5973install - Agilent · 32 2 ci ci ci msd hp 5973 msd pci/nci (g1999-90001) 1 ci msd ci 57 2 pci...

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5973

1998

Microsoft® Windows NT®

G1099-97006

, 5/99

LpA << 70 dB

HP 5973 MSD10

CI

10HP

(1234-1234)(12345-

12345)

HP

HP

HP 5973(MSD) I IEC 1010-1

MSD

MSD

X

Z

H

P

3

, 6, 8, 9

, 9, 9, 9, 10

, 10, 13

, 16, 17

GC , 18MSD , 22

CI MSD , 26MSD , 28GC, MSD, , 29EI , 30EI CI , 31

CI , 32, 34

, 36, 41

4

1

67913

6

HP 5973 HP

HP 5973 MSD

HP G1098A — HP 5973 MSD(“ MSD”)

HP G1099A — HP 5973 MSD(“ MSD”)

HP G1999A — PCI/NCI HP 5973 MSD(“CI MSD”)

HP 6890 Plus GC #112 #201HP 7683(

• PC MSD

MSD

1

7

HP 7983 ALS

HP 7983 ALS

HP 6890 GC

HP 5973 MSD

HP 7983 ALS

HP 7983 ALS

HP 6890 GC

CI

HP 5973 CI MSD

HP 5973 CI MSD

HP 5973 MSD

8

1

HP

• PCI/NCIMS D

• CI MSD

• /

• CI

• HP 6890

1

9

MSD GCMSD 1

30

MSD HPMSD

MSD 1

15° C – 35°C ( ±2° C ) -20° C – 70°C

15 % -9 565 °C 90% 24

4.6 km (15,000 ft)4.6km ( 15,000ft)

10

1

MSD IEC

( MSD )

120 220–240 +5%, -10% 47.5–63 Hz ,900 V400VAIEC (Overvoltag eCategory) IIIEC 2

GC

99.999%GC GC

GC

GC/ MS GC MSD

1

11

1

(cm) (cm) (cm) (Kg) (Volt-Amps) (KJoules/hr)

HP 5973 MSD

MSD 40.6 29.8 54 36.3 900 3,164

MSD 40.6 29.8 54 41 900 3,164

PCI/NCI MSD 40.6 30.3 54 44 900 3,164

HP 6890 Plus GC 50 58.5 50 50 2,250 8,100

--- --- --- --- 2,950 10,620

HP 6890 ALSHP 7683

GC 44 --- --- --- --- ---

HP 7683GC 30.3 --- --- --- --- ---

(inches) (inches) (inches) (pounds) (Volt-Amps) (Btu/hr)

HP 5973 MSD

MSD 16.0 11.75 21.25 80 900 3,000

MSD 16.0 11.75 21.25 90 900 3,000

PCI/NCI MSD 16 12 21.25 97 900 3,000

HP 6890 GC 21 23 21 110 2,250 7,681

--- --- --- --- 2,950 10,071

HP 6890 ALSHP 7683GC 17 --- --- --- --- ---

HP 7683GC 9 --- --- --- --- ---

12

PCI/NCI M SD

CI HP 5973

Matheson he Swagelok

G1999-8041

1/8

UHP 99.97%3320

J05Swagelok SS-200-7-2

99.53321 3320

J05Swagelok SS-200-7-

99.99%3332

J05Swagelok , SS-200-7-

1

13

• HP 5973MSD• HP MSD

• HP 5973MSD CD-ROM• HP 6890• HP GC• PC• PC• Optimizing splitless injections on your GC for high performance MS

analysis (5091-4587E)

• Hydrogen Carrier Gas Safety G uide (5955-5398)

• Window ® NT 4.0

14

2

17GC 18MSD 22

CI MSD 26MSD 29GC MSD MSD 30EI 31

EI CI 32CI 33

34

16

HP 5973 MSD

MSD

• GC

• MSD

• GC MSD

CI MSD

• /

EI MSD CI

• CI CI

• 2

• CI

• PCI

• NCI

CI MSD EI/CI

CI HP 59864

2

17

HPHP

1

2

3

4

18

2

GC

GC

(5181-8836)

7/16 2 (8710-0806)

GC GC/MS Optimizing splitless injections on your GC for high-performance MS analysis

1 GC

2 GC

GC EPC

3 6

/

/

MSD5955 5398

2

GC

19

4 5 - 8 psi (35 - 55 KPa).

5

6

7 EPC

8 EPC

20

9 GC MSD

10 HP-IB GC HP-IB

11 GC

12 GC GC

GC

13 GC HP-IB 15

GC Options/Communication/HP -IBaddress / 1 5 Enter

14 GC MSD

GC Config/Column1/co lumnpa rameters.: 30 M: 0.25

: HP-5 MS: 19091S-433 MS

15 50 psi

16 7 ml/minute

20

2

GC

17 1

18 Merlin Microseal.

19 250°C.

20 40°C 15°C/ 280°C 1035°C.

21 GC

22

23

24 GC

25

26 GC

27 GC GC/MSD GC

2

GC

21

GC/MSDGC

22

2

MSD

MSD

HP 5973MSD G1099-90001HP 5973MSD G1099-90009HP 5973MSD P CI/NCI G1999-90001

1/4-inch × 5/16-inch 8710-0510HP 5973MSD G1099-60565HP 5973MSD C I G1999-60582

1 MSD

2 MSD

3 MSD

4

5 MSD 990

6 MSD HP 5973 MSD MSD

7

CI MSD

MSDMSD

2

MSD

23

8 HP-IB/MSD HP-IB 20

1 O

ONOFF

N2

345678

MSD

HP-IB

HP-IB

24

2

MSD

9 GC/MSD MS GC

10 GC MSD HP-IB

11 MSD GC

GC/MSD GC CI MSD EI MSD GC

12 GC MSD

CI MSD

13 CI 26

14 HP 59864B (CI MSD )

HP 5973 M SD MSD

15 MSD

HP 6890 GC

HP 5973 MSD

GC/MSDGC

GC/MSDMSD

2

MSD

25

16 MSD

17 GC

18 GC 1.0 ml/min

19 GC/MSD .

CI MSD HP 5973 M SD C I G1999-90001

20 GC/MSD .

MSD CI MSDCI MSD

21 MSD

HP 5973 MSDMSD

MSD

MSD

300 mTorr

100 1

80 5 10

22

26

2

CI MSD

CI MSD

CI MSD HP 5973 M SD P CI/NCI (G1999-90001)

:/ (G1999-80410)

1/8- (7157-0210)Swagelok 1/87/16 (8710-0806)

1 /

2 20psig

3 1/8

4

5

6

7 CI

8 Gas A

Gas A Gas BSwagelok

2

CI MSD

27

9 Gas B

Gas B

Gas B

Gas A

28

2

MSD

MSD

1 PC

2 PC

3 PC

PC

4 HP-IB GC PC

5

6

7 PC

HP-IB

HP-IB

2

GC, MSD

29

GC, MSD

MSD (G1701-90031)

1

2 MS MSD MSD GC

CI MSD

3 Instrument MSD

4 MSD

— View Diagnostics/V a cuumCo ntrol Vacuum Pumpdown

— GC/MSD 280° C.

5 ATUNE.U

— Diagnostics/VacuumCo ntrol DiagnosticsEditMSparams

— MoreParams Temperatures MSD

MS Sourc e:230° CMS Quad : 150°

— OK MS Zones

6

— Prof. .

— Stop MSOff.

— OK Edit Parameters

— MSD 60

7

Fil Save Tune Values

30

2

EI

EI

1 60

2 GC 150°C 1.0 ml/min

3 Instrument Control view Qualify checout Tune

4 Qualify Tune Evaluation

5 OK

1 1 pg/µl 0.001 ppm OFN (8500-5441)

2 1 µl

3 Instrument Control view Qualify Sensitivitiy Check

C:\HPCHEM\1\5973\OFN_SN.M.

4 Instrument | Edit

5 OK

6 RMS 10:1

2

EI CI

31

EI CI

CI MSD HP 5973 MSD PCI/NCI (G1999-90001)

NCI PCI CI MSD

1 MSD MSD CI 38

2

3 EI

4 CI MSD CI 46

5

6 MSD MSD CI 40

7 MSD

8 MSD CI 52

9 MSD 54

10 m/z 32 m/z 19 m/z 17

HP 5973 MSD 98

32

2

CI

CI

CI MSD HP 5973 MSD PCI/NCI (G1999-90001)

1 CI MSD CI 57

2 PCI MSD CI 59

MS 75:1.

3 CI MSD 58

4 CI MSD CI 60

RMS 500:1.

CI

2

33

CI MSD

• CI CIPFDTD

• NCI

CI CICI 40

• NCI

NCI

• PCI PFDT PCINH3.U.

• .

• HP5973 MSD CI

34

3

3640

36

3

HP

.

.

DM

/

3

37

GC

GCGC

5 - 8 psi (35 - 55 KPa) GCHP-IB MSD

GCGCGC

GC HP-IB 15

50 psi (34 5KPa)7 ml /min

Merlin Microsea250° C

15° C /min 4 0 °C 280° C 10GC

GCALS

GC GC/MSDGC

38

3

MSD

MSDMSD

990MSD

GC/MSDMSD HP-IB 20GC MSD HP-I

/ CI MSDCI MSD

HP 59864B CI MSDAC MSD

MSD ACGC

GC 1.0 ml /minGC/MSD

MSD

60

MSD

PCPCGC PC HP-IB

PC

GC MSD

MS Confi MSD GCinstrument MSD

Edit MS Param Profile Scan

3

39

EI CI

MSDEICI

MSD 2CI

CI

PCIPCI

NCINCI

HP 5973 MSD

EI S/N (RMS)

PCI S/N (RMS)

NCI S/N (RMS)

40

3

• HP

—PC Windo w s N T 4 .0 Window

—MSD PC

— deuser.mac

— US EPA

3

41

MSDCI MSD

ALS

PC

PCWindows N T 4 .0MSD

EI CI CI MSD

MSD

MSD

42

3

OFN_SN.M, GC MSScan SIM

Snapshot

TIC

TIC

ESTD ISTD

MSD

HPCHEM

3

43

GCMSD

MSD Reference Collection CD

Qualif yTune charts

HPHP—

/

/

44

MSD

MSD

+5% -10%IEC664

Category II

MSD

MSD

MSDMSD

HP 59555398

G1099-970061998

1999 6

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