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Microalloyed Steels Conference 2005 held in San Sebastian
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Microalloying for New Steel Processes and Applications, September 7-9, 2005, Donostia-San Sebastián
Optimization of Rolling Conditions in Nb Microalloyed Steels Processed by Thin Slab
Casting and Direct Rolling Route: Processing Maps
P. Uranga, A.I. Fernández, B. López and J.M. Rodriguez-Ibabe
CEIT and tecnun (University of Navarra)Donostia-San SebastiánBasque Country, Spain
Objective• Definition of Optimal Processing Conditions
for different grades under a wide variety of Industrial Rolling Conditions
• Special attention to:
– Avoidance of microstructural heterogeneities in thick plates and high levels of microalloying additions
– Conditioning of austenite structure prior to transformation
Procedure
• Classical approach:– Not enough to predict heterogeneities
• New model:– Particular characteristics of TSDR Technology
• Initial As-cast Structure• Specific Thermomechanical Deformation
Route• Processing Maps:
– Suitable for visual understanding
ModelDescription
• Main difference:– Expansion of Classical Microstructural
Modeling to Grain Size Distributions• Input:
– Grain Size Distribution measured in a real Thin Slab
• Output:– Recrystallized and Unrecrystallized Grain
Size histograms and Retained Strain
D
3-D
Freq
uenc
y
[d0] i
[fv] i
kpth interval np1 … …
......
Rex Unrex...
Final MicrostructureHistograms
Recrystallized Fraction Unrecrystallized Fraction
Grain Size
Are
a Fr
actio
n
Grain Size
Are
a Fr
actio
n
[ ]ird [ ]iud [ ]iX
pth rollingpass
[ ]iX
1− [ ]ir ε
Rex Unrex
1st rollingpass
i1th interval n11 … …
......, , ,
Log-normal Distribution
[drex] i
Freq
uenc
y
D
D
3-D
Freq
uenc
y
[d0] i
[fv] i
kpth interval np1 … …
......
Rex Unrex...
Final MicrostructureHistograms
Recrystallized Fraction Unrecrystallized Fraction
Grain Size
Are
a Fr
actio
n
Grain Size
Are
a Fr
actio
n
[ ]ird [ ]iud [ ]iX
pth rollingpass
[ ]iX
1− [ ]ir ε
Rex Unrex
1st rollingpass
i1th interval n11 … …
......, , ,
Log-normal Distribution
[drex] i
Freq
uenc
y
D
D
3-D
Freq
uenc
y
[d0] i
[fv] i
kpth interval np1 … …
......
Rex Unrex...
Final MicrostructureHistograms
Recrystallized Fraction Unrecrystallized Fraction
Grain Size
Are
a Fr
actio
n
Grain Size
Are
a Fr
actio
n
[ ]ird [ ]iud [ ]iX
pth rollingpass
[ ]iX
1− [ ]ir ε
Rex Unrex
1st rollingpass
i1th interval n11 … …
......, , ,
Log-normal Distribution
[drex] i
Freq
uenc
y
D
D
3-D
Freq
uenc
y
[d0] i
[fv] i
kpth interval np1 … …
......
Rex Unrex...
Final MicrostructureHistograms
Recrystallized Fraction Unrecrystallized Fraction
Grain Size
Are
a Fr
actio
n
Grain Size
Are
a Fr
actio
n
[ ]ird [ ]iud [ ]iX
pth rollingpass
[ ]iX
1− [ ]ir ε
Rex Unrex
1st rollingpass
i1th interval n11 … …
......, , ,
Log-normal Distribution
[drex] i
Freq
uenc
y
D
Rolling Simulations
• 0.035% Nb Microalloyed Steel (0.06%C, 0.008%N, 1.1%Mn)
• Initial thickness: 55 mm
• Final thicknesses: 1.5 to 12.65 mm
• Rolling entry temperatures: 1040 to 1100ºC
• Interpass times: function of strain-rates
• Final cooling rate: 20ºC/s to 800ºC
RollingSchedules
• Large reductions during first passes
e (mm)Pass no. Strain Rate tip Strain Rate tip
1 0.7 5 6 0.5 5 6 352 0.7 10 4 0.5 10 4 303 0.55 15 3 0.45 15 5 304 0.45 30 2.1 ⎯ ⎯ ⎯ 305 0.35 50 1.8 0.3 20 2.7 306 0.25 70 0.25 25 ⎯
4 10 ΔT
SimulationResults
• Final Austenite Microstructure
0.0
0.1
0.2
0.3
0.4
0.5
10 30 50 70 90 MoreAustenite Grain Size (μm)
Are
a Fr
actio
n
Ti = 1100ºC
e = 4 mm
0.0
0.1
0.2
0.3
0.4
0.5
10 30 50 70 90 MoreAustenite Grain Size (μm)
Are
a Fr
actio
n
Ti = 1040ºCTi = 1100ºC
e = 4 mm
0.0
0.1
0.2
0.3
0.4
0.5
10 30 50 70 90 MoreAustenite Grain Size (μm)
Are
a Fr
actio
n
Ti = 1100ºC
e = 10 mm
0.0
0.1
0.2
0.3
0.4
0.5
10 30 50 70 90 MoreAustenite Grain Size (μm)
Are
a Fr
actio
n
Ti = 1040°CTi = 1100ºC
e = 10 mmDmean= 9 μm
Dmean= 15 μmDmean= 16 μm
Dmean= 21 μm
ParameterDefinition
• Histograms not very useful when analyzing wide spread of conditions and/or materials
• General parameters defined:– Dmean
– Dmax
– Dc (10% of the volume fraction of grains have a bigger size than Dc)
– ZD (=Dmax/Dmean)
Parameter Evolution
• e = 4 mm: Homogeneous Structure. ZD < 8
• e = 10 mm: Microstructural Heterogeneities. ZD > 8
Entry Rolling Temperature: 1040ºC
0
200
400
600
800
1000
1200
1400
1600
1 2 3 4 5 6Interstand
Gra
in S
ize
( μm
)
0
2
4
6
8
10
12
14
ZD P
aram
eter
DmeanDcDmaxZD
e = 4 mmTi = 1040ºC
0
200
400
600
800
1000
1200
1400
1600
1 2 3 4 5 6Interstand
Gra
in S
ize
( μm
)0
2
4
6
8
10
12
14
ZD P
aram
eter
DmeanDcDmaxZD
e = 10 mmTi = 1040ºC
Effect of thefinal gauge thickness
• Dmean
– Strain ↑: Dmean↓– Ti ↑: Dmean ↑
• Heterogeneities unrevealed
Final thickness (mm)
12.65 7 6 4 3 1.5210
0
5
10
15
20
25
30
1 2 3 4 5Total Strain
Mea
n A
uste
nite
Gra
in S
ize
( μm
)
Ti = 1100°CTi = 1040°C
a) Dmean
Effect of thefinal gauge thickness
• Dc
– Strain ↑: Dc↓– Ti ↑: Dc ↑
Final thickness (mm)
12.65 7 6 4 3 1.5210
0
20
40
60
80
1 2 3 4 5Total Strain
Dc
Aus
teni
te G
rain
Siz
e ( μ
m)
Ti = 1100°CTi = 1040°C
b) Dc
• 1040ºC: sharp increase for low strains and low Ti
Effect of thefinal gauge thickness
• ZD– Ti ↑: ZD constant– Strain ↓ and Ti ↓ :
ZD ↑• Heterogeneities
revealed
Final thickness (mm)
12.65 7 6 4 3 1.5210
0
5
10
15
20
25
1 2 3 4 5
Total Strain
ZD P
aram
eter
Ti = 1100°CTi = 1040°C
c) ZD
Processing Maps
• Dc isoclines combined with Processing Regions
2 2.5 3 3.5 41040
1050
1060
1070
1080
1090
1100
202525
3030
3035
35
35 35
4040
40
40
50
50
50
60
60
60
70
Final Gauge Thickness (mm)
Total Strain
Rol
ling
Entr
yTe
mpe
ratu
re(º
C)
12.65 7 6 4 3 1.52
Dc
Optimum Processing Zone
10
Residual unrefined
as-castgrains
Processing Maps
• Retained strain isoclines combined with Processing Regions
2 2.5 3 3.5 41040
1050
1060
1070
1080
1090
11000.2
0.2
0.2
0.3
0.30.3
0.30.4
0.4
0.4
0.4
0.50.5
0.50.5
0.6
0.6 0.6 0.60.7 0.70.8
RetainedStrain
Final Gauge Thickness (mm)
Total Strain
Rol
ling
Entr
yTe
mpe
ratu
re(º
C)
12.65 7 6 4 3 1.52
Optimum Processing Zone
10
Residual unrefinedas-castgrains
Processing Maps
• e ≤ 6-7 mm: Dc ↔ Ti relationship.Homogeneous structure.
2 2.5 3 3.5 41040
1050
1060
1070
1080
1090
11000.2
0.2
0.2
0.3
0.30.3
0.30.4
0.4
0.40.4
0.50.5
0.50.5
0.6
0.6 0.6 0.60.7 0.70.8
RetainedStrain
Final Gauge Thickness (mm)
Total Strain
Rol
ling
Entr
yTe
mpe
ratu
re(º
C)
12.65 7 6 4 3 1.52
Optimum Processing Zone
10
Residual unrefinedas-castgrains
2 2.5 3 3.5 41040
1050
1060
1070
1080
1090
1100
2025
25
30
30
30
35
35
35 35
4040
40
40
50
50
50
60
60
60
70
Final Gauge Thickness (mm)
Total Strain
Rol
ling
Entr
yTe
mpe
ratu
re(º
C)
12.65 7 6 4 3 1.52
Dc
Optimum Processing Zone
10
Residual unrefinedas-castgrains
• e > 6-7 mm: Dc independent from Ti. Minimum Ti required to avoid heterogeneities.
Conclusions
• The microstructural evolution during hot rolling of coarse grain sized austenite has been modeled considering all the microstructural reactions that can take place during an industrial TSDR production of a Nbmicroalloyed steel.
• The model is able to predict possible heterogeneities present in the final austenite microstructure before transformation.
• Based on the results obtained with the model, processing maps have been drawn for a 0.035% Nb microalloyed steel, considering the following parameters: initial rolling temperature, total reduction and rolling schedule.
• The influence of the previous parameters on the microstructural refinement and homogeneity has been evaluated. The processing maps have revealed as a very useful tool to define optimum processing conditions in order to exploit all the benefices of the Nb microalloying in thin slab direct rolling
Acknowledgments
• Basque Government• CICYT (MAT2002-01174 project)
• Materials Department - Thermomechanical Treatments Group (CEIT)
• CEIT and tecnun• Carnegie Mellon University and Professor
A.W. Cramb
Microalloying for New Steel Processes and Applications, September 7-9, 2005, Donostia-San Sebastián
Optimization of Rolling Conditions in Nb Microalloyed Steels Processed by Thin Slab
Casting and Direct Rolling Route: Processing Maps
P. Uranga, A.I. Fernández, B. López and J.M. Rodriguez-Ibabe
CEIT and tecnun (University of Navarra)Donostia-San SebastiánBasque Country, Spain
Grain Size Distribution in an Industrial Thin Slab
0
5
10
15
20
25
30
0 500 1000 1500 2000 2500 3000
Grain Size (μm)
Freq
uenc
y (%
)
CenterNear Surface Mixed
Columnar-Equiaxed Structure
Dγ > 2000 μm → Volume Fraction > 20%