluene
135-TriniCrobcnzene
m-Dinittobenzene
p-NirrorQuene
Concentration 500
500
500
500
SOO SOO SOO 500
1000
500
i 500
500
500
SOO soo
-~
U
U
U
U
U
U
u I
U -I U
U i
U i U
U
U
~J
Concentrwon =0
Instrument X Concentllllted Bxrract Volumll X Dilution Value Sam~e Amoun Factor
Page 1 of 2
Page 17 of 329
T-782 POO7l013 F-443 $ +5056060864Jan-15-200S 04 26pm From-EP TA2l __r
GEL lAboratQlies LLC Report Dllte AuguSll 2007
PCB Page 1 of 1 Certificate of Analysis
Sample Summary
SDG NUlllber 07-293 Da~ Collected 07171Z0071200 Man-Ix SOIL
Lab Sample ID 189817001 Date Reccied 071l9J200709)0 Moislure 7 Client SlUllple 12 Client LANL006 Project LANLOOGOO ClientID RE2-07-3893 Method SW846)082 SOP Ref CL-OA-E-04ll
Batch ID 653073 lrut ECD2A1 DIlution 1
Run Daoo 0712712007 1258 AnaYBt JXM Inj Vol tIlL lnpDllte 071J320070800 Aliquot 30~ FInal Volume ImL Dab File 014tl401d Column 1 eLFl Level LOW
014b140~d 2CLP2
CAS No Parnmame Qualifler Result Units Ml)ULOD PQULOQ CoIWl1lI
12674-lJ-2 Aroclor-1016 U 336 uglkg Ll2 336
11104-28-2 Aroclor-1221 U 3~6 uglkg 112 336
1114l-16-) Atoclor-1232 U 336 lIglkg 112 336
53469-21-9 Arocor-1242 U 336 Ilglkg LI2 336
12672-29-lt ArocIOr-l24amp U 336 uSlkg 112 336
1I097-6H Aroclor-12S4 J 120 lIgkg 112 336
11096-82-5 Aroclar-1260 U 336 uglkg 112 336
Page 208 of329
-----
~ 2 ~ o lt0
f
o (N
~ ltll
g 01
-~ - --~
11gt319
21-353 21-485 J I Investigation area
~ Ifor SWMU 21-027(a) j( 4-in floor drain pipe ~ U engineerillg drawing location) I
f r I ~~ ~12~n storm drarfl cemeflt culvert _lturveyecl location)
J I I
_I I I J
I J J shylI
I -~
-
cJ Slructu ra
l- I Former slructure
Jilvestigalion area
bull Proposed sample toeation
reg Prop()Sed borehole location amp Previous sample localirm euroI Previous bOfehole localion
Pipeline (surveyed location)
Pjpeline (enQineering drawjng localion)
Road
Fenoe 10-fl c1I110Uf
0 40 80
FEET 19113 HAl) t
bull 7rlltJ bull
- _shy
- ~ ~ 7050---middot
- -------- -~--~-
-
-- ~-~
- -~ --~ --- ~ - -- - -~~t= _
- - - --~~~
r050- _15 - -~- -- - - -~
---- ~ -~- _--_ -
- ~ ~--~~ -- ~ ----- -----~-i~ ~~-~ shy ~ - ~ ~
Slu1s GISLab tA201224 061 4ll4 mgtflfied far F5193 IlPwai sile 1l3D1igt5 plrn
Figure 519-3 SWMU 21-027(a) proposed sample locations
tI ll (()
ft ) ltc co ~ (0 fIl iii p a IJ)
s ~ ~ IJ)
amp 3
~ ~ J1)J
L
-
I c c 0
c jgt
0 = C 5 I
~
+ UI c UI en cl
cl jo
-4
-I ltXl
C
= = ltXl- = cJ
-n I
___
Jilil-IO-UUO U4QPm rrum-tr IA +bUb1i060664 T-78Z P009013 F-443 LU~ fllUllU~ rl~110nal Luoorarory Page I or
SAMPLE COLLECTION LOGFIELD CHAIN OF CUSTODY EVENT ID 198 EVENT NAME CU21-027(a) DP Site Summer]a1l2007
) SAMPLE ID RE21-07-SS93
ASPLANNtP
DATE COLLECfED(MMlDDIVYYV)
TIME COLLECTED (HlIMM)
PRS ID ZHIZ(JI
LOCATIONm ~~11u1 LOCATION TYPE GENpoundRlC
~~v
TOP DEPTH-fIljrid 7
BonOM DEPTH -r i01 FIElJlMTR1X --5- ~~~I
i ~( ~()T COMPOSITETVPpound --
ASCQLLECTpoundll
2 ftro 7
u C bull 2( o h
R- II01d-2S lei( 4b
4 0 ft- 4 0 f 1shy
bull (
MEDIA
SUBmiddotli--shy~w
SAMPLE TECH CODE
FIELD QCTVPE
FIELD PREP
SAMlLtlJSAGE
SCREENIlOlU DESC
AS PLANNED rev
~ lJhlt77
W 11 rJ
~ 1)
amp
amp
INV
A
ASCQLLECTED
(1 h 1- 3 D tC1 A Cd t
1
tY
EXCAVATED YfSte~N--A----------------Ii
COMPOSITpoundnME1NTERVAL WATER FLOWING YES~NA
BOREHOLE YES~A BOREHOLE DECLINATION ___~__ BOREHOLE DIRECTION shy
PRIOnlTY ORD~R CNTNR PRESERVATIVE COLLECTED YIN
SPECIAL INSTRUCTIONS
2
2
1
8082
8290
NMED Explosives list
125MLGLASS
125MLGLASS
250 l1L AMBER GLASS
_ _-_ _shy
Ice
Ice
Ice
V y
L _____ --_ )SAMPLE DESC t Quck I uGrvi- 15~ Gr~v TIImiddotH
SAMPLE COMMENTS
LOCATIONDESC Y-1lt~tLev ~k
shy
~c~~ 4(0 ]n Ie r fr-Dt71 (one) 113 ~r~ 1110 CIir
FIELD SCREENINGIMEASUREMENT RESULTS flO bf-c ygtY1rxi- 0 -0 r31r
f ~ I rf olcJ1f p j tJ~ Ot p17d 7-tdfM
REVIEWED BY (PRINT ___________COLLECT~DBY (pRINT) _ __---Vi shyr shy -
DateffilneDateffime RECEIVED BYRELINQUISHED BY I070 r (Printed Name)
(Signature)
(Printed Name) )C20(Signature) Jo~~
RECEIVED BY Datetrime
I (Printed Name)
DateITimeRELINQUISHED BY
(Printed N arne)
(Signature)(Signature)
I I
I
I
CL
cYgt
shy
u Sample ill RE21-07-5893 (Q
Client Data = Los Alamoo National Laboratory 0amp-347 S-Dee-07 0830
Samlc Data
Malrix Soil Sample Size t 13 g
middotSolids 894
shycgt
cgt
Name Project Date Collected Time Collected
co I Analyte Cone (pglg) DL a EWCb Qualifierst-
2378-TCDD 12378-PeCDD
l23478-HxCDD
123678-HxCDD
ltJgt CO Cgt 123789-HxCDDUgt cgt lt0 LO
1234678-HpCDD = In + OeDD
2378-TCDF
12378-PeCDF 23478-PeCDF
123478-HxCDF 12367 8-HxC DF
23 467amp-HxCDF
123789middotHxCDF
1234678-HpCDF 1234789-HpCDF
aCDF
Totals
0599 322
63amp
379
16l
1320
15200 0302
0503 L4J
492
382
692
129 [52
142
503
423
279 259 2790
643
276
205
726
435
284
699
J
I J
J B
B
EPA lVlcthod 8290
labontoa Data
Lab Sample 30042~OOl Dare Reeeind 7-Dec-07 QC Batch No 9763 Date ExlIllc[ltd 1O-Dec-07 Dale Analyzed DB-5 13-Dee-07 [)ate Analyzrd DB-225 NA
_shy
Labeled Standard R LeL-UCLd Qualifiers _ shy
IS t3C-2J78-TCDD 898 4) - 13S 13C-[2J7S-PeCDD 916 40 - 135 13C-l23478-HxCDD 935 40- 135 13C-l236 78-HltCD 0 816 40 - 135
lJC-l234678-HpCDD 104shy 40 shy 135 13C-OCDD 122 40 shy l35 13C-2378-TCDF 100 40 - 135 llC-l 2378- PeC DF [04 40- 135 13C-23478-PeCDF 109 40- fJ5 [3C-I2JA78-HKCDF 914 40 - 135
l3C- 123678-HxCDF 792 4() - lJ5 l3C-234678-HxCDP 842 40 shy 135
13C-l23789-HxCDF 9l2 40- 135 [3C-1234678-HpCDF 847 40 shy [35
13C-1234789-HpCDF 991 40 - DS L3C-QCDF 985 40 shy 135
CRS 37Cl-2378-TCDD 936 40 shy 135 eTodc Equivalent Qnotient (fEQ) Data
-lt t-CL UJ
I E o ~
LL
E n
lt0
cgt agt lt=gt cgt
I tn
I c
TotalrCDD
Total PeCDD Total HxCDD Total HpCDD Total TCDF Total PeCDF Total HxCDF
Tota[ HpCDF
Anal~st MAS
P
P
P BP
TEQ(Min) 413
a Sample specific etimated detection j iInil
b Eslilnated maximum possible cQfcenlfatioll
c Method detec1iol1lirniL
d Lo1r~oltrollimil- uppNcolltrollimit
e 7EQ based an (1989) [nternatiooal roxie EquiaIent Filltturs (ITEn
The fltlltl-Wll are repooed in dry weighl The sam pIe size is rej)lJrtild in wltt weight
AwrovedBy Martha M Maier lJ-Dec-2007 1527
T-782 P 011013 F-443Jilll-IO-UUO U4 opm rrom-II III +5056060864
1 High Explosives Analysls Data Sheet
I CalNo 118-96-7
I 121~14-2 Irshy 121-82-4
19406-51-0
2691-41middot0
35572~7g2
479-45-8
606middot20middot2 78-11-5
88-72-2
98-95-3
99-08-1 -~
9935-4
99middot65middot0 f
99w99-0l
Lab Name General Engineering Lahorarcries Client Sample ID RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sample ID 198941001
Moistm-e 103Sample Amount pound
Amoullt Units l Date Received 07~DECmiddot07
Extl8ction Type Sonicatioll Extraction Batch In 709399
COllcenhated Extlllct Volume (UlL) ill Dale Extracted 12middotDEC-07
PllutlOll Facto ~ Injection Volume CuLl ~
Date Analyzed 1H)EC-07 1529GEL (lata tJle EXP12l20S7a
Units ugJkg __ n _
ComJound Concentration -Q]- - 500246-Trinitrotoh Hme 1 U I
~ 24middotDinitrotolu~ene SOD I U
Rl)X 500 I u1 4-Amino-26dinibmiddoto l) illene 500 r-u-
HMX
2-Amino-46-dinitro ojuelle
Tetryl
I 26-Dlllltrotolul~ ~ lUi middot-------~------~----~-----~--t
a
PElN 1000 U wNitrotoluellc
500 ~-1 Nitrobenzen 500 I U
i m-NitrotolUefle SOD I u 135-Tdnitrober zelle 500 I U
ffi-Dinitrobenzi ne 1 500 lUi p-Nitrotoluel1e 500 I U
____ ___-l_____ _ __ ___ L___~ - ~
_ soo U
500 U -i 500 U
-J
-----~~------------ ----- shy Concentration
Instnment X ConcenUllred Extract Volume X Dilutioll Value Samele ArnouD Factor
Page of 2
Page 93 of344
Jan-IO-UU~ U4pm Irom-t IAll +5056060864 T-782 P012013 F-443
1 High Explosives Analysis DII tn Sheet
Lab Name Qeneml Engineering Laboratories Client Sample llgt RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sam)Je lD 198947001
Moisture 103Sample Amount 2
Date Received 07-DEC-07Amount Unitli g
Extmction Type Sonication Extractiou Batch ID 709399
Concentrated Extract Volume (mL) 12 Date Extracted 12-DECmiddot07
Dilution Fact6r Injection Volume (uL) 50
Date Analyzed 17middotDECmiddot07 1903 GEL data file EXS12 17035wiff
Units ugkg
Cas No 3058middot386
59229-7S-3
Compound TATB
26-Diminc-4-nitI
- shy --- Concentnnkm -~T-0-1 1000 -~
2000 1u 618middot87-1 3SmiddotDinitroaniIinc 1000 U
6629--29-4
78-30-8
24Dlamlno-6-iroii~n-trls(o-cresyl) phosphate _~___~ bull -
- ] 2000 U bull
1000 U -1I __bullbull_ bullbullbull___ ~_________ I--_~ I
-~-------- ---shyConcenlrarion
IloSlfllmem X Concanrated Etracr Volllrne Dilution L Value ~__~ Sample Amoun X Factor
Page 2 of 2
Page 96 of344
-
II-IO-UUC Uflpm rrom-cr 111pound I +5056060864 T-782 P013013 F-443
GE~ Inboratories LLe Report Date December 15 2007
SDGNuwber 08-348 Lab Sample ill 198947001
CilelltID REZT-Ol-S893
)llltch fI) 10954l
RunDllte 1211412007 0149
Prep Date 121102007 1953
DlItli FIle 049f4901d
049b49111d
CAS No Fucmname --shy
12674-Il-2 Aruclor-l 0 16
11104-28-2 Arocior-1221
11141-16-5 AroelOr- 1232
53469-21-9 Aroclor-1242
12672-29-6 Aroclor-1248
11097-69-1 Aroclor-1254
11096-81-5 Aroclor-1260
PCB Certifieate of Analysts
Sample Summary
Date Collected 1210512007 1200
Dute Received 120712007 0930 Client LANL008
Method SW84ti8082
In8t EC02Al
Analyst JXM Aliquot 29911 Column lCLPl
2CLP2
Quulitiec Result l1nits ------ U 373 Ij1kg
U 373 uglkg
U 373 ujlkg
U 373 uglkg
U 373 u1kg
950 uglkg
690 uglkg
Page I of 1
Ma[th S
Moistllre 103 Project LANLOO800 SOPRlf GL-oA-E-040 Dilution 1
Inj Vol luI binlll Volume ImL
Level LOW
MDLtrOD PQt1OQ Column shy
124 373
124 373
124 373
124 373
24 373
124 373 2
124 373
Page 232 of 344
-
T-782 POO7l013 F-443 $ +5056060864Jan-15-200S 04 26pm From-EP TA2l __r
GEL lAboratQlies LLC Report Dllte AuguSll 2007
PCB Page 1 of 1 Certificate of Analysis
Sample Summary
SDG NUlllber 07-293 Da~ Collected 07171Z0071200 Man-Ix SOIL
Lab Sample ID 189817001 Date Reccied 071l9J200709)0 Moislure 7 Client SlUllple 12 Client LANL006 Project LANLOOGOO ClientID RE2-07-3893 Method SW846)082 SOP Ref CL-OA-E-04ll
Batch ID 653073 lrut ECD2A1 DIlution 1
Run Daoo 0712712007 1258 AnaYBt JXM Inj Vol tIlL lnpDllte 071J320070800 Aliquot 30~ FInal Volume ImL Dab File 014tl401d Column 1 eLFl Level LOW
014b140~d 2CLP2
CAS No Parnmame Qualifler Result Units Ml)ULOD PQULOQ CoIWl1lI
12674-lJ-2 Aroclor-1016 U 336 uglkg Ll2 336
11104-28-2 Aroclor-1221 U 3~6 uglkg 112 336
1114l-16-) Atoclor-1232 U 336 lIglkg 112 336
53469-21-9 Arocor-1242 U 336 Ilglkg LI2 336
12672-29-lt ArocIOr-l24amp U 336 uSlkg 112 336
1I097-6H Aroclor-12S4 J 120 lIgkg 112 336
11096-82-5 Aroclar-1260 U 336 uglkg 112 336
Page 208 of329
-----
~ 2 ~ o lt0
f
o (N
~ ltll
g 01
-~ - --~
11gt319
21-353 21-485 J I Investigation area
~ Ifor SWMU 21-027(a) j( 4-in floor drain pipe ~ U engineerillg drawing location) I
f r I ~~ ~12~n storm drarfl cemeflt culvert _lturveyecl location)
J I I
_I I I J
I J J shylI
I -~
-
cJ Slructu ra
l- I Former slructure
Jilvestigalion area
bull Proposed sample toeation
reg Prop()Sed borehole location amp Previous sample localirm euroI Previous bOfehole localion
Pipeline (surveyed location)
Pjpeline (enQineering drawjng localion)
Road
Fenoe 10-fl c1I110Uf
0 40 80
FEET 19113 HAl) t
bull 7rlltJ bull
- _shy
- ~ ~ 7050---middot
- -------- -~--~-
-
-- ~-~
- -~ --~ --- ~ - -- - -~~t= _
- - - --~~~
r050- _15 - -~- -- - - -~
---- ~ -~- _--_ -
- ~ ~--~~ -- ~ ----- -----~-i~ ~~-~ shy ~ - ~ ~
Slu1s GISLab tA201224 061 4ll4 mgtflfied far F5193 IlPwai sile 1l3D1igt5 plrn
Figure 519-3 SWMU 21-027(a) proposed sample locations
tI ll (()
ft ) ltc co ~ (0 fIl iii p a IJ)
s ~ ~ IJ)
amp 3
~ ~ J1)J
L
-
I c c 0
c jgt
0 = C 5 I
~
+ UI c UI en cl
cl jo
-4
-I ltXl
C
= = ltXl- = cJ
-n I
___
Jilil-IO-UUO U4QPm rrum-tr IA +bUb1i060664 T-78Z P009013 F-443 LU~ fllUllU~ rl~110nal Luoorarory Page I or
SAMPLE COLLECTION LOGFIELD CHAIN OF CUSTODY EVENT ID 198 EVENT NAME CU21-027(a) DP Site Summer]a1l2007
) SAMPLE ID RE21-07-SS93
ASPLANNtP
DATE COLLECfED(MMlDDIVYYV)
TIME COLLECTED (HlIMM)
PRS ID ZHIZ(JI
LOCATIONm ~~11u1 LOCATION TYPE GENpoundRlC
~~v
TOP DEPTH-fIljrid 7
BonOM DEPTH -r i01 FIElJlMTR1X --5- ~~~I
i ~( ~()T COMPOSITETVPpound --
ASCQLLECTpoundll
2 ftro 7
u C bull 2( o h
R- II01d-2S lei( 4b
4 0 ft- 4 0 f 1shy
bull (
MEDIA
SUBmiddotli--shy~w
SAMPLE TECH CODE
FIELD QCTVPE
FIELD PREP
SAMlLtlJSAGE
SCREENIlOlU DESC
AS PLANNED rev
~ lJhlt77
W 11 rJ
~ 1)
amp
amp
INV
A
ASCQLLECTED
(1 h 1- 3 D tC1 A Cd t
1
tY
EXCAVATED YfSte~N--A----------------Ii
COMPOSITpoundnME1NTERVAL WATER FLOWING YES~NA
BOREHOLE YES~A BOREHOLE DECLINATION ___~__ BOREHOLE DIRECTION shy
PRIOnlTY ORD~R CNTNR PRESERVATIVE COLLECTED YIN
SPECIAL INSTRUCTIONS
2
2
1
8082
8290
NMED Explosives list
125MLGLASS
125MLGLASS
250 l1L AMBER GLASS
_ _-_ _shy
Ice
Ice
Ice
V y
L _____ --_ )SAMPLE DESC t Quck I uGrvi- 15~ Gr~v TIImiddotH
SAMPLE COMMENTS
LOCATIONDESC Y-1lt~tLev ~k
shy
~c~~ 4(0 ]n Ie r fr-Dt71 (one) 113 ~r~ 1110 CIir
FIELD SCREENINGIMEASUREMENT RESULTS flO bf-c ygtY1rxi- 0 -0 r31r
f ~ I rf olcJ1f p j tJ~ Ot p17d 7-tdfM
REVIEWED BY (PRINT ___________COLLECT~DBY (pRINT) _ __---Vi shyr shy -
DateffilneDateffime RECEIVED BYRELINQUISHED BY I070 r (Printed Name)
(Signature)
(Printed Name) )C20(Signature) Jo~~
RECEIVED BY Datetrime
I (Printed Name)
DateITimeRELINQUISHED BY
(Printed N arne)
(Signature)(Signature)
I I
I
I
CL
cYgt
shy
u Sample ill RE21-07-5893 (Q
Client Data = Los Alamoo National Laboratory 0amp-347 S-Dee-07 0830
Samlc Data
Malrix Soil Sample Size t 13 g
middotSolids 894
shycgt
cgt
Name Project Date Collected Time Collected
co I Analyte Cone (pglg) DL a EWCb Qualifierst-
2378-TCDD 12378-PeCDD
l23478-HxCDD
123678-HxCDD
ltJgt CO Cgt 123789-HxCDDUgt cgt lt0 LO
1234678-HpCDD = In + OeDD
2378-TCDF
12378-PeCDF 23478-PeCDF
123478-HxCDF 12367 8-HxC DF
23 467amp-HxCDF
123789middotHxCDF
1234678-HpCDF 1234789-HpCDF
aCDF
Totals
0599 322
63amp
379
16l
1320
15200 0302
0503 L4J
492
382
692
129 [52
142
503
423
279 259 2790
643
276
205
726
435
284
699
J
I J
J B
B
EPA lVlcthod 8290
labontoa Data
Lab Sample 30042~OOl Dare Reeeind 7-Dec-07 QC Batch No 9763 Date ExlIllc[ltd 1O-Dec-07 Dale Analyzed DB-5 13-Dee-07 [)ate Analyzrd DB-225 NA
_shy
Labeled Standard R LeL-UCLd Qualifiers _ shy
IS t3C-2J78-TCDD 898 4) - 13S 13C-[2J7S-PeCDD 916 40 - 135 13C-l23478-HxCDD 935 40- 135 13C-l236 78-HltCD 0 816 40 - 135
lJC-l234678-HpCDD 104shy 40 shy 135 13C-OCDD 122 40 shy l35 13C-2378-TCDF 100 40 - 135 llC-l 2378- PeC DF [04 40- 135 13C-23478-PeCDF 109 40- fJ5 [3C-I2JA78-HKCDF 914 40 - 135
l3C- 123678-HxCDF 792 4() - lJ5 l3C-234678-HxCDP 842 40 shy 135
13C-l23789-HxCDF 9l2 40- 135 [3C-1234678-HpCDF 847 40 shy [35
13C-1234789-HpCDF 991 40 - DS L3C-QCDF 985 40 shy 135
CRS 37Cl-2378-TCDD 936 40 shy 135 eTodc Equivalent Qnotient (fEQ) Data
-lt t-CL UJ
I E o ~
LL
E n
lt0
cgt agt lt=gt cgt
I tn
I c
TotalrCDD
Total PeCDD Total HxCDD Total HpCDD Total TCDF Total PeCDF Total HxCDF
Tota[ HpCDF
Anal~st MAS
P
P
P BP
TEQ(Min) 413
a Sample specific etimated detection j iInil
b Eslilnated maximum possible cQfcenlfatioll
c Method detec1iol1lirniL
d Lo1r~oltrollimil- uppNcolltrollimit
e 7EQ based an (1989) [nternatiooal roxie EquiaIent Filltturs (ITEn
The fltlltl-Wll are repooed in dry weighl The sam pIe size is rej)lJrtild in wltt weight
AwrovedBy Martha M Maier lJ-Dec-2007 1527
T-782 P 011013 F-443Jilll-IO-UUO U4 opm rrom-II III +5056060864
1 High Explosives Analysls Data Sheet
I CalNo 118-96-7
I 121~14-2 Irshy 121-82-4
19406-51-0
2691-41middot0
35572~7g2
479-45-8
606middot20middot2 78-11-5
88-72-2
98-95-3
99-08-1 -~
9935-4
99middot65middot0 f
99w99-0l
Lab Name General Engineering Lahorarcries Client Sample ID RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sample ID 198941001
Moistm-e 103Sample Amount pound
Amoullt Units l Date Received 07~DECmiddot07
Extl8ction Type Sonicatioll Extraction Batch In 709399
COllcenhated Extlllct Volume (UlL) ill Dale Extracted 12middotDEC-07
PllutlOll Facto ~ Injection Volume CuLl ~
Date Analyzed 1H)EC-07 1529GEL (lata tJle EXP12l20S7a
Units ugJkg __ n _
ComJound Concentration -Q]- - 500246-Trinitrotoh Hme 1 U I
~ 24middotDinitrotolu~ene SOD I U
Rl)X 500 I u1 4-Amino-26dinibmiddoto l) illene 500 r-u-
HMX
2-Amino-46-dinitro ojuelle
Tetryl
I 26-Dlllltrotolul~ ~ lUi middot-------~------~----~-----~--t
a
PElN 1000 U wNitrotoluellc
500 ~-1 Nitrobenzen 500 I U
i m-NitrotolUefle SOD I u 135-Tdnitrober zelle 500 I U
ffi-Dinitrobenzi ne 1 500 lUi p-Nitrotoluel1e 500 I U
____ ___-l_____ _ __ ___ L___~ - ~
_ soo U
500 U -i 500 U
-J
-----~~------------ ----- shy Concentration
Instnment X ConcenUllred Extract Volume X Dilutioll Value Samele ArnouD Factor
Page of 2
Page 93 of344
Jan-IO-UU~ U4pm Irom-t IAll +5056060864 T-782 P012013 F-443
1 High Explosives Analysis DII tn Sheet
Lab Name Qeneml Engineering Laboratories Client Sample llgt RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sam)Je lD 198947001
Moisture 103Sample Amount 2
Date Received 07-DEC-07Amount Unitli g
Extmction Type Sonication Extractiou Batch ID 709399
Concentrated Extract Volume (mL) 12 Date Extracted 12-DECmiddot07
Dilution Fact6r Injection Volume (uL) 50
Date Analyzed 17middotDECmiddot07 1903 GEL data file EXS12 17035wiff
Units ugkg
Cas No 3058middot386
59229-7S-3
Compound TATB
26-Diminc-4-nitI
- shy --- Concentnnkm -~T-0-1 1000 -~
2000 1u 618middot87-1 3SmiddotDinitroaniIinc 1000 U
6629--29-4
78-30-8
24Dlamlno-6-iroii~n-trls(o-cresyl) phosphate _~___~ bull -
- ] 2000 U bull
1000 U -1I __bullbull_ bullbullbull___ ~_________ I--_~ I
-~-------- ---shyConcenlrarion
IloSlfllmem X Concanrated Etracr Volllrne Dilution L Value ~__~ Sample Amoun X Factor
Page 2 of 2
Page 96 of344
-
II-IO-UUC Uflpm rrom-cr 111pound I +5056060864 T-782 P013013 F-443
GE~ Inboratories LLe Report Date December 15 2007
SDGNuwber 08-348 Lab Sample ill 198947001
CilelltID REZT-Ol-S893
)llltch fI) 10954l
RunDllte 1211412007 0149
Prep Date 121102007 1953
DlItli FIle 049f4901d
049b49111d
CAS No Fucmname --shy
12674-Il-2 Aruclor-l 0 16
11104-28-2 Arocior-1221
11141-16-5 AroelOr- 1232
53469-21-9 Aroclor-1242
12672-29-6 Aroclor-1248
11097-69-1 Aroclor-1254
11096-81-5 Aroclor-1260
PCB Certifieate of Analysts
Sample Summary
Date Collected 1210512007 1200
Dute Received 120712007 0930 Client LANL008
Method SW84ti8082
In8t EC02Al
Analyst JXM Aliquot 29911 Column lCLPl
2CLP2
Quulitiec Result l1nits ------ U 373 Ij1kg
U 373 uglkg
U 373 ujlkg
U 373 uglkg
U 373 u1kg
950 uglkg
690 uglkg
Page I of 1
Ma[th S
Moistllre 103 Project LANLOO800 SOPRlf GL-oA-E-040 Dilution 1
Inj Vol luI binlll Volume ImL
Level LOW
MDLtrOD PQt1OQ Column shy
124 373
124 373
124 373
124 373
24 373
124 373 2
124 373
Page 232 of 344
-
-----
~ 2 ~ o lt0
f
o (N
~ ltll
g 01
-~ - --~
11gt319
21-353 21-485 J I Investigation area
~ Ifor SWMU 21-027(a) j( 4-in floor drain pipe ~ U engineerillg drawing location) I
f r I ~~ ~12~n storm drarfl cemeflt culvert _lturveyecl location)
J I I
_I I I J
I J J shylI
I -~
-
cJ Slructu ra
l- I Former slructure
Jilvestigalion area
bull Proposed sample toeation
reg Prop()Sed borehole location amp Previous sample localirm euroI Previous bOfehole localion
Pipeline (surveyed location)
Pjpeline (enQineering drawjng localion)
Road
Fenoe 10-fl c1I110Uf
0 40 80
FEET 19113 HAl) t
bull 7rlltJ bull
- _shy
- ~ ~ 7050---middot
- -------- -~--~-
-
-- ~-~
- -~ --~ --- ~ - -- - -~~t= _
- - - --~~~
r050- _15 - -~- -- - - -~
---- ~ -~- _--_ -
- ~ ~--~~ -- ~ ----- -----~-i~ ~~-~ shy ~ - ~ ~
Slu1s GISLab tA201224 061 4ll4 mgtflfied far F5193 IlPwai sile 1l3D1igt5 plrn
Figure 519-3 SWMU 21-027(a) proposed sample locations
tI ll (()
ft ) ltc co ~ (0 fIl iii p a IJ)
s ~ ~ IJ)
amp 3
~ ~ J1)J
L
-
I c c 0
c jgt
0 = C 5 I
~
+ UI c UI en cl
cl jo
-4
-I ltXl
C
= = ltXl- = cJ
-n I
___
Jilil-IO-UUO U4QPm rrum-tr IA +bUb1i060664 T-78Z P009013 F-443 LU~ fllUllU~ rl~110nal Luoorarory Page I or
SAMPLE COLLECTION LOGFIELD CHAIN OF CUSTODY EVENT ID 198 EVENT NAME CU21-027(a) DP Site Summer]a1l2007
) SAMPLE ID RE21-07-SS93
ASPLANNtP
DATE COLLECfED(MMlDDIVYYV)
TIME COLLECTED (HlIMM)
PRS ID ZHIZ(JI
LOCATIONm ~~11u1 LOCATION TYPE GENpoundRlC
~~v
TOP DEPTH-fIljrid 7
BonOM DEPTH -r i01 FIElJlMTR1X --5- ~~~I
i ~( ~()T COMPOSITETVPpound --
ASCQLLECTpoundll
2 ftro 7
u C bull 2( o h
R- II01d-2S lei( 4b
4 0 ft- 4 0 f 1shy
bull (
MEDIA
SUBmiddotli--shy~w
SAMPLE TECH CODE
FIELD QCTVPE
FIELD PREP
SAMlLtlJSAGE
SCREENIlOlU DESC
AS PLANNED rev
~ lJhlt77
W 11 rJ
~ 1)
amp
amp
INV
A
ASCQLLECTED
(1 h 1- 3 D tC1 A Cd t
1
tY
EXCAVATED YfSte~N--A----------------Ii
COMPOSITpoundnME1NTERVAL WATER FLOWING YES~NA
BOREHOLE YES~A BOREHOLE DECLINATION ___~__ BOREHOLE DIRECTION shy
PRIOnlTY ORD~R CNTNR PRESERVATIVE COLLECTED YIN
SPECIAL INSTRUCTIONS
2
2
1
8082
8290
NMED Explosives list
125MLGLASS
125MLGLASS
250 l1L AMBER GLASS
_ _-_ _shy
Ice
Ice
Ice
V y
L _____ --_ )SAMPLE DESC t Quck I uGrvi- 15~ Gr~v TIImiddotH
SAMPLE COMMENTS
LOCATIONDESC Y-1lt~tLev ~k
shy
~c~~ 4(0 ]n Ie r fr-Dt71 (one) 113 ~r~ 1110 CIir
FIELD SCREENINGIMEASUREMENT RESULTS flO bf-c ygtY1rxi- 0 -0 r31r
f ~ I rf olcJ1f p j tJ~ Ot p17d 7-tdfM
REVIEWED BY (PRINT ___________COLLECT~DBY (pRINT) _ __---Vi shyr shy -
DateffilneDateffime RECEIVED BYRELINQUISHED BY I070 r (Printed Name)
(Signature)
(Printed Name) )C20(Signature) Jo~~
RECEIVED BY Datetrime
I (Printed Name)
DateITimeRELINQUISHED BY
(Printed N arne)
(Signature)(Signature)
I I
I
I
CL
cYgt
shy
u Sample ill RE21-07-5893 (Q
Client Data = Los Alamoo National Laboratory 0amp-347 S-Dee-07 0830
Samlc Data
Malrix Soil Sample Size t 13 g
middotSolids 894
shycgt
cgt
Name Project Date Collected Time Collected
co I Analyte Cone (pglg) DL a EWCb Qualifierst-
2378-TCDD 12378-PeCDD
l23478-HxCDD
123678-HxCDD
ltJgt CO Cgt 123789-HxCDDUgt cgt lt0 LO
1234678-HpCDD = In + OeDD
2378-TCDF
12378-PeCDF 23478-PeCDF
123478-HxCDF 12367 8-HxC DF
23 467amp-HxCDF
123789middotHxCDF
1234678-HpCDF 1234789-HpCDF
aCDF
Totals
0599 322
63amp
379
16l
1320
15200 0302
0503 L4J
492
382
692
129 [52
142
503
423
279 259 2790
643
276
205
726
435
284
699
J
I J
J B
B
EPA lVlcthod 8290
labontoa Data
Lab Sample 30042~OOl Dare Reeeind 7-Dec-07 QC Batch No 9763 Date ExlIllc[ltd 1O-Dec-07 Dale Analyzed DB-5 13-Dee-07 [)ate Analyzrd DB-225 NA
_shy
Labeled Standard R LeL-UCLd Qualifiers _ shy
IS t3C-2J78-TCDD 898 4) - 13S 13C-[2J7S-PeCDD 916 40 - 135 13C-l23478-HxCDD 935 40- 135 13C-l236 78-HltCD 0 816 40 - 135
lJC-l234678-HpCDD 104shy 40 shy 135 13C-OCDD 122 40 shy l35 13C-2378-TCDF 100 40 - 135 llC-l 2378- PeC DF [04 40- 135 13C-23478-PeCDF 109 40- fJ5 [3C-I2JA78-HKCDF 914 40 - 135
l3C- 123678-HxCDF 792 4() - lJ5 l3C-234678-HxCDP 842 40 shy 135
13C-l23789-HxCDF 9l2 40- 135 [3C-1234678-HpCDF 847 40 shy [35
13C-1234789-HpCDF 991 40 - DS L3C-QCDF 985 40 shy 135
CRS 37Cl-2378-TCDD 936 40 shy 135 eTodc Equivalent Qnotient (fEQ) Data
-lt t-CL UJ
I E o ~
LL
E n
lt0
cgt agt lt=gt cgt
I tn
I c
TotalrCDD
Total PeCDD Total HxCDD Total HpCDD Total TCDF Total PeCDF Total HxCDF
Tota[ HpCDF
Anal~st MAS
P
P
P BP
TEQ(Min) 413
a Sample specific etimated detection j iInil
b Eslilnated maximum possible cQfcenlfatioll
c Method detec1iol1lirniL
d Lo1r~oltrollimil- uppNcolltrollimit
e 7EQ based an (1989) [nternatiooal roxie EquiaIent Filltturs (ITEn
The fltlltl-Wll are repooed in dry weighl The sam pIe size is rej)lJrtild in wltt weight
AwrovedBy Martha M Maier lJ-Dec-2007 1527
T-782 P 011013 F-443Jilll-IO-UUO U4 opm rrom-II III +5056060864
1 High Explosives Analysls Data Sheet
I CalNo 118-96-7
I 121~14-2 Irshy 121-82-4
19406-51-0
2691-41middot0
35572~7g2
479-45-8
606middot20middot2 78-11-5
88-72-2
98-95-3
99-08-1 -~
9935-4
99middot65middot0 f
99w99-0l
Lab Name General Engineering Lahorarcries Client Sample ID RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sample ID 198941001
Moistm-e 103Sample Amount pound
Amoullt Units l Date Received 07~DECmiddot07
Extl8ction Type Sonicatioll Extraction Batch In 709399
COllcenhated Extlllct Volume (UlL) ill Dale Extracted 12middotDEC-07
PllutlOll Facto ~ Injection Volume CuLl ~
Date Analyzed 1H)EC-07 1529GEL (lata tJle EXP12l20S7a
Units ugJkg __ n _
ComJound Concentration -Q]- - 500246-Trinitrotoh Hme 1 U I
~ 24middotDinitrotolu~ene SOD I U
Rl)X 500 I u1 4-Amino-26dinibmiddoto l) illene 500 r-u-
HMX
2-Amino-46-dinitro ojuelle
Tetryl
I 26-Dlllltrotolul~ ~ lUi middot-------~------~----~-----~--t
a
PElN 1000 U wNitrotoluellc
500 ~-1 Nitrobenzen 500 I U
i m-NitrotolUefle SOD I u 135-Tdnitrober zelle 500 I U
ffi-Dinitrobenzi ne 1 500 lUi p-Nitrotoluel1e 500 I U
____ ___-l_____ _ __ ___ L___~ - ~
_ soo U
500 U -i 500 U
-J
-----~~------------ ----- shy Concentration
Instnment X ConcenUllred Extract Volume X Dilutioll Value Samele ArnouD Factor
Page of 2
Page 93 of344
Jan-IO-UU~ U4pm Irom-t IAll +5056060864 T-782 P012013 F-443
1 High Explosives Analysis DII tn Sheet
Lab Name Qeneml Engineering Laboratories Client Sample llgt RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sam)Je lD 198947001
Moisture 103Sample Amount 2
Date Received 07-DEC-07Amount Unitli g
Extmction Type Sonication Extractiou Batch ID 709399
Concentrated Extract Volume (mL) 12 Date Extracted 12-DECmiddot07
Dilution Fact6r Injection Volume (uL) 50
Date Analyzed 17middotDECmiddot07 1903 GEL data file EXS12 17035wiff
Units ugkg
Cas No 3058middot386
59229-7S-3
Compound TATB
26-Diminc-4-nitI
- shy --- Concentnnkm -~T-0-1 1000 -~
2000 1u 618middot87-1 3SmiddotDinitroaniIinc 1000 U
6629--29-4
78-30-8
24Dlamlno-6-iroii~n-trls(o-cresyl) phosphate _~___~ bull -
- ] 2000 U bull
1000 U -1I __bullbull_ bullbullbull___ ~_________ I--_~ I
-~-------- ---shyConcenlrarion
IloSlfllmem X Concanrated Etracr Volllrne Dilution L Value ~__~ Sample Amoun X Factor
Page 2 of 2
Page 96 of344
-
II-IO-UUC Uflpm rrom-cr 111pound I +5056060864 T-782 P013013 F-443
GE~ Inboratories LLe Report Date December 15 2007
SDGNuwber 08-348 Lab Sample ill 198947001
CilelltID REZT-Ol-S893
)llltch fI) 10954l
RunDllte 1211412007 0149
Prep Date 121102007 1953
DlItli FIle 049f4901d
049b49111d
CAS No Fucmname --shy
12674-Il-2 Aruclor-l 0 16
11104-28-2 Arocior-1221
11141-16-5 AroelOr- 1232
53469-21-9 Aroclor-1242
12672-29-6 Aroclor-1248
11097-69-1 Aroclor-1254
11096-81-5 Aroclor-1260
PCB Certifieate of Analysts
Sample Summary
Date Collected 1210512007 1200
Dute Received 120712007 0930 Client LANL008
Method SW84ti8082
In8t EC02Al
Analyst JXM Aliquot 29911 Column lCLPl
2CLP2
Quulitiec Result l1nits ------ U 373 Ij1kg
U 373 uglkg
U 373 ujlkg
U 373 uglkg
U 373 u1kg
950 uglkg
690 uglkg
Page I of 1
Ma[th S
Moistllre 103 Project LANLOO800 SOPRlf GL-oA-E-040 Dilution 1
Inj Vol luI binlll Volume ImL
Level LOW
MDLtrOD PQt1OQ Column shy
124 373
124 373
124 373
124 373
24 373
124 373 2
124 373
Page 232 of 344
-
___
Jilil-IO-UUO U4QPm rrum-tr IA +bUb1i060664 T-78Z P009013 F-443 LU~ fllUllU~ rl~110nal Luoorarory Page I or
SAMPLE COLLECTION LOGFIELD CHAIN OF CUSTODY EVENT ID 198 EVENT NAME CU21-027(a) DP Site Summer]a1l2007
) SAMPLE ID RE21-07-SS93
ASPLANNtP
DATE COLLECfED(MMlDDIVYYV)
TIME COLLECTED (HlIMM)
PRS ID ZHIZ(JI
LOCATIONm ~~11u1 LOCATION TYPE GENpoundRlC
~~v
TOP DEPTH-fIljrid 7
BonOM DEPTH -r i01 FIElJlMTR1X --5- ~~~I
i ~( ~()T COMPOSITETVPpound --
ASCQLLECTpoundll
2 ftro 7
u C bull 2( o h
R- II01d-2S lei( 4b
4 0 ft- 4 0 f 1shy
bull (
MEDIA
SUBmiddotli--shy~w
SAMPLE TECH CODE
FIELD QCTVPE
FIELD PREP
SAMlLtlJSAGE
SCREENIlOlU DESC
AS PLANNED rev
~ lJhlt77
W 11 rJ
~ 1)
amp
amp
INV
A
ASCQLLECTED
(1 h 1- 3 D tC1 A Cd t
1
tY
EXCAVATED YfSte~N--A----------------Ii
COMPOSITpoundnME1NTERVAL WATER FLOWING YES~NA
BOREHOLE YES~A BOREHOLE DECLINATION ___~__ BOREHOLE DIRECTION shy
PRIOnlTY ORD~R CNTNR PRESERVATIVE COLLECTED YIN
SPECIAL INSTRUCTIONS
2
2
1
8082
8290
NMED Explosives list
125MLGLASS
125MLGLASS
250 l1L AMBER GLASS
_ _-_ _shy
Ice
Ice
Ice
V y
L _____ --_ )SAMPLE DESC t Quck I uGrvi- 15~ Gr~v TIImiddotH
SAMPLE COMMENTS
LOCATIONDESC Y-1lt~tLev ~k
shy
~c~~ 4(0 ]n Ie r fr-Dt71 (one) 113 ~r~ 1110 CIir
FIELD SCREENINGIMEASUREMENT RESULTS flO bf-c ygtY1rxi- 0 -0 r31r
f ~ I rf olcJ1f p j tJ~ Ot p17d 7-tdfM
REVIEWED BY (PRINT ___________COLLECT~DBY (pRINT) _ __---Vi shyr shy -
DateffilneDateffime RECEIVED BYRELINQUISHED BY I070 r (Printed Name)
(Signature)
(Printed Name) )C20(Signature) Jo~~
RECEIVED BY Datetrime
I (Printed Name)
DateITimeRELINQUISHED BY
(Printed N arne)
(Signature)(Signature)
I I
I
I
CL
cYgt
shy
u Sample ill RE21-07-5893 (Q
Client Data = Los Alamoo National Laboratory 0amp-347 S-Dee-07 0830
Samlc Data
Malrix Soil Sample Size t 13 g
middotSolids 894
shycgt
cgt
Name Project Date Collected Time Collected
co I Analyte Cone (pglg) DL a EWCb Qualifierst-
2378-TCDD 12378-PeCDD
l23478-HxCDD
123678-HxCDD
ltJgt CO Cgt 123789-HxCDDUgt cgt lt0 LO
1234678-HpCDD = In + OeDD
2378-TCDF
12378-PeCDF 23478-PeCDF
123478-HxCDF 12367 8-HxC DF
23 467amp-HxCDF
123789middotHxCDF
1234678-HpCDF 1234789-HpCDF
aCDF
Totals
0599 322
63amp
379
16l
1320
15200 0302
0503 L4J
492
382
692
129 [52
142
503
423
279 259 2790
643
276
205
726
435
284
699
J
I J
J B
B
EPA lVlcthod 8290
labontoa Data
Lab Sample 30042~OOl Dare Reeeind 7-Dec-07 QC Batch No 9763 Date ExlIllc[ltd 1O-Dec-07 Dale Analyzed DB-5 13-Dee-07 [)ate Analyzrd DB-225 NA
_shy
Labeled Standard R LeL-UCLd Qualifiers _ shy
IS t3C-2J78-TCDD 898 4) - 13S 13C-[2J7S-PeCDD 916 40 - 135 13C-l23478-HxCDD 935 40- 135 13C-l236 78-HltCD 0 816 40 - 135
lJC-l234678-HpCDD 104shy 40 shy 135 13C-OCDD 122 40 shy l35 13C-2378-TCDF 100 40 - 135 llC-l 2378- PeC DF [04 40- 135 13C-23478-PeCDF 109 40- fJ5 [3C-I2JA78-HKCDF 914 40 - 135
l3C- 123678-HxCDF 792 4() - lJ5 l3C-234678-HxCDP 842 40 shy 135
13C-l23789-HxCDF 9l2 40- 135 [3C-1234678-HpCDF 847 40 shy [35
13C-1234789-HpCDF 991 40 - DS L3C-QCDF 985 40 shy 135
CRS 37Cl-2378-TCDD 936 40 shy 135 eTodc Equivalent Qnotient (fEQ) Data
-lt t-CL UJ
I E o ~
LL
E n
lt0
cgt agt lt=gt cgt
I tn
I c
TotalrCDD
Total PeCDD Total HxCDD Total HpCDD Total TCDF Total PeCDF Total HxCDF
Tota[ HpCDF
Anal~st MAS
P
P
P BP
TEQ(Min) 413
a Sample specific etimated detection j iInil
b Eslilnated maximum possible cQfcenlfatioll
c Method detec1iol1lirniL
d Lo1r~oltrollimil- uppNcolltrollimit
e 7EQ based an (1989) [nternatiooal roxie EquiaIent Filltturs (ITEn
The fltlltl-Wll are repooed in dry weighl The sam pIe size is rej)lJrtild in wltt weight
AwrovedBy Martha M Maier lJ-Dec-2007 1527
T-782 P 011013 F-443Jilll-IO-UUO U4 opm rrom-II III +5056060864
1 High Explosives Analysls Data Sheet
I CalNo 118-96-7
I 121~14-2 Irshy 121-82-4
19406-51-0
2691-41middot0
35572~7g2
479-45-8
606middot20middot2 78-11-5
88-72-2
98-95-3
99-08-1 -~
9935-4
99middot65middot0 f
99w99-0l
Lab Name General Engineering Lahorarcries Client Sample ID RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sample ID 198941001
Moistm-e 103Sample Amount pound
Amoullt Units l Date Received 07~DECmiddot07
Extl8ction Type Sonicatioll Extraction Batch In 709399
COllcenhated Extlllct Volume (UlL) ill Dale Extracted 12middotDEC-07
PllutlOll Facto ~ Injection Volume CuLl ~
Date Analyzed 1H)EC-07 1529GEL (lata tJle EXP12l20S7a
Units ugJkg __ n _
ComJound Concentration -Q]- - 500246-Trinitrotoh Hme 1 U I
~ 24middotDinitrotolu~ene SOD I U
Rl)X 500 I u1 4-Amino-26dinibmiddoto l) illene 500 r-u-
HMX
2-Amino-46-dinitro ojuelle
Tetryl
I 26-Dlllltrotolul~ ~ lUi middot-------~------~----~-----~--t
a
PElN 1000 U wNitrotoluellc
500 ~-1 Nitrobenzen 500 I U
i m-NitrotolUefle SOD I u 135-Tdnitrober zelle 500 I U
ffi-Dinitrobenzi ne 1 500 lUi p-Nitrotoluel1e 500 I U
____ ___-l_____ _ __ ___ L___~ - ~
_ soo U
500 U -i 500 U
-J
-----~~------------ ----- shy Concentration
Instnment X ConcenUllred Extract Volume X Dilutioll Value Samele ArnouD Factor
Page of 2
Page 93 of344
Jan-IO-UU~ U4pm Irom-t IAll +5056060864 T-782 P012013 F-443
1 High Explosives Analysis DII tn Sheet
Lab Name Qeneml Engineering Laboratories Client Sample llgt RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sam)Je lD 198947001
Moisture 103Sample Amount 2
Date Received 07-DEC-07Amount Unitli g
Extmction Type Sonication Extractiou Batch ID 709399
Concentrated Extract Volume (mL) 12 Date Extracted 12-DECmiddot07
Dilution Fact6r Injection Volume (uL) 50
Date Analyzed 17middotDECmiddot07 1903 GEL data file EXS12 17035wiff
Units ugkg
Cas No 3058middot386
59229-7S-3
Compound TATB
26-Diminc-4-nitI
- shy --- Concentnnkm -~T-0-1 1000 -~
2000 1u 618middot87-1 3SmiddotDinitroaniIinc 1000 U
6629--29-4
78-30-8
24Dlamlno-6-iroii~n-trls(o-cresyl) phosphate _~___~ bull -
- ] 2000 U bull
1000 U -1I __bullbull_ bullbullbull___ ~_________ I--_~ I
-~-------- ---shyConcenlrarion
IloSlfllmem X Concanrated Etracr Volllrne Dilution L Value ~__~ Sample Amoun X Factor
Page 2 of 2
Page 96 of344
-
II-IO-UUC Uflpm rrom-cr 111pound I +5056060864 T-782 P013013 F-443
GE~ Inboratories LLe Report Date December 15 2007
SDGNuwber 08-348 Lab Sample ill 198947001
CilelltID REZT-Ol-S893
)llltch fI) 10954l
RunDllte 1211412007 0149
Prep Date 121102007 1953
DlItli FIle 049f4901d
049b49111d
CAS No Fucmname --shy
12674-Il-2 Aruclor-l 0 16
11104-28-2 Arocior-1221
11141-16-5 AroelOr- 1232
53469-21-9 Aroclor-1242
12672-29-6 Aroclor-1248
11097-69-1 Aroclor-1254
11096-81-5 Aroclor-1260
PCB Certifieate of Analysts
Sample Summary
Date Collected 1210512007 1200
Dute Received 120712007 0930 Client LANL008
Method SW84ti8082
In8t EC02Al
Analyst JXM Aliquot 29911 Column lCLPl
2CLP2
Quulitiec Result l1nits ------ U 373 Ij1kg
U 373 uglkg
U 373 ujlkg
U 373 uglkg
U 373 u1kg
950 uglkg
690 uglkg
Page I of 1
Ma[th S
Moistllre 103 Project LANLOO800 SOPRlf GL-oA-E-040 Dilution 1
Inj Vol luI binlll Volume ImL
Level LOW
MDLtrOD PQt1OQ Column shy
124 373
124 373
124 373
124 373
24 373
124 373 2
124 373
Page 232 of 344
-
I
CL
cYgt
shy
u Sample ill RE21-07-5893 (Q
Client Data = Los Alamoo National Laboratory 0amp-347 S-Dee-07 0830
Samlc Data
Malrix Soil Sample Size t 13 g
middotSolids 894
shycgt
cgt
Name Project Date Collected Time Collected
co I Analyte Cone (pglg) DL a EWCb Qualifierst-
2378-TCDD 12378-PeCDD
l23478-HxCDD
123678-HxCDD
ltJgt CO Cgt 123789-HxCDDUgt cgt lt0 LO
1234678-HpCDD = In + OeDD
2378-TCDF
12378-PeCDF 23478-PeCDF
123478-HxCDF 12367 8-HxC DF
23 467amp-HxCDF
123789middotHxCDF
1234678-HpCDF 1234789-HpCDF
aCDF
Totals
0599 322
63amp
379
16l
1320
15200 0302
0503 L4J
492
382
692
129 [52
142
503
423
279 259 2790
643
276
205
726
435
284
699
J
I J
J B
B
EPA lVlcthod 8290
labontoa Data
Lab Sample 30042~OOl Dare Reeeind 7-Dec-07 QC Batch No 9763 Date ExlIllc[ltd 1O-Dec-07 Dale Analyzed DB-5 13-Dee-07 [)ate Analyzrd DB-225 NA
_shy
Labeled Standard R LeL-UCLd Qualifiers _ shy
IS t3C-2J78-TCDD 898 4) - 13S 13C-[2J7S-PeCDD 916 40 - 135 13C-l23478-HxCDD 935 40- 135 13C-l236 78-HltCD 0 816 40 - 135
lJC-l234678-HpCDD 104shy 40 shy 135 13C-OCDD 122 40 shy l35 13C-2378-TCDF 100 40 - 135 llC-l 2378- PeC DF [04 40- 135 13C-23478-PeCDF 109 40- fJ5 [3C-I2JA78-HKCDF 914 40 - 135
l3C- 123678-HxCDF 792 4() - lJ5 l3C-234678-HxCDP 842 40 shy 135
13C-l23789-HxCDF 9l2 40- 135 [3C-1234678-HpCDF 847 40 shy [35
13C-1234789-HpCDF 991 40 - DS L3C-QCDF 985 40 shy 135
CRS 37Cl-2378-TCDD 936 40 shy 135 eTodc Equivalent Qnotient (fEQ) Data
-lt t-CL UJ
I E o ~
LL
E n
lt0
cgt agt lt=gt cgt
I tn
I c
TotalrCDD
Total PeCDD Total HxCDD Total HpCDD Total TCDF Total PeCDF Total HxCDF
Tota[ HpCDF
Anal~st MAS
P
P
P BP
TEQ(Min) 413
a Sample specific etimated detection j iInil
b Eslilnated maximum possible cQfcenlfatioll
c Method detec1iol1lirniL
d Lo1r~oltrollimil- uppNcolltrollimit
e 7EQ based an (1989) [nternatiooal roxie EquiaIent Filltturs (ITEn
The fltlltl-Wll are repooed in dry weighl The sam pIe size is rej)lJrtild in wltt weight
AwrovedBy Martha M Maier lJ-Dec-2007 1527
T-782 P 011013 F-443Jilll-IO-UUO U4 opm rrom-II III +5056060864
1 High Explosives Analysls Data Sheet
I CalNo 118-96-7
I 121~14-2 Irshy 121-82-4
19406-51-0
2691-41middot0
35572~7g2
479-45-8
606middot20middot2 78-11-5
88-72-2
98-95-3
99-08-1 -~
9935-4
99middot65middot0 f
99w99-0l
Lab Name General Engineering Lahorarcries Client Sample ID RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sample ID 198941001
Moistm-e 103Sample Amount pound
Amoullt Units l Date Received 07~DECmiddot07
Extl8ction Type Sonicatioll Extraction Batch In 709399
COllcenhated Extlllct Volume (UlL) ill Dale Extracted 12middotDEC-07
PllutlOll Facto ~ Injection Volume CuLl ~
Date Analyzed 1H)EC-07 1529GEL (lata tJle EXP12l20S7a
Units ugJkg __ n _
ComJound Concentration -Q]- - 500246-Trinitrotoh Hme 1 U I
~ 24middotDinitrotolu~ene SOD I U
Rl)X 500 I u1 4-Amino-26dinibmiddoto l) illene 500 r-u-
HMX
2-Amino-46-dinitro ojuelle
Tetryl
I 26-Dlllltrotolul~ ~ lUi middot-------~------~----~-----~--t
a
PElN 1000 U wNitrotoluellc
500 ~-1 Nitrobenzen 500 I U
i m-NitrotolUefle SOD I u 135-Tdnitrober zelle 500 I U
ffi-Dinitrobenzi ne 1 500 lUi p-Nitrotoluel1e 500 I U
____ ___-l_____ _ __ ___ L___~ - ~
_ soo U
500 U -i 500 U
-J
-----~~------------ ----- shy Concentration
Instnment X ConcenUllred Extract Volume X Dilutioll Value Samele ArnouD Factor
Page of 2
Page 93 of344
Jan-IO-UU~ U4pm Irom-t IAll +5056060864 T-782 P012013 F-443
1 High Explosives Analysis DII tn Sheet
Lab Name Qeneml Engineering Laboratories Client Sample llgt RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sam)Je lD 198947001
Moisture 103Sample Amount 2
Date Received 07-DEC-07Amount Unitli g
Extmction Type Sonication Extractiou Batch ID 709399
Concentrated Extract Volume (mL) 12 Date Extracted 12-DECmiddot07
Dilution Fact6r Injection Volume (uL) 50
Date Analyzed 17middotDECmiddot07 1903 GEL data file EXS12 17035wiff
Units ugkg
Cas No 3058middot386
59229-7S-3
Compound TATB
26-Diminc-4-nitI
- shy --- Concentnnkm -~T-0-1 1000 -~
2000 1u 618middot87-1 3SmiddotDinitroaniIinc 1000 U
6629--29-4
78-30-8
24Dlamlno-6-iroii~n-trls(o-cresyl) phosphate _~___~ bull -
- ] 2000 U bull
1000 U -1I __bullbull_ bullbullbull___ ~_________ I--_~ I
-~-------- ---shyConcenlrarion
IloSlfllmem X Concanrated Etracr Volllrne Dilution L Value ~__~ Sample Amoun X Factor
Page 2 of 2
Page 96 of344
-
II-IO-UUC Uflpm rrom-cr 111pound I +5056060864 T-782 P013013 F-443
GE~ Inboratories LLe Report Date December 15 2007
SDGNuwber 08-348 Lab Sample ill 198947001
CilelltID REZT-Ol-S893
)llltch fI) 10954l
RunDllte 1211412007 0149
Prep Date 121102007 1953
DlItli FIle 049f4901d
049b49111d
CAS No Fucmname --shy
12674-Il-2 Aruclor-l 0 16
11104-28-2 Arocior-1221
11141-16-5 AroelOr- 1232
53469-21-9 Aroclor-1242
12672-29-6 Aroclor-1248
11097-69-1 Aroclor-1254
11096-81-5 Aroclor-1260
PCB Certifieate of Analysts
Sample Summary
Date Collected 1210512007 1200
Dute Received 120712007 0930 Client LANL008
Method SW84ti8082
In8t EC02Al
Analyst JXM Aliquot 29911 Column lCLPl
2CLP2
Quulitiec Result l1nits ------ U 373 Ij1kg
U 373 uglkg
U 373 ujlkg
U 373 uglkg
U 373 u1kg
950 uglkg
690 uglkg
Page I of 1
Ma[th S
Moistllre 103 Project LANLOO800 SOPRlf GL-oA-E-040 Dilution 1
Inj Vol luI binlll Volume ImL
Level LOW
MDLtrOD PQt1OQ Column shy
124 373
124 373
124 373
124 373
24 373
124 373 2
124 373
Page 232 of 344
-
T-782 P 011013 F-443Jilll-IO-UUO U4 opm rrom-II III +5056060864
1 High Explosives Analysls Data Sheet
I CalNo 118-96-7
I 121~14-2 Irshy 121-82-4
19406-51-0
2691-41middot0
35572~7g2
479-45-8
606middot20middot2 78-11-5
88-72-2
98-95-3
99-08-1 -~
9935-4
99middot65middot0 f
99w99-0l
Lab Name General Engineering Lahorarcries Client Sample ID RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sample ID 198941001
Moistm-e 103Sample Amount pound
Amoullt Units l Date Received 07~DECmiddot07
Extl8ction Type Sonicatioll Extraction Batch In 709399
COllcenhated Extlllct Volume (UlL) ill Dale Extracted 12middotDEC-07
PllutlOll Facto ~ Injection Volume CuLl ~
Date Analyzed 1H)EC-07 1529GEL (lata tJle EXP12l20S7a
Units ugJkg __ n _
ComJound Concentration -Q]- - 500246-Trinitrotoh Hme 1 U I
~ 24middotDinitrotolu~ene SOD I U
Rl)X 500 I u1 4-Amino-26dinibmiddoto l) illene 500 r-u-
HMX
2-Amino-46-dinitro ojuelle
Tetryl
I 26-Dlllltrotolul~ ~ lUi middot-------~------~----~-----~--t
a
PElN 1000 U wNitrotoluellc
500 ~-1 Nitrobenzen 500 I U
i m-NitrotolUefle SOD I u 135-Tdnitrober zelle 500 I U
ffi-Dinitrobenzi ne 1 500 lUi p-Nitrotoluel1e 500 I U
____ ___-l_____ _ __ ___ L___~ - ~
_ soo U
500 U -i 500 U
-J
-----~~------------ ----- shy Concentration
Instnment X ConcenUllred Extract Volume X Dilutioll Value Samele ArnouD Factor
Page of 2
Page 93 of344
Jan-IO-UU~ U4pm Irom-t IAll +5056060864 T-782 P012013 F-443
1 High Explosives Analysis DII tn Sheet
Lab Name Qeneml Engineering Laboratories Client Sample llgt RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sam)Je lD 198947001
Moisture 103Sample Amount 2
Date Received 07-DEC-07Amount Unitli g
Extmction Type Sonication Extractiou Batch ID 709399
Concentrated Extract Volume (mL) 12 Date Extracted 12-DECmiddot07
Dilution Fact6r Injection Volume (uL) 50
Date Analyzed 17middotDECmiddot07 1903 GEL data file EXS12 17035wiff
Units ugkg
Cas No 3058middot386
59229-7S-3
Compound TATB
26-Diminc-4-nitI
- shy --- Concentnnkm -~T-0-1 1000 -~
2000 1u 618middot87-1 3SmiddotDinitroaniIinc 1000 U
6629--29-4
78-30-8
24Dlamlno-6-iroii~n-trls(o-cresyl) phosphate _~___~ bull -
- ] 2000 U bull
1000 U -1I __bullbull_ bullbullbull___ ~_________ I--_~ I
-~-------- ---shyConcenlrarion
IloSlfllmem X Concanrated Etracr Volllrne Dilution L Value ~__~ Sample Amoun X Factor
Page 2 of 2
Page 96 of344
-
II-IO-UUC Uflpm rrom-cr 111pound I +5056060864 T-782 P013013 F-443
GE~ Inboratories LLe Report Date December 15 2007
SDGNuwber 08-348 Lab Sample ill 198947001
CilelltID REZT-Ol-S893
)llltch fI) 10954l
RunDllte 1211412007 0149
Prep Date 121102007 1953
DlItli FIle 049f4901d
049b49111d
CAS No Fucmname --shy
12674-Il-2 Aruclor-l 0 16
11104-28-2 Arocior-1221
11141-16-5 AroelOr- 1232
53469-21-9 Aroclor-1242
12672-29-6 Aroclor-1248
11097-69-1 Aroclor-1254
11096-81-5 Aroclor-1260
PCB Certifieate of Analysts
Sample Summary
Date Collected 1210512007 1200
Dute Received 120712007 0930 Client LANL008
Method SW84ti8082
In8t EC02Al
Analyst JXM Aliquot 29911 Column lCLPl
2CLP2
Quulitiec Result l1nits ------ U 373 Ij1kg
U 373 uglkg
U 373 ujlkg
U 373 uglkg
U 373 u1kg
950 uglkg
690 uglkg
Page I of 1
Ma[th S
Moistllre 103 Project LANLOO800 SOPRlf GL-oA-E-040 Dilution 1
Inj Vol luI binlll Volume ImL
Level LOW
MDLtrOD PQt1OQ Column shy
124 373
124 373
124 373
124 373
24 373
124 373 2
124 373
Page 232 of 344
-
Jan-IO-UU~ U4pm Irom-t IAll +5056060864 T-782 P012013 F-443
1 High Explosives Analysis DII tn Sheet
Lab Name Qeneml Engineering Laboratories Client Sample llgt RE21-07-5893
Lab Code GEL GEL Job No (SDG) ~
Matrix SOIL GEL Sam)Je lD 198947001
Moisture 103Sample Amount 2
Date Received 07-DEC-07Amount Unitli g
Extmction Type Sonication Extractiou Batch ID 709399
Concentrated Extract Volume (mL) 12 Date Extracted 12-DECmiddot07
Dilution Fact6r Injection Volume (uL) 50
Date Analyzed 17middotDECmiddot07 1903 GEL data file EXS12 17035wiff
Units ugkg
Cas No 3058middot386
59229-7S-3
Compound TATB
26-Diminc-4-nitI
- shy --- Concentnnkm -~T-0-1 1000 -~
2000 1u 618middot87-1 3SmiddotDinitroaniIinc 1000 U
6629--29-4
78-30-8
24Dlamlno-6-iroii~n-trls(o-cresyl) phosphate _~___~ bull -
- ] 2000 U bull
1000 U -1I __bullbull_ bullbullbull___ ~_________ I--_~ I
-~-------- ---shyConcenlrarion
IloSlfllmem X Concanrated Etracr Volllrne Dilution L Value ~__~ Sample Amoun X Factor
Page 2 of 2
Page 96 of344
-
II-IO-UUC Uflpm rrom-cr 111pound I +5056060864 T-782 P013013 F-443
GE~ Inboratories LLe Report Date December 15 2007
SDGNuwber 08-348 Lab Sample ill 198947001
CilelltID REZT-Ol-S893
)llltch fI) 10954l
RunDllte 1211412007 0149
Prep Date 121102007 1953
DlItli FIle 049f4901d
049b49111d
CAS No Fucmname --shy
12674-Il-2 Aruclor-l 0 16
11104-28-2 Arocior-1221
11141-16-5 AroelOr- 1232
53469-21-9 Aroclor-1242
12672-29-6 Aroclor-1248
11097-69-1 Aroclor-1254
11096-81-5 Aroclor-1260
PCB Certifieate of Analysts
Sample Summary
Date Collected 1210512007 1200
Dute Received 120712007 0930 Client LANL008
Method SW84ti8082
In8t EC02Al
Analyst JXM Aliquot 29911 Column lCLPl
2CLP2
Quulitiec Result l1nits ------ U 373 Ij1kg
U 373 uglkg
U 373 ujlkg
U 373 uglkg
U 373 u1kg
950 uglkg
690 uglkg
Page I of 1
Ma[th S
Moistllre 103 Project LANLOO800 SOPRlf GL-oA-E-040 Dilution 1
Inj Vol luI binlll Volume ImL
Level LOW
MDLtrOD PQt1OQ Column shy
124 373
124 373
124 373
124 373
24 373
124 373 2
124 373
Page 232 of 344
-
II-IO-UUC Uflpm rrom-cr 111pound I +5056060864 T-782 P013013 F-443
GE~ Inboratories LLe Report Date December 15 2007
SDGNuwber 08-348 Lab Sample ill 198947001
CilelltID REZT-Ol-S893
)llltch fI) 10954l
RunDllte 1211412007 0149
Prep Date 121102007 1953
DlItli FIle 049f4901d
049b49111d
CAS No Fucmname --shy
12674-Il-2 Aruclor-l 0 16
11104-28-2 Arocior-1221
11141-16-5 AroelOr- 1232
53469-21-9 Aroclor-1242
12672-29-6 Aroclor-1248
11097-69-1 Aroclor-1254
11096-81-5 Aroclor-1260
PCB Certifieate of Analysts
Sample Summary
Date Collected 1210512007 1200
Dute Received 120712007 0930 Client LANL008
Method SW84ti8082
In8t EC02Al
Analyst JXM Aliquot 29911 Column lCLPl
2CLP2
Quulitiec Result l1nits ------ U 373 Ij1kg
U 373 uglkg
U 373 ujlkg
U 373 uglkg
U 373 u1kg
950 uglkg
690 uglkg
Page I of 1
Ma[th S
Moistllre 103 Project LANLOO800 SOPRlf GL-oA-E-040 Dilution 1
Inj Vol luI binlll Volume ImL
Level LOW
MDLtrOD PQt1OQ Column shy
124 373
124 373
124 373
124 373
24 373
124 373 2
124 373
Page 232 of 344
-
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